site 3 - head of the lagoon - united states environmental ... applied sciences laboratory client...
TRANSCRIPT
Cor vail is Applied
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Sciences Laboratory
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Analyte
Arsenic, ICPCadmium, ICPChromium, ICPCopper, ICPLead, ICPMercury, Cold VaporNickel, ICPZinc, ICP
•A Recti.:- "•'•':'.• •,:-.:,:-,,,„.:.;„;«
Instrument ReportingLimit Limit
3.0 100.20 50.25 102.0 250.80 31.0 1.80.80 400.50 20
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liilliltlliS II ifeK:: ' &«'S@[iS!:llli!| SI68 K i|Spi>ii: Si|iSl i1 !JiiC:u!iilli!|;illiSllll 111 1
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Sample DateResult Qualifier Units Method Analyzed
86.5 pg/L EPA200.7 2/14/950.20 U ug/L EPA200.7 2/14/953.2 B ug/L EPA200.7 2/14/952.0 U ug/L EPA200.7 2/14/951.6 B ug/L EPA200.7 2/14/951.0 U pg/L EPA245.1 12/16/948.5 B pg/L EPA200.7 2/14/9540.5 pg/L EPA200.7 2/14/95
U=Not detected at specified instrument limitsB=Not detected at specified reporting limits
fti303323
Corvallis Applied Sciences Laboratory
Client Information !Project Name: Halby Chemical
Project Manager: Jerry Bllls/GLOSampled By: Illegible :
Client Sample ID: 3ZEOLITESampling Date: 1 1/1 9/94 ; /Sampling Time: Not given
Type: GrabMatrix: WaterBaas: As Rec'd.
Instrument ReportingAnalvte Limit Limit
Arsenic, ICP 3.0 10Cadmium, ICP 0.20 5Chromium, ICP 0.25 10Copper, ICP 2.0 25Lead, ICP 0.80 3Mercury, Cold Vapor 1 .0 1 .8Nickel, ICP 0.80 40Zinc, ICP 0.50 20
U=Not detected at specified instrument limitsB=Not detected at specified reportinq limits
Lab InformationDate Rec'd: 12/1 3/94
:::;:,: Lab ID: 796318Report Revision No.: 0
Reported By: R. McMorrisReviewed By: t £}~&6 —
Sample DateResult Qualifier Units Method Analyzed
125 ug/L EPA200.7 2/14/950.34 B ug/L EPA200.7 2/14/954.9 B ug/L. EPA200.7 2/14/952.0 U ug/L. EPA200.7 2/14/952.4 B |jg/L EPA200.7 2/14/951.0 U ug/L EPA245.1 12/16/941.0 B ug/L EPA200.7 2/14/95192 ug/L EPA200.7 2/14/95
Corvallis Applied Sciences Laboratory
Client Information
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' • • •••••.- . . o3SI*
Analyte
Arsenic, ICPCadmium, ICPChromium, ICPCopper, ICPLead, ICPMercury, Cold VaporNickel, ICPZinc, ICP
U=Not detected at specifiedB=Not detected at specified
.r'As 'Rec*d :' ''"" ' '•'.' :;:'::™8:Si:?;;F :: :':'3t'::5 ';*
Instrument ReportingLimit Limit
3.0 100.20 50.25 102.0 250.80 31.0 1.80.80 400.50 20
instrument limitsreporting limits
WIlillllE ^ ^
'*•'• -ySiM! S!at»Liab'SfD' Ji iSSI 9': • • -« :- t: -'- .:':' • : '-" ':"' "-- -'- l' J'::j::::|i|i;:!i|ie||!l:ilfa:s;|||!!i!i|!» • •;'•.••:-_- Sf Jr /H i? . ••'•;. -:; • ••••":1::'':* S II'H6jS:irtTOiByji'R«?McM6 ns\i"i." ,:',;: :;'.:..;;».,; ...-..-.. .'..-.^ ^ ^ ^ ^ • ^ ^ ^ ••;' •' " : '
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Sample DateResult Qualifier Units Method Analyzed
131 ug/l. EPA200.7 2/14/950.61 B ug/L EPA200.7 2/14/956.4 B ug/L EPA200.7 2/14/952.0 U ug/L EPA200.7 2/14/952.6 B ug/L EPA200.7 2/14/951.0 B ug/L EPA245.1 12/16/942.1 B ug/L EPA200.7 2/14/95140 ug/L EPA200.7 2/14 5
ft'R 3 033 2 5
Corvallis Applied Sciences Laboratory
Client InformationProject Name: Halby Chemical
Project Manager: Jerry Bills/GLOSampled By: Illegible
Client Sample ID: 3CATIONSampling Date: 11/28/94Sampling Time: Not given
Type: GrabMatrix: WaterBasis: As Recy.
Instrument ReportingAnalyte Limit Limit
Arsenic, ICP 3.0 10Cadmium, ICP 0.20 5Chromium, ICP 0.25 10Copper, ICP 2.0 25Lead, ICP 0.80 3Mercury, Cold Vapor 1 .0 ' 1 .8Nickel, ICP 0.80 40Zinc, ICP 0.50 20
U=Not detected at specified instalment limitsB=Not detected at specified reporting limits
Lab InformationDate Rec'd: 12/1 3/94
Lab ID: 796320Report Revision No.: 0
Reported By: R. McMorrisReviewed By: u A-itf""""
Sample DateResult Qualifier Units Method Analyzed
222 M9/L EPA200.7 2/14/950.83 B ug/L EPA200.7 2/14/959.0 B pg/L EPA200.7 2/14/9510.9 B ug/L EPA200.7 2/14/955.3 pg/L EPA200.7 2/14/951.0 B Mg/L EPA245.1 12/16/941.8 B (jg/L EPA200.7 2/14/95549 ug/L EPA200.7 2/14/95
AR303326
Corvallis Applied Sciences Laboratory
Client • Information • •' '• \ : "'" ? - siff SK ••* '• i sst&f'-K- f:SKiS£::''-;Steiii 'Information "''~' * ' ''-"•'•' '' ' ' '-":?'' "K XS& i '£. -" • 'SS!S':s
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; : i- Sampling time:' • •-• ... . . l /iiType:
,; : : •••'- ; Matrix:' ' • "::• • "•• -- -K:;.'-Basis:
Analyte
"3CATZEO, .'•'...', / - •- • '""..-.".. '• 'R orted By R/'MdMo'rns \ , ,-'.C.;:Q6'.','!.''...''- ~-»*
\ A i«* l ' -!'v'1;;i:'!" , ' V:'?-' '.' • ":" ' "" : " '••. ' -:'i.v -:;-"- -yC! i;i;i '"Ui;;ii!;i:ii-;!El' : :; :ii;l- iiii i :ili ;ii;: ^ ?<+:Water:_, , • -.,.;::- • •.. ..,..;.-,,..:... ^ liilllliSSiPtS sglllliSiiilS ^ ^ ^ #'«(','
Instrument Reporting Sample DateLimit Limit Result Qualifier Units Method Analyzed
Arsenic, ICP 3.0 10 157 ug/L EPA200.7 2/14/95Cadmium, ICP 0.20 5 0.43 B ug/L EPA200.7 2/14/95Chromium, ICP 0.25 10 5.6 B ug/L EPA200.7 2/14/95Copper, ICP 2.0 . 25 2.0 U ug/L EPA200.7 2/14/95Lead, ICP 0.80 3 3.3 ug/L EPA200.7 2/14/95Mercury, Cold Vapor 1.0 1.8 1.0 U ug/L EPA245.1 12/16/94Nickel, ICP 0.80 40 2.0 B ug/L EPA200.7 2/14/95Zinc, ICP 0.50 20 82.9 ug/L EPA200.7 2/14/95
U=Not detected at specified instrument limitsB=Not detected at specified reporting limits
AR303327
Corvallis Applied Sciences Laboratory
Client Information Lab InformationProject Name: Halby Chemical Date Rec'd:
Project Manager; Jerry Bills/QLO Lab ID:Sampled By: Illegible Report Revision No.:
Client Sample ID: 3AIRZEO Reported By:Sampling Date: 11/28/94 Reviewed By:Sampling Time: Not given
Type: GrabMatrix: WaterBasis: As Rec'd.
Instrument Reporting SampleAnalyte Limit Limit Result Qualifier
Arsenic, ICP 3.0 10 132Cadmium, ICP 0.20 5 0.20 UChromium, ICP 0.25 10 2.9 BCopper, ICP 2.0 25 2.0 ULead, ICP 0.80 3 0.82 BMercury, Cold Vapor 1.0 1.8 1.0 UNickel, ICP 0.80 40 0.82 BZinc, ICP 0.50 20 50.8
U=Not detected at specified instrument limitsB=Not detected at specified reporting limits
12/13/9479.6321'..,."......0R. McMorrisU»V5 r"
DateUnits Method Analyzed
ug/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95pg/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95ug/L EPA245.1 12/16/94ug/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95
AH303328
Corvallis Applied Sciences Laboratory
Client InformationF
Pro! ! •':.'•:rt5• ™•"'•''•''"'•/'v:--!;'; I ah' in-"7.Qfi393:•-..,,<~«:«b«s-..«».:.*:-s.•..;!.-,»;v"i :•>,-',:,,.•.:',:«n»-,^ ^ gj l g ^ B fi aa
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Instrument Reporting Sample DateAnalyte____________Limit____Limit___Result Qualifier___Units____Method Analyzed
Arsenic, ICP 3.0 10 167 M9/L EPA200.7 2/14/95Cadmium, ICP 0.20 5 0.20 U M9/L EPA200.7 2/14/95Chromium, ICP 0.25 10 6.0 B ug/L EPA200.7 2/14/95Copper, ICP 2.0 25 3.5 B ug/L EPA200.7 2/14/95Lead, ICP 0.80 3 1.5 B ug/L EPA200.7 2/14/95Mercury, Cold Vapor 1.0 1.8 1.0 U ug/L EPA245.1 12/16/94Nickel, ICP 0.80 40 2.4 B ug/L EPA200.7 2/14/95Zinc, ICP 0.50 20 370 ug/L EPA200.7 2/14/95
U=Not detected at specified instrument limitsB=Not detected at specified reporting limits
At303329
Corvallis Applied Sciences Laboratory
Client Information i•:;:.;. -,. :::>;;;::P,rect'-Name:• .:.:,:,„ -.:::, . '• pfffyoft, Manager?;?;' S%?!e?i?
":? - :i'5;:;< Sampling Date:: • Sampling Time:
-•-- •- -...•;.•.'. :I :: -Type:'" ': ''•" '.' 'i' 'vf1/':- Matrix:. . . -•i:.:/::.;:.;.:.:::..- ;-.•• :".: V-••:u- .,...• ;:- •-••- , .:::.:•;,«„:•, .'.--Basis:
Analyte
Arsenic, ICPCadmium, ICPChromium, ICPCopper, ICPLead, ICPMercury, Cold VaporNickel, ICPZinc, ICP
Jerry BillL6:':|:Siliil•!•."* ... •- •j----i':iil:-: t1- :-'-:.:-----!:' "-'-Illegible -; • ..';f;;vSi33|@
ll/lf;:'.;;;:^!!
Not given .' • ••.'• .SKtisiiijS
Water . '. '.'.:.$!:?%$AsRec'd. \V,:-.:: «:!f::;":i?:;
Instrument ReportingLimit Limit
3.0 100.20 50.25 102.0 . 250.80 31.0 1.80.80 400.50 20
SSSHi Bi ^ !?? M MSKI
SampleResult Qualifier
3.0 U0.20 U0.25 U2.0 U2.5 B1.0 U0.80 U12.6 B
DateUnits Method Analyzed
ug/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95ug/L EPA245.1 12/16/94Mg/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95
U=Not detected at specified instrument limitsB=Not detected at specified reporting limits
A130333I
Corvallis Applied Sciences Laboratory
CHent InformationProject Name: Halby Chemical
Project Manager: Jerry Bills/GLO 'Sampled By: Illegible
Client Sample ID: ZEOBLANKSampling Date: 11/19/94Sampling Time: Not given
Type: GrabMatrix: WaterBasis: As Rec'd.
Instrument ReportingAnalyte Limit Limit
Arsenic, ICP 3.0 10Cadmium, ICP 0.20 5Chromium, ICP 0.25 10Copper, ICP 2.0 25Lead, ICP 0.80 3Mercury, Cold Vapor 1 .0 1 .8Nickel, ICP 0.80 40Zinc, ICP 0.50 20
U=Not detected at specified instrument limitsB=Not detected at specified reporting limits
Lab InformationDate Rec'd: 12/1 3/94
LabID:Report Revision No.:
Reported By:Reviewed By:
SampleResult Qualifier
3.0 U0.20 U0.25 U2.0 U2.1 B1.0 U0.80 U27.2
7963090R. McMorrist,w*<r"
DateUnits Method Analyzed
ug/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95Hg/L EPA200.7 2/14/95ug/L EPA245.1 12/16/94ug/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95
AR303332
ICorvallis Applied Sciences Laboratory
Client Information' ' : :'• aillil;
Project iManager:
:!.:;; J:;nfliifej
: Matrix:•: ••• • '•' Basis:
Analyte
iSSiiiiillliC " " ' ' .'"' ':'; •--".-. •-:••:• #:;: ;;.:;?-;'"::!3;Si5:iii. ffi'SjiS
frlBiiio;1!*!1!!!;!!!!!!^^
W3ISr ' , . , • ';. •' ' • •'••'••'; ', " '-'-' '-hhiiiriliil ii''^^ ''';';--;.:''' :•!•', 'JU't;!'':''!:!:. "• • ' - :•' V; • • ': ' " ,;:;i;::i::1P;:H'!!!'''-!i;iiti::!::;:H'B'^!':-;':.-rl;:;-::!-:-:".. •'•'•• -. |:>;V •.•••v'ij'h'iijsiiiVji-i!:*&i&''';--W? ^ ' ' : :5i - •- . f. .rffl
Instrument Reporting Sample DateLimit Limit Result Qualifier Units Method Analyzed
Arsenic, ICP 3.0 10 3.0 U ug/L EPA200.7 2/14/95Cadmium, ICP 0.20 5 0.20 U ug/L EPA200.7 2/14/95Chromium, ICP 0.25 10 0.25 U \ig/L EPA200.7 2/14/95Copper, ICP 2.0 25 2.0 U ug/L EPA200.7 2/14/95Lead, ICP 0.80 3 2.8 B ug/L EPA200.7 2/14/95Mercury, Cold Vapor 1.0 1.8 1.0 U ug/L EPA245.1 12/16/94Nickel, ICP 0.80 40 1.4 B ug/L EPA200.7 2/14/95Zinc, ICP 0.50 20 13.0 B ug/L EPA200.7 2/14/95
U=Not detected at specified instrument limitsB=Not detected at specified reporting limits
AR303333
Corvallis Applied Sciences Laboratory
Client Information :-:: ,v,Project Name: Halby Chemical
Project Manager: Jerry Bills/GLOSampled By: Illegible
Client Sample ID: ZEOAIRBLKSampling Date: 11/19/94Sampling Time: Not given
Type: GrabMatrix: WaterBasis: As Rec'd.
Instrument ReportingAnalyte Limit Limit
Arsenic, ICP 3.0 10Cadmium, ICP 0.20 5Chromium, ICP 0.25 10Copper, ICP 2.0 25Lead, ICP 0.80 3Mercury, Cold Vapor 1 .0 1 .8Nickel, ICP 0.80 40Zinc, ICP 0.50 20
U=Not detected at specified instrument limitsB=Not detected at specified reporting limits
Lab Information: Date Rec'd: 12/1 3/94
• :- ;:-:-., .• "-•;;:V .-|JabfD:--796312Report Revision No.: 0
,. . :......:. Reported By: R. McMorris: ; -Reviewed By: i, ft- C"
Sample DateResult Qualifier Units Method Analyzed
3.0 U ug/L EPA200.7 2/14/950.20 U ug/L EPA200.7 2/14/950.31 B ug/L EPA200.7 2/14/9516.5 B ug/L EPA200.7 2/14/956.1 ug/L EPA200.7 2/14/951.0 U ug/L EPA245.1 12/16/941.6 B ug/L EPA200.7 2/14/9530.8 ug/L EPA200.7 2/1 4/95
AR3Q3331*
Corvallis Applied Sciences Laboratory
Client Inforrnatibn 'v':-W:;£-'.v- ;V:.::r:\;::i5:elpp
.-.•.,'.. .,::/:i:r;*|Sampling 'iTiirpe:. , • ••• KSssssssyM'f'S p -
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Analyte
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' S:i:iVVStSr 'ii;'.Vr -' '''•'' 'T'::'-i -\'1--'-;';-i•' 1••• F:::ii!H%:• r•••:- >: ;i:;i ii1n•;.i• •=:=.-.•.••• '.- - -. ••:'•-.••:-.:.• ."• .. ;••.-*':'•.-.; >.i;;.=;: :"-: ;;;-.=! l:".::-r;-.ri:":; ;;;;!'V=T:":':' '-:"-'": ; ": ••'"'''••' •" '.',' '.' "' •!:'.|!'i;.!:!::!!:,:;:: 'i":::.!'::-'1- ;: ="; : ';.'!.;..':-.;Y !;'•' :!'-i;::::!/!i)'-l-l!!.;'-'!:;!:E:r;;:1! !;,"•:;:." •':;'. '.' .':-' :.: ''. i1:" • ' :-H 'C;'-> .' " ' • - -- ••-'*. 3*'AS RSCxi"1""1-' ' '" *.i"":'"i '•'•","• "'' '" ' •• '• • .:"----:"".v:-!1r-:::.!-!-"-:r!!f;i:-1. •••-•'• !-i:i::-,!-i;!-::!;!-i"..!- :•":•:'! !:i!;:|!ji):::"i::i;-;VViv:!:I:i!ifi;':i!1.'i:-V:i%'" . . ' ' ' " • -:::i::; i':3/l-: iV-!" v:"-:v!!:
Instrument Reporting Sample DateLimit Limit Result Qualifier Units Method Analyzed
Arsenic, ICP 3.0 10 3.0 U ug/L EPA200.7 2/14/95Cadmium, ICP 0.20 5 0.20 U ug/L EPA200.7 2/14/95Chromium, ICP 0.25 10 0.53 B ug/L EPA200.7 2/14/95Copper, ICP 2.0 25 2.0 U ug/L EPA200.7 2/14/95Lead, ICP 0.80 3 1.4 B ug/L EPA200.7 2/14/95Mercury, Cold Vapor 1.0 1.8 1.0 U ug/L EPA245.1 12/16/94Nickel, ICP 0.80 40 0.80 U ug/L EPA200.7 2/14/95Zinc, ICP 0.50 20 28.9 ug/L EPA200.7 2/14/95
U=Not detected at specified instrument limitsB=Not detected at specified reporting limits i
AB303335
Corvallis Applied Sciences Laboratory
Client InformationProject Name: Halby Chemical
Project Manager: Jerry Bills/GLOSampled By: Illegible
Client Sample ID: CATZEOBLKSampling Date: 1 1/1 9/94Sampling Time: Not given
Type: GrabMatrix: WaterBasis: As Rec'd.
