summary report consultants, inc. volume 2 of 2

URSQuality ControlSummary Report CONSULTANTS, INC.

VOLUME 2 OF 2

Pre-design InvestigationDelaware Sand And GravelSuperfund Site (Phase II)

New Castle, Delaware

Prepared for:U.S. Army Corps of Engineers

Omaha DistrictOmaha, Nebraska

Contract No. DACW 45-89-C-0518

Acting for:U.S. Environmental Protection Agency

Region IIIPhiladelphia, Pennsylvania

Prepared by:URS Consultants, Inc.

Buffalo, New York

March 1993

A-E

VOLUME 2

A-E QUALITY CONTROL SUMMARY REPORT

TABLE OF CONTENTSPage No

1.0 SCOPE OF PROJECT .................................... 1

2.0 PROJECT DESCRIPTION ................................. 1

3.0 SAMPLING PROCEDURES ................................. 1

4.0 SUMMARY OF A-E DAILY QUALITY CONTROL REPORTS ........ 1

5.0 ANALYTICAL PARAMETERS ............................... 2

6.0 DATA PRESENTATION ................................... 36.1 Analytical Data Format ........................ 36.2 Data Qualifier Definitions .................... 46.3 Air Monitoring Data Presentation .............. 5

7.0 QUALITY CONTROL ACTIVITIES .......................... 6

7.1 Presentation of Field Screening LaboratoryAnalytical Results ............................ 6

7.2 Presentation of Laboratory Analytical Results . 67.3 Analytical Data Assessment .................... 6

7.3.1 Completeness ............................ 77.3.2 Data Assessment Summary ................. 8

8.0 CONCLUSIONS .......................................... 9

f l R I O I 3 8 5

LIST OF TABLES

FollowingTables Page No.5-1A - 5-1G Required Analysis - Schedule A-G ........ 26-1 Organic Samples - Data Qualifiers ....... 46-2 Inorganic Samples * Data Qualifiers ..... 47-1 - 7-11 Analytical Data Assessment Summaries .... 97-12 Analytical Completeness ................. 9

LIST OF APPENDICES

Volume NumberA Daily Quality Control Reports ................. 15 Field Investigations Analytical Results ....... 1&2C Stage 1 Onsite Lab Screening and Onsite Lab

Compatibility Testing Results ................. 2D Stage 2 Onsite Composite Testing Results ...... 2

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AR 1011*1*2

QUALITY CONTROL DATA

AR 10

. TABLE B-l

SAMPLE DELIVERY GROUPS (SDG)

SDG #*

3193

3210/3215

3238

3338

3368

3385

3471

3491

3505

Sample ID

SDD-2, SDD-3, TP-1-1, TP-2-1,UR-1, UR-2, UR-3, UR-4, UR-6and UR-7

SDR-1, SDR-2, TP-3-1, TP-3-2,TP-3-3, TP-4-1, Tp-4-2, TP-4-3, UR-5. UR-8 through UR-21,and UR-23

SDD-1, SDD-5, SDR-3, TP-2-2,TP-5-1, TP-5-2, TP-6-1, TP-6-2, UR-22, and UR-24 throughUR-46

UD-18-10, U0-1B-11, UD-18-12,UD-23-10, and UD-23-12

UD-6-10, UD-6-11, UD-6-12,UB-21-11, UD-21-12, and UD-21-13

UD-16A-9, UD-16A-10, UD-16A-11, UD-17-9, UD-17-10, UD-17-11, UD-19-8, UD-19-10, UD-19-13, UD-30-10, UD-30-12, andUD-30-13

UD-7-10^ UD-7-11, UD-7-12,UD-11A-11, UD-11A-12, UD-11A-13, UD-26-8, UD-26-9, UD-26-10, UD-26-10B, UD-27-9, UD-27-10, and UD-27-15

UD-14-8, UD-14-9, UD-14-10,UD-28-8, UD-28-9, and UD-28-10

UB-13-8, UD-13-10, UD-13-11,UD-20-10, UD-20-11, and UD-20-12

Associated QC Sample ID **

UR-2 Field Dup.

UR-9 Field Dup., UR-11-MS/MSD, UR-18-MS/MSD, and UR-23 Field Dup.

TP-6-1 Field Dup., TP-6-2-MS/MSD, UR-27 Field Dup., UR-29-MS/MSD, UR-36-MS/MSD, UR-43 Field Dup. , and UR-44-MS/MSD

None

None

None

UD_7_10-MS/MSD, UD-7-11 FieldDup., UD-7-12-MS/MSD, UD-11A-11 Field Dup., UD-11A-12-MS/MSD, UD-11A-13 Field Dup.,UD-26-8 Field Dup., UD-26-9-MS/MSD, UD-26-10 Field Dup.,UD-26-10B-MS/MSD, UD-27-9Field Dup., UD-27-10-MS/MSD,and UD-27-15

UD-14-8 Field Dup., UD-14-9-MS/MSD, UD-14-10 Field Dup.,UD-28-8-MS/MSD, UD-28-9 FieldDup., and UD-28-10-MS/MSD

None

TABI3; B-l (Continued)

SDG #*

3520

3615

3616

3617

3620

3676/3677

3678

4875

5013/5345

5014

5037/5345

12728

11913/12583

Sample ID

UD-2-8, UD-2-9, UD-2-12, UD-5-7, UD-5-11, and UD- 5 -12

UD-3-10, UD-3-13, UD-3-14,UD-4-10, UD-4-12, and UD-4-16-

DW-1 -

GT-1 through GT-24

UD-9-8, UD-9-9, UD-15A-6, UD-15A-8, UD-25-9, and UD- 25 -10

DC-1, DC-2, DW-2

BC -5-1 through BC-5-6. BC-6-1through BC-6-6, BC-7-1through BC-7-6, BC-8-1through BC-8-6, BC-9-1, BC-9-2, BC-10-1, and BC-10-2

TR-2

TTC-1

TBR-1 (14'), TBR-1 (241),TBR-1 -(34'), TBR-3 (13'),TBR-3 (23') and TBR-3 (33')

TBC-1

(TBC and TTC) -1/1200/15,-1/1200/30, -1/1200/45,-1/1500/15, -1/1500/30,-1/1500/45, -1/1800/15,-1/1800/30, -1/1800/45

Air Monitoring Samples (Stage1 and 2)

Associated QC Sample ID **

None

None

DW-1 Dup., RB-1 and TB-1

Not Applicable

None

DC-1-MS/MSD

BD-5-2 Dup., BC-6-1-MS/MSD,BC-6-3 Dup., BC-6-4-MS/MSD,BC-7-2-MS/MSD, and BC-7-3Dup.

None

TTC-1 Dup., TTC-1-MS/MSD

None

TBC-1 Dup., TBC-1-MS/MSD

6 Samples sent to USACE asDuplicates

None

NOTES:

* Corresponds to laboratory report numbers.** URS deignated QC (lab QC not .included on Table A-l but located within

associated data packages).

3BSOIL VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLlCAfE RECOVERY

Lab Names SHL-TUL5A____________• Contract: URS_______

Lab Code: STOK Case No.: URS SAS No.: ____' SDG No-:. T p -<* - .1

3p,Ue^- EPA Sample No.: fT a jT _____ Level:<low/med) MED''"

COMPOUND

1 . 1-Dichloroetheng* ricnloroethene&«nsen«TolueneChlorobenrene

SPIKEADDEDCug/Kg)

9330933093309 /=: 30 -933O

SAMPLECONCENTRATION

.(ug/Kg)

O0

28201570

0

MSCONCENTRATION

_ <ug/Kg)

114008940

1 2300129OO9980

MS*••',

REC 4*

122=?61021211U7

QCLIMITSREC.

59-17262-13766-14259-13960-J33

i

COMPOUND

1 „ i-DichloroetheneTrichloroethenet-en^eneTcluonv

, Chlorobenzene

SPIKEADDED(ug/Kg)

9330933093309330937.0

MSDCONCENTRATION

<ug/Kg )

1130088801270O12700 -10100

MSDV.REC #

12195106119108

7.RPD #

i1

-42

-1 "

QC LIMITS jRPD ! REC.

22 ! 59- 17224 ! 62-13721 ! be— 14221 159 -13.?21 ! 60 -133

!

t Column to bm used to -flag recovery and RPD values with an asterisk

* "alues outside o-f QC limits

PFD: _g. out o-f _5. outside limitsSoil 9 Recovgrv: 0 out o-f 10 outside limits

COMMENTS: URS TP-6-1INST:D

FORM I 11 VOA-2 *• mm.

3DSOIL SEMWQLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

_sb Name: 3WL-TULSA Contract: URS

_ab Code: SWOK Case No.: URS SAS No-: SDG No.:

latrix Spike - EPA Sample

COMPOUND

Phenol2-Chlorobhenol1 ,4-DichlorabenzeneN-Nitroso-di-n-prop. ( 1 )1 ,2.4-Trichlorobenzene_4-C h 1 ara-3-me thy 1 phenolAcenacjhthene4~Nitrophenol2 . 4-Dinitrotoluene ____Psn tac h 1 or o phenolPvrene

No.: TP-6-2 Level :( low/med ) LOW

SPIKEADDED(ug/Kg )

17100171 OO854085403540

17100 . .S540171 008540

1 7 1 003540

SAMPLECONCENTRATION

(ug/Kg")

0o~00OO0- - - £-0£)Q

MSCONCENTRATION

(ug/Kg)

126001 3400726072107470146006330137007510

17100 . .93 10

MS"•

REC tt

7478•55S4878530 .SO38 '1 0 010

DCLIMITS

REC.

"A Q ("I

25-l'i223 "In441 12633 lf>726 1' '3- 1 1 _• /11-11419- 3?

- 17-10975-142

COMPOUND

Phenol2~ChloraDhenol1 , 4-DichloraberireneN-Nitroso-di-n-prop. ( 1 )1 ,2?4™Trichlorobenzene_4 -Chloro-3-methyl phenolAcenaphthene4-Nitro phenol2 ,,4-Dinitro toluene ____Pen tachloro phenolPvrene

SPIKEADDED(ug/Kg)

17100171003540B540B540

171OO8540

171008540

171008540

MSDCONCENTRATION

C ug/Kg)

1210O125006B3O66207210145006490 .143006450167OOS92O

MSD•//•REC #

7173BO7984B576847698104

'/.RPD #

A-nr

"6740e."

_='w/

15i5

QC LIMITSRPD : FEC.

50~ ~7*_ /—— Q_-o

1950474736

26- 9025-1022B 10441 12633 10726 10331-1371 1-1 142B- '3917-1 0935-142

(1) N-Nitroso-di-n-propylamine

tt Column to be used to -flag recovery and RPD values with an asterisk* Values outside o-f QC limits

RPD: _0 out of 11_ outside limitsSpike Recovery: _0 : out 'o-f 22 outside limits

COMMENTS: TP-6-2 . URSINSTsF SWLtt323S.37

6-00037:,'FORM: III SV-2 ' i/87 Rev

A R I O U U 7

3FSOIL PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Names SWL-TULSA______________ Contract: URS_______

Lab Codes SUJOK Case No.: URS SAS No.: ______ SDG No.s

Matrix Spike - EPA Sample No.: TP-6-2_____ Level:<low/med) LQUI

COMPOUNDsssaa5ESe= a ^ ^ ^ s:»z2 e s

g»mma-BHC (Lindane) ___HeotachlorAldrinDieldrinEndrin4,4'-DDT

.

SPIKEADDED< ug/Kg)

68.268.2AQ *?OO m 1

170170170

SAMPLECONCENTRATION

(ug/Kg)

000000

MSCONCENTRATION

( ug/Kg >==SKassMta:x:aESS£

000000 • .

MS7.

REC #

0 *0 *0 *0 *0 *0 *

QCLIMITSREC.

46-12735-13034-13231-13442-13923-134

!;1 COMPOUND

! gamma-BHC (Lindane) ___{ Heptachlor! Aldrin! Dieldrin! Endrin1 4. 4' -DOTi

SPIKEADDED( ug/Kg >

68.268.268.2170170170

MSDCONCENTRATION

(ug/Kg)

000000

MSD

REC #

0 *0 *0 *0 *0 *0 *

7.RPD #

000000

QC LJRPD

503143•— 'H4550

IMITSUIREi^B

46-12735-13034-13231-13442-139T3-134

i

# Column to be used to flag recovery and RPD values with an asterisk

* Values outside o-f GC limits

RPD: _ g. out o-f _ & outside limitsSpike Recovery! 12 out o-f 12 outside limits

COMMENTS: , -5^ C£**tc**ft UA*t V\CST6;\Vu.v%6v\ c

6-OU037JFORM III PEST-2 3/87 R

«K£R1CAM ANAL/T!CAJ. & TECHNICALNATRI* SPIKE EVALUATION FORfl

SAWPLE

*ET JIT.

noadded

Z373 TC3F 2.5HPCBF 10OCDF 25

2373 TCDO 2.5-CDD 10HXCDD 10

SAHPLE ID

MET HT.

2378 TCDFHPCDFOCDF

2378 TCDDPCDDHICDO

URS

ID TP-6-2MS

10.0

itount aiountin spi. addedppt ppt

25010002500

2501000

0 1000

DUPLICATE

TP-6-2MS

10.0

* fountin spi.ppt

351.31371.02763.6

275.91115.41157.2

aiountdetected 2ppt recovery351.3 14it1371.0 1372763.6 111

275.? 1101115.4 1121157.2 116

SAMPLE EVALUATION

TP-6-2HSO

10.0

iiount RPDin sol.ppt373.7 6,01628.1 17.12993.2 3.0

241.3 13.41067.7 4.41120.6 3.2

TARGETrecovery iiiits60 - 140 I60 - 140 I60 - 140 !

60 - 140 I60 - 140 I60 - 140 2

A R I O I U U 9

US AI£8!CA» ANALYTICAL i TECHNICAL SERVICES

HATRI1 SPIKE EVALUATION FORM

URS

SAMPLE ID TP-3-1HS

XET KT. 10.0

iiount iiount aiountno in spi. addid detected " TAR6ET

sddid ppt pat ppt recovery recovery liiits2373 TCDF 2.5 0 250 314.5 126 60 - 140 IHPCDF 10 0 1000 1163.1 U6 60 - 140 ZQCDF 25 0 2500 2899.4 116 60 - 140 I

2373 TCDD 2.5 0 250 277.B 111 60 - 140 t?CDD 10 0 1000 1104.9 110 60 - 140 IHXCBD 10 0 1000 1540.5 !54t 60 - 140 ;

DUPLICATE SAMPLE EVALUATION

SA*L£ 13 TP-3-WS TP-3-1HS0

KT *T. 10.0 10.0

iiount iiount RPDin sol. in sol.ppt ppt

2378 TCDF '314.5 226.7 32.4HPCDF 1163.1 1176.4 1.1QCDf 2899.4 3086.6 6.3

2378 TCDS 277.8 424.3 41.7?CDD 1104.9 1118.6 1.2HXCDD 1540.5 1471.8 4.6

*§D AFRICAN ANALYTICAL i TECHNICAL SERVICES

HATRII SPIKE EVALUATION FORM

URS

SAMPLE !3 TP-3-1HSD

*ET *T. — ~ 10.0

aiount aiount iiountno in spl. added detected I TARGET

added ppt ppt ppt recovery recovery Uiits2378 TCDF 2.5 ' 0 '250 "226.7 91 60 - 140 IHPCSF 10 0 1000 1176.4 113 60 - 140 IQCDF 25 0 2500 3086.6 123 60 - 140 I

2378 TCDD 2.5 0 250 424.3 170t 60 - 140 IPCDD 10 0 1000 1118.6 112 60 - 140 IHXCDD 10 0 1000 1471.3 • 147* 60 - 140 I

DUPLICATE SAMPLE EVALUATION

SA«PLE ID TP-3-1MS TP-3-IHS0

BET «T. 10.0 10.0

aiount aiouflt RPDin sol. in spl.ppt ppt

2378 TCDF 314.5 226.7 32.4HPCDF 1163.1 U76.4 1.1OCUF - 2899.4 3086.4 6.3

2378 TCDB 277.8 424.3 41.7PCDD 1104.9 1113.6 1.2HXCDD 1540.5 1471.8 4.6

6-OG037G

1ATRU SPIKE EVALUATION FORK

URS

SWftE !D TP-6-2«S0<

MET KT. 10.0

aiount Mount aiountng in spl. added detected Z TARGET

iddtd apt ppt ppt recovery recovery lints2378 TC0F 2.5 'o 250 373.7 1491 60 - 140 IHPCBF 10 0 1000 1628.1 1631 60 - 140 IOCDF 25 0 2500 2993.2 120 60 - 140 Z

2378 TCDD 2.5 0 250 241.3 97 60 - 140 IPCDD 10 0 1000 1067.7 107 60 - 140 IHXCDD -10 0 1000 1120.6 112 60 - 140 I

DUPLICATE SAMPLE EVALUATION'

TP-6-2WS TP-6-2MSD

10.0 10.0

a tount aiount RPDin spi. in spl.ppt ppt

2371 TCDF 351.8 373.7 6.0HfCDF 1371.0 1628.1 17.1OCDF 2763.6 2993.2 8.0

237S TCDD 275.9 241.3 13.4PCQB ' 1115.4 1067.7 4.4HXCDD 1157.2 1120.6 3.2

£'000377

A R I O I U 5 2

U.S. ERA -CLPERA SAMPLE NO.

DUPLICATESMU3S37D

Lab Name: SOUTHWEST LAB OF OK - Contract: 6B-D9-OOS9 TP (£ - X

Lab Code: SWOK Case No.: 32381 SAS No.: SDG No.: MU3S01

Matrix (water/soil): SOIL Level (low/med): LOW

7. Solids for Sample: 41.7 7. Solids -for Duplicate: 51.1

Concentration Units (ug/L or mg/kg dry weight): MS/KB

11

! Analyter

! Aluminum! Antimony.'Arsenic! BariumI Beryl lium! CadmiurrjI Calcium! Chromium! Cobaltj CopperI IronILeadI MagnesiumI ManganeseI MercuryINickelI Potassium! Sel-eniumISilver! SodiumI Thai lium! VanadiumIZinc! Cyanide

ControlLimit

23. 5

95 . 0

2.4

~

4.7 •

23.7

Sample (S) C

29762. 9590 i79 . 0829 12. 7257 IB

258.1931!1 . 7905 ! B6 . 4959 !

944 . 3550 I B133.0927!22. 1395 IB81.3416!

111226.4700!660.0624!1222. 7184 IB729.3603 13.3307!

367.2108!573 . 7O49 I B

1.4246JU6.9589!

194. 8972 IB1.4246 I U75.4716!464.7225!4 . 5940 ! U

''

_ Duplicate <D> C

37191.9370!5"T '•IIBT 1

._• . •_:•.£. d tJ I

4.0S86IB331.4555!2.1132IB6 . 2730 I

995. 7738 !B173.0695!22. 7933 IB70.9173!

74566.3710!631.9645!1428. 4788 IB806.9240!4.0876!

502.7947!878. 2453 !B

1.4246JU4 . 9047 1

174.2764IU1.4246 I U95.3136!367.3275!4.7021 !U

7.RPD

.ted£. . iTQ CD

40 . 024.816.53.5cr -r*J • —•26.12.913.739.54.315.510.120 . 431 .241 .9

34.6200 . 0

23.223.4

i«QIM

I*!P

1 PIFIFIPIP_! P _* IPIPIP

*!PIFI r"

IP

* !CV*IPIPIFIPIPIFIP

* IP1C

FORM VI - IN7/88

gr000373

""IOU53

U.S. ERA - CLP

3A EPA SAMPLE NO.SPIKE SAMPLE RECOVERY

MU3337SName: SOUTHWEST LAB OF OK Contract: 6S-D9-O089

uab Cod*: SWOK Case No.:,32381 SAS No.: SDG No.: MU3SO1

Matrix: SOIL Level <low/med): LOW

r. Solids -for Sample: 41.7

Concentration Units (ug/L or mg/kg dry weight): MG/KG

I \ ControlI ! Limit! Analyte ! 7.Ri «i i! Aluminum Ii Antimony 175-125! Arsenic 175-125! Barium ! 75-125I Beryl lium 175-125! Cadmium .'75-125ICalcium I! Chromium ! 75-125I Cobalt ! 75-125! Capper 175-125llron ISLead !'agnesium!.anganesei 75-125

! Mercury 175-125! Nickel 175-125! Potassium II Selenium 175-125! Silver 175-125! Sodium I! Thai lium 175-125I Vanadium 173-125IZinc 175-1251 Cyanide 175-125• it i

Spiked SampleResult (SSR)

91.750017.8705

1275.845725.493939.6483

242.2413257 . 6499195.0100

480.1918"

1089.33655.3O85

615.6831

3.92813O . 0007

1 8 . 3633346.7213595.437244.6995

_

CSample

Result (SR) C

!79.0829!2 . 7257 ! B

258.1931 !1 . 7905 I B6.4959!

!133.0927!22. 1395 JB81 .3416!

J660.0624!

I729 . 3603 13 . 3307 !

367.2108!!

1.4246IU• 6.95891

!1 .4246IU

75.47161464.7225!4.59401U.i

SpikeAdded C3A)

239.3119.18

959.2323.9823 . 98

95.92239.31119.90

9.59

239.311.09

239.31

4.8023.98

23.93239.31239.8148.54

7.R

5.379 . 0

106.193.8

138.3

113.398.294. S

-1875.6

150.1131.4103.6

si. e96.1

78.7113.154.592.1

Q!M

!NRNIPIFIPIP

NIP!NRIP-IPIP!NRIFINRJ

N!P "NICVIP!NRIFIP;NRIFIP

NIP1C ',1

Comments:

FORM V (Part 1) - IN

6^000370

SOUTHWEST LABORATORY OF OKLAHOMA, INC1700 W. Albany . Suite "C" . Broken Arrow, Oklahoma 74012 . 918-251-2858

ANALYTICAL REPORT

URS CONSULTANTS. INC. REPORT: 3238-1570 Delaware AvenueBuffalo, New York 14202

REPORT DATE: 08/24/90

SWLO IDENTIFICATION

SAMPLE NO. : 3238.01 ~~£3238.43BATE RECEiyiI>: 07/26/90 - &&&t

PARAMITKR RESULTS

MATRIX SPIKE TP-6-2 TOTAL SULFIDE 82% RECOVERY

DUPLICATE TP-6-2 TOTAL SULFIDE 7, IX RPD

ARIO|lt55

HEAHIH RESEARCH AND TESTING, INC.SHEET

CUSTOMER NAME: URS COSSUIgMTrS - MR. JTOAID JAODBI

SAMPLE SOURCE: Delaware Sand &•

SAMPLE TYffi: Spike Recoveries

DAIE RECEIVED: 07-25-90

ANaiATST: M, C&ceer & J* T ler

©ravel fProiect No.: 35214)

E80JECT NO. : 11913

DATE ANALYZED: 08-15/22-90

LAB NOTEBOOK NO. : 117 .Pa. 56

SAMPLE NOS.EHRT NO. CUSTCMER NO.

ANALYSIS & PERCENTMEIHOD

NIOSH Method 1300Methyl Ethyl KetcneMet±yl Isobutyl Ketone

NIOSH Method 1003

HbXXJVKHTKS(%)

6891

1 , 2-Diciiloroethane 97 . 3

NIOSH Method 1501Toluene

NIOSH Method 1501BenzeneEthylbenzeneTotal Benzene

NIOSH Method 5020Bis(2-Ethyl Hexyl) HithalateDi-N-Butyl Rithalate

NIOSH Method 5503PCB

113

111115108

11195

84

000381A R I O I U 5 6

U.S. EPA - CLP

5A EPA SAMPLE NO.SPIKE SAMPLE RECOVERY .———————-——__

ENVIRONMENTAL HEALTH SPIKE 1 |Lab Name: RESEARCH AND TESTING, INC. Contract: URS CONSULTANTS i

Lab Code: _____ Case No.: ____ SAS No.: _____ SDC No.: _____

Matrix ; Air Level (low/medj:

Concentration Units (ug/* Filter)

I11lAnalyte1I Aiuninutn"I Antimony^I ArsenicI Barium1 Beryl liura[ Cadmium[Calciumi Chromium; CobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThallium-'anadiumline-yanideTin

ControlLimitc,%R ,

-• - -

.

Spiked Samplemfiult fSSR)

*•-.- •&«•£•* *fc '----

8.88

16.0

15,9015.8013.90

15.80. .

17.50

13.70

18.30

0.64

CfcI1

Sample .vJNisurt,<sg*--'1 --- * - ' -- 3f3t*T5?««rtr- r- -• -r s

'0.5

0.2

0.850.1*0.32

0.5

0.39

0.20

0.23

2.3

-BJ>-

" '

U

u

^u

TJ

'U

U

'"* tf , ^JSpike :

*$£*<* (SA)5- ^ z", . 1' ,-' .:*fs«M«----s-1- . jsa I.J- -

15.0

15.0

15.015.015.0

15,0

15.0.

1S.U

15. U ,

15.0

-*R.-"•CPi" :

•' f

59

1U7

10010691

105

m91

99

< 1.0

Q

*

.

