scientific program - 13isssb.unideb.hu13isssb.unideb.hu/images/final program.pdfchiral hplc...

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1 Scientific program MONDAY 01.07.2013 19.00 - 22.00 Registration and Welcome TUESDAY 02.07.2013 9.00 9.30 Opening UNIDEB Pro-rector, CEEPUS network coordinator, Symposium chair SESSION 1 Chairman: Attila Gáspár (University of Debrecen) 9.30 - 9.50 L1 15 years with CEEPUS Ferenc Kilár, University of Pécs 9.50 10.20 L2 Some Theoretical and Practical Aspects of Microchip Electrophoresis in Bioanalysis Marián Masár, Comenius University in Bratislava 10.20 10.40 L3 System Peak Behavior in Complexing Background Electrolytes Martina Riesová, Charles University in Prague 10.40 11.00 CB-1 Coffee Break SESSION 2 Chairwoman: Tamara Paypanova (University of Blagoevgrad) 11.00 11.30 L4 Why the Enantioseparation is a "Must"? Radu Oprean, Iuliu Hatieganu University of Medicine & Pharmacy 11.30 11.50 L5 Chiral HPLC Separations of Unusual Amino Acids in Reversed Phase and Polar-Organic Modes Květa Kalíková, Jiří Vozka, Eva Tesarova, Charles University in Prague 11.50 12.10 L6 Application Possibilities of Capillary Electrophoresis on a Chip in Separations of Selected Amino Acids and their Enantiomers in Body Fluids Katarina Uhlarova, Comenius University in Bratislava 12.10 12.30 L7 Properties of Dual-cyclodextrin Separation Systems: Experimental Verification of Proposed Model Ludmila Müllerová, Charles University in Prague 12.30 13.30 LB-01 Lunch

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Page 1: Scientific program - 13isssb.unideb.hu13isssb.unideb.hu/images/final program.pdfChiral HPLC Separations of Unusual Amino Acids in Reversed Phase and Polar-Organic Modes Květa Kalíková,

1

Scientific program

MONDAY 01.07.2013

19.00 - 22.00 Registration and Welcome

TUESDAY 02.07.2013

9.00 – 9.30 Opening

UNIDEB Pro-rector,

CEEPUS network coordinator,

Symposium chair

SESSION 1

Chairman: Attila Gáspár (University of Debrecen)

9.30 - 9.50 L1 15 years with CEEPUS

Ferenc Kilár, University of Pécs

9.50 – 10.20 L2

Some Theoretical and Practical Aspects of Microchip Electrophoresis in

Bioanalysis

Marián Masár, Comenius University in Bratislava

10.20 – 10.40 L3 System Peak Behavior in Complexing Background Electrolytes

Martina Riesová, Charles University in Prague

10.40 – 11.00 CB-1 Coffee Break

SESSION 2 Chairwoman: Tamara Paypanova (University of Blagoevgrad)

11.00 – 11.30 L4 Why the Enantioseparation is a "Must"?

Radu Oprean, Iuliu Hatieganu University of Medicine & Pharmacy

11.30 – 11.50 L5

Chiral HPLC Separations of Unusual Amino Acids in Reversed Phase and

Polar-Organic Modes

Květa Kalíková, Jiří Vozka, Eva Tesarova, Charles University in Prague

11.50 – 12.10 L6

Application Possibilities of Capillary Electrophoresis on a Chip in Separations

of Selected Amino Acids and their Enantiomers in Body Fluids

Katarina Uhlarova, Comenius University in Bratislava

12.10 – 12.30 L7

Properties of Dual-cyclodextrin Separation Systems: Experimental

Verification of Proposed Model

Ludmila Müllerová, Charles University in Prague

12.30 – 13.30 LB-01 Lunch

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SESSION 3 Chairman: Marian Masar (Comenius University in Bratislava)

14.00 – 14.30 L8

Identification of Genetically Modified Foods using Protein Profiling with CE

Chips

Ewa Pobozy, University of Warsaw

14.30 – 14.50 L9

Comparison of Real-Time PCR Assays with Commercial ELISA Kits for the

Detection of Potentially Allergenic Mustard

Monika Palle-Reisch, University of Vienna

14.50 – 15.10 L10

Exploring the Interactions of Novel RGD Analogues with Integrin by Docking

Studies

Tatyana Dzimbova, University of Blagoevgrad

15.10 – 15.30 L11

Methylation Status of Interleukin-1 Receptor type 2 as a Promising Biomarker

for Juvenile Idiopathic Arthritis?

