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SOIL SAMPLING REPORT AUTO SALVAGE YARD

for

STATE ROUTE 11 AND THE OTAY MESA EAST

PORT OF ENTRY

SAN DIEGO COUNTY, CALIFORNIA DISTRICT 11–SD –ROUTE 11

PM 0.0/2.8 EA056310 DISTRICT 11–SD –ROUTE 905

PM R8.4/10.1

TIER II ENVIRONMENTAL IMPACT REPORT/ ENVIRONMENTAL IMPACT STATEMENT

November 2010

For individuals with sensory disabilities, this document is available in Braille, large print, on audiocassette, or computer disk. To obtain a copy in one of these alternate formats, please call or write to Caltrans District 11, Attn: Sandra Lavender, Environmental Analysis Branch A, 4050 Taylor Street, MS 242, San Diego, CA 92110; (619) 688-3135 Voice, or use the California Relay Service TTY number, 711.

SOIL SAMPLING REPORT AUTO SALVAGE YARD

PROPOSED SR-11 ALIGNMENT APN 648-070-13

SAN DIEGO, CALIFORNIA

PREPARED FOR: AECOM

7807 Convoy Court, Suite 200 San Diego, California 92111

PREPARED BY: Ninyo & Moore

Geotechnical and Environmental Sciences Consultants 5710 Ruffin Road

San Diego, California 92123

February 5, 2010 Project No. 106637001

February 5, 2010 Project No. 106637001

Mr. Kirk Bradbury AECOM 7807 Convoy Court, Suite 200 San Diego, California 92111

Subject: Soil Sampling Report Auto Salvage Yard

Proposed SR-11 Alignment San Diego, California APN 648-070-13

Dear Mr. Bradbury:

In accordance with our task order dated July 22, 2009, Ninyo & Moore has performed soil sam-pling activities at the above-referenced site. The attached report presents our findings, opinions, and recommendations.

We appreciate the opportunity to be of service to you on this project.

Respectfully submitted, NINYO & MOORE

Jeanette Ninyo Senior Staff Geologist

Stephan A. Beck, C.E.G. 1512, HG. 126 Manager, Environmental Sciences Division

JN/SLS/SB/gg

Distribution: (3) Addressee

Proposed SR-11 Alignment February 5, 2010 San Diego, California Project No. 106637001

106637001 R.doc i

TABLE OF CONTENTS Page

1. INTRODUCTION ....................................................................................................................1 1.1. Purpose .........................................................................................................................1 1.2. Site Description ............................................................................................................1 1.3. Background...................................................................................................................1 1.4. Contaminants of Potential Concern ..............................................................................2 1.5. Scope of Work ..............................................................................................................2

2. SAMPLING PROGRAM .........................................................................................................2 2.1. Site Safety.....................................................................................................................2 2.2. Soil Sampling................................................................................................................3

3. ANALYTICAL TESTING PROGRAM ..................................................................................3

4. FINDINGS................................................................................................................................4

5. COMPARISON OF ANALYTICAL RESULTS TO SCREENING CRITERIA....................5

6. RECOMMENDATIONS..........................................................................................................6

7. LIMITATIONS.........................................................................................................................7

8. REFERENCES .......................................................................................................................10

Figures Figure 1 – Site Location Map Figure 2 – Sample Locations and Analytical Results

Table Table 1 – Summary of Soil Sample Analytical Results

Appendix Appendix A – Laboratory Reports


106637001 R.doc 1

1. INTRODUCTION

Ninyo & Moore conducted soil sampling at the automobile salvage yard associated with the pro-

posed State Route 11 (SR-11) expansion and Otay Mesa East Port of Entry (POE) development

project. The site consists of a portion of an automobile salvage yard located southwest of the inter-

section of Otay Mesa Road and Alta Road, in San Diego, California (Figure 1). This soil sampling

report is intended for use by AECOM and the California Department of Transportation (Caltrans),

and has been conducted in general accordance with Task Order 13 05-04-004 dated July 22, 2009.

1.1. Purpose

The site is located within the proposed SR-11 alignment. The purpose of this soil sampling report

is to provide a screening-level evaluation of the presence of contaminants of potential environ-

mental concern (COPCs) associated with the site from auto salvage and storage activities.

1.2. Site Description

The site consists of approximately 4 acres in the southern portion of the auto salvage yard

assigned Assessor’s Parcel Number (APN) 648-070-13 (Figure 2). The northernmost site

boundary as depicted on Figure 2 represents the boundary of the proposed SR-11 alignment.

The eastern, western, and southern boundaries of the site correspond to parcel boundaries.

The site consists of unpaved gravel lots. The eastern and western portions of the site are op-

erated by two separate businesses, Desert View Auto Auction and A to Z Towing,

respectively. Both of the lots are utilized for vehicle and boat storage, as well as auctions.

1.3. Background

For a previous Initial Site Assessment (ISA) report, Ninyo & Moore conducted a review of

historical aerial photographs to evaluate historical site usage. Based on a review of historical

sources, the area now occupied by the automobile salvage yard was graded, and vehicles be-

gan to be stored sometime between 1989 and 1995. The site was undeveloped and/or used

for agriculture prior to that time (Ninyo & Moore, 2007).


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1.4. Contaminants of Potential Concern

COPCs, as described in the task order, that may be associated with vehicle storage at salvage

yards, include: total petroleum hydrocarbons (TPH), volatile organic compounds (VOCs), semi-

volatile organic compounds (SVOCs), polychlorinated biphenyls (PCBs), lead, and metals.

1.5. Scope of Work

Ninyo & Moore's scope of work for this screening-level soil sampling evaluation included

the activities listed below.

• Preparation of a site-specific health and safety plan.

• Coordination with the property owner, Kouladjian Family Trust, to obtain site access. Notification was provided to applicable parties in accordance with the Permit to Enter agreement dated November 18, 2009.

• Selection of 15 soil sampling locations, located approximately 100 feet apart, and mark-ing locations using a global positioning system (GPS) device.

• Collection of one surface sample at 0.5 feet below ground surface (bgs) and one subsur-face sample at 2 feet bgs at each of the 15 soil sampling locations.

• Submittal of the soil samples to a state-certified laboratory for analysis of COPCs.

• Compilation of analytical data and preparation of this report, summarizing sample re-sults and providing conclusions and recommendations regarding the presence of COPCs in shallow soil.

2. SAMPLING PROGRAM

This section describes the fieldwork portion of the soil sampling activities.

2.1. Site Safety

On-site work was performed in accordance with procedures and guidelines outlined in the

site-specific Health and Safety Plan (HASP). The HASP was signed by field personnel ac-

knowledging their understanding of, and agreement to abide by, its contents. The plan

included information regarding potential chemical and physical hazards that may be en-


106637001 R.doc 3

countered during fieldwork, methods and procedures to reduce workers exposure and risk,

and plans and maps indicating the closest route to the hospital.

2.2. Soil Sampling

To screen for the presence of COPCs in soil, 15 sample locations (HA-1 through HA-15)

were chosen. One surface sample (0.5 feet bgs) and one subsurface sample (2 feet bgs) were

collected at each of the 15 locations. Sample locations are depicted on Figure 2.

Subsurface samples were collected using a hand auger. Non-disposable and non-dedicated

tools that contacted the samples, such as trowels and hand augers, were cleaned with a three-

step soap and water wash and distilled water rinse prior to the collection of each sample and

between each sample location. Minimal quantities of decontamination water was generated

by utilization of spray bottles and paper towels to clean equipment. Soil cuttings were placed

on plastic sheeting during hand auger activities and then placed in California Department of

Transportation-compliant 55-gallon drums pending receipt of analytical results. Soil sam-

pling expendables such as nitrile gloves and paper towels used for decontamination were

contained in plastic bags and disposed of as municipal trash. Borings were backfilled with

hydrated bentonite chips to original grade.

Soil samples were collected in laboratory-supplied glass jars, labeled with pertinent identify-

ing information (e.g., project number, project name, sample location, sample collection date

and time, sampler’s initials), placed in a cooler with ice, and transferred to Advanced Tech-

nology Laboratories (ATL) of Signal Hill, California under standard chain-of-custody

protocol for analyses.

3. ANALYTICAL TESTING PROGRAM

The analytical testing methods for soil samples are described below. In accordance with the Task

Order, deeper samples collected from 2 feet bgs were held for analysis pending results of the

shallower samples collected from 0.5 feet bgs.


106637001 R.doc 4

• All shallow samples collected from 0.5 feet bgs were submitted for analysis of total lead and TPH extended range (carbon range C8 through C40) by United States Environmental Protec-tion Agency (USEPA) test methods 6010B and 8015B(M), respectively.

• Based on the analytical results of the shallow samples, five of the deeper samples (2 feet bgs) were also analyzed for TPH.

• Five samples collected from 0.5 feet bgs with the highest concentrations of TPH were ana-lyzed for VOCs by USEPA test method 8260B.

• Two samples collected from 0.5 feet bgs with the highest concentrations of TPH were ana-lyzed for SVOCs by USEPA test method 8270C.

• Two samples collected from 0.5 feet bgs with the highest concentrations of TPH were ana-lyzed for PCBs by USEPA test method 8082.

• Two samples collected from 0.5 feet bgs with the highest concentrations of total lead were analyzed for Title 22 metals by USEPA test method 6010B/7471A.

• Two equipment rinse (field) blanks were collected and analyzed for total lead, TPH, VOCs, SVOCs, PCBs, and/or Title 22 metals.

• Two duplicate soil samples (DUP-01 and DUP-02) were collected as field duplicates of HA-1-0.5 and HA-9-0.5, respectively and analyzed for total lead and TPH.

• One laboratory-provided trip blank was transported with the collected samples and ana-lyzed for VOCs.

4. FINDINGS

The purpose of the soil sampling activities described herein was to screen for the presence of

COPCs in soil. The following is a summary of analytical results for COPCs at the site:

• Total lead was detected in all of the samples collected from 0.5 feet bgs, at concentrations up to 37 milligrams per kilogram (mg/kg).

• TPH was detected in 14 of the 15 surficial samples collected from 0.5 feet bgs, at concentra-tions ranging from 17 to 2,300 mg/kg. TPH was detected up to 3,100 mg/kg in one of the duplicate surficial samples collected from the location of HA-9. In general, concentrations of TPH were detected within the higher-end carbon ranges (e.g., C28 through C40). TPH was not detected above the practical quantitation limit (PQL) in the five deeper samples analyzed from 2 feet bgs.


106637001 R.doc 5

• VOCs were not detected above the PQL in the selected samples analyzed.

• SVOCs and PCBs were not detected above the PQL in the selected samples analyzed.

• Title 22 metals were detected in the two samples analyzed.

• TPH, VOCs, SVOCs, and PCBs were not detected above the PQL in the two equipment rinse (field) blanks; however, barium, silver, and antimony were detected in the equipment blanks. Barium and silver were detected at 0.040 milligrams per liter (mg/l) and 0.011 mg/l, respectively, in QCEB-01. Antimony and silver were detected in QCEB-02 at 0.0066 mg/l and 0.0093 mg/l, respectively. The low concentrations of metals detected in the equipment rinse (field) blanks are not interpreted to be significant. Therefore, for the purposes of this screening-level soil sampling and analysis, the data are considered usable.

• Total lead concentrations and TPH concentrations for primary samples and their duplicates were generally within the relative difference expected due to natural heterogeneity of soil matrix samples.

• VOCs were not detected above the PQL in the trip blank analyzed.

Soil analytical data are presented on Table 1 and Figure 2. Copies of the laboratory analytical

reports, including quality control/quality assurance data and chain-of-custody documentation, are

included in Appendix A.

5. COMPARISON OF ANALYTICAL RESULTS TO SCREENING CRITERIA

Analytical results of soil samples were compared to California and federal hazardous waste clas-

sification guidelines for lead-impacted soil. Soil with total lead concentrations (Total Threshold

Limit Concentration for lead) exceeding 1,000 mg/kg or Soluble Threshold Limit Concentra-

tion (STLC) exceeding 5.0 mg/l is classified as California-hazardous waste. Soil is classified as

federally hazardous under the Resource Conservation and Recovery Act (RCRA) when soluble

lead concentrations, as extracted by the Toxicity Characteristic Leaching Procedure (TCLP), ex-

ceed 5.0 mg/l. Using these guidelines, shallow soil at the site (e.g., up to 2 feet bgs) would not be

classified as California-hazardous waste for lead, as the maximum concentration of lead detected was

37 mg/kg, below the 50 mg/kg solubility screening criterion. Due to the low levels of lead detected

below hazardous waste screening levels of 50 mg/kg, samples were not analyzed for soluble lead


106637001 R.doc 6

by the Waste Extraction Test (WET) or TCLP methods, and deeper samples (e.g., from 2 feet

bgs) were not analyzed for total lead.

Most of the soil sampled would be considered a waste based on concentrations of TPH in se-

lected samples up to 3,100 mg/kg.

6. RECOMMENDATIONS

The soil sampling activities described herein have documented the presence of soil on the site

impacted with concentrations of TPH and metals. Based upon the findings of this assessment,

our recommendations are summarized below.

• Soil generated at the site from subsurface disturbance activities, including grading, excava-tion, or trenching for utilities, may be considered a waste, and should be managed, profiled, transported, and disposed of in accordance with all applicable regulations.

• Further assessment should be performed at the site if discolored soil or other potential envi-ronmental issues are encountered during future subsurface disturbance activities.

• Appropriate references to the potential to encounter contaminated soil should be included in construction specifications.

• Prior to initiation of soil disturbance (e.g., excavation/grading activities) at the site, a soil management plan should be prepared that would address the notification, monitoring, sam-pling, testing, handling, storage, and disposal of contaminated media or substances that may be encountered. In addition, a site and community health and safety plan should be prepared prior to initiation of soil disturbance to manage potential health and safety haz-ards to workers and the public.

It should be noted that the intent of the soil sampling was not to delineate the extent of contami-

nation, if any, or to characterize soils prior to disturbance of export/reuse. Rather, it is limited to

evaluating the potential presence of specific constituents of concern in shallow soil. Collection

and analysis of deeper samples, or additional assessment activities, may be warranted, depending

on the course of action proposed for the site.


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Recommendations presented herein are based on limited sampling activities to obtain data from

shallow soil. There is no evaluation detailed enough to reveal every subsurface condition, and

conditions can vary significantly between sampling locations.

7. LIMITATIONS

The environmental services described in this report have been conducted in general accordance

with current regulatory guidelines and the standard-of-care exercised by environmental consult-

ants performing similar work in the project area. No warranty, expressed or implied, is made

regarding the professional opinions presented in this report. Variations in site conditions may ex-

ist and conditions not observed or described in this report may be encountered during subsequent

activities. Please also note that this study did not include an evaluation of geotechnical condi-

tions or potential geologic hazards.

Ninyo & Moore's opinions and recommendations regarding environmental conditions, as presented

in this report, are based on limited subsurface assessment and chemical analysis. Further assess-

ment of potential adverse environmental impacts from past on-site and/or nearby use of hazardous

materials may be accomplished by a more comprehensive assessment. The samples collected and

used for testing, and the observations made, are believed to be representative of the area(s) evalu-

ated; however, conditions can vary significantly between sampling locations. Variations in soil

and/or groundwater conditions will exist beyond the points explored in this evaluation.

The environmental interpretations and opinions contained in this report are based on the results

of laboratory tests and analyses intended to detect the presence and concentration of specific

chemical or physical constituents in samples collected from the subject site. The testing and

analyses have been conducted by an independent laboratory which is certified by the State of

California to conduct such tests. Ninyo & Moore has no involvement in, or control over, such

testing and analysis. Ninyo & Moore, therefore, disclaims responsibility for any inaccuracy in

such laboratory results.


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Our conclusions, recommendations, and opinions are based on an analysis of the observed site

conditions. It should be understood that the conditions of a site could change with time as a result

of natural processes or the activities of man at the subject site or nearby sites. In addition,

changes to the applicable laws, regulations, codes, and standards of practice may occur due to

government action or the broadening of knowledge. The findings of this report may, therefore, be

invalidated over time, in part or in whole, by changes over which Ninyo & Moore has no control.

This document is intended to be used only in its entirety. No portion of the document, by itself, is

designed to completely represent any aspect of the project described herein. Ninyo & Moore

should be contacted if the reader requires any additional information, or has questions regarding

content, interpretations presented, or completeness of this document.

This report is intended exclusively for use by the client. Any use or reuse of the findings, conclu-

sions, and/or recommendations of this report by parties other than the client is undertaken at said

parties’ sole risk.


106637001 R.doc 10

8. REFERENCES

AECOM (Formerly Boyle Engineering Corporation), 2009, Task Order Number 13 05-04-004: dated July 22.

Kearney Foundation of Soil Science, Division of Agriculture and Natural Resources, University of California, 1996, Kearney Foundation Special Report on the Background Concentra-tions of Trace and Major Elements in California Soils: dated March.

Ninyo & Moore, 2007, Hazardous Materials and Hazardous Waste Initial Site Assessment, Cal-trans/SR-11 San Diego, California: dated March 14.

Ninyo & Moore, 2009, Initial Site Assessment State Route 11 and Otay Mesa Port of Entry San Diego, California: dated October 30.

Regional Water Quality Control Board, 2010, Conditional Waiver No. 8 - Discharges/Disposal of Solid Wastes to Land, http://www.swrcb.ca.gov/rwqcb9/board_decisions/waivers/docs/Conditional_Waiver_8_Final.pdf: accessed in January.

M E X I C OU S A

LowerOtay Reservoir

O

tay River

NOTE: ALL DIRECTIONS, DIMENSIONS AND LOCATIONS ARE APPROXIMATE

0 0.75 1.5 MILES

APPROXIMATE SCALE

LEGEND

SR-11 PROJECT AREA

SR-11 AUTO SALVAGE YARDSAN DIEGO, CALIFORNIA

SITE LOCATION MAP FIGURE

1PROJECT NO. DATE

106637001 2/10

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DATE

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FIGURE

2

SAMPLE LOCATIONSAND ANALYTICAL RESULTS

SR-11 AUTO SALVAGE YARDSAN DIEGO, CALIFORNIA

mg/kg μg/kg mg/kg Detected Metal mg/kg

Arsenic 3.0Barium 110

Chromium 24

Cobalt 3.3Copper 9.1Lead 37

Nickel 10

Vanadium 26

Zinc 32HA-9-2 ND -- -- -- --

37

Sample ID

TPH (C8-C40) VOCs Lead Title 22

Metals

HA-9-0.5 1600 ND

mg/kg mg/kgHA-1-0.5 120 6.9HA-1-2 -- --

Sample IDTPH

(C8-C40) Lead

mg/kg mg/kgHA-2-0.5 17 5.2HA-2-2 -- --

Sample IDTPH

(C8-C40) Lead

mg/kg mg/kgHA-3-0.5 75 5.9HA-3-2 -- --

Sample IDTPH

(C8-C40) Lead

mg/kg mg/kgHA-10-0.5 180 10HA-10-2 -- --

Sample IDTPH

(C8-C40) Lead

mg/kg mg/kgHA-12-0.5 190 4.4HA-12-2 -- --

Sample IDTPH

(C8-C40) Lead

mg/kg mg/kgHA-13-0.5 180 4.8HA-13-2 -- --

Sample IDTPH

(C8-C40) Lead

mg/kg mg/kgHA-15-0.5 73 13HA-15-2 -- --

Sample IDTPH

(C8-C40) Lead

mg/kg μg/kg mg/kgHA-11-0.5 1700 ND 12HA-11-2 ND -- --

Sample IDTPH

(C8-C40) VOCs Lead

mg/kg mg/kg Detected Metal mg/kg

Arsenic 10Barium 110

Chromium 16Cobalt 4.5Copper 17Lead 21

Nickel 9.7Vanadium 27

Zinc 43HA-4-2 -- -- -- --

21

TPH (C8-C40)

HA-4-0.5

Sample ID

440

Title 22 MetalsLead

mg/kg μg/kg mg/kgHA-5-0.5 1700 ND 11HA-5-2 ND -- --

LeadSample ID

TPH (C8-C40) VOCs

mg/kg mg/kgHA-6-0.5 ND 5.9HA-6-2 -- --

Sample IDTPH

(C8-C40) Lead

mg/kg μg/kg μg/kg μg/kg mg/kgHA-7-0.5 1800 ND ND ND 15HA-7-2 ND -- -- -- --

SVOCs PCBs LeadSample ID

TPH (C8-C40) VOCs

mg/kg μg/kg μg/kg μg/kg mg/kgHA-8-0.5 2300 ND ND ND 12HA-8-2 ND -- -- -- --

Sample IDTPH (C8-

C40) VOCs SVOCs PCBs Lead

NOTE: mg/kg - MILLIGRAMS PER KILOGRAM bgs - BELOW GROUND SURFACE ND - NOT DETECTED AT OR ABOVE THE INDICATED REPORTING LIMIT PCBs - POLYCHLORINATED BIPHENYLS BY USEPA TEST METHOD 8082 SVOCs - SEMIVOLATILE ORGANIC COMPOUNDS BY USEPA TEST METHOD 8270C TPH (C8-C40) - TOTAL PETROLEUM HYDROCARBONS EXTENDED RANGE BY USEPA TEST METHOD 8015B(M) ug/kg - MICROGRAMS PER KILOGRAM VOCs - VOLATILE ORGANIC COMPOUNDS BY USEPA TEST METHOD 8260B -- NOT ANALYZED TITLE 22 METALS - TITLE 22 METALS BY USEPA TEST METHOD 6010B

ALL DIRECTIONS, DIMENSIONS AND LOCATIONS ARE APPROXIMATE

APPROXIMATE SCALE

0 100 20050 FEETLEGEND

SAMPLE LOCATION

SITE

SR-11 PROJECT AREA

HA-15

MAP EXTENT

mg/kg mg/kgHA-14-0.5 58 7.7HA-14-2 -- --

Sample IDTPH

(C8-C40) Lead

SR-11 - Auto Salvage YardSan Diego, California

February 5, 2010Project No. 106637001

mg/kg µg/kg µg/kg µg/kg mg/kg Detected Metal mg/kg

HA-1 DUP-01 0.5 1/6/2010 ND -- -- -- 6.2 -- --

HA-1-0.5 0.5 1/6/2010 120 -- -- -- 6.9 -- --

HA-1-2 2.0 1/6/2010 -- -- -- -- -- -- --

HA-2-0.5 0.5 1/6/2010 17 -- -- -- 5.2 -- --

HA-2-2 2.0 1/6/2010 -- -- -- -- -- -- --

HA-3-0.5 0.5 1/6/2010 75 -- -- -- 5.9 -- --

HA-3-2 2.0 1/6/2010 -- -- -- -- -- -- --

Arsenic 10

Barium 110

Chromium 16

Cobalt 4.5

Copper 17

Lead 21

Nickel 9.7

Vanadium 27

Zinc 43

HA-4-2 2.0 1/6/2010 -- -- -- -- -- -- --

HA-5-0.5 0.5 1/6/2010 1700 ND -- -- 11 -- --

HA-5-2 2.0 1/6/2010 ND -- -- -- -- -- --

HA-6-0.5 0.5 1/6/2010 ND -- -- -- 5.9 -- --

HA-6-2 2.0 1/6/2010 -- -- -- -- -- -- --

HA-7-0.5 0.5 1/6/2010 1800 ND ND ND 15 -- --

HA-7-2 2.0 1/6/2010 ND -- -- -- -- -- --

HA-8-0.5 0.5 1/6/2010 2300 ND ND ND 12 -- --

HA-8-2 2.0 1/6/2010 ND -- -- -- -- -- --

HA-9 DUP-02 0.5 1/7/2010 3100 -- -- -- 14 -- --

21

Sample Depth

(feet bgs)

Table 1 - Summary of Soil Sample Analytical Results

HA-4HA-4-0.5 0.5 1/6/2010 440 -- -- --

HA-2

Title 22 Metals

HA-1

VOCs Total LeadSVOCs PCBsBoring

IDSample

ID

HA-6

HA-7

Date Collected

TPH (C8-C40)

HA-8

HA-3

HA-5

106637001 T Analytical.xls 1 of 2

SR-11 - Auto Salvage YardSan Diego, California

February 5, 2010Project No. 106637001

mg/kg µg/kg µg/kg µg/kg mg/kg Detected Metal mg/kg

Sample Depth

(feet bgs)

Table 1 - Summary of Soil Sample Analytical Results

Title 22 MetalsVOCs Total LeadSVOCs PCBsBoring

IDSample

IDDate

Collected

TPH (C8-C40)

Arsenic 3.0

Barium 110

Chromium 24

Cobalt 3.3

Copper 9.1

Lead 37

Nickel 10

Vanadium 26

Zinc 32

HA-9-2 2.0 1/7/2010 ND -- -- -- -- -- --

HA-10-0.5 0.5 1/7/2010 180 -- -- -- 10 -- --

HA-10-2 2.0 1/7/2010 -- -- -- -- -- -- --

HA-11-0.5 0.5 1/7/2010 1700 ND -- -- 12 -- --

HA-11-2 2.0 1/7/2010 ND -- -- -- -- -- --

HA-12-0.5 0.5 1/7/2010 190 -- -- -- 4.4 -- --

HA-12-2 2.0 1/7/2010 -- -- -- -- -- -- --

HA-13-0.5 0.5 1/7/2010 180 -- -- -- 4.8 -- --

HA-13-2 2.0 1/7/2010 -- -- -- -- -- -- --

HA-14-0.5 0.5 1/7/2010 58 -- -- -- 7.7 -- --

HA-14-2 2.0 1/7/2010 -- -- -- -- -- -- --

HA-15-0.5 0.5 1/7/2010 73 -- -- -- 13 -- --

HA-15-2 2.0 1/7/2010 -- -- -- -- -- -- --

Notes:

-- = not analyzed

bgs = below ground surface

mg/kg = milligrams per kilogram

ND = not detected at or above the laboratory reporting limit

PCBs = polychlorinated biphenyls by USEPA test method 8082

TPH (C8-C40) = total petroleum hydrocarbons extended range by USEPA test method 8015B(M)

ug/kg = micrograms per kilogram

Title 22 Metals = title 22 metals by USEPA test method 6010B

SVOCs = semivolatile organic compounds by USEPA test method 8270C

Total Lead = total lead by USEPA test method 6010B

HA-9-0.5 0.5 1/7/2010 1600 ND -- -- 37

HA-12

HA-9

HA-10

HA-11

VOCs = volatile organic compounds by USEPA test method 8260B

HA-13

HA-14

HA-15

106637001 T Analytical.xls 2 of 2


106637001 R.doc

APPENDIX A

LABORATORY REPORTS

3275 Walnut Avenue, Signal Hill, CA 90755 Tel: 562. 989.4045 Fax: 562.989.4040

14-Jan-10Date:Advanced Technology Laboratories

Project: SR-11: AUTO SALVAGE YARD, 106637001CLIENT: Ninyo & Moore

Lab Order: 109486Work Order Sample Summary

Lab Sample ID Client Sample ID Collection DateMatrix Date Received

Contract No:

Date Reported

109486-001A DUP-01 1/6/2010 1/7/2010 1/14/2010Soil

109486-002A HA-1-0.5 1/6/2010 8:44:00 AM 1/7/2010 1/14/2010Soil

109486-004A HA-2-0.5 1/6/2010 9:15:00 AM 1/7/2010 1/14/2010Soil

109486-006A HA-3-0.5 1/6/2010 9:39:00 AM 1/7/2010 1/14/2010Soil

109486-007A HA-3-2 1/6/2010 9:44:00 AM 1/7/2010 1/14/2010Soil

109486-008A HA-4-0.5 1/6/2010 10:29:00 AM 1/7/2010 1/14/2010Soil

109486-009A HA-4-2 1/6/2010 10:36:00 AM 1/7/2010 1/14/2010Soil

109486-010A HA-5-0.5 1/6/2010 10:59:00 AM 1/7/2010 1/14/2010Soil

109486-011A HA-5-2 1/6/2010 11:02:00 AM 1/7/2010 1/14/2010Soil

109486-012A HA-6-0.5 1/6/2010 12:37:00 PM 1/7/2010 1/14/2010Soil

109486-013A HA-6-2 1/6/2010 12:47:00 PM 1/7/2010 1/14/2010Soil

109486-014A HA-8-0.5 1/6/2010 1:01:00 PM 1/7/2010 1/14/2010Soil

109486-015A HA-8-2 1/6/2010 1:05:00 PM 1/7/2010 1/14/2010Soil

109486-016A HA-7-0.5 1/6/2010 1:32:00 PM 1/7/2010 1/14/2010Soil

109486-017A HA-7-2 1/6/2010 1:41:00 PM 1/7/2010 1/14/2010Soil

109486-018B QCEB-01 1/6/2010 1:59:00 PM 1/7/2010 1/14/2010Water

109486-018C QCEB-01 1/6/2010 1:59:00 PM 1/7/2010 1/14/2010Water

109486-018D QCEB-01 1/6/2010 1:59:00 PM 1/7/2010 1/14/2010Water

109486-018E QCEB-01 1/6/2010 1:59:00 PM 1/7/2010 1/14/2010Water

Page 1 of 1

2 of 25




Lab Order: 109486CASE NARRATIVE

Sample Receiving / General Comments

Samples for EPA 8082 and EPA 8270C analyses were preserved with sodium thiosulfate.

