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State of Kansas Department of Health and Environment CERTIFICATE This is to certify that Certification No.: E-10290 Microbac Laboratories, Inc-Ohio Valley Division 15 8 Starlite Drive Marietta, OH 45750 has been accredited in accordance with KS.A. 65-1,109a under the standards adopted in KA.R. 28-15-36for performing environmental analyses for the parameters listed on the most current scope of accreditation. Continuous accreditation depends on successful, ongoing participation in the program. Clients are urged to verify with this agency the laboratory's certification status for particular methods and analytes. Effective Date: 11 /1/2017 Secretary Department of Health and Environment Expiration Date: 10/ 31 /2018 Section C , ef Department of Health and

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State of Kansas Department of Health and Environment

CERTIFICATE This is to certify that Certification No.: E-10290

Microbac Laboratories, Inc-Ohio Valley Division

15 8 Starlite Drive Marietta, OH 45750

has been accredited in accordance with KS.A. 65-1,109a under the standards adopted in KA.R. 28-15-36for performing environmental analyses for the parameters listed on the most current scope of accreditation. Continuous accreditation depends on successful, ongoing participation in the program. Clients are urged to verify with this agency the laboratory's certification status for particular methods and analytes.

Effective Date: 11/1/2017

Secretary Department of Health and Environment

Expiration Date: 10/31/2018

Section C , ef Department of Health and

The Kansas Department of Health and Environment encourages all clients and data users to verify the most current scope of accreditation for certification number E-10290

The analytes tested and the corresponding matrix and method which a laboratory is authorized to perform at any given time will be those indicated in the most recently issued scope of accreditation. The most recent scope of accreditation supersedes all previously issued scopes of accreditation. It is the certified laboratory’s responsibility to review this document for any discrepancies. This scope of accreditation will be recalled in the event that your laboratory’s certification is revoked.

Accreditation Start: 2/13/2018 Accreditation End: 10/31/2018

Kansas Department of Health and Environment

Kansas Health and Environmental LaboratoriesEnvironmental Laboratory Improvement Program6810 SE Dwight Street Topeka, KS 66620-0001

phone (785) 296-3811fax (785) 559-5207

Jeff Anderson, Acting Secretary Jeff Colyer, M.D., Governor

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 1 of 23

CWA (Non Potable Water)Program/Matrix:

EPA 120.1Method

Conductivity FL

EPA 160.4Method

Residue-volatile FL

EPA 1664AMethod

Oil & Grease FL

EPA 180.1Method

Turbidity FL

EPA 200.7Method

Aluminum FLAntimony FLArsenic FLBarium FLBeryllium FLBoron FLCadmium FLCalcium FLChromium FLCobalt FLCopper FLHardness FLIron FLLead FLMagnesium FLManganese FLMolybdenum FLNickel FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 2 of 23

CWA (Non Potable Water)Program/Matrix:

Potassium FLSelenium FLSilica-dissolved FLSilver FLSodium FLThallium FLTin FLTitanium FLVanadium FLZinc FL

EPA 200.8Method

Antimony FLArsenic FLBarium FLCadmium FLChromium FLCobalt FLCopper FLLead FLManganese FLNickel FLSelenium FLSilver FLThallium FLVanadium FLZinc FL

EPA 245.1Method

Mercury FL

EPA 300.0Method

Bromide FLChloride FLFluoride FLNitrate FLNitrite FLSulfate FL

EPA 310.2Method

Alkalinity as CaCO3 FL

EPA 350.1Method

Ammonia as N FL

EPA 351.2Method

Kjeldahl Nitrogen (Total Kjeldahl Nitrogen-TKN) FL

EPA 353.2Method

Nitrate FLNitrate-nitrite FL

EPA 365.4Method

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 3 of 23

CWA (Non Potable Water)Program/Matrix:

Phosphorus FL

EPA 410.4Method

Chemical oxygen demand FL

EPA 420.1Method

Phenols (Petroleum) FL

EPA 6010Method

Arsenic FLCadmium FLChromium FLCopper FLLead FLMolybdenum FLNickel FLSelenium FLZinc FL

