AUG 2 0 2015

Jon A. Franke Site Vice President

U.S. Nuclear Regulatory Commission Attn: Document Control Desk Director, Spent Fuel Project Office

Susquehanna Nuclear, LLC 769 Salem Boulevard

Berwick, PA 18603 Tel. 570.542.2904 Fax 570.542.1504

jon.franke@talenenergy.com

Office of Nuclear Material Safety and Safeguards Washington, D.C. 20555-0001

SUSQUEHANNA STEAM ELECTRIC STATION 10 CFR 71.95 REPORT REGARDING ENERGY SOLUTIONS 8-120B CASK CERTIFICATE OF COMPLIANCE 9168 PLA-7374

TAL EN~ ENERGY

Docket Nos. 50-387 and 50-388

Talen Energy, Susquehanna Nuclear, LLC hereby submits the attached report in accordance with 10 CFR 71.95(a)(3). Licensees are required to submit a report regarding the instances in which the conditions of approval in the Certificate of Compliance for the 8-120B Cask (Certificate of Compliance #9168) were not observed when making a shipment. The circumstances regarding the need to submit this report are described in Energy Solutions Report, CD15-0149, dated June 24, 2015 (Enclosure 1).

Susquehanna Nuclear, LLC has made four (4) shipments with an affected cask (numbers 8-120B-1, 8-120B-2, 8-120B-6 and 8-120B-1S) during the affected 21-month period as described in the Energy Solutions report. Information regarding the four shipments made by Susquehanna Nuclear, LLC is included in Enclosure 2 to this letter.

If you have any questions regarding this letter, please contact Mr. Jeffery N. Grisewood, Manager, Nuclear Regulatory Affairs, at (570) 542-1330.

This lett ·contains no new regulatory commitments.

0--J. k.. Franke

;:losure l) Energy Solutions Report, CDl5-0149, dated June 24,2015 ~~~~losure 2) List of Susquehanna Nuclear, LLC Shipments Using the Affected Energy Solutions 8-120B Cask

- 2-

Copy: Mr. J. E. Greives, NRC Sr. Resident Inspector Mr. D. E. Jackson, NRC Region I Mr. J. A. Whited, NRC Project Manager Mr. M. Shields, PA DEP/BRP

Document Control Desk PLA-7374

Enclosure 1 to PLA-7374

Energy Solutions Report CDlS-0149, dated June 24, 2015

~ ================ENERGYSOLUTIONS================

June 24, 2015

Mark Lombard, Director Division of Spent Fuel Management Office of Nuclear Material Safety and Safeguards U.S. Nuclear Regulatory Commission Washington DC 20555-0001

ATTN: Document Control Desk

Subject: 10 CFR 71.95 Report on the 8-120B Cask \

Dear Mr. Lombard:

CD15-0149

EnergySolutions hereby submits the attached report providing the information required by 10 CFR 71 .95(a)(3) for instances in which the conditions of approval in the Certificate of Compliance for the 8-120B Cask (Certificate of Compliance #9168) may not have been observed in making certain shipments. The circumstances described in this repmi are applicable to approximately 235 shipments made by EnergySolutions as a licensee and user of the 8-120B cask over a 21 month period.

If you have any questions regarding this submittal, please contact me at 801-649-2109.

Daniel B. Shrum

dJaJ£L Senior Vice President, Regulatory Affairs EnergySolutions LLC

Dan Shrum Jun 24 2015 2:58PM

Attachment: Failure to Observe Certificate of Compliance Conditions for the 8-120B Vent Port Leak Pre-Shipment Leak Test

cc: Michele Sampson, Chief Spent Fuel Licensing Branch

Pierre M . Saverot Licensing Branch

299 South Main Street, Suite 1700 • Salt Lake City, Utah 84111

{801) 649-2000 • Fax: (801) 880-2879 • www.energysolutions.com

~ ==============~ENERGYSOLUTIONS==============~

Failure to Observe Certificate of Compliance Conditions for the 8-120B Vent Port Pre-Shipment Leak Test

June 24, 2015

1) Abstract During the vent port seal pre-shipment leak rate test, a neoprene gasket that was added under

the test manifold may have reduced the test sensitivity below the required value. The test

manifold and gasket are not licensed packaging components. The gasket was added to the

test manifold on some or all shipments to more reliably seal the manifold, saving test time and reducing personnel exposmes. The amount of reduction of the test sensitivity cannot be

determined for any patticular shipment due to several reasons as discussed below. The

gasket may have been used on as many as 100 shipments by EnergySolutions as the licensee

:fi:om September 2013 through June 2015. The condition was detennined not to have

significant safety consequence because the seals receive periodic helium leak testing as

required by the SAR, the vent ports are only opened rarely, there is a margin of conservatism

of approximately a factor of 9 on the prescribed vent port leak rate test, and there have been

no observations of contamination around the vent port openings that would suggest leakage.

There will be no further tests made using the gaskets since EnergySolutions has replaced all

of the subject gaskets with a modified version that does not have the potential to reduce the test sensitivity.

It is uncertain whether, or by how much, the sensitivity of the vent po1t pre-shipment leak

tests was reduced because: 1) Use ofthe gasket was optional- the gasket may, or may not

have been in place for the tests, and 2) The force with which the gasket was compressed

dming testing is unknown, so it is uncertain if caused the gasket to constrict onto the head of

the vent p01t cap screw.

2) Narrative Description of the Event

a) Status of Components All ofthe 8-120B packaging components are operating normally. The neoprene gaskets

that caused the event have all be removed from service and replaced with a new manifold gasket, as discussed in ( 4) below.

b) Dates of Occunences From September 2013, when pre-shipment leak tests were first performed using the

neoprene gasket, to present, approximately 1 00 shipments were made by EnergySolutions as the licensee. Most of these shipments used the neoprene gasket to perf01m the pre­shipment leak rate test of the vent port.

2

~ ================ENERG ~OLUTIONS================~

c) Cause of Enor New 8-120B lids went into service in September 2013. It was found that the manifold sometimes had problems sealing with the vent port on these new lids. EnergySolutions

personnel found that adding an extra neoprene gasket helped to reduce the false test failures. Since the pre-shipment leak rate test is performed in a radiation environment,

false failures are undesirable because they increase the personnel exposure. The personnel did not realize that the gaskets had the potential to reduce the test sensitivity.

Attachment 1 has a detailed description of the test configuration.

d) Failure Mode, Mechanism, and Effects The neoprene gasket can constrict on the head of the vent port plug cap screw when it is

compressed by the bottom end of the test manifold stinger, which could reduce the sensitivity of the pre-shipment leak test. Consequently, the vent port pre-shipment leak tests performed using the neoprene gasket may not have provided the required test sensitivity of 1 x 1 o-3 ref-cm3 I sec.

e) Systems or Secondary Functions Affected Not applicable.

f) Method of Discovery of the Enor On Monday June 1, 2015, an 8-120B cask user identified a concem that the neoprene gasket could potentially affect the integrity of the vent port seal pre-shipment leak test. Later that week EnergySolutions perfonned a bench test that confirmed that the neoprene gasket can constrict on the head of the vent port plug cap screw when it is compressed by the manifold, resulting in a reduction of the test sensitivity.

3) Assessment of Safety Consequences Pre-shipment leak tests of all containment seals, including the vent port, were performed prior to every shipment in accordance with the requirements of Chapter 7 ofthe SAR. In addition, periodic and maintenance leak tests of the containment seals, using helium as the test gas, were performed after maintenance, repair, or replacement of the containment seals in accordance with the requirements of Chapter 8 ofthe SAR.

The 8-120B preshipment leak rate test criteria were sized for the large primary lid. Since the vent port has a much smaller test volume, the test specification is conservative. Calculations show that the test specified in the S AR is a factor of 9 more sensitive than the 1 x 1 o-3

ref-cm3/sec required by Chapter 8 of the SAR. However, due to the unce1iainties in the

effects of the gasket, and the behavior of seals in series, it is not possible to confirm whether the reduction in sensitivity is offset by the test criteria conservatism.

3

~ ================ENERG ~OLVTIONS================~

There has been no indication of any leakage from the vent port :fi·om any shipment, and

therefore, no exposure of individuals to radiation or radioactive materials due to the gaskets.

It is also noted that it is unusual for the vent port seal to be opened during cask operations, in

which case the previous helium leak test of the vent port seal provides added assurance of

seal integrity.