"«

1

•

;

-.merits:_ _ _ _ _ A t T»0° recommended by the Niosh method for digestion, arsenic Is pract1cally_deeofflpo*ea_ and tin is completely unstabT^ The filters were "spiked with 1 >5 ug/mL or 15 ug/nite*^_. _______for_each_element.______________ ~~" " "_.!_'". l - _____^ _ .

6T0003S-

OU57

U.S. EPA - CLP

EPA SAMPLE NO.SPIKE SAMPLE RECOVfcKX . ————————— ———— ]

ENVIRONMENTAL HEALTH SPIKE 2 • | ftu*VK- \Lab Name: RESEARCH AND TESTING, INC. contract: URS CONSULTANTS i s ?/£.£, x i

Lab Code: Case No.:

Matrix : Air

__ SAS No. :(> C-l

11913 SDG No. :

Level (low/med) :

Concentration Units (ug/pn r) ,,J_ _ .,_

I I Ij I Control I1 | Limit I Spiked Sample[Analyse | %R { Result (SSR) -1 ' I I(Aluminum | 1[Antimony j 11 Arsenic j [ 9.6521 Barium | IJBeryllluSi Ij Cadmium I I 16.3j Calcium | j1 Chromiua I 1 75. gi cobalt { I i*.5! Copper I I s-33: Iron | . [Lead | i 16.0Magnesiumj 1Manganese! jMercury j INickel __ i I 15,9Potassiuml jSelenium | I K» ?. Silver I |Sodium^ I IThallium I IVanadium j I-inc^ __ I I 17.*-yanide | Inn I I 1.86

C

i"I1.l_

SampleResult (SR)

0.5

0.2

O.flc,0.1*0.32

O.S

0.39

2.0

3.5

I.-*,

C

IT

jj

ii

u.

SpikeAdded (SA)

15.0

15.0

15.015.015.0

15.0 .._ .

!! [

*R Q K j1

6*

109 .

98<4753

107 I1ii

15.0 1C13 '1

U 15. 0 . 95 .J

i i _! '

I ' !

t 1 n n 93 _ • • _1 1 : _! U! 15.0 <1.0 .

sr.nents :

3DSOIL SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Name: SWL-TL'LSA_______________. Contract: URS_______

Lab Code: SMOK Case No.: URS SAS No.: ______ SDB No.:

Matrix Spike - EPA Sample No.: UD-3-10_____ Level:(low/mad) LOW

COMPOUND

Phenol2-Chlorophenol1 , 4-Dichlorobenzene ___N-Nitroso-di-n^prop. ( 1 )1 ,,2,4-Trichloroben-z©ne_4— Chl oro-3-methy 1 pheno 1Atenaohthene

( .4-NitroDheTVOl, j, 4-g_in i trojot uene ___ ^_"*, PentachlorbpherrolPvrene

SPIKEADDED(ug/Kg)

145001450072507250725014SOO7250!480C" Tiso . > :i48oof250

SAMPLECONCENTRATION

< ug/Kg)

o0

_ 000O0

-- ----- o"~ * 0

--- ~V o" - --- 0

MSCONCENTRATION

(ug/Kg)

77606880365035004010754O3840

-,,;- 7610

r- -~ - - 393O— -"'7.900

-V 444O

MS•/.

REC #

54475O4B55 .52535254 ;54 "61

DCLIMITS

REC.

26- 90<-?*=• -I /'I'-*A. *J 1 * J .L.

28 10441 12638 10726 10331-13711-11428- 89

r 17- 10935-142

COMPOUND

Phenol2-Chloroohenol1 ,4-Dichlorobenzene ___N-Nitroso-di-n-prop". ( 1 )1 . 2.4-Trichloroben2ene_4-Chl or o-3-methyl phenolAcenaohthene4-Nitrophenol2 ,4-Diriitro toluene ____PentachloroDhenolPvrene

SPIKE 'ADDED(ug"/Kg)

14500145007250725072501450072501 45007250145007250

MSDCONCENTRATION

(ug/Kg)

921086304630___4000444O79§0452O9350492037004810

MSD7.REC #

6460645561' 556264686O66

7.RPD **

-17-24-25-14-1O-6-16-21-23-11-8

1

DC LIMITSRPD

3550273323r?*"1950474736

REC.

26- 9025-10228 10441 12638 10726 10331-13711-11428- S917-10935-142

( 1 > N-Nitroso-di-n-propylamine

# Column to be used to -flag recovery and RPD values with an asterisk* Values outside o-f QC limits

RPD: _ 0.- .P_Mt p-f 1 1 outside limits. _Spike Recovery: _ O d"ut o-f 22' outside limits

COMMENTS : UD-3- 1 0 URSINST:F

- 0-000384FORM III SV-2 1/87 Rev,

A R I D ll*59


Lab Names SKL-TULSA_______________ Contract: URS_______'_

Lab Code: SWQK , Case No.: URS1 SAS No.: ______ . SDG No.:

Matrix Spike - EPA Sample No.:.UD-3-10____ Level:<low/med) LOW

COMPOUND

gamma-BHC (Lindane)HeDtachlorAldrinDieldrinEndrin4 4 ' — TiHTt « i iw t

SPIKEADDED(ug/Kg)

5.855.855.8514.614.614.6

SAMPLECONCENTRATION

(ug/Kg )

00ooo£)

MSCONCENTRATION

(ug/Kg )

3.6314.73.176.329.51

11 ^A A • ji.

MS7.

REC #

63251 *5443.6577

QCLIMITSREC.

46-12735-13O34-13231-13442-139

COMPOUND

qamma-BHC ( Lindane )HeptachlorAldrinDieldrinEndrin4,4' -DDT

SPIKEADDED(ug/Kg)

5.855.855.8514.614.614.6

MSDCONCENTRATION

(ug/Kg)

3.0219.13.6O8.9612.612.6

MSD7.REC t

52326 *62613686

y

RPD #

19-26-14-35-28-11

QC L]RPD

503143384550

i[MIT5 |

REC146-12735-1 3034-13231-13442-13923-134


* Values outside o-f QC limits

RPD: _£ out o-f _^ outside limitsSpike Recovery: _2 out o-f 12 outside limits

COMMENTS:

FORM III PEST-2 - 8/87

A R ! O i H 6 0

U.S. EPA - CLP

7LABORATORY CONTROL SAMPLE

'€'

Lab Name: SOUTHWEST LAB OF OK Contract: 6S-D9-0089

Lab Code: SWOK Case No.: 3505 SAS No.: SDG No.: MUO501

Solid LCS Source: EPA0287

Aqueous LCS Source:

* . . ""*"

! Analyjte^

[Aluminum.'AntimonyI Arsenic! BariumI Bery I liumJ Cadmium! CalciumChromiumCobal-t

I Copper! Iron.' LeadI Magnesium! Manganesei Mercurv! Nickel! Potassiumi Seleniumi Silver1 Sodiumi Thai 1 ium! VanadiumI Zinc! Cvanide•'

Aqueous < ug/L )True Found. __ 7.R

'

"

•

Solid, ung/kg)L_=.J*"M_3 ^F_Qun_g___ .^G ' r ..Limits JCR

•-•.S »tU

211 .0917. 04.819.445.4

1962OO.O99.6

1 44 . 0691O.O224 3O . O236 . 0

113100.0208 . 012.760 . 950.039.2T-> ''I

50 . 039 . 065.8187.05.6

" 254.3140.4382 .3

5. 117". 444.2

151853.693.3142.7

A*7~TA TO —'** . *

19974.0225 . 0

119420.3197.0If .162.169 . 0"i«7 "i— /..*.15.999.241 .056.6177.560• *-

•

B

U

BB

£25 -.01 27 . 0635.00 . 016.5•-•*j . /

1668OO.O79.2'124.06006 . 017770.0188.0

1004OO.O1 77 . 03.549.20 . 0

19.115.5O.O24.651.7138.04.3

424.0294 . 01 1 99 . 040 . OT-( T&.*! • •-*

.55.1225600 . 0

'1 2O . '162.n7S20."2708O.U285. (

129900.1239 . '17. i72.6

1000.059.429.0

1 000 . 053.579.9

' 236 . 06.9

73.26a.596.3106.2-89.797.477.494 m 99, 19*:> . 289.195.3

1 0 1 . 194.787.4102.0• 0 . 0o9.471 .6193.4105. 136 . 094.9

110.7ii

FORM VII - IN7/88

MJ00386

ARIOU6

U.S. EPA - CLP

75 LABORATORY CONTROL SAMPLE

Lab Name: SOUTHWEST LAB OF OK Contract: 68-D9-OOB9

Lab Code: SWQK Case No.: 3505 SAS No.: SDG No.: MU0501

Solid LCS Source: EPA02S7

Aqueous LCS Source:

An a 1 y tm

AluminumAntitnonvArsenicBariumBervl liumCadmium

i CalciumChromiumCobalt

t Copper{ IronJLemd; Magnesium' ManganeseJ MercuryINid elIPotAMtUffl; Selenium{Silvar! Sodium! Thai lium! VanadiumIZinc! Cyanideii

Aqueous (ug/L )True Found '/.R

\-

Solid (mg/kg)True Found C Limits 7.R

-

5.6

t11111

!:<ii;!

iiii<ii*t!iiiti;Ii

6.2!

-

4.3 6.9

(

110.7

FORM VII - IN

A R I O U 6 2

U.S. EPA - CLP

" 7~LABORATORY CONTROL SAMPLH

Lab Name: SOUTHWEST LAB OF OK • Contract: 68-D9-OOS9

Lab Code: SWOK Case No.: 3505 SAS No.: SDG Mo.: MUO501


Aqueous LCS Source:

Anal vte

AluminumAn tirnonvArsenicBariumBery 1 liumCadmiumCalciumChromiumCobal'tCopperIranLeadMagnesiumManganeseMercuryNickelPotassium"SeleniumSilverSodiumThai liumVanadiumZincCvanide

Aqueous (.ug/L)True Found *'.R

_

-

So lieTrue Found

-

5.6

.

6.6 4.3 6.9 117.9

FORM VII - IN7/38

£r000388

A R I O I U 6 3

U.S. EPA - CLP


Lab Name: SOUTHWEST LAB OF OK Contract: 63-D9-OO39

Lab Code: SWQK Case No.: 36151 SAS No.: SDG No.: MU1501


Aqueous LCS Source:

ii

I AnalyteJJ Aluminum! Antimony! ArsenicJ Bariumi Beryl 1 iumt Cadmium3 CalciumI ChromiumCobalt

. Copper1 Iran!Lead1 Magnesiumf Manganese! Mercury(Nickel! Potassium! Selenium(Silver'Sodium! Thai 1 ium! VanadiumI ZincI Cyanide

'Aqueous (ug/L)

True Found MR

J! -

1 1

"

Solid (mg/kg)Tr ue Found C Limits ''.R

325.0! 294.621 I. O! 162.9917.0! 994.3

4.8! 5.919.4! 17.345.4! 43.5

196200.0! 195376.799.6! 79.6144.0! 123. 1

6910. O! 6699.32243O.O! 17881.7236.0! 240.3

118100.0! 121260.7208.0! 199. 11.2.7! 13.560.9! 50,950.0! 67.639.2! 28.322.2! 20.25O.O! 416.139.0! 38.165.3! 55.1187.0! 163.25.6! 6.6

B

U

B

225.0127.0

- 635. 00 . 0

: 16.5• T5 "*166800.0

79.2124.06006.01777O.O138.0

100400.0177.0

. . 3.549.20.019, 115*50. 0

24.651.7138.04.3

424.0294. 01199.0

40.022. 355.1

225600.012O.O162. O7320. O27080. O285.0

129900.0239. 017.072.6

100O. 059.4

_ 29.01000. O

53.579.9236.06.9

9O.677.2103.4122.939.295.399.679 a3. H9. H79 P101.3102.795.7106.3S3. 60.0

•* •!• • <-.

91 . 0_Q->'-i • -:_97.733.737.3117.9

FORM VII - IN7/83

#-§00 89

U.S. EPA - CLP

7^. LABORATORY CONTROL SAMPLEM& ... --. _ . . ..,, . ,*££-SB:' " *

Lab Names SOUTHWEST LAB OF OK Contract: 68-D9-OO89

Lab Code: SWOK Case No.: 36151 SAS No.: SDG No.: MU1501


Aqueous LCS Source:

1

1

! Analyte

! Aluminumf Antimonv! Arsenic! Bari umI Beryl 1 i um! Cadmiumi Calcium.ChromiumCobalt(Copper! Iron!Lead! Magnesium! Manganese! MercuryINickel! Potassium! Selenium! Silver! SodiumJ Thallium! VanadiumJZinc! Cyanide

Aqueous (ug/L)True Found "/.R

Solid (mg/kg)True Found C Limits XR

12.7

'5.6

9.3

6.1

:

8.5

4.3

17.0

6.9

73. 2

103.9

FORM VII - IN. 7/SS

OOOSuO

flRI01U65

SOUTHWEST LABORATORY OF OKLAHOMA, INC. **1700 W. Albany . Suite "C" . Broken Arrow, Oklahoma 74012 . 918-251-2858

CLIENTS URS CONSULTANTS* INC. REPORT: 3520»570 DELAWARE AVE.BUFFALO, NY 14202 DATEs 09-06-90ATTNs PETER FAIRBANKS

LABORATORY BLANK

SAMPLE MATRIX* SOIL SAMPLE AMOUNT: 30GSAMPLE ID» METHOD BLANK DILUTION FACTOR: 1

DETECTION AHOUNT FOUNDCOMPOUND______________LIMIT dm/Kg)______________(mo/Kg)

TPH 10.0 ND

TPH MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY DATA

SAMPLE MATRIX i SOILSWLQ # 35Q5.05 (MS)PROJECT: DELAWARE SAND & GRAVELSAMPLE ID I UD-2-9 (MS)

SPIKE CONC. SAMPLE CONC. MS CONC. MS PERCENT<ttg/Kg) Cag/Kg)* («g/Kg)« RECOVERY

TPH 667 O 570 85'/.

SAMPLE MATRIX s SOILSWLO * 35O5.05 (MSD)PROJECT*-. DELAWARE SAND & GRAVELSAMPLE JO i UD-2-9 (MSD)

MBD CONC. . PERCENT . RECOVERY PERCENTRECOVERY DIFFERENCE

TPH 570 85 0%

* * DILUTION FACTOR NOT APPLIED TO THESE CONCENTRATIONS

£-000391

- . AR10U66

SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Suite "C* . Broken Arrow, Oklahoma 74012 . 91 251-2858

METHOD t| TPH (FREON EXTRACTION; ANALYSIS BY IR)ANALYSIS DATE 4> 09/07/90

LABORATORY BLANK

MATRIX : SoilSAMPLE ID. : SBLK09O69001SAMPLE AMOUNT : 305 DILUTION FACTOR: 1

HUANTITATION AMOUNT FOUNDU I M 1 T tmg/kg) (ir.g> kg )

TPH 10.0 10.0 ND

MATRIX.SPIKE/MATRIX SPIKE DUPLICATE RESULTS

1574.05 1574.05MSCOMPOUND SPIKE CONC. SAMPLE CONC. MATRIX SPIKE PERCENT

(mg/kg) (mg/kg) * CONC, (mg/kg) * RECOVERY

fPH 667 0 600 90 V.

1574.05MSD'-'ATRIX SPIK'EDUPLICATE PERCENT RECOVERY PERCENTCONC, (mg/kg) * RECOVERY DIFFERENCE

TPH 59O 83" 2

* DILUTION FftfetfcftS NfOT APPLIED TO THESE CONCENTRATIONS

COMPOUND SAMPLE CCNC. DUPLICATE CONC. RELATIVE PERCENT DtFF.(mg/kg) (mg/kg) */.

TPH .0

• ft- '000392

SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Suite "C" . Broken Arrow, Oklahoma 74012 . 918-251-2858

METHOD i TPH (FREQN EXTRACTION; ANALYSIS BY IR)ANALYSIS DATE : O9/O7/oo ' - :

LABORATORY BLANK

MATRIX : SoilSAMPLE ID. : SBLK09069002SAMPLE AMOUNT : 305 DILUTION FACTOR: 1

2UANTITATION" A.^LI^IT (rr.g/kgj (r.q/*

TPH 10.0 10.0 ND

MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULTS


(mg/kg) (mg/kg)* CONC. Cmg/kg) * RECOVERY

TPH 667 0 620 93 */.

1580.01MSDMATRIX SPIKEDUPLICATE PERCENT RECOVERY PERCENTCONC. (mg/kg) * RECOVERY DIFFERENCE

TPH 630 94 -2 7.

* DILUTION FACTORS NOT APPLIED TO THESE CONCENTRATIONS

bAMPLE HE3ULTS

COMPOUND SAMPLE CONC. DUPLICATE CONC. RELATIVE PERCENT DIFF(mg/kg ) £ mg/kg ) "/.

TPH

/* ^ «R 1011.68 . (V-00039.-;

SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Suite "C" . Broken Arrow, Oklahoma 74012 . 918-251-285$

METHOD : TPH (FREON EXTRACTION; ANALYSIS BY IR)ANALYSIS DATE : 09/07/PO

LABORATORY BLANK

MATRIX : SoilSAMPLE ID. : SBLK09O69002SAMPLE AMOUNT : 30G DILUTION FACTOR: 1

3UANTITATICN AMOUNT F-~!:jNDLIj-UT (ng/kg) (^5/^5)

TPH 10.0 10.0 NO



(mg/kg) (mg/kg)* CONC. (mg/kg ) * RECOVERY

TPH 667 0 620 93 7.

1580.01MSDMATRIX SPIKEDUPLICATE PERCENT RECOVERY PERCENTCONC. (mg/kg) * RECOVERY DIFFERENCE

TPH i r, 630 94 -2 7.•*. - -

** DILUTION FACTORS NOT APPLIED TO THESE CONCENTRATIONS

DUPLICATE SAMPLE HE3ULTS \

COMPOUND SAMPLE CONC. DUPLICATE CONC. RELATIVE PERCENT DIFF,(mg/kg) (mg/kg) 7.

TPH .0

ftRIOlW

3DSOIL SEMIVDLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Namns SWL-TULSA_______________ Contract: URS_______

Lab Code: SHDK Camm No.: URS SAS No.: ______ , SDG No.:

Matrut Spike - EPA Sample No.: UD-7-10_____ Level!<low/med) LOW

COMPOUND

Ph*nol2-Chlorooh^nol1 ,4-Dichlorob@n2eneN-Mitroso-di-n~prop. < 1 )1 ,2.4-Trichlorobenz©ne_4-Chloro-3-methvl phenolAcenaohthen©4-Wi Lraohenol2.4-DinitrotoIuenePentachloroDhgnolPvren^ *

•

SPIKEADDED< ug/Kg)

167OO167OO8340334033401670083401 67OO33 4 O167008340

SAMPLECONCENTRATION

(ug/Kg )

OOOO

4OOoOOo0o

MSCONCENTRATION

< ug/Kg )

41709346220470O439O384O5990349039901 320O720O

MS7.

REC #

-ve- 4.-i.-j *6 *

75 •564353TJ-I/ X.

21727936 "

DC !LIMITS!REC . !

— — — — — — t26- 90!cr i ,-,"1

23 1<»441 12633 lo726 l'»331-13711-1 1 £.23- 8s?17-10935-142

COMPOUND

Phenol2-Chlorophenol1 ,4-DichlorobenzeneN-Nitromo-di-n-prop. ( 1 )1 «2,4-Trichlorobenz©ng4-Chl a ro-3-methyl phonalAcenaphthen©4-Nitrophenol2 ,4-DinitrotoluenePentachlorophenolPvrene

SPIKEADDED(ug/Kg)

16700167OO834083408340167OO83401670O8340167008340

MSDCONCENTRATION

(ug/Kg)

3440129O6580572046509840625094206310135007630

MSD7.REC #

21 *3 *796951597556768191

7.RPD #

17_^Q^L 7

-5__'"* 1-L. i-6

~ -11-4

-91 *-5— .__y-6

QC LIMITS^RPD

" 5-SO738<~1 T

"T,7

195O474736

RECM

26- 9025- 1 0223 10441 12633 10726 10331-13711-11*23- 3917-10935-142

<1) N-Nitro&o-di-n-propylamine

# Column to be used to -flag recovery and RPD values with ;an asteriskt Values outmidg of QC limits

RPD: _L out o-f 11 outmide limits ~'.m Recovery: _4 out o-f 22 outside limits

COMMENTS: UD-7-10 URSSWLS3471.G8 3

^ttQQ39FORM III SV-2 -.-- —— - 1/37

ARIOU70


Lab Name!! SWL-TULSA______________ Contract: URS_____

Lab Codes SUIQK ••*' Case No.: fJRS SAS No.: ______ :SDQ No.:

Matrix Spike - EPA Sample No.: UD-7-12____,_... Level:<low/med) LOW

COMPOUND

Phenol2-Chlorophenol1 ,4-DichlorobenseneN-Nitroso-di-n-prop. ( 1 )1 .2?4-Trichlorobenzene_4-Chloro-3-me thy 1 phenolAce.naohthene ..— .4-Nitrophenol _._.... -2 , 4-D i n i t r o to 1 uen e _____PentachloroohenolPvrene

SPIKEADDED< ug/Kg)

1590015900794O794079401590O ._7940159007940

".159OO7940

! SAMPLE! CONCENTRATION! < ug/Kg)

! 0: o! 0' ' " 0! 150 =A - " . ". 0 " ._ ~:

\ 00

! 0

! O;

MSCONCENTRATION

<ug/Kg )

1 1 40O9050646063605910

" __.1250O54209610

• 6130" 127t)0 ~"

60*70

MS/.

REC #

72573180737963"6073SO77"

"•""

QCLIMITSREC.

26- 9025- 1 0223 10441 .12633 1 0726 1 0331-13-*11-114

17-10935-142

COMPOUND

Phenol2-Ch 1 or D phenol1 ,4-DichlorobenzeneN-Nitroso-di-h-prop. < 1 )1 ,,2,4-Trichlaroberizene_4-Chlo:ro-3-methy 1 phenolAcenaD'hthene4-Nitrophenol2. 4-Dinitro toluenePentachlorophenol .. . .Pvrene

SPIKEADDED(ug/Kg )

159OO15900794079407940159007940

1 59007940

1 59007940

MSDCONCENTRATION

(ug/Kg)

11300~ 9130

642066906 1 30

1 2300557062206690132005980

MSD•/REC #

_ 7157313476777039348375

y.RPD #

100—5-4

; O«— -li42-7"~43

QC LIMITSRPD

35502733<"JT

— ]T,

1950474736

REC.

26- 9025-10223 10441 12633. .10726 10331-13711-11423- 8917-10935-142

. (1>.N-Nitroso-di-n-propylamine

^ Column to be used to -flag recovery ana RPD values with an asterisk* Values outside o - f Q C limits - - . . _ = .

RPD: _0_ out o-f 11 outside 1 imitsSpike Recovery: _0_ out of 22 outside limits

COMMENTS: UD-7-12 URSSWL#3471.i3 30G/0.9 - - - ~ -- - .

FORM III 3V-.2 . , ... , 1/37 Rev,

A R I Q . 1 L 7 1


Lab Name: 3WL-TULSA______________ Contract: URS________

Lab Code: SUJQK Case No.: URS 3AS No.: ______ , SDG No.:

Matrix Spike - EPA Sample No.: UD-11 A-12 Level :(low/med ) LDUJ

COMPOUND

Phenol2-Chloro phenol1 ,4-DichlorobenzeneN-Nitroso-di-n-prop. ( 1 )1 ,2.4-Trichloroben2ene_4-Chloro-3-methy I phenolAcenaphthene4— Ni tronhenol2. 4-D in itro toluenePentachlorophenolPvrene

SPIKEADDED(ug/Kg >

15300153007660766076601530076601 53007660153007660

SAMPLECONCENTRATION

(ug/Kg )

0000

6660C)0C)0o

MSCONCENTRATION

(ug/Kg)

136OO1340074307390739014OOO6580

60 1 088007460

MS7.

REC #

393897 .96pnoo9286E-DUO

735397 '

QCLIMITSREC.

26- °025-10223 10441 12633 10726 10331-1371 1 - 1 t -'i23- 3?.17-10935-142

COMPOUND

Phenol2-Chlorophftnol1 ,4-DichlorobenreneN-Nitroso-di-n-prop. ( 1 ;•

4-Chloro-3-methy 1 phenolAcenaohthene4-Nitroohenol2, 4-D in itro toluene ____PentachlorophenolPyren^

SPIKEADDED<ug/Kg>

1 53001530O7660766076 6 O

1 530O766015300766O153007660

MSDCONCENTRATION

(ug/Kg)

124001 0800586048605630109OO555010100398076205470

MSD7.

REC #

8171766365717266525071

7.RPD 1*

o212442 *T fi i•MI '»_* *

13-134O1531

QC L]RPD

35502733

1950474736

MREC^

26- *.025-10228 1 0441 12633 1 0726 10731-13711-1 1429— 99.17-10935-142

( 1 ) N-Nitromo—di-n-propylamine

# Column to b© uwd to -flag recovery and RPD values with an asterisk# Values outside o-f OC limits

RPD: _2. out of 11 outside limits "" ~"Spike Recovery: __£ "but of 22 outside limits :

COMMENTS: UD-ilA-12 URSSWL#3471.03 30G/O.9

FORM III SV-2 1/S7 Rev

ARIOU72

3 F - - • • • •SOIL PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Name: SML-TUL5A_______________ Contracts 69-D9-OO25

Lab Code: SWDK Case No.: URS1 SAS No.: ______ SDG No.s __

Matrix Spike - EPA Sample No.: 'UD-7-.1O____ Level!(low/med) LOUJ

COMPOUND

gamma-BHC (Lindane) ___HeotachlorAldrinDieldrinEndrin4,4'-DDT

SPIKEADDED(ug/Kg)

66.5AA e.j-iL. =;oo . u166166166

SAMPLECONCENTRATION

(ug/Kg)

OO"

0O

54.1

MSCONCENTRATION

(ug/Kg)

2.66i~? o«=: i1"?1J • O.4.