EPA 6020Method

Arsenic FLCadmium FLChromium FLCopper FLLead FLNickel FLSelenium FLZinc FL

EPA 608Method

4,4'-DDD FL4,4'-DDE FL4,4'-DDT FLAldrin FLalpha-BHC (alpha-Hexachlorocyclohexane) FLAroclor-1016 (PCB-1016) FLAroclor-1221 (PCB-1221) FLAroclor-1232 (PCB-1232) FLAroclor-1242 (PCB-1242) FLAroclor-1248 (PCB-1248) FLAroclor-1254 (PCB-1254) FLAroclor-1260 (PCB-1260) FLbeta-BHC (beta-Hexachlorocyclohexane) FLChlordane (tech.)(N.O.S.) FLdelta-BHC FLDieldrin FLEndosulfan I FLEndosulfan II FLEndosulfan sulfate FLEndrin FLEndrin aldehyde FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 4 of 23

CWA (Non Potable Water)Program/Matrix:

gamma-BHC (Lindane, gamma-HexachlorocyclohexanE) FLHeptachlor FLHeptachlor epoxide FLToxaphene (Chlorinated camphene) FL

EPA 624Method

1,1,1-Trichloroethane FL1,1,2,2-Tetrachloroethane FL1,1,2-Trichloroethane FL1,1-Dichloroethane FL1,1-Dichloroethylene FL1,2-Dichlorobenzene (o-Dichlorobenzene) FL1,2-Dichloroethane (Ethylene dichloride) FL1,2-Dichloropropane FL1,3-Dichlorobenzene FL1,4-Dichlorobenzene FL2-Chloroethyl vinyl ether FLAcrolein (Propenal) FLAcrylonitrile FLBenzene FLBromodichloromethane FLBromoform FLCarbon tetrachloride FLChlorobenzene FLChlorodibromomethane FLChloroethane (Ethyl chloride) FLChloroform FLcis-1,3-Dichloropropene FLEthylbenzene FLMethyl bromide (Bromomethane) FLMethyl chloride (Chloromethane) FLMethylene chloride (Dichloromethane) FLTetrachloroethylene (Perchloroethylene) FLToluene FLtrans-1,2-Dichloroethylene FLtrans-1,3-Dichloropropylene FLTrichloroethene (Trichloroethylene) FLTrichlorofluoromethane (Fluorotrichloromethane, Freon 11) FLVinyl chloride FL

EPA 625Method

1,2,4-Trichlorobenzene FL2,2'-Oxybis(1-chloropropane), bis(2-Chloro-1-methylethyl)ether FL2,4,6-Trichlorophenol FL2,4-Dichlorophenol FL2,4-Dimethylphenol FL2,4-Dinitrophenol FL2,4-Dinitrotoluene (2,4-DNT) FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 5 of 23

CWA (Non Potable Water)Program/Matrix:

2,6-Dinitrotoluene (2,6-DNT) FL2-Chloronaphthalene FL2-Chlorophenol FL2-Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol) FL2-Nitrophenol FL3,3'-Dichlorobenzidine FL4-Bromophenyl phenyl ether FL4-Chloro-3-methylphenol FL4-Chlorophenyl phenylether FL4-Nitrophenol FLAcenaphthene FLAcenaphthylene FLAnthracene FLBenzidine FLBenzo(a)anthracene FLBenzo(a)pyrene FLBenzo(b)fluoranthene FLBenzo(g,h,i)perylene FLBenzo(k)fluoranthene FLbis(2-Chloroethoxy)methane FLbis(2-Chloroethyl) ether FLButyl benzyl phthalate FLChrysene FLDi(2-ethylhexyl) phthalate (bis(2-Ethylhexyl)phthalate, DEHP) FLDibenz(a,h) anthracene FLDiethyl phthalate FLDimethyl phthalate FLDi-n-butyl phthalate FLDi-n-octyl phthalate FLFluoranthene FLFluorene FLHexachlorobenzene FLHexachlorobutadiene FLHexachlorocyclopentadiene FLHexachloroethane FLIndeno(1,2,3-cd) pyrene FLIsophorone FLNaphthalene FLNitrobenzene FLn-Nitrosodimethylamine FLn-Nitrosodi-n-propylamine FLn-Nitrosodiphenylamine FLPentachlorophenol FLPhenanthrene FLPhenol FLPyrene FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 6 of 23

CWA (Non Potable Water)Program/Matrix:

EPA 7470Method

Mercury FL

HACH 8000Method

Chemical oxygen demand FL

SM 2120 BMethod

Color FL

SM 2310 BMethod

Acidity, as CaCO3 FL

SM 2320 BMethod

Alkalinity as CaCO3 FL

SM 2340 C-1997Method

Hardness FL

SM 2510 BMethod

Conductivity FL

SM 2540 BMethod

Residue-total FL

SM 2540 CMethod

Residue-filterable (TDS) FL

SM 2540 DMethod

Residue-nonfilterable (TSS) FL

SM 2540 FMethod

Residue-settleable FL

SM 3500-Cr BMethod

Chromium VI FL

SM 4500-Cl EMethod

Chloride FL

SM 4500-CN¯ EMethod

Cyanide FL

SM 4500-CN¯ GMethod

Available Cyanide FL

SM 4500-F¯ CMethod

Fluoride FL

SM 4500-H+ BMethod

pH FL

SM 4500-NH3 GMethod

Ammonia as N FL

SM 4500-P E-1988Method

Orthophosphate as P FL

SM 4500-S2¯ FMethod

Sulfide FL

SM 5210 BMethod

Biochemical oxygen demand FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 7 of 23

CWA (Non Potable Water)Program/Matrix:

Carbonaceous BOD, CBOD FL

SM 5310 CMethod

Total organic carbon FL

SM 5540 CMethod

Surfactants - MBAS FL

TKN-NH3-CALMethod

Organic nitrogen FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 8 of 23

RCRA (Non Potable Water)Program/Matrix:

EPA 1010Method

Ignitability FL

EPA 6010Method

Aluminum FLAntimony FLArsenic FLBarium FLBeryllium FLBoron FLCadmium FLCalcium FLChromium FLCobalt FLCopper FLIron FLLead FLLithium FLMagnesium FLManganese FLMolybdenum FLNickel FLPhosphorus FLPotassium FLSelenium FLSilica as SiO2 FLSilver FLSodium FLStrontium FLThallium FLTin FLTitanium FLVanadium FLZinc FL

EPA 6020Method

Antimony FLArsenic FLBarium FLCadmium FLChromium FLCobalt FLCopper FLLead FLManganese FLNickel FLSelenium FLSilver FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 9 of 23

RCRA (Non Potable Water)Program/Matrix:

Thallium FLVanadium FLZinc FL

EPA 7196Method

Chromium VI FL

EPA 7470Method

Mercury FL

EPA 8011Method

1,2-Dibromo-3-chloropropane (DBCP) FL1,2-Dibromoethane (EDB, Ethylene dibromide) FL

EPA 8015Method

Diesel range organics (DRO) FLEthanol FLEthylene glycol FLGasoline range organics (GRO) FLIsopropyl alcohol (2-Propanol, Isopropanol) FLMethanol FL

EPA 8081Method

4,4'-DDD FL4,4'-DDE FL4,4'-DDT FLAldrin FLalpha-BHC (alpha-Hexachlorocyclohexane) FLalpha-Chlordane, cis-Chlordane FLbeta-BHC (beta-Hexachlorocyclohexane) FLChlordane (tech.)(N.O.S.) FLdelta-BHC FLDieldrin FLEndosulfan I FLEndosulfan II FLEndosulfan sulfate FLEndrin FLEndrin aldehyde FLEndrin ketone FLgamma-BHC (Lindane, gamma-HexachlorocyclohexanE) FLgamma-Chlordane FLHeptachlor FLHeptachlor epoxide FLMethoxychlor FLToxaphene (Chlorinated camphene) FL

EPA 8082Method

Aroclor-1016 (PCB-1016) FLAroclor-1221 (PCB-1221) FLAroclor-1232 (PCB-1232) FLAroclor-1242 (PCB-1242) FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 10 of 23

RCRA (Non Potable Water)Program/Matrix:

Aroclor-1248 (PCB-1248) FLAroclor-1254 (PCB-1254) FLAroclor-1260 (PCB-1260) FL

EPA 8151Method

2,4,5-T FL2,4-D FL2,4-DB FLDalapon FLDicamba FLDichloroprop (Dichlorprop) FLDinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP) FLMCPA FLMCPP FLPentachlorophenol FLSilvex (2,4,5-TP) FL