Instrument ReportingAnalyte Limit Limit
Arsenic, ICP 3.0 10Cadmium, ICP 0.20 5Chromium, ICP 0.25 10Copper, ICP 2.0 25Lead, ICP 0.80 3Mercury, Cold Vapor 1.0 1.8Nickel, ICP 0.80 40Zinc, ICP 0.50 20
U=Not detected at specified instrument limitsB=Not detected at specified reportinq limits
Lab InformationDate Rec'd: 12/1 3/94
Lab ID: 796317Report Revision No.: 0
Reported By: R. McMorrisReviewed By: t-fcv& CT*
SampleResult Qualifier
3.5 B0.20 U0.25 U2.0 U4.51.0 U2.7 B19.2 B
DateUnits Method Analyzed
ug/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95|jg/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95ug/L EPA245.1 12/16/94pg/L EPA200.7 2/14/95pg/L EPA200.7 2/14/95
fiR303336-
Corvallis Applied S
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• • .-A/:;;:;uJtSiiitly;:-:Client Sample :ID:
•; tl?}8iyp• •-"'•• "'."1!
Analyte
Arsenic, ICPCadmium, ICPChromium, ICPCopper, ICPLead, ICPMercury, Cold VaporNickel, ICPZinc, ICP
U=Not detected at specified iB=Not detected at specified r
ciences Laboratory
f SIilSSi'S iliiMitSiS i:*;ii»I8 §ni ^ f*^^•'':'-' :::--i:::rJ ^ K' p
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Instrument ReportingLimit Limit
3.0 100.20 50.25 102.0 250.80 31.0 1.80.80 400.50 20
nstrument limitseporting limits
Sample DateResult Qualifier Units Method Analyzed
3.0 U ug/L EPA200.7 2/14/950.20 U ug/L EPA200.7 2/14/950.25 U ug/L EPA200.7 2/14/954.8 B ug/L EPA200.7 2/14/957.4 pg/L EPA200.7 2/14/951.0 U ug/L. EPA245.1 12/16/941.9 B ug/L EPA200.7 2/14 525.3 ug/L EPA200.7 2/14/95
Ae303337
Corvallis Applied Sciences Laboratory
Client InformationProject Name: Halby Chemical
Project Manager: Jerry Bills/GLOSampled By: Illegible
Client Sample ID: AIRBLANKSampling Date: 11/19/94Sampling Time: Not given
Type: GrabMatrix: WaterBasis: As RecM
Instrument ReportingAnalyte Limit Limit
Arsenic, ICP 3.0 10Cadmium, ICP 0.20 5Chromium, ICP 0.25 10Copper, ICP 2.0 25Lead, ICP 0.80 3Mercury, Cold Vapor 1 .0 1 .8Nickel, ICP 0.80 40Zinc, ICP 0.50 20
U=Not detected at specified instrument limitsB=Not detected at specified reporting limits
Lab InformationDate Rec'd: 12/13/94v Lab ID: 796311
Report Revision No.:Reported By:Reviewed By:
SampleResult Qualifier
3.0 U0.20 U0.25 U2.0 U2.1 B1.0 U19.4 B129
0R. McMorrisCWS T"
DateUnits Method Analyzed
ug/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95ug/L EPA200.7 2/1 4/95ug/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95ug/L EPA245.1 12/16/94ug/L EPA200.7 2/14/95ug/L EPA200.7 2/14/95
AR303338
Corvallis Applied Sciences Laboratory
Client Information ';XJaiK•• • :.:!;; :::pect;Nam|
:•..,,.- Sampled By:
Sampling Date:Sampling Time:
Analvte
Sir'SSBlllIf SRSIill iill!!IIIIII|i:;:!5Jy!ll!lltl:?;:-" •: £96 Information " '' ": '•'•• •:' !' K£;;;slSS!l|ii|ltiS:!i;::;:|:|!S:::;;;!;;ii:: -; ; ."'iSfiJcifl
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t j|: ja ifeiSfti® °t'i-!Ki'&«!K'.- ' ' '• •::;! ; • *?r£: £~*~ .sewi!* •vSJiiMiiisir: :*W-:fe''w ?y » J .-" :A?'. :!ii •«!,Noj..given,- •. ..• ..•••. ..&,::;. :.;.?;:;,;>; -*• ~fff ,- •, -.-•- ••.- Kf:,i, :«,'-;«- .. :, •>• .. . •• . >~ ;-, , .-.I- .jiiaiissBEif si HSSjD«*!sjA.:-* z*'. ff x- . . .v '- 1 •:.:•••;•?;::!Grab'"' ' ;l- :":;' *"5 ':' : ••' *:M v :- •' i *K-" • PSii w, • • -^ *• : . ^' •:• : " • S:S0yi&S& m m ' V . : . : : . ' : ";: . •/•:. f?^ p i,,,;,,* , ^ ^ ^^ :;•:, ;:::vr3-:*31lf!ill|!|||i:S
Instrument Reporting Sample DateLimit Limit Result Qualifier Units Method Analyzed
Arsenic, ICP 3.0 10 3.0 U ug/L EPA200.7 2/14/95Cadmium, ICP 0.20 5 0.20 U ug/L EPA200.7 2/14/95Chromium, ICP 0.25 10 0.25 U ug/L EPA200.7 2/14/95Copper, ICP 2.0 25 2.0 U ug/L EPA200.7 2/14/95Lead, ICP 0.80 3 4.9 ug/L EPA200.7 2/14/95Mercury, Cold Vapor 1.0 1.8 1.0 U ug/L EPA245.1 12/16/94Nickel, ICP 0.80 40 0.80 U ug/L EPA200.7 2/14/95Zinc, ICP 0.50 20 19.3 B ug/L EPA200.7 2/14/95
U=Not detected at specified instrument limitsB=Not detected at specified reportinq limits
Corvallis Applied Sciences Laboratory
Client InformationProject Name:
Project Manager:Sampled By:
Client Sample ID:Sampling Date:Sampling Time:
Type:Matrix:Baa's:
Analvte
Arsenic, ICPCadmium, ICPChromium, ICPCopper, ICPLead, ICPMercury, Cold VaporNickel, ICPZinc, ICP
'Sample missing
Halby ChemicalJerry Bills/GLOIllegibleAIRCATBLK11/19/94Not givenGrabWaterAs Rec'd.
Instrument ReportingLimit Limit
3.0 100.20 50.25 102.0 250.80 31.0 1.80.80 400.50 20
Lab InformationDate Rec'd: 12/13/94
Lab ID: 796315Report Revision No.: 0
Reported By: R. McMorrisReviewed By: {_fr$& ~~ "
SampleResult Qualifier
UUUUUUUU
DateUnits Method Analyzed
ug/L EPA200.7ug/L EPA200.7ug/L EPA200.7ug/L EPA200.7ug/L EPA200.7ug/L EPA245.1ug/L EPA200.7ug/L EPA200.7
U=Not detected at specified instrument limitsB=Not detected at specified reporting limits
B USE ONLY
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CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(4 Reps. 1 -7 Treatments)
PROJECT No.: 7S£ ///.?, 32- CLIENT: /4/k/ C-h* — CA (TEST ORGANISM: Ce^-i'oAtlt** e A: AGE: /-2-lti LOT No.:SAMPLE DESCRIPTION: _____ fff- l 'h*- "&~ ISAMPLE No.teVLAB MEDIA/NO.: £** h*sv- +**-*{;«. CONTROL/DILUENT: L*& /»v»w:v__TEST START DATE: //-/g>9if TIME: &?&* TEST END DATE://- / 7- ?<*•/ TIME:ANALYST : J~ - Cxx3-£U-_____________________ CODE:________
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LAFormBLATIO V " " *" " Revise
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
95%95%
CONC. NUMBER% EXPOSED
6.25 20.12.50 20.25.00 20.50.00 20.100.00 20.
SPEARMAN-KARBER
TRIM: 10.00% PLC50: 31.864
LOWER CONFIDENCE: 23.697UPPER CONFIDENCE:
NUMBER PERCENTDEAD2.3.7.14.19.
THE BINOMIAL TEST SHOWS THATSOUND CONSERVATIVE 95LEVEL ASSOCIATED WITHAN APPROXIMATE LC50
PERCENT
DEAD10.0015.0035.0070.0095.00
12.50 ANDCONFIDENCE
THESE LIMITS IS 99FOR THIS DATA SET IS
42.846
BINOMIALPROB. (%).2012D-01.1288D+00.1316D+02.57660+01.20030-02
100.00 CAN BE USED ASLIMITS SINCE THE ACTUAL.8692 PERCENT.
33.581
STATISTICALLYCONFIDENCE
RESULTS USING MOVING AVERAGESPAN G LC50 95% CONFIDENCE LIMIT4 .103 30.50 22.68 42.92
****** RESULTS CALCULATED BY PROBIT METHODITERATIONS G H GOODNESS OF FIT
4 .110 1.00 .52
SLOPE = 2.4595% CONFIDENCE LIMITS: 1.64 AND 3.26
LC50= 29.5295% CONFIDENCE LIMITS: 22.17 AND 39.93
LC1 = 3.3195% CONFIDENCE LIMITS: 1.09 AND 5.91
DATE: 11/15/94 TEST NUMBER: 1 DURATION: 48 HOURSSAMPLE: PORE H2O 1 INITIAL SPECIES: CERIODAPHNIA dubia
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 33.581 12.500 100.000 87.500MAA 30.495 22.680 42.920 20.240PROBIT 29.522 22.173 39.927 17.754SPEARMAN 31.864 23.697 42.846 19.148
**** = LIMIT DOES NOT EXIST
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~7S<£"~ /V2~3 '•>TEST ORGANISM: Cjzslad**SAMPLE DESCRIPTION:SAMPLE No.(s): JZZ?<f 4>\LAB MEDIA/No.: CM. lh*/«— VTEST START DATE: /N/£-94ANALYST(s): ZS~. f wl U
*- CLIENT:4" -A- /blb,'*
hW. < _f-* - - /VT-W/0,
f TIME: I3OC>
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/ DG&d'1 * ——
CONTROL/DILUENT: /L i, r*x+t .'i.TEST END DATE: / / - / - TIME: /2- C?
CODE:
TREAT,NO.
1
2
r4
5
6
7
TESTSOLUTION
U6
U*1
I2-*/.
2.Z-/.
6-07.
I00'/r
•
DATE
REP ;
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DETERMINED BY
RER:EXPOSUREPERIOD (Hrs)
:. ,' , :?4 48
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COMMENTS
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FofmBO.T06 ' M-f-l-Vf W V-W T I L Revised \2tV2
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: 10.00%LC50: 56.326
95% LOWER CONFIDENCE: 42.19895% UPPER CONFIDENCE: 75.185
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)6.25 10. 0. .00 .9766D-0112.50 10. 0. .00 .97660-0125.00 10. 0. .00 .9766D-0150.00 10. 4. 40.00 .37700+02100.00 10. 9. 90.00 .1074D+01
THE BINOMIAL TEST SHOWS THAT 25.00 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 98.8281 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 56.732
RESULTS USING MOVING AVERAGESPAN G LC50 95% CONFIDENCE LIMIT2 .168 57.17 44.51 77.52
****** RESULTS CALCULATED BY PROBIT METHODITERATIONS G H GOODNESS OF FIT
7 .334 1.00 .96
SLOPE = 5.9295% CONFIDENCE LIMITS: 2.50 AND 9.34
LC50= 57.9895% CONFIDENCE LIMITS: 43.37 AND 78.20
LC1 = 23.4695% CONFIDENCE LIMITS: 6.52 AND 34.38
DATE: 11/16/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #1 BASELINE SPECIES: CERIODAPHNIA dubia
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 56.732 25.000 100.000 75.000MAA 57.172 44.506 77.521 33.015
VLPROBIT 57.978 43.366 78.203 34.837SPEARMAN 56.326 42.198 75.185 32.987
**** = LIMIT DOES NOT EXIST
AR3033tt8
ICH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
2-3PROJECT No.: - ~ ______ CLIENT:TEST ORGANISM: CJCLS IcJtcffhn ,'<*. tuL,' ' AGE: -2-C( tt LOT No.:SAMPLE DESCRIPTION: " f »~ U oj~t ^ II &c,&<i,h'rv-/ (~0 TA /O/L. __SAMPLE No.fs): " 'LAB MEDIA/NO.: C /fut/ -E-vW/X ______ CONTROL/DILUENT: L<EST START DATE: /f -? TIME: 13/ 0 TEST END DATE: ll~lf'ft TIME:ANALYSTS): J~> Ccxy ]o<-*~~___________________________ CODE:_______________
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1
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DETERMINED BY
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Foon BIAT06 M. I V W W W W T i/ Revised 12»2
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "T g" /72~5 -______ CLIENT: /4ft/k/ Chji '.C-tTEST ORGANISM: £W *cjC$crfbn ,'* djut>,'«~ ' AGE: -.TEST ORGANISM: ^ y . A =,' ________ __ AGE: -2- // LOT No.:SAMPLE DESCRIPTION: / «- < 4f ( / g&SeJJ J- /SO r<4-SAMPLE No.rs :LAB MEDlA/No.: C^K<»^-HKW/X __________ CONTRQLyDlLUENT:TEST START DATE: WL-W TIME: /J/ TEST END DATE: H"''?^ TIME:ANALYSTfe): rJ~>Cr^>k>U__________________________ CODE'
TREAT.NO.
1
2
3
4
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£/^Jc/Z-57
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FoonBtXTOaAR303350
Rcviced 12/92
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "T ^ tt2~3 ______ CLIENT:TEST ORGANISM: Cj&s taot L ,* LJ,,' ' AGE: <£-2.tjU LOT No.:SAMPLE DESCRIPTION: Av - 4"K / / A fid.'n*- / < ~£> 7>9 O ;/<L,SAMPLE No.(s :LAB MEDIA/NO.: C < /fu>/«— >^W/X______ CONTROL/DILUENT:.,/ _________TEST START DATE: Jf -/ -? TIME: /32-£>' TEST END DATE: H-l'S-"?*! TIME: /£ANALYSTS): ZJ"-Co? M-g—_________________________ CODE:______
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DATE
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CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
/l/2~3*. CLIENT:PROJECT No.:TEST ORGANISM: CWiCiflfey?,/?*,'c<. fitjz,'*-______, AGE: -2- ti LOT No.:SAMPLE DESCRIPTION:.SAMPLE No.(s):LAB MEDIA/NO.: Ox/Ka/u-K-vW/g.______ CONTROL/DILUENT:TEST START DATE: ) ~Hs>-°lH TIME: 733^ TEST END DATE: //-/g~?*f TIME:.ANALYSTS): J~> Co^l^t-g—_____._________________ CODE:______________
TREAT.NO.
1
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3
4
5
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TESTSOLUTION
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DATE
REP
A
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A
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FormBLATOe A-R303352 12/9?
ICH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~fe£' /*/2-3 -_____ CLIENT: /4ft/kr Ck>v ',£-<%/TEST ORGANISM: Ce .' y i.A /yLcb,'* ' AGE: 2.TEST ORGANISM: Cg .' y i.A /yLc ,' ______ AGE: <t-2.lfU LOT No.:SAMPLE DESCRIPTION: &yxa- &Afy- / / .gg //K< * ti-SAMPLE No.(sV -S~&5.01LAB MEDIA/NO.: C /K&*<— K>vW/'g._______ CONTROL/DILUENT:.TEST START DATE: Jf 7&-94' TIME: /33^» TEST END DATE: //-/g-9^ TIME:ANALYSTfs : ZT"> Co?)^U_______________________ CODE:________:
TREAT.NO.
1
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6
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DATE
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FocmBtXTOS M,MWUWV/\J Rev««JI2»2AU303353
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No,: "T g" /7Z-3 &~______ CLIENT: /4a/k/-»-*—*-*-T- rf- r-* . A k *ISN* * . X"^ _ ' _ _tf _/ ' _ / / * _ 'TEST ORGANISM: G .'<W i.A aLd>;<x_ _____ _______ AGE: Z-tjU LOT No.SAMPLE DESCRIPTION:SAMPLE No.(s): -SLAB MEDIA/NO.: t fu _ y*j i ______ CONTROL/DILUENT:TEST START DATE: fL-W TIME: 13 H& TEST END DATE: U-tf-f*(ANALYSTS): ZT-Ccx>k>tK—_____.___________________ CODE:
TREAT.NO.
1
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AR30335** 12/02
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
I
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TREAT.NO.
1
2
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4
5
6
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TESTSOLUTION
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DATE
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A
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CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~T££' /4'2~3> -______ CLIENT:TEST ORGANISM: Cg .'<Wy4*,A LtL,' _____ _______ AGE: * -2-</# LOT No.: 51$.SAMPLE DESCRIPTION: Pev . UJg-j~t & I / Cd A/<VW /SAMPLE No.(s):. ~"LAB MEDIA/NO.: C^lh*s*—>m*J;°*__________ CONTROL/DILUENT:.TEST START DATE: )1*-fe-eM TIME: I& TEST END DATE: //-/g-V TIME:
CODE:
TREAT.NO.
1
2
3
4
5
6
7
TESTSOLUTION
£/<?•-. /(
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DATEDETERMINED BY
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AR303356
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "T " fa ' 2-*3> *- _____ CLIENT:_____TEST ORGANISM: CJGS .'aoPc+yfai ,*. x t /W, , ' AGE: «t-2.(J H LOT No.: •5"7g,SAMPLE DESCRIPTION: £W. Ifrkfv*- # / / CAJ-I* / 7 AJ* //'•/-£. ______ ! ___SAMPLE No.fsl:LAB MEDIA/NO.: ^t^u-tow/.^ ______ CONTROL/DILUENT:TEST START DATE: Jfs-/6-9 TIME: IS S" TEST END DATE: //-/^-^V TIME:ANALYSTS): ZT"» Ceaa> le>U>_ _____ _________________ CODE: ________ ; ______
TREAT,NO.
1
2
r4
5
6
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TESTSOLUTION
6/**/c
(*-Z$'J.