Therefore, it is concluded that there has been no safety consequence from performing vent

pmt pre-shipment leak tests that may not have provided the required test sensitivity of 1x 1 o-3

ref-cm3 /sec.

4) PlaiUled Corrective Actions EnergySolutions has taken conective actions to assure that use of the old neoprene gasket

design for the vent port pre-shipment leak test is immediately discontinued.

• EnergySolutions notified all 8-120B cask users with upcoming shipments to require use of a new procedure, in conjunction with the new manifold gasket design, for pre­shipment leak testing ofthe vent port seal on all future shipments.

• EnergySolutions designed and tested new manifold gasket design that does not constrict onto the head of the vent p01t plus screw when compressed, and therefore it does not reduce the test sensitivity. The new gaskets have been distributed to all upcoming shipment users. The new manifold gasket design is shown in Attachment 1.

The EnergySolutions drawing for the 8-120B air drop manifold have been revised to include

the new gasket seal, and the air pressure drop test procedure TR-TP-002 has been revised to

incorporate the new pre-shipment leak test procedure for the vent port. Use of the new

procedure and the new manifold gasket will assure that the pre-shipment leak test satisfies

the required test sensitivity and that the manifold gasket is removed :fi·om the test port after

completing the pre-shipment leak test.

5) Previous Similar Events Involving the 8-120B No previous similar events have been identified.

6) Contact for Additional Information DanSlnum

EnergySolutions

Senior Vice President, Regulatory Affairs

(801) 649-2109

7) Extent of Exposure oflndividuals to Radiation or Radioactive Materials None.

4

~ =======================ENERG /SOLUTIONS==================

Attachment 1

Details of the 8-120B Vent Pott Leak Rate Test Setup

The 8-120B CoC requires the package to be prepared for shipment and operated in accordance with Chapter 7 of the SAR, and tested and maintained in accordance with Chapter 8 of the SAR. Step 7.1.14 ofthe SAR requires a pre-shipment leak test of the primary lid, secondary lid, and vent port seals to be performed in accordance with Section 8.3.2.2 prior to every shipment to assure that the containment system is properly assembled. Per Table 8-2 of the SAR, the pre­

shipment leak test of the vent port is performed by connecting a test manifold to the vent port, pressurizing the seal and head ofthe vent port cap screw to 18 psig with dry air or nitrogen, and monitoring the pressure for at least 15 minutes to assure that it does not drop by more than 0.1 psig.

The pre-shipment leak test of the vent pmt is a pressure drop test performed using a dedicated test manifold. The test manifold is not a part of the licensed package. It includes a stinger (shown below), an 0-ring seal that contacts the stinger and the bottom of the vent pmt hole, and a sleeve nut to compress the 0-ring seal. The test manifold was designed so that it surrounds the vent port cap screw, leaving a small gap between itself and the vent port cap screw. The 8-120B

cask fleet began to ship with a new lid design in September 2013, and operations staff noted more fi·equent difficulty getting the manifold to seal. It became desirable to fmd a better way to

seal the bottom of the manifold in order to minimize operator exposure. They found that adding a neoprene gasket (also not part of the licensed package) under the base of the stinger as shown below helped reduce testing time and exposure.

5

~ ==~~~~~~ENERGY SOLUTIONS==~~~~~==~

VENT PORT SEAL

VENT PORT CAP SCREW

6

MANIFOLD STINGER

MAN I FOLD SLEEVE NUT

MANIFOLD 0 -RING SEAL

(NOT LICENSED EQUIPMENT)

NEOPRENE GASKET- SHOWN UNCOMPRESSED

(NOT LICENSED EQUIPMENT)

::~ ======================ENE G 'SOLUTIONS==========================

Conective Action - Modified Test Seal

The new manifold gasket design, shown below, replaces the manifold 0 -ring seal and neoprene gasket previously used with a neoprene gasket that fits within the notch at the base of the manifold stinger.

PRIMARY LID

VENT PORT SEAL

'·

VENT PORT CAP SCREW

\

7

SLEEVE NUT

\

NEW MANIFOLD GASKET (SHOWN UNCOMPRESSED)

Enclosure 2 to PLA-7374

List of Susquehanna Nuclear, LLC Shipments Using the Affected Energy

Solutions 8-120B Cask

List of Susquehanna Nuclear, LLC Shipments Using the Affected Energy Solutions 8-120B Cask

Shipment Date User Shipment ID Cask CoC User Manifest ID 3/30/2015 15-026 8-120B-2 15-026 4/09/2015 15-027 8-120B-6 S150077 6/02/2015 15-032 8-120B-1S S150106 6/16/2015 15-033 8-120B-1 15-033

Shipment 15-026

--

FORM540 ENERGYSOLUTIONS BARNWELL PROCESSING .FACiliTY 5. SHIPPER -NAME AND FACILITY SHIPPER 1.0. NUMBER 7. FORM 540 AND 540A PAGE 1 OF _1_PAGE(S) a. MAN!FEST NUMBER ] (6-97) ?PL Susquehanna. L:...C NIA FORM 541 AND 541A _1_PAGE(S) (Use th!s number on a!l continuation pages)

UNIFORM LOW-LEVEL RADIOACTIVE Susquehanna SES (KJM) FORM ·542 AND 542A __ PAGE(S)

I 769 Salem Blvd COLLECTOR 15-026

WASTE MANIFEST ADDITIONAL INFORMATION __ PAGE(S}

BerNick, PA 18603 PROCESSOR

SHIPPING PAPER S.C. TRANSPORT PERMIT NUMBER: I SHIPMENT NUMBER GENERATOR TYPE 9 .. CONSIGNEE- Name and Fr.u;trrty Address :'2 CONTACT

1. EMERGENCY TELEPHONE NUMBER D I ~ J. -37- IS-" 15-

026 X (Spedfy)

Bamv.•en Processing Facility · ~ I (Include Are:<J Code) NP RogerSetow "(s70)s42-3907 ·~,·

CONTACT TELEPHONE NUMBER Duratec Consolidation and Services Facllit>,o ~~- ~ ··~ .. TELEPHONE NUMBER (Include Area Cod~}

! {InClude Area Code} 'i6042 Dunbanon Boulevard ORGANIZATION Kimberly Murchison eam"en. sc 29812 (800)60H199

Shift Manager (570)542-3169 .

6. CARRIER - Name an::i Andress EPA ID NUMSER SIGNATURE - k.Jthoriz.ed consignee 3cl'.nc~cin9 ·tv3Sie receip~ DATE 2. IS THIS AN "EXCLUSIVE USE" SHIPMENT? 3.TOTAL NUMBER OF Hittman Transport Ser~ttces (C} NIA

PACKAGES IDENTIRED 740 Osborn Road ~YES ON THIS MANIFEST 1 SHIPPING DATE 10. ·CERTIRCATION

NO Bamvten. SC 29812 03f30l2015 "'This ts to ·Certify th3t the hw.e"tn- name::! rr~~3ria!s arl3 prop.eriy classffied, described, packa;OO, rr.Clr'rted, ~ ----> -- labeled and are in proper condition for tr.Eielsp.Jrt.:>:Wn acoording ·to the c.pplicab!e regulations of the Oepann~

4. ~~~i~~~~~~~r;D 0 YES CONTACT TELEPHONE NUMBER

of Transportation. Tl\is at:so certifies t-..<i't tht~ r.'"latl'..ria.!s .are classified, packaged, marked • .and label.ed and are EPA MANIFEST NUMBER (ln::lude Area Code)

RogerBeto\ (865}'8Hl 222 in pro~r cond'iti::m for transport:ati<m .;:::1a ~las ~cscrihcd ·in :iCCOrdance with the a;::~~teable

MANIFEST ACCOMPANY THIS X NO req~.tirements "~ 10 CFR Parts 20 and G·'. c.r equ.•.-a!errt state ..-egulations. ~

SHIPMENT? N/A SIGNATURE P:h~~~~ging waste receipt 3ori.Fd?.lS A~RI:~ SIGNATURE I TI~ DATE

If ·ves," provide Manifest Number ====> ". \/L.. \--,F Shlo2-t~ "2.,L3:i -~ \ c:: 11 . U.S. DEPARTMENT OF TRANSPORTATION DESCRIPTION 12. 13. 14. 15. e)TO!r~~ACKAGE

j iT. 18. TOTAL WEIGHT 19.1DEN11FJCATh'1N ·

(Including UN 10 number, proper shipping name. hazard class. and any DO'i"LABEL TRANSPORT PHYSICAL AND CHEMICAL INDIVIDUAL RADIONUCUDES ~TY lSNSCO MlD OR VOLUME NUM9EROF

additional information) "RADIOACTIVE" INDEX FORM MBq met CLOSS (Use appropriate 1.mfts) PACKAGE