Headspace <5-6mm was noted on one of the voa vial of sample QCTB-01.

Analytical Comments for EPA 8015B(M)

Sample 109486-008ADUP, RPD for Sample Duplicate (DUP) is outside criteria; however, the Laboratory Control Sample (LCS) validated the analytical batch.

Page 2 of 22

3 of 25


Project: SR-11: AUTO SALVAGE YARD, 10663700

Client Sample ID: DUP-01Collection Date: 1/6/2010

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Ninyo & MooreLab Order: 109486

Lab ID: 109486-001A

DF

Advanced Technology Laboratories Print Date: 14-Jan-10

PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3050B

RunID: ICP8_100112E 61036QC Batch: PrepDate: 1/11/2010

Lead 1/12/2010 06:58 PM1.0 mg/Kg 16.2HYDROCARBON CHAIN IDENTIFICATION

EPA 8015B(M)

Analyst: CBR

LUFT

RunID: GC16_100111C 61027QC Batch: PrepDate: 1/11/2010

T/R Hydrocarbons: C8-C10 1/11/2010 05:15 PM10 mg/Kg 1NDT/R Hydrocarbons: C10-C18 1/11/2010 05:15 PM10 mg/Kg 1NDT/R Hydrocarbons: C18-C28 1/11/2010 05:15 PM10 mg/Kg 1NDT/R Hydrocarbons: C28-C36 1/11/2010 05:15 PM10 mg/Kg 1NDT/R Hydrocarbons: C36-C40 1/11/2010 05:15 PM10 mg/Kg 1NDT/R Hydrocarbons: C8-C40 Total 1/11/2010 05:15 PM10 mg/Kg 1ND Surr: p-Terphenyl 1/11/2010 05:15 PM57-144 %REC 1114

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation rangeH Holding times for preparation or analysis exceeded ND Not Detected at the Reporting LimitS Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

DO Surrogate Diluted Out

4 of 25



Client Sample ID: HA-1-0.5Collection Date: 1/6/2010 8:44:00 AM

Matrix: SOIL



Lab ID: 109486-002A

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3050B

RunID: ICP8_100111C 61028QC Batch: PrepDate: 1/11/2010


EPA 8015B(M)

Analyst: CBR

LUFT


T/R Hydrocarbons: C8-C10 1/11/2010 05:54 PM10 mg/Kg 1NDT/R Hydrocarbons: C10-C18 1/11/2010 05:54 PM10 mg/Kg 1NDT/R Hydrocarbons: C18-C28 1/11/2010 05:54 PM10 mg/Kg 1NDT/R Hydrocarbons: C28-C36 1/11/2010 05:54 PM10 mg/Kg 141T/R Hydrocarbons: C36-C40 1/11/2010 05:54 PM10 mg/Kg 175T/R Hydrocarbons: C8-C40 Total 1/11/2010 05:54 PM10 mg/Kg 1120 Surr: p-Terphenyl 1/11/2010 05:54 PM57-144 %REC 1119



5 of 25




Matrix: SOIL



Lab ID: 109486-004A

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3050B



EPA 8015B(M)

Analyst: CBR

LUFT


T/R Hydrocarbons: C8-C10 1/11/2010 05:36 PM10 mg/Kg 1NDT/R Hydrocarbons: C10-C18 1/11/2010 05:36 PM10 mg/Kg 1NDT/R Hydrocarbons: C18-C28 1/11/2010 05:36 PM10 mg/Kg 1NDT/R Hydrocarbons: C28-C36 1/11/2010 05:36 PM10 mg/Kg 1NDT/R Hydrocarbons: C36-C40 1/11/2010 05:36 PM10 mg/Kg 117T/R Hydrocarbons: C8-C40 Total 1/11/2010 05:36 PM10 mg/Kg 117 Surr: p-Terphenyl 1/11/2010 05:36 PM57-144 %REC 1110



6 of 25




Matrix: SOIL



Lab ID: 109486-006A

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3050B



EPA 8015B(M)

Analyst: CBR

LUFT





7 of 25




Matrix: SOIL



Lab ID: 109486-008A

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3050B


Lead 1/11/2010 03:12 PM1.0 mg/Kg 121HYDROCARBON CHAIN IDENTIFICATION

EPA 8015B(M)

Analyst: CBR

LUFT


T/R Hydrocarbons: C8-C10 1/11/2010 06:13 PM10 mg/Kg 1NDT/R Hydrocarbons: C10-C18 1/11/2010 06:13 PM10 mg/Kg 113T/R Hydrocarbons: C18-C28 1/11/2010 06:13 PM10 mg/Kg 121T/R Hydrocarbons: C28-C36 1/11/2010 06:13 PM10 mg/Kg 1190T/R Hydrocarbons: C36-C40 1/11/2010 06:13 PM10 mg/Kg 1220T/R Hydrocarbons: C8-C40 Total 1/11/2010 06:13 PM10 mg/Kg 1440 Surr: p-Terphenyl 1/11/2010 06:13 PM57-144 %REC 1120



8 of 25




Matrix: SOIL



Lab ID: 109486-010A

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3050B



EPA 8015B(M)

Analyst: CBR

LUFT


T/R Hydrocarbons: C8-C10 1/11/2010 06:41 PM10 mg/Kg 118T/R Hydrocarbons: C10-C18 1/11/2010 06:41 PM10 mg/Kg 128T/R Hydrocarbons: C18-C28 1/11/2010 06:41 PM10 mg/Kg 1140T/R Hydrocarbons: C28-C36 1/11/2010 06:41 PM10 mg/Kg 1750T/R Hydrocarbons: C36-C40 1/11/2010 06:41 PM10 mg/Kg 1730T/R Hydrocarbons: C8-C40 Total 1/11/2010 06:41 PM10 mg/Kg 11700 Surr: p-Terphenyl 1/11/2010 06:41 PM57-144 %REC 1131



9 of 25



Client Sample ID: HA-6-0.5Collection Date: 1/6/2010 12:37:00 PM

Matrix: SOIL



Lab ID: 109486-012A

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3050B



EPA 8015B(M)

Analyst: CBR

LUFT


T/R Hydrocarbons: C8-C10 1/11/2010 05:26 PM10 mg/Kg 1NDT/R Hydrocarbons: C10-C18 1/11/2010 05:26 PM10 mg/Kg 1NDT/R Hydrocarbons: C18-C28 1/11/2010 05:26 PM10 mg/Kg 1NDT/R Hydrocarbons: C28-C36 1/11/2010 05:26 PM10 mg/Kg 1NDT/R Hydrocarbons: C36-C40 1/11/2010 05:26 PM10 mg/Kg 1NDT/R Hydrocarbons: C8-C40 Total 1/11/2010 05:26 PM10 mg/Kg 1ND Surr: p-Terphenyl 1/11/2010 05:26 PM57-144 %REC 1129



10 of 25




Matrix: SOIL



Lab ID: 109486-014A

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3050B



EPA 8015B(M)

Analyst: CBR

LUFT





11 of 25




Matrix: SOIL



Lab ID: 109486-016A

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3050B



EPA 8015B(M)

Analyst: CBR

LUFT





12 of 25



Client Sample ID: QCEB-01Collection Date: 1/6/2010 1:59:00 PM

Matrix: WATER



Lab ID: 109486-018D

DF


PQL

ANALYTICAL RESULTS

HYDROCARBON CHAIN IDENTIFICATIONEPA 8015B(M)

Analyst: CBR

EPA 3510C

RunID: GC16_100111D 61041QC Batch: PrepDate: 1/11/2010

T/R Hydrocarbons: C8-C10 1/11/2010 09:14 PM0.20 mg/L 1NDT/R Hydrocarbons: C10-C18 1/11/2010 09:14 PM0.20 mg/L 1NDT/R Hydrocarbons: C18-C28 1/11/2010 09:14 PM0.20 mg/L 1NDT/R Hydrocarbons: C28-C36 1/11/2010 09:14 PM0.20 mg/L 1NDT/R Hydrocarbons: C36-C40 1/11/2010 09:14 PM0.20 mg/L 1NDT/R Hydrocarbons: C8-C40 Total 1/11/2010 09:14 PM0.20 mg/L 1ND Surr: p-Terphenyl 1/11/2010 09:14 PM35-131 %REC 148.4



13 of 25




Matrix: WATER



Lab ID: 109486-018E

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3010A

RunID: ICP8_100112D 61037QC Batch: PrepDate: 1/11/2010

Lead 1/12/2010 06:11 PM0.0050 mg/L 1ND



14 of 25




CLIENT: Ninyo & MooreWork Order: 109486

ANALYTICAL QC SUMMARY REPORTTestCode: 6010_S

Sample ID: MB-61028

Batch ID: 61028 TestNo: EPA 6010B Analysis Date: 1/11/2010

Prep Date: 1/11/2010

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/Kg

PQL

Client ID: PBS

RunNo: 116819

SeqNo: 1854722

MBLKSampType: TestCode: 6010_S

EPA 3050B

Lead 1.00.284

Sample ID: LCS-61028




Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 116819

SeqNo: 1854723

LCSSampType: TestCode: 6010_S

EPA 3050B

Lead 50.00 98.3 80 1201.0 0.284149.412

Sample ID: 109486-016ADUP




Units: mg/Kg

PQL

Client ID: HA-7-0.5

RunNo: 116819

SeqNo: 1854726

DUPSampType: TestCode: 6010_S

EPA 3050B

Antimony 202.0 0 0NDArsenic 201.0 1.992 6.171.872Barium 201.0 124.5 8.57114.255Beryllium 201.0 0 0NDCadmium 201.0 0.2641 00.283Chromium 201.0 12.51 13.010.983Cobalt 201.0 3.490 3.953.355Copper 202.0 7.314 7.437.878Lead 201.0 15.29 2.9315.748Molybdenum 201.0 0 0NDNickel 201.0 7.840 8.067.232Selenium 201.0 0 0NDSilver 201.0 0 0NDThallium 201.0 0 0NDVanadium 201.0 29.52 4.5630.898Zinc 201.0 28.23 1.0628.535

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interferenceDO Surrogate Diluted Out Calculations are based on raw values

15 of 25





Sample ID: 109486-016AMS




Units: mg/Kg

PQL

Client ID: HA-7-0.5

RunNo: 116819

SeqNo: 1854727

MSSampType: TestCode: 6010_S

EPA 3050B

Antimony 125.0 70.6 25 1062.0 088.261Arsenic 125.0 77.8 42 1131.0 1.99299.295Barium 125.0 65.3 19 1401.0 124.5206.055Beryllium 125.0 82.2 50 1091.0 0102.765Cadmium 125.0 75.9 48 1061.0 0.264195.150Chromium 125.0 80.2 44 1161.0 12.51112.715Cobalt 125.0 76.7 47 1071.0 3.49099.362Copper 125.0 87.7 49 1242.0 7.314116.965Lead 125.0 76.3 33 1201.0 15.29110.643Molybdenum 125.0 79.9 46 1111.0 099.894Nickel 125.0 76.9 43 1111.0 7.840103.976Selenium 125.0 73.2 43 1041.0 091.477Silver 125.0 85.0 53 1141.0 0106.224Thallium 125.0 76.5 41 1071.0 095.638Vanadium 125.0 80.7 48 1161.0 29.52130.393Zinc 125.0 74.5 24 1291.0 28.23121.360

Sample ID: 109486-016AMSD




Units: mg/Kg

PQL

Client ID: HA-7-0.5

RunNo: 116819

SeqNo: 1854728

MSDSampType: TestCode: 6010_S

EPA 3050B

Antimony 125.0 78.0 25 106 202.0 0 88.26 9.9297.474Arsenic 125.0 85.2 42 113 201.0 1.992 99.30 8.83108.468Barium 125.0 80.5 19 140 201.0 124.5 206.1 8.86225.149Beryllium 125.0 89.8 50 109 201.0 0 102.8 8.86112.288Cadmium 125.0 82.5 48 106 201.0 0.2641 95.15 8.25103.339Chromium 125.0 88.6 44 116 201.0 12.51 112.7 8.96123.294Cobalt 125.0 83.8 47 107 201.0 3.490 99.36 8.60108.295Copper 125.0 97.7 49 124 202.0 7.314 117.0 10.2129.483Lead 125.0 81.2 33 120 201.0 15.29 110.6 5.39116.776



16 of 25









Units: mg/Kg

PQL

Client ID: HA-7-0.5

RunNo: 116819

SeqNo: 1854728


EPA 3050B

Molybdenum 125.0 87.2 46 111 201.0 0 99.89 8.77109.058Nickel 125.0 84.2 43 111 201.0 7.840 104.0 8.44113.136Selenium 125.0 79.6 43 104 201.0 0 91.48 8.3499.438Silver 125.0 93.3 53 114 201.0 0 106.2 9.29116.568Thallium 125.0 82.3 41 107 201.0 0 95.64 7.33102.916Vanadium 125.0 90.5 48 116 201.0 29.52 130.4 8.98142.650Zinc 125.0 81.3 24 129 201.0 28.23 121.4 6.73129.817



17 of 25





Sample ID: MB-61036




Units: mg/Kg

PQL

Client ID: PBS

RunNo: 116884

SeqNo: 1855414


EPA 3050B

Lead 1.0ND





Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 116884

SeqNo: 1855415


EPA 3050B

Lead 50.00 98.8 80 1201.0 049.412





Units: mg/Kg

PQL

Client ID: DUP-01

RunNo: 116884

SeqNo: 1855417


EPA 3050B

Lead 201.0 6.196 8.185.709





Units: mg/Kg

PQL

Client ID: DUP-01

RunNo: 116884

SeqNo: 1855418


EPA 3050B

Lead 125.0 88.2 33 1201.0 6.196116.403





Units: mg/Kg

PQL

Client ID: DUP-01

RunNo: 116884

SeqNo: 1855419


EPA 3050B

Lead 125.0 85.8 33 120 201.0 6.196 116.4 2.55113.478



18 of 25




ANALYTICAL QC SUMMARY REPORTTestCode: 6010_W

Sample ID: MB-61037




Units: mg/L

PQL

Client ID: PBW

RunNo: 116883

SeqNo: 1855406

MBLKSampType: TestCode: 6010_W

EPA 3010A

Lead 0.0050ND





Units: mg/L

PQL

Client ID: LCSW

RunNo: 116883

SeqNo: 1855407

LCSSampType: TestCode: 6010_W

EPA 3010A

Lead 1.000 92.5 85 1150.0050 00.925

Sample ID: 109486-018EDUP




Units: mg/L

PQL

Client ID: QCEB-01

RunNo: 116883

SeqNo: 1855409

DUPSampType: TestCode: 6010_W

EPA 3010A

Antimony 200.0050 0 0NDArsenic 200.010 0 0NDBarium 200.0030 0.03999 0NDBeryllium 200.0030 0 0NDCadmium 200.0030 0 0NDChromium 200.0030 0.001231 0NDCobalt 200.0030 0 0NDCopper 200.0050 0 0NDLead 200.0050 0 0NDMolybdenum 200.0050 0 0NDNickel 200.0050 0 0NDSelenium 200.010 0 0NDSilver 200.0030 0.01108 7.240.010Thallium 200.015 0 0NDVanadium 200.0030 0 0NDZinc 200.010 0.006496 00.005



19 of 25





Sample ID: 109486-018EMS




Units: mg/L

PQL

Client ID: QCEB-01

RunNo: 116883

SeqNo: 1855410

MSSampType: TestCode: 6010_W

EPA 3010A

Antimony 2.500 98.5 64 1300.0050 02.464Arsenic 2.500 95.8 66 1280.010 02.395Barium 2.500 95.1 60 1290.0030 0.039992.418Beryllium 2.500 98.4 77 1180.0030 02.461Cadmium 2.500 93.9 72 1220.0030 02.347Chromium 2.500 96.3 77 1160.0030 0.0012312.408Cobalt 2.500 96.1 66 1240.0030 02.403Copper 2.500 99.3 70 1300.0050 02.482Lead 2.500 95.7 71 1210.0050 02.393Molybdenum 2.500 95.8 64 1290.0050 02.395Nickel 2.500 96.0 63 1250.0050 02.400Selenium 2.500 95.4 73 1240.010 02.384Silver 2.500 100 60 1380.0030 0.011082.523Thallium 2.500 98.8 66 1250.015 02.469Vanadium 2.500 97.6 79 1180.0030 02.441Zinc 2.500 94.1 71 1200.010 0.0064962.360

Sample ID: 109486-018EMSD




Units: mg/L

PQL

Client ID: QCEB-01

RunNo: 116883

SeqNo: 1855411

MSDSampType: TestCode: 6010_W

EPA 3010A

Antimony 2.500 97.0 64 130 200.0050 0 2.464 1.562.425Arsenic 2.500 94.1 66 128 200.010 0 2.395 1.732.354Barium 2.500 94.7 60 129 200.0030 0.03999 2.418 0.4592.407Beryllium 2.500 96.3 77 118 200.0030 0 2.461 2.152.409Cadmium 2.500 93.5 72 122 200.0030 0 2.347 0.4142.338Chromium 2.500 95.6 77 116 200.0030 0.001231 2.408 0.6652.392Cobalt 2.500 95.7 66 124 200.0030 0 2.403 0.4602.392Copper 2.500 98.5 70 130 200.0050 0 2.482 0.7872.462Lead 2.500 93.4 71 121 200.0050 0 2.393 2.392.336



20 of 25









Units: mg/L

PQL

Client ID: QCEB-01

RunNo: 116883

SeqNo: 1855411


EPA 3010A

Molybdenum 2.500 95.4 64 129 200.0050 0 2.395 0.4012.385Nickel 2.500 95.3 63 125 200.0050 0 2.400 0.6762.384Selenium 2.500 93.7 73 124 200.010 0 2.384 1.782.342Silver 2.500 99.4 60 138 200.0030 0.01108 2.523 1.072.496Thallium 2.500 97.0 66 125 200.015 0 2.469 1.812.425Vanadium 2.500 96.7 79 118 200.0030 0 2.441 0.9202.418Zinc 2.500 93.6 71 120 200.010 0.006496 2.360 0.6092.346



21 of 25




ANALYTICAL QC SUMMARY REPORTTestCode: HC_S_ATL

Sample ID: MB-61027

Batch ID: 61027 TestNo: EPA 8015B(M Analysis Date: 1/11/2010



Units: mg/Kg

PQL

Client ID: PBS

RunNo: 116841

SeqNo: 1854890

MBLKSampType: TestCode: HC_S_ATL

LUFT

T/R Hydrocarbons: C8-C10 10NDT/R Hydrocarbons: C10-C18 10NDT/R Hydrocarbons: C18-C28 10NDT/R Hydrocarbons: C28-C36 10NDT/R Hydrocarbons: C36-C40 10NDT/R Hydrocarbons: C8-C40 Total 10ND Surr: p-Terphenyl 80.00 119 57 14494.850





Units: mg/Kg

PQL

Client ID: HA-4-0.5

RunNo: 116841

SeqNo: 1854903

DUPSampType: TestCode: HC_S_ATL

LUFT

T/R Hydrocarbons: C8-C10 2010 0 0NDT/R Hydrocarbons: C10-C18 2010 13.19 13.311.550T/R Hydrocarbons: C18-C28 2010 20.80 1.9420.400T/R Hydrocarbons: C28-C36 2010 190.0 19.7155.930T/R Hydrocarbons: C36-C40 20 R10 218.0 27.5165.240T/R Hydrocarbons: C8-C40 Total 20 R10 442.0 22.3353.120 Surr: p-Terphenyl 80.00 126 57 144 00101.030



22 of 25




ANALYTICAL QC SUMMARY REPORTTestCode: HC_W_ATL

Sample ID: MB-61041




Units: mg/L

PQL

Client ID: PBW

RunNo: 116844

SeqNo: 1854981

MBLKSampType: TestCode: HC_W_ATL

EPA 3510C

T/R Hydrocarbons: C8-C10 0.20NDT/R Hydrocarbons: C10-C18 0.20NDT/R Hydrocarbons: C18-C28 0.20NDT/R Hydrocarbons: C28-C36 0.20NDT/R Hydrocarbons: C36-C40 0.20NDT/R Hydrocarbons: C8-C40 Total 0.20ND Surr: p-Terphenyl 0.08000 60.0 35 1310.048



23 of 25





ANALYTICAL QC SUMMARY REPORTBatchID: 61027





Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 116841

SeqNo: 1854869

LCSSampType: TestCode: 8015_S_DM

LUFT

DRO 1000 105 81 12810 01047.580 Surr: p-Terphenyl 80.00 141 57 144113.110





Units: mg/Kg

PQL

Client ID: HA-4-0.5

RunNo: 116841

SeqNo: 1854883

MSSampType: TestCode: 8015_S_DM

LUFT

DRO 1000 108 58 14510 46.391129.340 Surr: p-Terphenyl 80.00 143 57 144114.590





Units: mg/Kg

PQL

Client ID: HA-4-0.5

RunNo: 116841

SeqNo: 1854884

MSDSampType: TestCode: 8015_S_DM

LUFT

DRO 1000 102 58 145 2010 46.39 1129 5.941064.180 Surr: p-Terphenyl 80.00 137 57 144 00109.920



24 of 25










Units: mg/L

PQL

Client ID: LCSW

RunNo: 116844

SeqNo: 1854968

LCSSampType: TestCode: 8015_W_DM

EPA 3510C

DRO 1.000 76.2 42 1180.20 00.762 Surr: p-Terphenyl 0.08000 59.8 35 1310.048

Sample ID: MB-61041MS




Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 116844

SeqNo: 1854969

MSSampType: TestCode: 8015_W_DM

EPA 3510C


Sample ID: MB-61041MSD




Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 116844

SeqNo: 1854970

MSDSampType: TestCode: 8015_W_DM

EPA 3510C

DRO 1.000 87.9 42 118 200.20 0 0.8552 2.770.879 Surr: p-Terphenyl 0.08000 66.9 35 131 000.054



25 of 25






Contract No:

Date Reported

109494-001A HA-9-0.5 1/7/2010 8:56:00 AM 1/8/2010 1/15/2010Soil

109494-002A HA-9-2 1/7/2010 9:02:00 AM 1/8/2010 1/15/2010Soil

109494-003A HA-10-0.5 1/7/2010 9:18:00 AM 1/8/2010 1/15/2010Soil

109494-004A HA-10-2 1/7/2010 9:25:00 AM 1/8/2010 1/15/2010Soil

109494-005A HA-11-0.5 1/7/2010 9:38:00 AM 1/8/2010 1/15/2010Soil

109494-006A HA-11-2 1/7/2010 9:46:00 AM 1/8/2010 1/15/2010Soil

109494-007A HA-12-0.5 1/7/2010 10:15:00 AM 1/8/2010 1/15/2010Soil

109494-008A HA-12-2 1/7/2010 10:20:00 AM 1/8/2010 1/15/2010Soil

109494-009A HA-13-0.5 1/7/2010 10:40:00 AM 1/8/2010 1/15/2010Soil

109494-010A HA-13-2 1/7/2010 10:45:00 AM 1/8/2010 1/15/2010Soil

109494-011A DUP-02 1/7/2010 1/8/2010 1/15/2010Soil

109494-012A HA-14-0.5 1/7/2010 12:13:00 PM 1/8/2010 1/15/2010Soil

109494-013A HA-14-2 1/7/2010 12:24:00 PM 1/8/2010 1/15/2010Soil

109494-014A HA-15-0.5 1/7/2010 12:37:00 PM 1/8/2010 1/15/2010Soil

109494-015A HA-15-2 1/7/2010 12:41:00 PM 1/8/2010 1/15/2010Soil

109494-016A QCEB-02 1/7/2010 1:00:00 PM 1/8/2010 1/15/2010Water

109494-016B QCEB-02 1/7/2010 1:00:00 PM 1/8/2010 1/15/2010Water

109494-016C QCEB-02 1/7/2010 1:00:00 PM 1/8/2010 1/15/2010Water

109494-016D QCEB-02 1/7/2010 1:00:00 PM 1/8/2010 1/15/2010Water

109494-016E QCEB-02 1/7/2010 1:00:00 PM 1/8/2010 1/15/2010Water

Page 1 of 1

2 of 20







Analytical Comments for EPA 6010B

Sample 109494-014A-DUP, RPD for Sample Duplicate (DUP) is outside criteria; however, the Laboratory Control Sample (LCS) validated the analytical batch.