Melanie Spitzwieser, University of Vienna

15.30 – 15.50 L12

The Rapid and Orthogonal Assessment of Chiral Recognition in case of

Molecularly Imprinted Polymers Developed for Different Β-Blockers by

Electromigration Separation and Electrochemical Techniques

Bogdan-Cezar Iacob, Iuliu Hatieganu University of Medicine & Pharmacy

WEDNESDAY 03.07.2013

SESSION 4

Chairman: Radu Oprean (Iuliu Hatieganu University of Medicine and Pharmacy)

9.00 – 9.30 L13 Multiple Food Allergen Analysis

Margit Cichna-Markl, University of Vienna

9.30 – 9.50 L14 Simple Method for Determination of Drugs in Binary Systems

Gabriella Donath-Nagy, University of Medicine and Pharmacy Targu Mures

9.50 – 10.10 L15

ESI MS/MS Investigations of Aroylhydrazones Derived from Nicotinic Acid

Hydrazide

Nives Galic, University of Zagreb

10.10 – 10.30 L16

Development and Validation of a Real-Time PCR Method for the Identification

and Quantification of ROE DEER (CAPREOLUS CAPREOLUS) to Detect

Food Adulteration

Barbara Druml, University of Vienna

10.30 – 11.00 CB-2 Coffee Break

Page 3: Scientific program - 13isssb.unideb.hu13isssb.unideb.hu/images/final program.pdfChiral HPLC Separations of Unusual Amino Acids in Reversed Phase and Polar-Organic Modes Květa Kalíková,

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POSTER LECTURES I.

Chairwoman: Gabriella Donáth-Nagy (University of Medicine and Pharmacy Targu-Mures)

11.00 – 12.30 Posters 1-14.

12.30 – 13.30 LB-02 Lunch

POSTER LECTURES II.

Chairwoman: Nives Galic (University of Zagreb)

16.00 – 18.00 Posters 15-

18.00 – 18.30 DB-01 Dinner

THURSDAY 04.07.2013

SESSION 5 Chairwoman: Eva Tesarova (Charles University in Prague)

9.00 – 9.30 L17 Some Reflections on Lipidomics

Ernst Lankmayr, University of Technology Graz

9.30 – 10.00 L18

Assessment of the Genotoxic Potential of Novel RGD-mimetics using Comet

Assay

Tamara Pajpanova, University of Blagoevgrad

10.00 – 10.20 L19 Lipopolysaccharidomics

Ferenc Kilár, University of Pécs

10.20 – 10.40 L20 Antioxidant Properties of Food Samples

Anna Pekal, University of Warsaw

10.40 – 11.00 CB-3 Coffee Break

Page 4: Scientific program - 13isssb.unideb.hu13isssb.unideb.hu/images/final program.pdfChiral HPLC Separations of Unusual Amino Acids in Reversed Phase and Polar-Organic Modes Květa Kalíková,

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SESSION 6 Chairwoman: Margit Cichna-Markl (University of Vienna)

11.00 – 11.30 L21

Analysis of Illicit Drugs Using Chromatographic and Electrophoretic

Techniques

Martin Schmid, Karl-Franzens-University

11.30 – 11.50 L22

Complexation with Buffer Constituents: Impact on Determination of Stability

Constants

Martin Beneš, Charles University in Prague

11.50 – 12.10 L23 Calixarene Based Stationary Phases for Warfarin Enantiomer Separation

Ioana Daria Tiuca, Iuliu Hatieganu University of Medicine & Pharmacy

12.10 – 12.30 L24

Chiral Separation of some H1-antihistamines using Nonaqueous Capillary

Electrophoresis

Zoltán-István Szabó, University of Medicine and Pharmacy Targu Mures

12.30 – 13.30 LB-03 Lunch

SESSION 7 Chairman: Martin Schmid (Karl-Franzens-University)