UN2916, Radioactive material, Type B(U) package, 7 YELI..OWIU 4.0 Sefid/ H-3 C·14 5.76E<\'l6 (1.508-05) NIA 29756.2 Kg USAt916818{U)-G6 RQ - Radionudides Meta! Oxides 55600.0 Lbs 8-1209-2 1 Metal Cask Mn-54 Fe-55

Dewatered Reactor Water Clean-up Resin Go-58

I Co-60 l Ni-63 Zn-65

Sr-89 Sr-90

I Nb-95 (Tc-99-LLD)

(1-129-lLD} Cs-137

-

t-I

l l ' I

FOR CONSIGNEE USE ONLY 20. "Certification is hereby made to the South Csra£na Oep-al"tment of Health a:o.d Enviroorne.:'lt::d C Y.lrol t.~ ·this shipment of kw.·-level radioactive v.-aS1e has been Inspected in acccrdance w+th the requirements of South ·c.aro4.""<! 'Rad\.oa!':tive Material License 287-04 as amended. ar.d lhe effective consolidation facility acceptance criteria, within 4'8 hours prior to shipment. .and~ certif~Ca:ion is made tha.t the inspection revealed r.o tt.&>ns of non-compliance wit!'\ au aopticable laws, rules and regulations."

~- - \\ ~ ~gnature 0-:;{t:j~ Oa\e • :J._; ':::> ~ n · I \

TiUe and Organ!7..ation K\1 ~\I ~~'Yt~ Telephone No. ( --~· ) ':)'7-:z. 1.4Jl,7--,

---

FORM 541 (10-96)

ENERGYSOLUTIONS BARNWELL PROCESSING FACIUTY j 1. MANIFEST TOTALS 2. M.:.."'H'EST r>IUMBiOft ·~ NUMBEROF 1 1 SPECIAUJUCLo:ARMATERIAL(grams) " 5-02(; ~

UNIFORM LOW-LEVEL RADIOACTiVE WASTE MAN!fEST

PAC~.AGESJ NET WI<STE I NET WASTE I I ' ·~ CONTAJNE~- 3. • DISPOSAl,;= VOLUME WEIGHT U-233 U-.<35 Pu TOTAl ---!~

CONTAINER AND WASTE DESCRIPTION ----- N P NP N P NP 1 PAGE __ 1 __ PAG::. Of __ 1 __ ?.:~8-E(Sf )t m! 2.832 I >.g 2507.0 j I _ _ '• lb

5527•0 1 ~ - SHIPPER NAME r. !!3 100.()')

SOURCE ??L Susq;"'.l--""%, l.lC ~ f--- Adivilr(MSq/mCi)

·C-14 ALL NUCLIDES TRITIUM 'io·!fr" Additlonal Nucl~a.· Regulatory Commission {NRC) -Requirements far Cortlral, Tr2nsfer and

Dispcsat of Radioactive waste

1-129 ~

SH\PMENT \D NUMBER - ~· M5Q (9.37E-<l1) .:ti NP !

5. 6. ' · CONlAlNER CONTAINER

IDENTIFICATiON DESCRIPTION VOLUME

NUMBER/ (See Note 1 & S.C. TRANSPORT Note1A) PERMIT NUMBER

m3

I ftJ

L 10-09 (original sur 113-A 3.407

vey)

120 .30

PO-Q06727-1 EnergySolutions. t.LC CNS PL8-i20 DHEC-HIC-PL-001

·sl\ipffient Total : 3.407

120.30

NOTE 1: Cor:.tamer Oescriptio:'l Codi!S. For containerSl\1.-a~e requiring dispos.lt in approved stroctJ.:tral everpacks, the m.m~rical ccx:!e cr.ust be foll0041-'ed by .. -QP ...

1. Wooden Box or Crolte 2. ~~C'.al Sox 3 . ?!asllc Drum o; P<lil <. Metal Drum or Pail '5 . i\~J Tan~ cr Uner '0 . Concrete Tank or Uner 7. Polyethylene Tank or Uner 8 . Fiberglass Tank or Liner

9. Oernir.&alizer 10. Gas CY,~'\dw 1, . Bulk. Ur.padW'J-'ld W.!l.S".!" 1l. UrrP!.Ckaged cOmponents 13. Hig-h lx..~;t'J Centainer 19. O:net , 0 -!'SCJIOC> in item 6. 0!'" acal!ic:"'a\ page

mCI (2.53E-<l2) 1 \b "-'? NIA ~

0.

:URF~.CE llU. SURFACE

COHTAMIW>TION WASTE AND CONTAJ~~ER RAD1ATION M'Bq/100 cm2

WEIGHT LEVS.. dpm/100 cm2

kg mSvntr I ALPHA I SETA-GAMMA

\b mremlhr

2903.0 Kg 920.000 I <3.33E-<l7 I < 1.src:-os

'64oo.o Lbs 192ooo,o T < 20 I < 1000

2903:0-

64CD.O

WG H I

2.832

100.00 NP

"

I i 1 j---~-, r ] I l I I l

NOTE 1A:. Sam-KOII SpecifiC Container" DescriptiOn Codes {Oiocs<:! one cede as rmy be a~plicabSe . )

N0!2 2· Waste Desctlplor Ccc!es. (Choose up1o OVee w~.dl predominalc by volurr-.e.) 11 Wast.e Oes.::.rip.~~ . C.O.~. F<"...- n-e::liarnaetr..gd~/G.!G · S~ ~ ~2A.:Bam1.el~ JI'NOTE 3 : So\id'tfic.!.:lc\13'l\dSta'CAiiu.tkm~~:.<e · ~~i0\E'S)\:E.ii·:rr~ ~~

A High lr:::egrity Container - Pc*y El Higl'lln!egrity Conlalner - Poiy ~~h Steel St.et: C Hlgh rr.:egrity Drum ~pack - ?eli)· 0 High Integrity Container - SlainleM ~~ E H1gh lmegrlty Coma1ner- Fiber;!nss F Uner- Steel

2C.. Cl':larcoal 21 . 11"1Cinet"3tOfA'Sh Z2. Sc.i1 23 . ~s 24. 0i1 25. A.q~..z:; Uqu:d 26. Filte: Meola 27 Mecl".anlcal Fillrs 22. EPA Of Stc:te Ha2art!O'I:JS

29. Demolition Rut'ble 30. Catron lon~Exc:har.ge f~ia 31.A:!'"Iioo ton-Exdta.Tl'~U'~ 32. Mixed Bed 101'\-E~"'B ,.,.e<f~a JS. Contaminated Equi~ 34. Orge.nic Uquld (e~--c:ii) 35. Glassware or La.b'..are 36. Sealed Source~Dev'ic:e ~7 . Palr.tor Plntlng

58. Eva~tor 3ot:t.,m~"51~g~fC'M~rzl"'..t~:.l!'.es 39. Compactible i r.!l!>r• ~0 . Noncompac;!:::s Trc:s.t-t 41 . Amma1Ca~ <2. Siolog!ca l lll.e::e:"t<~l.~e~:vt a~l

catca!.s) ~3. Activa.J:-a.::1W.cteria l

sg 011\ef Oesoioo 1:1 t.~.:n t ~. N udoroc·.u-t page

(CI'IOO""...e 21U Cl~~cOOel... - S'..!'..ld.u!t!l !tll.':lility reQuircm&O!S, tn•::·nu::::r--. : ~~lSI . !Sd!D'~ lfic;Y.ion - ~·:, co.1fi rt"U:lbefc:k:!~ P.,-"'-s-". RJ:Ci'. : ,<ft.\t:! '~Zttit\u~fjc(l 1r S'Ollcfitlr.at\tln~i~.th~ver\Cior-a-~t.mra:: ·~.:r , f~~!aCO'U:.;. )$

G 0~"3te."'«" • • musl.:r.!sobeide.ntifi l!d tn Item 13.Coer-!: 200-'2 ·~ 1tcr~r;"\ls-l,:OI~o{l- \l