Analytical Comments for EPA 8015B(M)


Page 2 of 17

3 of 20




Matrix: SOIL



Lab ID: 109494-001A

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3050B



EPA 8015B(M)

Analyst: CBR

LUFT

RunID: GC16_100112A 61068QC Batch: PrepDate: 1/12/2010




4 of 20




Matrix: SOIL



Lab ID: 109494-003A

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3050B



EPA 8015B(M)

Analyst: CBR

LUFT





5 of 20




Matrix: SOIL



Lab ID: 109494-005A

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3050B



EPA 8015B(M)

Analyst: CBR

LUFT


T/R Hydrocarbons: C8-C10 1/12/2010 09:50 PM10 mg/Kg 1NDT/R Hydrocarbons: C10-C18 1/12/2010 09:50 PM10 mg/Kg 1NDT/R Hydrocarbons: C18-C28 1/12/2010 09:50 PM10 mg/Kg 1120T/R Hydrocarbons: C28-C36 1/12/2010 09:50 PM10 mg/Kg 1680T/R Hydrocarbons: C36-C40 1/12/2010 09:50 PM10 mg/Kg 1880T/R Hydrocarbons: C8-C40 Total 1/12/2010 09:50 PM10 mg/Kg 11700 Surr: p-Terphenyl 1/12/2010 09:50 PM57-144 %REC 193.9



6 of 20




Matrix: SOIL



Lab ID: 109494-007A

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3050B



EPA 8015B(M)

Analyst: CBR

LUFT





7 of 20




Matrix: SOIL



Lab ID: 109494-009A

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3050B



EPA 8015B(M)

Analyst: CBR

LUFT





8 of 20



Client Sample ID: DUP-02Collection Date: 1/7/2010

Matrix: SOIL



Lab ID: 109494-011A

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: SMH

EPA 3050B

RunID: ICP8_100113F 61040QC Batch: PrepDate: 1/11/2010


EPA 8015B(M)

Analyst: CBR

LUFT





9 of 20




Matrix: SOIL



Lab ID: 109494-012A

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: SMH

EPA 3050B



EPA 8015B(M)

Analyst: CBR

LUFT





10 of 20




Matrix: SOIL



Lab ID: 109494-014A

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: SMH

EPA 3050B



EPA 8015B(M)

Analyst: CBR

LUFT





11 of 20




Matrix: WATER



Lab ID: 109494-016D

DF


PQL

ANALYTICAL RESULTS


Analyst: CBR

EPA 3510C

RunID: GC16_100111D 61041QC Batch: PrepDate: 1/11/2010

T/R Hydrocarbons: C8-C10 1/11/2010 10:11 PM0.20 mg/L 1NDT/R Hydrocarbons: C10-C18 1/11/2010 10:11 PM0.20 mg/L 1NDT/R Hydrocarbons: C18-C28 1/11/2010 10:11 PM0.20 mg/L 1NDT/R Hydrocarbons: C28-C36 1/11/2010 10:11 PM0.20 mg/L 1NDT/R Hydrocarbons: C36-C40 1/11/2010 10:11 PM0.20 mg/L 1NDT/R Hydrocarbons: C8-C40 Total 1/11/2010 10:11 PM0.20 mg/L 1ND Surr: p-Terphenyl 1/11/2010 10:11 PM35-131 %REC 150.0



12 of 20




Matrix: WATER



Lab ID: 109494-016E

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3010A


Lead 1/12/2010 06:28 PM0.0050 mg/L 1ND



13 of 20






Sample ID: MB-61036




Units: mg/Kg

PQL

Client ID: PBS

RunNo: 116884

SeqNo: 1855414


EPA 3050B

Lead 1.0ND





Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 116884

SeqNo: 1855415


EPA 3050B

Lead 50.00 98.8 80 1201.0 049.412





Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 116884

SeqNo: 1855417


EPA 3050B

Lead 201.0 6.196 8.185.709





Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 116884

SeqNo: 1855418


EPA 3050B

Lead 125.0 88.2 33 1201.0 6.196116.403





Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 116884

SeqNo: 1855419


EPA 3050B

Lead 125.0 85.8 33 120 201.0 6.196 116.4 2.55113.478



14 of 20





Sample ID: MB-61040




Units: mg/Kg

PQL

Client ID: PBS

RunNo: 116936

SeqNo: 1856221


EPA 3050B

Lead 1.0ND





Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 116936

SeqNo: 1856222


EPA 3050B

Lead 50.00 100 80 1201.0 050.225

Sample ID: 109494-014A-DUP




Units: mg/Kg

PQL

Client ID: HA-15-0.5

RunNo: 116936

SeqNo: 1856226


EPA 3050B

Lead 20 R1.0 13.42 23.610.591

Sample ID: 109494-014A-MS




Units: mg/Kg

PQL


RunNo: 116936

SeqNo: 1856227


EPA 3050B

Lead 125.0 84.8 33 1201.0 13.42119.437

Sample ID: 109494-014A-MSD




Units: mg/Kg

PQL


RunNo: 116936

SeqNo: 1856228


EPA 3050B

Lead 125.0 88.1 33 120 201.0 13.42 119.4 3.37123.534



15 of 20





Sample ID: MB-61037




Units: mg/L

PQL

Client ID: PBW

RunNo: 116883

SeqNo: 1855406


EPA 3010A

Lead 0.0050ND





Units: mg/L

PQL

Client ID: LCSW

RunNo: 116883

SeqNo: 1855407


EPA 3010A

Lead 1.000 92.5 85 1150.0050 00.925





Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 116883

SeqNo: 1855409


EPA 3010A

Lead 200.0050 0 0ND





Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 116883

SeqNo: 1855410


EPA 3010A

Lead 2.500 95.7 71 1210.0050 02.393





Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 116883

SeqNo: 1855411


EPA 3010A

Lead 2.500 93.4 71 121 200.0050 0 2.393 2.392.336



16 of 20




ANALYTICAL QC SUMMARY REPORTTestCode: HC_S_ATL

Sample ID: MB-61068




Units: mg/Kg

PQL

Client ID: PBS

RunNo: 116902

SeqNo: 1855621


LUFT






Units: mg/Kg

PQL

Client ID: HA-9-0.5

RunNo: 116902

SeqNo: 1855633


LUFT

T/R Hydrocarbons: C8-C10 2010 0 0NDT/R Hydrocarbons: C10-C18 2010 11.98 14.713.880T/R Hydrocarbons: C18-C28 2010 145.4 18.9175.790T/R Hydrocarbons: C28-C36 2010 747.3 12.6847.680T/R Hydrocarbons: C36-C40 20 R10 697.2 26.9914.240T/R Hydrocarbons: C8-C40 Total 2010 1602 19.71951.590 Surr: p-Terphenyl 80.00 129 57 144 00103.000



17 of 20




ANALYTICAL QC SUMMARY REPORTTestCode: HC_W_ATL

Sample ID: MB-61041




Units: mg/L

PQL

Client ID: PBW

RunNo: 116844

SeqNo: 1854981

MBLKSampType: TestCode: HC_W_ATL

EPA 3510C

T/R Hydrocarbons: C8-C10 0.20NDT/R Hydrocarbons: C10-C18 0.20NDT/R Hydrocarbons: C18-C28 0.20NDT/R Hydrocarbons: C28-C36 0.20NDT/R Hydrocarbons: C36-C40 0.20NDT/R Hydrocarbons: C8-C40 Total 0.20ND Surr: p-Terphenyl 0.08000 60.0 35 1310.048



18 of 20










Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 116902

SeqNo: 1855580


LUFT






Units: mg/Kg

PQL

Client ID: HA-9-0.5

RunNo: 116902

SeqNo: 1855592


LUFT

DRO 1000 112 58 14510 214.31333.540 Surr: p-Terphenyl 80.00 135 57 144107.850





Units: mg/Kg

PQL

Client ID: HA-9-0.5

RunNo: 116902

SeqNo: 1855593


LUFT

DRO 1000 134 58 145 2010 214.3 1334 15.31554.530 Surr: p-Terphenyl 80.00 129 57 144 00103.050



19 of 20










Units: mg/L

PQL

Client ID: LCSW

RunNo: 116844

SeqNo: 1854968

LCSSampType: TestCode: 8015_W_DM

EPA 3510C






Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 116844

SeqNo: 1854969

MSSampType: TestCode: 8015_W_DM

EPA 3510C






Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 116844

SeqNo: 1854970

MSDSampType: TestCode: 8015_W_DM

EPA 3510C

DRO 1.000 87.9 42 118 200.20 0 0.8552 2.770.879 Surr: p-Terphenyl 0.08000 66.9 35 131 000.054



20 of 20






Contract No:

Date Reported

109486-001A DUP-01 1/6/2010 1/7/2010 1/22/2010Soil

109486-002A HA-1-0.5 1/6/2010 8:44:00 AM 1/7/2010 1/22/2010Soil

109486-004A HA-2-0.5 1/6/2010 9:15:00 AM 1/7/2010 1/22/2010Soil

109486-006A HA-3-0.5 1/6/2010 9:39:00 AM 1/7/2010 1/22/2010Soil

109486-007A HA-3-2 1/6/2010 9:44:00 AM 1/7/2010 1/22/2010Soil

109486-008A HA-4-0.5 1/6/2010 10:29:00 AM 1/7/2010 1/22/2010Soil

109486-009A HA-4-2 1/6/2010 10:36:00 AM 1/7/2010 1/22/2010Soil

109486-010A HA-5-0.5 1/6/2010 10:59:00 AM 1/7/2010 1/22/2010Soil

109486-011A HA-5-2 1/6/2010 11:02:00 AM 1/7/2010 1/22/2010Soil

109486-012A HA-6-0.5 1/6/2010 12:37:00 PM 1/7/2010 1/22/2010Soil

109486-013A HA-6-2 1/6/2010 12:47:00 PM 1/7/2010 1/22/2010Soil

109486-014A HA-8-0.5 1/6/2010 1:01:00 PM 1/7/2010 1/22/2010Soil

109486-015A HA-8-2 1/6/2010 1:05:00 PM 1/7/2010 1/22/2010Soil

109486-016A HA-7-0.5 1/6/2010 1:32:00 PM 1/7/2010 1/22/2010Soil

109486-017A HA-7-2 1/6/2010 1:41:00 PM 1/7/2010 1/22/2010Soil

109486-018A QCEB-01 1/6/2010 1:59:00 PM 1/7/2010 1/22/2010Water

109486-018B QCEB-01 1/6/2010 1:59:00 PM 1/7/2010 1/22/2010Water

109486-018C QCEB-01 1/6/2010 1:59:00 PM 1/7/2010 1/22/2010Water

109486-018D QCEB-01 1/6/2010 1:59:00 PM 1/7/2010 1/22/2010Water

109486-018E QCEB-01 1/6/2010 1:59:00 PM 1/7/2010 1/22/2010Water

Page 1 of 1

2 of 71







Headspace <5-6mm was noted on one of the voa vial of sample QCTB-01.

Analytical Comments for EPA 8270C

Samples 109486-014A and 109486-016A, dilution was necessary due to sample extract was black.

Sample 109486-016A, surrogate recovery biased low possibly due to matrix interferences.

Samples 109486-016AMS and 109486-016AMSD, Matrix Spike (MS) and Matrix Spike Duplicate (MSD) are outside recovery criteria; however, the analytical batch was validated by the Laboratory Control Sample (LCS).

Page 2 of 27

3 of 71




Matrix: SOIL



Lab ID: 109486-008A

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3050B


Antimony 1/11/2010 03:12 PM2.0 mg/Kg 1NDArsenic 1/11/2010 03:12 PM1.0 mg/Kg 110Barium 1/11/2010 03:12 PM1.0 mg/Kg 1110Beryllium 1/11/2010 03:12 PM1.0 mg/Kg 1NDCadmium 1/11/2010 03:12 PM1.0 mg/Kg 1NDChromium 1/11/2010 03:12 PM1.0 mg/Kg 116Cobalt 1/11/2010 03:12 PM1.0 mg/Kg 14.5Copper 1/11/2010 03:12 PM2.0 mg/Kg 117Lead 1/11/2010 03:12 PM1.0 mg/Kg 121Molybdenum 1/11/2010 03:12 PM1.0 mg/Kg 1NDNickel 1/11/2010 03:12 PM1.0 mg/Kg 19.7Selenium 1/11/2010 03:12 PM1.0 mg/Kg 1NDSilver 1/11/2010 03:12 PM1.0 mg/Kg 1NDThallium 1/11/2010 03:12 PM1.0 mg/Kg 1NDVanadium 1/11/2010 03:12 PM1.0 mg/Kg 127Zinc 1/11/2010 03:12 PM1.0 mg/Kg 143

MERCURY BY COLD VAPOR TECHNIQUEEPA 7471A

Analyst: ILRunID: AA1_100119C 61215QC Batch: PrepDate: 1/19/2010

Mercury 1/19/2010 02:46 PM0.10 mg/Kg 1ND



4 of 71




Matrix: SOIL



Lab ID: 109486-010A

DF


PQL

ANALYTICAL RESULTS

VOLATILE ORGANIC COMPOUNDS BY GC/MSEPA 8260B

Analyst: HHRunID: MS4_100115B K10VS018QC Batch: PrepDate:

1,1,1,2-Tetrachloroethane 1/15/2010 07:27 PM5.0 µg/Kg 1ND1,1,1-Trichloroethane 1/15/2010 07:27 PM5.0 µg/Kg 1ND1,1,2,2-Tetrachloroethane 1/15/2010 07:27 PM5.0 µg/Kg 1ND1,1,2-Trichloroethane 1/15/2010 07:27 PM5.0 µg/Kg 1ND1,1-Dichloroethane 1/15/2010 07:27 PM5.0 µg/Kg 1ND1,1-Dichloroethene 1/15/2010 07:27 PM5.0 µg/Kg 1ND1,1-Dichloropropene 1/15/2010 07:27 PM5.0 µg/Kg 1ND1,2,3-Trichlorobenzene 1/15/2010 07:27 PM5.0 µg/Kg 1ND1,2,3-Trichloropropane 1/15/2010 07:27 PM5.0 µg/Kg 1ND1,2,4-Trichlorobenzene 1/15/2010 07:27 PM5.0 µg/Kg 1ND1,2,4-Trimethylbenzene 1/15/2010 07:27 PM5.0 µg/Kg 1ND1,2-Dibromo-3-chloropropane 1/15/2010 07:27 PM10 µg/Kg 1ND1,2-Dibromoethane 1/15/2010 07:27 PM5.0 µg/Kg 1ND1,2-Dichlorobenzene 1/15/2010 07:27 PM5.0 µg/Kg 1ND1,2-Dichloroethane 1/15/2010 07:27 PM5.0 µg/Kg 1ND1,2-Dichloropropane 1/15/2010 07:27 PM5.0 µg/Kg 1ND1,3,5-Trimethylbenzene 1/15/2010 07:27 PM5.0 µg/Kg 1ND1,3-Dichlorobenzene 1/15/2010 07:27 PM5.0 µg/Kg 1ND1,3-Dichloropropane 1/15/2010 07:27 PM5.0 µg/Kg 1ND1,4-Dichlorobenzene 1/15/2010 07:27 PM5.0 µg/Kg 1ND2,2-Dichloropropane 1/15/2010 07:27 PM5.0 µg/Kg 1ND2-Chlorotoluene 1/15/2010 07:27 PM5.0 µg/Kg 1ND4-Chlorotoluene 1/15/2010 07:27 PM5.0 µg/Kg 1ND4-Isopropyltoluene 1/15/2010 07:27 PM5.0 µg/Kg 1NDBenzene 1/15/2010 07:27 PM5.0 µg/Kg 1NDBromobenzene 1/15/2010 07:27 PM5.0 µg/Kg 1NDBromodichloromethane 1/15/2010 07:27 PM5.0 µg/Kg 1NDBromoform 1/15/2010 07:27 PM5.0 µg/Kg 1NDBromomethane 1/15/2010 07:27 PM5.0 µg/Kg 1NDCarbon tetrachloride 1/15/2010 07:27 PM5.0 µg/Kg 1NDChlorobenzene 1/15/2010 07:27 PM5.0 µg/Kg 1NDChloroethane 1/15/2010 07:27 PM5.0 µg/Kg 1NDChloroform 1/15/2010 07:27 PM5.0 µg/Kg 1NDChloromethane 1/15/2010 07:27 PM5.0 µg/Kg 1NDcis-1,2-Dichloroethene 1/15/2010 07:27 PM5.0 µg/Kg 1ND



5 of 71




Matrix: SOIL



Lab ID: 109486-010A

DF


PQL

ANALYTICAL RESULTS



cis-1,3-Dichloropropene 1/15/2010 07:27 PM5.0 µg/Kg 1NDDibromochloromethane 1/15/2010 07:27 PM5.0 µg/Kg 1NDDibromomethane 1/15/2010 07:27 PM5.0 µg/Kg 1NDDichlorodifluoromethane 1/15/2010 07:27 PM5.0 µg/Kg 1NDEthylbenzene 1/15/2010 07:27 PM5.0 µg/Kg 1NDHexachlorobutadiene 1/15/2010 07:27 PM5.0 µg/Kg 1NDIsopropylbenzene 1/15/2010 07:27 PM5.0 µg/Kg 1NDm,p-Xylene 1/15/2010 07:27 PM10 µg/Kg 1NDMethylene chloride 1/15/2010 07:27 PM5.0 µg/Kg 1NDn-Butylbenzene 1/15/2010 07:27 PM5.0 µg/Kg 1NDn-Propylbenzene 1/15/2010 07:27 PM5.0 µg/Kg 1NDNaphthalene 1/15/2010 07:27 PM5.0 µg/Kg 1NDo-Xylene 1/15/2010 07:27 PM5.0 µg/Kg 1NDsec-Butylbenzene 1/15/2010 07:27 PM5.0 µg/Kg 1NDStyrene 1/15/2010 07:27 PM5.0 µg/Kg 1NDtert-Butylbenzene 1/15/2010 07:27 PM5.0 µg/Kg 1NDTetrachloroethene 1/15/2010 07:27 PM5.0 µg/Kg 1NDToluene 1/15/2010 07:27 PM5.0 µg/Kg 1NDtrans-1,2-Dichloroethene 1/15/2010 07:27 PM5.0 µg/Kg 1NDTrichloroethene 1/15/2010 07:27 PM5.0 µg/Kg 1NDTrichlorofluoromethane 1/15/2010 07:27 PM5.0 µg/Kg 1NDVinyl chloride 1/15/2010 07:27 PM5.0 µg/Kg 1ND Surr: 1,2-Dichloroethane-d4 1/15/2010 07:27 PM70-130 %REC 1108 Surr: 4-Bromofluorobenzene 1/15/2010 07:27 PM70-130 %REC 186.7 Surr: Dibromofluoromethane 1/15/2010 07:27 PM70-130 %REC 190.3 Surr: Toluene-d8 1/15/2010 07:27 PM70-130 %REC 185.6



6 of 71



Client Sample ID: HA-5-2Collection Date: 1/6/2010 11:02:00 AM

Matrix: SOIL



Lab ID: 109486-011A

DF


PQL

ANALYTICAL RESULTS


Analyst: CBR

LUFT


T/R Hydrocarbons: C8-C10 1/20/2010 10:51 AM10 mg/Kg 1NDT/R Hydrocarbons: C10-C18 1/20/2010 10:51 AM10 mg/Kg 1NDT/R Hydrocarbons: C18-C28 1/20/2010 10:51 AM10 mg/Kg 1NDT/R Hydrocarbons: C28-C36 1/20/2010 10:51 AM10 mg/Kg 1NDT/R Hydrocarbons: C36-C40 1/20/2010 10:51 AM10 mg/Kg 1NDT/R Hydrocarbons: C8-C40 Total 1/20/2010 10:51 AM10 mg/Kg 1ND Surr: p-Terphenyl 1/20/2010 10:51 AM57-144 %REC 1136



7 of 71




Matrix: SOIL



Lab ID: 109486-014A

DF


PQL

ANALYTICAL RESULTS

PCBS BY GC/ECDEPA 8082

Analyst: BB

EPA 3550B

RunID: GC5_100119B 61238QC Batch: PrepDate: 1/19/2010

Aroclor 1016 1/20/2010 11:31 AM16 µg/Kg 1NDAroclor 1221 1/20/2010 11:31 AM33 µg/Kg 1NDAroclor 1232 1/20/2010 11:31 AM16 µg/Kg 1NDAroclor 1242 1/20/2010 11:31 AM16 µg/Kg 1NDAroclor 1248 1/20/2010 11:31 AM16 µg/Kg 1NDAroclor 1254 1/20/2010 11:31 AM16 µg/Kg 1NDAroclor 1260 1/20/2010 11:31 AM16 µg/Kg 1NDAroclor 1262 1/20/2010 11:31 AM16 µg/Kg 1NDAroclor 1268 1/20/2010 11:31 AM16 µg/Kg 1ND Surr: Decachlorobiphenyl 1/20/2010 11:31 AM30-124 %REC 174.0 Surr: Tetrachloro-m-xylene 1/20/2010 11:31 AM40-118 %REC 1101



1,1,1,2-Tetrachloroethane 1/15/2010 07:42 PM5.0 µg/Kg 1ND1,1,1-Trichloroethane 1/15/2010 07:42 PM5.0 µg/Kg 1ND1,1,2,2-Tetrachloroethane 1/15/2010 07:42 PM5.0 µg/Kg 1ND1,1,2-Trichloroethane 1/15/2010 07:42 PM5.0 µg/Kg 1ND1,1-Dichloroethane 1/15/2010 07:42 PM5.0 µg/Kg 1ND1,1-Dichloroethene 1/15/2010 07:42 PM5.0 µg/Kg 1ND1,1-Dichloropropene 1/15/2010 07:42 PM5.0 µg/Kg 1ND1,2,3-Trichlorobenzene 1/15/2010 07:42 PM5.0 µg/Kg 1ND1,2,3-Trichloropropane 1/15/2010 07:42 PM5.0 µg/Kg 1ND1,2,4-Trichlorobenzene 1/15/2010 07:42 PM5.0 µg/Kg 1ND1,2,4-Trimethylbenzene 1/15/2010 07:42 PM5.0 µg/Kg 1ND1,2-Dibromo-3-chloropropane 1/15/2010 07:42 PM10 µg/Kg 1ND1,2-Dibromoethane 1/15/2010 07:42 PM5.0 µg/Kg 1ND1,2-Dichlorobenzene 1/15/2010 07:42 PM5.0 µg/Kg 1ND1,2-Dichloroethane 1/15/2010 07:42 PM5.0 µg/Kg 1ND1,2-Dichloropropane 1/15/2010 07:42 PM5.0 µg/Kg 1ND1,3,5-Trimethylbenzene 1/15/2010 07:42 PM5.0 µg/Kg 1ND1,3-Dichlorobenzene 1/15/2010 07:42 PM5.0 µg/Kg 1ND1,3-Dichloropropane 1/15/2010 07:42 PM5.0 µg/Kg 1ND1,4-Dichlorobenzene 1/15/2010 07:42 PM5.0 µg/Kg 1ND2,2-Dichloropropane 1/15/2010 07:42 PM5.0 µg/Kg 1ND



8 of 71




Matrix: SOIL



Lab ID: 109486-014A

DF


PQL

ANALYTICAL RESULTS



2-Chlorotoluene 1/15/2010 07:42 PM5.0 µg/Kg 1ND4-Chlorotoluene 1/15/2010 07:42 PM5.0 µg/Kg 1ND4-Isopropyltoluene 1/15/2010 07:42 PM5.0 µg/Kg 1NDBenzene 1/15/2010 07:42 PM5.0 µg/Kg 1NDBromobenzene 1/15/2010 07:42 PM5.0 µg/Kg 1NDBromodichloromethane 1/15/2010 07:42 PM5.0 µg/Kg 1NDBromoform 1/15/2010 07:42 PM5.0 µg/Kg 1NDBromomethane 1/15/2010 07:42 PM5.0 µg/Kg 1NDCarbon tetrachloride 1/15/2010 07:42 PM5.0 µg/Kg 1NDChlorobenzene 1/15/2010 07:42 PM5.0 µg/Kg 1NDChloroethane 1/15/2010 07:42 PM5.0 µg/Kg 1NDChloroform 1/15/2010 07:42 PM5.0 µg/Kg 1NDChloromethane 1/15/2010 07:42 PM5.0 µg/Kg 1NDcis-1,2-Dichloroethene 1/15/2010 07:42 PM5.0 µg/Kg 1NDcis-1,3-Dichloropropene 1/15/2010 07:42 PM5.0 µg/Kg 1NDDibromochloromethane 1/15/2010 07:42 PM5.0 µg/Kg 1NDDibromomethane 1/15/2010 07:42 PM5.0 µg/Kg 1NDDichlorodifluoromethane 1/15/2010 07:42 PM5.0 µg/Kg 1NDEthylbenzene 1/15/2010 07:42 PM5.0 µg/Kg 1NDHexachlorobutadiene 1/15/2010 07:42 PM5.0 µg/Kg 1NDIsopropylbenzene 1/15/2010 07:42 PM5.0 µg/Kg 1NDm,p-Xylene 1/15/2010 07:42 PM10 µg/Kg 1NDMethylene chloride 1/15/2010 07:42 PM5.0 µg/Kg 1NDn-Butylbenzene 1/15/2010 07:42 PM5.0 µg/Kg 1NDn-Propylbenzene 1/15/2010 07:42 PM5.0 µg/Kg 1NDNaphthalene 1/15/2010 07:42 PM5.0 µg/Kg 1NDo-Xylene 1/15/2010 07:42 PM5.0 µg/Kg 1NDsec-Butylbenzene 1/15/2010 07:42 PM5.0 µg/Kg 1NDStyrene 1/15/2010 07:42 PM5.0 µg/Kg 1NDtert-Butylbenzene 1/15/2010 07:42 PM5.0 µg/Kg 1NDTetrachloroethene 1/15/2010 07:42 PM5.0 µg/Kg 1NDToluene 1/15/2010 07:42 PM5.0 µg/Kg 1NDtrans-1,2-Dichloroethene 1/15/2010 07:42 PM5.0 µg/Kg 1NDTrichloroethene 1/15/2010 07:42 PM5.0 µg/Kg 1NDTrichlorofluoromethane 1/15/2010 07:42 PM5.0 µg/Kg 1ND



9 of 71




Matrix: SOIL



Lab ID: 109486-014A

DF


PQL

ANALYTICAL RESULTS



Vinyl chloride 1/15/2010 07:42 PM5.0 µg/Kg 1ND Surr: 1,2-Dichloroethane-d4 1/15/2010 07:42 PM70-130 %REC 1104 Surr: 4-Bromofluorobenzene 1/15/2010 07:42 PM70-130 %REC 184.2 Surr: Dibromofluoromethane 1/15/2010 07:42 PM70-130 %REC 191.6 Surr: Toluene-d8 1/15/2010 07:42 PM70-130 %REC 183.2

SEMIVOLATILE ORGANIC COMPOUNDS BY GC/MSEPA 8270C

Analyst: DMP

EPA 3550B

RunID: MS 13_100120A 61240QC Batch: PrepDate: 1/20/2010

1,2,4-Trichlorobenzene 1/21/2010 02:32 AM6600 µg/Kg 10ND1,2-Dichlorobenzene 1/21/2010 02:32 AM6600 µg/Kg 10ND1,3-Dichlorobenzene 1/21/2010 02:32 AM6600 µg/Kg 10ND1,4-Dichlorobenzene 1/21/2010 02:32 AM6600 µg/Kg 10ND2,4,5-Trichlorophenol 1/21/2010 02:32 AM6600 µg/Kg 10ND2,4,6-Trichlorophenol 1/21/2010 02:32 AM6600 µg/Kg 10ND2,4-Dichlorophenol 1/21/2010 02:32 AM33000 µg/Kg 10ND2,4-Dimethylphenol 1/21/2010 02:32 AM6600 µg/Kg 10ND2,4-Dinitrophenol 1/21/2010 02:32 AM33000 µg/Kg 10ND2,4-Dinitrotoluene 1/21/2010 02:32 AM6600 µg/Kg 10ND2,6-Dinitrotoluene 1/21/2010 02:32 AM6600 µg/Kg 10ND2-Chloronaphthalene 1/21/2010 02:32 AM6600 µg/Kg 10ND2-Chlorophenol 1/21/2010 02:32 AM6600 µg/Kg 10ND2-Methylnaphthalene 1/21/2010 02:32 AM6600 µg/Kg 10ND2-Methylphenol 1/21/2010 02:32 AM6600 µg/Kg 10ND2-Nitroaniline 1/21/2010 02:32 AM33000 µg/Kg 10ND2-Nitrophenol 1/21/2010 02:32 AM6600 µg/Kg 10ND3,3´-Dichlorobenzidine 1/21/2010 02:32 AM13000 µg/Kg 10ND3-Nitroaniline 1/21/2010 02:32 AM33000 µg/Kg 10ND4,6-Dinitro-2-methylphenol 1/21/2010 02:32 AM33000 µg/Kg 10ND4-Bromophenyl-phenylether 1/21/2010 02:32 AM6600 µg/Kg 10ND4-Chloro-3-methylphenol 1/21/2010 02:32 AM13000 µg/Kg 10ND4-Chloroaniline 1/21/2010 02:32 AM13000 µg/Kg 10ND4-Chlorophenyl-phenylether 1/21/2010 02:32 AM6600 µg/Kg 10ND4-Methylphenol 1/21/2010 02:32 AM6600 µg/Kg 10ND4-Nitroaniline 1/21/2010 02:32 AM33000 µg/Kg 10ND4-Nitrophenol 1/21/2010 02:32 AM33000 µg/Kg 10ND