125181234

MS ! QC7. iLIMITSREC *! REC.

4 * 146-127Tt-7 * ' TET 1 TI-J

B *!-*4-13275 131-134109 142-139108 123-134

r

COMPOUND

gamma-BHC ( Lindane ) ___HeptachiorAldrinDieldrinEndrin4,4'-DDT

SPIKEADDED(ug/Kg )

66.566.566.5166166166

MSDCONCENTRATION

(ug/Kg)

2.4218.07.78

129176231

MSD7.REC *

4 *27 *12 *781O6107

7.RPD ft

0O

-40' -4

31

QC L3RPD

503143384550

[MITSREC.

46-12735-13034-13231-13442-13923-134

# Column to be used to -flag recovery and RPD values with an asterisk


RPD: _O out o-f _6 outside limitsSpike Recovery: _6, out o-f 12 outside limits

COMMENTS:

5-000397FORM III PEST-2 S/87 Rev,

ARIOU73


Lab Name i SUJL-TULSA _____________ Contract: 69-D9-OO25

Lab Code: SKOK Came No.: URS1 SAS No.: ______ SDG No.: ___

Matrix Spike - EPA Sample No. s UD-7-12____ Level 2 (low/med) LOW

!it! COMPOUND] TMWwaif'CTtTiri=fyT"'F f <- iv — ~" ™ "•" " n n nt

i gamma-BHC (Lindane) ___i Heptachlor1 Aldrin! Dieldrin1 Endrin{ 4,4'-DDT!

SPIKEADDED(ug/Kg)

ssssssseszmss

63.363.363.3158158158

SAMPLECONCENTRATION

(ug/Kg)

000O00

-

MSCONCENTRATION

(ug/Kg)

2.9927.96.4624.043.076.2

MS7.

REC #

5 *4410 *15 *27 *48

QCLIMITSREC.

46-12735-13034-13231-13442-13923-134

COMPOUND

gamma-BHC (Lindane),Heptachlor________Aldrin________'. _ _ _Dieldrin__________Endrin___________4,4'-DOT__________

SPIKEADDED(ug/Kg)

3 —2*S = 35SES

63.363.363.3158158158

MSDCONCENTRATION

<ug/Kg)

3.O623.66.7525.136.6112

MSD7.

REC ft==5SSX

5 *3711 *16 *23 *71

7.RPD *-ssaessae

O17

-10-616-39

QC LIMITSRPD

503143384550

REC

46-135-13034-13231-13442-13923-134



RPD: _2 out o-f _6 outside limitsSpike Recovery * '_g. out o-f 12 outside limits

COMMENTS:

6-000398FORM III PEST-2 8/37 Re

A R I D 11*71*


Lab Name: SWL-TULSA_______________ Contract: 69-D9-OQ25

Lab Code: SWDK Case No.: URS1 SAS No.: __. SDG No. s ———

Matrix Spike - EPA Sample No.: «UD-11A-12 Level:<low/med) LOW——

COMPOUND

aamma-BHC (Lindane )HeotachlorAldrinDieldrinEndrin4 4 ' nnT

SPIKEADDED(ug/Kg )

M"i• *!•

61.261 .2153153153

SAMPLECONCENTRATION

(ug/Kg>

0OO0

81.70

MSCONCENTRATION

(ug/Kg)

16.720.9O

201108

2410

MS7.

REC #

27 *34 *O *

13117 *

1 =17 *1 >J / <J *

QCLIMITSREC.

46-12735-13034-13231-13442-13923-134

COMPOUND

gamma-BHC (Lindane); ___HeotachlorAldrinDieldrinEndrin4, 4 '-DOT

SPIKEADDED< ug/Kg)

61.261.261.2153153153

MSDCONCENTRATION

(ug/Kg)

11.920.30

1552131690 ~

MSDy

REC #

19 *33 *0 *

10186

1105 *

•/

RPD #

353O26

-134 *35

QC LJRPD

503143384550

[MITSREC.

46-12735- 1 30• /i 1 " ^o*f — 1 -j-i31-13442-13923-134



RPD: __1. out of _6 outside limitsSpike Recovery: _9. out of 12 outside limits

COMMENTS:

5-000399FORM III PEST-2 a/87 Rev'

ARIOU75

U.S. EPA - CLPEPA SAMP1 E NO.

Lab Names SOUTHWEST LAB OF OK Contract: 68-D9-0089MU7108D

Lab Cod©: SWOK Case No.: 34711 SAS No.: SDG No.: MU7101

Matrix (water/soil): SOIL Level (low/med >: LOW

7. Solids -for Samples 81.9 7. Solids -for Duplicates 91.4


11! Analyte

I Aluminum! Antimony! ArsenicI BariumI Beryl lium! Cadmium{ CalciumI ChromiumI CobaltI Capper! I ranILesdI MagnesiumI Manganese{ Mercury! Nickel\ PotassiumI Selenium! Silvert SodiumI Th«*l lium! VanadiumIZincI Cyanide»i

ControlLimit

9.8-

1 r? *•?I-C. . -i.

Sample (S) C

7967.3926!11 .3043 IB1.7265 IB14. 2846 IB

- .7139IB1 . O5O6 I B

241. 3773 IB18.922013.938B!B4.1431 IB

20236.5880!4 . 3053 I

268.5371 IB34.7977!1.0175IU15.2351!

370 . 7795 I B.7326!U

1.1466 IB179. 4955 IB

.7326IU16.04681106.2992!2. 2780 I U

ti

Duplicate (D) C

6945.4422112. 1B33!B1 .7729 IB

1 1 . 7544 ! B.6662 IB

1 .1647JB206.1417!B19.1959!4. Il5l IB4.3217IB

17841 .7710!3.7924!

197.7716JB23.5786!

.1110SU16.4284!

366. 7199 IB.7326 ill.9381 !B

16S.2156IB.7326 I U

13.9047!129.261312.1726IUi

7.RPD

13.77.52.7

19.46.9

10.315.71 .44.34.2

12.612.730 . 419.6

7.51 .1

20 . 06.5

14.319.5

Q M

PPf-"PPPPPPPFFpPCVP •PFF*0pPPC

ARIOU76

FORM VI - IN7/83

U.S. EPA - CLP

5A EPA SAMPLE NO.SPIKE SAMPLE RECOVERY ______

MU7108SLab Name: SOUTHWEST LAB OF OK Contract: 68-D9-0089

Lab Code: SWQK -H Case No.: 34711 SAS No.: SDG No.: MU7101

Matrix: SOIL Level (low/med): LOW

"/. Solids -for Sample: 81.9


! Anal vte

! Aluminum! Antimony! Arsenic1 Barium! &p?r v 1 1 iumrCadmium! Calcium1 Chromium•CobaltI Cdpp'erJ Iron.'Lead! Magnesium! ManganeseI Mercurv! NickelI Potassium! SeleniumI Si 1 verI SodiumI Thai liumI VanadiumI Zinc! Cyanido

ControlLimit7.R ..-_

7?-"12575—125 ..75-12575-125 "75-125

75-125.75-12575-123

75-125

75-12575-12575-125

75- 1 2575-125

75-12575-12575-.125 ...75-125

Spiked Sample__ Result (SSR).

76 . 23407.8266

508.0795~" " " 12.3079

18.3812

68 .7720. .__ - 126.0737

67.2276

9.0183

162.7676.. 5840

143,9410

1 .946313.9207

12.6789139.7329227 . O57024.0751

CSample

_{

ll.:3O43!B1.7265 IB14.2846IB,7139 IB1,0506!B

I18.922013/9388 IB4. 1431 IB

!4 . 3053 I

!34.7977!1 .0175IU15.2351!

i.7326!U

1. 1466 IB!

. 7326 I U16.04681106.2992!2.2780IU

SpikeAdded (SA)

122. 109.77

438 . 4012.211 2 . 2 1

48.84' 122. 10

61.05

4.83

122.10.53

122. 10

2.4412.21

12.21122.10122.1022.70

-,:R

e- -?- 'i

t 2 .

101.1OQ . M

141.9

102. 1. -10-J.f'107. 7

96.6

104.81 1 f'» . r105.4

79.8104. t

107.8101,"99. P

"106.1

a : M

:NRN ! P"N;F:p: P

M ! P:NR;p: P:p: MR: F:NR; p* rv:p! Nft: F; P:NR: F:P:P: C

Comments:


000-101

« D ! O ' *i 7 7HR I U I 4 / /

U.S. EPA - CLPEPA SAMPLE NO.

6DUPLICATES

MU7113DLab Nami?s SOUTHWEST LAB OF OK Contract: 68-D9-0089

Lab Code: SWOfC Case No.: 34711 SAS No.: SDG No.: MU7101

Matrix (water/soil)s SOIL Level (low/med): LOW

•/. Solids -for Sample: 86.4 7. Solids -for Duplicate: 84.1

Concentration Units (ug/L or mg/kg dry weight): MG/KGiiI Analyte

I Aluminum! Antimony! Arsenic! Barium! Beryl liumI Cadmium! CalciumI Chromium! CobaltI CopperI Iron! L©adI Magnesium! Manganese! MercuryI NickelI PotassiumI Selenium{SilverI Sodium! Thai 1 iumI Vanadium! ZincI Cyanide!

ControlLimit"

_.

5.S

.7

9.3

11.64.61*7

.__

Sample (S) C

6554.5790!6.0185IU1 . 1574 !U

21. 0170 !B. 7034 ! B.6944 I U

522. 0623 IB17.0509!3. 6856 IB7.4167!

10269.5300!7.4306!

527. 2055 !B147.5821 I

. 0857 I U29.9677!646. 4960 IB

. 6944 I U4 OD . 1 i C*

142. 0880 IB. 6944 I U

20.4112!23 . 7738 I1 .7071 !U

!

Duplicate (D) C"

5383.0015!6.0185IU1.1574 I U

18.3714IB-6160JB. 6944 ! U

354.6791 IB15.5471 !4.O344IB5.9480!

10347.2900 I4.9144!

456. 4212 IB202 . 3202 !

.OS'57 I U24.4235!527.2021 IB

.6944 I U

. 4630 I U141 .8010 IB

.6944 I U16.3364!20 . 8067 !1 .8974 I U

ir

7.RPD

19.6

13.413.2

38.29.29.022.0

.84O.314.431.3

20,4Ofj T

200. 0.2

22. 213.3

Q

*

M

PPFPP

MP 1PPPFPPCVPPFPPF -PPC

i

FORM VI - IN7/G8

ARIOU78

U.S. EPA - CLP

^ 5A EPA SAMPLE NO.\( SPIKE SAMPLE RECOVERY _______

MU7113SLab Warns: SOUTHWEST LAB OF OK . Contract: 68-D9-0089 ((O-l-i*

Lab Code: SWOK . .. Case. No. : 34711 SAS No.: . t SDG No.: MU7101

Matrix: SOIL .. Level (low/med): LOW

"/. Solids -far Sample: 86.4


! Analyte

i AluminumI Antimony! ArsenicI BariumI Beryl 1 iumI CadmiumI CalciumI Chromium: Cobalt! Copper! I ranI LeadI Magnesium! Manganese! MercuryINickelI Potassium! Selenium! SilverI SodiumI Thai 1 ium! Vanadium! ZincI Cyanide;

ControlLimit

•/.R

75-1-2575-12575-12575-12575-125

75-12575-12575-125

-71=;.. i ••?'=:t j i ,«.<j

75-12575-12575-125

75-12575-125

75-12575-125'75-12575-125


54.09147.7060

472.977611.710415.. 5725

-64.2725116.-214565.0241

9.7315

331.3440.4897

147.9721

1.495412.5184

14.2963129.8186130.663815.2778

CSample

Result (SR) C

6.6l85!U1 .1574 I U

2 1.0 170 IB.7034 IB.6944 I U

i17.0509!3. -6856 IB7.4167!

ti7.4306!

!14 7". 5821"!

,OS57!U29 . 9677 !

j.6944 I U.6822 IB

{.6944IU

20-4112! ., 23.7738!

1.7071 !UI

SpikeAdded <SA>

115.749.26

462.9611 .5711.57

46.30115.7457.87

4.63,115.74

.44115.74

2.3211.57

11.57115.74115.7416.09

7.R

46 . 7- 33.297.695. 1

1 34 . 6

102.097.299.5

49.7

15S.8111.3102.0

64.51 02 . 3

123.694.592.495.0

11

DIM

:NRN I P"IFIPIP

NIPI WRIPIP

- IP!NR

N!F! NR

NIPICVIP1 NR

NIFIPINRIFIP| p

!C• i

Comments:


6T000403

A R I O f f i 7 9

U.S. EPA - CLPEPA SAMPLE NdT

6DUPLICATES

MU7103OLab Name: SOUTHWEST LAB OF OK Contract: 68-D9-0089



7. Solids -for Sample: 86.2 --7. Solids -f or" Dupl icate: 86.9

Concentration Units (ug/L or mg/kg dry weight >: MG/KG

i•! Analyte

I AluminumI AntimonyI ArsenicI Barium! BerylliumI Cadmium! CalciumI ChromiumI CobaltI Copper! IronI Lead! Magnesium! Manganese! MercuryI NickelI Potassium! Selenium! Silver! Sodium! Thallium! VanadiumI ZincI Cyanidet»

Control_ Limit

2.346.4

1160.1*? "T

11.65.8

'

,1..

~

476

Sample (S) C

4423.5200!6. 0325 I U2 . 7285 !

146.2281 I. 4584 I B.6961 IU

5587.1194!7-8639!21.876816 . 9089 !

11541.5730!3.7401!

449. 6563 IB1121.41-681

.0892 I U5.2697IB

260. 3555 IB.6961IU.5541 IB

147.0211 IB.6961,'U

9. 8577 IB17,011912. 2927 I Ui

» Ll ,

Duplicate (D) C'

4212.7347!6.0325IU3.7425!

152.1421 I. 5020 I B. 696 1 I U

3292. 1782!8.6496!23.7064!7 . 7052 !

12181 .7570!3.9165!

349. 9366 IB1017.3726!

.0967IU6.7687!B

298. 2839 IB. 5800 ! U-5915IB

211 .5406" IB.69.61 IU

10. 7300 IB18.6445!1 .8651 !Ui•

"

7.RPD

4.9

31 .34.09. 1

51 .79.58.010.95.44.624 .99.7

24.913.6

6.536 . 0

8.59.2

:""":o;;!;*;: t";I;;;I;Ij!;!;:,';;,1 —

M

F1PrpF'

HPpF' "FPPcvPF-C"

FP*-"FF'C

FORM VI - IN7/88

&-D00401

fU.S. EPA - CLP

5A EPA SAMPLE NO.SPIKE SAMPLE RECOVERY ______'

MU7103S .Lab Name: SOUTHWEST LAB OF OK Contract: 6S-D9-0089 MJ) - H ft •

Lab Code: SWOK ..— Case No.: 34711 SAS No.: SDG No.: MU7101

Matrix: SOIL . Level (low/mod): LOW

7. Solids -for Sample: 86.2 - -, , =- - - = - - - -:

Concentration Units (ug/L or mg/kg. ..dry., weight) : MG/KG .

1

Analyte

AluminumAntimonyArsenicBariumBeryl LiumCadmiumIpalcium '.fchromium^CobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSi 1 v<srSodiumThai 1 iumVanadiumZ-.1 n cCVAH ielt?

Control.Limit

-7.R

75-12575-12575-125TCT _ 1 <-ver/ wJ i. ji-wJ

75-125

75-125"7Cv_ 1 r>«=:/ »J — 1 oL»J

75-125

75-125

75-12575-125

75-12575-125

75-12575-125~7 ,~ \ Ri —i . 1 *- *J"/•=• i f fS'/ ..j— 1 *•:.«*


46.23256.5568

587.90291 1 . 403915.5720

55 . 67831 26 . 524O62.6472

7.4223

"7" 923.9978.4400

120. SI O2

1 .382812.1 7OO

12.0464123.6183

. _ 125.31941 8 . 3206

CSample

Result (SR>p

6 . 03252.7285

146.2281.4584.6961

7.363921 .87686.9089

3.7401

Tl2~i-416S..08925.2697

.6961

.5541

,69619.857717.01192.2927

C

U

BU

UB

UB

UB

U

. SpikeAdded (SA)

116.019.23

464.041 1 . 601 1 . 60

46.40116.0153.00

4.64:

,. i16^

- 40116.01

TI "T"?

11.60

1 1 . 601 16.01116.0118.53

" 7.R

39.941-395.294.4134.2

1 03 . 090 . 296. 1

79.4

-170.2110.099.6

59.61 00 . 1

103.893. 193.89R.7

Q

NN

N

N

M

NRPFPPPNRPPPNRFNRPcvPNRFPNRcr

PPC

Comments;


A-00040A R I O U 8 I


CLIENT: URS CONSULTANTS, INC. REPORT; 347if570 DELAWARE AVE.BUFFALO, NY 14202 DATEs 09-06-90ATTNs PETER FAIRBANKS

LABORATORY BLANK

SAMPLE MATRIX: SOIL SAMPLE AMOUNT: 30GSAMPLE IDs METHOD BLANK DILUtlON FACTOR: 1

DETECTION AMOUNT FOUNDCOMPOUND_______________LIMIT (mo/Kg)_______________dug/Kg)

TPH 10.0 ND


SAMPLE MATRIX: SOILSWLD # 3471.8, 9 (MS)PROJECT: DELAWARE SAND «t GRAVELSAMPLE IDi UD-7-10, UD-7-10 MS (MS)

SPIKE CONC. SAMPLE CONC.(•Q/Kg) (mg/Kg)*

MS CONC.(*Q/Kg)t

MS PERCENTRECOVERY

TPH 667 9560 9980 637.

SAMPLE MATRIXJ SOILSWLO # 3471.1O (MSD)PROJECTS DELAWARE SAND & GRAVELSAMPLE IDs UD-7-10 MSD (MSD)

9PIJCE CONC. SAMPLE CONC. RECOVERY PERCENT{•g/Kg) (mg/Kg>* DIFFERENCE

TPH 113OO 261 -122'/.

* « DILUTION FACTOR NOT APPLIED TO THESE CONCENTRATIONS

(3471.6) (3471.7)UD-11A-13 UD-11A-13 FIELD DUPSAMPLE CONC. DUPLICATE CONC RELATIVE PERCENT(•g/Kg) RECOVERY DIFFERENCE

TPH 2790 ' AR i 0 I l*82(2.B>0 OOO'iOG


CLIENT: URS CONSULTANTS, INC. REPORT: 3471©570 DELAWARE AVE.BUFFALO, NY 14202 DATE: 09-06-90ATTN: PETER FAIRBANKS

LABORATORY BLANK

SAMPLE MATRIX: SOILSAMPLE ID: METHOD BLANK

DETECTIONCOMPOUND LIMIT (ma/Ka)

TPH 10. O

TPH MATRIX SPIKE/MATRIX SPIKE DUPLICATE

SAMPLE MATRIX i SOIL^ SWLO # 3471.13, 14 (MS)P PROJECT: DELAWARE SAND & GRAVEL

SAMPLE ID: UD-7-12, UD-7-12 MS (MS)

SPIKE CONC. SAMPLE CONC. 1(•g/Kg) (Kg/Kg)*

TPH • 667 296

SAMPLE MATRIX: SOILSWLO # 3471.15 (MSD)PROJECT: DELAWARE SAND «e GRAVELSAMPLE ID* UD-7-12 MSD (MSD)

SPIKE CONC. SAMPLE CONC.(•g/Kg) (mg/Kg)*

1

SAMPLE AMOUNT: 30S"DILUTION FACTOR: 1

AMOUNT FOUND(ma /Kg)

ND

RECOVERY DATA

MS CONC. MS PERCENT(•g/Kg)* RECOVERY

935 967.

RECOVERY PERCENTDIFFERENCE

TPH 1013 107 -127.

* = DILUTION FACTOR NOT APPLIED TO THESE CONCENTRATIONS

(3471.li) (3471.12)UD-7-11 UD-7-11 FIELD DUPSAMPLE CONC. DUPLICATE CONC RELATIVE PERCENT(•g/Kg) RECOVERY DIFFERENCE

TPH 61 63 (3.2*01U83 6-00040 V

SOUTHWEST LABORATORY OF OKLAHOMA, INC1700 Wi Albany . Suite T . Broken Arrow, Oklahoma 74012 . 918-251-2858

CLIENT: URS CONSULTANTS, INC. REPORT: 3471g570 DELAWARE AVE.BUFFALO, NY 14202 DATE: 09-06-90ATTNs PETER FAIRBANKS

LABORATORY BLANK

SAMPLE MATRIX i SOILSAMPLE IDs METHOD BLANK

DETECTIONCOMPOUND LIMIT (M/Kd)

TPH 10.0


SAMPLE MATRIX* SOILSWLO # 3471.3, 4 (MS)PROJECT: DELAWARE SAND & GRAVELSAMPLE IDs UD-11A-12, UD-ilA-12 MS (MS)

SPIKE CONC. SAMPLE CONC. 1(•g/Kg) (wg/Kg)*

TPH 667 4250

SAMPLE MATRIX i SOILSWLO # 3471.5 (MSD)PROJECTS DELAWARE SAND & GRAVELSAMPLE IDs UD-11A-12 MSD (MSD)

SPIKE CONC. SAMPLE CONC.(•g/Kg) (Mg/Kg)«

SAMPLE AMOUNTS 30GDILUTION FACTOR: 1

AMOUNT FOUND(•a/Ka)

ND

RECOVERY DATA

IS CONC. MS PERCENT(•g/Kg)* RECOVERY

3730 -7B%


TPH 90 73 20.9


(3471.1) (3471.2)UD-llA-il UD-llA-il FIELD DUPSAMPLE CONC. DUPLICATE CONC RELATIVE PERCENT(•g/Kg) RECOVERY DIFFERENCE

TPH 90 73 ?0.9

A R I O I U 8 1 * n n 1 n

BOIL VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Name: 3UJL - TULSA__________' Contract: URS______

Lab Code: 5WOK Case No.: .URS SAS No.: ______ , SDG No.: __

Matrix Soike - EPA Samole No.: UD-14-9 Level:(low/med) LOW

COMPOUND

1 . 1-DichloroetheneTrichloroetheneBenzeneTolueneChlorobenzene

SPIKEADDED(ug/Kg,)

54.954.954.954.954.9

SAMPLECONCENTRATION

_( ug/Kg)

002 . 007.79O

MSCONCENTRATION

< ug/Kg)

49.743.350.954 . 048 . 2

MS•>/•

REC #

9179393433

QCLIMITSREC.

59-17262-13766-14259-13960- 133

COMPOUND

1 , 1-DichloroetheneT r I c h 1 or oe t hen eBenzeneTolueneChlorobennene

SPIKEADDED(ug/Kg _)

54.954.954.954.954.9

MSDCONCENTRATION

( u_g /Kg )

49.145.554.956.95O.5

MSD•/REC #

8933968992

'/.RPD 4*

'?-S-8-6-4

QC L]RPD

T"T?

24*? 1

2121

EMITSREC.

59-17262-13766-14259-13960-133

$ Column to be used to -flag recovery and RPD values with an asterisk


RPD: _0 -.put .o-f _5 .outside limits .] _ _ _ _ _ _ _ _ -,."_ _\^ _ .S D i k e Rec o ver v: _0 _. ou t of 10 outside limits

COMMENTS: UD-14-9 " URSINSTrl SWL83491.03 5

fc-00040_3-QRM III VOA-2 1/S7 Rev

f i R I O I U S S


Lab Name: SWL - TULSA____________ Contract: URS_______

Lab Code: SWDK Came No.: URS 3AS No.: ______ , SDB No.:

Matrix Spike - EPA Sample No.: UP-14-9 Levels(low/med) LOW

COMPOUND

Phanol2-ChloroDhenol1 ,4-DichlorobenzeneN-Nitromo-di-n-prop. ( 1 )1 .^-Trichlorobenzene^4-Chloro-3-m@thy 1 phenolAcentiDhthene4-Nitrophenol2.4-Dinitrotoluena ____PentachloroonenolPvrene

SPIKEADDEDC ug/Kg )

1470014700733073307330147007330147OO7330147007330

SAMPLECONCENTRATION

< ug/Kg )

O000

106000o00

MSCONCENTRATION

(ug/Kg)

9900968O51204730saoo1 04OO5140990052101150O5270

MS ! DC !'/: ! LIMITS!REC #! REC.

