smartlab + hypix-3000 system instruction manual · 2017. 4. 19. · smartlab + hypix-3000 system 1...

SmartLab + HyPix-3000 System Instruction Manual

This manual describes the correct use of the product as well the usage precautions to be observed. To obtain full-expected performance from the product, thoroughly read this manual.

Also, store this manual at an easily accessible place so that you can promptly refer to it whenever it is necessary.

The contents of this manual are subject to change without prior notice. This manual described in it may not be disclosed to a third party or copied, in whole or in part, without

the written consent of Rigaku Corporation. In no event will Rigaku Corporation be responsible for the results of the use of this manual. As a rule, one set of the instruction manual has to be purchased for each product. If there are any missing or incorrectly collated pages in the delivered instruction manual, please

contact the sales representative who you purchased the instrument from for instruction manual replacement.

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SmartLab + HyPix-3000 System i

Contents Overview ............................................................................................................ 1

Configuration .................................................................................................... 3

Specifications .................................................................................................... 5

Mounting HyPix-3000 on SmartLab ................................................................. 7

Mounting position of HyPix-3000 and receiving optical device for 0D and 1D measurement mode ............................................................................................... 7 Mounting HyPix-3000 and receiving optics for 0D and 1D measurement mode ..... 8 Mounting HyPix-3000 for 2D measurement mode .................................................11 Wiring HyPix-3000 and SmartLab and PCs.......................................................... 12 Starting up HyPix-3000 ........................................................................................ 13 Using the vertical mount holder for SmartLab (optional) ....................................... 15 Setting and controlling in SmartLab Guidance ..................................................... 16

HyPix-3000 dialog box .................................................................................. 16 Setup HyPix detector Part ............................................................................. 17 Create Mask File Part ................................................................................... 18 Renew correction data Part ........................................................................... 18 Camera Length Measurement Part ............................................................... 19

Shutting down HyPix-3000 ................................................................................... 20 Item No. A00001644 Manual No. ME15736A01 2014. 07 (1st Edition)

SmartLab + HyPix-3000 System 1

Overview

HyPix-3000 is a hybrid multi-dimensional pixel detector as an optional component for SmartLab. The combination of SmartLab and HyPix-3000 enables not only 2D measurement but also 1D and 0D measurements. This instruction manual describes the procedure to use HyPix-3000 with SmartLab.

Overall view of SmartLab + HyPix-3000 System


Configuration

The standard configuration of HyPix-3000 includes the following components.

・HyPix-3000

(1) HyPix-3000 main unit

(2) Mount holder for SmartLab (horizontal mount)

(3) HyPix server PC

(4) HyPix server software

(5) Camera link cable

(6) Frame Grabber card

(7) Power circuit board

(8) Power cable

(9) TDI signal cable

(10) LAN cable

・Standard accessory

(1) Protection cover

(2) Absorber and filter for HyPix-3000

(3) Mask slit (for 0D, 1D measurement)

(4) Package case

・Optional parts

(1) Direct beam stopper (for 1D, equivalent to that for D/teX Ultra, dedicated for SmartLab (Powder))

(2) Knife edge (for 1D, equivalent to that for D/teX Ultra, dedicated for SmartLab (Powder))

(3) Scattered radiation protector (for 1D, equivalent to that for D/teX Ultra)

(4) Mount holder for SmartLab (vertical mount)


Specifications

・Detector

(1) Pixel size: 100 μm x 100 μm

(2) Active area: 38.5 mm x 77.5 mm

(3) Number of pixels: 385 x 775 = 298375 pixels

(4) Count rate per pixel: >1 x 106 cps/pixel

(5) Global count rate: >2.9 x 1011 cps

(6) Readout mode: Long (31 bit), Diff, 0dead

(7) Framing rate: 131 fps : Diff, 87 fps : Long (31 bit)

(8) Energy range: 4 keV ～ 30 keV

(9) Counting efficiency: 99% (at CuKα)

(10) Energy resolution: < 25% at CuKα

(11) Guaranteed operating temperature*1: 15 °C to 35 °C (59 °F to 95 °F)

(12) Guaranteed operating humidity: 20% to 65%RH

(13) Guaranteed operating temperature*2: Tcorr. ±4°C (7 °F)

(14) Weight: Approx. 2 kg (4.41 lb.)