EPA 8260Method

1,1,1,2-Tetrachloroethane FL1,1,1-Trichloroethane FL1,1,2,2-Tetrachloroethane FL1,1,2-Trichloroethane FL1,1-Dichloroethane FL1,1-Dichloroethylene FL1,1-Dichloropropene FL1,2,3-Trichlorobenzene FL1,2,3-Trichloropropane FL1,2,4-Trichlorobenzene FL1,2,4-Trimethylbenzene FL1,2-Dibromo-3-chloropropane (DBCP) FL1,2-Dibromoethane (EDB, Ethylene dibromide) FL1,2-Dichlorobenzene (o-Dichlorobenzene) FL1,2-Dichloroethane (Ethylene dichloride) FL1,2-Dichloropropane FL1,3,5-Trimethylbenzene FL1,3-Dichlorobenzene FL1,3-Dichloropropane FL1,4-Dichlorobenzene FL1,4-Dioxane (1,4- Diethyleneoxide) FL1-Chlorohexane FL2,2-Dichloropropane FL2-Butanone (Methyl ethyl ketone, MEK) FL2-Chloroethyl vinyl ether FL2-Chlorotoluene FL2-Hexanone FL2-Nitropropane FL4-Chlorotoluene FL4-Isopropyltoluene (p-Cymene,p-Isopropyltoluene) FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 11 of 23

RCRA (Non Potable Water)Program/Matrix:

4-Methyl-2-pentanone (MIBK) FLAcetone FLAcetonitrile FLAcrolein (Propenal) FLAcrylonitrile FLAllyl chloride (3-Chloropropene) FLBenzene FLBromobenzene FLBromochloromethane FLBromodichloromethane FLBromoform FLCarbon disulfide FLCarbon tetrachloride FLChlorobenzene FLChlorodibromomethane FLChloroethane (Ethyl chloride) FLChloroform FLChloroprene (2-Chloro-1,3-butadiene) FLcis-1,2-Dichloroethylene FLcis-1,3-Dichloropropene FLDibromomethane (Methylene bromide) FLDichlorodifluoromethane (Freon-12) FLDiethyl ether FLEthyl acetate FLEthyl methacrylate FLEthylbenzene FLHexachlorobutadiene FLIodomethane (Methyl iodide) FLIsobutyl alcohol (2-Methyl-1-propanol) FLIsopropylbenzene FLMethacrylonitrile FLMethyl bromide (Bromomethane) FLMethyl chloride (Chloromethane) FLMethyl methacrylate FLMethyl tert-butyl ether (MTBE) FLMethylene chloride (Dichloromethane) FLm-Xylene FLNaphthalene FLn-Butyl alcohol (1-Butanol, n-Butanol) FLn-Butylbenzene FLn-Propylbenzene FLo-Xylene FLPropionitrile (Ethyl cyanide) FLp-Xylene FLsec-Butylbenzene FLStyrene FLtert-Butyl alcohol FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 12 of 23

RCRA (Non Potable Water)Program/Matrix:

tert-Butylbenzene FLTetrachloroethylene (Perchloroethylene) FLToluene FLtrans-1,2-Dichloroethylene FLtrans-1,3-Dichloropropylene FLtrans-1,4-Dichloro-2-butene FLTrichloroethene (Trichloroethylene) FLTrichlorofluoromethane (Fluorotrichloromethane, Freon 11) FLVinyl acetate FLVinyl chloride FL

EPA 8270Method

1,2,4,5-Tetrachlorobenzene FL1,2,4-Trichlorobenzene FL1,2-Dichlorobenzene (o-Dichlorobenzene) FL1,2-Diphenylhydrazine FL1,3,5-Trinitrobenzene (1,3,5-TNB) FL1,3-Dichlorobenzene FL1,3-Dinitrobenzene (1,3-DNB) FL1,4-Dichlorobenzene FL1,4-Naphthoquinone FL1,4-Phenylenediamine FL1-Naphthylamine FL2,3,4,6-Tetrachlorophenol FL2,4,5-Trichlorophenol FL2,4,6-Trichlorophenol FL2,4-Dichlorophenol FL2,4-Dimethylphenol FL2,4-Dinitrophenol FL2,4-Dinitrotoluene (2,4-DNT) FL2,6-Dichlorophenol FL2,6-Dinitrotoluene (2,6-DNT) FL2-Acetylaminofluorene FL2-Chloronaphthalene FL2-Chlorophenol FL2-Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol) FL2-Methylaniline (o-Toluidine) FL2-Methylnaphthalene FL2-Methylphenol (o-Cresol) FL2-Naphthylamine FL2-Nitroaniline FL2-Nitrophenol FL2-Picoline (2-Methylpyridine) FL3,3'-Dichlorobenzidine FL3,3'-Dimethylbenzidine FL3-Methylcholanthrene FL3-Methylphenol (m-Cresol) FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 13 of 23