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DATE
REP
A
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A
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A
B
A
B
A
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A
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DETERMINED BY
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COMMENTS
-
M303357 Revfced 12/82
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "T e" /VZ S -_____ CLIENT: n^lhy C-hjm\C-<*lJEST ORGANISM: (IWIctdetfhn .A /£>*&,''*-___________ AGE: -2-<4H LOT No.: -6 7IT. "7f_SAMPLE DESCRIPTION:___SAMPLE No.(s): 6-f. JLAB MEDIA/NO.:.TEST START DATE: /fW£-<K TIME: WOO TEST END DATE: //-/P - f^ TIME: /J/g>ANALYST(s):_3HQad^=_____________________ CODE:___________________
TREAT.NO.
1
2
3
4
5
6
7
TESTSOLUTION
/Z-C5/
25 /
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REP
A
B
A
B
A
B
A
B
A
B
A
B
A
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DATEDETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Hrs)24 48
O00Q>
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TOTALFATALITIES
(5
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MEANSURVIVAL
1007.
1001
100 J.
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COMMENTS
FoonBLATOC AR303358 Renccd 1Z/82
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: 50.00%LC50: 100.000 _
95% CONFIDENCE LIMITSARE UNRELIABLE.
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)12.50 10. 0. .00 .9766D-0125.00 10. 0. .00 .97660-01 ;50.00 10. 0. .00 .97660-01100..00 10. 5. 50.00 .6230D+02
THE BINOMIAL TEST SHOWS THAT 50.00 AND +INFINITY CAN BE USED AS STATISTICAL!SOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.9023 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 100.000
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS AT _WHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 11/16/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #1 CAT / EDTA lOmg/L SPECIES: CERIODAPHNIA dubia
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 100.000 50.000 ******* *******MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 100.000 ******* ******* ******* ;
**** = LIMIT DOES NOT EXIST ;
Afi-303359
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "T g" /VZ«J _______ CLIENT: /4ft/k/TEST ORGANISM: (° .Vvafla i .k d+Js,'* __________TEST ORGANISM: Cgi .'oo/Wa i .A L,' _____ ______ AGE: - H LOT No.: -6 7 ,SAMPLE DESCRIPTION: ^ / «- 4f"e - / X < >-/vWvSAMPLE No.s:__LAB MEDIA/NO.: C t /K&*<- > W/'.°._______ CONTROL/DILUENT:_______TEST START DATE: /f"-/£-94> TIME: M/O TEST END DATE: // -/£* - TIME:,ANALYST(s : J~>Cryyl^U________________________ CODE:.
TREAT.NO.
1
2
3
4
5
6
7
TESTSOLUTION
ii-ey.2$ 'Y,
s'vy./ooy
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DATE
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Hrs)24 48
O
0o0oo&o
l/'lffa
TOTALFATALITIES
0o0o0(31O
MEANSURVIVAL
/0#
/ O/
/Od^W/
COMMENTS
I
FoonBtATOaAR303360
12/O2
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~fe£' 2-3 ?~_____ CLIENT:TEST ORGANISM: CgXW«y»L.A j,' ' AGE: 4-2.lffJ LOT No.: 6 7.SAMPLE DESCRIPTION: " f , UJa-htr- & \ Co f/Oi . Z-? t> 7ZLSAMPLE No.(s):___LAB MEDIA/NO.: C<xfuv«-K-*W/'o. _______ CQNTROL/DJLUENT:TEST START DATE: )-h-fc-<M TIME: / / " TEST END DATE: l\-l^^^ TIME: /3ANALYSTS: J~>C^a?I^U_________________________ CODE:_________:
TREAT.NO.
1
2
r4
5
6
7
TESTSOLUTION
I2-S X
'/.
&OY.
Wo/
DATE
REP
A
B
A
B
A
B
AB
A
B
A
B
A
B
DETERMINED BY
fy TALITIESPER EXPOSUREPERIOD (Mrs)24 48
0
&c?0o0oo
ll-lt^
TOTALFATALITIES
£>r>o<9o00o
MEANSURVIVAL
fOO'f
tooiJ00'(.
luo-/.
• :• :::•••;-:•;•:-:-'•;,., . ' •
COMMENTS
-
FomiBUM06 AR30336 I
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
/*
PROJECT No.: T ~ ______ CLIENT:TEST ORGANISM: .Va Q a » i .A =,'»^ , AGE: - H LOT No.:SAMPLE DESCRIPTION:SAMPLE No.(s):LAB MEDIA/NO.: ^tfuv^-KK-W/^ ______ CONTROL/DILUENT.-TEST START DATE: /f-/6-9 TIME: ItZ-O TEST END DATE: I/-/P'?H TIME:ANALYSTfs): -J~> Cgol^U^._____._______________________ CODE:______________
TREAT.NO.
1
2
3
4
5
6
7
TESTSOLUTION
v3/ G/\/\ /f
o * *- A
/W,
25'X
S-O'l.
lOO'/.
DATE
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Mrs)24 48
0
0
O
0
0
00of(-*.3
Ih/fn
TOTALFATALITIES
00
oo00Q0/,2..•?
MEANSURVIVAL
f&y/CO/
too/,IOO'/.
&0'{
So/.
COMMENTS
jI
flR303362ReviMd 12»2
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
^^ SPEARMAN-KARBER '
P TRIM: 50.00%LC50: 100.000 -
95% CONFIDENCE LIMITS
CONC . NUMBER% EXPOSED6.25 10.12.50 10.25.00 10.50.00 10.100.00 10.
NUMBERDEAD0.0.0.2.5.
THE BINOMIAL TEST SHOWS THAT 25SOUND CONSERVATIVE 95LEVEL ASSOCIATED WITHAN APPROXIMATE LC50
PERCENTDEAD
.00
.00
.0020.0050.00
.00 AND
ARE UNRELIABLE. ;
BINOMIALPROB. (%).9766D-01.97660-01.9766D-01.5469D+01.62300+02
-(-INFINITY CAN BE USED AS STATISTICALLPERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCETHESE LIMITSFOR THIS DATA
IS 99.SET IS
9023 PERCENT.100.000 ;
RESULTS USING MOVING AVERAGESPAN G LC50 95% CONFIDENCE LIMIT1 2.169 100.00 0 + INFINITY
•TT:****** RESULTS CALCULATED BY PROBIT METHODERATIONS G H GOODNESS OF FIT7 .582 1.00 .94
SLOPE = 3.6795% CONFIDENCE LIMITS: .87 AND 6.46
LC50= 95.5895% CONFIDENCE LIMITS: 66.73 AND 355.28
LC1 = 22.1795% CONFIDENCE LIMITS: .57 AND 38.74
DATE: 11/16/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #1 AIR SPECIES: CERIODAPHNIA dubia
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 100.000 25.000 ******* *******MAA 100.000 ******* ******* ******* ]
X PROBIT 95.585 66.727 355.285 288.558SPEARMAN 100.000 ******* ******* *******
k*** = LIMIT DOES NOT EXIST
&R3G3363
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~fe£' A/2~S _____ CLIENT: MflJ/?y C-bj \ C-* ITEST ORGANISM: CW.'oofWyAn ,A 0Ltt>,'<><-_____f AGE: - L(H LOT No.:SAMPLE DESCRIPTION:__SAMPLE No.(s):___s£&2i£L(LAB MEDIA/NO.: CU*/fu>/«— y^^i^__________ CONTROL/DILUENT:.TEST START DATE: )J /&~<M TIME: I 3O TEST END DATE: I/~ If'- l TIME: J3ANALYST(s):_3HC£22k^£=_______________________ CODE:.__________________
TREAT.NO.
1
2
3
4
5
6
7
TESTSOLUTION
(oO/-
,«7?/oo/.
DATE
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Hrs)24 48
O
0^3s5
//-/£ffA-
TOTALFATALITIES
O0z.3S5
MEANSURVIVAL
/oo/
SO/
07.
COMMENTS
FoonBLATOe ftR3Q336i* Revicod 12/02
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: T&S" 'Ll2~3, ~______ CLIENT:TEST ORGANISM: j&s ;&O<ff>n , * t=,'*i- _______ AGE: -2.1 H LOTNo.:SAMPLE DESCRIPTION: U f^~ 4fv / X / ULxvy /Wi / Z-fcg // f~° — ___SAMPLE No.(s):LAB MEDiA/No.: ctx^>^<- mW/X _________ CONTROL/DILUENT:TEST START DATE: / -/ " ^ TIME: yk/Z-S" TEST END DATE: //"V " / TIME: 133£~ANALYST(s): J~. Cc^|oU_______________________________ CODE:___________________
TREAT-NO.
1
2
»
5
6
7
TESTSOLUTION
_M
US7.
,1.
*•/.So-,
ICO'/.
DATE
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Hrs)24 48
0O
0
O
O
0
O0
o0o0
I/-/?n
TOTALFATALITIES
O0o0o0C500000
MEANSURVIVAL
/<#/
IOO'/.
ioo/.100'f.
IOO'/.
loo/.
COMMENTS
'
Fom BIAT06 AR303365
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIO ASS AY SURVIVAL DATA(2 Replicates)
PROJECT No.: "T g" /V2~5 -______ CLIENT:TEST ORGANISM: j2j2V loot**?hri ,'&. 0bJs,'o<-_____SAMPLE DESCRIPTION: ^ fi»s*- UJc.- ^ & ( / flSAMPLE No.(s):___LAB MEDIA/NO.: ^u^t-H^-W/ip,______ CONTROL/DILUENT:TEST START DATE: /f -? TIME: W^O TEST END DATE: //- /^ -?V TIME
TREAT.NO.
1
2
3
4
5
6
7
TESTSOLUTION
6/ fc.
£.££'/
)Z-S'/
157
S&'(.
I&O'L
REP
A
B
A
B
AB
A
B
A
B
A
B
A
B
DATEDETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Hrs)24 48
00
0
(9
0060#O1
-i—s
//-/*;-
TOTALFATALITIES
(3C3
C?6O0O0
O1
-4 ———£
MEANSURVIVAL
/CO/
/C<5/
/oe/./ /y /yfi/
COMMENTS
4/
FonmBLATOS AR303366 Reviccd 12/02
CT-TOX: BINOMIAL, MOVING AVERAGE, PROSIT, AND SPEARMAN METHODS
SPEARMAN-KARBER :
TRIM: 10.00% ;LC50: 70.711
95% LOWER CONFIDENCE: 62.95195% UPPER CONFIDENCE: 79.427
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB. (%)
6.25 10. 0. .00 .9766D-0112.50 10. 0. .00 .97660-0125.00 10. 0. .00 .9766D-0150.00 10. 1. 10.00 .1074D+01100.00 10. 9. 90.00 .10740+01
THE BINOMIAL TEST SHOWS THAT 50.00 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 97.8516 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 70.711
RESULTS USING MOVING AVERAGESPAN G LC50 95% CONFIDENCE LIMIT '-.2 .168 70.71 55.12 104.31
.._____.—-.—._._....—.,— _-.__...»..__..-«._.__._.__.,£.....«.*.__..._.___._._._._.._....__._._,___. »— — _«...._.. ___*..-_______»._..i
lc***** RESULTS CALCULATED BY PROBIT METHODERATIONS G H GOODNESS OF FIT7 .337 1.00 1.00
SLOPE = 8.5295% CONFIDENCE LIMITS: 3.57 AND 13.47
LC50= 70.7295% CONFIDENCE LIMITS: 55.19 AND .90.74
LC1 =37.7195% CONFIDENCE LIMITS: 15.00 AND 50.10 i
DATE: 11/16/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #1 AIR / CAT SPECIES: CERIODAPHNIA dubia !
METHOD LC50 CONFIDENCE LIMITS '••LOWER UPPER SPAN
BINOMIAL 70.711 50.000 100.000 50.000MAA 70.711 55.120 104.313 49.193 !
APROBIT 70.717 55.193 90.744 35.551SPEARMAN 70.711 62.951 79.427 16.476 ',
** = LIMIT DOES NOT EXIST
&R303367
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
/V2-J ______ CLIENT:PROJECT No.: __TEST ORGANISM: Cj>s [odcfflin ,'&. aktk,'* , ' AGE: £-2-ijH LOT No.:SAMPLE DESCRIPTION: H L. US»j-tr- / / X « *»f f'c. / &0TASAMPLE No.(s):LAB MEDIA/NO.: ^Ka/**— Kv>W/X ______ CONTROL/DILUENT:TEST START DATE: )J lb-eM TIME: 7 5 TEST END DATE: //- /iff -f TIME: /3 ffoTANALYSTfs): J~> Cco l^t-g—_______________________ CODE"______________________
TREAT.NO.
1
2
3
4
5
6
7
TESTSOLUTION
/£ '/OT T l
2sy.S~6'/
lOO'/,
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DATEDETERMINED BY
f OALITIESPER EXPOSUREPERIOD (Hrs)
:';24"" ' ' 48
0
0
0000z.3
//-/^^
TOTALFATALITIES
0o0oG0
z3
MEANSURVIVAL
IOO'/.
W/.
(Off/.
507
COMMENTS
j/
AR303368Fom> BLATOfl , . _ . Rev««) 12/92
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: 50.00% ; :"77LC50: 100.000
95% CONFIDENCE LIMITSARE UNRELIABLE.
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)12.50 10. 0. .00 .9766D-0125.00 10. 0. .00 .97660-0150.00 10. 0. .00 .9766D-01100.00 10. 5. 50.00 .6230D+02
THE BINOMIAL TEST SHOWS THAT 50.00 AND +INFINITY CAN BE USED AS STATISTICAL!SOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.9023 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 100.000
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 11/16/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #1 AIR / EDTA lOmg/L SPECIES: CERIODAPHNIA dubia
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 100.000 50.000 ******* *******MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 100.000 ******* ******* *******
**** = LIMIT DOES NOT EXIST i
A8303369
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: A$<£ /H2~S^- CLIENT: m/bw Oh>w*,£.<%/TEST ORGSAMPLE CSAMPLE (sLAB MEDITEST STAANALYST(
TREAT.NO.
1
2
3
4
5
6
7
JANISM: Cjes loofeyyhn ,'*. aido,' , ' AGE: - H LOT No.: -5 7lf, «£"7f)ESCRIPTION: Aw«_ U a t - & 1 / $J-*rodrl< / (S-OTA 2-G /L,lo.fs): Gf.Oi 'A/No.: C*-t/fui/«— yy Ai CONTROL/DILUENT: l~a,L ?***?;<*-RTDATF- )-h-/&>~9tf TIME: /V4*<? TEST END DATE: //-/ - TIME: yj i?sV. ZT". CcwI U-.
TESTSOLUTION
,, ,
«.s7
2 7
sSoy.;o*X
DATE
REP
A
B
A
B
A
B
AB
A
B
A
B
A
B
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Mrs)24 48
•0-
& ~
00
O0
O6
1
d
rt-/r<K
CODE:
TOTALFATALITIES
>-~
&—
0
0
O
000/n
MEANSURVIVAL
-fWyf-
/ /
ICO'/.
/OO/
?*•/
COMMENTS
y/
/(J5y fT.o~r P<?c-VorvK« xv£/ - ————
; I
FixmBlATOC AR303370 Bcvked 12/92
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "7? A'Z-S ______ CLIENT: hUlhy_______________________TEST ORGANISM: des.'oo/W? - •' _____.- AGE: ~2.i{H LOT No.: -6 7£SAMPLE DESCRIPTION: . 4fc / /eSe'<Oy^ / e* TA-SAMPLE No.(s):LAB MEDIA/No.: <2 t fuv**— \v-**{i _________ CONTROL/DILUENT:TEST START DATE: /f / -fr TIME: IW TEST END DATE: H"/?- ?1 TIME:ANALYST(s): J~> Ccol^^^—_______________________ CODE:
TREAT.NO.
1
2
P*4
5
6
7
TESTSOLUTION
IZ-SV.U> • 'li1.?
2-S't
&07.
10°' 6
DATE
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Hrs)24 48
OO
od333>
^
//-/r^
TOTALFATALITIES
0oooJ?J7f
MEANSURVIVAL
/oo/
loo-/.
toy.30/.
COMMENTS
/
- —
«=om.BlAT06 Wt\ U U U W / I Rcv««J 12/92&R30337I
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: 30.00% PLC50: 47.880
95% LOWER CONFIDENCE: 24.89295% UPPER CONFIDENCE: ' 92.097
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD12.50 10. 0.25.00 10. 0.50.00 10. 6.100.00 10. 7.
THE BINOMIAL TEST SHOWS THATSOUND CONSERVATIVE 95 PERCENT
DEAD PROB.(%).00 .97660-01.00 .97660-01
60.00 .37700+0270.00 .17190+02
25.00 AND +INFINITY CAN BECONFIDENCE LIMITS SINCE THE
USED AS STATISTICALLACTUAL CONFIDENCE
LEVEL ASSOCIATED WITH THESE LIMITS IS 99.9023 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 45.793
RESULTS USING MOVING AVERAGESPAN G LC50 95% CONFIDENCE LIMIT2 .273 55.85 39.97 84.78
****** RESULTS CALCULATED BY PROBIT METHODITERATIONS G H GOODNESS OF FIT
5 .314 1.00 .17
SLOPE = 3.8195% CONFIDENCE LIMITS: 1.67 AND 5.95
LC50= 59.7195% CONFIDENCE LIMITS: 42.71 AND 93.32
LC1 = 14.6395% CONFIDENCE LIMITS: 2.66 AND 24.80
DATE: 11/16/94 TEST NUMBER: DURATION: 48 HSAMPLE: #1 AIR/EDTA 40mg/L SPECIES: CERIODAPHNIA DUBIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 45.793 25.000 ******* *******MAA 55.851 39.974 84.780 44.805
X PROBIT 59.711 42.708 93.318 50.610SPEARMAN 47.880 24.892 92.097 67.205
**** = LIMIT DOES NOT EXIST
AR303372
ICH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: 7-S£ /V < ~5 _____ CLIENT: /4ft//*___________________ ___ y_ _TEST ORGANISM: (L&s (odtcffhn ;& atuL,'*-________ AGE: <£-2-l{H LOT No.: - 7 .SAMPLE DESCRIPTION: ~ r vu 4f"t - / /SAMPLE No.(s):.LAB MEDIA/NO.: ^cfu^<— ^i^_______ CONTROL/DILUENT:TEST START DATE: /f /£-9 TIME: I SV TEST END DATE: }l-/8-ftf TIME:ANALYSTS: J~>Cc»bU______________________ CODE:_________,_____
^
TREAT.NO.
1
2
r4
5
6
7
TESTSOLUTION
/S/A^/C
&-2S7
1Z.S/
Z£'/.
6(7
(00 /
REP ;
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DATEDETERMINED BY
vilfliF TALITIESRERlEXPOSURE
I PERIOD (Mrs): ' v!24' ' 48
0
0
ao<9#ooO00o
//-/?/0c
TOTALFATALITIES
6£>
aO
oOoOoooo
MEANSURVIVAL
too/.
