Syllabus of B. E. – I

(Metallurgical and Materials Engineering)

(Effected from July 2015) Revised syllabus of Materials Science

F.S. B.E.-I (C, M, E, Ch., Met & Mats., IWM, Comp. Sci., Text. Engg.)

MET 1101 Theory : 100 Marks L – 3 hrs. Total: 100 Marks T - 1 hr

1. Introduction of Engineering Materials: Metalica Materials, Ceramic Material, Polymers, Composite and Nano-materials.

2. Crystal Structure: crystallography, Atomic structure and; Structure of crystalline solids; Lattices, unit cells; Crystal systems, Bravais lattices; Indexing of directions and planes, notations, Inter-planar spacings and angles, co-ordination number, packing factors stacking sequence in BCC, FCC and HCP.

3. Mechanical Properties of Materials: Concepts of stress and strain, Stress-Strain diagrams;

Properties obtained from the tensile test; Elastic deformation, Plastic deformation. Impact Testing & toughness behavior. Hardness of materials.

4. Phase diagram: Gibbs phase rule, Binary phase diagram its types, solid solution – Hume

Rothery Rules. Imperfections: Point defects, Line defects and surface defects – grain boundary, tilt boundary and twin boundary, Grain, Grain size number. Burgers vector and its representation.

5. Ceramic Materials Introduction, ceramic structures, silicate structures, Processing of

ceramics; Properties, glasses; Composite Materials- Introduction, classification, metal-matrix, ceramic–matrix and

polymer matrix composites. 6. Corrosion: Types of corrosion – Dry and Wet corrosion, Electro chemical and oxidation

(Chemical) corrosion. Corrosion prevention – anodic and cathodic protection & coatings 7. Electrical & Electronic Materials: Intrinsic and Extrinsic Semi conductivity, Dielectric

material, Piezo-electric materials. Magnetic Materials: Introduction, classification of magnetic materials, soft & hard magnetic

materials. 8. Advanced Materials : Nano Materials & its application, Metallic glasses, Super conducting

material, optic fibers, smart materials.

Text/Reference Books:

1. Askeland D.R.,& P. P. Fullay (2007), The Science and Engineering of Materials –4th Cengage Learning Publishers 45 2. William D. Callister, Jr (2008), Callister‟s Materials Science and Engineering, (Adopted by R. Balasubramaniam) Wiley-Eastern 3. A.S. Edelstein and R.C. Cammarata Ed.(1998), Nano Materials: Synthesis, Properties and Applications, Inst. Of Physics Publishing, UK 4. Raghavan V (2007), Materials Science and Engineering - A First Course, Prentice Hall, India 5. James F. Shackelford (1996), Introduction to Materials Science for Engineers, Prentice Hall, India

Revised syllabus of B.E.-I – 2015

Applied Physics I 1. Interference: Types of interference. Fresnel’s biprism. White light fringes. Determination

of thickness of thin sheet. Interference in thin films (conditions for normal incidence). Necessity of extended source. Newton’s rings, Michelson interferometer. Types of fringes. Uses of Michelson interferometer. Antireflection coating. Interference filters.

2. Diffraction: Fraunhoffer diffraction at a circular aperture. Plane diffraction grating.

Formation of multiple spectra and determination of wavelength. Dispersive power of grating. Resolving power of optical instruments. Meaning of resolving power. Rayleigh’s criterion of resolution. Resolving power of grating, prism, telescope and microscope.

3. Polarization: Geometry of calcite crystal. Double refraction, quarter wave plate. Half

wave plate. Elliptically and circularly polarized light and production of circularly polarized light. Optical activity. Specific rotation. Fresnel’s theory of optical rotation. Laurent’s half-shade polarimeter. Photoelasticity.

4. Lasers : Spontaneous & stimulated emission. Population inversion. Structure of a Laser.

Properties of Laser light (monochromatic, low divergence, coherence.). Types of Laser with specifications. Applications.