10 of 71




Matrix: SOIL



Lab ID: 109486-014A

DF


PQL

ANALYTICAL RESULTS


Analyst: DMP

EPA 3550B


Acenaphthene 1/21/2010 02:32 AM6600 µg/Kg 10NDAcenaphthylene 1/21/2010 02:32 AM6600 µg/Kg 10NDAnthracene 1/21/2010 02:32 AM6600 µg/Kg 10NDBenzidine (M) 1/21/2010 02:32 AM33000 µg/Kg 10NDBenzo(a)anthracene 1/21/2010 02:32 AM6600 µg/Kg 10NDBenzo(a)pyrene 1/21/2010 02:32 AM6600 µg/Kg 10NDBenzo(b)fluoranthene 1/21/2010 02:32 AM6600 µg/Kg 10NDBenzo(g,h,i)perylene 1/21/2010 02:32 AM6600 µg/Kg 10NDBenzo(k)fluoranthene 1/21/2010 02:32 AM6600 µg/Kg 10NDBenzoic acid 1/21/2010 02:32 AM33000 µg/Kg 10NDBenzyl alcohol 1/21/2010 02:32 AM13000 µg/Kg 10NDBis(2-chloroethoxy)methane 1/21/2010 02:32 AM6600 µg/Kg 10NDBis(2-chloroethyl)ether 1/21/2010 02:32 AM6600 µg/Kg 10NDBis(2-chloroisopropyl)ether 1/21/2010 02:32 AM6600 µg/Kg 10NDBis(2-ethylhexyl)phthalate 1/21/2010 02:32 AM6600 µg/Kg 10NDButylbenzylphthalate 1/21/2010 02:32 AM6600 µg/Kg 10NDChrysene 1/21/2010 02:32 AM6600 µg/Kg 10NDDi-n-butylphthalate 1/21/2010 02:32 AM6600 µg/Kg 10NDDi-n-octylphthalate 1/21/2010 02:32 AM6600 µg/Kg 10NDDibenz(a,h)anthracene 1/21/2010 02:32 AM6600 µg/Kg 10NDDibenzofuran 1/21/2010 02:32 AM6600 µg/Kg 10NDDiethylphthalate 1/21/2010 02:32 AM6600 µg/Kg 10NDDimethylphthalate 1/21/2010 02:32 AM6600 µg/Kg 10NDFluoranthene 1/21/2010 02:32 AM6600 µg/Kg 10NDFluorene 1/21/2010 02:32 AM6600 µg/Kg 10NDHexachlorobenzene 1/21/2010 02:32 AM6600 µg/Kg 10NDHexachlorobutadiene 1/21/2010 02:32 AM13000 µg/Kg 10NDHexachlorocyclopentadiene 1/21/2010 02:32 AM13000 µg/Kg 10NDHexachloroethane 1/21/2010 02:32 AM6600 µg/Kg 10NDIndeno(1,2,3-cd)pyrene 1/21/2010 02:32 AM6600 µg/Kg 10NDIsophorone 1/21/2010 02:32 AM6600 µg/Kg 10NDN-Nitrosodi-n-propylamine 1/21/2010 02:32 AM6600 µg/Kg 10NDN-Nitrosodiphenylamine 1/21/2010 02:32 AM6600 µg/Kg 10NDNaphthalene 1/21/2010 02:32 AM6600 µg/Kg 10NDNitrobenzene 1/21/2010 02:32 AM6600 µg/Kg 10ND



11 of 71




Matrix: SOIL



Lab ID: 109486-014A

DF


PQL

ANALYTICAL RESULTS


Analyst: DMP

EPA 3550B


Pentachlorophenol 1/21/2010 02:32 AM33000 µg/Kg 10NDPhenanthrene 1/21/2010 02:32 AM6600 µg/Kg 10NDPhenol 1/21/2010 02:32 AM6600 µg/Kg 10NDPyrene 1/21/2010 02:32 AM6600 µg/Kg 10ND Surr: 1,2-Dichlorobenzene-d4 1/21/2010 02:32 AM45-105 %REC 1075.5 Surr: 2,4,6-Tribromophenol 1/21/2010 02:32 AM41-129 %REC 1061.5 Surr: 2-Chlorophenol-d4 1/21/2010 02:32 AM55-108 %REC 1077.3 Surr: 2-Fluorobiphenyl 1/21/2010 02:32 AM56-114 %REC 1087.1 Surr: 2-Fluorophenol 1/21/2010 02:32 AM50-108 %REC 1075.7 Surr: 4-Terphenyl-d14 1/21/2010 02:32 AM59-141 %REC 1081.1 Surr: Nitrobenzene-d5 1/21/2010 02:32 AM45-114 %REC 1079.9 Surr: Phenol-d5 1/21/2010 02:32 AM46-118 %REC 1074.1



12 of 71



Client Sample ID: HA-8-2Collection Date: 1/6/2010 1:05:00 PM

Matrix: SOIL



Lab ID: 109486-015A

DF


PQL

ANALYTICAL RESULTS


Analyst: CBR

LUFT





13 of 71




Matrix: SOIL



Lab ID: 109486-016A

DF


PQL

ANALYTICAL RESULTS


Analyst: BB

EPA 3550B

RunID: GC5_100119B 61238QC Batch: PrepDate: 1/19/2010

Aroclor 1016 1/20/2010 12:01 PM16 µg/Kg 1NDAroclor 1221 1/20/2010 12:01 PM33 µg/Kg 1NDAroclor 1232 1/20/2010 12:01 PM16 µg/Kg 1NDAroclor 1242 1/20/2010 12:01 PM16 µg/Kg 1NDAroclor 1248 1/20/2010 12:01 PM16 µg/Kg 1NDAroclor 1254 1/20/2010 12:01 PM16 µg/Kg 1NDAroclor 1260 1/20/2010 12:01 PM16 µg/Kg 1NDAroclor 1262 1/20/2010 12:01 PM16 µg/Kg 1NDAroclor 1268 1/20/2010 12:01 PM16 µg/Kg 1ND Surr: Decachlorobiphenyl 1/20/2010 12:01 PM30-124 %REC 176.1 Surr: Tetrachloro-m-xylene 1/20/2010 12:01 PM40-118 %REC 195.9



1,1,1,2-Tetrachloroethane 1/15/2010 07:58 PM5.0 µg/Kg 1ND1,1,1-Trichloroethane 1/15/2010 07:58 PM5.0 µg/Kg 1ND1,1,2,2-Tetrachloroethane 1/15/2010 07:58 PM5.0 µg/Kg 1ND1,1,2-Trichloroethane 1/15/2010 07:58 PM5.0 µg/Kg 1ND1,1-Dichloroethane 1/15/2010 07:58 PM5.0 µg/Kg 1ND1,1-Dichloroethene 1/15/2010 07:58 PM5.0 µg/Kg 1ND1,1-Dichloropropene 1/15/2010 07:58 PM5.0 µg/Kg 1ND1,2,3-Trichlorobenzene 1/15/2010 07:58 PM5.0 µg/Kg 1ND1,2,3-Trichloropropane 1/15/2010 07:58 PM5.0 µg/Kg 1ND1,2,4-Trichlorobenzene 1/15/2010 07:58 PM5.0 µg/Kg 1ND1,2,4-Trimethylbenzene 1/15/2010 07:58 PM5.0 µg/Kg 1ND1,2-Dibromo-3-chloropropane 1/15/2010 07:58 PM10 µg/Kg 1ND1,2-Dibromoethane 1/15/2010 07:58 PM5.0 µg/Kg 1ND1,2-Dichlorobenzene 1/15/2010 07:58 PM5.0 µg/Kg 1ND1,2-Dichloroethane 1/15/2010 07:58 PM5.0 µg/Kg 1ND1,2-Dichloropropane 1/15/2010 07:58 PM5.0 µg/Kg 1ND1,3,5-Trimethylbenzene 1/15/2010 07:58 PM5.0 µg/Kg 1ND1,3-Dichlorobenzene 1/15/2010 07:58 PM5.0 µg/Kg 1ND1,3-Dichloropropane 1/15/2010 07:58 PM5.0 µg/Kg 1ND1,4-Dichlorobenzene 1/15/2010 07:58 PM5.0 µg/Kg 1ND2,2-Dichloropropane 1/15/2010 07:58 PM5.0 µg/Kg 1ND



14 of 71




Matrix: SOIL



Lab ID: 109486-016A

DF


PQL

ANALYTICAL RESULTS



2-Chlorotoluene 1/15/2010 07:58 PM5.0 µg/Kg 1ND4-Chlorotoluene 1/15/2010 07:58 PM5.0 µg/Kg 1ND4-Isopropyltoluene 1/15/2010 07:58 PM5.0 µg/Kg 1NDBenzene 1/15/2010 07:58 PM5.0 µg/Kg 1NDBromobenzene 1/15/2010 07:58 PM5.0 µg/Kg 1NDBromodichloromethane 1/15/2010 07:58 PM5.0 µg/Kg 1NDBromoform 1/15/2010 07:58 PM5.0 µg/Kg 1NDBromomethane 1/15/2010 07:58 PM5.0 µg/Kg 1NDCarbon tetrachloride 1/15/2010 07:58 PM5.0 µg/Kg 1NDChlorobenzene 1/15/2010 07:58 PM5.0 µg/Kg 1NDChloroethane 1/15/2010 07:58 PM5.0 µg/Kg 1NDChloroform 1/15/2010 07:58 PM5.0 µg/Kg 1NDChloromethane 1/15/2010 07:58 PM5.0 µg/Kg 1NDcis-1,2-Dichloroethene 1/15/2010 07:58 PM5.0 µg/Kg 1NDcis-1,3-Dichloropropene 1/15/2010 07:58 PM5.0 µg/Kg 1NDDibromochloromethane 1/15/2010 07:58 PM5.0 µg/Kg 1NDDibromomethane 1/15/2010 07:58 PM5.0 µg/Kg 1NDDichlorodifluoromethane 1/15/2010 07:58 PM5.0 µg/Kg 1NDEthylbenzene 1/15/2010 07:58 PM5.0 µg/Kg 1NDHexachlorobutadiene 1/15/2010 07:58 PM5.0 µg/Kg 1NDIsopropylbenzene 1/15/2010 07:58 PM5.0 µg/Kg 1NDm,p-Xylene 1/15/2010 07:58 PM10 µg/Kg 1NDMethylene chloride 1/15/2010 07:58 PM5.0 µg/Kg 1NDn-Butylbenzene 1/15/2010 07:58 PM5.0 µg/Kg 1NDn-Propylbenzene 1/15/2010 07:58 PM5.0 µg/Kg 1NDNaphthalene 1/15/2010 07:58 PM5.0 µg/Kg 1NDo-Xylene 1/15/2010 07:58 PM5.0 µg/Kg 1NDsec-Butylbenzene 1/15/2010 07:58 PM5.0 µg/Kg 1NDStyrene 1/15/2010 07:58 PM5.0 µg/Kg 1NDtert-Butylbenzene 1/15/2010 07:58 PM5.0 µg/Kg 1NDTetrachloroethene 1/15/2010 07:58 PM5.0 µg/Kg 1NDToluene 1/15/2010 07:58 PM5.0 µg/Kg 1NDtrans-1,2-Dichloroethene 1/15/2010 07:58 PM5.0 µg/Kg 1NDTrichloroethene 1/15/2010 07:58 PM5.0 µg/Kg 1NDTrichlorofluoromethane 1/15/2010 07:58 PM5.0 µg/Kg 1ND



15 of 71




Matrix: SOIL



Lab ID: 109486-016A

DF


PQL

ANALYTICAL RESULTS



Vinyl chloride 1/15/2010 07:58 PM5.0 µg/Kg 1ND Surr: 1,2-Dichloroethane-d4 1/15/2010 07:58 PM70-130 %REC 1103 Surr: 4-Bromofluorobenzene 1/15/2010 07:58 PM70-130 %REC 184.8 Surr: Dibromofluoromethane 1/15/2010 07:58 PM70-130 %REC 194.1 Surr: Toluene-d8 1/15/2010 07:58 PM70-130 %REC 181.6


Analyst: DMP

EPA 3550B


1,2,4-Trichlorobenzene 1/21/2010 02:04 AM1600 µg/Kg 5ND1,2-Dichlorobenzene 1/21/2010 02:04 AM1600 µg/Kg 5ND1,3-Dichlorobenzene 1/21/2010 02:04 AM1600 µg/Kg 5ND1,4-Dichlorobenzene 1/21/2010 02:04 AM1600 µg/Kg 5ND2,4,5-Trichlorophenol 1/21/2010 02:04 AM1600 µg/Kg 5ND2,4,6-Trichlorophenol 1/21/2010 02:04 AM1600 µg/Kg 5ND2,4-Dichlorophenol 1/21/2010 02:04 AM8200 µg/Kg 5ND2,4-Dimethylphenol 1/21/2010 02:04 AM1600 µg/Kg 5ND2,4-Dinitrophenol 1/21/2010 02:04 AM8200 µg/Kg 5ND2,4-Dinitrotoluene 1/21/2010 02:04 AM1600 µg/Kg 5ND2,6-Dinitrotoluene 1/21/2010 02:04 AM1600 µg/Kg 5ND2-Chloronaphthalene 1/21/2010 02:04 AM1600 µg/Kg 5ND2-Chlorophenol 1/21/2010 02:04 AM1600 µg/Kg 5ND2-Methylnaphthalene 1/21/2010 02:04 AM1600 µg/Kg 5ND2-Methylphenol 1/21/2010 02:04 AM1600 µg/Kg 5ND2-Nitroaniline 1/21/2010 02:04 AM8200 µg/Kg 5ND2-Nitrophenol 1/21/2010 02:04 AM1600 µg/Kg 5ND3,3´-Dichlorobenzidine 1/21/2010 02:04 AM3300 µg/Kg 5ND3-Nitroaniline 1/21/2010 02:04 AM8200 µg/Kg 5ND4,6-Dinitro-2-methylphenol 1/21/2010 02:04 AM8200 µg/Kg 5ND4-Bromophenyl-phenylether 1/21/2010 02:04 AM1600 µg/Kg 5ND4-Chloro-3-methylphenol 1/21/2010 02:04 AM3300 µg/Kg 5ND4-Chloroaniline 1/21/2010 02:04 AM3300 µg/Kg 5ND4-Chlorophenyl-phenylether 1/21/2010 02:04 AM1600 µg/Kg 5ND4-Methylphenol 1/21/2010 02:04 AM1600 µg/Kg 5ND4-Nitroaniline 1/21/2010 02:04 AM8200 µg/Kg 5ND4-Nitrophenol 1/21/2010 02:04 AM8200 µg/Kg 5ND



16 of 71




Matrix: SOIL



Lab ID: 109486-016A

DF


PQL

ANALYTICAL RESULTS


Analyst: DMP

EPA 3550B


Acenaphthene 1/21/2010 02:04 AM1600 µg/Kg 5NDAcenaphthylene 1/21/2010 02:04 AM1600 µg/Kg 5NDAnthracene 1/21/2010 02:04 AM1600 µg/Kg 5NDBenzidine (M) 1/21/2010 02:04 AM8200 µg/Kg 5NDBenzo(a)anthracene 1/21/2010 02:04 AM1600 µg/Kg 5NDBenzo(a)pyrene 1/21/2010 02:04 AM1600 µg/Kg 5NDBenzo(b)fluoranthene 1/21/2010 02:04 AM1600 µg/Kg 5NDBenzo(g,h,i)perylene 1/21/2010 02:04 AM1600 µg/Kg 5NDBenzo(k)fluoranthene 1/21/2010 02:04 AM1600 µg/Kg 5NDBenzoic acid 1/21/2010 02:04 AM8200 µg/Kg 5NDBenzyl alcohol 1/21/2010 02:04 AM3300 µg/Kg 5NDBis(2-chloroethoxy)methane 1/21/2010 02:04 AM1600 µg/Kg 5NDBis(2-chloroethyl)ether 1/21/2010 02:04 AM1600 µg/Kg 5NDBis(2-chloroisopropyl)ether 1/21/2010 02:04 AM1600 µg/Kg 5NDBis(2-ethylhexyl)phthalate 1/21/2010 02:04 AM1600 µg/Kg 5NDButylbenzylphthalate 1/21/2010 02:04 AM1600 µg/Kg 5NDChrysene 1/21/2010 02:04 AM1600 µg/Kg 5NDDi-n-butylphthalate 1/21/2010 02:04 AM1600 µg/Kg 5NDDi-n-octylphthalate 1/21/2010 02:04 AM1600 µg/Kg 5NDDibenz(a,h)anthracene 1/21/2010 02:04 AM1600 µg/Kg 5NDDibenzofuran 1/21/2010 02:04 AM1600 µg/Kg 5NDDiethylphthalate 1/21/2010 02:04 AM1600 µg/Kg 5NDDimethylphthalate 1/21/2010 02:04 AM1600 µg/Kg 5NDFluoranthene 1/21/2010 02:04 AM1600 µg/Kg 5NDFluorene 1/21/2010 02:04 AM1600 µg/Kg 5NDHexachlorobenzene 1/21/2010 02:04 AM1600 µg/Kg 5NDHexachlorobutadiene 1/21/2010 02:04 AM3300 µg/Kg 5NDHexachlorocyclopentadiene 1/21/2010 02:04 AM3300 µg/Kg 5NDHexachloroethane 1/21/2010 02:04 AM1600 µg/Kg 5NDIndeno(1,2,3-cd)pyrene 1/21/2010 02:04 AM1600 µg/Kg 5NDIsophorone 1/21/2010 02:04 AM1600 µg/Kg 5NDN-Nitrosodi-n-propylamine 1/21/2010 02:04 AM1600 µg/Kg 5NDN-Nitrosodiphenylamine 1/21/2010 02:04 AM1600 µg/Kg 5NDNaphthalene 1/21/2010 02:04 AM1600 µg/Kg 5NDNitrobenzene 1/21/2010 02:04 AM1600 µg/Kg 5ND



17 of 71




Matrix: SOIL



Lab ID: 109486-016A

DF


PQL

ANALYTICAL RESULTS


Analyst: DMP

EPA 3550B


Pentachlorophenol 1/21/2010 02:04 AM8200 µg/Kg 5NDPhenanthrene 1/21/2010 02:04 AM1600 µg/Kg 5NDPhenol 1/21/2010 02:04 AM1600 µg/Kg 5NDPyrene 1/21/2010 02:04 AM1600 µg/Kg 5ND Surr: 1,2-Dichlorobenzene-d4 1/21/2010 02:04 AM45-105 %REC 546.6 Surr: 2,4,6-Tribromophenol S 1/21/2010 02:04 AM41-129 %REC 538.5 Surr: 2-Chlorophenol-d4 S 1/21/2010 02:04 AM55-108 %REC 546.1 Surr: 2-Fluorobiphenyl S 1/21/2010 02:04 AM56-114 %REC 551.6 Surr: 2-Fluorophenol S 1/21/2010 02:04 AM50-108 %REC 545.6 Surr: 4-Terphenyl-d14 S 1/21/2010 02:04 AM59-141 %REC 547.2 Surr: Nitrobenzene-d5 1/21/2010 02:04 AM45-114 %REC 550.2 Surr: Phenol-d5 S 1/21/2010 02:04 AM46-118 %REC 545.6



18 of 71



Client Sample ID: HA-7-2Collection Date: 1/6/2010 1:41:00 PM

Matrix: SOIL



Lab ID: 109486-017A

DF


PQL

ANALYTICAL RESULTS


Analyst: CBR

LUFT





19 of 71




Matrix: WATER



Lab ID: 109486-018A

DF


PQL

ANALYTICAL RESULTS


Analyst: SLLRunID: MS11_100118A A10VW016QC Batch: PrepDate:

1,1,1,2-Tetrachloroethane 1/18/2010 11:16 AM5.0 µg/L 1ND1,1,1-Trichloroethane 1/18/2010 11:16 AM5.0 µg/L 1ND1,1,2,2-Tetrachloroethane 1/18/2010 11:16 AM5.0 µg/L 1ND1,1,2-Trichloroethane 1/18/2010 11:16 AM5.0 µg/L 1ND1,1-Dichloroethane 1/18/2010 11:16 AM5.0 µg/L 1ND1,1-Dichloroethene 1/18/2010 11:16 AM5.0 µg/L 1ND1,1-Dichloropropene 1/18/2010 11:16 AM5.0 µg/L 1ND1,2,3-Trichlorobenzene 1/18/2010 11:16 AM5.0 µg/L 1ND1,2,3-Trichloropropane 1/18/2010 11:16 AM5.0 µg/L 1ND1,2,4-Trichlorobenzene 1/18/2010 11:16 AM5.0 µg/L 1ND1,2,4-Trimethylbenzene 1/18/2010 11:16 AM5.0 µg/L 1ND1,2-Dibromo-3-chloropropane 1/18/2010 11:16 AM5.0 µg/L 1ND1,2-Dibromoethane 1/18/2010 11:16 AM5.0 µg/L 1ND1,2-Dichlorobenzene 1/18/2010 11:16 AM5.0 µg/L 1ND1,2-Dichloroethane 1/18/2010 11:16 AM5.0 µg/L 1ND1,2-Dichloropropane 1/18/2010 11:16 AM5.0 µg/L 1ND1,3,5-Trimethylbenzene 1/18/2010 11:16 AM5.0 µg/L 1ND1,3-Dichlorobenzene 1/18/2010 11:16 AM5.0 µg/L 1ND1,3-Dichloropropane 1/18/2010 11:16 AM5.0 µg/L 1ND1,4-Dichlorobenzene 1/18/2010 11:16 AM5.0 µg/L 1ND2,2-Dichloropropane 1/18/2010 11:16 AM5.0 µg/L 1ND2-Chlorotoluene 1/18/2010 11:16 AM5.0 µg/L 1ND4-Chlorotoluene 1/18/2010 11:16 AM5.0 µg/L 1ND4-Isopropyltoluene 1/18/2010 11:16 AM5.0 µg/L 1NDBenzene 1/18/2010 11:16 AM5.0 µg/L 1NDBromobenzene 1/18/2010 11:16 AM5.0 µg/L 1NDBromodichloromethane 1/18/2010 11:16 AM5.0 µg/L 1NDBromoform 1/18/2010 11:16 AM5.0 µg/L 1NDBromomethane 1/18/2010 11:16 AM5.0 µg/L 1NDCarbon tetrachloride 1/18/2010 11:16 AM5.0 µg/L 1NDChlorobenzene 1/18/2010 11:16 AM5.0 µg/L 1NDChloroethane 1/18/2010 11:16 AM5.0 µg/L 1NDChloroform 1/18/2010 11:16 AM5.0 µg/L 1NDChloromethane 1/18/2010 11:16 AM5.0 µg/L 1NDcis-1,2-Dichloroethene 1/18/2010 11:16 AM5.0 µg/L 1ND



20 of 71




Matrix: WATER



Lab ID: 109486-018A

DF


PQL

ANALYTICAL RESULTS



cis-1,3-Dichloropropene 1/18/2010 11:16 AM5.0 µg/L 1NDDibromochloromethane 1/18/2010 11:16 AM5.0 µg/L 1NDDibromomethane 1/18/2010 11:16 AM5.0 µg/L 1NDDichlorodifluoromethane 1/18/2010 11:16 AM5.0 µg/L 1NDEthylbenzene 1/18/2010 11:16 AM5.0 µg/L 1NDHexachlorobutadiene 1/18/2010 11:16 AM5.0 µg/L 1NDIsopropylbenzene 1/18/2010 11:16 AM5.0 µg/L 1NDm,p-Xylene 1/18/2010 11:16 AM10 µg/L 1NDMethylene chloride 1/18/2010 11:16 AM5.0 µg/L 1NDn-Butylbenzene 1/18/2010 11:16 AM5.0 µg/L 1NDn-Propylbenzene 1/18/2010 11:16 AM5.0 µg/L 1NDNaphthalene 1/18/2010 11:16 AM5.0 µg/L 1NDo-Xylene 1/18/2010 11:16 AM5.0 µg/L 1NDsec-Butylbenzene 1/18/2010 11:16 AM5.0 µg/L 1NDStyrene 1/18/2010 11:16 AM5.0 µg/L 1NDtert-Butylbenzene 1/18/2010 11:16 AM5.0 µg/L 1NDTetrachloroethene 1/18/2010 11:16 AM5.0 µg/L 1NDToluene 1/18/2010 11:16 AM5.0 µg/L 1NDtrans-1,2-Dichloroethene 1/18/2010 11:16 AM5.0 µg/L 1NDTrichloroethene 1/18/2010 11:16 AM5.0 µg/L 1NDTrichlorofluoromethane 1/18/2010 11:16 AM5.0 µg/L 1NDVinyl chloride 1/18/2010 11:16 AM5.0 µg/L 1ND Surr: 1,2-Dichloroethane-d4 1/18/2010 11:16 AM70-130 %REC 198.8 Surr: 4-Bromofluorobenzene 1/18/2010 11:16 AM70-130 %REC 1114 Surr: Dibromofluoromethane 1/18/2010 11:16 AM70-130 %REC 1102



21 of 71




Matrix: WATER



Lab ID: 109486-018B

DF


PQL

ANALYTICAL RESULTS


Analyst: DMP

EPA 3510C

RunID: MS 13_100108B 61000QC Batch: PrepDate: 1/8/2010

1,2,4-Trichlorobenzene 1/9/2010 12:09 AM10 µg/L 1ND1,2-Dichlorobenzene 1/9/2010 12:09 AM10 µg/L 1ND1,3-Dichlorobenzene 1/9/2010 12:09 AM10 µg/L 1ND1,4-Dichlorobenzene 1/9/2010 12:09 AM10 µg/L 1ND2,4,5-Trichlorophenol 1/9/2010 12:09 AM10 µg/L 1ND2,4,6-Trichlorophenol 1/9/2010 12:09 AM10 µg/L 1ND2,4-Dichlorophenol 1/9/2010 12:09 AM10 µg/L 1ND2,4-Dimethylphenol 1/9/2010 12:09 AM10 µg/L 1ND2,4-Dinitrophenol 1/9/2010 12:09 AM50 µg/L 1ND2,4-Dinitrotoluene 1/9/2010 12:09 AM10 µg/L 1ND2,6-Dinitrotoluene 1/9/2010 12:09 AM10 µg/L 1ND2-Chloronaphthalene 1/9/2010 12:09 AM10 µg/L 1ND2-Chlorophenol 1/9/2010 12:09 AM10 µg/L 1ND2-Methylnaphthalene 1/9/2010 12:09 AM10 µg/L 1ND2-Methylphenol 1/9/2010 12:09 AM10 µg/L 1ND2-Nitroaniline 1/9/2010 12:09 AM50 µg/L 1ND2-Nitrophenol 1/9/2010 12:09 AM10 µg/L 1ND3,3´-Dichlorobenzidine 1/9/2010 12:09 AM20 µg/L 1ND3-Nitroaniline 1/9/2010 12:09 AM50 µg/L 1ND4,6-Dinitro-2-methylphenol 1/9/2010 12:09 AM50 µg/L 1ND4-Bromophenyl-phenylether 1/9/2010 12:09 AM10 µg/L 1ND4-Chloro-3-methylphenol 1/9/2010 12:09 AM50 µg/L 1ND4-Chloroaniline 1/9/2010 12:09 AM20 µg/L 1ND4-Chlorophenyl-phenylether 1/9/2010 12:09 AM10 µg/L 1ND4-Methylphenol 1/9/2010 12:09 AM10 µg/L 1ND4-Nitroaniline 1/9/2010 12:09 AM20 µg/L 1ND4-Nitrophenol 1/9/2010 12:09 AM50 µg/L 1NDAcenaphthene 1/9/2010 12:09 AM10 µg/L 1NDAcenaphthylene 1/9/2010 12:09 AM10 µg/L 1NDAnthracene 1/9/2010 12:09 AM10 µg/L 1NDBenzidine (M) 1/9/2010 12:09 AM50 µg/L 1NDBenzo(a)anthracene 1/9/2010 12:09 AM10 µg/L 1NDBenzo(a)pyrene 1/9/2010 12:09 AM10 µg/L 1NDBenzo(b)fluoranthene 1/9/2010 12:09 AM10 µg/L 1NDBenzo(g,h,i)perylene 1/9/2010 12:09 AM10 µg/L 1ND