*1: All the detector functions operate normally within the range of guaranteed operating

temperature. *2: All the specifications written in this manual are guaranteed within the range of guaranteed

operating temperature. Tcorr. indicates the corrected temperature.

・ HyPix server PC

(1) OS: Microsoft Windows 8.1 Pro (64 bit)

(2) CPU: Intel Core i7 (3.4 GHz)

(3) Memory: 16 GB

(4) HDD: 500 GB

Specifications

6 SmartLab + HyPix-3000 System

・Camera length

(1) 0D and 1D measurement mode: 300-mm fixed

(2) 2D measurement mode: Selectable within the range of 150 to 300 mm (Standard)

CAUTION

The camera length can be extended up to 110 mm by removing the positioning screw from the theta_d arm. In that case, depending on the mounted attachment, HyPix-3000 may collide with it. Confirm that they do not collide with each other beforehand, and use the camera length at your own risk.

Theta_d arm positioning screw

(3) Theta_d angle upper limit: 100° (In-plane arm system with a 150-mm camera length only)

(4) 2 theta-chi angle limit: 90° (In-plane arm system only)

Other variable ranges depend on the specification of SmartLab.


Mounting HyPix-3000 on SmartLab

Mounting position of HyPix-3000 and receiving optical device for 0D and 1D measurement mode For the normal 0D and 1D measurement mode, mount the following devices on the theta_d arm of SmartLab in order from the sample side: standard receiving slit box # 2, receiving optics unit # 1 (ROD), receiving optics unit # 2 (RPS), optics of HyPix-3000 and HyPix-3000. The names of variable axes of the receiving slit box # 2 are as follows:

Receiving slit: RS1 Height adjustment axis: Zr

Also, limiting the active area of HyPix-3000 functions as a virtual receiving slit. The name of each device is as follows:

Virtual receiving slit: RS2 Virtual height adjustment axis: Zd

Mounting position of HyPix-3000 and receiving optics for 0D and 1D measurement mode



Mounting HyPix-3000 and receiving optics for 0D and 1D measurement mode This section explains the procedure to mount HyPix-3000 and receiving optics on SmartLab for 0D and 1D measurement mode.

1 Mount HyPix-3000 on SmartLab. ① Mount the HyPix-3000 on the theta_d arm of SmartLab so that the

reference line of HyPix-3000 points at 350 mm. Then fix it with the Allen wrench provided. The reference line of HyPix-3000 is positioned at +50 mm from the detection plane. Thus, the detection plane is actually positioned at 300-mm camera length (goniometer center - detection plane distance).

Camera length and reference line (The camera length is set to 300-mm in this picture.)

② Connect the cable to COUNTER of the receiving connector box. At this moment, we recommend attaching the protective cover on the detection window of HyPix-3000. It prevents the detection window from being damaged while mounting optics and HyPix-3000.

When using HyPix-3000 with SmartLab in 0D and 1D measurement mode, it needs to be mounted at 300-mm camera length.

Mounting HyPix-3000 and receiving optics for 0D and 1D measurement mode


2 Mount an RPS adapter and a parallel slit. ① Mount the RPS adapter and the parallel slit in front of the HyPix-3000,

and fix them with the Allen wrench provided.

② Connect the cable to ADPT2 of the receiving connector box.

3 Mount an ROD adapter and a parallel slit.

① In the same way as step 2, mount the ROD adapter and the parallel slit analyzer in front of the RPS adapter and the parallel slit, and fix them with the Allen wrench provided.

② Connect the cable to ADPT1 of the receiving connector box.



4 Mount receiving slit box # 2. ① Press the receiving slit box # 2 against the positioning screw on the

theta_d arm, and fix it with the Allen wrench provided.

② Connect the cable to SLIT2 of the receiving connector box.

Be sure to connect the cable of receiving slit box # 2 to SLIT2.