16.00 – 16.30 L25

Combination of Separation Techniques with Mass Spectrometry used in the

Analyses of Different Biological Samples

Jozef Marák, Comenius University in Bratislava

16.30 – 17.00 L26 LC Analysis of Drugs of Abuse from Biological Matrices

Béla Kiss, Iuliu Hatieganu University of Medicine & Pharmacy

17.00 – 17.20 L27

LC-MS/MS Method Development for the Determination of Triazines and

Triazoles Migrating from Food Packaging Materials

Zsolt Bodai, Eötvös Loránd University

17.20 – 17.40 L28

Determination of Valsartan from Human Plasma by a Rapid LC-MS Method

Szende Vancea, University of Medicine and Pharmacy Targu Mures

18.00 – 18.30 DB-02 Dinner

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FRIDAY 05.07.2013

SESSION 8

Chairman: Ernst Lankmayr (University of Technology, Graz)

9.00 – 9.30 L29 Investigations on Biodiesel Fabrication through Enzyme Catalysis

Florin Dan Irimie, Babes-Bolyai University

9.30 – 9.50 L30 Green Analytical Chemistry

Gábor Dibó, Eötvös Loránd University

9.50 – 10.10 L31 Analysis of Lake Sediments

Mihály Braun, University of Debrecen

10.10 – 10.30 L32

Determination of Biliverdin and Protoporhyrin from Avian Eggshells by High

Performance Liquid Chromatography

Zsuzsanna Eke, Eötvös Loránd University

10.30 – 11.00 CB-4 Coffee Break

SESSION 9 Chairman: Marek Trojanowicz (University of Warsaw)

11.00 – 11.30 L33

Inductively Coupled Plasma - Mass Spectrometry (ICP-MS) and Inductively

Coupled Plasma – Optical Emission Spectrometry (IP-OES) Analysis of

Elements in Macedonian Wines

Violeta Ivanova-Petropulos, University "Goce Delčev"-Štip

11.30 – 12.00 L34 Applications of Electrochemistry coupled to Mass Spectrometry

Ede Bodoki, Iuliu Hatieganu University of Medicine & Pharmacy

12.00 – 12.20 L35 Various Types of PAL in the Biotransformation of Unnatural Amino Acids

Csaba Paizs, Babes-Bolyai University

12.30 – 13.30 LB-04 Lunch

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SATURDAY 06.07.2013

SESSION 10

Chairman: Ferenc Kilár (University of Pécs)

10.00 – 10.30 L36

Application of HPLC for the Monitoring of Yield and Products of

Decomposition of Organic Pollutants in Waters Using Ionizing Radiation for

Environmental Protection

Marek Trojanowicz, University of Warsaw

10.30 – 11.00 L37 From Aerogels to Artificial Bone Substitution

István Lázár, University of Debrecen

11.00 – 11.20 L38 Development of Microchips with Multichannel Systems

Andrea Nagy, University of Debrecen

11.30 – 12.00 Closure/Poster Prize

12.30 – 13.30 LB-05 Lunch

SUNDAY 07.07.2013 9.00 – 12.00 Departure

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POSTER PRESENTATIONS

P1

Elemental Analysis of Human Blood Serum of Patients with Autoimmune Disease using

Microwave Plazma AES

E. Baranyai*, Cs. N. Tóth, M. Braun, T. Tarr, I. Csípő, M. Zeher, J. Posta

University of Debrecen

P2

Synthesis and Characterization of Metal Ion Specific Aerogels

H. F. Bereczki*, M. Braun, I. Lázár

University of Debrecen

P3

Ag/TiO2 Based on Nanomaterials used in Food Preservation

C. O. Cadar*, A. Mihaly-Cozmuta, A. Peter, C. Nicula, L. Mihaly-Cozmuta, M. Metenti

Technical University of Cluj-Napoca

P4

Elaboration of Optimal Technology and Pharmaceutical Availability Study of Combined

Oinments with Izohydrafural and Methyluracil

E. Donici*, I. Donici, L. Uncu

State University of Medicine and Pharmacy "Nicolae Testemitanu" Chisinau

P5

Chemical Stability and Pharmacological Evaluation of Novel Endomorphin-2 Analogs

K. Georgiev*, L. Georgiev, T. Pajpanova

Medical University of Varna

P6

Enantioseparation of Profens on Immobilized Polysaccharide-based Columns in Reverse Phase

Separation Systems

R. Geryk*, D. Plecitá, K. Kalíková,, E. Tesařová

Charles University in Prague

P7

Determination of Phenylethanoid Glycosides and Iridoid Glycosides from Therapeutically