22 of 71




Matrix: WATER



Lab ID: 109486-018B

DF


PQL

ANALYTICAL RESULTS


Analyst: DMP

EPA 3510C


Benzo(k)fluoranthene 1/9/2010 12:09 AM10 µg/L 1NDBenzoic acid 1/9/2010 12:09 AM50 µg/L 1NDBenzyl alcohol 1/9/2010 12:09 AM20 µg/L 1NDBis(2-chloroethoxy)methane 1/9/2010 12:09 AM10 µg/L 1NDBis(2-chloroethyl)ether 1/9/2010 12:09 AM10 µg/L 1NDBis(2-chloroisopropyl)ether 1/9/2010 12:09 AM10 µg/L 1NDBis(2-ethylhexyl)phthalate 1/9/2010 12:09 AM10 µg/L 1NDButylbenzylphthalate 1/9/2010 12:09 AM10 µg/L 1NDChrysene 1/9/2010 12:09 AM10 µg/L 1NDDi-n-butylphthalate 1/9/2010 12:09 AM10 µg/L 1NDDi-n-octylphthalate 1/9/2010 12:09 AM10 µg/L 1NDDibenz(a,h)anthracene 1/9/2010 12:09 AM10 µg/L 1NDDibenzofuran 1/9/2010 12:09 AM10 µg/L 1NDDiethylphthalate 1/9/2010 12:09 AM10 µg/L 1NDDimethylphthalate 1/9/2010 12:09 AM10 µg/L 1NDFluoranthene 1/9/2010 12:09 AM10 µg/L 1NDFluorene 1/9/2010 12:09 AM10 µg/L 1NDHexachlorobenzene 1/9/2010 12:09 AM10 µg/L 1NDHexachlorobutadiene 1/9/2010 12:09 AM20 µg/L 1NDHexachlorocyclopentadiene 1/9/2010 12:09 AM10 µg/L 1NDHexachloroethane 1/9/2010 12:09 AM10 µg/L 1NDIndeno(1,2,3-cd)pyrene 1/9/2010 12:09 AM10 µg/L 1NDIsophorone 1/9/2010 12:09 AM10 µg/L 1NDN-Nitrosodi-n-propylamine 1/9/2010 12:09 AM10 µg/L 1NDN-Nitrosodiphenylamine 1/9/2010 12:09 AM10 µg/L 1NDNaphthalene 1/9/2010 12:09 AM10 µg/L 1NDNitrobenzene 1/9/2010 12:09 AM10 µg/L 1NDPentachlorophenol 1/9/2010 12:09 AM50 µg/L 1NDPhenanthrene 1/9/2010 12:09 AM10 µg/L 1NDPhenol 1/9/2010 12:09 AM10 µg/L 1NDPyrene 1/9/2010 12:09 AM10 µg/L 1ND Surr: 1,2-Dichlorobenzene-d4 1/9/2010 12:09 AM46-97 %REC 170.6 Surr: 2,4,6-Tribromophenol 1/9/2010 12:09 AM59-124 %REC 190.9 Surr: 2-Chlorophenol-d4 1/9/2010 12:09 AM49-93 %REC 167.3 Surr: 2-Fluorobiphenyl 1/9/2010 12:09 AM57-107 %REC 174.4



23 of 71




Matrix: WATER



Lab ID: 109486-018B

DF


PQL

ANALYTICAL RESULTS


Analyst: DMP

EPA 3510C


Surr: 2-Fluorophenol 1/9/2010 12:09 AM27-60 %REC 139.5 Surr: 4-Terphenyl-d14 1/9/2010 12:09 AM69-132 %REC 1114 Surr: Nitrobenzene-d5 1/9/2010 12:09 AM52-107 %REC 174.1 Surr: Phenol-d5 1/9/2010 12:09 AM15-50 %REC 125.2



24 of 71




Matrix: WATER



Lab ID: 109486-018C

DF


PQL

ANALYTICAL RESULTS


Analyst: BB

EPA 3510C


Aroclor 1016 1/12/2010 09:38 AM0.50 µg/L 1NDAroclor 1221 1/12/2010 09:38 AM1.0 µg/L 1NDAroclor 1232 1/12/2010 09:38 AM0.50 µg/L 1NDAroclor 1242 1/12/2010 09:38 AM0.50 µg/L 1NDAroclor 1248 1/12/2010 09:38 AM0.50 µg/L 1NDAroclor 1254 1/12/2010 09:38 AM0.50 µg/L 1NDAroclor 1260 1/12/2010 09:38 AM0.50 µg/L 1NDAroclor 1262 1/12/2010 09:38 AM0.50 µg/L 1NDAroclor 1268 1/12/2010 09:38 AM0.50 µg/L 1ND Surr: Decachlorobiphenyl 1/12/2010 09:38 AM29-130 %REC 170.5 Surr: Tetrachloro-m-xylene 1/12/2010 09:38 AM48-126 %REC 169.5



25 of 71




Matrix: WATER



Lab ID: 109486-018E

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3010A


Antimony 1/12/2010 06:11 PM0.0050 mg/L 1NDArsenic 1/12/2010 06:11 PM0.010 mg/L 1NDBarium 1/12/2010 06:11 PM0.0030 mg/L 10.040Beryllium 1/12/2010 06:11 PM0.0030 mg/L 1NDCadmium 1/12/2010 06:11 PM0.0030 mg/L 1NDChromium 1/12/2010 06:11 PM0.0030 mg/L 1NDCobalt 1/12/2010 06:11 PM0.0030 mg/L 1NDCopper 1/12/2010 06:11 PM0.0050 mg/L 1NDLead 1/12/2010 06:11 PM0.0050 mg/L 1NDMolybdenum 1/12/2010 06:11 PM0.0050 mg/L 1NDNickel 1/12/2010 06:11 PM0.0050 mg/L 1NDSelenium 1/12/2010 06:11 PM0.010 mg/L 1NDSilver 1/12/2010 06:11 PM0.0030 mg/L 10.011Thallium 1/12/2010 06:11 PM0.015 mg/L 1NDVanadium 1/12/2010 06:11 PM0.0030 mg/L 1NDZinc 1/12/2010 06:11 PM0.010 mg/L 1ND


Analyst: ILRunID: AA1_100112D 61035QC Batch: PrepDate: 1/11/2010

Mercury 1/12/2010 01:53 PM0.20 µg/L 1ND



26 of 71



Client Sample ID: QCTB-01Collection Date: 1/6/2010

Matrix: WATER



Lab ID: 109486-019A

DF


PQL

ANALYTICAL RESULTS






27 of 71



Client Sample ID: QCTB-01Collection Date: 1/6/2010

Matrix: WATER



Lab ID: 109486-019A

DF


PQL

ANALYTICAL RESULTS



cis-1,3-Dichloropropene 1/18/2010 10:55 AM5.0 µg/L 1NDDibromochloromethane 1/18/2010 10:55 AM5.0 µg/L 1NDDibromomethane 1/18/2010 10:55 AM5.0 µg/L 1NDDichlorodifluoromethane 1/18/2010 10:55 AM5.0 µg/L 1NDEthylbenzene 1/18/2010 10:55 AM5.0 µg/L 1NDHexachlorobutadiene 1/18/2010 10:55 AM5.0 µg/L 1NDIsopropylbenzene 1/18/2010 10:55 AM5.0 µg/L 1NDm,p-Xylene 1/18/2010 10:55 AM10 µg/L 1NDMethylene chloride 1/18/2010 10:55 AM5.0 µg/L 1NDn-Butylbenzene 1/18/2010 10:55 AM5.0 µg/L 1NDn-Propylbenzene 1/18/2010 10:55 AM5.0 µg/L 1NDNaphthalene 1/18/2010 10:55 AM5.0 µg/L 1NDo-Xylene 1/18/2010 10:55 AM5.0 µg/L 1NDsec-Butylbenzene 1/18/2010 10:55 AM5.0 µg/L 1NDStyrene 1/18/2010 10:55 AM5.0 µg/L 1NDtert-Butylbenzene 1/18/2010 10:55 AM5.0 µg/L 1NDTetrachloroethene 1/18/2010 10:55 AM5.0 µg/L 1NDToluene 1/18/2010 10:55 AM5.0 µg/L 1NDtrans-1,2-Dichloroethene 1/18/2010 10:55 AM5.0 µg/L 1NDTrichloroethene 1/18/2010 10:55 AM5.0 µg/L 1NDTrichlorofluoromethane 1/18/2010 10:55 AM5.0 µg/L 1NDVinyl chloride 1/18/2010 10:55 AM5.0 µg/L 1ND Surr: 1,2-Dichloroethane-d4 1/18/2010 10:55 AM70-130 %REC 1100 Surr: 4-Bromofluorobenzene 1/18/2010 10:55 AM70-130 %REC 1113 Surr: Dibromofluoromethane 1/18/2010 10:55 AM70-130 %REC 1103



28 of 71






Sample ID: MB-61028




Units: mg/Kg

PQL

Client ID: PBS

RunNo: 116819

SeqNo: 1854722


EPA 3050B

Antimony 2.0NDArsenic 1.0NDBarium 1.0NDBeryllium 1.0NDCadmium 1.00.009Chromium 1.0NDCobalt 1.0NDCopper 2.0NDLead 1.00.284Molybdenum 1.00.083Nickel 1.0NDSelenium 1.0NDSilver 1.0NDThallium 1.0NDVanadium 1.0NDZinc 1.00.270





Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 116819

SeqNo: 1854723


EPA 3050B

Antimony 50.00 94.3 80 1202.0 047.125Arsenic 50.00 92.8 80 1201.0 046.416Barium 50.00 98.6 80 1201.0 049.319Beryllium 50.00 98.3 80 1201.0 049.132Cadmium 50.00 98.0 80 1201.0 0.00896249.009Chromium 50.00 101 80 1201.0 050.715Cobalt 50.00 99.6 80 1201.0 049.822



29 of 71









Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 116819

SeqNo: 1854723


EPA 3050B

Copper 50.00 100 80 1202.0 049.998Lead 50.00 98.3 80 1201.0 0.284149.412Molybdenum 50.00 102 80 1201.0 0.0835051.052Nickel 50.00 98.0 80 1201.0 049.002Selenium 50.00 90.9 80 1201.0 045.453Silver 50.00 96.6 80 1201.0 048.292Thallium 50.00 97.3 80 1201.0 048.643Vanadium 50.00 102 80 1201.0 051.014Zinc 50.00 96.5 80 1201.0 0.270048.506





Units: mg/Kg

PQL

Client ID: HA-7-0.5

RunNo: 116819

SeqNo: 1854726


EPA 3050B

Antimony 202.0 0 0NDArsenic 201.0 1.992 6.171.872Barium 201.0 124.5 8.57114.255Beryllium 201.0 0 0NDCadmium 201.0 0.2641 00.283Chromium 201.0 12.51 13.010.983Cobalt 201.0 3.490 3.953.355Copper 202.0 7.314 7.437.878Lead 201.0 15.29 2.9315.748Molybdenum 201.0 0 0NDNickel 201.0 7.840 8.067.232Selenium 201.0 0 0NDSilver 201.0 0 0NDThallium 201.0 0 0NDVanadium 201.0 29.52 4.5630.898Zinc 201.0 28.23 1.0628.535



30 of 71









Units: mg/Kg

PQL

Client ID: HA-7-0.5

RunNo: 116819

SeqNo: 1854727


EPA 3050B

Antimony 125.0 70.6 25 1062.0 088.261Arsenic 125.0 77.8 42 1131.0 1.99299.295Barium 125.0 65.3 19 1401.0 124.5206.055Beryllium 125.0 82.2 50 1091.0 0102.765Cadmium 125.0 75.9 48 1061.0 0.264195.150Chromium 125.0 80.2 44 1161.0 12.51112.715Cobalt 125.0 76.7 47 1071.0 3.49099.362Copper 125.0 87.7 49 1242.0 7.314116.965Lead 125.0 76.3 33 1201.0 15.29110.643Molybdenum 125.0 79.9 46 1111.0 099.894Nickel 125.0 76.9 43 1111.0 7.840103.976Selenium 125.0 73.2 43 1041.0 091.477Silver 125.0 85.0 53 1141.0 0106.224Thallium 125.0 76.5 41 1071.0 095.638Vanadium 125.0 80.7 48 1161.0 29.52130.393Zinc 125.0 74.5 24 1291.0 28.23121.360





Units: mg/Kg

PQL

Client ID: HA-7-0.5

RunNo: 116819

SeqNo: 1854728


EPA 3050B

Antimony 125.0 78.0 25 106 202.0 0 88.26 9.9297.474Arsenic 125.0 85.2 42 113 201.0 1.992 99.30 8.83108.468Barium 125.0 80.5 19 140 201.0 124.5 206.1 8.86225.149Beryllium 125.0 89.8 50 109 201.0 0 102.8 8.86112.288Cadmium 125.0 82.5 48 106 201.0 0.2641 95.15 8.25103.339Chromium 125.0 88.6 44 116 201.0 12.51 112.7 8.96123.294Cobalt 125.0 83.8 47 107 201.0 3.490 99.36 8.60108.295Copper 125.0 97.7 49 124 202.0 7.314 117.0 10.2129.483Lead 125.0 81.2 33 120 201.0 15.29 110.6 5.39116.776



31 of 71









Units: mg/Kg

PQL

Client ID: HA-7-0.5

RunNo: 116819

SeqNo: 1854728


EPA 3050B

Molybdenum 125.0 87.2 46 111 201.0 0 99.89 8.77109.058Nickel 125.0 84.2 43 111 201.0 7.840 104.0 8.44113.136Selenium 125.0 79.6 43 104 201.0 0 91.48 8.3499.438Silver 125.0 93.3 53 114 201.0 0 106.2 9.29116.568Thallium 125.0 82.3 41 107 201.0 0 95.64 7.33102.916Vanadium 125.0 90.5 48 116 201.0 29.52 130.4 8.98142.650Zinc 125.0 81.3 24 129 201.0 28.23 121.4 6.73129.817



32 of 71






Sample ID: MB-61037




Units: mg/L

PQL

Client ID: PBW

RunNo: 116883

SeqNo: 1855406


EPA 3010A

Antimony 0.0050NDArsenic 0.010NDBarium 0.0030NDBeryllium 0.0030NDCadmium 0.0030NDChromium 0.0030NDCobalt 0.0030NDCopper 0.0050NDLead 0.0050NDMolybdenum 0.0050NDNickel 0.0050NDSelenium 0.010NDSilver 0.0030NDThallium 0.015NDVanadium 0.0030NDZinc 0.0100.004





Units: mg/L

PQL

Client ID: LCSW

RunNo: 116883

SeqNo: 1855407


EPA 3010A

Antimony 1.000 94.5 85 1150.0050 00.945Arsenic 1.000 92.3 85 1150.010 00.923Barium 1.000 93.7 85 1150.0030 00.937Beryllium 1.000 94.0 85 1150.0030 00.940Cadmium 1.000 91.9 85 1150.0030 00.919Chromium 1.000 91.3 85 1150.0030 00.913Cobalt 1.000 95.1 85 1150.0030 00.951



33 of 71









Units: mg/L

PQL

Client ID: LCSW

RunNo: 116883

SeqNo: 1855407


EPA 3010A

Copper 1.000 94.3 85 1150.0050 00.943Lead 1.000 92.5 85 1150.0050 00.925Molybdenum 1.000 94.3 85 1150.0050 00.943Nickel 1.000 91.7 85 1150.0050 00.917Selenium 1.000 91.6 85 1150.010 00.916Silver 1.000 96.2 85 1150.0030 00.962Thallium 1.000 95.7 85 1150.015 00.957Vanadium 1.000 93.4 85 1150.0030 00.934Zinc 1.000 91.2 85 1150.010 0.0040920.916





Units: mg/L

PQL

Client ID: QCEB-01

RunNo: 116883

SeqNo: 1855409


EPA 3010A




34 of 71









Units: mg/L

PQL

Client ID: QCEB-01

RunNo: 116883

SeqNo: 1855410


EPA 3010A






Units: mg/L

PQL

Client ID: QCEB-01

RunNo: 116883

SeqNo: 1855411


EPA 3010A




35 of 71









Units: mg/L

PQL

Client ID: QCEB-01

RunNo: 116883

SeqNo: 1855411


EPA 3010A




36 of 71






Sample ID: MB-61215

Batch ID: 61215 TestNo: EPA 7471A Analysis Date: 1/19/2010



Units: mg/Kg

PQL

Client ID: PBS

RunNo: 117094

SeqNo: 1859194


Mercury 0.10ND





Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 117094

SeqNo: 1859195


Mercury 0.8300 110 80 1200.10 00.914





Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 117094

SeqNo: 1859196


Mercury 0.8300 114 70 1300.10 0.058831.005





Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 117094

SeqNo: 1859197


Mercury 0.8300 114 70 130 200.10 0.05883 1.005 0.3821.001

Sample ID: 109600-061A-DUP




Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 117094

SeqNo: 1859199


Mercury 200.10 0.05883 00.058



37 of 71






Sample ID: MB-61035




Units: µg/L

PQL

Client ID: PBW

RunNo: 116857

SeqNo: 1855117


Mercury 0.20ND





Units: µg/L

PQL

Client ID: LCSW

RunNo: 116857

SeqNo: 1855118


Mercury 10.00 96.0 85 1150.20 09.598

Sample ID: 109494-016E-MS




Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 116857

SeqNo: 1855119


Mercury 10.00 95.5 70 1300.20 09.552

Sample ID: 109494-016E-MSD




Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 116857

SeqNo: 1855120


Mercury 10.00 95.5 70 130 200.20 0 9.552 0.04239.548

Sample ID: 109494-016E-DUP




Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 116857

SeqNo: 1855122


Mercury 200.20 0 0ND



38 of 71





ANALYTICAL QC SUMMARY REPORTBatchID: K10VS018

Sample ID: K100115LC2

Batch ID: K10VS018 TestNo: EPA 8260B Analysis Date: 1/15/2010

Prep Date:


Units: µg/Kg

PQL

Client ID: LCSS

RunNo: 117024

SeqNo: 1858541


1,1-Dichloroethene 50.00 98.3 70 1305.0 049.150Benzene 100.0 93.0 70 1305.0 093.040Chlorobenzene 50.00 96.7 70 1305.0 048.360MTBE 50.00 94.2 70 1305.0 047.110Toluene 100.0 98.0 70 1305.0 098.020Trichloroethene 50.00 97.1 70 1305.0 048.560 Surr: 1,2-Dichloroethane-d4 50.00 90.5 70 13045.230 Surr: 4-Bromofluorobenzene 50.00 94.7 70 13047.370 Surr: Dibromofluoromethane 50.00 79.6 70 13039.810 Surr: Toluene-d8 50.00 87.6 70 13043.780

Sample ID: K100115MB2


Prep Date:


Units: µg/Kg

PQL

Client ID: PBS

RunNo: 117024

SeqNo: 1858542


1,1,1,2-Tetrachloroethane 5.0ND1,1,1-Trichloroethane 5.0ND1,1,2,2-Tetrachloroethane 5.0ND1,1,2-Trichloroethane 5.0ND1,1-Dichloroethane 5.0ND1,1-Dichloroethene 5.0ND1,1-Dichloropropene 5.0ND1,2,3-Trichlorobenzene 5.0ND1,2,3-Trichloropropane 5.0ND1,2,4-Trichlorobenzene 5.0ND1,2,4-Trimethylbenzene 5.0ND1,2-Dibromo-3-chloropropane 10ND1,2-Dibromoethane 5.0ND



39 of 71







Prep Date:


Units: µg/Kg

PQL

Client ID: PBS

RunNo: 117024

SeqNo: 1858542


1,2-Dichlorobenzene 5.0ND1,2-Dichloroethane 5.0ND1,2-Dichloropropane 5.0ND1,3,5-Trimethylbenzene 5.0ND1,3-Dichlorobenzene 5.0ND1,3-Dichloropropane 5.0ND1,4-Dichlorobenzene 5.0ND2,2-Dichloropropane 5.0ND2-Chlorotoluene 5.0ND4-Chlorotoluene 5.0ND4-Isopropyltoluene 5.0NDBenzene 5.0NDBromobenzene 5.0NDBromodichloromethane 5.0NDBromoform 5.0NDBromomethane 5.0NDCarbon tetrachloride 5.0NDChlorobenzene 5.0NDChloroethane 5.0NDChloroform 5.0NDChloromethane 5.0NDcis-1,2-Dichloroethene 5.0NDcis-1,3-Dichloropropene 5.0NDDibromochloromethane 5.0NDDibromomethane 5.0NDDichlorodifluoromethane 5.0NDEthylbenzene 5.0NDHexachlorobutadiene 5.0NDIsopropylbenzene 5.0NDm,p-Xylene 10ND



40 of 71







Prep Date:


Units: µg/Kg

PQL

Client ID: PBS

RunNo: 117024

SeqNo: 1858542


Methylene chloride 5.0NDn-Butylbenzene 5.0NDn-Propylbenzene 5.0NDNaphthalene 5.0NDo-Xylene 5.0NDsec-Butylbenzene 5.0NDStyrene 5.0NDtert-Butylbenzene 5.0NDTetrachloroethene 5.0NDToluene 5.0NDtrans-1,2-Dichloroethene 5.0NDTrichloroethene 5.0NDTrichlorofluoromethane 5.0NDVinyl chloride 5.0ND Surr: 1,2-Dichloroethane-d4 50.00 101 70 13050.630 Surr: 4-Bromofluorobenzene 50.00 86.3 70 13043.140 Surr: Dibromofluoromethane 50.00 89.3 70 13044.660 Surr: Toluene-d8 50.00 86.7 70 13043.330



Prep Date:


Units: µg/Kg

PQL

Client ID: HA-5-0.5

RunNo: 117024

SeqNo: 1858543


1,1-Dichloroethene 50.00 86.6 70 1305.0 043.280Benzene 100.0 82.2 70 1305.0 082.180Chlorobenzene 50.00 71.2 70 1305.0 035.620MTBE 50.00 90.5 70 1305.0 045.240Toluene 100.0 79.7 70 1305.0 079.710Trichloroethene 50.00 86.0 70 1305.0 042.990 Surr: 1,2-Dichloroethane-d4 50.00 99.5 70 13049.730



41 of 71







Prep Date:


Units: µg/Kg

PQL

Client ID: HA-5-0.5

RunNo: 117024

SeqNo: 1858543


Surr: 4-Bromofluorobenzene 50.00 89.0 70 13044.510 Surr: Dibromofluoromethane 50.00 88.1 70 13044.040 Surr: Toluene-d8 50.00 86.8 70 13043.400



Prep Date:


Units: µg/Kg

PQL

Client ID: HA-5-0.5

RunNo: 117024

SeqNo: 1858544


1,1-Dichloroethene 50.00 87.2 70 130 205.0 0 43.28 0.76043.610Benzene 100.0 84.1 70 130 205.0 0 82.18 2.3284.110Chlorobenzene 50.00 70.3 70 130 205.0 0 35.62 1.3035.160MTBE 50.00 86.8 70 130 205.0 0 45.24 4.2043.380Toluene 100.0 80.3 70 130 205.0 0 79.71 0.76280.320Trichloroethene 50.00 89.6 70 130 205.0 0 42.99 4.1044.790 Surr: 1,2-Dichloroethane-d4 50.00 97.1 70 130 20048.540 Surr: 4-Bromofluorobenzene 50.00 92.8 70 130 20046.390 Surr: Dibromofluoromethane 50.00 84.5 70 130 20042.270 Surr: Toluene-d8 50.00 87.1 70 130 20043.570



Prep Date:


Units: µg/Kg

PQL

Client ID: HA-5-0.5

RunNo: 117024

SeqNo: 1858545


1,1,1,2-Tetrachloroethane 205.0 0 0ND1,1,1-Trichloroethane 205.0 0 0ND1,1,2,2-Tetrachloroethane 205.0 0 0ND1,1,2-Trichloroethane 205.0 0 0ND1,1-Dichloroethane 205.0 0 0ND1,1-Dichloroethene 205.0 0 0ND



42 of 71







Prep Date:


Units: µg/Kg

PQL

Client ID: HA-5-0.5

RunNo: 117024

SeqNo: 1858545


1,1-Dichloropropene 205.0 0 0ND1,2,3-Trichlorobenzene 205.0 0 0ND1,2,3-Trichloropropane 205.0 0 0ND1,2,4-Trichlorobenzene 205.0 0 0ND1,2,4-Trimethylbenzene 205.0 0 0ND1,2-Dibromo-3-chloropropane 2010 0 0ND1,2-Dibromoethane 205.0 0 0ND1,2-Dichlorobenzene 205.0 0 0ND1,2-Dichloroethane 205.0 0 0ND1,2-Dichloropropane 205.0 0 0ND1,3,5-Trimethylbenzene 205.0 0 0ND1,3-Dichlorobenzene 205.0 0 0ND1,3-Dichloropropane 205.0 0 0ND1,4-Dichlorobenzene 205.0 0 0ND2,2-Dichloropropane 205.0 0 0ND2-Butanone 2050 0 0ND2-Chloroethyl vinyl ether 205.0 0 0ND2-Chlorotoluene 205.0 0 0ND2-Hexanone 2050 0 0ND4-Chlorotoluene 205.0 0 0ND4-Isopropyltoluene 205.0 0 0ND4-Methyl-2-pentanone 2050 0 0NDAcetone 2050 0 0NDAcrolein 2050 0 0NDAcrylonitrile 2050 0 0NDBenzene 205.0 0 0NDBromobenzene 205.0 0 0NDBromochloromethane 205.0 0 0NDBromodichloromethane 205.0 0 0NDBromoform 205.0 0 0ND



43 of 71







Prep Date:


Units: µg/Kg

PQL

Client ID: HA-5-0.5

RunNo: 117024

SeqNo: 1858545


Bromomethane 205.0 0 0NDCarbon disulfide 205.0 0 0NDCarbon tetrachloride 205.0 0 0NDChlorobenzene 205.0 0 0NDChloroethane 205.0 0 0NDChloroform 205.0 0 0NDChloromethane 205.0 0 0NDcis-1,2-Dichloroethene 205.0 0 0NDcis-1,3-Dichloropropene 205.0 0 0NDCyclohexanone 2050 0 0NDDi-isopropyl ether 205.0 0 0NDDibromochloromethane 205.0 0 0NDDibromomethane 205.0 0 0NDDichlorodifluoromethane 205.0 0 0NDEthyl Acetate 2050 0 0NDEthyl Ether 2050 0 0NDEthyl Tert-butyl ether 205.0 0 0NDEthylbenzene 205.0 0 0NDFreon-113 205.0 0 0NDHexachlorobutadiene 205.0 0 0NDIodomethane 205.0 0 0NDIsopropylbenzene 205.0 0 0NDm,p-Xylene 2010 0 0NDMethylene chloride 205.0 0 0NDMTBE 205.0 0 0NDn-Butylbenzene 205.0 0 0NDn-Propylbenzene 205.0 0 0NDNaphthalene 205.0 0 0NDo-Xylene 205.0 0 0NDsec-Butylbenzene 205.0 0 0ND



44 of 71







Prep Date:


Units: µg/Kg

PQL

Client ID: HA-5-0.5

RunNo: 117024

SeqNo: 1858545


Styrene 205.0 0 0NDTert-amyl methyl ether 205.0 0 0NDTert-Butanol 20100 0 0NDtert-Butylbenzene 205.0 0 0NDTetrachloroethene 205.0 0 0NDToluene 205.0 0 0NDtrans-1,2-Dichloroethene 205.0 0 0NDtrans-1,3-Dichloropropene 205.0 0 0NDTrichloroethene 205.0 0 0NDTrichlorofluoromethane 205.0 0 0NDVinyl acetate 2050 0 0NDVinyl chloride 205.0 0 0NDXylenes, Total 2015 0 0ND Surr: 1,2-Dichloroethane-d4 50.00 109 70 130 20054.470 Surr: 4-Bromofluorobenzene 50.00 88.8 70 130 20044.400 Surr: Dibromofluoromethane 50.00 94.0 70 130 20047.020 Surr: Toluene-d8 50.00 85.4 70 130 20042.690