100'f.
/cor.loo/.
100'f.
I ooi
COMMENTS
•
A1303373 Revised 12/O2
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~fe£' tt 2~3 ______ CLIENT: /4ft /k/TEST ORGANISM: C^/W.g. x?/ ./V 'TEST ORGANISM: ^ / . g . x?./V AGE: ^# LOT No.:SAMPLE DESCRIPTION: < «- >f-c - / /SAMPLE No.(s): ~LAB MEDIA/NO.: C^tK«Ac-K>x^/X ___ CONTROL/DILUENT:TEST START DATE: S/-^ TIME: " TEST END DATE: }l-(Z- 4 TIME:ANALYSTS): rr>C col U_ ____ __ _______________ CODE: ____________
TREAT.NO.
1
2
3
4
5
6
7
TESTSOLUTION
tJ k.
57
£_•* * ,__*' /
£*', } /
<S&Y.
loo~/
REP
AB
A
B
A
B
A
B
A
B
A
B
A
B
DATEDETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Mrs)24 48
0
0
0
oQ000
00Oo
11-19^
TOTALFATALITIES
OooOaoe>0oo00
MEANSURVIVAL
100'/.
too/.too-/./ooy.10V'/.
/ooy
COMMENTS
I
FoctnBLATOa AR30337UReviced 12/92
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~1 <S / 2 3, ?~_____ CLIENT: Mft/k/ C\v ',TEST ORGANISM: Cg .' y /i.A djJ*.'* ' AGE: ____SAMPLE DESCRIPTION: " Pos*- UJ*-\~tv- & I J 2 e.G *-/ &Tp Trt JO /L-SAMPLE No.(s):LAB MEDIA/NO.: C^\^u^~yy^i^__________ CONTROL/DILUENT: L<EST START DATE: J±±/£j L_TIME: /v5~OO TEST END DATE: //- (& - TIME:
___________________ CODE:________
TREAT.NO.
1
2
P'4
5
6
7
TESTSOLUTION
/2.,--/
2-s"/
7
looy.
DATE
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DETERMINED BY
•FATALITIESPER EXPOSUREPERIOD (Hrs)24 48
O
O
00OO
00
//-/?o/_
TOTALFATALITIES
O0O00000
MEANSURVIVAL
loO'f.,00;.
/06/
loo-/.
COMMENTS
•
FtxmBlATOS AR303375
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~fe£' / 2 3> *-_______ CLIENT: Hft/fTEST ORGANISM: Gev.>WyAr» ,'&. /?Uti>,'° _____ ______ AGE: ~-2-l H LOT No.:SAMPLE DESCRIPTION: < v - UJai~tr & I / Z.e*>\'/'f*- /gr? T/»SAMPLE No.(s):_LAB MEDIA/NO.-. (2*4.lh&"~ **-**{i'*,______ CONTROL/DILUENT: L-<EST START DATE: Ib'W TIME: / Tg<" TEST END DATE: //- /g -fV TIME:ANALYSTS): J~> Co?)^U_____________________ CODE:
TREAT.NO.
1
2
3
4
5
6
7
TESTSOLUTION
I23'/
25'/
'/
/w/.
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DATE
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Mrs)24 48
Oo00o0oo
/I-/?/ft.
TOTALFATALITIES
0
O
O
0
O
0
G>0
MEANSURVIVAL
too'/.
loo-/,
w/.
IOOJ.
COMMENTS
«
FxxmBCATOS &R303376Revved !2/»?
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "T e" /V2LJ -_______ CLIENT: Ma|l?y CJu ', £-*t /• >r—r r y^ r^ y^ « * I «^N • a /* * _ u _ I * S I * . * A **X r~_ ^ OTEST ORGANISM: (lev,'oofLi,'*. 0Ltb,'i-__________ AGE: -2-</// LOT No.:SAMPLE DESCRIPTION: ATAC. LeJaJ-t*- & I / /L**//£<-./tZ/J-TA UP**?//SAMPLE No.(s):___ /~'/ ° "'LAB MEDIA/NO.: C^t/K^<-»>^^f/^_______ CONTROL/DILUENT:.TEST START DATE: )-h-/&-cM TIME: / "/< TEST END DATE: //-/ - TIME:ANALYST(s):_3lLCc22k)! =_______________________ CODE:________;______
TREAT.NO.
1
2
1 3
4
5
6
7
TESTSOLUTION
/1.S-/
25 '/
^O/
too'/.
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DATE
DETERMINED BY
S RP:MJMCS>f^iiEXPOSURE
j: PERIOD (Hrs)•'. ' ""24" 48
^
0
O00000
It' It^
TOTALFATALITIES
Ooooo0o0
MEANSURVIVAL
loo 7.
;a?7./OO'/
/oo 7.
COMMENTS
•
F<xmBtAT06 ftI3G3377
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~7 < A/2~J ?-_____ CLIENT: J4a/!?y Cj-utw,', £-3: I-f -f -T- vx »—»S^ A • * *^% • * f* * ^ 0 _ I * m l * - * • ^ f~_ ^ OTEST ORGANISM: Cjzs <oc$c*s?ln ,'c*. /^M^»'^____________ AGE: -2. /y LOT No.:SAMPLE DESCRIPTION: r «_ UJaj-t*>- & / / xSAMPLE No.(s):____Jr]£l_1tflLAB MEDIA/NO.: C /ft -K W/o.______ CONTROL/DILUENT:.TEST START DATE: li*-/£>-eW TIME: t&SsT TEST END DATE: //-/f-W TIME: 2.<TANALYST(s):_33LQa2J^£=_______________________ CODE:_____________________
TREAT.NO.
1
2
3
4
5
6
7
TESTSOLUTION
&Wo
'i
/z-Z5X
5&X
Vo-/.
DATE
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Mrs)24 48
0
' 0
O
0
O
0
0oo0
-jj _
//-/s*/%
TOTALFATALITIES
60
OOOGOOOD^^
iX'
MEANSURVIVAL
/#>/
700 /.
/oo/IOO'/.
/ooi
i°7.
COMMENTS
PomiBtAToaM303378
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: 10.00%LC50: 73.487
95% CONFIDENCE LIMITSARE UNRELIABLE.
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)
6.25 10. 0. .00 .97660-0112.50 10. 0. .00 .9766D-0125.00 10. 0. .00 .97660-0150.00 10. 0. .00 .97660-01100.00 10. 9. 90.00 .10740+01
THE BINOMIAL TEST SHOWS THAT 50.00 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 98.8281 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 76.073 :
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 11/16/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #1 ZEO / CAT SPECIES: CERIODAPHNIA dubia
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 76.073 50.000 100.000 50.000MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******
X SPEARMAN 73.487 ******* ******* *******
**** = LIMIT DOES NOT EXIST i
ftI303379
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: T5E 141*3 2- _______ CLIENT:TEST ORGANISM: /*7i/<r/V?f___________.___________ AGE: 3 gfayr<; LOT No.:SAMPLE DESCRIPTION: PoS<-SAMPLE No.(s): .Sfc>f .rt 2-LAB MEDIA/No.: 2 f-TPa /g. /te/-,V\_______ CONTROL/DILUENT:.TEST START DATE: J2.-6-7*/ TIME: I(OO TEST END DATE: IL-&~Jtf TIME:.ANALYSTfsl: IT- C^xvfcX*—__________________________ CODE:_____________
TREAT.NO.
1
2
Ps
4
5
6
7
TESTSOLUTION
L/4B
fc.*7.12- 7.
?*7.O'/
loo-/.
DATE
REP
AB
A
B
A
B
A
B
A
B
A
B
A
B
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Mrs)24.
17-
48
OO
0
00O/0IIs^
/;--T(
TOTALFATALITIES
OO
O
0
O
O
1
OI15"£
MEANSURVIVAL
\o° /
>«>•/.
toe?'/
Q o /
?OY.°l
COMMENTS
I
Bit30338 Ifxxm BCAT06
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
95%95%
CONC. NUMBER% EXPOSED6.25 10.12.50 10.25.00 10.50.00 10.100.00 10.
SPEARMAN-KARBER J^
TRIM: .00%LC50: 57.435
LOWER CONFIDENCE: 46.130UPPER CONFIDENCE:
NUMBER PERCENTDEAD0.0.1.2.10.
THE BINOMIAL TEST SHOWS THATSOUND CONSERVATIVE 95LEVEL ASSOCIATED WITHAN APPROXIMATE LC50
PERCENT
DEAD.00.00
10.0020.00100.00
25.00 ANDCONFIDENCE
THESE LIMITS IS 98FOR THIS DATA SET IS
71.511
BINOMIALPROB. (%).97660-01.97660-01.10740+01.54690+01.9766D-01
100.00 CAN BE USED ASLIMITS SINCE THE ACTUAL.8281 PERCENT.
62.190
STATISTICALLYCONFIDENCE
RESULTS USING MOVING AVERAGESPAN G LC50 95% CONFIDENCE LIMIT2 .168 56.36 43.81 76.07
****** RESULTS CALCULATED BY PROBIT METHODITERATIONS G H GOODNESS OF FIT
8 .313 1.00 .23
SLOPE = 5.4695% CONFIDENCE LIMITS: 2.40 AND 8.51
LC50= 55.4395% CONFIDENCE LIMITS: 41.20 AND 75.55
LC1 = 20.7695% CONFIDENCE LIMITS: 5.73 AND 31.08
DATE: 12/6/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #2 BASELINE SPECIES: MYSIDOPSIS BAHIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 62.190 25.000 100.000 75.000MAA 56.356 43.814 76.071 32.258
•Xl PROBIT 55.428 41.203 75.548 34.345SPEARMAN 57.435 46.130 71.511 25.381
**** = LIMIT DOES NOT EXIST
AR303382
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~T5E I4Z*3 2- _________ CLIENT:TEST ORGANISM: / (XC/gf __________ ________ AGE: 3 L a < LOT No.:SAMPLE DESCRIPTION]: P&s<- UJcfa L / T'o. /SAMPLE No.fsl: £,5 .t>1—LAB MEDIA/No.: 2yf-7Pfc;^ Mas',t\ ________ CONTROL/DILUENT:TEST START DATE: J2--£-?*/ TIME: /7oO TEST END DATE: / Z- -^ "?V TIME: //,j GANALYSTS: IT> Coe;JUL»__________________ CODE:_____________________
TREAT.NO.
1
2
br4
5
6
7
TESTSOLUTION
^y^vv-ifCfezffC
L>-tS'/.
/Z-S2z*lS~OY.
1007.
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DATE
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Hrs)24 48
O
0
0
0CjtoOO
^O1/
I2.-1fa-
TOTALFATALITIES
£
O
0O
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0O0
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MEANSURVIVAL
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COMMENTS
'
AH-303383FormBLATOe Revised 12/97
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: 1 :1413 2-TEST ORGANISM: My.<,'c\SAMPLE DESCRIPTION: PoS*. UJc&t+-SAMPLE No.(s): <£? *-LAB MEDIA/No.: 2 >jf*i~ Trr>f>:c- Wcc<r',r\TEST START DATE:") Z-^-V 4 TIME:ANALYST(s): T- CooJbL*—
CLIENT:
• ""^ / s
1200
/4/k/ Cl*(L '.c*\AGE: 2—tpfay
-&oliT~<- / /Ttf« s» >• '"v-x
CONTROL/DILUENT: / >ATEST END DATE: 12. ~& ~
CODE:
<: LOT No.: / 7V
»v«W,'o«_-f" TIME: /O"0
TREAT.NO.
1
2
3
4
5
6
7
TESTSOLUTION
&/-*
7.
7B^
X/O^X
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DATE
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Hrs)24 48
QO
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TOTALFATALITIES
C?
0
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MEANSURVIVAL
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7®/
COMMENTS
>
ftR30338i*FwmBlAToa Reviwd \1KT2
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Reps. 1 -4 Treatments)
CLIENT: M? /b (Zh*wt i'c.4 /PROJECT No.:TEST ORGANISM: /Tlv/S.'of _________ . _________________ AGE: 3L<>r3 LOT No.:SAMPLE DESCRIPTION: Pare-. USafJi 2SAMPLE No.fel: ________LAB MEDIA/No.: 2- + Tsofi /Mar f CONTROL/DILUENT: ^TEST START DATE: IZ-£^K TIME: jZnO TEST END DATE:_/2_r?j5 /___ TIME:ANALYSTS): tJ~> CygJ^-______________________ CODE:
TREA1";';"•NO/""'
1
2
t..3
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I2.-S/
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REP
A
B
A
B
A
B
A
B
DATEDETERMINED BY
FATALITIESPEREXPO^IJREPERiOD;(Hrs)24 48
O
0
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OO
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MEANSURVIVAL
iwy.looy.
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101
COMMENTS
COMMENTS:
FocmBLATOSA
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Reps. 1 -4 Treatments)
PROJECT No.: TSgT /fZ<J? Z_ ____ CLIENT: /3 \.lTEST ORGANISM: Alys/of_______________________ AGE: 2.a(ay-3 LOT No.: /4-7"fSAMPLE DESCRIPTION:/ ~r77~Z:^7~^ ~~ - " ~ LSAMPLE No.(s):.LAB MEDIA/NO.: 2-g~/>0± ~\s<x>;c.Mir;*i_____ CONTROL/DILUENT:TEST START DATE: IZ-I -'K TIME: I? QC? TEST END DATE: / 2. - g* -?t/ TIME: ) U OANALYST(s):_^HC^2jM<-=_______________________ CODE:____________________
TREAT.NO.
1
2
3
4
TESTSOLUTION
/ L. 'V^ /
^ "%-5 /
5'<?X
,00 'IDATE
REP
A
B
A
B
A
B
AB
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Hrs)24 48
O
0
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TOTALFATALITIES
0OGOCb(\I
. I
MEANSURVIVAL
100 '/.
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COMMENTS
••
I
COMMENTS:
ForniBtATOfiA Revteed 12/92
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Reps. 1-4 Treatments)
PROJECT No.: TSxg" /f£d? 2_____ CLIENT: //Q/£y <C-A-e-vo-7 /Cq /______TEST ORGANISM: Alv/s/of_____________________ AGE: 2 oy~5 LOT No.:SAMPLE DESCRIPTION:.SAMPLE No.(s):_LAB MEDIA/NO.: 2..s>:/- ~Tso*ic, /vkr;* _____ CONTROL/DILUENT:————*T .,-.„,.„., « r ~~ ^ ~_TEST START DATE: l2-£-9<f TIME: IZ&O TEST END DATE: ll-G-QH TIME: / /J OANALYSTS: tJ". Cy^M<-._______________________ CODE:____________________
Tfti r;;:i.
1
2
3
4
'Hii--/.&-(.1007.DATE
-iR'EP'
A
B
A
B
A
B
A
B
DETERMINED BY
FATALITIESPER;; |oiS(JI5E
24 48 :
O
O
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/2_-£$/—
TOTALFATALITIES
O
0
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MEANSURVIVAL
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COMMENTS
COMMENTS:
RxmBLATOOA , M11 *J U U O U / Revte«l 12AKM 3-0 33 a 7
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~T5E I4Z3 2-______ CLIENT: / Q/ky C_\*<LM',C*,\TEST ORGANISM: /Y)\s<Z,'c>\___________________ AGE: 3~gfay<; LOT No.:SAMPLE DESCRIPTION: PoS*- UJc - ZL / ~/Le>r>\' *- ) Cg»-f.SAMPLE No.fs : >£^f'.^2-_____________________________LAB MEDIA/NO.: 2 f- 7 y/<L Ma/-;r\________ CONTROL/DILUENT:.TEST START DATE: ;2.-£-7*/ TIME: /Z.g>C> TEST END DATE: /£ - 'IH TIME: //J OANALYSTfs): j"-Coc/JcJL*—______________________ CODE:___________________
TREAT.NO.
1
2
3
4
5
6
7
TESTSOLUTION
g/fevrA
£>,£&'/
A2. 6 '/
•'/.S'O't
ioo'/f
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DATEDETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Hrs)24 48
O
000O00000^7_
/L-r/%
TOTALFATALITIES
O
O
O
O
O
O
O
a0O
1.?_
MEANSURVIVAL
/CO/
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\ooy
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loo/
°7.
COMMENTS
AR303388
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Reps. 1 -4 Treatments)
PROJECT No.: ~7S&~ /f2j? Z_ _____ CLIENT: //3//>v/ <C-/ie-vv7 /C<3 \ _ _ _ _ _TEST ORGANISM: /Ky s '.c( _____________ _____ AGE: ZdaS LOTNo.: A T fSAMPLE DESCRIPTION/ P re. *Ofrfe«- ^X / Qje lL ffttSAMPLE No.(s): ~LAB MEDIA/No.: 2. + "7 /c. /&<-:*/______ CONTROL/DILUENT:TEST START DATE: \Z~C, tl TIME: I/&O TEST END DATE: /Z - fr -?f TIME: //<£*=>ANALYST(s): t-Tr C^gf^^_______________________ CODE:_____________________
'TREAT:;1:'NO;
——\ ....
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":SQi Ul|0N;;
o'/.i .r• f^r
4
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REP
A
B
A
B
A
B
A
B
DATE
DETERMINED BY
FATALITIESPER^RiSUREPERIOC)l(Hrs)24 48
00
oo0o
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TOTALSFATALITIES!
/>O00o0
s-lKlEA'N'itJR IVAL
ito-f.loo/.loo/.
COMMENTS
1
COMMENTS:
Fom,8l>.ToaA H H J U W O U .3 Bevised \2KKAR303389
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Reps. 1-4 Treatments)
PROJECT No.: fSg' IQ-<L<2 Z______ CLIENT: M?/£y C-he ilc, \TEST ORGANISM: m\f<'.d ' AGE: 'Z.AwX LOT No.: AT^SAMPLE [SAMPLE fLAB MEDTEST ST/SANALYST
TREAT.NO.