67 126- 9066 125-10270 123 10465 141 12673 133 10771 !26 10370 !:3I-13767 111-11471 !23- S973 ! 17-10972 135-142

*i

COMPOUND

Phenol2-Chloroohenoli ,4-DichlorobenzeneN-Nitromo-di-n-prop. ( 1 )1,2, 4— Trichlorobenzene—4-Chloro-3-methyl phenolAcenaphthene4-Nitro phenol2, 4-Dinitro tolueneP^ntachlorophenolPvr»n*

SPIKEADDED(ug/Kg )

1470014700733073307330147007330

i 470073301470O7330

MSDCONCENTRATION

(ug/Kg)

9090916046504340525096305O5093105200111005110

MSD<y

REC t

626 !635970666963717670

'/.RPD #

36U1011"»1

0^"

1

iiQC LIMITS^RPD 1 RECfl

35 126- 9050 125-10227 !2S 10433 141 12623 133 1O733 126 10319 131-137r'l '11 1 1 &ijV ill i 1 *T

47 ;2S-iS947 117-10936 135-142

i

< 1 ) N-Nitroso-di-n-propylamine

Column to b* used to -flag recovery and RPD values with an asteriskoutside o-f QC limits

RPD: _ 2. o"t o-f U outside limitsSpike Recovervs _ O out o-f 22 outside limits

COMMENTS: UD-14-9 URSINST:F SWLS3491.03

1 000410FORM III SV-2 1/B7 R'

ARIOU86


Lab Name: 5WL-TULSA______________ Contract: UR§_______

Lab Cdde: SWOK Case No.: URS3 SAS No.: ______ SDG No.:

Matrix Spike - EPA Sample No.;.UD-14-9 Level:(low/med) LOW

COMPOUND

qamma-BHC (Lindane)HeotachlorAldrinDieldrinEndrin4.4'-DDT

SPIKEADDED(ug/Kg )

RQ RhJO . *J

58.558.5146146146

SAMPLECONCENTRATION

( ug/Kg >

0O0O00

MSCONCENTRATION

(ug/Kg)

0O00o0

MS7.

REC #

O *0c>0oo

QCLIMITSREC.

46-12735-13034-13231-13442-13923-134

COMPOUND

gamma-BHC ( Lindane ) ___HeotachlorAldrinDieldrinEndrin4.4'-DDT

SPIKEADDED(ug/Kg)

58 • t-i\ifB • ij58.5146146146

MSDCONCENTRATION

(ug/Kg>

0o0000

MSD7.REC #

0 *0 #O *0 *0 *0 *

y

RPD #

00000o

QC LRPD

= = = =!»_•

50314338455O

EMITSREC.

46-12735-13034-13231-13442-13923-134


* Values outside of QC limits

RPD: _0 out o-f _6 outside limitsSpike Recovery i _12 out o-f 12 outside limits

COMMENTS:

6-000411FORM III PEST-2 . 8/87 Rev.

U.S. EPA - CLP- EPA SAMPLE N

6 _________DUPLICATES I

I MU9103DLab Name: SOUTHWEST LAB OF OK Contract: 68-D9-0089 ! aft - >V-<-J

cSBI


Matrix (water/Mil): SOIL Level (low/med): LOW

"/. Solids for Samples 91.1 . 7. Solids for Duplicate: 90.5


11

Ana 1 vte

AluminumAntimonyArsenicBariumBeryl liumCadmiumCalciumChromiumCabal t! Copoer! IronJLead! MagnesiumI Munasnss©I MercuryiNickel• Potassium! Selenium[Silver! Sodium! The! ] ium! Vanadium! Zinc _! Cyanide,•

ControlLimit \

"

2.2

5.4

—r

. 1

_

_..

4.3_

i«Sample (S) C!

•t2569.O449! !

5.6515IU!1 ,0868!U:

23.3026IB!. 3820 ! B !.6521 !U!

149.56101B!3.5462! !6.29341B!5.4353! !

7284.O824I !*•> s—H-l-TJ 1 t*£ • ji-.-'O i i

217.9826SB!92.4547! I

. 0955 J U !4.6413IB!

1 86. 0777! B!.4347 I U!.6561 IB!

S5,2482!B!.6521IU!

5 . 3869 ! B !10.3456! !1.6532IU!i i• '

!Duplicate (D) C!

2411 .4050! !5.6515!U!1 . 0868 ! U 122.3454 !B!.3607! B!.6521JU!

174.O6951B!3 . 3663 I !6 . 7556 1 B !5. 1 1&2IB:

6788. OOSO! !1.9346! !

211 .8332 IB!126.8023! !

. 09.§B I U !6. 9728"! B I

229.2743!B!.4347 I U:.6154!BI

104.7275 !B!.6521 !UI

5. 1559JB!1 0 . 0640 1 12.1191JUI

r iI i

i

3CRPD I

6.3!i!

4.2!5.7!

!15.1 15.2!7. 1 I6.0!7. 1 I13.9!2,9!

31 .71;

40 . i ;20. S!

!6.4!

20 . 5 Ir

4.4!<"> Q 1*_ . O i

t

ri

I

Q!M

IPIP!F;pIPIP!P ,IP !!P;p:P!FIP

* IP!CVr r"

I P

IFIPIPIKIPIF'1Ci. — * — .

FORM VI - IN7/88

£-000412

ARIOU88

U.S. EPA - CLP


Lab Name;: SOUTHWEST LAB OF OK Contract: 68-D9-0089MU9103S

Lab Code: STOK _ Case No_. : 34911 SAS No.: SDG No.: MU9101

Matrix: SOIL . . . . . . . ___^_ _ Level (low/med): LOW

7. Solids -for Sample: 91.1 ._ .

Concentration Units <ug/L or mg/kg dry weight): MG/KG

Comments:

1! Analvte

I AluminumI AntimonvI Arsenic1 BariumI Bervl 1 ium! Cadmium .! Calcium! Chromium.'Cobalt! Copper1 I ronI LeadI Magnesium! Manganese1 MercuryI Nickel! Potassium1 SeleniumISilverI Sod ium1 Thai lium1 VanadiumI Zinc1 Cvanirfe1

ControlLimit•/.R

75-12575--125"7 ,— 1 '"•»•=..' wJ i *.— J

75-12575-125

__°— i, ,it_j_. _

/ 5— 1 2575-125_

75—1 25

~rcj— 1 T112!

75—12575-125

TCT . -->Eri >J I *-*J

75-125

75—125T"1".——— r 1 ^CT' wJ J. i. wJ

"*'=:_- 1 *"?«:•• — J i -1. J7-5- 1 25


N.

V35.56864 . 0430

433.432510.43-5114.4747

46 . 6478105.4533.57.6631

7.9860

226.5150. 4757

. 105.7328

1 . 262910.3184

10.2423110.0543112.568622.7361

CSample

Result (SR) C

I5.6515SU1 . 0868 ! U

23 . 3O26 1 B: 3820 ! B.6521 !U

!3.5462!6.2934SB5 .4353 !

!.£ • iiilOO i

ii92.4547!

. 0955 I U4.6413JB

;.4347IU.6561 ,'B

!.6521 ! LI

5 . 3869 I B10.3456!1 , 6532 J U

*

SpikeAdded <SA)

109.77S . 70

439 . 031 0 . 9g10.93

43.91109.7754.33

4.35

1 09 . 77.46

1O9.77

2.1710.98

10. 37109.77109.7721 .61

7.R

32.4"46.593.4'91.6131.8

93.290 . 395.2

132.5

1 *-- . 1103.492.1

53.288.0

94.295.493. 1

l'^5J2

[; .

Q:M! NR

N 1 PNIFIPIP

NIPJNRIPIPIP!NR

NIF!NRIP'• CVIPIMF;

NIFIP:NRi p!P!P

_ 1C1

FORM V (Fart 1> - IN

A R I O I I . 8 9

6-000413

SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Suite "C1 . Broken Arrow, Oklahoma 74012 . 918-25J-2858

CLIENT: URS CONSULTANTS, INC. REPORTS 3505a570 DELAWARE AVE.BUFFALO, NY 14202 DATE: 09-06-90ATTN: PETER FAIRBANKS

LABORATORY BLANK

SAMPLE MATRIXi SOIL SAMPLE AMOUNT: 30GSAMPLE IDs METHOD BLANK DILUTION FACTOR: i

DETECTION AMOUNT FOUND_______________LIMIT (me/Kg)_______________(mo/Kg)

TPH 10.0 ND


SAMPLE MATRIX: SOIL .SWLO * 3505.01 (MB)PROJECT: DELAWARE SAND St GRAVELSAMPLE IDs UD-13-B (MS)

SPIKE CONC. SAMPLE CONC. MS CONC. MS PERCENT<»g/Kg) (MQ/Kg)* (mg/Kg)* RECOVERY

TPH 667 55 7OO 97'/.

SAMPLE MATRIX: SOILSWLO * 35O5.01 (MSD)PROJECTS DELAWARE SAND & BRAVELSAMPLE IDs UD-13-S (MSD)

MSD CONC. . PERCENT .(•g/Kg) RECOVERY

TPH 1100 157 -477.


! #'000414flRIOIi.90

SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Suite "C" . Broken Arrow, Oklahoma 74012 . 91&-251-28S8

CLIENT. URS CONSULTANTS, INC. REPORTS 3491a570 DELAWARE AVE.BUFFALO, NY 14202 DATEs 09-06-9OATTNs PETER FAIRBANKS

LABORATORY BLANK

SAMPLE MATRIX i SOILSAMPLE IDs METHOD BLANK

DETECTIONCOMPOUND LIMIT (ma/Ka)

TPH 10.0

TPH MATRIX SPIKE/MATRIX SPIKE DUPLICATE.... .._. _ .. . ...

SAMPLE MATRIX! SOIL^ SWLO * 3491.03, 04 (MS)B PROJECT! DELAWARE SAND & GRAVEL^ SAMPLE ID I UD-14-9, UD-14-9 MS (MS)

SPIKE CONC. SAMPLE CONC. 1(•g/Kg) (»g/Kg)*

TPH 667 25

SAMPLE MATRIX! SOILSWLO # 3491.05 (MSD)PROJECTS DELAWARE SAND Se GRAVELSAMPLE ID i UD-14-9 MSD (MSD)


SAMPLE AMOUNT: 30GDILUTION FACTORS 1

AMOUNT FOUND(mg/Kq)

ND

RECOVERY DATA

MS CONC. MS PERCENT(mg/Kg)* RECOVERY

607 377.


TPH 573 82 67.


(3491.01) (3491.02)UD-14-8 UD-14-B FIELD DUPSAMPLE CONC. DUPLICATE CONC RELATIVE PERCENT( mg / Kg) RECOVERY DIFFERENCE

TPH 3630 3260 LO.5^000415

1700 W, Albany . Suite "C" . Broken Arrow, Oklahoma 74012 . 918-251-2858

METHOD S TPH (FREON EXTRACTION; ANALYSIS BY IR)ANALYSIS DATE s 09/O7/90

LABORATORY BLANK

MATRIX : SoilSAMPLE ID. s S9LK09069001SAMPLE AMOUNT s 30G DILUTION FACTCR: i

i— IT"!I T C .n^ / *;Q ; ^ i mg / -s.u

TPH 1O.O 10.0 ND

MATRIX SPIKE/MATRIX SPIK'E DUPLICATE 'RESULTS

1574.05 1574.05MSCOMPOUND SPIKE CONC. SAMPLE CONC. MATRIX SPIKE ' PERCENT

(mg/kg) (mg/kg) * CONC. (mg/kg) * RECOVERY

TPH 667 0 600 90 '/.

1574.05MSDMATRIX SPIKE 1_DUPLICATE PERCENT RECOVERY PERCENTCONC. (mg/kg) * RECOVERY DIFFERENCE

TPH 590 88


DUPLICATE Sa^=LS SES'JLTS

COMPOUND SAMPLE CONC. DUPLICATE CONC. RELATIVE PERCENT DIFF(mg/kg) (mg/kg ) "/.

TPH .O

A R I O U 9 2


METHOD : TPH (FREON EXTRACTION; ANALYSIS BY IR)ANALYSIS DATE : 09/07/90

LABORATORY BLANK

MATRIX : SoilSAMPLE ID. : SBLK09069002SAMPLE AMOUNT : 30G DILUTION FACTOR: 1

CLIANT I TAT I ON AMOUNT crLIMIT {.Tig/kg) (mg/kg

TPH 10.0 10.0 ND



(mg/kg) (mg/kg) * CONC. ,(mg/kg') * RECOVERY

TPH 667 0 620 93 7.

1580.01MSDMATRIX 3=IKEDUPLICATE PERCENT RECOVERY PERCENTCONC. . tmg/kg) * RECOVERY DIFFERENCE

TPH • 630 94 -2 7.


RESULTS

COMPOUND SAMPLE CONC. DUPLICATE CONC. RELATIVE PERCENT DIFF(mg/kg) (mg/kg) 7.

TPH , .0


Lab Names SVJL-TULSA______________ Contract: URS_______

Lab Codes SUJDK Case No. s URS SAS No.: ______ SDG No. s

Matrix Spike - Er*A Sample No.s EID-16A-9____ Level:(low/med> LQW_

COMPOUNDB s s* at at ME a* ac K JB acjcac imm. ^ SE s scaE

Phenol2-Chlorophenol1 . 4-Dichloroben2ene ___N-Nitroso-di-n-prop. ( 1 )1 f 2,4-Trichlorobenzene_4-Ch 1 oro-3-me t hy 1 pheno 1Acenaphthene4-NitroDhenol2 , 4-Dini tro toluenePentachlorophenolPvrene

SPIKEADDED(ug/Kg)

_sa^ss____1450014500725O7250725O145007250145007250145OO7250

•

SAMPLECONCENTRATION

(ug/Kg )

OC)0000o000o

MSCONCENTRATION

(ug/Kg)ssss3&a::sai*aB3E3s=E

819075405020518047101O3004460776048608410514O

MS7.REC #

5652697165716254

' 67. 58/ 71 '

: QC :SLIMITS!! REC. !J 3=n=»== J

!26- 90 !125-102!128 104!141 126!138 107!!26 103!S31-137!! 11-114!!28- 89!! 17-109!' T«=;— , 1 d.T" 'i w*J i. •t*. i

I !

COMPOUNDKacsaacKVKxsEjESxmssssssaBEKSss:

Phenol2-Chlorophenol1 .4-Dichlorobensene ___N-Nitroso-di-n— prop. ( 1 )1 ?2.4-Trichlorobenzene_4-Chloro-3-methyl phenolAcenaphthene4-Nitroph«nol2, 4-Dini tro toluene ____PentachloroohenolPvrene

SPIKEADDED(ug/Kg)

;====:==== sss

145OO14500725072507250145007250145007250145OO7250

MSDCONCENTRATION

(ug/Kg)= =s == =====: s sssss:

812074OO5340547048OO1020O33907020473087705000

MSD7.

REC #=S=SS:=SB

5651747566704748656069

7.RPD #SSSS53S

0

2—7-5-21

"•Q +4.O +

123-33

DC LIMITSRPD ! REC.J

sssssss: J =ts====Jl

35 !26- 9050 125-10227 !28 10438 !41 12623 138 10733 !26 10319 131^13750 111-11447 !2S- 8947 117-10936 135-142

i

( 1 ) N-Nitroso-di-n-propylamine

Column to be used to -flag recovery and RPD values with an asteriskValues outside of QC limits

RPD: __ L °ut of 11 outside limitsSpike Recovery; _ Q_ out o-f 22 outside limits

COMMENTS : UD- 1 6A-9 URSSWLS3335 . 07 30B/O .9

FORM III SV-2 _— 1/87 Re

f l R I O; r


Lab Name: SWL-TULS_A_______________ Contract: URS_______

Lab Code: SUIQK Case No.: URS3 SAS No.: ______ SDG No.:

Matrix Spike - EPA Sample No.;' UD-16A-9 Level:(low/med) LOW

COMPOUND

qamma-BHC < Lindane )HeptachlorAldrinDieldrinEndrin4,4'-DDT

SPIKEADDED(ug/Kg)

57.857.857.8145145145

SAMPLECONCENTRATION

(ug/Kg)

000000

MSCONCENTRATION

( ug/Kg >

^_>2 . 975.045.711813080.7

MS7.REC #

5713079819056

! QC iJLIMITS;! REC. !

146-127!135-130!! 34-132!131-134!! 42-139!! 23-134!t ii *

COMPOUND

qamma-BHC (Lindane) ._._,HeptachlorAldrinDieldrinEndrin4, 4 '-DOT

SPIKEADDED(ug/Kg)

57.857.857.8145145145

MSDCONCENTRATION

(ug/Kg)

34.877.152.0139154105

MSD7.REC #

60133 *909610672

7.RPD #

-5-2-13-17-16-25

QC LIMITSRPD ! REC.

50 ! 46- 12731 135-13043 134-13238 ! 31-13445 142-13950 123-134

t


# Values outside of QC limits

RPD: _0 out o-f _6 outside limitsSpike Recovery: _1_ out of 12 outside limits

COMMENTS:

000419FORM III PEST-2 8/a7 Rev'

A R I O I U 9 5

U.S. EPA - CLP

LABORATORY" CONTROL SAMPLE

MAn>»- SOUTHWEST LAB OF OK Contract: 68-D9-0080

i. ,-)<-: 'P' _ Ca-,e No.: 33851 . 3A9 No . :__ W

Source:

! An-ilvtg»! Aluminum1 Antimo'-'vI Arsetn LC! Barium! Bervl lium! Cadmium* Calcium! ChromiumtCobaltI Copper! I ronrL^ad! Magnesium

on vumI Si 1 v*r! Sod i omI Thai 1 ium

! Z inc

Aqueous (ug/L)Trus Found 7.R

- _

_

-. . ._ .. t

Solid (mg/kg>True Pound C - Lin

325.0! 301 .5!211.0! 175.4!917.0! 1O40.8!4.8! 4.6JB19.4! 18.5!45.4! 45,2!

1 96200 . 0 ! 208300 » 0 I99.6! 84.1!144. Of 130.7!6910.0! 7324.0!22430.0! 13578.4!236.0! 272.5!

11S10O.O! 128860,0!SOS. 01 208. 1 !12.7! 10,6!60.9! 53,1 !50. O! 69.0 JU39.2! 43,4!T^ ^ i i e- E: ij .*l . A. i 1 -»J • wJ i50.0! 218, 9!B39.0! 44.4!65.8! 58.5!187'.0! 160.7!

5 • 6 i o . ••> iI !

"127.0\_ £33 . 0

0 . 0~" 16.5

-r F? -rw' u . /166SOO.O

7p.2124.060O6.017770.0

1 i-JQ . f"$1 0040O . ft

1 7.03 C T. uJ

" 49 . 20 . 019.1ir .*50 . 024.651 .7T3S.O

"- 4.3

FORM VII - IN7 • '88

6-000420A R I Q | L » 9 6

U.S. EFA - CLP .


,-rti I-TLII ICTCT r AC HP' nk" Contract: 6S-D9-OOQ9...ah" -.>m« : SOUTH WEST_ Lfto UP ur-. -<-" .

I *b r--c1«- -«'JOH. Case No. : 33851 _9A5_N_a^: ^_ "'C'

' Aqueous (ug/L)Analvts ! True .; Found _ 7.R

Aluminum 'Antimony '•Arsenic !F ;:? r- i 'j m ;L^rv-T ] .i rr, jCadmium . : . ..Calcium iChromium 1Cobalt !Copper :I rein !Lead .. !.Magnesium !Manganese 'Marcurv 'nickel iPotass iuim !'"pi an" turn !3 j 1 v P i" ;'-;r>r| i t .;t.

I "he- 1 1 ''.LlTt '.

Van^cl ium !7 1 *~i i~ i

,

-- - -

SolidTrue Found

— -

... . _.. ....

5.6

- — .- .

6 r »* ji.

(C

-

U

FORM VII - IN

L.imi t-

'000421A R I O U 9 7


CLIENT: URS CONSULTANTS, INC. REPORT: 3385a570 DELAWARE AVE.BUFFALO, NY 14202 DATEs 09-06-90ATTN: PETER FAIRBANKS

TPH 6iO 91% 2%


000422ARIOU98

LABORATORY BLANK

SAMPLE MATRIX s SOILSAMPLE IDs METHOD BLANK

DETECTIONCOMPOUND LIMIT (iw/Ka)

TPH . 10. 0


SAMPLE MATRIX j SOILSWLO ft 3385.12 (MS/MSD)PROJECT! DELAWARE SAND & GRAVELSAMPLE IDs UD-19-13 (MS/MSD)

SPIKE CONC. SAMPLE CONC. 1(•g/Kg) (-g/KgX

TPH 667 0

MSD CONC. MSD PERCENT(•g/Kg) RECOVERY

., -.

SAMPLE AMOUNT: 30GDILUTION FACTORS 1

AMOUNT FOUND(ma/Ka)

ND

RECOVERY DATA

IS CONC. MS PERCENT(Mg/Kg)* RECOVERY

620 937.


SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. AB>any . Suite "C* . Broken Arrow, Oklahoma 74012 . 918-251-2858

CLIENT: URS CONSULTANTS. INC. REPORT, 3368*570 DELAWARE AVE.BUFFALO, NY 14202 DATEs 09-06-90ATTNs PETER FAIRBANKS

LABORATORY BLANK

SAMPLE MATRIX: SOIL SAMPLE AMOUNT: 30GSAMPLE IDs METHOD BLANK DILUTION FACTOR: i

DETECTION AMOUNT FOUNDCOMPOUND_______________LIMIT fmq/Ko)_______________(mg/Kg)

TPH 10.0 ND


SAMPLE MATRIX a SOILSWLO * 3368.02 (MS/MSD)PROJECT: DELAWARE SAND & GRAVELSAMPLE IDs UD-21-12 (MS/MSD)

SPIKE CONC. SAMPLE CONC. MS CONC. MS PERCENT(•g/Kg ) (ng/Kg ) * (mg/Kg ) * RECOVERY

TPH 667 0 620 93%

MSD CONC. MSD PERCENT RECOVERY PERCENT( mg/Kg ) RECOVERY DIFFERENCE

TPH 64O 96V. 3'/»

* - DILUTION FACTOR NOT APPLIED TO THESE CONCENTRATIONS

000423A R I O U 9 9


CLIENT: URS CONSULTANTS, INC. REPORTS 3338a570 DELAWARE AVE.BUFFALO, NY 14202 DATEs 09-06-90ATTNs PETER FAIRBANKS

LABORATORY BLANK

SAMPLE MATRIXs SOIL SAMPLE AMOUNT: 308SAMPLE IDs METHOD BLANK DILUTION FACTOR: 1

DETECTION AMOUNT FOUNDCOMPOUND_____________LIMIT (mo/Kg)______________(mp/Ko)

TPH 10.0 ND


SAMPLE MATRIXs SOILSWLO # 3338.O4 (MS/MSD)PROJECTS DELAWARE SAND «t GRAVELSAMPLE IDs UD-23-10 (MS/MSD)

SPIKE CONC. SAMPLE CONC. MS CONC. MS PERCENT(mg/Kg) (mg/Kg)* (mg/Kg)* RECOVERY

TPH 667 0 59O 887.

* » DILUTION FACTOR NOT APPLIED TO THESE CONCENTRATIONS

6^0042-1A R I O I 5 0 0

3BSOIL VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Names SWL-TUL5A______________ Contract: URS ______

Lab Code: SWDK Case No. s URS SAS No.s ______ SDG No.:

Matrix Spike - EPA Sample No.: UD-26-9_____ Level:(low/roed) MED

COMPOUND

1 . 1-DichloroetheneTrichloroetheneBenzeneTolueneChlorobenzene

SPIKEADDED< ug/Kg)

76207620762076207620

SAMPLECONCENTRATION

(ug/Kg)

OO0

204OO• 0

MSCONCENTRATION

< ug/Kg)

913065707330291OO7470

MS I QC7. JLIMITS

REC ft! REC.

120 139-172B6 162-13796 166-142

' 114 159-13998 160-133

i

COMPOUND

1 9 1-Dichloroethene ____Tr'ichloroetheneBenzeneTolueneChlorobenzene

SPIKEADDED(ug/Kg)

7620762O762076207620

MSDCONCENTRATION

(ug/Kg)

9310688074503230O7770

MSD7.REC #

SSSSSS==5=

1229098156 *102

7.RPD #

_*5*£_ *=:*j-2-31 *-4

:QC LIMITSRPD ! REC.

22 159-17224 162-13721 166-14221 159-13921 160-133

*i



RPD: _1. out o-f _5 outside limitsSpike Recovery: _1_ out o-f 10 outside limits

COMMENTS: URS UD-26-9INSTsD SWLft3471.18 4 - - •

#-000425FORM III VOA-2 1/87 Rev,

A R I O I 5 0


Lab Name: 5VJL-TULSA______________ Contract: URS_______

Lab Code: SViQK " Case No.: URS SAS No.: ______ SDB No. s

Matrix Spike - EPA Sample No.s UD-26-10B L«v«li<low/med) LOW

COMPOUND

1 ,, 1-Dichloroethene ____TrichloroetheneBenzeneTolueneChlorobenzen*

SPIKEADDED<ug/Kg>

50.050.050. 050,050.0

SAMPLECONCENTRATION

(ug/Kg)

O00O0

t MS! CONCENTRATION1 < ug/Kg){ z»«mm=»««a«ats££

! 46.5* A"t nt *TO • *T

! 49.4I 42.5t 48.5ti

MS7.