45 of 71





ANALYTICAL QC SUMMARY REPORTBatchID: A10VW016

Sample ID: A100118LCS1

Batch ID: A10VW016 TestNo: EPA 8260B Analysis Date: 1/18/2010

Prep Date:


Units: µg/L

PQL

Client ID: LCSW

RunNo: 117064

SeqNo: 1859578

LCSSampType: TestCode: 8260_WP

1,1-Dichloroethene 20.00 106 70 1305.0 021.140Benzene 40.00 97.9 70 1305.0 039.170Chlorobenzene 20.00 99.9 70 1305.0 019.980MTBE 20.00 107 70 1305.0 021.470Toluene 40.00 103 70 1305.0 041.380Trichloroethene 20.00 106 70 1305.0 021.290 Surr: 1,2-Dichloroethane-d4 25.00 101 70 13025.230 Surr: 4-Bromofluorobenzene 25.00 117 70 13029.200 Surr: Dibromofluoromethane 25.00 101 70 13025.360 Surr: Toluene-d8 25.00 106 70 13026.600

Sample ID: A100118MB2MS


Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 117064

SeqNo: 1859579

MSSampType: TestCode: 8260_WP

1,1-Dichloroethene 20.00 101 70 1305.0 020.280Benzene 40.00 96.2 70 1305.0 038.460Chlorobenzene 20.00 100 70 1305.0 020.090Toluene 40.00 102 70 1305.0 040.920Trichloroethene 20.00 103 70 1305.0 020.530 Surr: 1,2-Dichloroethane-d4 25.00 100 70 13025.060 Surr: 4-Bromofluorobenzene 25.00 118 70 13029.420 Surr: Dibromofluoromethane 25.00 102 70 13025.380 Surr: Toluene-d8 25.00 105 70 13026.280



46 of 71





Sample ID: A100118MB2MSD


Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 117064

SeqNo: 1859580

MSDSampType: TestCode: 8260_WP

1,1-Dichloroethene 20.00 105 70 130 205.0 0 20.28 3.7321.050Benzene 40.00 95.8 70 130 205.0 0 38.46 0.33938.330Chlorobenzene 20.00 98.8 70 130 205.0 0 20.09 1.6619.760Toluene 40.00 102 70 130 205.0 0 40.92 0.49040.720Trichloroethene 20.00 103 70 130 205.0 0 20.53 0.24320.580 Surr: 1,2-Dichloroethane-d4 25.00 96.6 70 130 20024.160 Surr: 4-Bromofluorobenzene 25.00 115 70 130 20028.770 Surr: Dibromofluoromethane 25.00 99.5 70 130 20024.870 Surr: Toluene-d8 25.00 104 70 130 20026.000

Sample ID: A100118MB2


Prep Date:


Units: µg/L

PQL

Client ID: PBW

RunNo: 117064

SeqNo: 1859581

MBLKSampType: TestCode: 8260_WP

1,1,1,2-Tetrachloroethane 5.0ND1,1,1-Trichloroethane 5.0ND1,1,2,2-Tetrachloroethane 5.0ND1,1,2-Trichloroethane 5.0ND1,1-Dichloroethane 5.0ND1,1-Dichloroethene 5.0ND1,1-Dichloropropene 5.0ND1,2,3-Trichlorobenzene 5.0ND1,2,3-Trichloropropane 5.0ND1,2,4-Trichlorobenzene 5.0ND1,2,4-Trimethylbenzene 5.0ND1,2-Dibromo-3-chloropropane 5.0ND1,2-Dibromoethane 5.0ND1,2-Dichlorobenzene 5.0ND1,2-Dichloroethane 5.0ND1,2-Dichloropropane 5.0ND



47 of 71







Prep Date:


Units: µg/L

PQL

Client ID: PBW

RunNo: 117064

SeqNo: 1859581


1,3,5-Trimethylbenzene 5.0ND1,3-Dichlorobenzene 5.0ND1,3-Dichloropropane 5.0ND1,4-Dichlorobenzene 5.0ND2,2-Dichloropropane 5.0ND2-Chlorotoluene 5.0ND4-Chlorotoluene 5.0ND4-Isopropyltoluene 5.0NDBenzene 5.0NDBromobenzene 5.0NDBromodichloromethane 5.0NDBromoform 5.0NDBromomethane 5.0NDCarbon tetrachloride 5.0NDChlorobenzene 5.0NDChloroethane 5.0NDChloroform 5.0NDChloromethane 5.0NDcis-1,2-Dichloroethene 5.0NDcis-1,3-Dichloropropene 5.0NDDibromochloromethane 5.0NDDibromomethane 5.0NDDichlorodifluoromethane 5.0NDEthylbenzene 5.0NDHexachlorobutadiene 5.0NDIsopropylbenzene 5.0NDm,p-Xylene 10NDMethylene chloride 5.0NDn-Butylbenzene 5.0NDn-Propylbenzene 5.0ND



48 of 71







Prep Date:


Units: µg/L

PQL

Client ID: PBW

RunNo: 117064

SeqNo: 1859581


Naphthalene 5.0NDo-Xylene 5.0NDsec-Butylbenzene 5.0NDStyrene 5.0NDtert-Butylbenzene 5.0NDTetrachloroethene 5.0NDToluene 5.0NDtrans-1,2-Dichloroethene 5.0NDTrichloroethene 5.0NDTrichlorofluoromethane 5.0NDVinyl chloride 5.0ND Surr: 1,2-Dichloroethane-d4 25.00 96.6 70 13024.150 Surr: 4-Bromofluorobenzene 25.00 111 70 13027.700 Surr: Dibromofluoromethane 25.00 101 70 13025.180 Surr: Toluene-d8 25.00 104 70 13026.070

Sample ID: 109486-018A


Prep Date:


Units: µg/L

PQL

Client ID: QCEB-01

RunNo: 117064

SeqNo: 1859584

DUPSampType: TestCode: 8260_WP

1,1,1,2-Tetrachloroethane 205.0 0 0ND1,1,1-Trichloroethane 205.0 0 0ND1,1,2,2-Tetrachloroethane 205.0 0 0ND1,1,2-Trichloroethane 205.0 0 0ND1,1-Dichloroethane 205.0 0 0ND1,1-Dichloroethene 205.0 0 0ND1,1-Dichloropropene 205.0 0 0ND1,2,3-Trichlorobenzene 205.0 0 0ND1,2,3-Trichloropropane 205.0 0 0ND1,2,4-Trichlorobenzene 205.0 0 0ND



49 of 71







Prep Date:


Units: µg/L

PQL

Client ID: QCEB-01

RunNo: 117064

SeqNo: 1859584


1,2,4-Trimethylbenzene 205.0 0 0ND1,2-Dibromo-3-chloropropane 205.0 0 0ND1,2-Dibromoethane 205.0 0 0ND1,2-Dichlorobenzene 205.0 0 0ND1,2-Dichloroethane 205.0 0 0ND1,2-Dichloropropane 205.0 0 0ND1,3,5-Trimethylbenzene 205.0 0 0ND1,3-Dichlorobenzene 205.0 0 0ND1,3-Dichloropropane 205.0 0 0ND1,4-Dichlorobenzene 205.0 0 0ND2,2-Dichloropropane 205.0 0 0ND2-Butanone 2050 0 0ND2-Chloroethyl vinyl ether 205.0 0 0ND2-Chlorotoluene 205.0 0 0ND2-Hexanone 2050 0 0ND4-Chlorotoluene 205.0 0 0ND4-Isopropyltoluene 205.0 0 0ND4-Methyl-2-pentanone 2050 0 0NDAcetone 2050 0 0NDAcrolein 2050 0 0NDAcrylonitrile 2050 0 0NDBenzene 205.0 0 0NDBromobenzene 205.0 0 0NDBromochloromethane 205.0 0 0NDBromodichloromethane 205.0 0 0NDBromoform 205.0 0 0NDBromomethane 205.0 0 0NDCarbon disulfide 205.0 0 0NDCarbon tetrachloride 205.0 0 0NDChlorobenzene 205.0 0 0ND



50 of 71







Prep Date:


Units: µg/L

PQL

Client ID: QCEB-01

RunNo: 117064

SeqNo: 1859584


Chloroethane 205.0 0 0NDChloroform 205.0 0 0NDChloromethane 205.0 0 0NDcis-1,2-Dichloroethene 205.0 0 0NDcis-1,3-Dichloropropene 205.0 0 0NDCyclohexanone 2050 0 0NDDi-isopropyl ether 205.0 0 0NDDibromochloromethane 205.0 0 0NDDibromomethane 205.0 0 0NDDichlorodifluoromethane 205.0 0 0NDEthyl Acetate 2050 0 0NDEthyl Ether 2050 0 0NDEthyl tert-butyl ether 205.0 0 0NDEthylbenzene 205.0 0 0NDFreon-113 205.0 0 0NDHexachlorobutadiene 205.0 0 0NDIodomethane 205.0 0 0NDIsopropylbenzene 205.0 0 0NDm,p-Xylene 2010 0 0NDMethylene chloride 205.0 0 0NDMTBE 205.0 0 0NDn-Butylbenzene 205.0 0 0NDn-Propylbenzene 205.0 0 0NDNaphthalene 205.0 0 0NDo-Xylene 205.0 0 0NDsec-Butylbenzene 205.0 0 0NDStyrene 205.0 0 0NDTert-amyl methyl ether 205.0 0 0NDTert-Butanol 20100 0 0NDtert-Butylbenzene 205.0 0 0ND



51 of 71







Prep Date:


Units: µg/L

PQL

Client ID: QCEB-01

RunNo: 117064

SeqNo: 1859584


Tetrachloroethene 205.0 0 0NDToluene 205.0 0 0NDtrans-1,2-Dichloroethene 205.0 0 0NDtrans-1,3-Dichloropropene 205.0 0 0NDTrichloroethene 205.0 0 0NDTrichlorofluoromethane 205.0 0 0NDVinyl acetate 2050 0 0NDVinyl chloride 205.0 0 0NDXylenes, Total 2015 0 0ND Surr: 1,2-Dichloroethane-d4 25.00 103 70 130 20025.710 Surr: 4-Bromofluorobenzene 25.00 116 70 130 20028.950 Surr: Dibromofluoromethane 25.00 103 70 130 20025.670 Surr: Toluene-d8 25.00 103 70 130 20025.840



52 of 71










Units: mg/Kg

PQL

Client ID: HA-8-2

RunNo: 117113

SeqNo: 1859613


LUFT

DRO 1000 143 58 145 2010 0 1414 1.221431.580 Surr: p-Terphenyl 80.00 144 57 144 00114.930





Units: mg/Kg

PQL

Client ID: HA-8-2

RunNo: 117113

SeqNo: 1859614


LUFT






Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 117113

SeqNo: 1859705


LUFT


Sample ID: MB-61185




Units: mg/Kg

PQL

Client ID: PBS

RunNo: 117113

SeqNo: 1859706


LUFT




53 of 71









Units: mg/Kg

PQL

Client ID: HA-5-2

RunNo: 117113

SeqNo: 1859710


LUFT

T/R Hydrocarbons: C8-C10 2010 0 0NDT/R Hydrocarbons: C10-C18 2010 0 0NDT/R Hydrocarbons: C18-C28 2010 0 0NDT/R Hydrocarbons: C28-C36 2010 0 0NDT/R Hydrocarbons: C36-C40 2010 0 0NDT/R Hydrocarbons: C8-C40 Total 2010 0 0ND Surr: p-Terphenyl 80.00 133 57 144 00106.400



54 of 71






Sample ID: MB-61238

Batch ID: 61238 TestNo: EPA 8082 Analysis Date: 1/19/2010



Units: µg/Kg

PQL

Client ID: PBS

RunNo: 117125

SeqNo: 1859849


EPA 3550B

Aroclor 1016 16NDAroclor 1221 33NDAroclor 1232 16NDAroclor 1242 16NDAroclor 1248 16NDAroclor 1254 16NDAroclor 1260 16NDAroclor 1262 16NDAroclor 1268 16ND Surr: Decachlorobiphenyl 16.67 93.2 30 12415.537 Surr: Tetrachloro-m-xylene 16.67 92.7 40 11815.449

Sample ID: LCSA-61238




Units: µg/Kg

PQL

Client ID: LCSS

RunNo: 117125

SeqNo: 1859850


EPA 3550B

Aroclor 1016 166.7 69.7 56 11316 0116.147Aroclor 1260 166.7 78.2 58 11116 0130.348 Surr: Decachlorobiphenyl 16.67 79.8 30 12413.305 Surr: Tetrachloro-m-xylene 16.67 77.1 40 11812.855

Sample ID: 109632-089AMSA




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 117125

SeqNo: 1859851


EPA 3550B

Aroclor 1016 166.7 80.5 51 11116 0134.222Aroclor 1260 166.7 88.8 39 12316 0148.066 Surr: Decachlorobiphenyl 16.67 96.8 30 12416.142



55 of 71





Sample ID: 109632-089AMSA




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 117125

SeqNo: 1859851


EPA 3550B

Surr: Tetrachloro-m-xylene 16.67 87.9 40 11814.657

Sample ID: 109632-089AMSDA




Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 117125

SeqNo: 1859852


EPA 3550B

Aroclor 1016 166.7 87.4 51 111 016 0 134.2 8.20145.699Aroclor 1260 166.7 100 39 123 016 0 148.1 12.1167.216 Surr: Decachlorobiphenyl 16.67 106 30 124 0017.715 Surr: Tetrachloro-m-xylene 16.67 99.6 40 118 0016.604

Sample ID: 109486-014ADUPA




Units: µg/Kg

PQL

Client ID: HA-8-0.5

RunNo: 117125

SeqNo: 1859891


EPA 3550B

Aroclor 1016 2016 0 0NDAroclor 1221 2033 0 0NDAroclor 1232 2016 0 0NDAroclor 1242 2016 0 0NDAroclor 1248 2016 0 0NDAroclor 1254 2016 0 0NDAroclor 1260 2016 0 0NDAroclor 1262 2016 0 0NDAroclor 1268 2016 0 0ND Surr: Decachlorobiphenyl 16.67 68.2 30 124 0011.366 Surr: Tetrachloro-m-xylene 16.67 98.0 40 118 0016.337



56 of 71






Sample ID: MB-61043




Units: µg/L

PQL

Client ID: PBW

RunNo: 116845

SeqNo: 1854995


EPA 3510C

Aroclor 1016 0.50NDAroclor 1221 1.0NDAroclor 1232 0.50NDAroclor 1242 0.50NDAroclor 1248 0.50NDAroclor 1254 0.50NDAroclor 1260 0.50NDAroclor 1262 0.50NDAroclor 1268 0.50ND Surr: Decachlorobiphenyl 0.5000 96.7 29 1300.483 Surr: Tetrachloro-m-xylene 0.5000 109 48 1260.543





Units: µg/L

PQL

Client ID: LCSW

RunNo: 116845

SeqNo: 1854996


EPA 3510C

Aroclor 1016 5.000 80.7 59 1130.50 04.035Aroclor 1260 5.000 87.3 60 1140.50 04.366 Surr: Decachlorobiphenyl 0.5000 84.7 29 1300.424 Surr: Tetrachloro-m-xylene 0.5000 90.9 48 1260.455





Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 116845

SeqNo: 1854997


EPA 3510C

Aroclor 1016 5.000 80.4 59 1130.50 04.019Aroclor 1260 5.000 87.7 60 1140.50 04.385 Surr: Decachlorobiphenyl 0.5000 84.6 29 1300.423



57 of 71









Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 116845

SeqNo: 1854997


EPA 3510C

Surr: Tetrachloro-m-xylene 0.5000 91.5 48 1260.457





Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 116845

SeqNo: 1854998


EPA 3510C

Aroclor 1016 5.000 80.6 59 113 200.50 0 4.019 0.2704.030Aroclor 1260 5.000 88.2 60 114 200.50 0 4.385 0.6134.412 Surr: Decachlorobiphenyl 0.5000 85.5 29 130 000.427 Surr: Tetrachloro-m-xylene 0.5000 91.6 48 126 000.458



58 of 71






Sample ID: MB-61240

Batch ID: 61240 TestNo: EPA 8270C Analysis Date: 1/20/2010



Units: µg/Kg

PQL

Client ID: PBS

RunNo: 117136

SeqNo: 1860063

MBLKSampType: TestCode: 8270_S_FUL

EPA 3550B

1,2,4-Trichlorobenzene 330ND1,2-Dichlorobenzene 330ND1,3-Dichlorobenzene 330ND1,4-Dichlorobenzene 330ND2,4,5-Trichlorophenol 330ND2,4,6-Trichlorophenol 330ND2,4-Dichlorophenol 1600ND2,4-Dimethylphenol 330ND2,4-Dinitrophenol 1600ND2,4-Dinitrotoluene 330ND2,6-Dinitrotoluene 330ND2-Chloronaphthalene 330ND2-Chlorophenol 330ND2-Methylnaphthalene 330ND2-Methylphenol 330ND2-Nitroaniline 1600ND2-Nitrophenol 330ND3,3´-Dichlorobenzidine 660ND3-Nitroaniline 1600ND4,6-Dinitro-2-methylphenol 1600ND4-Bromophenyl-phenylether 330ND4-Chloro-3-methylphenol 660ND4-Chloroaniline 660ND4-Chlorophenyl-phenylether 330ND4-Methylphenol 330ND4-Nitroaniline 1600ND4-Nitrophenol 1600NDAcenaphthene 330ND



59 of 71





Sample ID: MB-61240




Units: µg/Kg

PQL

Client ID: PBS

RunNo: 117136

SeqNo: 1860063


EPA 3550B

Acenaphthylene 330NDAnthracene 330NDBenzidine (M) 1600NDBenzo(a)anthracene 330NDBenzo(a)pyrene 330NDBenzo(b)fluoranthene 330NDBenzo(g,h,i)perylene 330NDBenzo(k)fluoranthene 330NDBenzoic acid 1600NDBenzyl alcohol 660NDBis(2-chloroethoxy)methane 330NDBis(2-chloroethyl)ether 330NDBis(2-chloroisopropyl)ether 330NDBis(2-ethylhexyl)phthalate 330NDButylbenzylphthalate 330NDChrysene 330NDDi-n-butylphthalate 330NDDi-n-octylphthalate 330NDDibenz(a,h)anthracene 330NDDibenzofuran 330NDDiethylphthalate 330NDDimethylphthalate 330NDFluoranthene 330NDFluorene 330NDHexachlorobenzene 330NDHexachlorobutadiene 660NDHexachlorocyclopentadiene 660NDHexachloroethane 330NDIndeno(1,2,3-cd)pyrene 330NDIsophorone 330ND



60 of 71





Sample ID: MB-61240




Units: µg/Kg

PQL

Client ID: PBS

RunNo: 117136

SeqNo: 1860063


EPA 3550B

N-Nitrosodi-n-propylamine 330NDN-Nitrosodiphenylamine 330NDNaphthalene 330NDNitrobenzene 330NDPentachlorophenol 1600NDPhenanthrene 330NDPhenol 330NDPyrene 330ND Surr: 1,2-Dichlorobenzene-d4 3330 73.6 45 1052452.000 Surr: 2,4,6-Tribromophenol 3330 81.3 41 1292705.667 Surr: 2-Chlorophenol-d4 3330 75.5 55 1082514.333 Surr: 2-Fluorobiphenyl 3330 74.2 56 1142471.333 Surr: 2-Fluorophenol 3330 75.2 50 1082505.333 Surr: 4-Terphenyl-d14 3330 91.1 59 1413032.667 Surr: Nitrobenzene-d5 3330 81.6 45 1142717.333 Surr: Phenol-d5 3330 77.7 46 1182587.000





Units: µg/Kg

PQL

Client ID: LCSS

RunNo: 117136

SeqNo: 1860064

LCSSampType: TestCode: 8270_S_FUL

EPA 3550B

1,2,4-Trichlorobenzene 3330 84.8 67 107330 02823.0001,4-Dichlorobenzene 3330 79.3 64 99330 02642.0002,4-Dinitrotoluene 3330 88.2 81 122330 02938.6672-Chlorophenol 3330 75.1 62 112330 02499.3334-Chloro-3-methylphenol 3330 83.8 64 138660 02789.3334-Nitrophenol 3330 75.3 60 1421600 02506.667Acenaphthene 3330 83.3 70 116330 02774.667N-Nitrosodi-n-propylamine 3330 89.7 73 115330 02987.000Pentachlorophenol 3330 87.8 59 1351600 02923.333



61 of 71









Units: µg/Kg

PQL

Client ID: LCSS

RunNo: 117136

SeqNo: 1860064

LCSSampType: TestCode: 8270_S_FUL

EPA 3550B

Phenol 3330 79.0 61 120330 02630.000Pyrene 3330 81.9 75 117330 02727.000 Surr: 1,2-Dichlorobenzene-d4 3330 73.3 45 1052441.667 Surr: 2,4,6-Tribromophenol 3330 83.5 41 1292781.667 Surr: 2-Chlorophenol-d4 3330 74.9 55 1082495.333 Surr: 2-Fluorobiphenyl 3330 78.6 56 1142617.333 Surr: 2-Fluorophenol 3330 73.2 50 1082439.000 Surr: 4-Terphenyl-d14 3330 87.6 59 1412917.667 Surr: Nitrobenzene-d5 3330 81.7 45 1142720.000 Surr: Phenol-d5 3330 76.5 46 1182548.667





Units: µg/Kg

PQL

Client ID: HA-7-0.5

RunNo: 117136

SeqNo: 1860165

MSSampType: TestCode: 8270_S_FUL

EPA 3550B

1,2,4-Trichlorobenzene 3330 69.3 62 1091600 02306.6671,4-Dichlorobenzene 3330 63.5 57 991600 02115.0002,4-Dinitrotoluene 3330 56.5 76 126 S1600 01880.0002-Chlorophenol 3330 62.1 52 1201600 02066.6674-Chloro-3-methylphenol 3330 57.2 63 137 S3300 01905.0004-Nitrophenol 3330 45.4 52 144 S8200 01513.333Acenaphthene 3330 66.4 61 1211600 02210.000N-Nitrosodi-n-propylamine 3330 75.1 67 1161600 02500.000Pentachlorophenol 3330 41.0 47 143 S8200 01366.667Phenol 3330 63.4 54 1261600 02111.667Pyrene 3330 64.3 68 121 S1600 02141.667 Surr: 1,2-Dichlorobenzene-d4 3330 58.5 45 1051946.667 Surr: 2,4,6-Tribromophenol 3330 52.7 41 1291753.333 Surr: 2-Chlorophenol-d4 3330 61.3 55 1082040.000 Surr: 2-Fluorobiphenyl 3330 66.7 56 1142220.000



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Units: µg/Kg

PQL

Client ID: HA-7-0.5

RunNo: 117136

SeqNo: 1860165

MSSampType: TestCode: 8270_S_FUL

EPA 3550B

Surr: 2-Fluorophenol 3330 58.6 50 1081950.000 Surr: 4-Terphenyl-d14 3330 61.7 59 1412053.333 Surr: Nitrobenzene-d5 3330 64.1 45 1142135.000 Surr: Phenol-d5 3330 61.0 46 1182030.000





Units: µg/Kg

PQL

Client ID: HA-7-0.5

RunNo: 117136

SeqNo: 1860166

MSDSampType: TestCode: 8270_S_FUL

EPA 3550B

1,2,4-Trichlorobenzene 3330 77.9 62 109 201600 0 2307 11.82595.0001,4-Dichlorobenzene 3330 70.6 57 99 201600 0 2115 10.62351.6672,4-Dinitrotoluene 3330 66.8 76 126 20 S1600 0 1880 16.82225.0002-Chlorophenol 3330 69.3 52 120 201600 0 2067 11.02308.3334-Chloro-3-methylphenol 3330 65.9 63 137 203300 0 1905 02195.0004-Nitrophenol 3330 58.4 52 144 208200 0 1513 01945.000Acenaphthene 3330 76.5 61 121 201600 0 2210 14.22548.333N-Nitrosodi-n-propylamine 3330 81.7 67 116 201600 0 2500 8.432720.000Pentachlorophenol 3330 53.0 47 143 208200 0 1367 01763.333Phenol 3330 70.4 54 126 201600 0 2112 10.42343.333Pyrene 3330 77.1 68 121 201600 0 2142 18.12566.667 Surr: 1,2-Dichlorobenzene-d4 3330 63.8 45 105 002123.333 Surr: 2,4,6-Tribromophenol 3330 62.4 41 129 002076.667 Surr: 2-Chlorophenol-d4 3330 66.1 55 108 002201.667 Surr: 2-Fluorobiphenyl 3330 74.4 56 114 002478.333 Surr: 2-Fluorophenol 3330 64.4 50 108 002145.000 Surr: 4-Terphenyl-d14 3330 68.4 59 141 002278.333 Surr: Nitrobenzene-d5 3330 71.4 45 114 002378.333 Surr: Phenol-d5 3330 65.8 46 118 002190.000



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Units: µg/Kg

PQL

Client ID: HA-8-0.5

RunNo: 117136

SeqNo: 1860169

DUPSampType: TestCode: 8270_S_FUL

EPA 3550B

1,2,4-Trichlorobenzene 206600 0 0ND1,2-Dichlorobenzene 206600 0 0ND1,2-Diphenylhydrazine 206600 0 0ND1,3-Dichlorobenzene 206600 0 0ND1,4-Dichlorobenzene 206600 0 0ND1,4-Dioxane 206600 0 0ND2,4,5-Trichlorophenol 206600 0 0ND2,4,6-Trichlorophenol 206600 0 0ND2,4-Dichlorophenol 2033000 0 0ND2,4-Dimethylphenol 206600 0 0ND2,4-Dinitrophenol 2033000 0 0ND2,4-Dinitrotoluene 206600 0 0ND2,6-Dinitrotoluene 206600 0 0ND2-Chloronaphthalene 206600 0 0ND2-Chlorophenol 206600 0 0ND2-Methylnaphthalene 206600 0 0ND2-Methylphenol 206600 0 0ND2-Nitroaniline 2033000 0 0ND2-Nitrophenol 206600 0 0ND3,3´-Dichlorobenzidine 2013000 0 0ND3-Nitroaniline 2033000 0 0ND4,6-Dinitro-2-methylphenol 2033000 0 0ND4-Bromophenyl-phenylether 206600 0 0ND4-Chloro-3-methylphenol 2013000 0 0ND4-Chloroaniline 2013000 0 0ND4-Chlorophenyl-phenylether 206600 0 0ND3/4-Methylphenol 206600 0 0ND4-Methylphenol 206600 0 0ND4-Nitroaniline 2033000 0 0ND4-Nitrophenol 2033000 0 0ND



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Units: µg/Kg

PQL

Client ID: HA-8-0.5

RunNo: 117136

SeqNo: 1860169


EPA 3550B

Acenaphthene 206600 0 0NDAcenaphthylene 206600 0 0NDAniline 206600 0 0NDAnthracene 206600 0 0NDBenzidine (M) 2033000 0 0NDBenzo(a)anthracene 206600 0 0NDBenzo(a)pyrene 206600 0 0NDBenzo(b)fluoranthene 206600 0 0NDBenzo(g,h,i)perylene 206600 0 0NDBenzo(k)fluoranthene 206600 0 0NDBenzoic acid 2033000 0 0NDBenzyl alcohol 2013000 0 0NDBis(2-chloroethoxy)methane 206600 0 0NDBis(2-chloroethyl)ether 206600 0 0NDBis(2-chloroisopropyl)ether 206600 0 0NDBis(2-ethylhexyl)phthalate 206600 0 0NDButylbenzylphthalate 206600 0 0NDCarbazole 206600 0 0NDChrysene 206600 0 0NDDi-n-butylphthalate 206600 0 0NDDi-n-octylphthalate 206600 0 0NDDibenz(a,h)anthracene 206600 0 0NDDibenzofuran 206600 0 0NDDiethylphthalate 206600 0 0NDDimethylphthalate 206600 0 0NDFluoranthene 206600 0 0NDFluorene 206600 0 0NDHexachlorobenzene 206600 0 0NDHexachlorobutadiene 2013000 0 0NDHexachlorocyclopentadiene 2013000 0 0ND