1
DESCRIPTION:' p/,rc_ -f .7 Qc.<*-]; j# '4*l;us}~vlo.(s): JS~£5,Ol. • ' fA/No.: 2-£T/)6'l- ~T/"cyic- /Had fkRTDATE: /Z-4-7<f TIME: //GO(s): ~3~' Co&V —
TESTSOLUTION
\OO i •'M i • S
2 Ly^x3
,
4
*sT
DATE
REP
A
B
A
B
A
B
A
B
DETERMINED BY
FATALITIES• • '• •' .;•• • • :• ' : •• '••'• '/ •'•'•:.!:,•
r*>r~r T*r P ^ ?l''t[T?rJ ••( Cl* ' T~^ J"kl- \j*%? %_i* n Tr ' . '' •
PERidD;(Hre) •24 ':: -48; ;.'.:;.,
5-
S0$0
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/ 'f< L
CONTROL/DILUENT: / ?4 f W/TEST END DATE: /2 -ts- 4 TIME: //25t7
•v tbpjiLir,:
£~r5v^
5-5
CODE:
MEAN;SURVIVAL
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COMMENTS
|
COMMENTS:
AR303390Fom,BLAT08A t2»2
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~J5E'141*3 2-_______ CLIENT:TEST ORGANISM: Mys,'c\__________t________' AGE: '3 Jt<*y<z LOT No.:_______SAMPLE DESCRIPTION: PoS*- tOcfe*- **3 // Cfl-/"/>wSAMPLE No.fsl:LAB MEDIA/NO.: 2f-77z/^ /%a/-/n _____ CONTROL/DILUENT:TEST START DATE: J£-£~?4 TIME: JJ0Q TEST END DATE: /-- TIME:ANALYSTS: IT> CookJ — __________________________ CODE: ________ | _______
TREAT.NO.
1
2
a4
5
6
7
TESTSOLUTION
g L
(,.IS>/.
,l.sy_
2*7
<S~0'A
iooy•
DATE
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Hrs)24 48
OO
O
O
O0
0o0£>% ^
\
/£-frf/ _
TOTALFATALITIES
O>
O
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(3
0
O
O
O
O
G>&,<
MEANSURVIVAL
l&O'f.
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i°°Y.°'£
COMMENTS
AR30339I
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: .00%LC50: 70.711
95% CONFIDENCE LIMITSARE UNRELIABLE.
«. ^____ «T ___ <•»«•• ^ «M B •• B ••• «W •• B B •« W» « B •» •• ••«••*••* M ••——••••I—— ———— «• •__ UK «• «• «>•»•<••____ nT l~
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)
6.25 10. 0. .00 .9766D-0112.50 10. 0. .00 .9766D-0125.00 10. 0. .00 .9766D-0150.00 10. 0. .00 .9766D-01100.00 10. 10. 100.00 .9766D-01
THE BINOMIAL TEST SHOWS THAT 50.00 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.8047 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 70.711
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 12/6/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #2 CATION EXCHANGE SPECIES: MYSIDOPSIS BAHIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 70.711 50.000 100.000 50.000MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 70.711 ******* ******* *******
**** = LIMIT DOES NOT EXIST
AR303392
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Reps. 1 -4 Treatments)
PROJECT No.: 7S5g" t -2- 2_ _____ CLIENT: j4t)lb\J C-he~-> n /C<% ITEST ORGANISM: JY\\]<z'.c{ ' AGE: ^da«S LOT No.: AT 4SAMPLE ISAMPLE fLAB MEDTEST ST/ANALYST
in1
0Z3
4
DESCRIPTION/ P/>r«_ UJefftt A _ / C*-f;'<n jtf <4-0( ,'<-,<;'*'Mo.(s): -£"&f.<02- 7 f t /A/No.: 2-£T/><o't~ l/'o tc- /rt»ri*iiiRTDATE: l2-£-?<( TIME: ' 1 (O &(s): CT-C M
X;.;. ;,;.•.;';, -.;,•,• • .•;_;.!.:• !•;• X-XvX-' •'; ' ; ' ''!''vi<v;*l'!' '!'''i:! '!'!•:•;•:•!*;•'''•:•:-"•:-'-" '-••••;:
• '• ''.'',•'•''' •' i :t Xi I'Mvi': '' .•'•
' .s-7.S-
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REP
A
B
AB
A
B
A
B
DATE
DETERMINED BY
liiii:,24" •;- 48
~
,
^
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CONTROL/DILUENT:/. mJlfcTEST END DATE: /2-S1- ^ TIME: /S&o
6TS~^$"
6~g
CODE:
::-:IR::'.'V'i::''':i::i^iiNJEAN1 .•"StJR iVAL: •
£>/
. t;/
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COMMENTS
COMMENTS:
ft* 3=03393
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~I3£.I4Z*3 Z-_______ CLIENT:TEST ORGANISM: Wygjc*_______________________ AGE: £W«y<; LOT No.:SAMPLE DESCRIPTION: PoS*. UJcfa L. / C.0rticr I A Sc,+ 'SAMPLE No.(s): < "& .*> T-____________________________LAB MEDIA/NO.:2£ f-TT v M*s'.r\________ CONTROL/DILUENT:.TEST START DATE: J2.-fe>-74 TIME: /3QC> TEST END DATE: IZ. s-7 TIME:ANALYSTfs : T'Co&kJ^—_______________________ CODE:_____________
TREAT.NO.
1
2
3
4
5
6
7
TESTSOLUTION
t>/*«, k
L>-z$y.!2,.5'/_
25-/
vS"V
loo/
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DATEDETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Hrs)24 48
c>c>ooooo0aa^£~
/Z-^(M
TOTALFATALITIES
O
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COMMENTS
I
HR303391*
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: .00%LC50: 70.711
95% CONFIDENCE LIMITSARE UNRELIABLE.
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB. (%)6.25 10. 0. .00 .97660-0112.50 10. 0. .00 .97660-0125..00 10. 0. .00 .9766D-0150.00 10. 0. .00 .97660-01100.00 10. 10. 100.00 .97660-01
THE BINOMIAL TEST SHOWS THAT 50.00 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.8047 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 70.711 ——=
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEY STATISCALLY SOUND RESULTS.
DATE: 12/6/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #2 CATION / AERATION SPECIES: MYSIDOPSIS BAHIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 70.711 50.000 100.000 50.000MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 70.711 ******* ******* *******
**** = LIMIT DOES NOT EXIST
At303395
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~75£142 3 2-______ CLIENT: tiolky C\*<L ',c*ATEST ORGANISM: M tX<T,V?f __. __ ___ AGE: 3- .TEST ORGANISM: My<z;c\______ _____?_________ AGE: 3-ugfayg LOT No.:SAMPLE DESCRIPTION:_£ -«-SAMPLE No.(s):.LAB MEDIA/NO.-.2 +f\-~i7cx,:c Marl^_____ CONTROL/DILUENT:.TEST START DATE: J2.~ £-•?*/ TIME: iJ C TEST END DATE: /Z- -g ^ TIME: /2.£>OANALYSTfs): iT-Coc/U-*—______________________ CODE:____________________
TREAT.NO.
1
2
3
4
5
6
7
TESTSOLUTION
6J-*1>.2SI
ll.S7.
sy.&y.
/<*>'(.
DATE
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Hrs)24 48
0
O
O
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O
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O
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O
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MEANSURVIVAL
/oo/
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loo/
looy.tooy.<&-t
COMMENTS
»
AR303396
CH2M HILL Milwaukee Bioassay Laboratory
PROJECT No.:
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Reps. 1-4 Treatments)
/4-Z ? 2_ CLIENT: //Q/£v/ Che~m /C<3 fTEST ORGANISM: Mv '.d ' AGE: ^AavS LOT No.: A-7~4SAMPLE ISAMPLE \LAB MEDTEST STAANALYST
•, ''V;",';';-"', ';•:•:• ••';';•''. •, .;.\>v.v. --•,.,,. ;,,
'" \'., .'.•_• •,, ••• • , • ,
1
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DESCRIPTION:' P/>,"c_ lA>eAiv- **• 3 / Ccf+.'G- 0 TA /'£>*~,/L.o.fs : -5T iP-02—A/No.: 2-.5>*-f "TsofSc. Mtr!*fiRTDATEr'l'z-i.- ^ TIME: ' ILV&'(s): iT"- O? M-«
:iai|ii-sy.2-67.
50 y
IOOY
REP :
A
B
A
B
A
B
A
B
DATE
DETERMINED BY
: FA|A;LITJES;V '
;:;"''';;:piFt|6E>'i:|H.rs), ....24 48
OO
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TOTALFATALITIES
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' £
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CODE:
MEANSURVIVAL
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COMMENTS
COMMENTS:
FocmBLATOOA fill *J U \f V *> / Revised IZftCAR303397
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: .00%LC50: 70.711
95% CONFIDENCE LIMITSARE UNRELIABLE.
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)12.50 10. 0. .00 .9766D-0125.00 10. 0. .00 .97660-0150.00 10. 0. .00 .9766D-01100.00 10. 10. 100.00 .9766D-01
THE BINOMIAL TEST SHOWS THAT 50.00 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.8047 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 70.711
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 12/6/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #2 CATION / EDTA lOmg/L SPECIES: MYSIDOPSIS BAHIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 70.711 50.000 100.000 50.000MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 70.711 ******* ******* *******
**** = LIMIT DOES NOT EXIST
RR303398
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Reps. 1-4 Treatments)
PROJECT No.: TSg" /f2.c 2_ CLIENT: M? /£y (CA.e-wr/C ITEST ORGANISM: /ttvs/cf AGE: 2.da./vS LOT No.: A 7~ 4SAMPLE ISAMPLE \LAB MEDTEST ST/*ANALYST
rip
1
p =
3
4
DESCRIPTION:' Por«z_ Weitt Jft- 3 . 1 Ceti~!0r\ &J9TA cs i/L,Nlo.te): .Sfc*,*>1- 'A/No.: 2-5T/)A~l~ T/'cytc. /rlari lLRTDATE:"l'z-6.- ^ TIME: ' iZVS^(s): T' O3><?J < .
/z 72
/
/00/DATE
i REP
AB
A
B
A
B
A
B
DETERMINED BY
'.,: ":•' ._,;,;,,;.;.,,;.,;,-•;•,;.;.•.,,;,•:•.:•,;,;.',•. ...'I' v' , . ', _; ; ';'.
:'Of* r '::f*7\yp' 'Olil Ctt^ ' '•'' ''i 'irrn''r' "L** -kixv?\./ i r.'' ' '1 '''f rrir\.i vJU-'-f HfSj • • * '.•24 •"•.'.:. 8'
O(3
00O0££/?--*Ot -
CONTROL/DILUENT: L&L nwtl*TEST END DATE: 17 - - H TIME: /2 ^
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CODE:
SURVIVAL
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:
COMMENTS:
Focm8lAT06A H H «J U 4J \J J J ftevteed 12/82M303399
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: .00%LC50: 70.711
95% CONFIDENCE LIMITSARE UNRELIABLE.
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD . DEAD PROB. (%)12.50 10. 0. .00 .9766D-0125.00 10. 0. .00 .9766D-0150.00 10. 0. .00 .9766D-01100.00 10. 10. 100.00 .97660-01
THE BINOMIAL TEST SHOWS THAT 50.00 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.8047 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 70.711
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 12/6/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #2 CATION / EDTA 20mg/L SPECIES: MYSIDOPSIS BAHIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 70.711 50.000 100.000 50.000MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 70.711 ******* ******* *******
**** = LIMIT DOES NOT EXIST
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Reps. 1 -4 Treatments)
//3/Qv/ O-ne y\lc. IPROJECT No.: ASjg" 1 -2- 2-_____ CLIENT:TEST ORGANISM: /Y\\js/of______________ _____' AGE: 2> dayS LOT No.:SAMPLE DESCRIPTION:" ft>r ' ' '~/ ^ ' •' '~ -•SAMPLE No.(s):_LAB MEDIA/NO.: 2. />a+ -~fro*;c./t&r f CONTROL/DILUENT:/-TEST START DATE: IZ-6--?<( TIME: 12- 5" TEST END DATE: /2. -g" - TIME:.ANALYSTS: CT> OygM-g-._______________________ CODE:______________
TREAT;NO.
1
|3
4
scillp:IZ,S7
ZS'/.
££)'/
/OO'/
DATE
REP
A
B
A
B
A
B
A
B
DETERMINED BY
PEfiMPOSUREiiwii'i .'' 'i.:V;. :.«'PERIOD;(Hrs)24 48
6
>
OO00^5"
/z,-?^
TOTALFATALITIES
0
O
O
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0Og-*?
MEANSURVIVAL
**>?.
/OO'£
°2O'i
COMMENTS
COMMENTS:
ft.R.303^01 Revleed 12/82
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: .00%LC50: 70.711
95% CONFIDENCE LIMITSARE UNRELIABLE.
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)12.50 10. 0. .00 .97660-0125.00 10. 0. .00 .97660-0150.00 10. 0. .00 .97660-01100.00 10. 10. 100.00 .9766D-01
THE BINOMIAL TEST SHOWS THAT 50.00 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.8047 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 70.711
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 12/6/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #2 CATION / EDTA 40mg/L SPECIES: MYSIDOPSIS BAHIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 70.711 50.000 100.000 50.000MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 70.711 ******* ******* *******
**** = LIMIT DOES NOT EXIST
AR303W2
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~1S /4Z 3 2-_______ CLIENT: A/o/kyTFST ORGANISM: />7iX<-,V>fTEST ORGANISM: />7yx:<Vg>f____________ __________ AGE: _2± fevS_LOT No.:SAMPLE DESCRIPTION: f%/>_ UJdht*' 3 / & 4 *- / /= <? 7 -SAMPLE No.(s): - "£f - >Z-___________________________'_LAB MEDIA/NO.:Zg r/-7P / Mas',r\________ CONTROL/DILUENT:TEST START DATE: H-tr-fl TIME: J/OO TEST END DATE: /2-fr-^ TIME:ANALYST(s): Xj~-CooJU*—_______________________ CODE:_________________
TREAT.NO.
1
2
br4
5
6
7
TESTSOLUTION
»/.
11.6't,
6y.£oy.joey.
DATE
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Mrs)24
O
O
06
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48
00O
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TOTALFATALITIES
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6
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MEANSURVIVAL
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COMMENTS
Aa303-«*03Form BLATO6
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: .00%LC50: 70.711
95% CONFIDENCE LIMITSARE UNRELIABLE.
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)12.50 10. 0. .00 .97660-0125.00 10. 0. .00 .97660-0150.00 10. 0. .00 .9766D-01100.00 10. 10. 100.00 .9766D-01
THE BINOMIAL TEST SHOWS THAT 50.00 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.8047 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 70.711
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 12/6/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #2 BASE / EDTA lOmg/L SPECIES: MYSISOPSIS BAHIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 70.711 50.000 100.000 50.000MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 70.711 ******* ******* *******
**** = LIMIT DOES NOT EXIST
AR3 031*014
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: 15E.'I4Z*3 Z-______ CLIENT: A/Q/ky £_kg>vi.'cxjTEST ORGANISM: / (/<r/g>f ___________ __________ AGE: _3 /S_LOT No.:SAMPLE DESCRIPTION: PoSt. UJ<& **3 / fi<*£.a- / tSO O /L _______SAMPLE No.(s): £~6>1'&Z- _______________________________LAB MEDIA/No.: Zgyf-"77 y>.V Mecs',*\ ______ .__ CONTROL/DILUENT: L&L. ______ __ ___TEST START DATE: J2.~£-7*/ TIME: // ^ TEST END DATE: /Z>g" / TIME:ANALYSTfs): T Co JUU— ______________________ CODE:
TREAT.NO.
1
2
^4
5
6
7
TESTSOLUTION
oy.IZ-S'/
267
•So'/.
/ooy.
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DATE
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD(Hrs)24 48
O
oO0
o0II.£"^
M-£^
TOTALFATALITIES
0
0
0
OOO
I(£g
MEANSURVIVAL
lOo'J.
iooy.•/ooy.
O'/.
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COMMENTS
[IB 3-0 3-^0 5FormBLAToe Bcvised 12/9?
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER ^
95%95%
CONC. NUMBER% EXPOSED12.50 10.25.00 10.50.00 10.100.00 10.
TRIM:LC50:
LOWER CONFIDENCE:UPPER CONFIDENCE:
NUMBER PERCENTDEAD DEAD
0. .000. .002. 20.0010. 100.00
THE BINOMIAL TEST SHOWS THAT 25.00 ANDSOUND CONSERVATIVE 95LEVEL ASSOCIATED WITHAN APPROXIMATE LC50
PERCENT CONFIDENCETHESE LIMITS IS 99FOR THIS DATA SET IS
.00% ^61.55751.65673.356
BINOMIALPROB. (%).9766D-01.9766D-01.5469D+01.9766D-01
100.00 CAN BE USED AS STATISTICALLYLIMITS SINCE THE ACTUAL CONFIDENCE.8047 PERCENT.
62.190
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 12/6/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #2 BASE / EDTA 20mg/L SPECIES: MYSIDOPSIS BAHIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 62.190 25.000 100.000 75.000MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 61.557 51.656 73.356 21.699
**** = LIMIT DOES NOT EXIST
AR303I*06
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "TSSVflgcJ 2- CLIENT: //Q/J3y C_\*<L™'.C*\TEST ORGANISM: MyZ.'d___________, _________ AGE: 3~ <*y<; LOT No.:SAMPLE DESCRIPTION: Pos*. uJ<& &3 /SAMPLE No.fs): O£. 7.0 T—LAB MEDIA/NO.: 2£ -7 * v. />fo^r\_____ CONTROL/DILUENT:.TEST START DATE: JZ-£-f*/ TIME: I//5C> TEST END DATE: (Z- -7 TIME:.ANALYSTS: U~- Coc/JU^—______________________ CODE:_____________
TREAT.NO.
1
2
*
4
5
6
7
TESTSOLUTION
oy-&&'/•Z6'f.
6-oy.100'f.
DATE
REP
AB
A
B
A
B
A
B
A
B
A
B
A
B
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Hrs)24 48
O0O0OOOO£-^
/l-ffa-
TOTALFATALITIES
0O
00
00O0
£&
MEANSURVIVAL
\oo i
\00'/.
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oy.
COMMENTS
AI3031* 07Form 8LATOO
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: .00%LC50: 70.711
95% CONFIDENCE LIMITSARE UNRELIABLE.
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)12.50 10. 0. .00 .9766D-0125.00 10. 0. .00 .9766D-0150.00 10. 0. .00 .97660-01100.00 10. 10. 100.00 .9766D-01
THE BINOMIAL TEST SHOWS THAT 50.00 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.8047 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 70.711
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 12/6/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #2 BASE / EDTA 40mg/L SPECIES: MYSIDOPSIS BAHIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 70.711 50.000 100.000 50.000MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 70.711 ******* ******* *******
**** = LIMIT DOES NOT EXIST
AR303U08
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~15£ 142.3 Z-________ CLIENT: /te/k/ C_TEST ORGANISM: /^i/lC/^_____________ ._______^__ AGE: ;Way<: LOT No.:SAMPLE DESCRIPTION: Vc. Jo, X / /9 v**~ffV>SAMPLE No.(s):.LAB MEDIA/No.:2 r/-777y/ Mc*s',r\_________ CONTROL/DILUENT:TEST START DATE: JZ-^-fV TIME: IW& TEST END DATE: ]2-<& '7 TIME:.ANALYSTS): -CT- Coc/H*—__________________________ CODE:_________!_____
TREAT.NO.