REC ft

93B7Q /998597

1 QC !1LIMITS!I REC. !

159-1721» z,r* i T7 '

166-142!159-139!160-133!i ii i

II1 COMPOUNDI mmttmmmx'mmmmsxxsmmmmmmmmm\ 1 , 1-Dichloroethene ____! Trichloroethen*! Benzene1 Toluem*I Chlorobenzen*ii

SPIKEADDED(ug/Kg)

aCKBB^SS^aM

68.5OO . wt

68.568.568.5

MSDCONCENTRATION

(ug/Kg>sss atKKBBxaesses

64.762.171.462.969.3

MSD !% I 7.

REC #! RPD ftES33C3E3 { ES3EBSBB

94 ! -191 ! -4104 ! -592 ! -81O1 ! -4

i

QC LIMITS mRPD ! REC . 1

SSBSSiB } SZS53S=5J3 =

22 139-17224 162-13721 166-14221 159-13921 16O-133

i

# Column to b» used to -flag recovery and RPD values with an asterisk


RPDs _Q. out o-f _§. outside limitsSpike Recovery? _Q. out o-f 10 outside limits

COMMENTS:

00042tFORM III VOA-2 "* 1/87 Rev

A R I O I 5 0 2


Lab Names 5WL-TULSA______________ Contract: URS_______

Lab Codes SWDK Case No.: URS SAS No.: ______ SDG No.s

Matrix Spike - EPA Sample No.: UD-27-10 Level *(low/med) LOW

COMPOUND

1 ., 1-Dichloroetheng ____TrichloroetheneBenzeneTolueneChlorobenzene

SPIKEADDED< ug/Kg)

33.253.253.2*S;*T n.JO • *_ff f Owo . Z

SAMPLECONCENTRATION

(ug/Kg)

O0OOO

MSCONCENTRATION

< ug/Kg)

49.447.354.745.752 . 4

MS7.

REC ft

93891038698

QCLIMITSREC.

59-17262-13766-14259-1396O-133

1

1 SPIKE

COMPOUND=SS=S = S = »S=5=±=SS = ===SSS35=SSSS

1 , 1-Dichloroethene ____TrichloroetheneBenzeneTolueneChl-orobenz©ne

ADDED(ug/Kg)

====sss===

53.253.253.253.2

MSD ! MSDCONCENTRATION

(ug/Kg)==S = = = = =8 =B= !S = =5 ±=

30.247.055.848.431.5

%REC ft==ssss=94881059197

7.RPD ft

— — — =c==-11

— **?-61

QC LIMITSRPD

SESSSST3

2224212121

REC.==s:sss=

59-17262-13766-14259-13960-133

ft Column to be used to -flag recovery and RPD values with an asterisk

t Values outside o-f QC limits

RPD: _0 out o-f _J5 ' outside limitsSpike Recovery: _0, out o-f 10 outside 1 imits

COMMENTS:

£-000427FORM III VOA-2 1/S7 Rev,

A R I Q I 5 0 3


Lab Name: StgL-TULSA_______________ Contract: URS_______

Lab Codes SWQK .." Came No.: URS SAS No.: ______ ~ SDG No.:

Matriu Spike - EPA Sample No.s UD-26-9_____ Levels<law/med) LQUJ

COMPOUND

Phenol2-Chloraphenol1 f 4-Dichlorobenzene _ _____N-Nitroso-di-n-prop. ( 1 )1 ,2j4-Trichlorobenzene_^-Chloro-3-methyl phenolAcenaphthene4-Nitraphenal2 , 4-DinitrotoluenePentachloraphenolPyrene

SPIKEADDED< ug/Kg)

1630O1630O813O81308130

1 63003130

1 63OO81301 630O3 1 3O

SAMPLECONCENTRATION

(ug/Kg)

0• 0

0000000""00

MSCONCENTRATION

(ug/Kg)

952092705510586055401 0500595097605400137005990

MS7-

REC #

5857687263647360663474

QCLIMITSREC.

26- 9025- 1 O223 10441 12633 10726 1O331-13711-11423- 3917-10935-142

COMPOUND

Phenol2-Chl oropheno 11 ,4-DichlorobenzeneW-Nitromo-di-n-prop. ( 1 )t ?2.4-Trichlorobenzene__4-Chloro-3-me thy 1 phenolAcenaphthene4-Nitrophenol2 , 4-Dinitrotoluene ____PentachlorophenolPvrene . .

SPIKEADDED(ug/Kg)

1 63001 63003 1 3O81303130163008130163003130

1 63003130

MSDCONCENTRATION

(ug/Kg)

935039506OGO55805580.106OQ5970

1 1 6005180115006150

MSD7.REC #

575575_:6969657371.647176

7.RPD *

j-j4

-104

—•* 1— '"?O

— 1 "7— 1 /•J>17-3

.

QC L]RPD

35502733TT*- -

1950474736

MITS mREC.

26- 9025-10228 1O441 12633 10726 1-0331-13711-11423- 3917-10935-1*2

<1) N-Nitro*o-di-n—propylsmine

# Column to be- used to -flag recovery and RPD values with an asterisk* Values outside o-f QC limits -~:

RPOs _£. out of 11 outside limitsSpike Recovery: _0 out o-f 22 outside limits _._ ___ '__

COMMENTS: UD-26-9 URSSWL#3471.ia 306/0.9

6^00042,FORM III SV-2 - 1/87 Rev

10 I 501*

3DSOIL SEMIVOLAT:LE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Name: SWL-TULSA_______________ Contract: URS_______

Lab Code: SUJOK Case No.s URS 3AS No.: ______ SDG No.s

Matrix Spike - EPA Sample No.: UD-27-10____ Level:<low/med) LOW

COMPOUND

Phenol2-Chlorophenol1 . 4-DichlorobenzeneN-Nitrosa-di-n— prop. < 1 )1 .2.4-Trichlorobenzene_4-Chloro-3-methy 1 phenolAcenaphthene4-Nitrophenbl2.4-Dinitrotoluene .PentachlorophenolPvrene

SPIKEADDED(ug/Kg)

142OO14200 -71OO710O •7 1 OO142007 1 001420071001 42OO7 1 OO

SAMPLECONCENTRATION

(ug/Kg)

0bo0 _ _0 ________00ooQ

o

MS-CONCENTRATION

(ug/Kg )

809072405150.48905150915051409930453094405120

MS7.

REC #

5751736973647270 -646672

QCLIMITS

REC.

26- 9025-10228 " 10441 126,33 10726 10331-13711-114'">Q_ GO^.O C T

17-10935-142

COMPOUND

Phenol2-Chlorophenol1 ,4-DichlorobenzeneN-Nitrc'50-di-n-prop. ( 1 )l.,2.,4-Trichlarabensene_4-Chloro-3-me thy 1 phenolAcensDhthene4-Nitrophenol2, 4-DinitrotoluenePentachlorophenolPvrene

SPIKEADDED< ug/Kg)

1420014200710071OO7 1 00

1 420071001420O7100142007100

MSDCONCENTRATION

< ug/Kg )

766069904790465048207590472098604310103005090

MSD.//«REC #

54"49676568536669617372

/*RPD ..

ij496719915

-100

QC LRPD

35SO2738T*^-

1950474736

LMITSREC.

26- oo25-10223 10441 12633 10726 10331-13711-11428- 3917-10935-142

(1) N-Nitroso-di-n-propylamine . " "

4. Column to be used to -flag recovery and RPD values with an asterisk* Values outside o-f QC limits

RPD: _0. out o-f .11 outside 1 imitsSpike Recovery! __O.'out of 22 outside limits

COMMENTS: UD-27-10 URSSWL#347i.28 30S/0.9

6- 000429FORM III SV-2 , 1/87 ReVl

A R I O I 5 0 5


Lab Name: Sl-JL-TULSA_______________ Contract: 69-D9-OO25

Lab Code: SWOK Case No.: URS1 SAS No.: ______ SDG Mo.: __

Matrix Spike - EPA Sample No. ;* UD-26-9____ Level:<low/med) LOW

COMPOUND

gamma-BHC (Lindane)HeptachlorAldrinDieldrinEndrinA 4, * — nnT•T * " r u 1-1 <

SPIKEADDED< ug/Kg)

IE S SSffi 3SS3S IS

64.964.964.9162162lO-i

SAMPLECONCENTRATION

(ug/Kg)

00O0o

MSCONCENTRATION

< ug/Kg)_EKSSSSafaaE.___

7.5625.64.22

,46.928.8oo • v

MS7.REC #

12 *397 *29 *IS *51hj

QCLIMITSREC.

46-12735-13034-13231-13442-139~?T 1 TA

Jf! COMPOUND

I gamma-BHC (Lindane) ___} Heptachlor1 Aldrin! Dieldrin! Endrin! 4,4'-DDTii

SPIKEADDED< ug/Kg)

64.964.964.9162162162

MSDCONCENTRATION

(ug/Kg)

6.4241.06T"l. £.£.

26.920.448.5

MSD7.REC #

ssaeassKttaa

10 *6310 *17 *13 *30

7.RPD #sseses

13-47 *— •.> -jt52 *3252 *

QC L3RPD

503143384550

i

[HITS MREC V

46-127!35-130134-132!31-134!42-139!23-134!

ii


* Values outside o-f QC limits . _ -T

RPD: _5 out o-f _£. outside limitsSpike Recovery: _§. out o-f 12 outside limits

COMMENTS:

FORM III PEST-2 8/87 Re


Lab Names SWL-TUL5A_______________ Contract: 69-D9-O025

Lab Code: SWOK Case No.: UR51 SAS No.: ______ SDG No.: __

Matrix Spike - EPA Sample No.: .UD-27-10 Level:(law/med) LOW

COMPOUND

gamma-BHC (Lindane ) ___HeptachlorAldrinDieldrinEndrin4. 4 '-DOT

SPIKEADDED(ug/Kg)

56.656.6«j6 • 6

1 AO1 *r«i142142

SAMPLECONCENTRATION

< ug/Kg)

O00

O0

MSCONCENTRATION

(ug/Kg)

4.0517.44.3710.412.315.4

MS*/REC *

7 *31 *9 X7 *9 *11 *

C1CLIMITSREC.

46-12735-17034-T3231-1344^-13?23-134

COMPOUND

gamma-BHC ( Lindane ) ___HeptachlorAldrinDieldrinEndrin4, 4 '-DOT

SPIKEADDED(ug/Kg)

56.656.656.6142142142

MSDCONCENTRATION

(ug/Kg)

"_ -."?•

15.92.388.4911.015.7

MSD7.REC #

4 *28 *4 *6 *3 *11 *

7.RPD *

55 *1O77 *151 *">i *.0

QC LIMITSRPD

503143'384350

REC.

46-12735-13034-13231-13442-13923-134



RPD: _2 out of _6 outside limitsSpike Recovery: 12 out of 12 outside limits

COMMENTS: ~

#'000431FORM III PEST-2 8/87 Rev,

A R I O I 5 0 7

U.S. EPA - CLP

5ASPIKE SAMPLE RECOVERY

/-' 5A EPA SAMPLE NO.

b Warn*?: SOUTHWEST LAB OF OK Contract: 68-09-0089MU7113S

I PH Cod*?: SWQf Case No.: 34711 SAS No.: SDG Nc.: MU7101

Matri:;: SOIL -_=_ - - Level f. lo-'/.i^d) : LOW

:-, "Solid-. *'jr .Sample: 82.1

Concentration Units (ug/L or mg/kg dry weight,1: HG, ! 0

FORM V (P^rt 1) - IN

'i~c nt.rolI Limit

An*l V* ' v.f,

A 1 UTU n "n ,

A f e& n i r: 1 ~^~ 1 25Barium ;~*5-l25fervl liL'rr.: '- -T^5.rsdmutm ; 7"> IT5-!>lCJViH ICht omj ..in :"!a-l15Cn-bal t : 'n~lT3Copo^r ; '5—125Iron :L^adM U'T ^ ' ' *n .'M^na-s'.na^s;M^rcur*. I 5-1 _'5Nact *1 I -I'- ITS

Sp*lPnI.'.]nffl;7 --l25'« ; 1 s£*t ' "*"i--1 2r^

ThtlVTM.!* : -r-trJ• 'nnMM iM^ : r»-t r:s^.trr. I -'".— i 2Sc ^-n.i- : •":--! 25

Spiked SamoleResult CSSP) C

41 . 1 166!. 12.3331 !525.33001.. 12.0°1 I I .

1- . _ 16,62241!

63.6065!.124.9619;71 .06251

I12-8867!

*422.340OI

. 63BO !.125.0394!

1 .4519!13.5486!

11 .1011 !145.3405!3 44.6271 !22.8327!

SampleResult <SR>

9.339S10.3~7fc44.4749

.72'T9

.7236

13. 197116.04499,2119

21 .5463

564 . 0334. 105°

1 2 . 048 1

.72361 . 1739

. ?23627. O 4 283O.54352 i 2308

C

B

BBU

U

UB

U

LI

SpikeAdded (SA)

~ 121. SO^ . 74

_.407.7lj__ji2. j_e

12. t -3

: 4S . 72• 121 . «'"•..„. .60.90

4 . B7

^ 121 .80.58

121 .60

" J 2.441 _ _ _^j

'. 1 2 . i y121. PO

_--| 71 .;:••:

" ;• .1 . c .'•-

26 ."0Z;5 . 6•?8 . S03-4-3

1 36 . 5

103.5g-~. /IU'l .6

-'-177.9

- 1 .1 '. ,-31 1 o :. o92 .-?:

59.51 0 1 _- ii

91 . 1" 97. I

. * i ~*tM7._o

;p; PIIP

i : MRIP1 F':r

; CV

1MR

:p:NR: i:; p! '''":c

/HJ00432

U.S. EPA - CLPEPA SAMPLE MO.

6 ______DUPLICATES

Lab Name: SOUTHWEST LAB OF OK = Contract: 63-D9-OO89MU711BD

Lab Code: SWOK ..Case No.: 34711 SAS No.: SDG No.: MU7101

Matrix (water/sail): SOIL Level (low/med): LOW

"/. Solids -for Sample: 82.1 7. Solids -For Duplicate: -81.0


Ana 1 y te

AluminumAn timonyArsenicBariumHery 1 ]. iumCadmiumC^ 1 ciumChromiumCobal tCopperIronLeadMagnesiumManganeseMercuryNickel 'PotassiumSeleniumSi 1 verSodiumThai liumvanadium .ZincCyanide

Control. Limit

2 -:4_

_ _

12, 16.0

.7

.

9.6

... . _.

1 1i _ . i

^ J . • rfw

Sample (S) C

7833.2704!9. 3898 IB

10.. 3376!44. 4749 IB.7279 IB. 7236 ! U

197. 3684 IB13. 1971 I16.0449!9.21191

20811 .4500!21.5468!613.1355IB564.0384!

.105911112.0481 !

644.2161 IB_7236!U

1,1 738 IB128.6036IB

,7236 I U27.04281

. . . . . 30.5435!T> *TJT/"iQ ' 1 1*L . 'l_*U I U

I

_

Duplicate (D) C

83 1 0.0.1 Z6 !9 . 06~07 ! B7.96351

41 .999019. 7577 I B-730S.IU

296. 6852 IB12.2747!18.837619.31551

13275.2110117.0767!

7S4.9454IB1269.9271 I

. 1 1 60 ! U1 1 . 589-9 !

820. 7474 !B. 7303 ! U

1.316.513109.05M IB

. 7308 I U25.4772!29.6771 I2 . 3069 I U

c

"/.RPD

5.93 . 625 . 9

. 5.74 . t..-

40 .2~7 '"*

16.01. 113.023 . 124.677 . 0

3 . 924. 1

11 .516.5

6 . 0n .£?

O1

M !

P !F' 'F ;P !p :p ;p :p :P !p :P !F ;P !P !CV!P !F' !F !P iP \F "!p" jP !C i

ii

FORM VI - IN7/88

,VOOU433

U.S. EPA r CLPEPA SAMPLE NO

6 ______DUPLICATES !

! MU7128DLab Name: SOUTHWEST LAB OF OK Contract: 6S-D9-OOB9 ! u£>-_n-/g

Lab Code: SWCJK Case No.: 34711 SAS No.: SDG No.: MU7101

Matrix (water/soil): SOIL Level <law/med): LOW

7. Solids -for Sample: 94.8 7. Solids -for Duplicate: 94.3

Concentration Units (ug/L or mg/kg dry weight)

It

I Anal vte»i! Aluminum! Antimony! Arsenic! BariumI Beryl lium! CadmiumI CalciumI Chromiumt Cobalt! Capper1 IranJLeadI Magnesium! Manganese! MsrcuryJNickel! Potassium• SeleniumISilver* SodiumI Thai liumI VanadiumIZinc! Cyanider<

ControlLimit

*? 1JL • i

2. 1_z-

-5.3

.6~

4.31.8

iiSample (S) C!ii

2237.6733! I5. 7920. B!2.4123! !26.5101 ,'&{

T?'~>O i D '• .ri- •_•-£. V t C* i

. 63931 U I353. 1672! B!4.33031 I1O.44O8IB!7.4102! I

4191.7016! !2.310O1 !

201 .5872JBI876.55601 !

.0811 !UI4.0951 !B!

255. 6604 !B!6 TOT MMO"vO i U t

.4262!U!100. 6810! BI

-6393IU!7. 4847! B!10.2730! !1 .7818IU!

t ii i

Duplicate CD)

1964.4591"5,54062.371824.4178

.2147

.639314O.76983.3664

1 O . 56 1 57.3503

3685:40941.7496

142.7607860.8634

. 07274.00O4

204 . 292" r3.1965.4262

109.7973.6393

6.4405" 9 . 35521.5513"

C

U

BBUB

B

B

UBBUUBUB

U

7.RPD

13.0200 . 0

1 .73.2S. 1

36 . 025 . 01 . 1S

12.627.634.21 .3

o ~~oo *

3.7

15.04.2

a M

ppFP~PPPPF'PPFPF-cvPPFPPFPPC

MG/KG

FORM VI - IN7/83

.-,,,-,0434

U.3. EPA -. CLP .. _ -' ;

5A EPA SAMPLE NO.SPTKC SAMPLE RECOVERY . _ , _ ... ..__________

«! MU712G3

Lab N^m^: ?0'JTHWES.T. LAB OF OK . Contract: 6S-D9-CPS9 ! U0-*1-l3*

f-Jo.^ _ ,.Sp? JJc.: MU7101

rix: SOIL _ .. Level (,low/med^: LOW__

o]Jr*-= +^r Sample: 4.8 . . _.. _ _ __ _ _ _ _ . . _ _...:..._ _

Units (^y/M.cr_m2^^g_^r

Ana] vte

Ant i.monvAi —;>"•: ! i cr-< -4 r j i.( iii!;,».,,. 1 1 ^ .,,.,

r.V.imUimr,. ! r- i ..;:,

r.; '•-. com iumCobalt.CopperIron ...Lead . . . . .Msan«?siumM*na-ane.->**M^rcurv.Mi-l-t?!

S*1? 1 G? n i_uf7.c. •; . VFVJ-" --::v--..d,l i.'mTh,-\l 1 iumV fin ad turnJI A fir - —— - -

Cx-*ni.:1P

:' , -n l-r.-.l

Limit.";R

r«:.--i257P-12571™- t:':::7':::i — t i"!7T"75-125

75™L2.575- 1. 25 -•75-125::.75-125 ...

-7^-125

7 -12575-125

75-1.2575-125---'5-1257?- 125

Spiked Sample.Resuilt (SBP:)

77.5663—. B.7Q40„-. 4 r. 1.7151— 1.0— -1 f!73

14.7282

•7.439311.1 .0&3-9.57.8774

.6.2460

- - - 947.3352. 400 1

10:5 .,0147

1 . 30501 1 .2425

_. _.14.9810113,9135111.415514.3221

--

C

.. --.-.... _ _

Samp] e -..._.R.€is.Lili,../,SR). : .Q

0.7<?2o!l.2. 4 123!

".". .^-PfO.UT-t. 7 ""2 9 t F'.. o.v_V-Ji i 1 •

i'.J-r —r ,-. — (

- .-• _•' .' -,..' 1

1 o . 4408 ! P...... _7 .•._?_! 02 :._

i2.3100 I

!"7A,556rJ.!

. .03.11 ;y

,4262!U!

.6393! U7. 4347 IB

.10.2730!.

- - - ' - - - - , ; |

Spike : ; : ..-Add^d _. SA )_ ! _ %K . I Q : M

1 ' I

^O^.-.SS!" '67.4 !.M[r .,_-} .-.'2 i 7^ - y ; Mi !••

•a :i6. ::'"*! . 97.9; ;F:-l'"r; ^ ; "3.5"! ! Pl'>.^,: 13B.2!N!P

! ! I hJFi'd'"- i , "'• r 1 f 1 1 1 ' * P'-:_ . -'.. '• -t t - .' • ' ."

• 106.5'o-i . .:. 94.4 ! !P_ .S3.2SI .... ..73-S! LP .

; i 1 1 IF.- 4.2.6! 92,4! ..!F

; : IMP:'106.55: 6-S.4 I I !•'

. 3-6 I J t i . 1 I i '"'•',._iA06.5ri: ... :?4,/L;:!!

"" : 2/13! 34.7! I r10.66! 1.0?. 5! ._:.r

! ! ! NR10-66! 14 0.3! N I F ,106.55! P9.?:._JP_106.55! 94.9! IP

; 1.5. -"0 1 ' ?i..r; :c .i • '

FORM V (Part 1) -

ARI 0 I 5 I I

U.S. EPA - CLP

7LABORATORY CONTROL SAMPLE . . ..

Lab Name: SOUTHWEST LAB OF OK Contract: 68-D9-0089

Lab Code: SWOK Case No.s 34711 SAS No.: SDG No.: MU7101


Aqueous LCS Sources

1

1! Analyte

! Aluminum! Antimony! ArsenicI Barium! Beryl 1 ium! Cadmium. Calcium! Chromium[CobaltICopper! Iron! Lead! Magnesium! Manganese! Mercury! Nickel'! Potassium! Selenium! Silver! SodiumI Thallium! v>n*dxumIZinc! Cyanide

_ _Aquvouc ( ug /L )

True Found %R

-

.

- -

~

.

__ ._.

"

•

Solid (mg/kg)True Found C Limits "/.R

325 . 0211 .0

. 917.0• 4.819.445.4

196200.099.6144.0

6910.022430 . 0236 . 0

118100.0208.012.760.950 . 039.2*_>*_> *>50 . 039 . 065.3187.05.6

263.7142.6887.45.217.947.0

177133.5100.4147.9

6911. B20269.2248.9

120224.5209 . 511.967.369.023 . 917.373.423.460.5189.66.4

B

U

U

225.0_127.0635 . 00 . 016.535.7

166800.079.2

1 24 . 06006.017770.0

188.010O400.0

1 77 . 08.5

: 49.20 . 019.115.50 . 024.651.73.38.04.3

424.0294.01199. 040.0-i-i » '-•rrer *

225600.0120.0162.0

7S2O . 027030 . 0285. 0

12990O.O239 . 017.072.6

1000. 059.429 . 0

1000. 053 . 579.9236.0_ 6.9

Bl. 167.696.3108.3

t"*1U3 .-- - H70 i l

1 OO . 8102.7ioo.o90.4

1 05 . 5101 .8100.793.7110.50 . 0

61.077.90 . 072.891 .9101.41 14.3

FORM VII - IN7/93

flRIOI5'2

U.S. EPA - CLP


Lab Name: SOUTHWEST LAB OF OK ". - .Contract: 68-D9-0089

Lab' Code: SWOK Case No.: 34711 SAS No.: SDG No.: MU7101f

Solid LCS Source: EPA0287» _

Aqueous LCS Source: . . " . * . .

Aqueous (ug/L)True Found Y.R

-

___

__ _. _

...

Solid < mg/kg )True Found C Limits "/.R

5.6 6.4

_ . _ . , r __

i

4. 3

'

6.9

"

114.3

FORM VII - IN 7/ea

AR 101 51 3 £-OOU4o'<


CLIENT: URS CONSULTANTS, INC. REPORT: 347id570 DELAWARE AVE.BUFFALO, NY 14202 DATE: 09-06-90ATTNi PETER FAIRBANKS

LABORATORY BLANK

SAMPLE MATRIX: SOIL SAMPLE AMOUNTS 30BSAMPLE IDs METHOD BLANK DILUTION FACTOR: i

DETECTION AMOUNT FOUNDLIMIT (im/Kg) ____

TPH 10.0 ND


SAMPLE MATRIX: SOILSWLO * 3471.18, 19 (MS)PROJECT j DELAWARE SAND le GRAVELSAMPLE IDs UD-26-9, UD-26-9 MS (MS)

SPIKE CONC. SAMPLE CONC. MS CONC. MS PERCENT(•g/Kg) («g/Kg)ft (mg/Kg)* RECOVERY

TPH 667 0 596 897.