65 of 71









Units: µg/Kg

PQL

Client ID: HA-8-0.5

RunNo: 117136

SeqNo: 1860169


EPA 3550B

Hexachloroethane 206600 0 0NDIndeno(1,2,3-cd)pyrene 206600 0 0NDIsophorone 206600 0 0NDN-Nitrosodi-n-propylamine 206600 0 0NDN-Nitrosodimethylamine 206600 0 0NDN-Nitrosodiphenylamine 206600 0 0NDNaphthalene 206600 0 0NDNitrobenzene 206600 0 0NDPentachlorophenol 2033000 0 0NDPhenanthrene 206600 0 0NDPhenol 206600 0 0NDPyrene 206600 0 0NDPyridine 2033000 0 0ND Surr: 1,2-Dichlorobenzene-d4 3330 71.3 45 105 002373.333 Surr: 2,4,6-Tribromophenol 3330 52.1 41 129 001733.333 Surr: 2-Chlorophenol-d4 3330 70.1 55 108 002333.333 Surr: 2-Fluorobiphenyl 3330 78.9 56 114 002626.667 Surr: 2-Fluorophenol 3330 65.3 50 108 002173.333 Surr: 4-Terphenyl-d14 3330 72.3 59 141 002406.667 Surr: Nitrobenzene-d5 3330 71.1 45 114 002366.667 Surr: Phenol-d5 3330 68.9 46 118 002293.333



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Sample ID: MB-61000


Prep Date: 1/8/2010


Units: µg/L

PQL

Client ID: PBW

RunNo: 116813

SeqNo: 1854526

MBLKSampType: TestCode: 8270_W_FUL

EPA 3510C

1,2,4-Trichlorobenzene 10ND1,2-Dichlorobenzene 10ND1,3-Dichlorobenzene 10ND1,4-Dichlorobenzene 10ND2,4,5-Trichlorophenol 10ND2,4,6-Trichlorophenol 10ND2,4-Dichlorophenol 10ND2,4-Dimethylphenol 10ND2,4-Dinitrophenol 50ND2,4-Dinitrotoluene 10ND2,6-Dinitrotoluene 10ND2-Chloronaphthalene 10ND2-Chlorophenol 10ND2-Methylnaphthalene 10ND2-Methylphenol 10ND2-Nitroaniline 50ND2-Nitrophenol 10ND3,3´-Dichlorobenzidine 20ND3-Nitroaniline 50ND4,6-Dinitro-2-methylphenol 50ND4-Bromophenyl-phenylether 10ND4-Chloro-3-methylphenol 50ND4-Chloroaniline 20ND4-Chlorophenyl-phenylether 10ND4-Methylphenol 10ND4-Nitroaniline 20ND4-Nitrophenol 50NDAcenaphthene 10ND



67 of 71





Sample ID: MB-61000


Prep Date: 1/8/2010


Units: µg/L

PQL

Client ID: PBW

RunNo: 116813

SeqNo: 1854526


EPA 3510C

Acenaphthylene 10NDAnthracene 10NDBenzidine (M) 50NDBenzo(a)anthracene 10NDBenzo(a)pyrene 10NDBenzo(b)fluoranthene 10NDBenzo(g,h,i)perylene 10NDBenzo(k)fluoranthene 10NDBenzoic acid 50NDBenzyl alcohol 20NDBis(2-chloroethoxy)methane 10NDBis(2-chloroethyl)ether 10NDBis(2-chloroisopropyl)ether 10NDBis(2-ethylhexyl)phthalate 10NDButylbenzylphthalate 10NDChrysene 10NDDi-n-butylphthalate 10NDDi-n-octylphthalate 10NDDibenz(a,h)anthracene 10NDDibenzofuran 10NDDiethylphthalate 10NDDimethylphthalate 10NDFluoranthene 10NDFluorene 10NDHexachlorobenzene 10NDHexachlorobutadiene 20NDHexachlorocyclopentadiene 10NDHexachloroethane 10NDIndeno(1,2,3-cd)pyrene 10NDIsophorone 10ND



68 of 71





Sample ID: MB-61000


Prep Date: 1/8/2010


Units: µg/L

PQL

Client ID: PBW

RunNo: 116813

SeqNo: 1854526


EPA 3510C

N-Nitrosodi-n-propylamine 10NDN-Nitrosodiphenylamine 10NDNaphthalene 10NDNitrobenzene 10NDPentachlorophenol 50NDPhenanthrene 10NDPhenol 10NDPyrene 10ND Surr: 1,2-Dichlorobenzene-d4 100.0 52.6 46 9752.620 Surr: 2,4,6-Tribromophenol 100.0 70.7 59 12470.710 Surr: 2-Chlorophenol-d4 100.0 50.7 49 9350.660 Surr: 2-Fluorobiphenyl 100.0 59.4 57 10759.360 Surr: 2-Fluorophenol 100.0 29.6 27 6029.640 Surr: 4-Terphenyl-d14 100.0 102 69 132102.040 Surr: Nitrobenzene-d5 100.0 58.0 52 10758.010 Surr: Phenol-d5 100.0 21.2 15 5021.200



Prep Date: 1/8/2010


Units: µg/L

PQL

Client ID: LCSW

RunNo: 116813

SeqNo: 1854527

LCSSampType: TestCode: 8270_W_FUL

EPA 3510C

1,2,4-Trichlorobenzene 100.0 70.5 60 10610 070.4701,4-Dichlorobenzene 100.0 64.4 52 9810 064.4202,4-Dinitrotoluene 100.0 96.3 81 12310 096.3402-Chlorophenol 100.0 61.7 46 10510 061.6604-Chloro-3-methylphenol 100.0 78.9 51 14050 078.9104-Nitrophenol 100.0 39.8 20 7450 039.830Acenaphthene 100.0 85.6 64 11910 085.580N-Nitrosodi-n-propylamine 100.0 79.3 65 11710 079.290Pentachlorophenol 100.0 82.1 55 14250 082.060



69 of 71







Prep Date: 1/8/2010


Units: µg/L

PQL

Client ID: LCSW

RunNo: 116813

SeqNo: 1854527

LCSSampType: TestCode: 8270_W_FUL

EPA 3510C

Phenol 100.0 27.3 18 5210 027.270Pyrene 100.0 100 73 12010 0100.350 Surr: 1,2-Dichlorobenzene-d4 100.0 60.5 46 9760.520 Surr: 2,4,6-Tribromophenol 100.0 89.3 59 12489.300 Surr: 2-Chlorophenol-d4 100.0 60.9 49 9360.930 Surr: 2-Fluorobiphenyl 100.0 72.9 57 10772.900 Surr: 2-Fluorophenol 100.0 35.4 27 6035.440 Surr: 4-Terphenyl-d14 100.0 99.4 69 13299.400 Surr: Nitrobenzene-d5 100.0 68.6 52 10768.620 Surr: Phenol-d5 100.0 25.9 15 5025.940



Prep Date: 1/8/2010


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 116813

SeqNo: 1854528

MSSampType: TestCode: 8270_W_FUL

EPA 3510C

1,2,4-Trichlorobenzene 100.0 70.4 60 10610 070.4101,4-Dichlorobenzene 100.0 64.1 52 9810 064.0802,4-Dinitrotoluene 100.0 98.9 81 12310 098.9202-Chlorophenol 100.0 61.8 46 10510 061.7804-Chloro-3-methylphenol 100.0 79.8 51 14050 079.7704-Nitrophenol 100.0 40.9 20 7450 040.860Acenaphthene 100.0 88.1 64 11910 088.110N-Nitrosodi-n-propylamine 100.0 79.3 65 11710 079.310Pentachlorophenol 100.0 81.8 55 14250 081.810Phenol 100.0 27.4 18 5210 027.400Pyrene 100.0 98.3 73 12010 098.260 Surr: 1,2-Dichlorobenzene-d4 100.0 59.6 46 9759.590 Surr: 2,4,6-Tribromophenol 100.0 88.4 59 12488.380 Surr: 2-Chlorophenol-d4 100.0 60.3 49 9360.290 Surr: 2-Fluorobiphenyl 100.0 74.2 57 10774.230



70 of 71







Prep Date: 1/8/2010


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 116813

SeqNo: 1854528

MSSampType: TestCode: 8270_W_FUL

EPA 3510C

Surr: 2-Fluorophenol 100.0 34.6 27 6034.560 Surr: 4-Terphenyl-d14 100.0 95.3 69 13295.270 Surr: Nitrobenzene-d5 100.0 67.8 52 10767.840 Surr: Phenol-d5 100.0 25.4 15 5025.420



Prep Date: 1/8/2010


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 116813

SeqNo: 1854529

MSDSampType: TestCode: 8270_W_FUL

EPA 3510C

1,2,4-Trichlorobenzene 100.0 72.6 60 106 2010 0 70.41 3.0872.6101,4-Dichlorobenzene 100.0 65.1 52 98 2010 0 64.08 1.5965.1102,4-Dinitrotoluene 100.0 99.2 81 123 2010 0 98.92 0.25299.1702-Chlorophenol 100.0 64.5 46 105 2010 0 61.78 4.3764.5404-Chloro-3-methylphenol 100.0 81.3 51 140 2050 0 79.77 1.9281.3204-Nitrophenol 100.0 41.7 20 74 2050 0 40.86 041.720Acenaphthene 100.0 88.6 64 119 2010 0 88.11 0.53288.580N-Nitrosodi-n-propylamine 100.0 80.5 65 117 2010 0 79.31 1.5480.540Pentachlorophenol 100.0 85.0 55 142 2050 0 81.81 3.8285.000Phenol 100.0 28.2 18 52 2010 0 27.40 3.0228.240Pyrene 100.0 104 73 120 2010 0 98.26 5.83104.160 Surr: 1,2-Dichlorobenzene-d4 100.0 61.2 46 97 0061.210 Surr: 2,4,6-Tribromophenol 100.0 90.8 59 124 0090.840 Surr: 2-Chlorophenol-d4 100.0 62.2 49 93 0062.150 Surr: 2-Fluorobiphenyl 100.0 74.6 57 107 0074.580 Surr: 2-Fluorophenol 100.0 35.7 27 60 0035.740 Surr: 4-Terphenyl-d14 100.0 99.2 69 132 0099.240 Surr: Nitrobenzene-d5 100.0 70.2 52 107 0070.200 Surr: Phenol-d5 100.0 26.6 15 50 0026.640



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Contract No:

Date Reported

109494-001A HA-9-0.5 1/7/2010 8:56:00 AM 1/8/2010 1/25/2010Soil

109494-002A HA-9-2 1/7/2010 9:02:00 AM 1/8/2010 1/25/2010Soil

109494-003A HA-10-0.5 1/7/2010 9:18:00 AM 1/8/2010 1/25/2010Soil

109494-004A HA-10-2 1/7/2010 9:25:00 AM 1/8/2010 1/25/2010Soil

109494-005A HA-11-0.5 1/7/2010 9:38:00 AM 1/8/2010 1/25/2010Soil

109494-006A HA-11-2 1/7/2010 9:46:00 AM 1/8/2010 1/25/2010Soil

109494-007A HA-12-0.5 1/7/2010 10:15:00 AM 1/8/2010 1/25/2010Soil

109494-008A HA-12-2 1/7/2010 10:20:00 AM 1/8/2010 1/25/2010Soil

109494-009A HA-13-0.5 1/7/2010 10:40:00 AM 1/8/2010 1/25/2010Soil

109494-010A HA-13-2 1/7/2010 10:45:00 AM 1/8/2010 1/25/2010Soil

109494-011A DUP-02 1/7/2010 1/8/2010 1/25/2010Soil

109494-012A HA-14-0.5 1/7/2010 12:13:00 PM 1/8/2010 1/25/2010Soil

109494-013A HA-14-2 1/7/2010 12:24:00 PM 1/8/2010 1/25/2010Soil

109494-014A HA-15-0.5 1/7/2010 12:37:00 PM 1/8/2010 1/25/2010Soil

109494-015A HA-15-2 1/7/2010 12:41:00 PM 1/8/2010 1/25/2010Soil

109494-016A QCEB-02 1/7/2010 1:00:00 PM 1/8/2010 1/25/2010Water

109494-016B QCEB-02 1/7/2010 1:00:00 PM 1/8/2010 1/25/2010Water

109494-016C QCEB-02 1/7/2010 1:00:00 PM 1/8/2010 1/25/2010Water

109494-016D QCEB-02 1/7/2010 1:00:00 PM 1/8/2010 1/25/2010Water

109494-016E QCEB-02 1/7/2010 1:00:00 PM 1/8/2010 1/25/2010Water

Page 1 of 1

2 of 38







Analytical Comments for EPA 6010B


Page 2 of 12

3 of 38




Matrix: SOIL



Lab ID: 109494-001A

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3050B


Antimony 1/13/2010 03:28 PM2.0 mg/Kg 1NDArsenic 1/13/2010 03:28 PM1.0 mg/Kg 13.0Barium 1/13/2010 03:28 PM1.0 mg/Kg 1110Beryllium 1/13/2010 03:28 PM1.0 mg/Kg 1NDCadmium 1/13/2010 03:28 PM1.0 mg/Kg 1NDChromium 1/13/2010 03:28 PM1.0 mg/Kg 124Cobalt 1/13/2010 03:28 PM1.0 mg/Kg 13.3Copper 1/13/2010 03:28 PM2.0 mg/Kg 19.1Lead 1/13/2010 03:28 PM1.0 mg/Kg 137Molybdenum 1/13/2010 03:28 PM1.0 mg/Kg 1NDNickel 1/13/2010 03:28 PM1.0 mg/Kg 110Selenium 1/13/2010 03:28 PM1.0 mg/Kg 1NDSilver 1/13/2010 03:28 PM1.0 mg/Kg 1NDThallium 1/13/2010 03:28 PM1.0 mg/Kg 1NDVanadium 1/13/2010 03:28 PM1.0 mg/Kg 126Zinc 1/13/2010 03:28 PM1.0 mg/Kg 132


Analyst: CLRunID: AA5_100125B 61337QC Batch: PrepDate: 1/25/2010

Mercury 1/25/2010 11:56 AM0.10 mg/Kg 1NDVOLATILE ORGANIC COMPOUNDS BY GC/MS

EPA 8260B

Analyst: HHRunID: MS4_100118A K10VS019QC Batch: PrepDate:

1,1,1,2-Tetrachloroethane 1/18/2010 02:42 PM5.0 µg/Kg 1ND1,1,1-Trichloroethane 1/18/2010 02:42 PM5.0 µg/Kg 1ND1,1,2,2-Tetrachloroethane 1/18/2010 02:42 PM5.0 µg/Kg 1ND1,1,2-Trichloroethane 1/18/2010 02:42 PM5.0 µg/Kg 1ND1,1-Dichloroethane 1/18/2010 02:42 PM5.0 µg/Kg 1ND1,1-Dichloroethene 1/18/2010 02:42 PM5.0 µg/Kg 1ND1,1-Dichloropropene 1/18/2010 02:42 PM5.0 µg/Kg 1ND1,2,3-Trichlorobenzene 1/18/2010 02:42 PM5.0 µg/Kg 1ND1,2,3-Trichloropropane 1/18/2010 02:42 PM5.0 µg/Kg 1ND1,2,4-Trichlorobenzene 1/18/2010 02:42 PM5.0 µg/Kg 1ND1,2,4-Trimethylbenzene 1/18/2010 02:42 PM5.0 µg/Kg 1ND



4 of 38




Matrix: SOIL



Lab ID: 109494-001A

DF


PQL

ANALYTICAL RESULTS



1,2-Dibromo-3-chloropropane 1/18/2010 02:42 PM10 µg/Kg 1ND1,2-Dibromoethane 1/18/2010 02:42 PM5.0 µg/Kg 1ND1,2-Dichlorobenzene 1/18/2010 02:42 PM5.0 µg/Kg 1ND1,2-Dichloroethane 1/18/2010 02:42 PM5.0 µg/Kg 1ND1,2-Dichloropropane 1/18/2010 02:42 PM5.0 µg/Kg 1ND1,3,5-Trimethylbenzene 1/18/2010 02:42 PM5.0 µg/Kg 1ND1,3-Dichlorobenzene 1/18/2010 02:42 PM5.0 µg/Kg 1ND1,3-Dichloropropane 1/18/2010 02:42 PM5.0 µg/Kg 1ND1,4-Dichlorobenzene 1/18/2010 02:42 PM5.0 µg/Kg 1ND2,2-Dichloropropane 1/18/2010 02:42 PM5.0 µg/Kg 1ND2-Chlorotoluene 1/18/2010 02:42 PM5.0 µg/Kg 1ND4-Chlorotoluene 1/18/2010 02:42 PM5.0 µg/Kg 1ND4-Isopropyltoluene 1/18/2010 02:42 PM5.0 µg/Kg 1NDBenzene 1/18/2010 02:42 PM5.0 µg/Kg 1NDBromobenzene 1/18/2010 02:42 PM5.0 µg/Kg 1NDBromodichloromethane 1/18/2010 02:42 PM5.0 µg/Kg 1NDBromoform 1/18/2010 02:42 PM5.0 µg/Kg 1NDBromomethane 1/18/2010 02:42 PM5.0 µg/Kg 1NDCarbon tetrachloride 1/18/2010 02:42 PM5.0 µg/Kg 1NDChlorobenzene 1/18/2010 02:42 PM5.0 µg/Kg 1NDChloroethane 1/18/2010 02:42 PM5.0 µg/Kg 1NDChloroform 1/18/2010 02:42 PM5.0 µg/Kg 1NDChloromethane 1/18/2010 02:42 PM5.0 µg/Kg 1NDcis-1,2-Dichloroethene 1/18/2010 02:42 PM5.0 µg/Kg 1NDcis-1,3-Dichloropropene 1/18/2010 02:42 PM5.0 µg/Kg 1NDDibromochloromethane 1/18/2010 02:42 PM5.0 µg/Kg 1NDDibromomethane 1/18/2010 02:42 PM5.0 µg/Kg 1NDDichlorodifluoromethane 1/18/2010 02:42 PM5.0 µg/Kg 1NDEthylbenzene 1/18/2010 02:42 PM5.0 µg/Kg 1NDHexachlorobutadiene 1/18/2010 02:42 PM5.0 µg/Kg 1NDIsopropylbenzene 1/18/2010 02:42 PM5.0 µg/Kg 1NDm,p-Xylene 1/18/2010 02:42 PM10 µg/Kg 1NDMethylene chloride 1/18/2010 02:42 PM5.0 µg/Kg 1NDn-Butylbenzene 1/18/2010 02:42 PM5.0 µg/Kg 1NDn-Propylbenzene 1/18/2010 02:42 PM5.0 µg/Kg 1ND



5 of 38




Matrix: SOIL



Lab ID: 109494-001A

DF


PQL

ANALYTICAL RESULTS



Naphthalene 1/18/2010 02:42 PM5.0 µg/Kg 1NDo-Xylene 1/18/2010 02:42 PM5.0 µg/Kg 1NDsec-Butylbenzene 1/18/2010 02:42 PM5.0 µg/Kg 1NDStyrene 1/18/2010 02:42 PM5.0 µg/Kg 1NDtert-Butylbenzene 1/18/2010 02:42 PM5.0 µg/Kg 1NDTetrachloroethene 1/18/2010 02:42 PM5.0 µg/Kg 1NDToluene 1/18/2010 02:42 PM5.0 µg/Kg 1NDtrans-1,2-Dichloroethene 1/18/2010 02:42 PM5.0 µg/Kg 1NDTrichloroethene 1/18/2010 02:42 PM5.0 µg/Kg 1NDTrichlorofluoromethane 1/18/2010 02:42 PM5.0 µg/Kg 1NDVinyl chloride 1/18/2010 02:42 PM5.0 µg/Kg 1ND Surr: 1,2-Dichloroethane-d4 1/18/2010 02:42 PM70-130 %REC 184.3 Surr: 4-Bromofluorobenzene 1/18/2010 02:42 PM70-130 %REC 182.7 Surr: Dibromofluoromethane 1/18/2010 02:42 PM70-130 %REC 183.2 Surr: Toluene-d8 1/18/2010 02:42 PM70-130 %REC 188.1



6 of 38




Matrix: SOIL



Lab ID: 109494-002A

DF


PQL

ANALYTICAL RESULTS


Analyst: CBR

LUFT





7 of 38




Matrix: SOIL



Lab ID: 109494-005A

DF


PQL

ANALYTICAL RESULTS



1,1,1,2-Tetrachloroethane 1/18/2010 02:57 PM5.0 µg/Kg 1ND1,1,1-Trichloroethane 1/18/2010 02:57 PM5.0 µg/Kg 1ND1,1,2,2-Tetrachloroethane 1/18/2010 02:57 PM5.0 µg/Kg 1ND1,1,2-Trichloroethane 1/18/2010 02:57 PM5.0 µg/Kg 1ND1,1-Dichloroethane 1/18/2010 02:57 PM5.0 µg/Kg 1ND1,1-Dichloroethene 1/18/2010 02:57 PM5.0 µg/Kg 1ND1,1-Dichloropropene 1/18/2010 02:57 PM5.0 µg/Kg 1ND1,2,3-Trichlorobenzene 1/18/2010 02:57 PM5.0 µg/Kg 1ND1,2,3-Trichloropropane 1/18/2010 02:57 PM5.0 µg/Kg 1ND1,2,4-Trichlorobenzene 1/18/2010 02:57 PM5.0 µg/Kg 1ND1,2,4-Trimethylbenzene 1/18/2010 02:57 PM5.0 µg/Kg 1ND1,2-Dibromo-3-chloropropane 1/18/2010 02:57 PM10 µg/Kg 1ND1,2-Dibromoethane 1/18/2010 02:57 PM5.0 µg/Kg 1ND1,2-Dichlorobenzene 1/18/2010 02:57 PM5.0 µg/Kg 1ND1,2-Dichloroethane 1/18/2010 02:57 PM5.0 µg/Kg 1ND1,2-Dichloropropane 1/18/2010 02:57 PM5.0 µg/Kg 1ND1,3,5-Trimethylbenzene 1/18/2010 02:57 PM5.0 µg/Kg 1ND1,3-Dichlorobenzene 1/18/2010 02:57 PM5.0 µg/Kg 1ND1,3-Dichloropropane 1/18/2010 02:57 PM5.0 µg/Kg 1ND1,4-Dichlorobenzene 1/18/2010 02:57 PM5.0 µg/Kg 1ND2,2-Dichloropropane 1/18/2010 02:57 PM5.0 µg/Kg 1ND2-Chlorotoluene 1/18/2010 02:57 PM5.0 µg/Kg 1ND4-Chlorotoluene 1/18/2010 02:57 PM5.0 µg/Kg 1ND4-Isopropyltoluene 1/18/2010 02:57 PM5.0 µg/Kg 1NDBenzene 1/18/2010 02:57 PM5.0 µg/Kg 1NDBromobenzene 1/18/2010 02:57 PM5.0 µg/Kg 1NDBromodichloromethane 1/18/2010 02:57 PM5.0 µg/Kg 1NDBromoform 1/18/2010 02:57 PM5.0 µg/Kg 1NDBromomethane 1/18/2010 02:57 PM5.0 µg/Kg 1NDCarbon tetrachloride 1/18/2010 02:57 PM5.0 µg/Kg 1NDChlorobenzene 1/18/2010 02:57 PM5.0 µg/Kg 1NDChloroethane 1/18/2010 02:57 PM5.0 µg/Kg 1NDChloroform 1/18/2010 02:57 PM5.0 µg/Kg 1NDChloromethane 1/18/2010 02:57 PM5.0 µg/Kg 1NDcis-1,2-Dichloroethene 1/18/2010 02:57 PM5.0 µg/Kg 1ND



8 of 38




Matrix: SOIL



Lab ID: 109494-005A

DF


PQL

ANALYTICAL RESULTS



cis-1,3-Dichloropropene 1/18/2010 02:57 PM5.0 µg/Kg 1NDDibromochloromethane 1/18/2010 02:57 PM5.0 µg/Kg 1NDDibromomethane 1/18/2010 02:57 PM5.0 µg/Kg 1NDDichlorodifluoromethane 1/18/2010 02:57 PM5.0 µg/Kg 1NDEthylbenzene 1/18/2010 02:57 PM5.0 µg/Kg 1NDHexachlorobutadiene 1/18/2010 02:57 PM5.0 µg/Kg 1NDIsopropylbenzene 1/18/2010 02:57 PM5.0 µg/Kg 1NDm,p-Xylene 1/18/2010 02:57 PM10 µg/Kg 1NDMethylene chloride 1/18/2010 02:57 PM5.0 µg/Kg 1NDn-Butylbenzene 1/18/2010 02:57 PM5.0 µg/Kg 1NDn-Propylbenzene 1/18/2010 02:57 PM5.0 µg/Kg 1NDNaphthalene 1/18/2010 02:57 PM5.0 µg/Kg 1NDo-Xylene 1/18/2010 02:57 PM5.0 µg/Kg 1NDsec-Butylbenzene 1/18/2010 02:57 PM5.0 µg/Kg 1NDStyrene 1/18/2010 02:57 PM5.0 µg/Kg 1NDtert-Butylbenzene 1/18/2010 02:57 PM5.0 µg/Kg 1NDTetrachloroethene 1/18/2010 02:57 PM5.0 µg/Kg 1NDToluene 1/18/2010 02:57 PM5.0 µg/Kg 1NDtrans-1,2-Dichloroethene 1/18/2010 02:57 PM5.0 µg/Kg 1NDTrichloroethene 1/18/2010 02:57 PM5.0 µg/Kg 1NDTrichlorofluoromethane 1/18/2010 02:57 PM5.0 µg/Kg 1NDVinyl chloride 1/18/2010 02:57 PM5.0 µg/Kg 1ND Surr: 1,2-Dichloroethane-d4 1/18/2010 02:57 PM70-130 %REC 185.9 Surr: 4-Bromofluorobenzene 1/18/2010 02:57 PM70-130 %REC 185.7 Surr: Dibromofluoromethane 1/18/2010 02:57 PM70-130 %REC 182.2 Surr: Toluene-d8 1/18/2010 02:57 PM70-130 %REC 190.0



9 of 38




Matrix: SOIL



Lab ID: 109494-006A

DF


PQL

ANALYTICAL RESULTS


Analyst: CBR

LUFT





10 of 38




Matrix: WATER



Lab ID: 109494-016A

DF


PQL

ANALYTICAL RESULTS


Analyst: SLLRunID: MS11_100115B A10VW015QC Batch: PrepDate:




11 of 38




Matrix: WATER



Lab ID: 109494-016A

DF


PQL

ANALYTICAL RESULTS


Analyst: SLLRunID: MS11_100115B A10VW015QC Batch: PrepDate:

cis-1,3-Dichloropropene 1/16/2010 03:20 AM5.0 µg/L 1NDDibromochloromethane 1/16/2010 03:20 AM5.0 µg/L 1NDDibromomethane 1/16/2010 03:20 AM5.0 µg/L 1NDDichlorodifluoromethane 1/16/2010 03:20 AM5.0 µg/L 1NDEthylbenzene 1/16/2010 03:20 AM5.0 µg/L 1NDHexachlorobutadiene 1/16/2010 03:20 AM5.0 µg/L 1NDIsopropylbenzene 1/16/2010 03:20 AM5.0 µg/L 1NDm,p-Xylene 1/16/2010 03:20 AM10 µg/L 1NDMethylene chloride 1/16/2010 03:20 AM5.0 µg/L 1NDn-Butylbenzene 1/16/2010 03:20 AM5.0 µg/L 1NDn-Propylbenzene 1/16/2010 03:20 AM5.0 µg/L 1NDNaphthalene 1/16/2010 03:20 AM5.0 µg/L 1NDo-Xylene 1/16/2010 03:20 AM5.0 µg/L 1NDsec-Butylbenzene 1/16/2010 03:20 AM5.0 µg/L 1NDStyrene 1/16/2010 03:20 AM5.0 µg/L 1NDtert-Butylbenzene 1/16/2010 03:20 AM5.0 µg/L 1NDTetrachloroethene 1/16/2010 03:20 AM5.0 µg/L 1NDToluene 1/16/2010 03:20 AM5.0 µg/L 1NDtrans-1,2-Dichloroethene 1/16/2010 03:20 AM5.0 µg/L 1NDTrichloroethene 1/16/2010 03:20 AM5.0 µg/L 1NDTrichlorofluoromethane 1/16/2010 03:20 AM5.0 µg/L 1NDVinyl chloride 1/16/2010 03:20 AM5.0 µg/L 1ND Surr: 1,2-Dichloroethane-d4 1/16/2010 03:20 AM70-130 %REC 199.6 Surr: 4-Bromofluorobenzene 1/16/2010 03:20 AM70-130 %REC 1114 Surr: Dibromofluoromethane 1/16/2010 03:20 AM70-130 %REC 1102



12 of 38




Matrix: WATER



Lab ID: 109494-016E

DF


PQL

ANALYTICAL RESULTS

ICP METALSEPA 6010B

Analyst: CL

EPA 3010A


Antimony 1/12/2010 06:28 PM0.0050 mg/L 10.0066Arsenic 1/12/2010 06:28 PM0.010 mg/L 1NDBarium 1/12/2010 06:28 PM0.0030 mg/L 1NDBeryllium 1/12/2010 06:28 PM0.0030 mg/L 1NDCadmium 1/12/2010 06:28 PM0.0030 mg/L 1NDChromium 1/12/2010 06:28 PM0.0030 mg/L 1NDCobalt 1/12/2010 06:28 PM0.0030 mg/L 1NDCopper 1/12/2010 06:28 PM0.0050 mg/L 1NDLead 1/12/2010 06:28 PM0.0050 mg/L 1NDMolybdenum 1/12/2010 06:28 PM0.0050 mg/L 1NDNickel 1/12/2010 06:28 PM0.0050 mg/L 1NDSelenium 1/12/2010 06:28 PM0.010 mg/L 1NDSilver 1/12/2010 06:28 PM0.0030 mg/L 10.0093Thallium 1/12/2010 06:28 PM0.015 mg/L 1NDVanadium 1/12/2010 06:28 PM0.0030 mg/L 1NDZinc 1/12/2010 06:28 PM0.010 mg/L 1ND


Analyst: ILRunID: AA1_100112D 61035QC Batch: PrepDate: 1/11/2010

Mercury 1/12/2010 01:48 PM0.20 µg/L 1ND



13 of 38






Sample ID: MB-61036




Units: mg/Kg

PQL

Client ID: PBS

RunNo: 116884

SeqNo: 1855414


EPA 3050B

Antimony 2.0NDArsenic 1.0NDBarium 1.0NDBeryllium 1.0NDCadmium 1.0NDChromium 1.0NDCobalt 1.0NDCopper 2.0NDLead 1.0NDMolybdenum 1.00.132Nickel 1.0NDSelenium 1.0NDSilver 1.0NDThallium 1.0NDVanadium 1.0NDZinc 1.0ND





Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 116884

SeqNo: 1855415


EPA 3050B

Antimony 50.00 100 80 1202.0 050.047Arsenic 50.00 98.5 80 1201.0 049.251Barium 50.00 101 80 1201.0 050.470Beryllium 50.00 100 80 1201.0 050.079Cadmium 50.00 98.5 80 1201.0 049.273Chromium 50.00 99.4 80 1201.0 049.725Cobalt 50.00 102 80 1201.0 050.904



14 of 38









Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 116884

SeqNo: 1855415


EPA 3050B

Copper 50.00 103 80 1202.0 051.647Lead 50.00 98.8 80 1201.0 049.412Molybdenum 50.00 104 80 1201.0 0.131952.157Nickel 50.00 98.0 80 1201.0 049.021Selenium 50.00 95.4 80 1201.0 047.708Silver 50.00 102 80 1201.0 051.044Thallium 50.00 103 80 1201.0 051.358Vanadium 50.00 102 80 1201.0 050.967Zinc 50.00 98.4 80 1201.0 049.178





Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 116884

SeqNo: 1855417


EPA 3050B

Antimony 202.0 0 0NDArsenic 201.0 0.3298 0NDBarium 201.0 36.98 3.3935.746Beryllium 201.0 0.09936 0NDCadmium 201.0 0.1797 00.197Chromium 201.0 15.47 10.617.205Cobalt 201.0 15.22 1.6014.976Copper 20 R2.0 26.79 1107.822Lead 201.0 6.196 8.185.709Molybdenum 201.0 0 0NDNickel 201.0 14.01 17.216.646Selenium 201.0 0 0NDSilver 201.0 0.8246 00.667Thallium 201.0 0 0NDVanadium 201.0 10.46 19.112.667Zinc 201.0 18.03 19.121.842



15 of 38









Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 116884

SeqNo: 1855418


EPA 3050B

Antimony 125.0 87.5 25 1062.0 0109.373Arsenic 125.0 88.1 42 1131.0 0.3298110.462Barium 125.0 92.4 19 1401.0 36.98152.525Beryllium 125.0 91.1 50 1091.0 0.09936113.945Cadmium 125.0 87.2 48 1061.0 0.1797109.215Chromium 125.0 94.6 44 1161.0 15.47133.741Cobalt 125.0 81.6 47 1071.0 15.22117.266Copper 125.0 92.3 49 1242.0 26.79142.174Lead 125.0 88.2 33 1201.0 6.196116.403Molybdenum 125.0 91.9 46 1111.0 0114.892Nickel 125.0 91.2 43 1111.0 14.01128.047Selenium 125.0 84.0 43 1041.0 0105.048Silver 125.0 94.8 53 1141.0 0.8246119.322Thallium 125.0 89.5 41 1071.0 0111.904Vanadium 125.0 94.7 48 1161.0 10.46128.895Zinc 125.0 89.8 24 1291.0 18.03130.336





Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 116884

SeqNo: 1855419


EPA 3050B

Antimony 125.0 85.5 25 106 202.0 0 109.4 2.30106.890Arsenic 125.0 86.2 42 113 201.0 0.3298 110.5 2.24108.020Barium 125.0 97.7 19 140 201.0 36.98 152.5 4.25159.149Beryllium 125.0 89.8 50 109 201.0 0.09936 113.9 1.44112.319Cadmium 125.0 85.2 48 106 201.0 0.1797 109.2 2.32106.712Chromium 125.0 93.5 44 116 201.0 15.47 133.7 1.01132.396Cobalt 125.0 81.7 47 107 201.0 15.22 117.3 0.0385117.311Copper 125.0 82.7 49 124 202.0 26.79 142.2 8.82130.166Lead 125.0 85.8 33 120 201.0 6.196 116.4 2.55113.478



16 of 38









Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 116884

SeqNo: 1855419


EPA 3050B

Molybdenum 125.0 90.2 46 111 201.0 0 114.9 1.92112.703Nickel 125.0 90.4 43 111 201.0 14.01 128.0 0.858126.953Selenium 125.0 81.9 43 104 201.0 0 105.0 2.53102.428Silver 125.0 93.2 53 114 201.0 0.8246 119.3 1.70117.314Thallium 125.0 88.0 41 107 201.0 0 111.9 1.75109.965Vanadium 125.0 93.2 48 116 201.0 10.46 128.9 1.54126.924Zinc 125.0 84.5 24 129 201.0 18.03 130.3 5.26123.659



17 of 38






Sample ID: MB-61037




Units: mg/L

PQL

Client ID: PBW

RunNo: 116883

SeqNo: 1855406


EPA 3010A

Antimony 0.0050NDArsenic 0.010NDBarium 0.0030NDBeryllium 0.0030NDCadmium 0.0030NDChromium 0.0030NDCobalt 0.0030NDCopper 0.0050NDLead 0.0050NDMolybdenum 0.0050NDNickel 0.0050NDSelenium 0.010NDSilver 0.0030NDThallium 0.015NDVanadium 0.0030NDZinc 0.0100.004





Units: mg/L

PQL

Client ID: LCSW

RunNo: 116883

SeqNo: 1855407


EPA 3010A

Antimony 1.000 94.5 85 1150.0050 00.945Arsenic 1.000 92.3 85 1150.010 00.923Barium 1.000 93.7 85 1150.0030 00.937Beryllium 1.000 94.0 85 1150.0030 00.940Cadmium 1.000 91.9 85 1150.0030 00.919Chromium 1.000 91.3 85 1150.0030 00.913Cobalt 1.000 95.1 85 1150.0030 00.951



18 of 38









Units: mg/L

PQL

Client ID: LCSW

RunNo: 116883

SeqNo: 1855407


EPA 3010A

Copper 1.000 94.3 85 1150.0050 00.943Lead 1.000 92.5 85 1150.0050 00.925Molybdenum 1.000 94.3 85 1150.0050 00.943Nickel 1.000 91.7 85 1150.0050 00.917Selenium 1.000 91.6 85 1150.010 00.916Silver 1.000 96.2 85 1150.0030 00.962Thallium 1.000 95.7 85 1150.015 00.957Vanadium 1.000 93.4 85 1150.0030 00.934Zinc 1.000 91.2 85 1150.010 0.0040920.916





Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 116883

SeqNo: 1855409


EPA 3010A




19 of 38









Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 116883

SeqNo: 1855410


EPA 3010A






Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 116883

SeqNo: 1855411


EPA 3010A




20 of 38









Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 116883

SeqNo: 1855411


EPA 3010A




21 of 38






Sample ID: MB-61337




Units: mg/Kg

PQL

Client ID: PBS

RunNo: 117279

SeqNo: 1862494


Mercury 0.10ND





Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 117279

SeqNo: 1862495


Mercury 0.8300 97.9 80 1200.10 00.813





Units: mg/Kg

PQL

Client ID: HA-9-0.5

RunNo: 117279

SeqNo: 1862496


Mercury 0.8300 99.5 70 1300.10 0.029030.854





Units: mg/Kg

PQL

Client ID: HA-9-0.5

RunNo: 117279

SeqNo: 1862497


Mercury 0.8300 99.9 70 130 200.10 0.02903 0.8545 0.4840.859





Units: mg/Kg

PQL

Client ID: HA-9-0.5

RunNo: 117279

SeqNo: 1862499


Mercury 200.10 0.02903 00.029



22 of 38






Sample ID: MB-61035




Units: µg/L

PQL

Client ID: PBW

RunNo: 116857

SeqNo: 1855117


Mercury 0.20ND





Units: µg/L

PQL

Client ID: LCSW

RunNo: 116857

SeqNo: 1855118


Mercury 10.00 96.0 85 1150.20 09.598

Sample ID: 109494-016E-MS




Units: µg/L

PQL

Client ID: QCEB-02

RunNo: 116857

SeqNo: 1855119


Mercury 10.00 95.5 70 1300.20 09.552

Sample ID: 109494-016E-MSD




Units: µg/L

PQL

Client ID: QCEB-02

RunNo: 116857

SeqNo: 1855120


Mercury 10.00 95.5 70 130 200.20 0 9.552 0.04239.548

Sample ID: 109494-016E-DUP




Units: µg/L

PQL

Client ID: QCEB-02

RunNo: 116857

SeqNo: 1855122


Mercury 200.20 0 0ND



23 of 38






Sample ID: K100118LC1


Prep Date:


Units: µg/Kg

PQL

Client ID: LCSS

RunNo: 117070

SeqNo: 1858908


1,1-Dichloroethene 50.00 113 70 1305.0 056.420Benzene 100.0 103 70 1305.0 0103.040Chlorobenzene 50.00 104 70 1305.0 052.130MTBE 50.00 104 70 1305.0 051.900Toluene 100.0 103 70 1305.0 0103.190Trichloroethene 50.00 99.4 70 1305.0 049.700 Surr: 1,2-Dichloroethane-d4 50.00 95.5 70 13047.740 Surr: 4-Bromofluorobenzene 50.00 93.0 70 13046.520 Surr: Dibromofluoromethane 50.00 85.2 70 13042.590 Surr: Toluene-d8 50.00 89.4 70 13044.690



Prep Date:


Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 117070

SeqNo: 1858909


1,1-Dichloroethene 50.00 104 70 1305.0 051.930Benzene 100.0 98.3 70 1305.0 098.320Chlorobenzene 50.00 93.6 70 1305.0 046.820Toluene 100.0 100 70 1305.0 0100.190Trichloroethene 50.00 95.9 70 1305.0 047.960 Surr: 1,2-Dichloroethane-d4 50.00 101 70 13050.250 Surr: 4-Bromofluorobenzene 50.00 86.3 70 13043.130 Surr: Dibromofluoromethane 50.00 85.6 70 13042.810 Surr: Toluene-d8 50.00 88.6 70 13044.320



24 of 38







Prep Date:


Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 117070

SeqNo: 1858910


1,1-Dichloroethene 50.00 97.2 70 130 205.0 0 51.93 6.5848.620Benzene 100.0 96.8 70 130 205.0 0 98.32 1.5296.840Chlorobenzene 50.00 90.5 70 130 205.0 0 46.82 3.3945.260Toluene 100.0 98.4 70 130 205.0 0 100.2 1.7898.420Trichloroethene 50.00 94.7 70 130 205.0 0 47.96 1.3247.330 Surr: 1,2-Dichloroethane-d4 50.00 88.6 70 130 20044.310 Surr: 4-Bromofluorobenzene 50.00 89.0 70 130 20044.480 Surr: Dibromofluoromethane 50.00 81.1 70 130 20040.530 Surr: Toluene-d8 50.00 90.9 70 130 20045.430



Prep Date:


Units: µg/Kg

PQL

Client ID: PBS

RunNo: 117070

SeqNo: 1858911


1,1,1,2-Tetrachloroethane 5.0ND1,1,1-Trichloroethane 5.0ND1,1,2,2-Tetrachloroethane 5.0ND1,1,2-Trichloroethane 5.0ND1,1-Dichloroethane 5.0ND1,1-Dichloroethene 5.0ND1,1-Dichloropropene 5.0ND1,2,3-Trichlorobenzene 5.0ND1,2,3-Trichloropropane 5.0ND1,2,4-Trichlorobenzene 5.0ND1,2,4-Trimethylbenzene 5.0ND1,2-Dibromo-3-chloropropane 10ND1,2-Dibromoethane 5.0ND1,2-Dichlorobenzene 5.0ND1,2-Dichloroethane 5.0ND1,2-Dichloropropane 5.0ND



25 of 38







Prep Date:


Units: µg/Kg

PQL

Client ID: PBS

RunNo: 117070

SeqNo: 1858911





26 of 38







Prep Date:


Units: µg/Kg

PQL

Client ID: PBS

RunNo: 117070

SeqNo: 1858911


Naphthalene 5.0NDo-Xylene 5.0NDsec-Butylbenzene 5.0NDStyrene 5.0NDtert-Butylbenzene 5.0NDTetrachloroethene 5.0NDToluene 5.0NDtrans-1,2-Dichloroethene 5.0NDTrichloroethene 5.0NDTrichlorofluoromethane 5.0NDVinyl chloride 5.0ND Surr: 1,2-Dichloroethane-d4 50.00 92.7 70 13046.370 Surr: 4-Bromofluorobenzene 50.00 89.2 70 13044.580 Surr: Dibromofluoromethane 50.00 81.4 70 13040.690 Surr: Toluene-d8 50.00 87.5 70 13043.770



Prep Date:


Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 117070

SeqNo: 1858936





27 of 38







Prep Date:


Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 117070

SeqNo: 1858936


1,2,4-Trimethylbenzene 205.0 0 0ND1,2-Dibromo-3-chloropropane 2010 0 0ND1,2-Dibromoethane 205.0 0 0ND1,2-Dichlorobenzene 205.0 0 0ND1,2-Dichloroethane 205.0 0 0ND1,2-Dichloropropane 205.0 0 0ND1,3,5-Trimethylbenzene 205.0 0 0ND1,3-Dichlorobenzene 205.0 0 0ND1,3-Dichloropropane 205.0 0 0ND1,4-Dichlorobenzene 205.0 0 0ND2,2-Dichloropropane 205.0 0 0ND2-Chlorotoluene 205.0 0 0ND4-Chlorotoluene 205.0 0 0ND4-Isopropyltoluene 205.0 0 0NDBenzene 205.0 0 0NDBromobenzene 205.0 0 0NDBromodichloromethane 205.0 0 0NDBromoform 205.0 0 0NDBromomethane 205.0 0 0NDCarbon tetrachloride 205.0 0 0NDChlorobenzene 205.0 0 0NDChloroethane 205.0 0 0NDChloroform 205.0 0 0NDChloromethane 205.0 0 0NDcis-1,2-Dichloroethene 205.0 0 0NDcis-1,3-Dichloropropene 205.0 0 0NDDibromochloromethane 205.0 0 0NDDibromomethane 205.0 0 0NDDichlorodifluoromethane 205.0 0 0NDEthylbenzene 205.0 0 0ND



28 of 38







Prep Date:


Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 117070

SeqNo: 1858936


Hexachlorobutadiene 205.0 0 0NDIsopropylbenzene 205.0 0 0NDm,p-Xylene 2010 0 0NDMethylene chloride 205.0 0 0NDn-Butylbenzene 205.0 0 0NDn-Propylbenzene 205.0 0 0NDNaphthalene 205.0 0 0NDo-Xylene 205.0 1.130 01.310sec-Butylbenzene 205.0 0 0NDStyrene 205.0 0 0NDtert-Butylbenzene 205.0 0 0NDTetrachloroethene 205.0 0 0NDToluene 205.0 0 0NDtrans-1,2-Dichloroethene 205.0 0 0NDTrichloroethene 205.0 0 0NDTrichlorofluoromethane 205.0 0 0NDVinyl chloride 205.0 0 0ND Surr: 1,2-Dichloroethane-d4 50.00 105 70 130 20052.610 Surr: 4-Bromofluorobenzene 50.00 89.3 70 130 20044.630 Surr: Dibromofluoromethane 50.00 89.3 70 130 20044.660 Surr: Toluene-d8 50.00 94.2 70 130 20047.110



29 of 38






Sample ID: A100115LCS2


Prep Date:


Units: µg/L

PQL

Client ID: LCSW

RunNo: 117111

SeqNo: 1859551

LCSSampType: TestCode: 8260_WP

1,1-Dichloroethene 20.00 97.9 70 1305.0 019.580Benzene 40.00 93.8 70 1305.0 037.530Chlorobenzene 20.00 98.4 70 1305.0 019.680MTBE 20.00 107 70 1305.0 021.370Toluene 40.00 99.7 70 1305.0 039.870Trichloroethene 20.00 99.6 70 1305.0 019.920 Surr: 1,2-Dichloroethane-d4 25.00 100 70 13025.060 Surr: 4-Bromofluorobenzene 25.00 118 70 13029.540 Surr: Dibromofluoromethane 25.00 103 70 13025.750 Surr: Toluene-d8 25.00 107 70 13026.780

Sample ID: A100115MB4MS


Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 117111

SeqNo: 1859552

MSSampType: TestCode: 8260_WP

1,1-Dichloroethene 20.00 86.3 70 1305.0 017.260Benzene 40.00 90.1 70 1305.0 036.040Chlorobenzene 20.00 95.7 70 1305.0 019.130Toluene 40.00 94.7 70 1305.0 037.890Trichloroethene 20.00 92.8 70 1305.0 018.550 Surr: 1,2-Dichloroethane-d4 25.00 99.5 70 13024.880 Surr: 4-Bromofluorobenzene 25.00 116 70 13029.010 Surr: Dibromofluoromethane 25.00 104 70 13026.070 Surr: Toluene-d8 25.00 107 70 13026.690



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Sample ID: A100115MB4MSD


Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 117111

SeqNo: 1859553

MSDSampType: TestCode: 8260_WP

1,1-Dichloroethene 20.00 95.2 70 130 205.0 0 17.26 9.8119.040Benzene 40.00 93.2 70 130 205.0 0 36.04 3.3337.260Chlorobenzene 20.00 96.2 70 130 205.0 0 19.13 0.62519.250Toluene 40.00 98.1 70 130 205.0 0 37.89 3.5339.250Trichloroethene 20.00 99.1 70 130 205.0 0 18.55 6.6219.820 Surr: 1,2-Dichloroethane-d4 25.00 97.0 70 130 20024.250 Surr: 4-Bromofluorobenzene 25.00 113 70 130 20028.370 Surr: Dibromofluoromethane 25.00 102 70 130 20025.440 Surr: Toluene-d8 25.00 107 70 130 20026.670



Prep Date:


Units: µg/L

PQL

Client ID: PBW

RunNo: 117111

SeqNo: 1859554


1,1,1,2-Tetrachloroethane 5.0ND1,1,1-Trichloroethane 5.0ND1,1,2,2-Tetrachloroethane 5.0ND1,1,2-Trichloroethane 5.0ND1,1-Dichloroethane 5.0ND1,1-Dichloroethene 5.0ND1,1-Dichloropropene 5.0ND1,2,3-Trichlorobenzene 5.0ND1,2,3-Trichloropropane 5.0ND1,2,4-Trichlorobenzene 5.0ND1,2,4-Trimethylbenzene 5.0ND1,2-Dibromo-3-chloropropane 5.0ND1,2-Dibromoethane 5.0ND1,2-Dichlorobenzene 5.0ND1,2-Dichloroethane 5.0ND1,2-Dichloropropane 5.0ND



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Prep Date:


Units: µg/L

PQL

Client ID: PBW

RunNo: 117111

SeqNo: 1859554





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Prep Date:


Units: µg/L

PQL

Client ID: PBW

RunNo: 117111

SeqNo: 1859554


Naphthalene 5.0NDo-Xylene 5.0NDsec-Butylbenzene 5.0NDStyrene 5.0NDtert-Butylbenzene 5.0NDTetrachloroethene 5.0NDToluene 5.0NDtrans-1,2-Dichloroethene 5.0NDTrichloroethene 5.0NDTrichlorofluoromethane 5.0NDVinyl chloride 5.0ND Surr: 1,2-Dichloroethane-d4 25.00 93.4 70 13023.350 Surr: 4-Bromofluorobenzene 25.00 111 70 13027.670 Surr: Dibromofluoromethane 25.00 99.9 70 13024.980 Surr: Toluene-d8 25.00 104 70 13026.000



Prep Date:


Units: µg/L

PQL

Client ID: QCEB-02

RunNo: 117111

SeqNo: 1859556





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Prep Date:


Units: µg/L

PQL

Client ID: QCEB-02

RunNo: 117111

SeqNo: 1859556


1,2,4-Trimethylbenzene 205.0 0 0ND1,2-Dibromo-3-chloropropane 205.0 0 0ND1,2-Dibromoethane 205.0 0 0ND1,2-Dichlorobenzene 205.0 0 0ND1,2-Dichloroethane 205.0 0 0ND1,2-Dichloropropane 205.0 0 0ND1,3,5-Trimethylbenzene 205.0 0 0ND1,3-Dichlorobenzene 205.0 0 0ND1,3-Dichloropropane 205.0 0 0ND1,4-Dichlorobenzene 205.0 0 0ND2,2-Dichloropropane 205.0 0 0ND2-Butanone 2050 0 0ND2-Chloroethyl vinyl ether 205.0 0 0ND2-Chlorotoluene 205.0 0 0ND2-Hexanone 2050 0 0ND4-Chlorotoluene 205.0 0 0ND4-Isopropyltoluene 205.0 0 0ND4-Methyl-2-pentanone 2050 0 0NDAcetone 2050 0 0NDAcrolein 2050 0 0NDAcrylonitrile 2050 0 0NDBenzene 205.0 0 0NDBromobenzene 205.0 0 0NDBromochloromethane 205.0 0 0NDBromodichloromethane 205.0 0 0NDBromoform 205.0 0 0NDBromomethane 205.0 0 0NDCarbon disulfide 205.0 0 0NDCarbon tetrachloride 205.0 0 0NDChlorobenzene 205.0 0 0ND



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Prep Date:


Units: µg/L

PQL

Client ID: QCEB-02

RunNo: 117111

SeqNo: 1859556


Chloroethane 205.0 0 0NDChloroform 205.0 0 0NDChloromethane 205.0 0 0NDcis-1,2-Dichloroethene 205.0 0 0NDcis-1,3-Dichloropropene 205.0 0 0NDCyclohexanone 2050 0 0NDDi-isopropyl ether 205.0 0 0NDDibromochloromethane 205.0 0 0NDDibromomethane 205.0 0 0NDDichlorodifluoromethane 205.0 0 0NDEthyl Acetate 2050 0 0NDEthyl Ether 2050 0 0NDEthyl tert-butyl ether 205.0 0 0NDEthylbenzene 205.0 0 0NDFreon-113 205.0 0 0NDHexachlorobutadiene 205.0 0 0NDIodomethane 205.0 0 0NDIsopropylbenzene 205.0 0 0NDm,p-Xylene 2010 0 0NDMethylene chloride 205.0 0 0NDMTBE 205.0 0 0NDn-Butylbenzene 205.0 0 0NDn-Propylbenzene 205.0 0 0NDNaphthalene 205.0 0 0NDo-Xylene 205.0 0 0NDsec-Butylbenzene 205.0 0 0NDStyrene 205.0 0 0NDTert-amyl methyl ether 205.0 0 0NDTert-Butanol 20100 0 0NDtert-Butylbenzene 205.0 0 0ND



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Prep Date:


Units: µg/L

PQL

Client ID: QCEB-02

RunNo: 117111

SeqNo: 1859556


Tetrachloroethene 205.0 0 0NDToluene 205.0 0 0NDtrans-1,2-Dichloroethene 205.0 0 0NDtrans-1,3-Dichloropropene 205.0 0 0NDTrichloroethene 205.0 0 0NDTrichlorofluoromethane 205.0 0 0NDVinyl acetate 2050 0 0NDVinyl chloride 205.0 0 0NDXylenes, Total 2015 0 0ND Surr: 1,2-Dichloroethane-d4 25.00 99.3 70 130 20024.830 Surr: 4-Bromofluorobenzene 25.00 117 70 130 20029.220 Surr: Dibromofluoromethane 25.00 101 70 130 20025.310 Surr: Toluene-d8 25.00 106 70 130 20026.440



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Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 117113

SeqNo: 1859613


LUFT

DRO 1000 143 58 145 2010 0 1414 1.221431.580 Surr: p-Terphenyl 80.00 144 57 144 00114.930





Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 117113

SeqNo: 1859614


LUFT






Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 117113

SeqNo: 1859705


LUFT


Sample ID: MB-61185




Units: mg/Kg

PQL

Client ID: PBS

RunNo: 117113

SeqNo: 1859706


LUFT




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Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 117113

SeqNo: 1859710


LUFT

T/R Hydrocarbons: C8-C10 2010 0 0NDT/R Hydrocarbons: C10-C18 2010 0 0NDT/R Hydrocarbons: C18-C28 2010 0 0NDT/R Hydrocarbons: C28-C36 2010 0 0NDT/R Hydrocarbons: C36-C40 2010 0 0NDT/R Hydrocarbons: C8-C40 Total 2010 0 0ND Surr: p-Terphenyl 80.00 133 57 144 00106.400



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