5 Remove the protective cover (if attached) and insert a mask slit into the detection window.

Mounting HyPix-3000 and optical devices is now completed.

After this, perform initialization of the axes in the SmartLab Guidance. (Refer to Chapter 14 "Initialization of axes" of "SmartLab Guidance Reference Manual".)

Mounting HyPix-3000 for 2D measurement mode


Mounting HyPix-3000 for 2D measurement mode This section explains the procedure to mount HyPix-3000 on SmartLab for 2D measurement mode. Generally no receiving optics are mounted between HyPix-3000 and a sample in the 2D measurement mode. HyPix-3000 can be mounted at any position within the range of 150 - 300 mm camera length. For the camera length setting, subtract 50 mm from the position of the HyPix-3000's reference line.

HyPix-3000 mounting position for 2D measurement mode

Reference line of HyPix-3000 (The camera length is set to 300-mm in this picture.)

Mounting HyPix-3000 for 2D measurement mode is now completed.

After this, update the configuration for the currently mounted optical devices in SmartLab Guidance.



Wiring HyPix-3000 and SmartLab and PCs

1 Connect the two camera link cables from HyPix server PC to HyPix-3000. Then, connect the TDI signal cable and the power cable from the SmartLab main unit to the HyPix-3000.

2 Directly connect the SmartLab control PC and HyPix server PC with a LAN cable.

Systematic diagram of HyPix-3000 and PCs

Rear side view of HyPix-3000

TDI signal cable

Power cable

Camera link cables

Power switch

Status LED (Red) (Green)

HyPix server PC

SmartLab main unit LAN

SmartLab control PC

LAN 1000

BASE-T

HyPix-3000

Camera link cable (2 lines)

TDI signal cable

Power cable

1000BASE-T LAN card

Starting up HyPix-3000


Starting up HyPix-3000 Before starting up HyPix-3000, mount the HyPix-3000 and receiving optics on SmartLab for 0D and 1D measurement mode. The procedure to start up HyPix-3000 is described below.

1 Turn on the power switch on the rear side of HyPix-3000. When the HyPix-3000 turns on, the fan starts operating and the status LED starts blinking in green.

2 Connect HyPix server software and SmartLab Guidance. ① Turn on the power of HyPix server PC and wait for a while.

② Go to the Start menu on the SmartLab control PC, and select All Programs - Accessories - Remote Desktop Connection.

③ Enter "192.168.126.70" in the Computer box of the Remote Desktop Connection window, and then click Connect.



④ Click Use another account, and then enter "rigaku" in the user name box without a password. Then click OK.

⑤ Confirm that the following window appears on the desktop, indicating that the HyPix server software is running.

Server window

3 Update the hardware configuration. ① Start up the SmartLab Guidance in the SmartLab control PC.

② Click the Hardware Configuration command under the Options menu to display the Hardware Configuration dialog box. Then click the Update button.

③ HyPix-3000 will be recognized by updating the hardware configuration and be displayed in the Detector box of the Hardware Configuration dialog box.

When changing the receiving optics togher with connecting/removing the cable, perform initialization to the corresponding axes. (Refer to Chapter 14 "Initialization of axes" of "SmartLab Guidance Reference Manual".)

Using the vertical mount holder for SmartLab (optional)


Using the vertical mount holder for SmartLab (optional) The HyPix-3000 can be positioned vertically by using the vertical mount holder for SmartLab (optional). By mounting the detector vertically, the data can be obtained from a wide 2theta range in a single scan.

Horizontal mount holder (standard) Vertical mount holder (optional)

1 Procedure to set the mount holder (vertical mount) for SmartLab ① Loosen the four screws on rear side of HyPix-3000 and remove the

mount holder (horizontal).

② Turn the HyPix-3000 around so that its detection plane faces the right side. Place the mount holder (vertical) on the rear side of HyPix-3000, and fix it by tightening the four screws in the reverse way of step ①.

Fixing screws on the rear side of HyPix-3000

Detection plane



Setting and controlling in SmartLab Guidance For the settings and operations of theParts other than described here, refer to "SmartLab Guidance Reference Manual".