1
2
L-^3
4
5
6
7
TESTSOLUTION
Q 1
IP-IS'/.12-572S/
&°'f.
I00'{
DATE
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Hrs)24
•
48
&
O
oO
0
o(1oIfvT
/a-?^
TOTALFATALITIES
O
0
0
O
O
O
1
\
0/5"S'
MEANSURVIVAL
)00'/
/&>'/
1007.
%0'/
"107.
OL
COMMENTS
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER fc
95%95%
CONC . NUMBER% EXPOSED6.25 10.12.50 10.25.00 10.50.00 10.100.00 10.
TRIM:LC50:
LOWER CONFIDENCE:UPPER CONFIDENCE:
NUMBER PERCENTDEAD DEAD0. .000. .002. 20.001. 10.0010. 100.00
THE BINOMIAL TEST SHOWS THAT 12.50 ANDSOUND CONSERVATIVE 95LEVEL ASSOCIATED WITHAN APPROXIMATE LC50
PERCENT CONFIDENCETHESE LIMITS IS 99FOR THIS DATA SET IS
• •F-.00%
57.43546.02971.667
BINOMIALPROB. (%).9766D-01.97660-01.5469D+01.1074D+01.97660-01
100.00 CAN BE USED AS STATISTICALLYLIMITS SINCE THE ACTUAL CONFIDENCE.8047 PERCENT.
65.726
I
RESULTS USING MOVING AVERAGESPAN G LC50 95% CONFIDENCE LIMIT2 .215 59.93 45.19 87.75
****** RESULTS CALCULATED BY PROBIT METHODITERATIONS G H GOODNESS OF FIT
8 2.221 2.86 .04
SINCE THE PROBABILITY IS LESS THAN 0.05,RESULTS CALCULATED USING THE PROBIT METHODPROBABLY SHOULD NOT BE USED.
SLOPE = 4.2895% CONFIDENCE LIMITS: -2.10 AND 10.67
LC50= 55.5595% CONFIDENCE LIMITS: 0 AND + INFINITY
LC1 = 15.9095% CONFIDENCE LIMITS: 0 AND 39.11
DATE: 12/6/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #2 AERATION SPECIES: MYSIDOPSIS BAHIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 65.726 12.500 100.000 87.500MAA 59.927 45.193 87.746 42.553
L PROBIT 55.550 ******* ******* ******* II D O f\ O I I nSPEARMAN 57.435 46.029 71.667 25.637 A K 0 U O 4 I U
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Reps. 1-4 Treatments)
PROJECT No.: 7S£~ /4£ Z_ CLIENT: tkllo\fTEST ORGANISM: /fly xld___________________ AGE: ZJay3 LOT No.:SAMPLE DESCRIPTION: P/>re_ U/crfk*-SAMPLE No.(s): JLAB MEDIA/No.: 2-S~ + "T/- / / r,Vi/ CONTROL/DILUENT:/- ^TEST START DATE: IZ-^-^^f TIME: I[&& TEST END DATE: 12. -& -Itf TIME:ANALYSTS: '• C&0&*~~._____________________ CODE:_____________
1
TRE®';::'iN^ ?''•''
1
I'3
4
;: -i ft;SOLUTION
^
7 "
?-5"
DATE
REP
A
B
A
B
A
B
A
B
DETERMINED BY
FATALITIESPEREXPOSUREPERiOD(Hrs)24 48
JT
^
S'jr^S
/1-?///L
TOTALFATALITIES
,rtr&^£r
MEANSURVIVAL
*/
o/.o/.
COMMENTS
¥COMMENTS:
Forni BLAT08A H,J1 O U W T « « Revteed 1ZA»
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~15E I1Z+1 Z-_______ CLIENT: /te/k/ CJ CL '.ccATEST ORGANISM: Myx.'tA________________________ AGE: 3 ay5 LOT No.:SAMPLE DESCRIPTION:.SAMPLE No.(s): s5"&?LAB MEDIA/NO.: 2£ f- 77i*>,v_ />fe.r,v\_______ CONTROL/DILUENT:TEST START DATE: J2.-£-?*/ TIME: )HOO TEST END DATE: /£ -^ "f Y TIME:ANALYSTS: IT-Coc/JUU—______________________ CODE:_________'
TREAT.NO.
1
2
3
4
5
6
7
TESTSOLUTION
$|0
L.ZS-/
\2~sy.2&y.&•/.10 0 /
DATE
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Hrs)24 48
0
0
0
000o6oIS3
A-ff(?/--
TOTALFATALITIES
aO
oO
00O0
o/5-.!>
MEANSURVIVAL
i*>y.levy.ie*t100 '/
9 /
2 2
COMMENTS
j
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
•95%95%
CONC. NUMBER% EXPOSED6.25 10.12.50 10.25.00 10.50.00 10.100.00 10.
SPEARMAN-KARBER
TRIM: 20.00%LC50: 74.300
LOWER CONFIDENCE: 63.046UPPER CONFIDENCE:
NUMBERDEAD0.0.0.1.8.
THE BINOMIAL TEST SHOWS THAT 50SOUND CONSERVATIVE 95LEVEL ASSOCIATED WITHAN APPROXIMATE LC50
PERCENTDEAD
.00
.00
.0010.0080.00
.00 ANDPERCENT CONFIDENCETHESE LIMITSFOR THIS DATA
IS 98SET IS
87.562
BINOMIALPROB. (%).9766D-01.97660-01.9766D-01.10740+01 !.5469D+01
+INFINITY CAN BE USED AS STATISTICALLLIMITS SINCE THE ACTUAL CONFIDENCE.9258 PERCENT.
75.083
RESULTS USING MOVING AVERAGESPAN . G LC50 95% CONFIDENCE LIMIT1 .371 75.08 59.24 102.13
****** RESULTS CALCULATED BY PROBIT METHODITERATIONS G H GOODNESS OF FIT
7 .400 1.00 1.00
SLOPE = 7.0895% CONFIDENCE LIMITS: 2.60 AND 11.56
LC50= 76.0195% CONFIDENCE LIMITS: 57.72 AND 102.16
LC1 = 3 5 . 6 795% CONFIDENCE LIMITS: 9.47 AND 49.99
DATE: 123/6/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #2 AERATION / ZEOLITE SPECIES: MYSIDOPSIS BAHIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 75.083 50.000 ******* *******MAA 75.083 59.243 102.130 42.887PROBIT 76.006 57.723 102.161 44.438SPEARMAN 74.300 63.046 87.562 24.516
*** = LIMIT DOES NOT EXIST
Afl303k I 3
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Reps. 1-4 Treatments)
PROJECT No.: 7Sg" /f<£ _? Z_ ____ CLIENT: //Q /£TEST ORGANISM: /flys.'of_______________________ AGE: LafasS LOT No.:SAMPLE DESCRIPTION: Pore.SAMPLE No.fs : -S£f-02—LAB MEDIA/NO.: 2-s~fo+ /-of, ..... s_____ __.....___.___...._TEST START DATE: IZ-£-?*f TIME: MOO TEST END DATE: /2--&-?tf TIME:ANALYST(s):_3_JL^2^±==_____________________ CODE:.
TREAT,NO.
1
2
3
4
TESTSOLUTION
|2.5/.
Z5/
/
l*>'/.
REP
A
B
A
B
A
B
A
B
DATEDETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Hrs)24 48
00OO
IJ
.rj-M-5-ff*.
TOTALFATALITIES
a
<9>
O
0
f
J>
rr
.MEANSURVIVAL
tooltc*>lbfi/.0{
COMMENTS
j
COMMENTS:
FomBLATOCA ...... R«(«d 12»2
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
95%95%
CONC. NUMBER% EXPOSED12.50 10.25.00 10.50.00 10.100.00 10.
SPEARMAN-KARBER
TRIM: .00%LC50: 53.589
LOWER CONFIDENCE: 43.232UPPER CONFIDENCE:
NUMBERDEAD0.0.4.10.
THE BINOMIAL TEST SHOWS THAT 25SOUND CONSERVATIVE 95LEVEL ASSOCIATED WITHAN APPROXIMATE LC50
PERCENTDEAD
.00
.0040.00100.00
.00 AND
66.427
BINOMIALPROB. (%).9766D-01.9766D-01.3770D+02.9766D-01
100.00 CAN BE USED ASPERCENT CONFIDENCE LIMITS SINCE THE ACTUALTHESE LIMITSFOR THIS DATA
IS 99.SET IS
8047 PERCENT.54.594
STATISTICALLYCONFIDENCE
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 12/6/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #2 AERATION / EDTA lOmg/LSPECIES: MYSIDOPSIS BAHIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 54.594 25.000 100.000 75.000MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 53.589 43.232 66.427 23.195
**** = LIMIT DOES NOT EXIST
AH3034I5
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Reps. 1 -4 Treatments)
//3 /bPROJECT No.: TSg" /fZ Z, _____ CLIENT: 3_____TEST ORGANISM: /HysM _______________________ AGE: 2ka(a3 LOT No.: A T fSAMPLE DESCRIPTION: P/>re- USdftt X. / / x >t -*,W /SAMPLE No.(s): 'LAB MEDIA/No.: 2-)a+ "T^o^/r^ CONTROL/DILUENT:TEST START DATE: 12-4--^^ TIME: HQO TEST END DATE: /2- -&'ANALYSTS: CT- Co<?lf^~^.________________________ CODE:
TREAT.NO.
1
2
3
4
TESTSOLUTION
/ 5/
5/r5»/
W{.
REP
A
B
A
B
A
B
A
B
DATE
DETERMINED BY
FATALITIESPER EXPOSUREPERIOD (Hrs)24 48
O000
O0<rs~
l?>~Kfo
TOTALFATALmES
OO
0&
0O
£-^
MEANSURVIVAL
/OO/.
IOO'/.
100 /.
°t
COMMENTS
COMMENTS:
FoonBtATOaA AR303M6
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
^ SPEARMAN-KARBER
TRIM: .00%LC50: 70.711 ,
95% CONFIDENCE LIMITSARE UNRELIABLE. :
CONC. NUMBEREXPOSED
12.5025.0050.00100.00
10.10.10.10.
NUMBERDEAD0.0.0.10.
THE BINOMIAL TEST SHOWS THAT 50SOUND CONSERVATIVE 95LEVEL ASSOCIATEDAN APPROXIMATE
WITHLC50
PERCENTDEAD
.00
.00
.00100.00
.00 ANDPERCENT CONFIDENCETHESE LIMITSFOR THIS DATA
IS 99SET IS
BINOMIALPROB. (%).97660-01.9766D-01.97660-01.97660-01
100.00 CAN BE USED ASLIMITS SINCE THE ACTUAL.8047 PERCENT.
70.711
STATISTICALLYCONFIDENCE
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 12/6/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #2 AERATION / EDTA 20mg/LSPECIES: MYSIDOPSIS BAHIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 70.711 50.000 100.000 50.000MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 70.711 ******* ******* *******
**** = LIMIT DOES NOT EXIST ;
AR303M7
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Reps. 1 -4 Treatments)
PROJECT No.: /-S m-<L<2 Z______ CLIENT: ______TEST ORGANISM: /71y <;.'<?(______________ AGE: 'Z.J.av-S LOT No.: A 7~ fSAMPLE DESCRIPTION: Porc-SAMPLE No.(s):_LAB MEDIA/NO.: 2.g~/)6+ ifcWc- /n*r:*l_____ CONTROL/DILUENT:TEST START DATE: IZ-£-f*/' TIME: JH0& TEST END DATE: /2.-g"-W TIME:.ANALYST^: CT"* O<?M<-,_______________________ CODE:______________
TREAT.NO.
1
2
3 '
4
TESTSOLUTION
;a-s*is/.&oy.loo/
REP
A
B
A
B
A
B
A
B
DATEDETERMINED BY
FATALITIESPER EXPOSURE
' PERlOD:(Hrs)24 48
o0o0
0o5"S
\i~-«(tL
TOTALFATALmES
O
O
O
O
Oo^f
MEANSURVIVAL
iooy.IW{
10 O'/
o/.
COMMENTS
\
I
COMMENTS:
FwmBlATOCA « 11 W W U "T I W Rcvte«<l 12A»A-R303M8
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER '. :
™ TRIM: .00% ;LC50:
95% LOWER CONFIDENCE:95% UPPER CONFIDENCE:
61.55751.65673.356 !
1 -
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD6.25 10. 0. .0012.50 10. 0. .0025.00 10. 0. .0050.00 10. 2. 20.00100.00 10. 10. 100.00
THE BINOMIAL TEST SHOWS THAT 25.00 ANDSOUND CONSERVATIVE 95 PERCENT CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99AN APPROXIMATE LC50 FOR THIS DATA SET IS
PROB. (%).9766D-01.97660-01 ;.97660-01.54690+01.97660-01
100.00 CAN BE USED ASLIMITS SINCE THE ACTUAL.8047 PERCENT.
62.190
STATISTICALLYCONFIDENCE
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 12/6/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #2 AERATION / CATION SPECIES: MYSIDOPSIS BAHIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 62.190 25.000 100.000 75.000MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 61.557 51.656 73.356 21.699 I
**** = LIMIT DOES NOT EXIST ]
AB303k21
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(4 Reps. 1-7 Treatments)
TEST ORCSAMPLE [SAMPLE rLAB MEDITEST STAANALYST
|l$i!?fllifl|:
llfiiliS
1!11'•Y-T'xSx' ; -:,• .;•'•'••":•
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'•-'•',• '',',• ' ;'• '''',••' -'v ' '•'
IS-.O:'
U*4g :
3 AN ISM: {msj ipClaph+Li+. «£•«•£-**-DESCRIPTION: ' /V1*. U/ f ~ *
AGE: - V/ LOT No.: J6.J* ? ^^. /- v / Te**—
o.(s): J5~6>?J?1A/No.: £—<*/[ i~t*<r*< — t** -*(ft-RTDATE: /f-fi.9tf TIME: / / "(s): Tl CLcfrlVU.
CONTROL/DILUENT: 1 *4? +r,'*TEST END DATE:_1/- Z-/-?*/ TIME: //7C>«
CODE:
\ ;';i' '>:>:'!;:;i;:::;i-i'i' ;;;-iv '•;•*$!' i'ivi- !•:•:•:•;•:':•' '•:•! •;::::':' : : .;;;:• ' • '•' • \ttf'_ '!j'iivf'r':':''y:':':':'' ' ';:;:'': '•••'•••••••••••' | •T~' ?:f ::::,v!::vi:i-:':::;i:::•-;.'':->' ;';i;';i;''M'/:' .•.'."•:•:-.•;-;:;;:;;;;:•>"•";;;-'•:•;;;':•
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illlllll
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-
M303l»23Rxm BLATtO / ' Revised 12/82
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER k
95%95%
CONC. NUMBER% EXPOSED
6.25 20.12.50 20.25.00 20.50.00 20.100.00 20.
TRIM:LC50:
LOWER CONFIDENCE:UPPER CONFIDENCE:
NUMBER PERCENTDEAD DEAD0. .000. .007. 35.0020. 100.0020. 100.00
THE BINOMIAL TEST SHOWS THAT 12.50 ANDSOUND CONSERVATIVE 95LEVEL ASSOCIATED WITHAN APPROXIMATE LC50
PERCENT CONFIDENCETHESE LIMITS IS 99FOR THIS DATA SET IS
- ^.00%
27.73923.92732.159
BINOMIALPROB. (%).95370-04.9537D-04.13160+02.9537D-04.95370-04
50.00 CAN BE USED AS STATISTICALLYLIMITS SINCE THE ACTUAL CONFIDENCE.9998 PERCENT.
28.259
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 11/19/94 TEST NUMBER: 1 DURATION: 48 HOURSSAMPLE: PORE "WATER #3 SPECIES: CERIODAPHNIA dubia
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 28.259 12.500 50.000 37.500MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 27.739 23.927 32.159 8.233
**** = LIMIT DOES NOT EXIST
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~7S£' / Z.J Z- CLIENT: //G /A y C\ * /'c (______TEST ORGANISM: C ' f " ''<=- a th.' - ' AGE: - V LOT No.:SAMPLE DESCRIPTION:.SAMPLE No.(s):.LAB MEDIA/NO.: <*,w*- *w .x._____ CONTROL/DILUENT:TEST START DATE: H-If-f^ TIME: / # TEST END DATE: (/-Z~S-fy TIME:ANALYSTS): <T <^e»^i<-_______________________ CODE:
f.-.B:,
soy.so*'/
0
0
0 7007\i.sy. ———————°-
&s•/.
o/.
DATEDpnERMINEDBY
11-23
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
95%95%
CONC. NUMBER% EXPOSED6.25 10.12.50 10.25.00 10.50.00 10.100.00 10.
TRIM:LC50:
LOWER CONFIDENCE:UPPER CONFIDENCE:
NUMBER PERCENTDEAD ' DEAD0. .001. 10.001. 10.009. 90.0010. 100.00
THE BINOMIAL TEST SHOWS THAT 25.00 ANDSOUND CONSERVATIVE 95LEVEL ASSOCIATED WITHAN APPROXIMATE LC50
PERCENT CONFIDENCETHESE LIMITS IS 97FOR THIS DATA SET IS
.00%32.98826.26841.427
BINOMIALPROB. (%).9766D-01.10740+01.10740+01.1074D+01.9766D-01
50.00 CAN BE USED AS STATISTICALLYLIMITS SINCE THE ACTUAL CONFIDENCE.8516 PERCENT.
35.355
RESULTS USING MOVING AVERAGESPAN G LC50 95% CONFIDENCE LIMIT4 .114 31.33 22.95 45.36
****** RESULTS CALCULATED BY PROBIT METHODITERATIONS G H GOODNESS OF FIT
7 .256 1.00 .19
SLOPE =4.8295% CONFIDENCE LIMITS: 2.38 AND 7.27
LC50= 31.9795% CONFIDENCE LIMITS: 23.51 AND 43.50
LC1 =10.5395% CONFIDENCE LIMITS: 3.19 AND 16.24
DATE: 11/21/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #3 BASELINE SPECIES: CERIODAPHNIA dubia
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 35.355 25.000 50.000 25.000MAA 31.334 22.948 45.357 22.409
yLPROBIT 31.967 23.513 43.497 19.984SPEARMAN 32.988 26.268 41.427 15.159
**** = LIMIT DOES NOT EXIST
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
-: "73 /qZ.3 2- CLIENT: //ct/A./HSM: ( o .'sirLbahr,; fiLch:*
PROJECT No.TEST ORGANISM: Co fL h ; fiU<h: ______'__ AGE: <£-2XW- LOT No.:SAMPLE DESCRIPTION: _________ }/-.5f f/t i— /" FSAMPLE No.s:LAB MEDIA/NO.: c-u/u-. >v.'v. _____ CONTROL/DILUENT:TEST START DATE: H-ll-lH TIME: /OOf TEST END DATE: //-Z~5-ftf TIME:ANALYSTS: <Tx C^olL\<_______________________ CODE:
'N0; ;
oa 00 O
0
o oo
So/. o
DATEDETERMINED BY
Prwm fU ATO«
u-v
fl.R303i4.27
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER £|
95%95%
CONC. NUMBER% EXPOSED12.50 10.25.00 10.50.00 10.100.00 10.