RCRA (Non Potable Water)Program/Matrix:

3-Nitroaniline FL4-Aminobiphenyl FL4-Bromophenyl phenyl ether FL4-Chloro-3-methylphenol FL4-Chloroaniline FL4-Chlorophenyl phenylether FL4-Methylphenol (p-Cresol) FL4-Nitroaniline FL4-Nitrophenol FL4-Nitroquinoline 1-oxide FL5-Nitro-o-toluidine FL7,12-Dimethylbenz(a) anthracene FLa-a-Dimethylphenethylamine FLAcenaphthene FLAcenaphthylene FLAcetophenone FLAniline FLAnthracene FLAramite FLBenzidine FLBenzo(a)anthracene FLBenzo(a)pyrene FLBenzo(b)fluoranthene FLBenzo(g,h,i)perylene FLBenzo(k)fluoranthene FLBenzoic acid FLBenzyl alcohol FLbis(2-Chloroethoxy)methane FLbis(2-Chloroethyl) ether FLButyl benzyl phthalate FLChlorobenzilate FLChrysene FLDi(2-ethylhexyl) phthalate (bis(2-Ethylhexyl)phthalate, DEHP) FLDiallate FLDibenz(a,h) anthracene FLDibenzofuran FLDiethyl phthalate FLDimethoate FLDimethyl phthalate FLDi-n-butyl phthalate FLDi-n-octyl phthalate FLDinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP) FLDiphenylamine FLDisulfoton FLEthyl methanesulfonate FLFamphur FLFluoranthene FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 14 of 23

RCRA (Non Potable Water)Program/Matrix:

Fluorene FLHexachlorobenzene FLHexachlorobutadiene FLHexachlorocyclopentadiene FLHexachloroethane FLHexachlorophene FLHexachloropropene FLHexamethylphosphoramide (HMPA) FLIndeno(1,2,3-cd) pyrene FLIsodrin FLIsophorone FLIsosafrole FLKepone FLMalathion FLMethapyrilene FLMethyl methanesulfonate FLMethyl parathion (Parathion, methyl) FLNaphthalene FLNitrobenzene FLn-Nitrosodiethylamine FLn-Nitrosodimethylamine FLn-Nitroso-di-n-butylamine FLn-Nitrosodi-n-propylamine FLn-Nitrosodiphenylamine FLn-Nitrosomethylethalamine FLn-Nitrosomorpholine FLn-Nitrosopiperidine FLn-Nitrosopyrrolidine FLo,o,o-Triethyl phosphorothioate FLParathion, ethyl FLPentachlorobenzene FLPentachloronitrobenzene FLPentachlorophenol FLPhenacetin FLPhenanthrene FLPhenol FLPhorate FLPronamide (Kerb) FLPyrene FLPyridine FLSafrole FLSulfotep (Tetraethyl dithiopyrophosphate) FLTetrachlorvinphos (Stirophos, Gardona) Mixed isomers FLThionazin (Zinophos) FL

EPA 8315Method

Formaldehyde FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 15 of 23

RCRA (Non Potable Water)Program/Matrix:

EPA 8330Method

1,3,5-Trinitrobenzene (1,3,5-TNB) FL1,3-Dinitrobenzene (1,3-DNB) FL2,4,6-Trinitrotoluene (2,4,6-TNT) FL2,4-Dinitrotoluene (2,4-DNT) FL2,6-Dinitrotoluene (2,6-DNT) FL2-Amino-4,6-dinitrotoluene (2-am-dnt) FL2-Nitrotoluene FL3-Nitrotoluene FL4-Amino-2,6-dinitrotoluene (4-am-dnt) FL4-Nitrotoluene FLMethyl-2,4,6-trinitrophenylnitramine (tetryl) FLNitrobenzene FLOctahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX) FLRDX (hexahydro-1,3,5-trinitro-1,3,5-triazine) FL