H Solid '"-""' R""""""· . ~~l:<ol ~ , eomo·""""' soro>licalior. .a J t~':)n--carnbuT.it-l-.. , ' Y.l Cetretlt 94. Vinyt eter s-~~"\:e K~FIJtra{Y.)nri!"..&Z 91 C.:mc:~ 99 oa-.er.Ow .. r!be""l~~m 1 LA.'ibestr.-s (Ena;~la:Y."'fl~ 13 or addib:;m.al p.ia£! ~~ tJ \'/.;;.,,.._.., ~

S2 eitumM 1('0 /.'oi(X)~ F0:i~~ d C':l Vitwl rl'l lnrin"' \)

Shipment 15-027

FORM 540 ENERGYSOLUTIONS BARNWELL PROCESSING FACILITY 5. SHIPPER -NAME AND FACILITY SHIPPER I.D. NUMBER 7. FORM 540 AND 540A PAGE 1 OF _1_PAGE(S) B. MANIFEST NUMBER (6-97) PPL Susquehanna, LLC NIA FORM 541 AND 54 1A _ 1_ PAGE(S) (Use this number on all continuation pages}

.UNIFORM LOW-LEVEL RADIOACTIVE Susquehanna SES (KJM) FORM 542 AND 542A __ PAGE(S) 769 Salem Blvd COLLECTOR S150077 WASTE MANIFEST ADDITIONAL INFORMATION __ PAGE(S)

Berwick, PA 18603 PROCESSOR

SHIPPING PAPER S.C. TRANSPORT PERMIT NUMBER: .I SHIPMENT NUMBER GENERA TOR TYPE

9.CONSIGNEE- Name and Facility Address CONTACT (Sped1y) 1. EMERGENCY TELEPHONE NUMBER (Include Area Code) 0 l G:J--)--;-7 -IS -X s1soon

X NP 1(5 Roger 3etow Barnwell Processing Facility -- (5i0)542-3907

CONTACT TELEPHONE NUMBER (Include Area Code) 16043 Dunbarton Boulevard TELE?HONE NUMBER (Include Area Code)

ORGANIZATION Kimberly Murchison Bam'A~II. SC 29812 (800)607-6199 Shift Manager

(570)542-3169

6. CARRIER- Name and Address EPA ID NUMBER SIGNATURE- Authorized consignee acknowledging msta receipt DATE 2. IS THIS AN "EXCLUSIVE USE" SHIPMENT? 3.TOTAL NUMBER OF Hittman Transport Services (C) NIA

_.P4 YES PACKAGES IDENTIFIED 7'0 Osborn Road ON THIS MANIFEST 1 SHIPPING DATE 10. CERTIFICATION

NO Bamwei. sc 29812 04/09/2015 "This is to certify that the herelr. - named materials are properly classifi'3d. described, packaged, marked, and --=-> labeled and are In proper condition for transportation according to the applicable regulations of the Oepartmerrt TELEPHONE NUMBER

•· ~~~~~~~~~y~T;D w YES EPA MANIFEST NUMBER CONTACT (Include Area Code) of Transportation. This also certifies that the materials are cl3ssified. packaged, marked, and labeled and are

RogerBet~w (865)461-0222 in proper cor.dition for transportation and disposal as desalbed in accordance with ttie applicable

MANIFEST ACCOMPANY THIS X NO requirements of 10 CFR Parts 20 and 61, or equlvaient state Tegulations." SHIPMENT? N/A

SIGNATU! ' A~ .carrie acknowk!dging waste receipt oA4E k>t IS"'

AUTHCj5)ZED SIGNATURE TI)LE DATE

1f •ves," provide Manifest Num~r ====> . .~ .... r'/"-/L.... fL.-P . S.;~ i DPf r 41 q/lc_ 11 . U.S. DEPARTMENT OF TRANSPORTATION DESCRIPTION 12. 13. 14. 15. 16:TG>TAi(J>ACKAGE 17. 16. TOTAL W EIGHT 19. IDENTIFICATION

(Including UN 10 number, proper shipping name, hazard class, and any DOT LABEL TRANSPORT PHYSICAL AND CHEMICAL INDIVIDUAL RADIONUCLIDES - ' ACTIVITY LSAISCO AND OR VOLUME NUMBER OF

additional infonnatlon) "RADIOACTIVE" INDEX FORM MBq mCI CLASS (Use appropriate units} PACKAG!O

UN2916, Radioactive material, Type B(U) package, 7 YELLOW Ill 3.5 Sond/ H-3 C-14 3.58E-<06 (9.67E-<Q4) NIA 28622.2 Kg USA/9168/B(U)-96 RQ - Radlonuclldes Metal Oxides 63100.0 Lbs 8-1208-6 1 Metal Cask Mn-54 Fe-55

Oewatered Reactor Water Clean-up Resin Co-58 · Co-60

Nl-63 Zn-65

Sr-89 Sr-90

Nb-95 (Tc-99-LLD)

(1-129-LLD) Cs-137

FOR CONSIGNEE USE ONLY 20. "Certification is hereby made to the South Carolina Department of Health and Environmental COntrol ·that this shipment of k:l\-1-level radioactive waste has been inspected in accordance with the requirements of South Garcl!na Radioactive Material License 267-04 os amended, and the effective consor.dation facility acceptance criteria, '.vithin 48 hours prier to shipment. and further certification is made that tha Inspection revealed no ttems of non..compfiance with an applicable laws, rules and regu lations."'

Lf /~/IS I' / \(' Date Signature f ~ L__

I ' . \ , .. , I ,, c,-. 'RP ,-- ~ '-" ., .... Title and Organization . ,) -12fH'.!l · ·~ ; 1 <: l( v-t \i.!--1"\.f\p . .::::-, .._/_)

' . u Telephone No. ({I~(· ) 5'7-'2-Ci f ~~

FORM 540 (6-97) RfW8.2.1

FORM 541 (10-96)·

ENERGYSOLUTIONS BARNWELL PROCESSING FACILITY 1. MANIFEST TOTALS 2. MI>.NIFESI Nl.lf.liBER

NUMBER OF SPECIAL NUCLEAR MATERIAL (9<ams) s 1s~J77 UNIFORtM LOW-LEVEL RADIOACTIVE WASTE

MANIFEST

PACKAGES/ NS'WASTE DISPOSAL VOLUME U-233 U-CONTAINER~ -!---

235

I Pu

3.

rr.S 1.982 "" 1599.8 CONTAINER AND WASTE DESCRIPTION NP

I NP N P NP PAGE __ , _ _ PA'Gi: OF __ < __ PAG~.}

~.3 70.00 , 3527.0 4. SH!PPER NAME

Adivity(MB~tmCi)

C-14 I Tc-99 I 1-129 sour~.cE PPL Susquehanna, lLC

TRmUM Addt!fcoot Nuclesr Regulatort Commission {NRC) Requirements for Control. Transfer and

Disposal of Radioactive Waste MBQ 1 .37E+03 00) SHIPMB>!T 10 Nl1MSER

(5.98E-D1 )

3.6SE-t01 I (1AOE-01) (1.62E-D2_l N/A.

mCI I S.67E+e4 1 1 .38E+01 lb NP

DISPOSAL CONTAINER DESCRIPTICN WASTE DESCRIPTION FQR EACH WASTE TYPE m CONIAIW&. ·! IS.

5. ~ - 15.. RJI!)lQLOGiCAl DESCRfPTK)N WASTE o.

1

1

VOLUME

a. 12. 1 10. SURfACE ! P HYSICAL DESCRIPTION I 14. CHEMICAL DESCR1FTIOI~

CONTAINER CONTAINER IDENTIFICATION DESCRIPTION

NUMBER/ (See Note 1 & S.C. TRANS?ORT Note 1A)

CONT Alv11NA TION WASTE AND SURFACE I CONTAINER RADIATION M6Q/i00 cm2

WEIGHT LEVEL dprn/100 cm2

PERMn NUMBER

I m3

I ft3

l1 G-1C(ocOg;r>21Surv-~ I 3.407

ey}

I 120.30

kg mSvJt\r

ih :AL?t-iA 2ETA·GAtJJAJ:.. mremlhr

1995.8 Kg 823.000 < 3.33E-D7 < 1.67E-QS

4400.0 l bs 82300.0 <20 <1000

~----r-----,~-----t--------~-----r---------------------------------~·~J~~ON 11. 1L 1>.