5. Ultrasonic : Ultrasonic waves. Production and detection. Properties of ultrasonics.

Applications of ultrasonics waves. 6. Electricity and magnetism : Magnetic forces on a current. Torque on a current loop. Hall

effect and Hall devices. Circulating charges. Cyclotron and mass spectrometer. Faraday’s law of induction. Lenz’s law. Induction - quantitative study. Time varying magnetic fields. Betatron. Paramagnetism. Diamagnetism. Ferromagnetism. Nuclear magnetism and NMR.

7. Thermoelectricity: Seebeck effect. Variation of thermo-emf with temperature.

Thermoelectric series. Measurement of thermo-emf. Law of intermediate metals. Law of intermediate temperatures. Pelteir effect. Thomson effect. Total emf in a thermocouple. Thermoelectric power. Applications of thermoelectric effect.

8. Modern physics: Artificial transmutation. Nuclear reactions and Q-value. Types of

nuclear reactions. Structure of nucleus. Nuclear constituents. Proton-neutron theory. General properties of nucleus. Atomic mass unit. Mass defect and packing fraction. Nuclear binding energy. Nuclear forces. Nuclear models.

9. Nuclear fission : Theory of nuclear fission. Energy released in nuclear fission. The chain

reaction. Thermonuclear reactions. Atom bomb. Stellar energy. Nuclear reactors. 10. X-rays: Discovery & production of X-rays. Origin and properties of X-rays. Diffraction

of X-rays. Bragg’s law. X-ray spectrometer and crystal structure. Powder method. Applications of X-rays.

PRACTICALS : Practicals based on the above syllabus. TEXTS\REFERENCES 1) Engineering Physics : R.K.Gaur and S.L.Gupta, Dhanpat Rai & Sons. 2) Physics Part II – D.Halliday and R.Resnick, Wiley Eastern.

3) Introduction to modern and classical optics-- J R Meyer arendt, Prentice Hall. 4) Modern college Physics – H.E.White,Affiliated East-West Press.

Applied Mathematics I 1. CALCULUS Reorientation, Functions of one varible, Applications of Derivatives – curvature.

Successive Differentiation, Partial Derivatives, Leibnitz rule for the nth order derivative of a function, Techniques of partial derivatives.

2. INFINITE SERIES : Sequences and their convergence, convergence and divergence of infinite series,

Geometric series, P-series, A necessary condition for convergence, Comparision test, Absolute convergence and conditional convergence of alternating series. Expansion of functions : Macluarins & Taylor’s expansion with reminder form. Indeterminate forms, L’Hopsital’s rule.

3. COMPLEX ALGEBRA : Complex numbers & their geometrical representation, Complex numbers in polar form,

Demoivre’s theorem and its applications. Exponential, Logarithmic, Trigonometric & Hyperbolic functions.

4. DIFFERENTIAL EQUATIONS :

Reorientation. Modelling of Engineering systems pertaining to first order differential equations, Exact differential equations, Integrating factors, Unified approach to first order ordinary differential equations, equations of first order and higher degree.

5. Linear differential equations of higher order with constant coefficients and with variable

Coefficients, models of higher order differential equations. 6. Method of variation of parameters and simultaneous linear differential equations.

Method of solution in series, Bessel and Legendre’s equations. Properties of Bessel functions, introduction to Legendre polynomials.

TEXT/REFERENCES 1. Advanced Engineering Mathematics by Erwin Kreyszig. (6th Edition) Johnwilley & Sons. 2. Text Book of Engineering Mathematics – Dhanpat Rai & Sons, Delhi by Srivastava – Dhavan 3. Differential Calculus by Shantinarayan S. Chand & Co. New Delhi. 4. Advanced Calcus by Willfred Kaplan – Addison Weseley Publ. Company, Inc. 5. Advanced Engineering Mathematics – C.R. wylie, Mc. Graw – Hill, Inc.