Used Plantago Species by CE-MEKC

S. Gonda*, N. M. Nguyen, G. Vasas

University of Debrecen

P8

Systematic Screening Approach for Chiral Separation of Beta-blockers by Capillary

Electrophoresis using Cyclodextrines as Chiral Selectors

G. Hancu*, A. Cârje, A. Rusu, Z. I. Szabó

University of Medicine and Pharmacy Targu Mures

P9

Comparison of the DNA-Methylation Status of Tumor, Adjacent and Surrounding Normal

Tissue of Breast Cancer Patients

E. Holzweber*, A. Raab, M. Spitzwieser, V. Fackler, N. Bayer, G. M. Cichna-Markl

University of Vienna

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P10

Sediment Analysis using ICP-AES

K. Hubay*, M. Braun

University of Debrecen

P11

The use of Capillary Electrophoresis Methods for the Analysis of Selected Acids in Human

Urine

M. Joanidisová*, R. Bodor, M. Masár

Comenius University in Bratislava

P12

Application of Immunotests in Identification of Genetically Modified Foods

K. Jastrzebska*, E. Poboży, A. Koc, M. Trojanowicz

University of Warsaw

P13

Immobilization of Trypsin on PDMS for On-line Digestion of Proteins

Á. Kecskeméti*, A. Gáspár

University of Debrecen

P14

Investigation of Active Site Structure and Mechanism of a β(1,6)-N-acetyl-glucosaminidase

Enzyme

G.Lehoczki*, E. Fazekas, Gy. Gyémánt

University of Debrecen

P15

Expression and Purification of Various Types of PAL and PAM

A. Mantu*, A. Varga, M. Tosa, F. D. Irimie, Cs. Paizs

Babes-Bolyai University

P16

Unnatural Amino Acids Stereoselective Enzymatic Synthesis

M. E. Moisă*, Cs. Paizs, F. D. Irimie, M. I. Toşa

Babes-Bolyai University

P17

CaL-A Mediated Kinetic Resolution of Racemic 2-hydroxy-2-(5-phenylthiophen-3-

yl)acetonitrile and its Derivatives

M. A. Naghi*, J. H. Vari, M. I. Tosa, Cs. Paizs, F. D. Irimie

Babes-Bolyai University

P18

Alternative Approaches for the Enantioselective Synthesis of (S) and (R)-bufuralol

B. Nagy*, N. Dima, M. I. Tosa, Cs. Paizs, F. D. Irimie

Babes-Bolyai University

P19

Application of Quantum Dots as Fluorophores in Flow Analysis

Z. Oleksiak*, E. Poboży, J. L. M. Santos, S. Rodrigues, V. Abreu, M. Trojanowicz

University of Warsaw

P20

Application of CE Chips for Determination of Proteins in Urine

N. Pacocha*, E. Poboży, M. Filaber, M. Trojanowicz

University of Warsaw

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P21

Antioxidant Activity and Contents of Anthocyanins from Different Berry Extracts

P. V. Podea*, A. Keresztes, A. Dunca, F. D. Irimie

Babes-Bolyai University

P22

Analysis of Humic Acids by Off-line Combination of Capillary Isotachophoresis and HPLC

Z. Radičová*, R. Bodor, R. Góra, M. Hutta, M. Masár

Comenius University in Bratislava

P23

Determination of N-acetylcysteine in Mucolytics by Electrophoresis on a Chip

M.Rudašová*, R. Bodor, M. Masár

Comenius University in Bratislava

P24

The Study of Peptide Digestion by Trypsin under RP HPLC Conditions

T. Šlechtová*, K. Kalíková, M. Gilar, E. Tesařová

Charles University in Prague

P25

Analysis of Tryptamines by GC-MS and Development of New Separation Methods using HPLC

and CE

M. Taschwer*, E. Ebner , S. Koch , M. G. Schmid

Karl-Franzens-University

P26

Phytoremediation Analysis for Removal of Crystal Violet Dyes using Aquatic Plant, Lenna

minor

A.Török*, C. Indolean, E. Buta, L. Silaghi-Dumitrescu, C. Majdik

Babes-Bolyai University

P27

Determination of Erythrosin and Parabens in Pharmaceuticals by Microchip and Capillary

Electrophoresis

P. Troška*, M. Masár, E. Poboży, R. Bodor

Comenius University in Bratislava

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POSTERS

P28

Determination of Temozolomide in Serum and Brain Tumor with Micellar Electrokinetic