WASTE APPROXIMATE SOLIDIFICATION DESCRIPTOR WASTE

OR I 'fOWME(S) IN STABILIZATION CONTAINER MEDIA

(See No132 & m3 (See Note 3 ~. Nate2A} M 1-lcte3A}

32G I 1.982 100 I fl

I i O.OO I I

CHEMICAL FOR.'"W j I 'NEIGHT% QiELATING

CHELA TING AGENT

I {F~~~~

Met:::! Oxides I NP

NP

ltiO.VIOU~L Rf.t•lONIX:t::DES AND ACTIVJTY AND C()(I.'TAJN2ll TOTAL; OR CONTA!.NER TOTAL l>CTI'IfTY i<!':D J<ADIO,,IUCLI!l:

PERCENT

·• ,t\S-~A

s:.v.x. Pl,J-J.;tanA ·t.tl'$t3:>'ie:

I ' B-el""' a RADIONUCC!~25 I l j·C-Cl=>C

Mao mCI iSl\~.i Gr::v;nsJ'Sr.Nr.J~ ~ Ki\og.-.w..!ij ~

5.0SE.C.2 H-3 -~ C-14 1..37£'63

Mn-54 j 4.10E<O:l

AS

Fe-5S ·, 1.T92t00 =-"'-:;-;;-" -+----+--+---'----!:----+----4----+--+---+-----~---~-eo.:=:--:=. ss=------·T -3 .. 7TE-04 J'

Co-<>l 1.6:2E+ll6

f\6-63 15EE+Q5 ~.1&E+03

L PQ-DQ6,., ·• ErergySolutions. LLC CNS PL&-120 DHEC-HIC-Pl-D01

1.3SE+01

3.~E+01

1. 11E-t-0'2

~.SSE+().<

t.<l2£.QS

4.S7~+04.

I Srlipmont Total .: 3.407-

120.30

NOTE 1: Cor.ti:iner ~oo Codes. For containersiWZ!:le requ!:ing <f~ in apj:I(O'I'Od .s.!n .• 'dr.:ra! c~erpads , lhe numerical code.must 'b! followed by ~-cp_•

1. Weeden Bole« C:ate 2.Wota!Bo." .3. Plastic Orur.'l or Fail 4. 'Matt~ ! Drum or Pa:t S.Metaf.'!'.anil:«llner 6. Ccr..crE.~ Tar~ C1' Une:r 7 . P~AeneTukO£Li::ter a. Rbe:ro;;:~ T.on.~t or Uncr

s. Oeminerallz.cu 10. Ge.z Cy!lnder 1·1. Bulk.. Un?ack.age:J Waste 12. UnP"tckag~ Components 1::. Hiljlh Integrity Col'llalner 1~. Other. Oescrioe In item 6. cr ae~i tion<:l P<~;.e

= .8

4400.0

NOTE 1A: Barnwell Spe.::inc Ccn:al:\cr Descrip~lon Coc!cs (Choose one·cod~ as rr.ay ·~ applicable.)

A High Integrity Container - Fc:y 8 High Integrity Con~lner • Foly with Sreer Shell C High Integrity Drum Overpack- Poly D High Integrity Con!.liner- St..nless Steel E H1gh lntegrtty Container • Flt;o.orgl<:ss i= Line: -Steel

Sr-6.1 3.22.E-QS S.S9E-11

N"D-9'.5 i.22E-1~ 3.29~-10

Zn-<:5 ,, 3.56800 9.61E•Q,I

Sr-90 , 6.S3Eo<J1 .

1

2.25!:<00

- -r----------------+------+Os""-·-1'-':rr"-'--·-- \ U6"•1)4 2.SSE>il2 +------' Tc·99 )I (5. 17E+00)1 (L4!le.Q~)

l l t~ate 2: W'.Z...Cfr. Ocs-oi\)!ot Coees. (Choose up to three wt.iCh preCtJIT~1'-.ate by IIO!:Jme.)

20. Ct\31C0.1C 21. lr.cine;;)"toc k.h 22. Soil 23.G~ 2~.0il 25.h;~s~ 26. Fi:t9( .Ycd'.a 27. Mech.t:ni~l=O.:er 28. EPA ·orS:a:eHz::atdoos

2S ~mclit~n Rulible 30. C:ttionJO:".-Exchanse Media 31. A.:·don r~n-Exohange M&C'ia 32. tl.bed Bee: lon-€xchm1~e Me-d\.a 3;:). Conl3.minated EQuipmer;: 34. Organic Ll.q!Jid (e~pc. ol!) 35. GlaSSVQt~ or LabY.-ar& 36. SealE-d Source/Device J7. Paint or P1ati.,;

38. Evzporetor Botto~'S.fudge:.;.'CC!tct!.:~1ltes

39. Co:nP']ctible Tr.!Sh 40. Ncncompactlble T~:-, 4 1 . Anima! carcass 42. Biolcglcal t-.13te-ria.t (eXo.."\:<pt anitr.;J\ catcass) 4~ . Activated Material 59 . Other. Describe in ite'n 1"1, Clfa1di'.l:l."t:Ll page

·, TOTta.LS: 3.5BE-+G6 9.Si'E-+04 1·129 I (!:.9BE-4l1) I (H:2E-C2!

3.58E~ '9.6/E. .... O<

_1 Note::.A 9a1'1'1'W1Sw...mc i't~w;;: 3. S:Ndif~~~c.Sta~:tt2no~)Jie.:f;o ~N~"'E3A:3a~~ WaSle C~:::'IC"'.or C.."des Cr.c.zs F!t' m~ tredn.g ~Gp.tr....aslt~ 1 S:.5cific {Choose all uD;:~frca~ codes

1~!re"lt:~Jvcl sta'!>lldy r~orrerrents, t!'le mJmtTlcal , SafdifJCOO.:!.:In

1 c::J~ ll"~t In foi!C"Wed by • -s- FOI &<1 S.iod S!abiJ~CI':

l :x:J~~>.:n :nedts, tM vendor am:i '=rfan.j f'ISI'l)!' y._oo13 Coa!!S G ~'3:ered 1-:r...t .. ;'( ulr.o b!!lk"~o!l'fej !n tte.~ 1::. OH- 100 .: {~ tru~ c-o1e i.f H Solid l ~'"'IS Re.:;j:Nad 1 apphcsb:e} I Ccm!::r.;t>llb;o ~i'TtcatkYI

l, J Non.-Comt~JStl'::lle 00 Ce-:oor.J 94 Vmyt Es~ Sty:"<!.-:'lt' K~FCitrztlOnF»'en j S'l ~C.:OWC::c 9S! Cttlor.Oe:.iCOIDeml::em lk:b95b:os $:1~~liol'l) 1 J ora:Vo;/"~·.~~ l ~Waxatnoe~

l ~"'2...e~ 100.~~?.e.,-u~j

L-------------------------------------.IL .. __________________________ ..J L-------------------------------------------------------------'' ~' ·l!~.V.,yf Cl>b<ide l FORM Y.ll (~fl..AA\

:·

Shipment 15-032

FORM54o (6-97)

ENERGYSOLUTIONS BARNWELL PROCESSING FACILITY

UNIFORM LOW-LEVEL RADIOACTIVE WASTE MANIFEST

SHIPPING PAPER

1. EMERGENCY TELEPHONE NUMBER (Include Area Code)

(570)542-3907

5. SHIPPER -NAME AND FACrcm· PPL Susquehanna, LLC Susquehanna SES (KJM) 769 Salem Btvd

Berwick, PA 18603

S.C. TRANSPORT PERMIT NUMBER: TSHIPMENT NUMBER

c; \ ~J- - ,· ~1 ~IS-r- 51!50106

SHIPPER 1.0 . NUMBER

1>Q32

X

COLLECTOR

PROCESSOR

GENERATOR TYPE (Specify)

NP

CONTACT TELEPHONE NUMBER (tndude Area Code)

7. FORM 540 AND 540A

FORM 541 AND 541A

FORM 542 AND 542A

PAGE 1 OF _ 1 __ PAGE\S) ,6. MAI41FcS:r NUMBER .I 1 PAGE(S) (Use tttis n~mber on a; co~:r.oation pa..,) I

=PAGE(S) i 5150106 . ADDITIONAL INFORMATION ___ PAGE(S)

9 .CONSIGNEE- Name and Faciiity Aridress

Sam-~.~ell Processing Facilit'l Ouratec Consolidation and Se."Vices Fad'fty

CONTACT RogerSetov:

T.ELEPriONE NUMBER (l:lclude kaa Codal ORGANIZATION Kimberly Murchison ~arnweu, :--• .,....,..-,"