SAMPLE MATRIX: SOILSWLO # 3471.20 (MSD)PROJECTS DELAWARE SAND Se GRAVELSAMPLE ID i UD-26-9 MSD (MSD)

. flPIKE CONC. SAMPLE CONC. RECOVERY PERCENT(•a/Kg) (»g/Kg)t DIFFERENCE

TPH 596 89 0%


(3471.16) (3471.17)UD-26-8 UD-26-8 FIELD DUPSAMPLE CONC. DUPLICATE CONC RELATIVE PERCENT(•g/Kg) RECOVERY DIFFERENCE

TPH <1O <10 A R I O I 5 U


CLIENT: URS CONSULTANTS, INC. REPORTS 3471b570 DELAWARE AVE.BUFFALO, NY 14202 DATEs 09-06-90ATTN: PETER FAIRBANKS

LABORATORY BLANK

SAMPLE MATRIX: SOILSAMPLE IDs METHOD BLANK

DETECTIONCOMPOUND LIMIT (mg/Ko)

TPH 10.0

m DUPLICATE

(3471.21)UD-26-10SAMPLE CONC.(•g/Kg)

SAMPLE RESULTS

(3471.22)UD-26-10 FIELDDUPLICATE CONCRECOVERY

SAMPLE AMOUNT: 30GDILUTION FACTOR: 1 '

AMOUNT FOUND(mc/Ka)

ND

DUPRELATIVE PERCENT

DIFFERENCE

TPH 47 21 76.57.

#-"000439

fiFUOISIS

SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Suite "C* . Broken Arrow, Oklahoma 74012 . 918-251-2858

CLIENT: URS CONSULTANTS, INC. REPORT: 347la570 DELAWARE AVE.BUFFALO, NY 14202 DATEs 09-06-90ATTN: PETER FAIRBANKS

LABORATORY BLANK

SAMPLE MATRIX: SOILSAMPLE IDs METHOD BLANK

DETECTIONCOMPOUND LIMIT (wg/Ka)

TPH 10.0

DUPLICATE SAMPLE RESULTS

(3471.26) (3471.27)UD-27-9 UD-27-9 FIELDSAMPLE CONC. DUPLICATE CONC(•g/Kg) RECOVERY

SAMPLE AMOUNT: 306DILUTION FACTOR: 1

AMOUNT FOUND(*a/Ka)

ND

DUPRELATIVE PERCENT

DIFFERENCE

TPH 695 660 5.2V.

£-000440


CLIENT: URS CONSULTANTS, INC. " REPORT: 347Ic570 DELAWARE AVE.BUFFALO, NY 14202 DATE: 09-06-30ATTN: PETER FAIRBANKS

LABORATORY BLANK

SAMPLE MATRIXs SOILSAMPLE IDs METHOD BLANK

DETECTIONCOMPOUND LIMIT <ma/Ka)

TPH 10.0

SAMPLE AMOUNT: 30GDILUTION FACTOR: i

AMOUNT FOUND(mq/Kg)

ND


^ SAMPLE MATRIXs SOIL• SWLO * 3471.28, 29 (MS)W PROJECT: DELAWARE SAND «t GRAVEL

SAMPLE IDs UD-27-10, UD-27-10 MS (MS)


TPH 667 0

SAMPLE MATRIXs SOILSWLO # 3471.30 (MSD)PROJECT; DELAWARE SAND & GRAVEL

. SAMPLE IDi UD-27-10 MSD (MSD)

SPIKE CONC. SAMPLE CONC.(•g/Kg) (aig/Kg)*

MS CONC. MS; PERCENT(mg/Kg)* RECOVERY

639 96'/.


TPH 595 89 77.

* - DILUTION FACTOR NOT APPLIED TO THESE CONCENTRATIONS


TPH <10 <10 fl n l n-i-r—.-* ° r\flR 101^ 17 fi'(K»U44l


Lab Name: SML - TULSA_____________ Contract: URS_____.

Lab Code: SWOK Case No.: ORS. SAS No.: ______ SDG No.:

Matrix Spike - EPA Sample No.s UD-2S-8______ Level:Clow/med) LOW

COMPOUND

1 . l-0ichloroeth^neTrichloro^thgneSenr^n©TolueneChlorobenz^ne

SPIKEADDED(ug/Kg)

54.954. <£54.954.954.9

SAMPLECONCENTRATION

(ug/Kg >

0004.360

MSCONCENTRATION

( ug /Kg >

47,644.550 . 455.451 .2

MS

REC #

3781292QT

QCLIMITS

REC. .

59-17262-13766-14259-13?6O-133

i

COMPOUND

1 , 1-Dichloro^th^n^Trichloro^thgn©BenrengTolu^nMChlorob©nr§n©

SPIKEADDED(ug/Kg )

54.954.954.954.954.9

MSDCONCENTRATION

(ug/Kg)n . . .50.748. 153.458.654.1

MSD

REC ft

* 2S397 j9899

'/. ! QC L3RPD tt! RPD

.*..s____ , _—_i. i T">O i — -

-8 ! 24— =: ' "• 1•~*j i — i-6 : 21-6 ; 21

1

[MITSREC.

5.9-17262-13766-14259-13960-1T.3

tt Column to bm ummd to -flag recovery and RPD values with an asterisk

* Values outside o-f QC limits "

RPD: _O out of __J outside limits :^DII e Recovery! _0. out o-f 10 outside limits

CDMMENTS s UD-28-S URSINSTtl SWL#3491.08 5 . I"

-00044.FORM III VOA-2 1/37 Pev

ARI 01 5 1 8


Lab Name: SWL - TULSA_____________ Contract: URS_______

Lab Code: 5U1DK Case Jvlo. : URS S'AS No. ; SDG No.:

Matrix Spike •- EPA Sample No.: UD-28r-10 -__-- ..Level.: ( low/med) LOW

COMPOUND

1 . 1-DichloroetheneT r i c h 1 o roe t heneBenzeneTolueneChlorobenzene - — -

SPIKEADDED(ug/Kg)

352352-352 - ..352715

SAMPLECONCENTRATION

< ug/Kg)

O0

*"? 1 T

5470

MSCONCENTRATION

(ug/Kg )

7*42302T./JI5

449

MS

REC tt

1~i~73689-28 *95

QCLIMITSREC.

59— i 7262-13766-14259-13960-133

COMPOUND

1 . 1-DichloroetheneTri'chloroetheneBenreneTolueneChlorobenrene ~

SPIKEADDED< ug/Kg)

34234234234-2342

MSDCONCENTRATION

(ug/Kg >

247264314890277

MSD*/

REC _tt

72"77

361 OOai

y.RPD tt

30 *11~>

-356 *16

QC LIMITSRPD ! REC .

22 '59-17224 162-13721 166-14221 159-13921 ! 60- 133

r


* Values outside o-f GC 1 imits

RRD: _2 .out of ' j outside 1imitsSpike Recovery: __1_ out o-f 10 outside I imits

COMMENTS: UD-2B-10 URS _ _ _ . . .INSTiI SWL83491. 13 1

6-000443FORM III VOA-2 1/37 Rev

f l R i O i 5 T 9 "

3DSOIL SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVER*

Lab Name: 5VJL - TULSA____________ Contract: URS_______

Lab Codes SWOK Came No.: URS SAS No.: ______ . SDG No.:

Matrix Spike - EPA Sample No.: UP-28-B_____ Level:<low/med) LOW

COMPOUND

Phenol2-ChloroDhenol1 ,4-DichlorobenseneN-Nitroso-di-n-prop. ( 1 >1 f2f 4-Trichlorob©nrene_4~Chloro-3-methyl phenolAcenaphthene4-Nitraohenal2, 4-Dini tro toluene ____PentsichloroDhenolPvrene

SPIKEADDED(ug/Kg ) *

147001 47OO733073307330147OO7330147007330147007330

SAMPLECONCENTRATION

(ug/Kg)

00000.0Q

0ooo

MSCONCENTRATION

(ug/Kg )

92408800442044_7050 1 0880047101040O5OOO98206080

MS

REC *

636060616B606471686783

DCLIMITSPEC,

26— 9025- 10223 1 0441 12633 10726 10331-1371 1-11423- 391 ~? - i f.i— B1 _ i /! _• J — 1 -i.

COMPOUND

Phenol2-ChloroDhenol1 , 4-DichlorobenzeneN-Nitroso-di-n-prop . < 1 )1 f 2?4-Trichlorobensene_-4-Chloro-3-methyl phenolAcenaphthene4-Nitroohenol2,4-Dinitrotoluene__ ___PentachloroohenolPvrene

SPIKEADDED(ug/Kg)

1470O1470O733073307330

1 4700733014700733O147007330

MSDCONCENTRATION

(ug/Kg)

9970343046804940509090904830

.105OO49SO101 OO5760

MSDXREC t

6857646769626671686979

'/.

RPD #

-85-6-9•— 1

— •1°'0O

"""'i15

DC LIMITS •RPD I REC.^

35 : 26- *o50 1 25- 10227 -'. 28 10433 41 i2623 ' :33 1'J733 -.A 2 6 193I5? :31-13750 '11-11447 ' 23- 9947 : 17-10936 - 35-142

;

<1) N-Nitroso-di-n-propylamine

% Column to be umed to -flag recovery and RPD values with an asterisk* Values outside o-f DC limits

RPD: _0 out o-f 11 outside limits ".Spike Recovery: _0 out OT 22 outside limits ."

COMMENTS: UD-28-8 URSINSTsF SWLtt3491.0S

00044FORM III SV-2 - -- -- - - —-- 1/87 Rav

.LOJ520-.


Lab Name: SWL - TULSA____'________ Contract: URS_______

Lab Code: 5UIDK Case No.: URS SAS No.: ______ SDG No.:

Matrix Spike - EPA Sample No.: UD-28-10_____ . .,Level:(low/med) LOW

COMPOUND

Phenol2-Chloroohenol1 . 4-Dichlorobenzene ___N-Nitroso-di-n-prop. ( 1 )1 .2.4-Trichlorobenzene_4-Chloro-3-methy 1 phenolAcenaohthene4-Ni tro phenol2 , 4-DinitrotoluenePen tac hi or a phenol --Pvrene •

COMPOUND

Phenol2-Chlorophenol1 -. 4-DichlorobenzeneN-Nitroso-di-n-prop. ( 1)1 .2,4-Trichloroben2ene_4 -Chloro-3-me thy 1 phenolAcenanhthene . _.4-Witroohenol2, 4-Dini tro toluene ____PentachlorophenolPvrene

SPIKEADDED(ug/Kg)"

93909390470047OO470O93 9O470 O93 9O470093904700.'

SAMPLECONCENTRATION

_< ug/Kg) . _

733O0O.OQO0 -O0o

MSCONCENTRATION

< ug/Kg)

665060103060301031605660295063 1O30306 ISO

. .„.._, J-^r.4O

MSy.REC #

62646564676O63

r 67646671

QCLIMITSREC.

25-10223 10441 12633 10726 10331-13711-11428- 8917-10935-142

SPIKEADDED(ug/Kg)

1 880018 BOO9390939093901 880093901880093 9O188OO9390

MSDCONCENTRATION

(ug/Kg)

"1360O. ""1Q90O621066606,710

1 44OO664O

1 740(1'7590

1 6OOO7680

MSDV.

_ REC S

68™" 53667171

""7771938185S~ >~*A

y.RPD *

-9' 10_ f^

-1O-6

'—.•"US'J_wj

— 12~ c?— •"•TJii.'-'

-25-14

QC LRFD

35SO2738*H«T

1950474736

IMITSREC.

26- 9025- 1 0223 10441 12638 10726 10331-13711-11428- 8917-10935-142

(1). N-Nitroso-di-n-propylamine

# Column to be used to -flag recovery and RPD values with an asterisk* Values outside o-f GC limits

RPD: _O. .out o-f 11 outside limit«_ • ='. - " - !Scike Recovery; _0~ out o-f 22 outside limi'ts

COMMENTS: UD-28-10 URSINST:F SWLtt3491.13

^000445FORM III 3V-2 " 1/87 Rev,

A f i i i J i 5 2 l


L*b Names SWL-TULSA______________ Contract: URS_______

Lab Code: SHOK Case No.: URS3 SAS No.: ______ SDG No.:

Matrix Spike - EPA Sample No. ;' UD-28-8____ Level:(low/med) LOW

I1

! COMPOUND

{ gamma-BHC (Lindane) ___! Heotachlor! Aldrin\ DieldrinJ Endrini A A * — nnTi

SPIKEADDED(ug/Kg)

58.558.558.51461461 4.A

SAMPLECONCENTRATION

(ug/Kg>

0O0000

MSCONCENTRATION

(ug/Kg)

0O0000

MS ! QC J"/. 1LIMITS!REC #i REC. !

0 #146-1271O *! 35-130 iO * 134-132!0 *I31-134!O * 142-139!0 * ! 23—134 J

i j

COMPOUND

gamma-BHC ( Lindane ) ___HeptachlorAldrinDieldrinEndrin4,4'-DDT

SPIKEADDED(ug/Kg)

58. 558.558.5146146146

MSDCONCENTRATION

<ug/Kg)

0O0000

USD7.REC *

O *0 *0 *0 *0 *o *

•//.

RPD #

O00000

QC LIMITS |RPD ! REC.™

50 146-12731 135-13043 134-13238 131-13445 142-139SO ! 23- 1 34

i

# Column to b* used to -flag recovery and RPD value* with an asterisk


RPD: _g_ out of _&. outside limitsSpike Recovery: 12 out o-f 12 outside limits

COMMENTS:

&-OOU446FORM III PEST-2 8/87 Re

•

A R I O I 5 2 2


Lab Name: SHL-TULSA______________ Contract: URS_______

Lab Code: SWOK Case No.: URS3 SAS No.: ______ SDG No.:

Matrix Spike - EPA Sample No.T UD-28-1O Level:(low/med) LOW

COMPOUND

gamma-BHC '(Lindane) ___HeptachlorAldrinDieldrinEndrin4.4'-DDT

SPIKEADDED(ug/Kg)

S5S3E3S = =S=Ce

74.974.974.9187187187

SAMPLECONCENTRATION

< ug/Kg)

OO0o00

MSCONCENTRATION

< ug/Kg)53 ssssaBSK as SB :±E

O19.42.285.575.639.22

MS 1 QC !7. 1LIMITS!

REC #1 REC. !soexas { ssssss !

6 *! 46-127126 * 135-130!3 * 134-13213 *!31-134!3 * 142-139!5 *!23-134f

! 1

COMPOUND

gamma-BHC ( Lindane ) __ __HeotachlorAldrinDieldrinEndrin4,4'-DDT

SPIKEADDED(ug/Kg >

74.974.974.9187187187

MSDCONCENTRATION

(ug/Kg)

35.146.74.68

11.112.917.2

MSD !7 ' 7REC #1 RPD #=ss*"* i &».47 1-200 *62 ! -82 *6 *! -67 *6 *l -67 *7 *! -8O *9 <: -57 *

i

QC LIRPD

503143384550

EMITS !REC. !

46-127!35-130!34-132131-134142-139123-134,'

ii


* Values outside of QC limits

RPD: _6 out of _6 outside limitsSpike Recovery: 10 out of 12 outside limits

COMMENTS:

FORM III PEST-2 B/87 Rev,

0-000447

A R I 0 1 5 2 3

U.S. EPA - CLP —

5A .. EPA SAMPLE NCSPIKE SAMPLE RECOVERY

Lab Nsme: SOUTHWEST LAB OF OK Contract: 6S-D9-OOS9MU9109S

Lab Code: SWOK Case No.: 34911 SAS No.: SDG No".: MU9101


7. Solids -for Sample: 92.3 """•

Concentration Units (ug/L or mg/kg dry weight): MG/l.G

ii<>\ Anm'lytet! Aluminum! Antimonv! ArsenicJ BariumJ Bervl liumJ Cadmium[Calcium! Chromium''Cobalt! Copper! IronI Lend! Magnesium! Manganese! MrrcurvJNict-el! Potass \um! SelsniumISilv^rI Sod ium! Thai lium! Vanadium! ZincICvanj d*=»i

ControlLimit"v.R

75-12575-125"7 — 1 ^t ZJ"*" JL *t, l7*^—1 If «J 1 J-wJ

7 ;— i r»^/ j~"I-i j

75-12575-12575-125

~" ~ i r"ie;• -J — t X.vJ

75-125T5-!257=5— t 'ner,f +J i. *—*J

75-12575-125

" •5 1 'HE'/ 5— Ij i75-12575-12575-125

Spiked SampleResult <SSR)

V53.94983.4300

4O2.03179.777414.0567

42.157599.O37652.5512

26.6956

115.1641.4B99

97.3223

.83629.9922

9.4171102.8554101.643319.4760

C

B

SampleResult (SR) C

_i

5. 5730 I U1.0727IU13.9001 ! B

.3281 IB,6436!U|

7.724712.9829 ! B3. 4326 I U

J1 .4310!

;29.6518:

. 0867 I U4. 4623 IB

i*.4291 !U. 9660 1 B

ii.6436JU

7.6559IB7 . 5O03 !2.0916IU

SpikeAdded t SA >

\108. 3 *B.67

. 433,371 0 . S31O.S3

43.34103.3454. 17

.1 21.&7

103". 34.47

1 03 . 34

2.171O.S3

10.83103.34108.3413-30

y.R

49.840 . 139.687.3129.8

79.468. S97 . 0

116.6

78.91 04 . 235.7

40. S83.3

S7.087.936. 9

" 1 06 . 4

i iii

Qiri

1NRNIPN!FIPIP

IM!P1NR;pi r-.lIF1NRIF: cv! F'!NR

NIF!P!NRIFIPIP1C

Comments:


0T000448

flRI.OI52i»

U.S. EPA - CLPEPA SAMPLE NO,

A

DUPLICATESMU9JO8D

Lab Name: SOUTHWEST LAB OF OK .Contract: 63-D9-0039

._ L Case No.: 349 .1 SAS No.: SDG No.: MU°101

Matrix (water/soil*..! 30.IL Level (low/ms-d): LOW

"/. Solids -for Sampler" 92.3 ._ " "'/. Solids f or. Dup_l icate: 92.5

Concentration Units (ug/L or mg/kg dry weight): MB/KG

Anal vie-

A3 uminumAntimonvArsenic. ...BariumB»ry 1 1 iumCadmiumCalciumChromiumCobaltCopperI ronLeadMagnesiumManaaneseMercurvNickelPotassiumSel en iumSilverSodiumThai 1 iumVanadiumZincCyanide

ControlLimit \

— -

.2. 1

.6. _ _

. i

4.3o 1

Sample (S) C_

2522.8166!5 . 573O I U1. 0727.1 U13.9001 IB

.3281 IB

.6436JU141. 8867! B7.724712. 8829 IB3.43261U

10661 .6440!1.43101

114.0137IB29.6'518I.08671U

4. 4623 IB137 .0880 IB

.4291 !U

.9660 IB86. 8963 IB.6436IU

7. 6559 IB7 . 500-3 I2.0916IU

-

Duplicate (D) C

2023.58,0215. 5780 1 U1 .0727 I U

« ~T es-EJiO^ ' p

. 229 1 ! B

.64361 U122.6381 IB3 . 1 094 !2.2901 IB3. 4326 I U

6263.0471 I1 . 4O09 I

107. 3540 IB26.30761

-1032IU3.32O5IB

115.4425IB.4291 !U.6766 IB

73. 7359 I U.64361U

4. 9057 IB5,1727!1 .4256!U

"

XRPD

22 . 0

2.535.5

14.685. 2'". O Q

52 . 02. 15.69.S

29 .317. 1

35. 2200 . 0

-43. S36 . 7

DIM

* IPIPIFIPIPt pIF

* IP!P!P

* !PIFIPIPICVi oi T

IP

IF• p1 n*i iIFIPIP1C

FOR-M VI - IN

AR10I525

U.S. EPA - CLP

5A __ .___ EPA SAMPLE NO.SPIKE SAMPLE RECOVERY ______

MU9113SLab M*mr,: SOUTHWEST LAB OF &K .. Contract: 63-D9-O089

f?: SWOr Cast? No.: 34911 SAS No.: SDG No.: MU9101

Meii.ri:.: £01L .... - ..._ -Level (low/med): LOW

"'. Solid? 4or Sample: 6B.5


1

I Anal vte

[Aluminum: An timanv1 Arssnic: BariumI B^rvl 1 iumI C^dnu um1 Cal CiumI Chromium'Cobalt1 CrspperI I ronI Lead1 Magnesium!Msnganf*«se1 M^rcurv! Nicf-.^l! Potassium1 Selenium! Silver' Sodium! Thallium' Vanadium1 SineICvsnids

Con trolLimit *7.R

75-12575-125-?ez _ . r>^/ ~J X ji- J

75-12575-125

75-12575-12575-125

75-125

75-125rrrr_ 1 *^^t *J i. —*J

75-12575-125

75-12575-12575-12575-123

"

Spiked SampleResult CSSR)

V33 . 96294.3102

745.534715.735413.2473

155.6607134.6723127.6200

116.2102

1766.6485.69O1

193.8230

.696717.6264

-1 1 . 5054201.1794286 . 334928 . 7580

C

B

SampleResult (SR) C

I20 . 5503 !

• 1.44541U192.7341!2.6492!2.1339!

!35.7599149.9731 !66.1761 1

15.824711

1386.4646!.1081 IU

59.0939,'I

-5782IU5.1577!|

.3672 I U66.32541144.2490!2.9197IU

SpikeAdded (SA)

'143.1211 .56

572.4914.31

': 14.31

57.25143. 1271.56

5.78

143. 12.66

143. 12

2.3914.31

14-45143. 12143. 1227.44

7.R

12.937.396.691 .4

1 12.6

122. 194. 135.9

1736. S

125.91O4.694.1

24. 137. 1

79.694.299.3104 .-8

:

Q:M

: MRNIPNIFIPIPIP; NR:pIP

1N I F™INRIPicvIPINR

NIFIPI MRl.FIPIP:c

Comments:


0004 0

R R 1 0 I 5 2 6


6 -' __ ________DUPLICATES

Lab Name:-SOUTHWEST LAB OF OK Contract: 63-D9-0099MLJ91 I'DUO-Ls /i-

Lab Code: SWOK Case No.: 34911 SAS Np.j__ SDG No.: MU9101

Matrix (water/soil>: SOIL Level. <low/med): IOW

"; Solids -for Sample: 68.5 X Solids far Duplicate: -^. 4

Concentration Units (ua/L or mg/kq dry weibht)

FORM VI - IN

j1 Anal vte -

! Aluminum1 An ticnony1 Arsenic1 BariumI Beryl 1 iumI Cadmium! Calcium! ChromiumI Cobalt .I CopoerI IronILead1 Magnesium1 Manganese! Mercury! Nickel1 PotassiumI SeleniumI SilverI SodiumI Thai 1 iumI VanadiumIZinc! Cyan ids

ControlLimit >•

17..3

57.81 .41 .4

1445.4

14.5

.91 445 . 4

.

1445.4

"? p-C- . 7

14- 5.2.9

Sample (S) C

22371.3510!20,5503!1 . 4454 ! U

192.784112 . 6492 !2.13891

1453.7170!35.7599!49.9731 !66. 1761 1

72582.1210!15.3247!

4453.237911536.4646!

.10B1IU59.0939!

3368.2399!.5732IU

5. 1577!254. 2322 IB

. 8672 1 U66.32541144.249OI2.9197IU

Duplicate (D) C

21763.952017.5161 IU1 .44541U

216.04461"2.8245!2 . 7022 1

1529.2735!90 . 0334 I57.3158164.5317!

73002.0230123.50.39!

4803 . 0067 !1649.2505!

. 12691U75.7511 I

3718.2328 I. 5732 1 U

5. 1546!255. 3464 IB

. 3672 ! U73.7967!174.5596!

2. 3402 I U

"/.RPD

2.7200. 0

11 .46.423 . 35. 14.913."

•-v c-*- . -J. s

39. 17.6T 'T

24.79.9

. 1

.4

10.7-19.0

MG/KG

PPCVPPFPPrp

£-000451f l R I O I 5 2 7

U.S. EPA - CLP

7LABORATORY CONTROL SAMPLE :..

Lab N*mes SOUTHWEST LAB OF OK Contract: 68-D9-0089

L*h Hodi?: 5WQK Case No.: 34911 SAS No.: SDG No.: MU9101

Solid LCS Source:" EPA02S7 ; _

LC3 Sourcfa : __'_

1

! Anal vte

1 Aluminum1 Antimonv! Ar^gnic! Barium1 Gwryl lium! CadmiumI C.9 Ic i ucn'i.'hrofniurnI CobalttCoopsrI I ronI L©?dJMaane^xumIMana^no^eI MercurvItMickel[PotassiumI Selenium!Silvf?r1 Sod 3 um! Thftl liumI V*n*d\um! Zinc!Cv.r,id*

Aqueous (ug/L JTrue Found 7.R

V

_

___

_

_ :

_"

_ __

Solid (mg/kg)True Found C Limits 7.R

325 . 0211 .0917.04.319.445.4

1962OO.O99.6144.0

6910.O22430 . 0236. 0

1181OO.O208.012.760 . 9

_ 50 . 039.222.250 . 039.065.8187.05.6

263.0!132.3!

1 OO9 . O !5 . 2 ! B

17. 1 145.31

2O2735 . B 195.1J143.6!7360 . 1 120066.4!229 . 7 !

126122.01197.0!12.7!62.4!69 . 0 1 Ur?*7 4 i15.91127. 01B38.1 157.61179.916.3!

225 . 0127.0635.00 . ft16.535.7

1668OO.T)'. ... 79 . '2124. 'J

6OO6 . O1777O.O1B3.0

1004OO.O: 177.0

3.549.20 . 019. 115.50 . 024.651 .7133.04.3

424.02 4.01199.O40.022. 355.1

225 6OO . O120.O1&2.O7 S 20.027030 . O235 . 0

129900.0239.O17.072.6

1000. 05Q. 429 . 0

1000. 053.579. 9236 . 0

80.962.=?