HyPix-3000 dialog box

In this dialog box, the setup information of HyPix-3000 can be referred and updated. Click Detector Setup - HyPix-3000 under the Options menu to open the HyPix-3000 dialog box.

Detector Settings Select a type of X-ray source and an energy mode. When selecting an energy mode, the values in the Discriminator settings1 and Discriminator settings2 boxes automatically change. Generally, change the energy mode in Setup HyPix detector Part which is described later. Enable mask processing Use this function when noise is observed in the detector. When the Enable mask processing box is checked, defective pixels will be complemented. To detect defective pixels, use the Create Mask File Part described later. ROI (Region of Interest) settings Specify the area in the detection plane to be used for 0D and 1D measurements. Set the conditions for 0D and 1D measurements and the range of 1D measurement which is performed with 2D measurement together. Click the 0D/1D tab or 2D tab to show the corresponding display.

Setting and controlling in SmartLab Guidance


0D/1D tab

Center position: Width -5, Height +5 by default

Detection area: Enter an arbitrary value in the X (depth) direction. Y direction changes depending on the set width of RS (receiving slit)2.

Camera length: 300-mm fixed

2D tab

Center position: Determined by executing Camera Length Measurement Part described later.

Detection area: Enter an arbitrary value in the X (depth) direction. Y direction changes depending on the set width of RS (receiving slit)2.

Camera length: Determined by executing Camera Length Measurement Part described later.

Click the Register button to register the entered values.

Note: For the details on the Parts described later, refer to the corresponding Part in Help – Help Topic of the SmartLab Guidance software.

Setup HyPix detector Part

When Package/Macro Measurement is selected, this Part can be selected from Preinstalled - Basic Parts. Count mode (Long (31 bit) /Diff/ 0DeadTime) and energy mode (Normal/ XRF reduction) can be selected or changed depending on the purpose.



Create Mask File Part

When Package/Macro Measurement is selected, this Part can be selected from Preinstalled - Utility Parts. Use this Part when noise is observed in the detector.

Renew correction data Part

When Package/Macro Measurement is selected, this Part can be selected from Preinstalled - Utility Parts. Use this Part to re-create the correction data of detector. This Part corrects sensitivity between pixels. If defective pixels exist, they are complemented.

Setting and controlling in SmartLab Guidance


Camera Length Measurement Part

When Package/Macro Measurement is selected, this Part can be selected from Preinstalled - Utility Parts. Camera length (the distance from sample center to detection plane) and detector center position will be automatically set by executing this Part.

Be sure to execute Camera Length Measurement Part when performing a measurement in 2D mode for the first time or changing camera length.



Shutting down HyPix-3000 The procedure to shut down HyPix-3000 is described below.

1 Disconnect HyPix server software and SmartLab Guidance. ① Click the Hardware Configuration command under the Options

menu to display the Hardware Configuration dialog box.

② Click the Detector button to display the Detector dialog box.

③ Change the item in the Detector #2 combo box from HyPix-3000 to None.

④ Click OK to close the Detector dialog box.

2 End the HyPix server software. ① Turn off the power switch of HyPix server PC.

② The HyPix server software ends and the power of the PC automatically turns off.

3 Turn off the power of HyPix-3000. ① Turn off the power switch on the rear side of the HyPix-3000.

② Confirm that the Status LED (Green) turns off.

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Specifications Subject to Change without Notice

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2013.10

OverviewConfigurationSpecificationsMounting HyPix-3000 on SmartLabMounting position of HyPix-3000 and receiving optical device for 0D and 1D measurement modeMounting HyPix-3000 and receiving optics for 0D and 1D measurement modeMounting HyPix-3000 for 2D measurement modeWiring HyPix-3000 and SmartLab and PCsStarting up HyPix-3000Using the vertical mount holder for SmartLab (optional)Setting and controlling in SmartLab GuidanceHyPix-3000 dialog boxSetup HyPix detector PartCreate Mask File PartRenew correction data PartCamera Length Measurement Part

Shutting down HyPix-3000

smartlab + hypix-3000 system instruction manual · 2017. 4. 19. · smartlab + hypix-3000 system 1...

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