1 ·~ ~- '"""''··@ . . I 10043 ~u~~~n: ~ulevard ,.:} {;.~ m nmFI.li'-6199

6. CARRIER- Name and Address EPA 10 NUMBER SIGNATURE - Authoc""d consigneo ockn~lng ~=o,...,.;pt r DATE

2 IS THIS AN "EXCLUSI\1!0 USE" SHIPMENT? 3.~?~~~~~~:_~~~IED Hittman Transport Services (C) WA

~YES 0N TIHIS MANI~ST 1

740 Osbom Road SHIPPING DATE 10. CERTIFICATiON ·,

I NO ---- Barnwell, sc 29612 0610212015 lhls is to certify that the h~rein ·- r.an1oed maleria!s are Pf~"tydass\'1ie;d. Ce.s:onbcc', pack-agad., ma~~. a:'lO

> TELEPHONE NUMBER laOO:ed and are in proper .corrd!t!on for tr.Jns;:or'~on accol\fi!'ig to &..e appliCC!bfe regulatklns of the Oa~tr~'it 4. DOES EPA REGULATED w YES EPA MANIFEST NUMSER CONTACT (lndu~e '-'"-" Coo•) ol Transportati<'.".This a!so certifies tr.al the·:na:erials are dassifli>d, pacJ<as<d, ma~ad. w ':abelod and are

WASTE REQUIRING A Roger aetow (B6S)48' -0222 "' proper cond1Uon for transportal1on aod d,._.l as d=r:l>ed m ar.o:mtanre with the ap~lcab!e MAo'\liFEST ACCOMPANY THIS X NO • requirements of 10 CFR Parts 20 and €1 , orequivulerrt st.ct.e C-">giJio:k.l".S.. ..

SHIPMENT? N!A . . SIGNATUv- Authort.edcarr-.eracknO\\i!Jdglngwasteroce!pt DATE AU.T .. HO. RIZEDStGNATURE 1T1Ze _- lOA.TE

If "Yes,· provide Mantf~ Number ==:=>

11. U.S. DEPARTMENT OF TRANSPORTATION DESCRIPTION

{lncluc!l"'Q UN 10 number. proper shipping name, haznrd class, and any addi"JonaJ infonnation}

UN2916, Radioactive material, Type B{U) package, 7 RQ- Radionucfides 1 Metal Cask

Dewatered RWCU Resin

FOR CONSIGNEE USE ONLY

FORM 540 (6-97)

12.

DOT LABEL "RADIOACTIVE"

YELLOW Ill

I ~.._,.;-- 7 . .. • I; /'.... /} ' () ( ' ' . f I "' ,- ( C ;( ~~A.z<;-.;._. (__,.,...,.-1 6 -.J- ·-·"'_"'__ _ r- r_y_,:r-.. . _ __ . _t_~}l,J·)O(_.r ~1. <71 ·~ 13. I 14. I 15. I 01~~TAL PACKAGE

TRANSPORT P~SICAL ANDCHE• TICAL INDIVIDUAL RADIONUCLIDES ~ ACTIVITY INDEX FORM MBq mCi

"i.7.

LS•tsco CtASS

1e. 10T.~L w .:JGHT I 19.10ENTiri':ATlCN A.'-10 OR \'OLL~IIC NUMBER OF

{Use ap;.r~prfate un:ts}.1

'?ACY..AG£

6.5 SoUdl Metal Oxides

(H-3-LLD)

Mn-54

Co-57

Co-60

Zn-65

Sr-90

(Tc-99-UD)

Ga-137

(C-1"-LLD)

Fe-55

Co-58

Ni-63

Sr-89

Nb-95

(1-129-LLD)

N/A (3.6SE+Ool Jm 37 2 «,g 1 USA.'91WE(Ul·95 .&3440 Cll.bs a-1 2:DS.1S

1.35E-t{)7

I

l I I I -t· I I i - .1

-'-----·

m 'I ·Certification is hereby made lo the South Carolina Department of Health and En1JW.:mmerrt2l Control that -:his ~.i::m!eR1: c1' .!Qw-leve! ' radioa.;-Jve waste has been inspected In accoroance wtj!t e requirements of SOlrlr. Carcfina 'RadiotlctiiJB Mawrtai .OO.il"'&., 2ST-04 .;;:s 2t'T1P.nc!>ad., .a~~e ' effective consofidatlon facility acceptance ~ria. wtthl 4& ours prior to shipment, and furthcrc.et.tiflca!!on is maC:s:tr-..crt ·:l"~ tns;w::tion rffi'~a!ad M~ c..of , non-cor.Jpliance with all app!icab!e laws, rules and. n..."gu ti6os." ~

Date h.jdJ_J5_ SignattJre --=.-c~:'--:,A/:-.i-/-\_,:_h.___=:.;·-,:--------. () 0 c 1-/ .. J.~.--- I <: -- "~ 't , - Lt L

rttl!l and OrganlzaUon 1> [ '") ~.·\ -......J. .. A f,i:'H J.Cr...;:tr, r ~·' . -<<i£Cl 9 1 ;;::;;- cf'iL,~ Telephone t'o.

RIW !12.1

FORM:i41 ENERGYSOLUTIONS BARNWELL PROCESSING FACILITY 1. MANIFEST TOTALS 2. MANIFEST NUMBER (10'96) NUMBER OF SPECIAL NUCLEAR MA: ERIAL (grams) S150106

UNIFORM LOW-LEVEL RADIOACTIVE WASTE PACKAGES/ NET WASTE NET WASTE DISPOSAL VOLUME WEIGHT U-233 lJ-235 Pu TOTAL

MANIFEST CONTAINERS 3.

""" 2.832 ., 1781.3 PAGE 1 PAGE OF __ 1 __ PAGE(S} CONTAINER AND WASTE DESCRIPTION 1 NP NP NP NP

I jtJ 100.00 lb 3927.0

4. SHIPPER NAME Activl1y(M8q/mCI)

P?l SuSQuehanna. LLC SOURCE ALL NUCLIDES TRITIUM C-14 Tc-99 1-129

ACditional Nuclear Regulatory Commission (NRC) Requirements for Contro~ Trnnsfer and

I SHIPMENT ID NUMBER

Disposal of RadioaclJv& Waste MBo 1.35E<-07 (4.20E+02) (1.73E+02) (1.44E.02) (4.95E+OO) kg NP 15-032

mCi 3.5SE.o5 (1.14E-<-01) (4.67E+OO) (3.88E+OO) (1.34E~1) lb NP

DISPOSAL CONTAINER DESCRIPTIOH WASTE DESCRIPTION FOR EACH WASTE TYl'E IN CONTAINER 16.

.5. 6. I 7. 8. 9. j 10. SURF'-CE PHYSICAL DESCRIPTION 14. CHEMICAL DESCRiPTION 15. RADIOLOGICAL DESCRIPTION WASTE ClASJF IGArtON

CONTAINER CONTAMINATIGN 11. 12. 13. I AS - CI&SSA CONTAINER

VOLUME WASTE AND SURFACE INDIVIDUAL RADIONUCLIDES AND ACTIVITY AND CONTAINER. S:able IDENT·IFICATION DESCRIPTION CONTAINER -"~~-,00~ WASTE APPROXIMATIE SOLIDIFICATION TOTAL; OR CONTAINER TOTAL ACTIVITY AND RADIONUCUDE AU...Cia$A NUMBER/ (See Note 1 & W EIGHT LEVEL dprrJ100 cm2 DE'SCRIPTOF VO~:E~~) IN STABI~~TION WEIGHT% PERCENT I.Jnstable CHEMICAL FORM I

S.C. TRANSPORT Note 1A) CHELATING AGENT CHELATtNG B-C:a~ss

PERMIT NUMBER CONTAINER MEDIA AGENT C-CicGS C m3 kg mSvlhr IF>0.1% RADlONUCUD:S

h3 - · - ALPHA BETA-GAMMA. (Seo Nets 2 & m3 (See Note 3 & (SNM GramsfSour::e MBQ mCi

lb mrem!h:-Not• 2A) ft3 Note 3A) IOiogamsJ

L15-01 13-A 3.407 2177.3 Kg 1soo.ooa < 3.32E..07 <1.67£-f)S 32 2.832 100 Metal Oxides NP Mn--54 3.30E+05 8.92E+03 AU

j Fe-55 4.76E+06 1.29E-<-05

120.30 4800.0 Lbs 150000.0 <20 < 1000 100.00 N P Co-57 1.63E-<-03 ~.40E+01

Co-58 7 .57E-<-02 2.05E.o1

?0620467-9

I Co-60 S.OSE-<-06 2.18E-<-05

EnergySolutlons, LLC M-63 2.35E-<-05 8.35E-<-03 CNS PLS-120

Zrl-65 1 1.27E-<-05 3.42£-<-03 DHEC-HIC-Pl~1 I

Sr-89 3.82E-01 1.03&0.2 ., Sr-90

I 3.58E-<-01 9.68E-01 I

l I Nb-95 1.07E~1 2.89E-03 l I Cs-t37 I 7.68E-<-03 2.08E+02

H-3 (4.20E.Q2) (1.14E-<-01)

l l':rt4 (1.73E+02) (~.67E->Q>J)