Engineering Drawing I 1. Plane Geometry, Types of Lines, Lettering, Commercial Construction, Tracing of Curves. 2. Projection of Points, Lines and Projection on Auxiliary Planes. 3. Orthographic Projection and Isometric Drawing of Machine parts and sections. 4. Threads, Bolts, Studs, Nuts, Setscrews, Split pins, Keys, Rivets, Shafts, Pulleys,

Foundation bolts, Standard sections. 5. Cotter joints, Knuckle joints, Riveted joints, Welded joints, Couplings. 6. Sketches of above parts. Material Science 1) Engineering requirements of materials. Criteria for selection of materials for engineering

applications on the basis of mechanical properties. 2) Metallic materials. Properties and applications. Imperfection in crystals. Elastic and

plastic deformation of metallic materials. 3) Cold working and annealing. Effect of grain size. Alloying elements and heat treatment

on properties of single phase and two phase materials. 4) Ceramic materials. Examples of ceramic materials-bricks. Concrete. Cement.

Refractories and glasses. Structures properties and applications of above materials. 5) Organic materials. Polymerization mechanisms. Hydrocarbon and polymers. Properties

and applications of plastic. Rubber. Resins and wood. 6) Composite materials. Brief description of metal matrix. Polymer matrix and ceramic

matrix composites. Elementary principles. Typical examples. 7) Electrical and magnetic materials. Electrical properties. Electrical conductivity.

Conductors. Insulators and semi-conductors. Magnetic behaviour. Soft and hard magnetic materials. Dielectric properties.

8) Stability of materials in service environment. Corrosion. Oxidation and thermal stability.

Protection against corrosion. 9) Examples of new developments. Superconducting materials. Metallic glasses. Electronic

materials. Elementary principles and examples. TEXT/REFERENCES Elements of Materials Science’ by Van Vlack

Fundamentals Of Civil Engineering (I) THEORY : A. ENGINEERING MATERIAL 1. (a) Introduction of Civil Engineering Materials used in Engineering works. Basic

properties. (b) Bricks. ISI classification. Qualities of good bricks. Tests for bricks. Fire bricks. (c) Stone common types of building stones. Qualities and use. Artificial stone. 2. (a) Lime classification and uses of lime. Properties of lime. (b) Cement. Characteristics and properties of ordinary Portland cement. Field tests on Portland cement. Types of cements and their uses.Storing of cement 3. (a) Mortar and concrete. Material used in mortar and concrete. Classification and uses. Properties of good mortar and concrete. (b) Timber . Merits and demerits of timber as construction materials. Qualities of good

timber. Objectives of timber seasoning. Preservation of timber construction. Various types of timber. Timber products and their uses.

4. (a) Steel. Different types of iron. Advantages for tor steel and mild steel. Various market

forms of steel. Uses of C.I. pipes (b) Plastics. Classification of plastics and their uses. (c) Glass. Classification, properties and uses of glass. B. BUILDING CONSTRUCTION: 5 (a) Bricks Masonry. Terms used in brick work. Bonds in brick work. English and Flemish

bond. Supervision of brick work. Thickness of brick work. (b) Opening in walls. Lintels and arches. 6 (a) Doors and windows. Locations. Size, type and purpose. (b) Building finishing items. Plastering , Pointing. (C) SURVEYING: 7. (a) Introduction, definition, classification, object. Uses and principles of Surveying, Basic

instruments for survey and their use in surveying. (b) Chain Surveying. Survey stations. Base line. Check line, Tie line Chaining and

offsetting. (c) Compass survey. Open and close traverse. Bearing. Types of bearing. Systems of

bearings. Direction of bearings. Local attraction and magnetic declination. Prismatic surveyor’s and trough compass. Temporary adjustments and uses of compass. Conversion of bearings. Calculations of angles and correction of bearings

8. Levelling. Definition and uses. Terms used in leveling. Instruments for leveling. Temporary adjustments of a Dumpy level. Principles of leveling. Collimation and Rise and fall methods. Examples on leveling and Fly levels