TRIM:LC50:
LOWER CONFIDENCE:UPPER CONFIDENCE:
NUMBER PERCENTDEAD DEAD0. .001. 10.000. .0010. 100.00
THE BINOMIAL TEST SHOWS THAT 50.00 ANDSOUND CONSERVATIVE 95LEVEL ASSOCIATED WITHAN APPROXIMATE LC50
PERCENT CONFIDENCETHESE LIMITS IS 99FOR THIS DATA SET IS
.00%65.97557.63775.520
BINOMIALPROB. (%).97660-01.10740+01.97660-01.97660-01
100.00 CAN BE USED ASLIMITS SINCE THE ACTUAL.8047 PERCENT.
70.711
^
STATISTICALLYCONFIDENCE
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 11/21/94 TEST NUMBER: HALBY DURATION: 48 HSAMPLE: #3 EDTA 10 SPECIES: CERIODAPHNIA DUBIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 70.711 50.000 100.000 50.000MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 65.975 57.637 75.520 17.883
NOTE: MORTALITY PROPORTIONS WERE NOT MONOTONICALLY INCREASING.ADJUSTMENTS WERE MADE PRIOR TO SPEARMAN-KARBER ESTIMATION.
**** = LIMIT DOES NOT EXIST
HR303U28
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "7 " / - 2- CLIENT: //Q / A./ C ^ i / C<v (TEST ORGANISM: C o*-:nfL*0lir, ; rtUtb:< . ' AGE: Z4fr LOT No.: -3 &3 . "75"SAMPLE CSAMPLE hLAB MEDITEST STAANALYST!
11t2
^3 '
4
5
6
7
)ESCRIPTION:Jo.fs): &<r.
(3cSi.Ji'KA_ f&VrA- 2J>*yK.-0$ ' "
A/No.: Cc<'/-/w> <_ /ws f.X CONTROL/DILUENT: ^ /»v W',VRTDATE: H-i/-^ TIME: /O /<? TEST END DATE: //-W-5^ TIME: /#</£>'Sjl TxCje A/*.
,'i
ftl13.-5/.
XSX
So/
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' FIF*P •'•'•'•1 • *^ ''r':;::
,.:.:; ",.i.;:&;
A. •'. ;
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A
. :£
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A
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A
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A
Br .-"——— -
DETERMINED BY
lilftiiiiii|;i':;ii;i:ii?i:;s! .>.,;.• !&. •"•:..•;;
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O
CODE:
illoo0oooo0oo
1007.
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'•
4R'3-03«#2'9
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "7 " /tfZ.3 2- CLIENT: //Q / A,, Ghj> ~ /C* (_____TEST ORGANISM: Cc r tLtfkr, ;*. tTUb:* ' .AGE: -Z ff- LOT No.: 36-3. 79-SAMPLE DESCRIPTION:.SAMPLE No.(s):_LAB MEDIA/NO.: <*,wj<— **»*•*._______ CONTROL/DILUENT.-TEST START DATE: ll-lf-^ TIME: lO/g' TEST END DATE: U-l -'i TIME:ANALYST(s): -CT% <^a^f<.________________________ CODE:
TREAT;NO.
1
2
3
4
5
6
7
TESTSOLUTION
(2)*XV
U-57,
as1/
go/
/oo/.
REP
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DATE
DETERMINED BY
::'-;::;-;:PAlAlllTIES:::'5V;;:;:BERiiEkPOSURE
':;'iaERilG)D.i:{Hrs)x::'.j,:":24" ;.:.:: 48
JyoO0oo0
r&
d'Ufa
• ;;TppMu,sFJ i|riiES;?
/(0000o0
jrS
MEANSUR I L;
9/oo
/oo/.!UU'/.
o/
COMMENTS
|'«
R.B303lt30FonneLATOfl
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER :
TRIM: .00%LC50: 70.711
95% CONFIDENCE LIMITSARE UNRELIABLE.
I
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)12.50 10. 0. .00 * .97660-0125.00 10. 0. .00 .9766D-0150.00 10. 0. .00 .9766D-01100.00 10. 10. 100.00 .9766D-01
THE BINOMIAL TEST SHOWS THAT 50.00 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.8047 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 70.711
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 11/21/94 TEST NUMBER: HALBY DURATION: 48 H.SAMPLE: #3 EDTA 40 SPECIES: CERIODAPHNIA DUBIA
METHOD LC50 CONFIDENCE LIMITS ILOWER UPPER SPAN
BINOMIAL 70.711 50.000 100.000 50.000MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 70.711 ******* ******* *******
i
**** = LIMIT DOES NOT EXIST
483031*31
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "73 /tyZ-J 2L CLIENT: //Q / A y C-h e — » /Co> ( ______TEST ORGANISM: o )o6?/ !< vU : ' AGE: -Z ff- LOT No.:SAMPLE DESCRIPTION:______S/CV>*-S p Jf- O-o(jt*.s+-SAMPLET ' • "—* '"LAB MEDIA/No.: C<W4w~— nW.y. CONTROL/DILUENT:,TEST START DATE: 7/-£/-«/*/ TIME: fO2o TEST END DATE: I f - Z>i-*> y TIME:.ANALYSTfs): -3~, C^xok,^______________________ CODE:_____________
TREATv-'.Np;r::;;
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4
5
6
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A
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A
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A
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A
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A
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Form BtATOfl
ICH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "T g" /tt? .3 2- CLIENT: //ft /k./ C- JL /Co- (TFST ORGANISM: C 0 -*A<xOl>ir, :< d b.' ' AGE: -Z ft- LOT No.: -J£-3 . "75'-SAMPLE CSAMPLE LAB MEDITEST STAANALYST
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CH2M HILL Milwaukee Bioassay Laboratory
4S-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "73 " /Z.,3 2- CLIENT: //ft /k,, Ol j—L /C<» (TEST ORGANISM: c^'^fi^ Ax. 0<,:<^ AGE: < -Z ft- LOT No.:SAMPLE DESCRIPTION:SAMPLE No.fel: .LAB MEDIA/NO.: <^wj— »vx.'^ CONTROUDILUENT.-TEST START DATE: 1 1- &/-**( TIME: /^J Q TEST END DATE: It-Z-t-'iy TIME:ANALYSTfs): T/gLag/fcl . _______________________ CODE:
TREAT.NO. ;
1
2
3
4
5
6
7
TESTSOLUTION ;
MuK
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l&oy
DATE
2A.- ::
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A
B
A
B
AB
A
B
A
B
A
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CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: .00% "—LC50: 70.711
95% CONFIDENCE LIMITSARE UNRELIABLE.
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)6.25 10. 0. .00 .9766D-0112.50 10. 0. .00 .97660-0125.00 10. 0. .00 .97660-0150.00 10. 0. .00 .9766D-01100.00 10. 10. 100.00 .9766D-01 !
THE BINOMIAL TEST SHOWS THAT 50.00 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.8047 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 70.711
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVE !ANY STATISCALLY SOUND RESULTS.
DATE: 11/21/94 TEST NUMBER: HALBY DURATION: 48 HSAMPLE: #3 ZEOLITE SPECIES: CERIODAPHNIA DUBIA
METHOD LC50 CONFIDENCE LIMITS :LOWER UPPER SPAN
BINOMIAL 70.711 50.000 100.000 50.000MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 70.711 ******* ******* *******
**** = LIMIT DOES NOT EXIST
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No,: "7 ~ / Z,J? Z- CLIENT: //Q / k . / C-ln* — i /C<» (TEST ORGANISM: Co .'rtfkxplir,; <iU<L>: ' AGE: -Z tt- LOT No.: -J^JSAMPLE DESCRIPTION: _________ Z.<2a f/'-U-SAMPLE No.(s):. -LAB MEDIA/NO.: C<*,(4us-j- >w.'. CONTROL/DILUENT:TEST START DATE: II-I/-W TIME: /O fT TEST END DATE: U-^-f^ TIME:ANALYSTS): Tx<^=«^i<-_________________________ CODE'
TREAT,NO.
1
2
3
4
5
6
7
TESTSOLUTION
fl~*n
12.57.?57
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REP:
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DATEDETERMINED BY
;::O?C:.:.:,;: ..""48; ',.
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COMMENTS
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER 7__
TRIM: 50.00% . __"LC50: 100.000
95% CONFIDENCE LIMITSARE UNRELIABLE.
1
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)6.25 10. 0. .00 .9766D-0112.50 10. 0. .00 .9766D-0125.00 10. 3. 30.00 .17190+0250.00 10. 0. .00 .97660-01100.00 10. 5. 50.00 .62300+02
THE BINOMIAL TEST SHOWS THAT 12.50 AND +INFINITY CAN BE USED AS STATISTICALLSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.9023 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 100.000
THE MOVING AVERAGE METHOD CANNOT BE USED WITHTHIS DATA SET BECAUSE NO SPAN WHICH PRODUCESAVERAGE ANGLES BRACKETING 45 DEGREES ALSO USESTWO PERCENT DEAD BETWEEN 0 AND 100 PERCENT.
NO CONVERGENCE IN 25 ITERATIONS. PROBIT METHODPROBABLY CAN NOT BE USE WITH THIS SET OF DATA.
DATE: 11/21/94 TEST NUMBER: HALBY DURATION: 48 HSAMPLE: #3 ZEOLITE/AIR SPECIES: CERIODAPHNIA DUBIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 100.000 12.500 ******* *******MAA ******* ******* ******* ******* :
PROBIT ******* ******* ******* *******SPEARMAN 100.000 ******* ******* *******
NOTE: MORTALITY PROPORTIONS WERE NOT MONOTONICALLY INCREASING.ADJUSTMENTS WERE MADE PRIOR TO SPEARMAN-KARBER ESTIMATION.
**** = LIMIT DOES NOT EXIST
AH 3-0.3 « 7
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
TEST ORGANISM: C o*-:s>Aj>0hr, ;<x_ rLcJn .' ' AGE: <*-Z~4tt- LOT No.: 36,3 . &79-SAMPLE CSAMPLE NLABMEDITESTSTAANALYST(
TREAT,NO.
1
2
3
4
5
6
7
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DATE
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DETERMINED BY
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COMMENTS
AB303U38
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~~73£~ /U? .3 2_ CLIENT: //a/h, (Zhj — t/c<y(TEST ORCSAMPLE CSAMPLE rLAB MEDITESTSTAANALYST
Tii1
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03
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CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "73 " /2..3 2- CLIENT: J4c. / kTEST ORGANISM: Co r fko&hr,; r£c<h:< l AGE: -Z H- LOT No.: -J^-3.SAMPLE DESCRIPTION: ______ Z. g-7 / / -h*- / 0 T/3-SAMPLE No.fs): ~LAB MEDIA/NO.: CW-/W.*- »w .x, CONTROL/DILUENT:TEST START DATE: //- ll-W TIME: /O^ o TEST END DATE: U-Z^-f^ TIME:.ANALYST(s): -3~,Cj*ok,\-L._______________________ CODE:_____________
TREAT,NO.
1
2
3
4
5
6
7
TESTSOLUTION
/m
TS'f.
£or[t
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DATE
REP
A
B
A
9
AB
A
B
A
B
A
B
A
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DETERMINED BY
; "REiti|fkN2)SURE
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COMMENTS
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CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: iS /UZ.3 2- CLIENT:TPST ORGANISM: Co . A li ;&. fjitJn .'« ' AGE: <Z-Z4tf- LOTNo.:-J£3, *S~7S>-SAMPLE CSAMPLE LAB MEDITEST STAANALYST
TREATSNO,
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1
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4
5
6
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DESCRIPTION: " «=L««///-t_ / / a--f /owJo. : 1 -03A/No.: CcW4«/'vi— *w C.X..RTDATE: fl-lf-fif TIME:(s): - r~'O=>fTO-l<- . .... _
•TEST:': .'.: SQLUTIO I ::
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FotmBLATOeftI303l^
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: .00%LC50: 70.711
95% CONFIDENCE LIMITSARE UNRELIABLE.
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)
6.25 10. 0. .00 .97660-0112.50 10. 0. .00 .9766D-0125.00 10. 0. .00 .97660-0150.00 10. 0. .00 .97660-01100.00 10. 10. 100.00 .97660-01
THE BINOMIAL TEST SHOWS THAT 50.00 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.8047 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 70.711
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 11/21/94 TEST NUMBER: HALBY DURATION: 48 HSAMPLE: #3 ZEOLITE/CATION SPECIES: CERIODAPHNIA DUBIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 70.711 50.000 100.000 50.000MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 70.711 ******* ******* *******
**** = LIMIT DOES NOT EXIST
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~7S£ /4Z..3 Z- CLIENT: //ct / A., CA) —i /C<v (TEST ORGANISM: Co . rL h ; rtUth: ' AGE: Z- /A LOT No.: -3 3 . ^ 75"SAMPLE CSAMPLE LAB MEDI
ASCRIPTION:Jo.(s): -S~G>$ .
U ^^a •f/<yy-\_ '<£?1
A/No.! CW4wrjc- >vus/.\_ CONTROL/DILUENT: £>*6 * *//X_TEST START DATE: H-Zl-W TIME: I/&O TEST END DATE: //-W--?y TIME: l)3>OANALYSTrsV-a'xr l CODE:
TS'.". '"': ';.; "
1
2
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AA303M3
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER ^
TRIM: 20.00% ^LC50: 41.243
95% LOWER CONFIDENCE: 22.63895% UPPER CONFIDENCE: 75.140
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD
6.25 10. 2.12.50 10. 4.25.00 10. 2.50.00 10. 4.100.00 10. 10.
THE BINOMIAL TEST SHOWS THATSOUND CONSERVATIVE 95 PERCENT
. DEAD PROB.(%)20.00 .5469D+0140.00 .37700+0220.00 .54690+0140.00 .3770D+02100.00 .9766D-01
.00 AND 100.00 CAN BE USED ASCONFIDENCE LIMITS SINCE THE ACTUAL
STATISTICALLYCONFIDENCE
LEVEL ASSOCIATED WITH THESE LIMITS IS 99.9023 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 54.594
RESULTS USING MOVING AVERAGESPAN G LC50 95% CONFIDENCE LIMIT4 .215 31.39 20.30 54.99
****** RESULTS CALCULATED BY PROBIT METHODITERATIONS G H GOODNESS OF FIT
5 2.789 2.77 .04
SINCE THE PROBABILITY IS LESS THAN 0.05,RESULTS CALCULATED USING THE PROBIT METHODPROBABLY SHOULD NOT BE USED.
SLOPE = 1.5195% CONFIDENCE LIMITS: -1.01 AND 4.03
LC50= 32.1395% CONFIDENCE LIMITS: 0 AND + INFINITY
LC1 = .9295% CONFIDENCE LIMITS: 0 AND 9.47
DATE: 11/21/94 TEST NUMBER: HALBY DURATION: 48 HSAMPLE: #3 CATION SPECIES: CERIODAPHNIA DUBIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 54.594 .000 100.000 100.000MAA 31.393 20.302 54.988 34.686PROBIT 32.126 ******* ******* *******SPEARMAN 41.243 22.638 75.140 52.502
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~73fe~/#Z.J2_ CLIENT: //«/A,y CA /Cd-lTEST ORCSAMPLE CSAMPLE f>LAB MEDITESTSTAANALYST
TH1
2
f'4
5
6
7
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A/No.: Cc*(4wJ— »v/.X. CONTROL/DILUENT: £>?£ /» W/V-RTDATE: ll-ll-ty TIME: ll Off TEST END DATE: //-2-4-*</ TIME: 'l3*T~[s): <Tx CL&e>lL\4~
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CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: .00%LC50: 70.711
95% CONFIDENCE LIMITSARE UNRELIABLE.
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)
6.25 10. 0. .00 .9766D-0112.50 10. 0. .00 .97660-0125.00 10. 0. .00 .9766D-0150.00 10. 0. .00 .97660-01100.00 10. 10. 100.00 .9766D-01
THE BINOMIAL TEST SHOWS THAT 50.00 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.8047 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 70.711
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 11/21/94 TEST NUMBER: HALBY DURATION: 48 HSAMPLE: #3 CATION/ZEOLITE SPECIES: CERIODAPHNIA DUBIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 70.711 50.000 lOO'.OOO 50.000MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 70.711 ******* ******* *******
**** = LIMIT DOES NOT EXIST
ICH2M HILL Milwaukee Bioassay Laboratory
A 48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "73 £" / Z.J 2- CLIENT: //o/A,TEST ORGANISM: Co . rLtfhr, rttuh:* ' AGE: -Z tti- LOT No.: J £3 . 7&-SAMPLE CSAMPLE rLAB MED!TESTSTAANALYST
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CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: .00%LC50: 50.000
95% LOWER CONFIDENCE: 37.67795% UPPER CONFIDENCE: 66.354
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)
6.25 10. 0. .00 .9766D-0112.50 10. 2. 20.00 .5469D+0125.00 10. 2. 20.00 .5469D+0150.00 10. 1. 10.00 .1074D+01100.00 10. 10. 100.00 .97660-01
THE BINOMIAL TEST SHOWS THAT 6.25 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.8047 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 65.726
RESULTS USING MOVING AVERAGESPAN G LC50 95% CONFIDENCE LIMIT2 .215 59.93 45.19 87.75
****** RESULTS CALCULATED BY PROBIT METHODITERATIONS G H GOODNESS OF FIT
5 2.946 4.05 .01
SINCE THE PROBABILITY IS LESS THAN 0.05,RESULTS CALCULATED USING THE PROBIT METHODPROBABLY SHOULD NOT BE USED.