Capillary Chromatography

M. Andrási*, B. Törzsök, Á. Klekner, A. Gáspár

University of Debrecen

P29

High Resolution Melting Analysis of Cell Free DNA from Serum Samples of Breast Cancer

Patients

N. Bayer*, M. Spitzwieser, E. Holzweber, A. Raab, G. Pfeiler, M. Cichna-Markl

University of Vienna

P30

Spectrophotometric Determination of Protonation Constants of Aroylhydrazones Derived from

Nicotinic Acid Hydrazide

T. Benković*, V. Tomišić, N. Galić

University of Zagreb

P31

Analysis of Proteins using Electrophoretic Focusing Techniques in Combination with Mass

Spectrometric Detection

N. Biherczová*, J. Marák, F. Kilár, Cs. Páger, V. Sándor

Comenius University in Bratislava

P32

Evaluation of the Ingestion of Parabens When Using Dental Care Products by Healthy Human

Volunteers

M. D. Croitoru*, M. M. Coman, I. Fülöp

University of Medicine and Pharmacy Targu Mures

P33

Detection Methods for On-chip Measurements

B. Csóka*, F. Kilár

University of Pécs

P34

New Methode for Activity Measurement of Glycogen Phosphorilase b

E. Fazekas*, G. Kis, K. Szabó, Gy. Gyémánt

University of Debrecen

P35

Designing and Fabrication of Microchips with Multicapillary Systems

A. Gáspár, A. Nagy*

University of Debrecen

P36

Hydrolytic Determination of Some Peptide Analogues by HPLC

L. Georgiev*, T. Dzimbova, T. Pajpanova

Institute of Molecular Biology Roumen Tsanev - Bulgarian Academy of Sciences

P37

Contribution of Filamentous Fungi from Plantago lanceolata L. leaves to the Pattern and

Stability of Bioactive Metabolites: a CE-MEKC and GC-MS Study

Zs. Szűcs, A. Kiss, T. Emri, G. Vasas, S. Gonda*

University of Debrecen

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P38

Two Dimensional Liquid Chromatography of Biomacromolecules Isolated from Environmental

Sources

R. Góra

Comenius University in Bratislava

P39

Synthesis and Study of New Simulated Body Fluids for In Vivo Testing of Artificial Bone

Substitutes

E. Győri*, I. Lázár

University of Debrecen

P40

Rapid Digestion of Sediments and Rock Samples

S. Harangi*, K. Hubay, M. Braun

University of Debrecen

P41

Ultrafast Haplotyping of Putative MicroRNA-binding Sites in the WFS1 Gene by Capillary Gel

Electrophoresis

M. Kerékgyártó*, N. Németh, T. Kerekes, Zs. Rónai, A. Guttman

University of Debrecen

P42

Application of Split-flow Injection in Microchips

P. I. Koczka*, A. Gáspár

University of Debrecen

P43

Analysis of Nucleic Acids using Electrophoretic Techniques

M. Kondeková*, J. Marák, M. Fraňo, M. Koiš

Comenius University in Bratislava

P44

Using of LC-DAD-MS Techniques for Analysis of Phenolic Compounds in Selected Tea

Samples

K. Krčová*, J. Marák

Comenius University in Bratislava

P45

Electroanalytical Sudy of Cyclodextrins Interactions with Some Pharmaceutical Compounds

L. Fritea*, M. Tertiş, T. L. Topală, R. Săndulescu

Iuliu Hatieganu University of Medicine & Pharmacy

P46

Zone Electrophoresis on Microchip

L. Makszin*, Á. Blaskó, T. Kiss, V. U. Weiss, F. Kilár

University of Pécs

P47

Biosorption of Cd(II) with Chemically Modified Fir Tree Sawdust

C. Manzatu*, B. Nagy, C. Indolean, D.L. Silaghi, C. Majdik

Babes-Bolyai University

P48

Study of Drug Metabolism using EC-LC-MS Technique

M. Radičová*, J. Marák, A. Staňová, R. Bodor

Comenius University in Bratislava

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P49

Synthesis and Adsorption Properties of Collagen-Silica Aerogel Hybrids

P. Veres*, I. Lázár

University of Debrecen

P50

Analysis of Selected Group of Profens by RP-HPLC

V. Vojtková*, M. Chalányová, I. Petránová, M. Hutta

Comenius University in Bratislava