EPA 9010Method

Amenable cyanide FLCyanide FL

EPA 9056Method

Bromide FLChloride FLFluoride FLNitrate FLNitrite FLSulfate FL

EPA 9060Method

Total organic carbon FL

KS LRH GC-FIDMethod

Total Petroleum Hydrocarbons C5 - C8 KS

KS MRH/HRH GC-FIDMethod

Total Petroleum Hydrocarbons C19 - C35 KSTotal Petroleum Hydrocarbons C9 - C18 KS

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 16 of 23

RCRA (Solid & Hazardous Material)Program/Matrix:

EPA 1010Method

Ignitability FL

EPA 1311Method

Toxicity Characteristic Leaching Procedure (TCLP) FL

EPA 1312 Synthetic Precipitation Leaching ProcedureMethod

Synthetic Precipitation Leaching Procedure (SCLP) FL

EPA 6010Method

Aluminum FLAntimony FLArsenic FLBarium FLBeryllium FLBoron FLCadmium FLCalcium FLChromium FLCobalt FLCopper FLIron FLLead FLLithium FLMagnesium FLManganese FLMolybdenum FLNickel FLPhosphorus FLPotassium FLSelenium FLSilver FLSodium FLStrontium FLThallium FLTin FLTitanium FLVanadium FLZinc FL

EPA 6020Method

Antimony FLArsenic FLBarium FLCadmium FLChromium FLCobalt FLCopper FLLead FLManganese FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 17 of 23

RCRA (Solid & Hazardous Material)Program/Matrix:

Nickel FLSelenium FLSilver FLThallium FLVanadium FLZinc FL

EPA 7196Method

Chromium VI FL

EPA 7471Method

Mercury FL

EPA 8015Method

Diesel range organics (DRO) FLEthanol FLEthylene glycol FLGasoline range organics (GRO) FLIsopropyl alcohol (2-Propanol, Isopropanol) FLMethanol FL

EPA 8081Method

4,4'-DDD FL4,4'-DDE FL4,4'-DDT FLAldrin FLalpha-BHC (alpha-Hexachlorocyclohexane) FLalpha-Chlordane, cis-Chlordane FLbeta-BHC (beta-Hexachlorocyclohexane) FLChlordane (tech.)(N.O.S.) FLdelta-BHC FLDieldrin FLEndosulfan I FLEndosulfan II FLEndosulfan sulfate FLEndrin FLEndrin aldehyde FLEndrin ketone FLgamma-BHC (Lindane, gamma-HexachlorocyclohexanE) FLgamma-Chlordane FLHeptachlor FLHeptachlor epoxide FLMethoxychlor FLToxaphene (Chlorinated camphene) FL

EPA 8082Method

Aroclor-1016 (PCB-1016) FLAroclor-1221 (PCB-1221) FLAroclor-1232 (PCB-1232) FLAroclor-1242 (PCB-1242) FLAroclor-1248 (PCB-1248) FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 18 of 23

RCRA (Solid & Hazardous Material)Program/Matrix:

Aroclor-1254 (PCB-1254) FLAroclor-1260 (PCB-1260) FL

EPA 8151Method

2,4,5-T FL2,4-D FL2,4-DB FLDalapon FLDicamba FLDichloroprop (Dichlorprop) FLDinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP) FLMCPA FLMCPP FLPentachlorophenol FLSilvex (2,4,5-TP) FL

EPA 8260Method

1,1,1,2-Tetrachloroethane FL1,1,1-Trichloroethane FL1,1,2,2-Tetrachloroethane FL1,1,2-Trichloroethane FL1,1-Dichloroethane FL1,1-Dichloroethylene FL1,1-Dichloropropene FL1,2,3-Trichlorobenzene FL1,2,3-Trichloropropane FL1,2,4-Trichlorobenzene FL1,2,4-Trimethylbenzene FL1,2-Dibromo-3-chloropropane (DBCP) FL1,2-Dibromoethane (EDB, Ethylene dibromide) FL1,2-Dichlorobenzene (o-Dichlorobenzene) FL1,2-Dichloroethane (Ethylene dichloride) FL1,2-Dichloropropane FL1,3,5-Trimethylbenzene FL1,3-Dichlorobenzene FL1,3-Dichloropropane FL1,4-Dichlorobenzene FL1,4-Dioxane (1,4- Diethyleneoxide) FL1-Chlorohexane FL2,2-Dichloropropane FL2-Butanone (Methyl ethyl ketone, MEK) FL2-Chloroethyl vinyl ether FL2-Chlorotoluene FL2-Hexanone FL2-Nitropropane FL4-Chlorotoluene FL4-Isopropyltoluene (p-Cymene,p-Isopropyltoluene) FL4-Methyl-2-pentanone (MIBK) FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 19 of 23