SLOPE = 2.4395% CONFIDENCE LIMITS: -1.74 AND 6.60
LC50= 51.6295% CONFIDENCE LIMITS: 0 AND + INFINITY
LC1 = 5.7095% CONFIDENCE LIMITS: 0 AND 25.76
DATE: 11/21/94 TEST NUMBER: HALBY DURATION: 48 HSAMPLE: #3 CATION/AIR SPECIES: CERIODAPHNIA DUBIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 65.726 6.250 100.000 93.750MAA 59.927 45.193 87.746 42.553PROBIT 51.619 ******* ******* *******SPEARMAN 50.000 37.677 66.354 28.677
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CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~^ X Z.3 ZL CLIENT: //Q /fr y Ol j ^ /Ct* ( ___________TEST ORGANISM: Ce .'aehxplir,; f?Uch: ' AGE: -Z H- LOT No.: 3 6>3 .SAMPLE DESCRIPTION:_______Cg+.'a /SAMPLE No.fs : "LAB MEDIA/NO.: c H /-.*-- »v\^x.^________ CONTROL/DILUENT:.TEST START DATE: H-M-tV TIME: //A5" TEST END DATE: //ANALYSTfs): <T^ ag/fci<_________________________ CODE:
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CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~ S /JJ2..3, 2- CLIENT: //g / Ay Cke~ /C<v(TEST ORGANISM: C cur.'aAe&hr, ;<~. aLcdj:*.SAMPLE DESCRIPTION: " C i'oi ) £SAMPLE No.fs): v£T&?.aJLAB MEDIA/NO.: C< 4«rj«— *w .xTEST START DATE: }\-Zl-em TIME: // 2 OANALYSTS): -CTx < ac»yfcl<_
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ICH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~73 " /#Z.J?Z- CLIENT: //Q/A,> Ck*x /C<v(TEST ORGANISM: C o r.'achxphr, ; tfUih: ' AGE: <£-Z fff- LOT No.: -3 3. "75SAMPLE DESCRIPTION: U Crt.-A/0-v-v &O7~A. "Z& /L-SAMPLE hLAB MEDITEST STAANALYSTj
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CT-TOX: BINOMIAL, MOVING AVERAGE, PROSIT, AND SPEARMAN METHODS
SPEARMAN-KARBER ^
TRIM: 20.00% ^LC50: 77.111
95% CONFIDENCE LIMITSARE UNRELIABLE.
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD12.50 10. 0.25.00 10. 0.50.00 10. 0.100.00 10. 8.
THE BINOMIAL TEST SHOWS THATSOUND CONSERVATIVE 95 PERCENT
DEAD PROB. (%).00 .97660-01.00 .97660-01.00 .97660-01
80.00 .5469D-K31
50.00 AND +INFINITY CAN BE USED AS STATISTICAL!CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCE
LEVEL ASSOCIATED WITH THESE LIMITS IS 99.9023 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 80.399
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 11/21/94 TEST NUMBER: HALBY DURATION: 48 HSAMPLE: #3 CATION/EDTA20 SPECIES: CERIODAPHNIA DUBIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 80.399 50.000 ******* *******MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 77.111 ******* ******* *******
**** = LIMIT DOES NOT EXIST
AR30H52
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: " !•$& /4Z.J2- CLIENT: //Q / A,, Chj~~ ,'c*(TEST ORGANISM: Co . L h / rtUth:< ' AGE: <£-Z H- LOT No.: -5<i . <5~ 75SAMPLE CSAMPLE h
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SPEARMAN-KARBER ^
95%95%
CONC. NUMBER% EXPOSED12.50 10.25.00 10.50.00 10.100.00 10.
TRIM:LC50:
LOWER CONFIDENCE:UPPER CONFIDENCE:
NUMBER PERCENTDEAD , DEAD0. .002. 20.001. 10.009. 90.00
THE BINOMIAL TEST SHOWS THAT 12.50 ANDSOUND CONSERVATIVE 95LEVEL ASSOCIATED WITHAN APPROXIMATE LC50
PERCENT CONFIDENCETHESE LIMITS IS 98FOR THIS DATA SET IS
10.00%65.78550.66585.418
BINOMIALPROB. (%).9766D-01.5469D+01.1074D+01.1074D+01
100.00 CAN BE USED AS STATISTICALLYLIMITS SINCE THE ACTUAL CONFIDENCE.8281 PERCENT.
70.711
RESULTS USING MOVING AVERAGESPAN G LC50 95% CONFIDENCE LIMIT2 .371 70.71 49.05 153.35
****** RESULTS CALCULATED BY PROBIT METHODITERATIONS G H GOODNESS OF FIT
5 4.805 3.07 .05
SINCE THE PROBABILITY IS LESS THAN 0.05,RESULTS CALCULATED USING THE PROBIT METHODPROBABLY SHOULD NOT BE USED.
SLOPE = 3.6295% CONFIDENCE LIMITS: -4.31 AND 11.55
LC50= 61.5595% CONFIDENCE LIMITS: 0 AND + INFINITY
LC1 = 14.0095% CONFIDENCE LIMITS: 0 AND 49.36
DATE: 11/21/94 TEST NUMBER: HALBY DURATION: 48 HSAMPLE: #3 CATION/EDTA 40 SPECIES: CERIODAPHNIA DUBIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 70.711 12.500 100.000 87.500MAA 70.711 49.053 153.352 104.300PROBIT 61.546 ******* ******* *******SPEARMAN 65.785 50.665 85.418 34.752
, AR 3-0 31» 51*
CH2M HILL Milwaukee Bioassay Laboratory i
46-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "73 / Z.J? 2- CLIENT: //o (ky C- j ^ /c*v(
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CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: 20.00%LC50: 16.494
95% LOWER CONFIDENCE: 9.83195% UPPER CONFIDENCE: 27.673
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)
6.25 10. 2. 20.00 .5469D4-0112.50 10. 5. 50.00 .6230D+0225.00 10. 5. 50.00 .6230D+0250.00 10. 10. 100.00 .9766D-01100.00 10. 10. 100.00 .9766D-01
THE BINOMIAL TEST SHOWS THAT .00 AND 50.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.9023 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 17.678
RESULTS USING MOVING AVERAGESPAN G LC50 95% CONFIDENCE LIMIT3 .215 15.55 9.94 22.67
****** RESULTS CALCULATED BY PROBIT METHODITERATIONS G H GOODNESS OF FIT
6 .239 1.00 .27
SLOPE =2.6295% CONFIDENCE LIMITS: 1.34 AND 3.90
LC50= 14.6995% CONFIDENCE LIMITS: 8.82 AND 21.84
LC1 = 1.9095% CONFIDENCE LIMITS: .21 AND 4.21
DATE: 11/21/94 TEST NUMBER: HALBY DURATION: 48 HSAMPLE: #3 AERATION SPECIES: CERIODAPHNIA DUBIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 17.678 .000 50.000 50.000MAA 15.547 9.937 22.674 12.736PROBIT 14.688 8.816 21.840 13.024SPEARMAN 16.494 9.831 27.673 17.842
**** = LIMIT DOES NOT EXIST
A.R303lf56
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.:TEST ORGANISM:SAMPLE DESCRIPTION:SAMPLE No.(s):__,,LAB MEDIA/NO.: -.*-- *vus.x.. CONTROL/DILUENT:TEST START DATE: H-ll-W TIME: 1/3 TEST END DATE: K- -'i TIME:
._____________________ CODE:
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CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER jj
TRIM: .00%LC50: 20.306
95% LOWER CONFIDENCE: 14.05395% UPPER CONFIDENCE: 29.342
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD
6.25 10. 0.12.50 10. 5.25.00 10. 7.50.00 10. 6.100.00 10. 10.
THE BINOMIAL TEST SHOWS THATSOUND CONSERVATIVE 95 PERCENT
DEAD PROB.(%).00 .9766D-01
50.00 .6230D+0270.00 . 1719D+0260.00 .3770D+02100.00 .9766D-01
6.25 AND 100.00 CAN BE USED ASCONFIDENCE LIMITS SINCE THE ACTUAL
STATISTICALLYCONFIDENCE
LEVEL ASSOCIATED WITH THESE LIMITS IS 99.8047 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 12.500
RESULTS USING MOVING AVERAGESPAN G LC50 95% CONFIDENCE LIMIT4 .114 21.46 15.05 29.40
****** RESULTS CALCULATED BY PROBIT METHODITERATIONS G H GOODNESS OF FIT
6 .231 1.00 .06
SLOPE = 2.3095% CONFIDENCE LIMITS: 1.20 AND 3.41
LC50= 20.2795% CONFIDENCE LIMITS: 12.33 AND 31.54
LC1 = 1.9895% CONFIDENCE LIMITS: .20 AND 4.65
DATE: 11/21/94 TEST NUMBER: DURATION: 48 HOURSSAMPLE: #3 AIR / ZEO SPECIES: CERIODAPHNIA dubia
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 12.500 6.250 100.000 93.750MAA 21.457 15.053 29.400 14.347PROBIT 20.266 12.326 31.539 19.212SPEARMAN 20.306 14.053 29.342 15.289
NOTE: MORTALITY PROPORTIONS WERE NOT MONOTONICALLY INCREASING.ADJUSTMENTS WERE MADE PRIOR TO SPEARMAN-KARBER ESTIMATION.
**** = LIMIT DOES NOT EXIST
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
, /l-fcxw-l /C<»1
TPST ORGANISM: Co Aj jli !< fb - ' AGE: <£-Z /#- LOTNo.:-? 3. "75SAMPLE CSAMPLE fvLAB MEDITEST STAANALYST
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CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: 20.00%LC50: 64.842
95% CONFIDENCE LIMITSARE UNRELIABLE.
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)
6.25 10. 3. 30.00 .1719D+0212.50 10. 2. 20.00 .5469D+0125.00 10. 2. 20.00 .54690+0150.00 10. 1. 10.00 .1074D+01100.00 10. 10. 100.00 .9766D-01
THE BINOMIAL TEST SHOWS THAT .00 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.9023 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 65.726
RESULTS USING MOVING AVERAGESPAN G LC50 95% CONFIDENCE LIMIT2 .215 59.93 45.19 87.75
****** RESULTS CALCULATED BY PROBIT METHODITERATIONS G H GOODNESS OF FIT
5 7.797 5.11 .00
SINCE THE PROBABILITY IS LESS THAN 0.05,RESULTS CALCULATED USING THE PROBIT METHODPROBABLY SHOULD NOT BE USED.
SLOPE = 1.2095% CONFIDENCE LIMITS: -2.15 AND 4.55
LC50= 52.7195% CONFIDENCE LIMITS: 0 AND + INFINITY
LC1 .6195% CONFIDENCE LIMITS: 0 AND 14.87
DATE: 11/21/94 TEST NUMBER: HALBY DURATION: 48 HSAMPLE: #3 AIR/CATION SPECIES: CERIODAPHNIA DUBIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 65.726 .000 100.000 100.000MAA 59.927 45.193 87.746 42.553PROBIT 52.706 ******* ******* *******SPEARMAN 64.842 ******* ******* ******* &R3Q3U60
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "T" /Z^I Z- CLIENT:TEST ORGANISM: Cdjr.'aJif hr-,; rAcb:«._____ ' AGE: <£-"Z ti- LOT No.: JLSAMPLE DESCRIPTION: U /ftSvf-ttSAMPLE No.(s):. "LAB MEDIA/NO.: O< HWX- *w*x.«i._____ CONTROL/DILUENT:.TEST START DATE: ll-lI-W TIME: /)#<£' TEST END DATE: If-l 'f f TIME:.ANALYSTfs): <Tx £xag£ /<_________________________ CODE:______________
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CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "T g" /42.J2- CLIENT: //Q/k./ C/-i v /C (_____TEST ORGANISM: Co thxphr, '.o. fTJCth.' ' AGE: -Z tf- LOT No.:SAMPLE DESCRIPTION: U 3&r+t-t'cy l f£0 "74-SAMPLE No.(s):.LAB MEDIA/NO.: CCW-JW.A- Jwx.i_______ CONTROL/DILUENT:.TEST START DATE: If- ll-*H{ TIME: ll&O TEST END DATE: If-Z^-ftj TIME: /2ANALYSTS): <TV £Lc»o/t (<________________________ CODE:________________
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CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: .00%LC50: 65.975
95% LOWER CONFIDENCE: 57.63795% UPPER CONFIDENCE: 75.520
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)12.50 10. 0. .00 .9766D-0125.00 10. 1. 10.00 .10740+0150.00 10. 0. .00 .9766D-01100.00 10. 10. 100.00 .97660-01
THE BINOMIAL TEST SHOWS THAT 50.00 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.8047 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 70.711
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 11/21/94 TEST NUMBER: HALBY DURATION: 48 HSAMPLE: #3 AIR/EDTA 10 SPECIES: CERIODAPHNIA DUBIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 70.711 50.000 100.000 50.000 -MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 65.975 57.637 75.520 17.883
NOTE: MORTALITY PROPORTIONS WERE NOT MONOTONICALLY INCREASING.ADJUSTMENTS WERE MADE PRIOR TO SPEARMAN-KARBER ESTIMATION.
**** = LIMIT DOES NOT EXIST
AR303463
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: "7 * /tjZ.3 Z- CLIENT: //a / A ./ Ghj / C<v (TEST ORGANISM: C°^-~aftfhr> ;< <i<!h:<^ ' AGE: -"Z ff- LOT No.:SAMPLE DESCRIPTION: /4*Wif«Vva £~0fA '2'°''* /<—SAMPLE No.fe):LAB MEDIA/NO.: CcW-W - /w''. CONTROUDILUENT:TEST START DATE: J/-E/-W TIME: I/&S~ TEST END DATE: //- -5y TIME: /ANALYSES): <TV C e>lL\< _______________________ CODE:
TREA17NO.
1
2
3
4
5
6
7
TESTSOLUTION
&••_/
«/,
So/
/DO/
,
DATE
RERi;
A
...B,,..
A
B
A
B
A
B
A
B
A
B
A
B
DETERMINED BY
T iB( rALlT;IES •;•••'••iifSlii&QSURE'' ;''Si||RiGiDHi-s):;u; ..;•-•*%%-••:*. ••' :W::.'
0601e^s~r
//-13(?f
TOt L ;FATXilliiES;;
>oo(o7.JT5
MEANSUR\/i\XAL
/CO/
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COMMENTS
i
FoanBCATOfi
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: .00% !LC50: 57.435
95% LOWER CONFIDENCE: 46.13095% UPPER CONFIDENCE: 71.511
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB. (%)12.50 10. 0. .00 .9766D-0125.00 10. 1. 10.00 .1074D+0150.00 10. 2. 20.00 .5469D+01100.00 10. 10. 100.00 .9766D-01
THE BINOMIAL TEST SHOWS THAT 25.00 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 98.8281 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 62.190
RESULTS USING MOVING AVERAGESPAN G LC50 95% CONFIDENCE LIMIT2 .168 56.36 43.81 76.07
****** RESULTS CALCULATED BY PROBIT METHODITERATIONS G H GOODNESS OF FIT
7 .313 l.OO .11 i
SLOPE =5.4695% CONFIDENCE LIMITS: 2.40 AND 8.51
LC50= 55.4395% CONFIDENCE LIMITS: 41.20 AND 75.55
LC1 =20.7695% CONFIDENCE LIMITS: 5.73 AND 31.08
DATE: 11/21/94 TEST NUMBER: HALBY DURATION: 48 HSAMPLE: #3 AIR/EDTA 20 SPECIES: CERIODAPHNIA DUBIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 62.190 25.000 100.000 75.000MAA 56.356 43.814 76.071 32.258PROBIT 55.428 41.203 75.548 34.345SPEARMAN 57.435 46.130 71.511 25.381
I**** = LIMIT DOES NOT EXIST
AR303U65
CH2M HILL Milwaukee Bioassay Laboratory
48-HOUR ACUTE BIOASSAY SURVIVAL DATA(2 Replicates)
PROJECT No.: ~7S /tjZ.3 2- CLIENT: //Q /k y G JL /C* (_______TEST ORGANISM: Ce -.'afLtflir, / r U : ' AGE: -Z ff- LOT No.:SAMPLE DESCRIPTION:_______/4««*»-frr*-s. £p 74.SAMPLE No.(s): -£LAB MEDIA/NO.: C< /4t x_ JwX.y._____ CONTROUDILUENT:_TEST START DATE: H-lf-^ TIME: IZOO TEST END DATE: //~Z ~'?</ TIME:.ANALYST(s): -3~, Cj*0lt\<-_________________________ CODE:______________
TREAT.NO.
1
2
3
4
5
6
7
TESTSOLUTION
M'L
7.So •/.loo 7
DATE
REp
A
B
A
B
A
B
A
B
A
B
A
B
A
B
DETERMINED BY
1 '••DC;t3'''ti:V'D' 'd'IC3C— "'•viCi"* '*— vi v/O^J itC>•'• ••'' ' •• • '':•' • • ; ' . . , ,
' :';O1 ' ' • ;''*' 48
32.O000JsT
J/-Z3* -
TOTALFATMlfiES
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MEANSURVIVAL
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COMMENTS
I
HR303U66
CT-TOX: BINOMIAL, MOVING AVERAGE, PROBIT, AND SPEARMAN METHODS
SPEARMAN-KARBER
TRIM: 16.67%LC50: 65.975
95% CONFIDENCE LIMITSARE UNRELIABLE.
CONC. NUMBER NUMBER PERCENT BINOMIAL% EXPOSED DEAD DEAD PROB.(%)12.50 10. 5. 50.00 .62300+0225.00 10. 0. .00 .97660-0150.00 10. 0. .00 .97660-01100.00 10. 10. 100.00 .97660-01
THE BINOMIAL TEST SHOWS THAT .00 AND 100.00 CAN BE USED AS STATISTICALLYSOUND CONSERVATIVE 95 PERCENT CONFIDENCE LIMITS SINCE THE ACTUAL CONFIDENCELEVEL ASSOCIATED WITH THESE LIMITS IS 99.9023 PERCENT.AN APPROXIMATE LC50 FOR THIS DATA SET IS 70.711
WHEN THERE ARE LESS THAN TWO CONCENTRATIONS ATWHICH THE PERCENT DEAD IS BETWEEN 0 AND 100, NEITHERTHE MOVING AVERAGE NOR THE PROBIT METHOD CAN GIVEANY STATISCALLY SOUND RESULTS.
DATE: 11/21/94 TEST NUMBER: HALBY DURATION: 48 HSAMPLE: #3 AIR/EDTA 40 SPECIES: CERIODAPHNIA DUBIA
METHOD LC50 CONFIDENCE LIMITSLOWER UPPER SPAN
BINOMIAL 70.711 .000 100.000 100.000MAA ******* ******* ******* *******PROBIT ******* ******* ******* *******SPEARMAN 65.975 ******* ******* *******
NOTE: MORTALITY PROPORTIONS WERE NOT MONOTONICALLY INCREASING.ADJUSTMENTS WERE MADE PRIOR TO SPEARMAN-KARBER ESTIMATION.
**** = LIMIT DOES NOT EXIST
AJJ 303i*6 7