I 1'c-9S (1.44E+02) (3.88E•~O)

I 1-129 (4.95E-<-OO) (1.3-!E--01}

TOTALS: 1.35E+07 3.65E-<-05 S'n•pment Total : 3.407 2177.3

I l - 120.30 - 4800.0-- ~ .35E+07 3.65E+05

NO"TE ·t : Co-.~lner Description Codes. For containers/waste NOTE 1A Barnwell Specific Contel.ner Nctc 2: W~e Oe£.Cri~!or Co~es . {Choose up to three which preclom!l'l3tB hy volume.) Note 2A: Bamwel Spec.'fic t.tDTE 3: Soirdiflcation and Stebiliution Media NOTE 3A: Barr.~!

requiring d~;~os:a! in approved structur3! overpacks. the nt.:merieal Description Codes (CriOOSa oN! cca~: a!. may tl" Waste Descriptor Codes C-:xles. i="cr meCita meotln~ disposal s."te Specifec

code C'IU'it bra f':l~low&d by "-OP: ap;Jticat;!e.) {C:loose aU ~popllcab!e cedes. :.tn.u:~u~l c;ta~l!ity requirements, t.-.,c nu:nllf\~ Sclidi~tcation 20 . Ch~ :29. Oerro!rtion Rubt::le :..a. Evsporntor Souoms!Sruc;e-..o".:ooo:t...,rt~t~ cede m!J!;t boa 'followed by ·.s~. Fer. all 3nd Stabilizaticn

1. Wood~ Sox or Crate 9. Demi~era!izer" 21 . lncinera:=.t ~ 30. Cation lon-Excnange Med!a 33. Comoactible Trash sollGiflca:tlon media, the vendor and t:ra:-~d r.ame M!dic. Codes. 2. M~..a.l3ox 10. Gas Cylind~ A High Integrity Conllli:-.er ·Putt 22. Scil 3'l. Anion lo.,·Exdlange Media .::o. Noncompactlble Tr<J!ih G Dewalered r.uJStalso be identified in iter."113. Co::le 100 ~ (Choose ll'\ls code lf 3 ~ir.DrumorPail 11 . Sulk, Unpackag!Jd Waste 3 Hlgtllntegrity Conls~r ·Poly with Sk~ Sh~1 2:!. Ga~ 32. Mixed Bed lon·Exchange Media .,., . AnimcJI Ccucass HSc!id Ncnt Required. awlicat»e) 4. II.~ I Dru<t1 or Pall 12. Un;ackaged Components C High Integrity Dru:n Cv~--p3ek - Poly 2.::. on 33. Contaminated Equlp;T~ent 42. Biological Material (exoe;::t ;~ • .,rr.'l:!.{ I Ccmbub1\ble Solidi:'ication

5 . t\.'let2! Ta;Ut; or Liner 13. High Integrity Container 0 Hiijh Integrity Cantalne:-- St.! in less Ste!) 2'5. AQU!!O::IS llquYJ 34. Organic Liquid (except oil) cercass) J Non..Combustible 90.Cf:.merrt 94. Vtnyt Ester Sly."eoe 6. Co::7.cC Tank or Uncr 19. Other. Describe i:t item 6. E Hlgli Integrity Cc."lt.e!ntH - Fi~gla3s 26. Fi!t.e! Media 35. Glassw.:re ~ labware 4J. Activated Material K AI.:' F)ltratbn -Fitters 21 . C:mcrete 99. Other. Describe in Item

I 7. Po!}'~thyter~ Tank or liner or additional ~ge F Lme~- Steel 27. W.edta..~...31 Flits:' 36. Scaled Soo~vice 5S. Othef. Oes.crlbe io item "l 1, u a-~C~ion.a! L Asl>estcs . (~psoli!'tion) 13 or additiroal page MWaxBindu &. Fit!~gJ;;.ss iank or liner ~. EPAcr$t£tto> Hw::a:COL'S 37. Painto:' Plating page S2. 8itum-et'l 100. Nooa Requirea

I SS:. ' .l;ny1 Chloride - --

FORM 5<:1 [1().96) R!W6.2.1

Shipment 15-033

FCRM-540 ENERGYSOLUTIONS BARNWELL PROCESSING FACILITY 5. SHIPPER -NAME AND FACILITY SHIPPER LD. NUMBER 7. FORM 540 AND 540A PAGE 1 OF _ 1_PAGE(S) 8. MANIFEST NUMBER (6-97) PPL Susquehanna, LLC S150123 FORM 541 AND 541A _1_PAGE(S) (Use this number on all continuation pages}

UNIFORM LOW-LEVEL RADIOACTIVE Susquehanna SES (KJM) FORM 542 AND 542A __ PAGE(S) 769 Sak>m Blvd COLLECTOR 1,5..{)33

WASTE MANIFEST ADDITIONAL INFORMATION __ PAGE(S)

Berwick. PA 18603 PROCESSOR

SHIPPING PAPER S.C. TRANSPORT PERMIT NUMBER: I SHIPMENT NUMBER GENERA TOR TYPE 9.CONSIGNEE · Name and Facility Addness CONTACT (Specify)

1. EMERGENCY TELEPHONE NUMBER (Include Area Code) 010'd.-3'l-t5-~ 15-033 X NP Roger Betow

(570)542-3907 ~=~;~=:~o~~~~tyServlces Facllity /f!. CONTACT TELEPHONE NUMBER TELEPHONE NUMBER (Include Anaa Code) (Include Area Code) 16043 Dunbarton Boulevard

ORGANI2A TION Kimberty Murchison Banmven. SC 29812 (800j607-Q199 Shift Manager

(570)542-3169

6. CARRIER- Name and Address EPA 10 NUMBER SIGNATURE- Authorized ccnsignee acknowledging waste recei~ DATE 2. IS THIS AN "EXCLUSIVE USE" SHIPMENT? 3.TOTAL NUMBER OF Hittman Transport Serv ices (C) NIA

PACKAGES IDENTIFIED 740 Osborn Road ~YES ON THIS MANIFEST 1 SHIPPING DATE 10. CERTIFICATION

NO -=--> Barnwell, SC 29812 06/16/2015 "This is to certify that the herein- named materials are property classified, described, packaged, marked, and labeled and ar~ In proper condition for transportation according to the applicable regulations of the Department

4. ~~~~~~~~~~y~T;o 0 YES CONTACT TELEPHONE NUMBER

of Transportation. This also certifies that the materials are classified, packaged, marked, and labeled and are EPA MANIFEST NUMBER (Include Area Code) RogerBetow (865)481·0222

In proper condition for transportation and disposal as described in accordance with the applicable I

MANIFEST ACCOMPANY THIS X NO requirements of 10 fFR Parts 20 and 61, or equivalent state regulations.~ I

SHIPMENT? N/A SIGNATUR~~~gingwasterecelpt

DATE ~f•0 AUTHN·~URE nTLK f S k; O(Hr DAT•Ef J// if ~es," provide Manifest Number ====> c, /b 'IS . . /.,.-..... 0 /io 15

11. U.S. DEPARTMENT OF TRANSPORTATION DESCRIPTION 12. n 14. 15. 1~4J_ ?:S;KAGE 17. ! 11s. TOTAL WEIGHT 19. IDENTlFICATION

(Including UN ID number, proper shipping name, hazard class, and any DOT LABEL TRANSPORT PHYSICAL AND CHEMICAL INDIVIDUAL RADIONUCLIDES i ~ LSAISCO ANu OR VOLUME NUMBER OF PACKAGE additional Information) "RADIOACTIVE" INDEX FORM MBq mCi CLASS (Usa appropriate units)