110. 0108.388.1

1 OO . 91 '"'3 . 395.5

97.3106.S94.7

1 OO . O102.50 . 0

57. 171.62^4 . 097.787 . 596.2

I 12.5

FORM VII - IN

6 00045:

U.S. EPA - CLP



Lab Code: SWOK.- Case No.: 34911 SAS No.: 3DG No.: MU9KU

Solid LCS" Source": EPA0237

Aqueous LCS Source:

1

1 Anal vte

I AluminumI AntimonyI ArsenicJ Bar ium1 Beryl lium

_^ 1 Cadmium' Calcium1 Chromium.'CobaltI CapperI IronJLead1 Magnesium1 Manganese! Mercury

•' I Nickel'...l-Potassium_.M Selenium'. ! Si 1 ver

9 /jSodium"^Thallium/•IrVanadium

1 Zinc! Cyanide

Aqueous (ug/L)True FaunW 7.R

_

Solid (mg/kg )True Found C Limits "'.R

5 _. 6 6.2 4,3 6.9

;

1 1 0 . 7

FORM VII - IN7/BS

AFU01529

SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Suite "C1 . Broken Arrow, Oklahoma 74012 . 91 -251-2858

CLIENT: URS CONSULTANTS, INC. REPORT: 349Ib570 DELAWARE AVE.BUFFALO, NY 14202 DATE: 09-06-90ATTNs PETER FAIRBANKS

LABORATORY BLANK

SAMPLE MATRIXs SOILSAMPLE ID« METHOD BLANK

DETECTIONCOMPOUND LIMIT <M/KCI>

TPH 10.0

TPH MATRIX SPIKE/MATRIX SPIKE DUPLICA'

' SAMPLE MATRIX i SOILSWLO # 3491.08, 09 (MS)PROJECT: DELAWARE SAND & GRAVELSAMPLE ID* UD-28-8, UD-28-S MS (MS)

SPIKE CONC. SAMPLE CONC.(•g/Kg) (fig/Kg)*

TPH 333 52

SAMPLE MATRIXj SOILSWLO # 3491. 1O (MSD)PROJECT: DELAWARE SAND ic 6RAVELSAMPLE ID i UD-28-8 MSD (MSD)

SPIKE CONC. SAMPLE CONC.(•g/Kg) («g/Kg)«

SAMPLE AMOUNT: 30GDILUTION FACTOR: 1

AMOUNT FOUND<*Q/Ka)

ND

PE RECOVERY DATA

MS CONC. MS PERCENT<»g/Kg)* RECOVERY

362 937.


TPH 343 87 67.



TPH <10 <io . 0

A R I O I 5 3 0

SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Suite "C1 . Broken Arrow, Oklahoma 74012 . 918-251-2858

CLIENT: URS CONSULTANTS, INC. REPORT: 3491c570 DELAWARE AVE.BUFFALO, NY 14202 DATEs 09-06-90ATTNs PETER FAIRBANKS

LABORATORY BLANK

SAMPLE MATRIXs SOIL SAMPLE AMOUNTS 30GSAMPLE IDI METHOD BLANK DILUTION FACTOR: i

DETECTION AMOUNT FOUNDCOMPOUND________ . _• LIMIT (•o/Ko*_________-

TPH 10.0 ND


SAMPLE MATRIX I SOILSWLO * 3491.13, 14 (MS)PROJECTS DELAWARE SAND & SRAVELSAMPLE ID8 UD-28-10, UD-28-1O MS (MS)

SPIKE CONC. SAMPLE CONC. MS CONC. MS PERCENT(•g/Kg) («g/Kg)* («g/Kg)* (RECOVERY

TPH 333 0 3O8 92V.

SAMPLE MATRIXi SOILSWLO * 3491.13 (MSD)PROJECTS DELAWARE SAND «c GRAVELSAMPLE IDs UD-28-10 MSD (MSD)

SPIKE CONC. SAMPLE CONC. RECOVERY PERCENT(•g/Kg) (wg/Kg>* DIFFERENCE

TPH 308 92 07.

* = DILUTION FACTOR NOT APPLIED TO THESE CONCENTRATIONS


TPH 470 428 9.4 000450

f l R i O i 5 3 1

U.S. EPA - CLP


Lab Name: SOUTHWEST LAB OF OK Contract: 68-E>9-0089

Lab Codes SWOK _C«e No.: 31931 SAS No.: SDG No.: MTP101


Aqueous LCS Source: EPA-LV

i Analytei

! Aluminum{Antimony! Arsenic! Barium{BerylliumI Cadmium: CalciumJ Chromium! Cobalt'Copper! Iron!Lead! Magnesium! Manganese! MercuryiNickel! Potassiumi SeleniumJ Silver! Sod ium(Thalliumt Vanadium!Zinc! Cyanidei

AquecTrue

.

aus (ug/LFound

»•/.R

.

SolidTrue Found C

325.0! 303.4!211.0! 171.6!917.0! 794.5!4G ' A ' R. O 1 *T . vJ » O

19.4! 18.2!45.4! 44.8!

196200.0! 195687. 8!99.6! 85.1!144. O! 129.6!

6910. O! 6858.1!22430.0! 18592.6!236.0! 222.4!

118100.0! 12OS01.4!208.0! 2O9.6!12.7! 10.7!60.9! 51.8!50.0! 69.7JU39.2! 51.5!22.2! 16.3!50.0! 220. S!B39.0! 42.2?65 .Si 61 • S i187. O! 165.5!

O • O i O . O i1 11 1

C mg/kg )Limits

225.0! 424.0127.0! 294.0635.0! 1199.00.0! 4O.O16.5! 22.335.7! 55,1

1 668OO . 0 ! 2256OO . 079.2! 120.0124.0! 162.0

. 60O6.0! 7S2O.O17770.0! 27O8O.O188.0! 285. O

1 004OO .011 2990O . 0177. O! 239.08.5! 17. O49.2! 72.6O.O! 1OOO.O19.1! 59.415.5! 29.0O.O! 1000.024.6! 53.551.7! 79.9138.0! 236.04.3! 6.9

7.R

OTv--/ . '

81.-86.,93.:93. i98.

M'•9OP99.82.94.102.100. i84.85.O.i

131.-/-.. . *

441. r108.193. c88.1117. «

FORM VII - IN7/8B

6^000456f t R i u i 5 3 2

U.S. EPA - CLP


Lab Name: SOUTHWEST LAB OF OK ^ - - - - - - - Contract: 6S-D9-OOS9

Lab Cade: SWOK =" Case No.: 31931 SAS No.: SDG No.: MTP101



Analyte

AluminumAntimonyArsenicBariumBeryl liumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThai liumVanadiumZincCyanide

- _.-. ;'• --- i-.-w-_quei

Truealts (ug/LFound

"

.

> ,'/.R

' i--. 2... " J - ; ."'4.- '--V . T_S_ -~ * *'T' *re— i ,• -t t- -*. .«#- - _ * fc*~«iO 1 Id <True Found C

325 . 0 ! 305 . 2 !211.01 175.3!917.0! 858.4!4.8! 4.6!B19.4! 18.2!45.4! 44.5!

19620O.OI2O4745.2!99.6! S3. 9!144.0! 128.4!691O.O! 7053.6!2243O.O! 18379.7!236. O! 27O.S!

118100. O! 126189.6!208. O! 206.3!i it i6O.9! 50.8!SO. 01 69.OJU39.2! 42.5!22.2! 16.2!5O.O! 232. 2!B39.0! 39.7!65.8! 58.4!187.0! 151.6!5.6! 6.0!

i ii i

[ragykg) "'-Limits

225.0! 424.0127.0! 294.0635.0! 1199.00.0! 4O.O

16.5! 22.335.7! 55.1

1 66800 . 0 ! 2256OO . 079.2! 120.0124.0! 162.06006.0! 7820,017770.0! 27080.0188.0! 2S5.0

100400.0! 1299OO.O177.0! 239.0

•i49.2! 72.60.0! 1OOO.O

19.11 59.41 R c. * "?o n1 J . *J 1 4.7 m U

0.0! 10OO.O24.6! 53.55i.7! 79.9138.0! 236.04.3! 6.9

i

•/.R

v-J> •

S3.93.95.93.98.104.84.89.

1O2.81.

114.106.99.

83.• o.1O8.73 .464.101.S3.81.

107.

FORM VII - IN7/SS

A R I O I 5 3 3


CLIENTS URS CONSULTANTS, INC. - REPORT: 3i93a570 DELAWARE AVE.BUFFALO, NY 142O2 DATE: 08-22-90ATTN: PETER FAIRBANKS

LABORATORY BLANK

SAMPLE MATRIXi SOIL SAMPLE AMOUNT: 30BSAMPLE ID: METHOD BLANK DILUTION FACTOR: 1

DETECTION AMOUNT FOUNDCOMPOUND_____________LIMIT <mq/Ka)______________(ag/Kgl

TPH 10.0 ' ND

Tgtf MATRIX SPIKE RECOVERY DATA

SAMPLE MATRIXi SOILSWLO # 3193.05 (MS)PROJECT: DELAWARE SAND It BRAVELSAMPLE IDi UR-1 (MS)

SPIKE CONC. SAMPLE CONC. MS CONC. MS PERCENT(•g/Kg) («g/Kg>* dug/Kg)* RECOVERY

TPH 667 17 600 87%


<?r00045SA R I O I 5 3 1 *


Lab Names SWL-TULSA_________. Contract: URS________

Lab Codes 5U.OK .._ Case No.: URS SAS No.: ______ SDG No.s

Matrix Spike - EPA Sample No.: UR-11_______ Level s < low/med ) LOW

COMPOUND

1 , l-Dichloro@thene ____Trie hi oroe then©Benzenetoluene = "*.Chloi^obenserie^^

SPIKEADDED< ug/Kg )

6t.O61.061 .O

:-- :^i-o^61 . 0

SAMPLECONCEh4TRATIQN

(ug/Kg)

O"O

' • O-tJ 4.93 -- - - j-" .- •----•-' - ---' *.---*.-?3O

MSCONCENTRATION

(ug/Kg>

64 . 055. 058.861.0

._! - . I9*£, •*

MS ! QCy. ILIMITS

REC #i REC.=— — s— = t ==— — -• —1O5 159-1729O 562-13796 J 66-142

aSffl A59-139: S. fcfi.0-133ii

COMPOUND

1 ? l-Dichloroeth©ne ___ ._TrichloroetheneBenzeneTolueneChlorobenzene

SPIKEADDED(ug/Kg)

S3 S3 5 5 KSBS53S

61.061.061 .061. 061 .0

MSDCONCENTRATION

(ug/Kg)_s_— .— a.SSK=E==ss

54.848.355.1hJO . 1

53. 5

MSD'/.REC #ssssas

90799O3488

y

RPD #

15136o

11

DC LJRPD

2224212121

:MITSREC.

59-17262-13766-14259-13960-133

$ Column to be used to -flag recovery and RPD values with an asterisk


RPD: _0 put of. __5_ outside limitsSpike Recovery***_0, out o-f 10 outside limits

COMMENTS: UR-11 URSINST:I SWL#3210.11 5

FORM III VOA-2 1/B7

f l R I O I 5 3 5


Lab Name: SUIL-TULSA ____________ Contract: URS _____ _

Lab Code: SUjQK Case No.: URS SAS No.: ______ SDG No.:

Matrix Spike - EPA Sample No. ; UR-18 _______ Level s ( low/med ) LOW

COMPOUNDatSKSEesKss3ssais9tssss=s:ss=

1 , 1-DichloroetheneTrichloraetheneBenzeneTolueneChlarobenzene

SPIKEADDED(ug/Kg)

61.061 .O61.061.061.0

SAMPLECONCENTRATION

(ug/Kg )

0001.120

MSCONCENTRATION

(ug/Kg)

48.246.852.352.247.9

MS7.REC #

7977868479

QCLIMITSREC.

59-17262-13766-14259-13960-133

"

COMPOUND__3_s_3S5___.£i___:__s__s__3__E,=ssss^^:=s:===;s=1 . 1-DichloroethgneTrichloroetheneB*nz«neTolueneChlorobenzene

SPIKEADDED(ug/Kg)

— Esss sssssa

61.061.061.061.061.0

MSDCONCENTRATION

(ug/Kg)

52 . 048.856.660.154.9

MSDyuREC #

masmmmm

85SO939790

7.RPD 4.

miBl£KK =

-7«4-8-14-13

QC LIRPD

*_>^242121•"* 4-il

11

MITS AREC . •

s— — — —T

59-17262-13766-14259-13960-13-

* Column to be used to flag recovery and RPD values with an asterisk


RPD: _g_ out of _5 outside limitsSpike Recoveryi _0. out o-f 10 outside limits ~~

COMMENTS:

FORM III VOA-2 1/97 Re

flRiOi536

3DSOIL SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERx

Lab Name: SWL-TUL5A__________' Contract: URS_______

Lab Code: SWOK Case No.: URS SAS No.: ______ SDG No.:

Matrix Spike - EPA Sample No.: LJR-U_______ Level: (low/med) LOW

COMPOUND

Phenol2-Chlorophenol1 , 4-Dic hi or o benzene ___N-Nitroso-di-n-prop . ( 1 )1 ,2,4— Trichlorobenzene___4-Chloro-3-me thy 1 phenolAcenaohthene4-Nitroohanol

." $', 4-Dinitrotolu^ne ____

.^•entachlorophahol '-Pvrene

— ---

SPIKEADDED(ug/Kg)

1630016300S13O31308130

1 630O8130163OO8130i630C "Si 30

SAMPLECONCENTRATION

(ug/Kg)

00O0oo0

'• . . "" O...Q

"•'-"""'""" Sg-tT"-o*

MSCONCENTRATION

(ug/Kg)

1O4001130055704900594O122OO5170

. 12800_ _r&S6O =

4 .£a ,.,,/'7410

MS ! HC7. ILIMCTS

REC **: FEC.

64 1 5- «0

69 \ZB 10460 !41 iZo73 !7S 10775 ! 6 10364 ! 7. 1 - i 3779 I 1 1 - i 1 4-BI ... ;?a- 39

: -95 "-H 7-10*9i ! 75- 142

;

COMPOUND

Phenol2-ChloroDh©nol1 .4-Dichlorobenzene ___N-Nitroso-di-n-prop. ( 1 )1 ,2,4-Trichlorabenzene_4-C h 1 oro-3-me t hy 1 pheno 1Acenaphthene4-Nitroohenol2 ., 4-Dini trotoluene ____PentachlorophenolPvrene

SPIKEADDED(ug/Kg)

==S:=&=S333:3

16300163008130813081301630O8130163OO313O163008130

MSDCONCENTRATION

(ug/Kg)

98401130O5610490058301160O52201330O6740157007700

MSD7.REC #

606969607*

,£.

716482839695

7.RPD *

6O0015O-4_ *•?-1-4

iQC LIMI T5 1RPD : REC. :

35 IT43- 90!50 : 25- 102127 IZ8 104!38 141 L26!23 :33 107!33 116 I '.'3!19 171-177!5O ! 1 1 - i 1 4 !47 I r8- 39!47 ! 17-1 '.'9!36 175-142!

< ii t


ft Column to be used to -flag recovery and RPD values with an asterisk* Values outsid* of QC limits

RPD: _0 out o-f 11 outside limitsSpike Recovery: _0. out o-f 22 outside limits

COMMENTS: UR-11 URS - 306/1 ML/ 1UL45/4-300 Si2 FSCC DB-5 3OM/1UM INSTR:B

FORM III SV-2 1/37 Pe^

6-000461

"TRiO I 537


Lab Name: SWL-TULSA______________ Contract: URS_______

Lab Codes SMQK Came No.: URS 3AS No.: ______ SDG No.:

Matrix Spike - EPA Sample No.: UR-18_______ Level:(low/med) LOW

COMPOUNDm m MJK vac MEK as K vae SEXSE ass s aiaa s saa

Phenol2-ChloroDh«nol1 ,4-Dichlorobenzen^N-Nitroso-di-n-prop. ( 1 )1 ,2, 4-Trichloroben2ene____.4-Chloro~3-me thy 1 phenolAcenaohthene4-Nitroohenol2 f 4-Dinitrotolu@ne ____Pen tmchlora phenolPvrene

SPIKEADDED(ug/Kg)

3K St3S 5 S3 = = ££

1 63001630081308 ISO81301 630O81301 630031301630O3130-

SAMPLECONCENTRATION

(ug/Kg ')

000o000o000

MSCONCENTRATION

(ug/Kg)

108001160O61805390607O

1160O338O1 320O6430125006980

MS7.

REC 4.

oo71766675

' 716631797736

DC iLIMITS!REC. !

26- 90!25-107:123 104!41 126!38 107!26 i 03 !^* i 1 T~r J• J- 1 1 -' / t

11-114!23- 89!17-109!35-142 !

i

COMPOUND

Phenol_______________2-Ch1o ropheno1________1,, 4—Dichlorobenzene___N-Nitroso-di-n—prop. ( i >

4-Chloro-3-methylphenolAcenaphthene_____"4-Nitrophenol_________2j4-Dinitrotoluene^PentachlorophenolPyrene

SPIKEADDED(ug/Kg);ssss5S3c;

163OO1630O813081308130163008130163008130

i 63OO8130

MSDCONCENTRATION

(ug/Kg>

11OOO112005780462O6180

112005380124OO6340

141OO8220

MSD7.REC #S33*E = S

67697157766966767886101

7.RPD

71-1

O61

•U•16

QC LIMITSRPD

os502738

1950474736

REC.

26-25-1QJ23 10441 12633 10726 10331-13711-11428- 3917-10935-142


tt Column to b* used to -flag recovery and RPD values with an asterisk* Valuer outsid» o-f QC limits

RPD; _0. out o-f 11 • outside limitsSpo.K» Recovery: _0. out of 22 outside limits

COMMENTS: UR-18 URS - 30G/1ML/1UL45/4-300 (112 FSCC DB-5 30M/1UM INSTRsB

FORM III SV-2 1/37 Rev

Gi538


Lab Name: SML-TULSA_______________ Contracts URS ____

Lab Code: SUIQK .. Case No.: UR52 SAS No.: ______ SDG No.:• V » r . . . . .

Matrix Spike - -jiPA Sample No.: UR-11______ Level:(low/med) LOW

COMPOUND

gamma-BHC (Lindane ) ___HeotachlorAldrin

r Dig-ldrin, EnBnin . .<•" t4.4lr-DOT "

SPIKEADDED(ug/Kg)

S=SS5S3Xa

O^t • T

64.964.9162

~ 1 A*3.. AO .

J162

SAMPLECONCENTRATION

(ug/Kg)

0000

0 '~ 0

• ••

MSCONCENTRATION

< ug/Kg)SWXSmXSVHBSBSeSSS

58.158.350.2124i Q•«=-••- -1-B31V

-.——...-., 151

MS7.REC #

90907777PADO81

I

QC !LIMITS;REC. !

46-127!35-130!34-132!31-134!**.£ iOT i

23-134!i

COMPOUND===3=a3s=ss=aeffi==sse===3s==E=se

gamma-BHC ( Lindane ) ___HeotachlorAldrinDieldrinEndrin4.4'-DDT

SPIKEADDED< ug/Kg)assssssss

64.964.964.9162162162

MSDCONCENTRATION

< ug/Kg)S=SSS===5=S3:=3

55.561.545.7115127127

MSDfm

REC ftSB 35== 3= J*

869570717878 .

y

RPD #5E=SS'3S

5—510810.4

QC LIMITSRPD

SSKSESS

503143384550

REC.SSSS5= = S

46*12735-13034-13231-13442-13923-134!

!



RPD: _0 out of _& outside limitsSpike Recovmr i:_g. out of 12 outside limits

COMMENTS:

FORM III PEST-2 8/87 Rev.

6-000463

A R I O I 5 3 9


Lab Name: SWL-TULSA______________ Contract: URS_______

Lab Code: SUJOK Case No.: URS2 SAS No.: ______ SDG No.:

Matrix Spike - EPA Sample No.:, UR-18______ Level:(low/med > LOW

COMPOUND

gamma-BHC ( Lindane ) ___HeotachlorAldrinDieldrinEndrin4.4' -DOT

•

SPIKEADDED(ug/Kg)

64.964.964.9162162162

SAMPLECONCENTRATION

(ug/Kg)——,_.:.__:— -s=___: ___.«__• ,s __E^

0

00

0

0

0

MSCONCENTRATION

(ug/Kg)eS»Z = IBSSSmBSE = =

61. 159.842.8131147133

MS'/.

REC *

949266819182

DCLIMITSREC.

46-12735-13034-L3231-13442-139C3-134

COMPOUND

gamma-BHC ( Lindane ) ___HeptachlorAldrinDieldrinEndrin4.4'-DDT

SPIKEADDED(ug/Kg)

64.964.964.9162162162

MSDCONCENTRATION

(ug/Kg)

48.147.0%iO> . sJ103113100

MSD•/.

REC #

747252647062

•/RPD tt

242424232628

QC L3RPD

___„,___503143384550

iCMITS REC M

46-12735-13034-13231-13442-13923-134


* Values outside of QC liraitm

RPDs _0 out of _6 outside limitsSpike Recovery: _g. out o-f 12 outside limits

COMMENTS:

FORM III PEST-2 , 8/87 R

£'000464

^

U.S. EPA - CLPEPA SAMPLE HO

6 • _________DUPLICATES

WUR011DLab Names SOUTHWEST LAB OF OK Contracts 68-D9-OO89

Lab Codes SWOK Case No.s 32101 SAS No.: SDG No.s MUR001

Matrix (water/soil): SOIL Level (low/med>: LOW

?•: Solids for Samples 81.8 , % Solids for Duplicates 81.7


Control

J

Analyte

', Aluminum!AntimonyI Arsenic!Barium\Beryllium!Cadmium.CalciumI Chromium!CobaltI Copper! Iron! Lead!MagnesiumI Manganese!MercuryI Nickel!Potassium'SeleniumI Silver!Sod iumJ Thallium-"! Vanadium-.Zinc.Cyanide

Limit

47.9

6.0

9.6

2.4

Sample (S)

6.2323',U6-. 7237. B

7O- 104911.1647 IB.7191.U

370. 1479 IB24-8607!8. 1521 IB9.31771

4798.4190 I15.8804:740. 3014 !B334.6542;

.llll.U16.93081562.O280IB

.7191IU2.5188.

143. 7088 IB.7191IU

48.5868137.1579!4.666OIU

Duplicate (D) C!*——__.-_ __._.«..«.«.»..«_ *16671.39361 J

6.3570.U;1.5379!BI64.35701 I.9738.B:.7335.UI

177.3499 IB!18.5755! t8.1877IB!8.5091! !

19575.99701 .16.68461 I585.8698 IB I336.11751 !~" .1063IUJ

1*> 1 fTct i tJO. m 4.4_«->%J \ .

364.5459!B!.7335IUI

2.1093IB!95.6516!B!

.7335IUI41.253O! I27.5274! I4.7754IU!

:RPD

44.7!

125.518.5!17.91

i70.4!28.9!.4!

9.1!5!

4.9!

.4!

33»1!42.61

17.7!40.21

•i16.3 I29.31

*',p:P!F;p

IP

IP :IP :

*:P :• p •i ~ iIP ;IP :ICVIIP :;P ;

> p 'i i iIF I:P :;c

FORM VI - INx 7/88

Cr-000465

U.S. EPA - CLP


NUR011SLab Name?: SOUTHWEST LAB OF OK Con tracts . A8-D9-OO89 __,_.__„__,__

Lab Codes SWOK Case Ho.3 32101 SAS No.: __ SIM3 No.a MUK001

Matrix: SOIL . _ Level (l.ow/med} : LOW

": Solid* for .Samples 81.8

Concentration Units (ug/L or ma/kg dry weight): MG/KG

! ! ControlI Limit

I Analyte I *^R

.Aluminum .[Antimony 175-125! Arsenic 175-125! Barium 175-125! Beryl lium I 75-125! Cadmium 175-125ICalcium IJ Chromium 175-125JCobalt 175-125

- Copper 175-125I Iron I[Lead 175-125I Maqnmium'! Manganese! 75—125I Mercury 175-125! Nickel 175-125', Potassium I[Selenium ! 75-125I Silver 175-125! Sod ium !! Thallium I 5-125! Vanadium I75-1Z5!2inc 175-125I Cyanide 175-125

Spiked SampleResult (SSR) C

_ — -— —™-— — ———••—•——• —

i oo R* **$9 *12.8264!499.6192112.3859!15.21611

166.06OOI1 20. 3339 164.45641

!21.75061

!394.6178!

.6296!129.2566!

ii3.1638!13.45471

it8.9O95!

154.2157!141.9919146.76651

— - I

SampleResult <SR) C

—»™w..__—— __.____«________ ™

6. 2323 I U6.7237IB70.1049!1.1647 IB-7191IU

!24.860718.1521IB9.31771

*15.38041

*334.65421

--1111IU16.9308!

j.7191IU

2-5188!;

.7191 I U48.5868137.1579!4 . 666O I U

!

SpikeAdded (SA>

— . ._«.-———, ___.

H oo o «;!*_*_• x- *,'

9.78489.00•10 oo1x1 . A.*!