RCRA (Solid & Hazardous Material)Program/Matrix:

Acetone FLAcetonitrile FLAcrolein (Propenal) FLAcrylonitrile FLAllyl chloride (3-Chloropropene) FLBenzene FLBromobenzene FLBromochloromethane FLBromodichloromethane FLBromoform FLCarbon disulfide FLCarbon tetrachloride FLChlorobenzene FLChlorodibromomethane FLChloroethane (Ethyl chloride) FLChloroform FLChloroprene (2-Chloro-1,3-butadiene) FLcis-1,2-Dichloroethylene FLcis-1,3-Dichloropropene FLDibromomethane (Methylene bromide) FLDichlorodifluoromethane (Freon-12) FLDiethyl ether FLEthyl acetate FLEthyl methacrylate FLEthylbenzene FLHexachlorobutadiene FLIodomethane (Methyl iodide) FLIsobutyl alcohol (2-Methyl-1-propanol) FLIsopropylbenzene FLMethacrylonitrile FLMethyl bromide (Bromomethane) FLMethyl chloride (Chloromethane) FLMethyl methacrylate FLMethyl tert-butyl ether (MTBE) FLMethylene chloride (Dichloromethane) FLm-Xylene FLNaphthalene FLn-Butyl alcohol (1-Butanol, n-Butanol) FLn-Butylbenzene FLn-Propylbenzene FLo-Xylene FLPropionitrile (Ethyl cyanide) FLp-Xylene FLsec-Butylbenzene FLStyrene FLtert-Butyl alcohol FLtert-Butylbenzene FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 20 of 23

RCRA (Solid & Hazardous Material)Program/Matrix:

Tetrachloroethylene (Perchloroethylene) FLToluene FLtrans-1,2-Dichloroethylene FLtrans-1,3-Dichloropropylene FLtrans-1,4-Dichloro-2-butene FLTrichloroethene (Trichloroethylene) FLTrichlorofluoromethane (Fluorotrichloromethane, Freon 11) FLVinyl acetate FLVinyl chloride FL

EPA 8270Method

1,2,4,5-Tetrachlorobenzene FL1,2,4-Trichlorobenzene FL1,2-Dichlorobenzene (o-Dichlorobenzene) FL1,2-Diphenylhydrazine FL1,3,5-Trinitrobenzene (1,3,5-TNB) FL1,3-Dichlorobenzene FL1,3-Dinitrobenzene (1,3-DNB) FL1,4-Dichlorobenzene FL1,4-Naphthoquinone FL1,4-Phenylenediamine FL1-Naphthylamine FL2,3,4,6-Tetrachlorophenol FL2,4,5-Trichlorophenol FL2,4,6-Trichlorophenol FL2,4-Dichlorophenol FL2,4-Dimethylphenol FL2,4-Dinitrophenol FL2,4-Dinitrotoluene (2,4-DNT) FL2,6-Dichlorophenol FL2,6-Dinitrotoluene (2,6-DNT) FL2-Acetylaminofluorene FL2-Chloronaphthalene FL2-Chlorophenol FL2-Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol) FL2-Methylaniline (o-Toluidine) FL2-Methylnaphthalene FL2-Methylphenol (o-Cresol) FL2-Naphthylamine FL2-Nitroaniline FL2-Nitrophenol FL2-Picoline (2-Methylpyridine) FL3,3'-Dichlorobenzidine FL3,3'-Dimethylbenzidine FL3-Methylcholanthrene FL3-Methylphenol (m-Cresol) FL3-Nitroaniline FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 21 of 23

RCRA (Solid & Hazardous Material)Program/Matrix:

4-Aminobiphenyl FL4-Bromophenyl phenyl ether FL4-Chloro-3-methylphenol FL4-Chloroaniline FL4-Chlorophenyl phenylether FL4-Methylphenol (p-Cresol) FL4-Nitroaniline FL4-Nitrophenol FL4-Nitroquinoline 1-oxide FL5-Nitro-o-toluidine FL7,12-Dimethylbenz(a) anthracene FLa-a-Dimethylphenethylamine FLAcenaphthene FLAcenaphthylene FLAcetophenone FLAniline FLAnthracene FLAramite FLBenzidine FLBenzo(a)anthracene FLBenzo(a)pyrene FLBenzo(b)fluoranthene FLBenzo(g,h,i)perylene FLBenzo(k)fluoranthene FLBenzoic acid FLBenzyl alcohol FLbis(2-Chloroethoxy)methane FLbis(2-Chloroethyl) ether FLButyl benzyl phthalate FLChlorobenzilate FLChrysene FLDi(2-ethylhexyl) phthalate (bis(2-Ethylhexyl)phthalate, DEHP) FLDiallate FLDibenz(a,h) anthracene FLDibenzofuran FLDiethyl phthalate FLDimethoate FLDimethyl phthalate FLDi-n-butyl phthalate FLDi-n-octyl phthalate FLDinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP) FLDiphenylamine FLDisulfoton FLEthyl methanesulfonate FLFamphur FLFluoranthene FLFluorene FL

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 22 of 23

RCRA (Solid & Hazardous Material)Program/Matrix:

Hexachlorobenzene FLHexachlorobutadiene FLHexachlorocyclopentadiene FLHexachloroethane FLHexachlorophene FLHexachloropropene FLHexamethylphosphoramide (HMPA) FLIndeno(1,2,3-cd) pyrene FLIsodrin FLIsophorone FLIsosafrole FLKepone FLMalathion FLMethapyrilene FLMethyl methanesulfonate FLMethyl parathion (Parathion, methyl) FLNaphthalene FLNitrobenzene FLn-Nitrosodiethylamine FLn-Nitrosodimethylamine FLn-Nitroso-di-n-butylamine FLn-Nitrosodi-n-propylamine FLn-Nitrosodiphenylamine FLn-Nitrosomethylethalamine FLn-Nitrosomorpholine FLn-Nitrosopiperidine FLn-Nitrosopyrrolidine FLo,o,o-Triethyl phosphorothioate FLParathion, ethyl FLPentachlorobenzene FLPentachloronitrobenzene FLPentachlorophenol FLPhenacetin FLPhenanthrene FLPhenol FLPhorate FLPronamide (Kerb) FLPyrene FLPyridine FLSafrole FLSulfotep (Tetraethyl dithiopyrophosphate) FLTetrachlorvinphos (Stirophos, Gardona) Mixed isomers FLThionazin (Zinophos) FL

EPA 8315Method

Formaldehyde FL

EPA 8330Method

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/

EPA Number: OH00218

Microbac Laboratories, Inc - Ohio Valley Division

Scope of Accreditation for Certification Number: E-10290

Primary AB

Page 23 of 23

RCRA (Solid & Hazardous Material)Program/Matrix:

1,3,5-Trinitrobenzene (1,3,5-TNB) FL1,3-Dinitrobenzene (1,3-DNB) FL2,4,6-Trinitrotoluene (2,4,6-TNT) FL2,4-Dinitrotoluene (2,4-DNT) FL2,6-Dinitrotoluene (2,6-DNT) FL2-Amino-4,6-dinitrotoluene (2-am-dnt) FL2-Nitrotoluene FL3-Nitrotoluene FL4-Amino-2,6-dinitrotoluene (4-am-dnt) FL4-Nitrotoluene FLMethyl-2,4,6-trinitrophenylnitramine (tetryl) FLNitrobenzene FLOctahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX) FLRDX (hexahydro-1,3,5-trinitro-1,3,5-triazine) FL

EPA 9010Method

Cyanide FL

EPA 9014Method

Cyanide FL

EPA 9030Method

Sulfide FL

EPA 9034Method

Sulfide FL

EPA 9040Method

pH FL

EPA 9045Method

pH FL

EPA 9056Method

Bromide FLChloride FLFluoride FLNitrate FLNitrite FLSulfate FL

EPA 9071Method

Oil & Grease FL

EPA 9095Method

Paint Filter Test FL

KS LRH GC-FIDMethod

Total Petroleum Hydrocarbons C5 - C8 KS

KS MRH/HRH GC-FIDMethod

Total Petroleum Hydrocarbons C19 - C35 KSTotal Petroleum Hydrocarbons C9 - C18 KS

End of Scope of Accreditation

6810 SE Dwight Street • Topeka, KS 66620-0001 • phone (785) 296-3611 • fax (785) 559-5207 www.kdheks.gov/envlab/