UN2916. Radioactive material. Type B(U) package. 7 YELLOW Il l 6.0 Solid/ (H-3·LLD) (C-14-LLD) 1.04E+07 (2.81E+05) NIA 30137.2 Kg USA/9168/S{U)-96 RQ • Radionuclides Meta l Oxides 66440.0 Lbs 8·1206-1 1 Metal Cask Mr>-54 Fe-55

Oewatered Reactor Water Clean Up Resin Co-57 Co-58

Co-60 NJ-63

Zn-QS Sr-89

Sr-90 Nb·95

(Tc·9S.LLD) (1·129-LLD)

Cs-137

I

FOR CONSIGNEE USE ONLY 20. "Certification is hereby made to the South CaroUna Departmem of Health and Environmental Control that this shipment of k::wol-level radioactive waste has been inspected in accordance with the requirements of South Carolina Radioactive Material License 287-04 as amended, and the effective consolidation facility acceptance criteria, wtt.hin 48 hours prior to shipment, and further certification is made that the Inspection revealed no items of non--compfiance with all appllcable laws, rules an~ulations. •

Date '-'/lh I' 5 Signature H xL Title and Organization -{2._ f' :) ki~M\ ,~l ·'-c..JJ l~IIJ117fi.V, L~ Telephone No. rzro > sr;:t, -q Ff.d-; L)

FORM 541 ENERGYSOLUTIONS BARNWELL PROCESSING FACILITY 1. MANIFEST TOTAlS 2. MANIFEST NUMBER (1D-96)

NUMBER OF SPECIAL NUCLEAR MATERIAL (grams) 15-033

UNIFORM LOW-LEVEL RADIOACTIVE WASTE PACKAGES/ NET WASTE NET WASTE DISPOSAL VOLUME W EIGHT U-233 U-235 Pu TOTAl

MANIFEST CONTAINERS 3.

m3 2.832 kg 1781 .3 PAGE 1 PAGE OF __ 1 _ PAGE(S) CONTAINER AND WASTE DESCRIPTION 1 NP NP NP N P «3 100.00 lb 3927.0

4. SHIPPER NAME Actlvity{MBqlmCi)

PPL Susquehanna, LLC SOURCE ALL NUCLIDES TRITIUM C-14 Tc-99 1-129

Additional Nuclear Regulatory Commission (NRC) Requirements for Control, Transfer and SHIPMENT ID NUMBER Disposal of Radioactive Waste MBq 1.04E+07 (4.20E+02) (1.73E+02) (1.44E+02) (4.95E+OO) kg NP

S150123 mCi 2.81 E+05 (1.14E+01) (4.67E+OO) (3.88E+OO) (1 .34E-01) lb NP

DISPOSAl CONTAINER DESCRIPTION WASTE DESCRIPTION FOR EACH WASTE TYPE IN CONTAINER 16.

5. 6. 7. 8. 9. 10. SURFACE PHYSICAL DESCRIPTION 14. CHEMICAL DESCRIPTION 15. RADIOLOGICAL DESCRIPTION WASTE

CONTAMINATION CLAStFICATtON CONTAINER 11. 12. 13. AS-Cia--...sA

IDENTIFICATION CONTAINER

VOLUME WASTE AND SURFACE INDMDUAL RAIDIONUCUDES AND ACTMTY AND CONTAINER Stable DESCRIPTION CONTAINER RADIATION MSq/100cm2 WASTE APPROXIMATE SOLIDIFICATION TOTAL; OR CONTAINER TOTAL ACTIVlTY AND RADIONUCLIDE AlJ.CiassA NUMBER/

(See Note 1 & WEIGHT LEVEL dpm/100 cm2 DESCRIPTOF WASTE OR WEIGHT% PERCENT Unstable CHEMICAL FORM I S.C. TRANSPORT Note1A) VOLUME(S) IN STABILIZATION CHELATING AGENT

CHELATING B-Ciass B PERMIT NUMBER

I BETA-GAMMA

CONTAINER MEDIA AGEI\'T C.Cias::o C m3 kg mSv/hr IF>0.1% RAIDIONUCLIDES

ALPHA (See Note 2 & m3 (SeeNote3& [SNM Grams/Source MEQ mCI ft3 lb mrem/hr

Note 2A) ft3 Note3A) Kilograms!

L15-02/ 13-A 3.407 2177.3 Kg 1000.000 < 3.33E-07 < 1.67E-05 32 G 2.832 100 Metal Oxides NP Mn-54 2.64E+OS 7.13E+03 AU

Fe-55 3.67E+06 9.93E+04

Olio9:37- IS-K 120.30 4800.0 Lbs 100000.0 <20 < 1000 100.00 NP Co-57 1.3"iE+03 3.55E+01

Co-58 7.26E+02 1.96E+01

P064438D-8 Co-60 I 6.15E+06 1.66E+05 EnergySolutions, LLC Ni-63 1.78E+05 4.82E+03 CNS PLB-120

Zn-55 :.03E..-os 2.77E+03 DHEC-HIC-PL-00 1 Sr-89 4.03E-01 1.09E-02

Sr-90 2 .72E+-01 1 7.35E-01

Nb-95 1.30E-01 1 3.53E-03

Cs-137 S.83E+03 1.5BE+02

H-3 (~.20E+02\ 11 .1 4E+01l

C-14 ( t.73E+02) (4.67E+OO)

Tc-99 (1.«E+02 (3.88E+OO)

1-129 {4.95E+CO) (1.34E-01)

TOTALS: 1.04E+07 2.81 E+OS S hipment T ota : 3.407 2177:3"

I 120.30 4800.0 1.04E+07 2.51 E+05

NOTE 1: Container Description Codes. For cont.ainerslwasto NOTE 1A: Bamwel! Specific Container Note 2: Wilsie Descriptor Codes. {Choose u~ to three which predominate by volume.) Note 2A: Bamwel Specific NOTE 3: Sol!oificatb:~ and Stabilization Media NOTE 3A: Barnw&ll requiring d~posal in approved structural overpacks, the numerical Descrlpt!on Codes (Choose one code as may be Waste Descriptor Codes Coees. For media moati:-3 disposal sile Specific COde must be followed by•-op: applicable.) (Choose au applicable codes., structu:"l staCiiity requlre:ner.ts, the numerical Sotidiflcatlon

20. Charcoal 29 . D&molilion Rubble 38 . Evaporator Bonoms/Siudges/Concentratcs cooe must bo follo'i'l'i.:d by "-S". For an and S:abilization 1. Wooden Box or Crate 9. Oemlneral!zor 21 . Incinerator Ash 30. Calion lon4 Excl'lange Media 39 . Compactible Trash solidlfiei!tion r:ledz. the venCor and brand neme Med~ cooes I 2. Metal Box 10. Gas CyHnder A High Integrity Container 4 Poly 22. Soil 31 . Anion 1on4 Exchange Media 40. Noncompactible Trash G Dewatered must also bo U:lentlf:ed in Item 13. Code 100 = (Choose this co6e rf 3. Plastic Orum or Pall 11 . sur~t, Unpackaged Waste 6 High Integrity Container - Poly with Steel Shell 23. Gas 32. Mixed Sed len-Exchange Media 41 . Animal Carcass H Solid None ReQu!red. applicable) 4. Metal Drum or Pall 12. Unpackaged Components C High Integrity Drum Overpack. - Poly 24. Oil 33. Contaminaled EGuipment 42 . Biologica l Materl31 {except omimill 1 Combustible Solidification 5. Metal Tank or Uner 13. High Integrity Container 0 High Integrity Container- Stainless Steel 25. Aquec.us Liquid 34. Organic Uquid (except all) carcass) J Ncn-Cembustlble 90. Cer.1ent 94 . VInyl Ester S!yrtone 6. Concrete Tank or Uner 19. Otl'1er. Describe In Item 6. E High Integrity Container- Fiberglass 26. Fllter Media 35 . Glassware or Ulbware 43. Activated Material K f.Jr Filtration Filters 91 . Concre:e 39. Otrer. Oes;;ribe In Item

M Wax Binder I 7. Polyethylene Tank or Liner or additional page F liner • Steel 27. Mecnank:al FUter 35 . Sealed Sou:-:e/Oevl:::e 59. Other. DescribE' in item 11. or additional l A.sbestcs (EncapsulatioC"T) 13 or addition.<ll page 8. Fiberglass Tank or liner 28. EPA or Sta:c- Hazardous :i7. Paint Of Plating page 192. Bitumen ~CO . None ReQuired

93. Vinyl C~loriGe