48.90122.2561.12

4.89-122.25

.61122.25

2.4412.22

12.22100 o •**414. •/.*.'

122.2548.70

t 11 11 1

":R : a ; M;~;HP

100.5! IP62.4IN.F87.8! IP91.81 IP124.51 [P

! !NR84.31 IP91.8! IP9O.2I IP (

: ; NK"120.0! IF

; INR49.0 ;N;P103.2! !CV91.9! !P

I INR129.7INIF89 . 5 ', ! P

! INR72 . 9 I N I F8<b . 4 ; ; p85.8! IP96. o; :c

1 1„ 1 . , 1 __

Comments:


4-00046*]

I O I 5 i » 2

r

u;s. EPA - CLPEPA SAMPLE NO.

6 .. ._ ___ . ___________DUPLICATES

MUR013DLab Names SOUTHWEST LAB OF OK Contracts 68-D9-0089

Lab Code: SWOK Case No.: 321O1 SAS No.: SDB No.s MUR001

Matrix (water/soil)s SOIL Level (low/med)s LOW

X Solids for Samples 83.4 . "•: Solids -for Duplicates 80.3


! Analyte>I AluminumI AntimonyI ArsenicI BariumI BerylliumI Cadmium!CalciumI ChromiumI CobaltI CopperI Iron!LeadI MagnesiumI ManganeseI Mercury!Nickel!PotassiumI Selenium« 3 i1ve r!SodiumI ThalliumI VanadiumI Zinc!Cyanide

ControlLimit

47.51.2

5.9

9.5

2.4

11.9

4.9

Sample (S) C

3034377903 i"6.1733IUST. 2224 IB74.493011.2091J-80O3IB

339. 1670 IB24.7395!10. 0909 IB14.16721

23197.487O!10.23931712.99461B368.1684!

-1142IU17.8207!61O.3079IB

.7123IU2 . 4739 I

133. 9031 IB-7123IU

47.6826!36 . O384 !4.8348IU

Duplicate CD. C

18793752527™6.2350IU1.1990 I U

• 60.15221.9954 IB.7194 I U

343. 9675 IB19.634517. 8465 IB10.66941

2O194.666OI10.53241

588. 0194 IB331.8914!

.1090 I U12.4859143O.8673IB

.7194 I U2 -1644 IB

113. 5546 IB.7194 I U

39.3763 I3O.7651 14 . 6838 ! U

SfiRPD

4775

200.021.319.4200.01.4

23.025.023.213.82*3

19.21O.4

35.234 . T~.

13.316.4

19.115.8

t1

QIM

*|p"IPIFIPIPIPIP

*!PIPIPIPIFIPIPlevIPi C'

IF: F'IPIF-IPIP1C

FORM VI - IN7/88

fl«IOI5l»3

U.S, EPA - Cl P

L'A - EP.i BAMPLli- Hu.,SPrKG" SAMPLE' RECOVERY

L«.b Hamefi SOUTHWEST LAl< OK OK <;<:mti-,?.c ..c A'3™»9--OOtt9

Lab Codes JtfijOK Cast? No.s 321 Ol Sfi£> Ha „ s feDt. llo.. s MUK'OOI

Matrix : TOIL L «•"*;. il •; :i.ow/mt*d "» •' U.t;i

M y o 1 i c( * * t c> r & a.*, p I e a 83. 4

CD.I c t? n t r & t i or> Un :i t s* f. u.g /L o i run -• I- o •:! ? v v. ** i g l i t / .t ril'/K 0

I Control!! Limit ! Spited Sample

• ii »t'i.I. UthXPK'.fH .

Ar.-i,:i,rh;,nx ? 7^-125 ' . :i.7.971Orirsenic ;/!.'-l£"> ! ^^^ll.t?JLJariwm ! 7P-:125 I 48B, 1.937.to-r y J. 1 i t»m I 7 5-1 ES | 1? » 4792C^dmiUHr ! 75-125 ! 1.5..947?C--i J cium ! I

! (?hr oiiiiuft* . 7S»-t2? ! .._ 71_rDi^OJkv.b .L t i;7?--.li?5 I 1.PV'\9:-7:09^•ppei - , i_~ .{. ,-,. ,:• , \*-r* • / .;}Vt»P;*" ;..,r _t|r ;

i'l -ion F3^ 1 1 urt ' 'H^r,gAne<3e I 75-1 5 ! 475.A98!Here i.n ')-' . ITS- 125. ! ." . J, 51''!-6i,jj r.iH .'| i Vf51.— -! 21?7"* ' 1 . A "•XirtS"-*

1 "'.-.••'- assinmJ :<5<?.U?n;i tun ! /S-l^b ! 1 . 94«-*8:•= i 1 v c? r \ :•' 5 - 1. :? !:• ! - 1 '^ . 7 J ? 8Sod ium ; I1 hai .1. ium. I /?;•- 1K5 • 13« 6?V:3Ov':-rv*dxum. ! 75-125 ! 159 0780Z 1 r> c- ; / s- 1 :r3 } l ^ „ V'"'" .>Cy^n ide ! 75-123 ! 43 . 5A37

t 1 t I I Ii : " ' ., « '

• ! !- "II-1!I o .. .1 -33,:. ! U ! J 19.. 9" ! I. !> . 'J I W ! r' !! ..v -rru r y ,S9 : 77. j. - j r .1 7 ,,- oQ!" ! 47.,.: ; t;ic. . ;?> j : r- :! :i ., i'o'r'l..! ; 1 :l. .'/','•{ •?-. Bo; ;»•• ;! , «oo:5:3»! 11 .,w: .ir i...1,-. ni:r :; ; ; ; ' ;MRI1 y^ .. 7w9!. ; ; 47-96 ! 96- Vi I : 1 '! 1.<>..09O9,B! 1. -l.y.9-0! ^5J « 7> ! ! I-1* !! . .1 <! .. 1 67^ ; I 59 .. 9!=> ! 9« . O ! ! I" IJ « t i t i j.,»r-.

! - 5.1 20O ; : -:| „ BV ; ;.:!8 c'i .. * ; i N i r"1 • i • i : i ji .

: ^8»x^6A: : 1.19.90! Bf.v; :V v; - . i j -^ ".•: • u : ., ^'0 * i ost.. <;? i i r. vi -i A-9nv ' > i -i o on ' •."«<.> o " • i •i I. f - OfcW A . .' i 1 7 •• • ' ' • .?..-, i It , , , , ||;;.; t i i tl»

1 - .4739! : 11.99! 9 .1?! ;»'•! ; ' J ; IMI-:: .7133111: lu^i 11.4. : ;r

4 / . *«.::.* ! J 1 1 - .. 90 ' -92,9! ! p; .':*.(»V-i^1 ; 119 .90: <?*. .7! IF1j 4.8Vie!U! 42--37J 1O2.H! ! n

FORM V (P:•>'"* I ; •- I

U.S. EPA - CLP



Lmb Code: SWOK Case No.: 32151 SAS No.: 30(3 rig.: .l??V_••<:• t


Aqueou« LCS Source:

ii

\ Analyte

! AluminumI Antimony! ArsenicI Barium! Beryl 1 iumI Cadmium! Calcium'Chromium! Cobalt! Copper! IronI Lead! Magnesiumf Manaanese! Mercury! Nickel'Potassium! SeleniumISilverI Sod iumJTh*ll ium! Vanadium!ZinciCvanide,*

Aqueous ( ug /L )True Found "/.R

Solid (mg/kg)True Found C Limits *'.R

325.0! 307.9!211.0! 172.6!917.0! 828.0!4.8! 4.4!B

19.4! 18.6!45.4! 46.3!

196200.01204097.6!99 . 6 ! 85 . 5 !144.0! 131.9!6910.0! 6931 .1 !22430. O! 18908.1 !236.0! 232.8!

118100.0! 123823.3!208.0! 212.0!12.7! 11.9!6O.9! 55.0!5O.O! 69.0JU39 . 2 ! 50 . 4 122.2! 16.1!5O.O! 22S.61B39 . 0 ! 38 . 7 !65.6! 59.1!187.0! 170.1 !

j « 6 I -j . v ir it i

225.0127.0635.00 . 0

16.535.7

166800.079.2

124.06O06 . 017770.0188.0

100400.0- 177.0

3.549.20 . 0

19.115.50 . 024 , 651.7

138. 04.3

424.029 4 . 01199.040 . 022. 755. 1

225600.01 20 . 0t ~>2,''

~"32C!.'"i27O9O . '"'

2Q*!> ."129900 . 0

TT^.O17.-:'"C. ij

t 0'"»O . • iS9 . 4. ""^ . ' '

i ;» t. . . .^ 7 . T''" f 5

^ r iz . ' *i

74.781 .890.7-91.795.910 2. 0104 .085.8«"'

98.6106.5P.'l .993.7'*''*) " ~~0 . 0

128.6— -s BT

457..:*~ ? • k.H9 .50 1 . 0

1 05 . 4

J;

T

FORM VII - IN7/88

U.S. EPA - CLP


Lab Name: SOUTHWEST LAB OF OK _ Contracts 68-D9-OO89 ... -.

Lab Code: SWOK Case No.: 32101 SAS No.: SDG No.: MURO01



I1

I Analyte

1 Aluminum1 Antimony! Arsenic! Barium! Beryllium

-J CadmiumICalcium! Chromium! Cobalt! Copper! I ronILead1 Magnesium: ManganeseI Mercury1 Nickel! Potassium! Selenium! S i 1 ve r1 SodiumI Thallium! VanadiumI Zinc: Cyanide

Aqueous ( ug/L )True Found ":R

__.__._—.

.-

-

•— — — —•-»•

Solid (mg/kg)True Found C , Limits ":R----- _ — ™£ , -

211.0! 170.8!- 917.0! 793.51

4.8! 4.4IB19.4! 18.1!45.4! 45.3!

19620O.O!2O310O.4!99.6! 34.41144.01 132.2!6910.0! 6914.0!22430.0! 18551.8!236.0J 243. 41,

11810O.O:i262O7.6!208. O! 209.1:12.7! 13.416O.9! 54.3!50.0! 68.3IU39.21 35.5!i l .-£. t ~ 1 0 . £. i

5O.O; 241. l.B39.0! 36.6!65.81 56.71187. O; 163.5!

5.61, 6.41

225.0! 424.01 92. i127.0! 294.0! 3O.9635.01 1199. O! 86.5

O.O; 4O.O! 91.7* 1 ml **>*•* -if l f*»T» "v16.O, .C4L.O. 9v>.O35.7! 55.1! 99.8

1668OO . 0 ! 225600 . 0 ! 103 . 579.21 120.0; 84.7124.0! 162.01 91.86OO6 . 0 ! 7820 . 0 1 1OO . 11 777O . 0 ! 27030 . O I 82.7188.01 285,0! 103.1

10040O . 0 ! 1 29900 „ O ! 106 . 9177. O! 239.O; 10O.58.5! 17.0! 105.5

49-21 72,61 89.2O.O! 1000... 01 O.O

19,11 59.4! 90.615.5'. 29.0! 73.0O.,01 10OO.O!48£.2

24-61 53.5! 93.851,71 79.9', 86. 2

1 38 „ 0 1 236 . O 1 37 . 44,3', 6 . 9 1 11 4 . 3 1

FORM VII - IN7/83

0-000470

U.S. EPA - CLP


Lab Names SOUTHWEST LAB OF OK Contract: 68HD9-OOB9

Lab Codes SWOK Cam© No.: 321O1 3AS No.: _j_ SDG No.s MUROO;

Solid LCS Sources EPAO2B7

Aqueous LCS Sources EPA-LV

111

I Analytei! Aluminum! Antimony! Arsenic! Barium! Beryllium

J' CadmiumCalcium

; Chromium! Cobalt1 Copper1 Iront Leadmagnesium1 Manganese! Mercury1 Nickel! Potass:! umI 3o Ionium1 Silver! Sodium! Thallium! VanadiumIZinc1 Cyanide)

Aqueous (ug/L )True Found ":R

'

"

Solid (mg/kg)True Found C : Limi ts "-R

*

5.6 6">. 4^ 4.3 6.9

I

110.7

FORM VII - IN7/88

&000471

flR/0151.7

''1

U.S. EPA - CLP


Lab Names SOUTHWEST LAB QF OK Contracts 68-D9-OO89

Lab Code: SWOK Case No.: 32101 3AS No.: SDG No.: MUROO1


Aqueous LCS Source: EPA-LV .

Analyte

AluminumAntimonyArsenicBariumBeryllium

XCadmium_J Calcium

ChromiumCobaltCopperIronLeadMagnesiumManganeseMe r cu r yNickelPotassiumSeleniumSilverSodiumThalliumVanadium.ZincCyanide-

Aqueous (ug/L)True Found "SR

_.»._ " ' '" "" ' ' ' ""

_ ._. _

Solid (mg/kg)True Found C Limits ":R

«.»..«. ..liuj-.——— l»l . ———

*

5.6

~"""™"~* *~ •••*•• •••|""~

*. <?V." • 7

*"• ——— ru —— ut —— .,—— _™ **"*

4.3! 6.9

"*" "* '

10,5.4

FORM VII - IN

0-00047;


CLIENTS URS CONSULTANTS, INC. REPORT, 3210b570 DELAWARE AVE.BUFFALO, NY 14202 DATE: O8-22-9OATTN: PETER FAIRBANKS

LABORATORY BLANK

SAMPLE MATRIX l SOILSAMPLE IDs METHOD BLANK

DETECTIONCOMPOUND LIMIT (Bd/Ka)

TPH 10. 0

TPH Tf*IX SPIKE/MATRIX SPIKE DUPLICA*

SAMPLE MATRIX! SOILSWLO # 3210.11/3210.12 (MS/MSD)PROJECT: DELAWARE SAND «c GRAVELSAMPLE ID: UR-11 (MS/MSD)

SPIKE CONC. SAMPLE CONC.(wg/Kg) (»g/Kg>*

TPH 667 16

USD CONC. USD PERCENT(»g/Kg) RECOVERY

SAMPLE AMOUNT j 30GDILUTION FACTORS 1

AMOUNT FOUND(mq/Ka)

ND

TE RECOVERY DATAi

MS CONC. MS PERCENT(Mg/Kg)* RECOVERY

660 97%


TPH 58O 857. 137.

* » DILUTION FACTOR NOT APPLIED TO THESE CONCENTRATIONS

00047J


CLIENTS URS CONSULTANTS, INC. ' REPORT. 321Oa570 DELAWARE AVE.BUFFALO, NY 14202 DATE! OB-22-9OATTN: PETER FAIRBANKS

LABORATORY BLANK

SAMPLE MATRIX: SOIL SAMPLE AMOUNT: 3OGSAMPLE ID: METHOD BLANK DILUTION FACTOR:. 1

DETECTION AMOUNT FOUNDCOMPOUND_______________LIMIT (no/Kg)_______________(»g/Kql

TPH 10.0 ND


SAMPLE MATRIXs SOILSWLO # 3210.01 (MS/MSD)PROJECTS DELAWARE SAND It SRAVELSAMPLE ID: UR-1B (MS/MSD)

SPIKE CONC. SAMPLE CONC. MS CONC. MS PERCENT(*g/Kg> (*g/Kg)* («g/Kg)« RECOVERY

TPH 667 12 600 887.

MSD CONC. MSD PERCENT RECOVERY PERCENT(•g/Kg) RECOVERY DIFFERENCE

TPH 620 91* -37.

* =* DILUTION FACTOR NOT APPLIED TO THESE CONCENTRATIONS

fe-00047fHO 1550


Lsb Name: SWL-TULSA_______________ Contract: URS______^_

O Code: 5UJQK Case No.: URS SAS No.: ______ "SDG No.:

ti- i.; 3oiJ» - EPA Sample No.: UR-2 9_______^_ Level :< low/rned . LOW

COMPOUND

i . 1-Dichloroethen*Tr i c n 1 oro© t h©n©BenzeneToluene . . _ChloroDensen©

SPIKEADDED( ug /Kg >

63.363 . 363 • 363 . 3<b3 . 3

SAMPLECONCENTRATION

(ug/Kg )

00000

MSCONCENTRATION

< ug/Kg )

60 . 952.957.36!3.86-2.4

MSy

REC 4*

968491

1 0190

QCLIMITSREC.

59- 17^67. -I I"766-14259- 1. :- -?60-133

COMPOUND

1 , 1-Dichloroethen©Trichloroethen©Ben:: anaTolueneChlorobenrene

SPIKEADDED(ug/Kg )

50 . 050 VO50.050 . 050 . 0

MSDCONCENTRATION

( ug/Kg )

46.342.147.049.448.4

MSD

REC #

93S4949997

RPD #

' o2

_

QC L]RPD

2421 .2 121

MIT'SREC.

59-17262-13766-142

60-17.3

!* Column to be um^d to fl^g recovery and RPD values with an asterisk


KpD s _0 out o-f _5 outside limits ;Soil,© Recovery: _Q. out of 10 outside 1 imits ] - -

•.DMMENTS: UR-29 URS . —INST:I SWL#3238.181

000470FORM III VQft-2 : I/37 Rev

A R 1 0 I 5 5 J


Lab Names SWL-TULSA_______________ Contract: URS_______

Lab Code: SWOK Case No.: URS SAS No.; SDG No.:

Matrix Spike - EPA Sample No.: «UR-29_______, J.ey©l : (low/med) LOW

COMPOUND

Phenol2— Ch lor o phenol1 ,4-DichlorobenseneN-Nitroso-di-n-prqp . ( 1 )1 P2,4-Trichloroben2ene_4-Chloro-3-methyl phenolAcenaohthene4-Nitro phenol2 . 4-Dini trotoluenePe'ntachloroohenolPvrene

SPIKEADDED(ug/Kg)

1 690O16900344034403440169OO3440169003440

1 690On n n --,CJ " i t *»'

! SAMPLE! CONCENTRATION

! 0! 01 0I • 0i 0! :T 0! 0! 0! 0; 0"-! 011

MSCONCENTRATION

_<ug/kg>

9370988049OO5230599O120004810116005990138006810

MS

REC ft

55585B62717157t Q

O7

7132Q 1O 1

GCLIMITSREC.

26- 9025-10228 10441 12633 10726" 10331-13711-1142S- 8917-10.935- 1 42"

'„-

COMPOUND

Phenol2-Chlorophenol1 , 4-Dichloro benzeneN-Nitroso-di-n-prop. ( 1 )1,2, 4-Trichlorobenzene4 -Chloro-3-me thy 1 phenolAcenaphthene4-Nitrophenol2, 4-Dini tro toluenePen tachloro phenolF'yrene

SPIKEADDED(ug/Kg)

1690016900844084408440169008440169OOS44O169008440

MSDCONCENTRATION

C ug/Kg)

10500106005860562066501330O538013 BOO6700147007620

MSD•/

REC tt

62636967797964B 1

798790

7.RPD ft

-12-a-17-8

- -u-11-12-17-11-6

-11

QC LIMITSRPD

•J'Zl

502738Tji-j331950474736

REC.

26- 9025- 1 022B 10441 12638 10726 10331-13711-11428- 8917-10935-142

(1> N-Nitraso-di-n-propylamine

4. Column to be used to -flag recovery and RPD values with an asteriskt Values outside of QC limits

RPD: 0 out o-f 11 outside limits"Spike Recovery: _0 out ot 22 outside 1imits

COMMENTS s UR-29 URSINST:F SWL#3238.IS

£-000476FORM III SV-2 I''87 Pev-

A R I O I 5 5 2


Lab Name: 51ML-TULSA_______________ Contract: URS_____

Lab Code: SWDK Case No.: URS SAS No.: ______ SDG No.:

Matrix Spike - EPA Sample No.: UR-29______ Level:(low/med > LOW

!.

COMPOUND

gamma-BHC (Lindane)HeptachlorAldrinDieldrxnEndrin4,4'-DDT

SPIKEADDED< ug/Kg)

67.4.67.467.4168168 "168

SAMPLECONCENTRATION

(ug/Kg)

000000

MSCONCENTRATION

( ug/Kg )

27.556 .142.8v 5 • •_>13979.7

MS'/.

REC ft

41 *8364578347

QC :LIMITS!REC. 1

—— ss ——— J

46-127!35-130134-132!31-134!42-139!23-134!

ti

COMPOUND

Qamma-BHC ( Lindane ) ___HeptachlorAldrinDigldrinEndrin4,4'-DDT

SPIKEADDED(ug/Kg>

67.467.467.4168168168

MSDCONCENTRATION

(ug/Kg)

32.170.450.710816395.0

MSD7.

REC ft

4810475649757

7.RPD ft

32SS3JSSS

-16-22-16-12-16-19

iQC LIMITS RPD

503143384550

REC m-==ss-™46-127!35-130!34-132!31-134!42-139!23-134!

ft Column to be used to -flag recovery and RPD values with an asterisk


RPD: _g. out o-f _6 outside limitsSpike Recoveryj _|_ out o-f _12 outside limits

COMMENTS:

FORM III PEST-2 Q/87 Re

fc-000477

flR I 01553"


6DUPLICATES

Lab Name: SOUTHWEST LAB OF QK Contract: 68-D9-O089MU3818D

Lab Code: SWOK Case No.: 32381 SAS No.: SDG No.: MU3S01


7. Solids for Sample: 80.8 7. Solids -for Duplicate: 80.5

Concentration Units <ug/L or mg/kg dry weight): MG/KG

J1 Analyte

{Aluminum! Antimony1 Arsenic! Barium! Beryl lium1 Cadmium! Ca 1 c Turn! ChromiumI Cobalt1 CopperI'lronILead(Magnesium! ManganeseI Mercury1 Nickel1 Potassium! Selenium1 Silver1 Sodium! Thai lium! VanadiumIZinc! Cyanide

ControlLimit

1213.4

.7

12.1

iSample (S) C!

12669.73101 110. 75731 BI1. 59681 B!

3S.4616'!B!.5859IB!. 728O ! U J

415.46B5IB!15.2248! !4 . 7935 ! B I3.8827JU!

11956.7090! !35-. 1145! !4S7.2812IB!193.4232! !

. 1076IUI7.9070IB!

317.8021 !B!.7280! U!

1.1 coo i B i89. 0604 "!U!

. 7280 ! U !29 . 4925 J !24.28231 !2. 1637IU!

i i

jDuplicate (D) C!

9489.6451 ! J7.1O34JB!1.2134IU!

f£. A . -TO l D i•-'O • O i OO i O l

. 4800 I B !• SI / •_> i 3 i

1418.1846! !12.5031.' !3.9152IB!3.8827IU!

1O423.1550! .'64.9146! J

527. 1464 IB!154.9957! I

. 0952 ! U J5. 8295! B!

25S.17461B!. 7260 ! U !.3757 !B!

89.0604JU!. 7280 ! U !

25.3255! !25.0888! i1.S695IU!

V.RPD

28.7. 40.9200 . 04.919.9200.0109.419.620.2

13.759.67.9

r** f.i— . • 1

30.220.7

25.8

15.2• T;

!Q!M

*!P!P;F!PIPIP! PIPIP!PIP

*IFIP

*!P!CVIPIPIFIP-IPIFIPIP1Cii

FORM VI - IN7/88

&-00047S

10 I 551*

U.S. EPA - CLP

SA EPA SAMPLE NO.SPIKE'SAMPLE RECOVERY

MU3313S',ab Name: SOUTHWEST LAB OF OK Contract: 6S-D9-0089

Lab Cod*: SWOK Case No.:.323Sl SAS No.: SDG No.: MU3801


7. Solids -for Sample: 80.8


! (ControlI I Limit1 Analyte i 7.R• i• i{Aluminum !.'Antimony ! 75-125.Arsenic 175-125J Barium ! 75-125! Bervl 1 ium i 75-125! Cadmium 175-125iCalcium !J Chromium I 7 -125ICobalt 175-125i Capper ! 75-125! Iron I! Lead \agnesium!

. i-langanese! 75-125! Mercury ! 75-125! Nickel ! 75-1251 Potassium!! Selenium 175-125! Silver 175-125! Sod ium !! Thallium 175-125! Vanadium !75-2?IZinc 175-1251 Cyanide ! 75-125• t

Spiked SampleResult (SSR) C

ii34 . 0555 !9 . 7252 !

540 . 0754 !13.3160!17.5714!

i65 . 5982 !129.6936!64.4117!

i38.3663!

ii258. 8459 J

.5518!137.2036!

i2.6634!13.7098!

»•1 1 . 5050 !154.8102!149.2531 '16.5940!

J

SampleResult (SR) C

~i

10.7573!B1 . 5968 ! B

•J. o • 46 lo i B, 5859 ! B. 7280 ! U

!15.2248!4 , 7935 ! B3 . 8827 ! U

ii35.1143!

•i193.4232!

.1076IU7. 9070 IB

ii. 7280 ! U

1.1356IBii

. 72SO 1 U29 . 4925 124 . 2823 !2.1637JU

•.

SpikeAdded (SA)

_123.769.90

495.0512.3812.38

49.50123.7661.88

4.95

1 OT TAJ. jl. . / Oe-'t. -f-i

T23.76

• 2.4812.38

.: .12.38123.76123.7613.98

7.R

13.832. 1101 .1102.3141.9

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107.4101 .6

92. 9toi .3101.087,4

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Comments:


£-000473

101555

summary report consultants, inc. volume 2 of 2

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