(II) TERM WORK : Termwork will consist of practicals, drawings and sketches based on the above topics of

the subjects. TEXT/REFERENCES : 1. Elementary Survey – B.C. Punmia Vol.I Publisher: Laxmi Publication, Dariya Gunj, New Delhi 2. Surveying and levelling – S.C. Rangwala, Publisher: Charotar Publishing House, Anand. 3. Surveying and leveling – Kanetkar and Kulkarni Vol. I Publisher: A.V.G. Prakashan,

Puna. 4. Textbook of Building Construction – S.P. Arora and S.P. Bindra Dhanbatrai and sons Publishers. 5. Engineering Materials – S.C. Rangwala, charotar Books Stall, Anand. 6. Building Materials – Janardan Jha. 7. Building Materials – Surendra Singh, Vikas Publishing Pvt. Ltd., New Delhi. 8. Building Construction – Sharma and Kaul. Publisher: S.Chand & Co. Pvt. Ltd. New

Delhi. 9. Building Construction – S.C.Rangwala, Charotar Books Stall, Anand.Materials of

construction –D.N.Ghose, Publisher: Tata Mc. Graw Hill Publishing Co. Ltd. New Delhi. 10. Introduction to Engineering Materials – Publisher: Agrawal, Tata Mc. Graw Hill

Publishing Co. Ltd. New Delhi. 11. Building Construction – Dr. B.C. Punima, Laxmi Publication, New Delhi.

WORKSHOP-I

Carpentry: Names, use and setting of hand tools, Construction of halved single mortise and tenon joints, dovetail joint, bridle joint, oblique mortise and tenon joints and refter joint. Smithy: Tools used for preparing simple jobs in hand forging. Term Work: Each candidate shall submit to the examiners, the term work as mentioned below which will be allotted marks upto a maximum of 50 with a certificate from the Dean, Faculty of Technology & Engineering that it was completed by him in a satisfactory manner within the walls of the college. Carpentry: At least 4 different joints. Smithy: At least 4 different jobs. When once a set of jobs has been submitted for the examination and marked. The marks will be carried over to a subsequent examination unless new jobs are presented. A candidate whose marks in term work are thus carried over shall be eligible for a class.

Applied Mechanics

THEORY: (A) STATICS : 1. Introduction to the subject of applied mechanics and its various branches. SI units.

Force and force systems : Coplanar, concurrent and non-concurrent force systems. Resultant and resolutions. Forces in space. Vectors. Operations on forces using vectors. Moment of force. Varignon’s theorem. Couple and its properties. Resultant of a coplanar force system.Concentrated and uniform loads. Resultant of a spatial force system. Wrench resultant.

2. Equilibrium : Equilibrium of a particle. External & internal forces. Equilibrium of a rigid body. Types of supports. Structural members and beams. Reactions of beams. Determinateness.

3. Properties of lines, areas and solids : Centre of gravity. Centroids of lines and of basic and composite areas. Built-up sections. Product of intertias. Mass moment of intertia.

4. Trusses, frames and mechanisms : Connected bodies. Two force and three force members. Trusses. Method of joints. Method of sections. Determinateness of truss. Rigid and non-rigid frames. Simple mechanisms. Space frames.

5. Friction : Types of friction. Characteristics of a dry friction. Equilibrium on rough inclined place. The wedge-The screw-The screw jack-Journal bearing, Axle friction. Thrust bearing-Disc friction-Clutches.

6. Transmission of power : Lifting Machine, Basic machines, The differential principle, Linear law, Belt drive, Velocity ratio. Compound belt drive-length of belt. Transmission of power. Gearings. Trains of wheels. Epicyclic gearing. Speed reduction gear. Differential gear.

(B) DYNAMICS : 1. Kinetics of particle : Review of kinematics of a particle. Force, mass and acceleration.

Rectilinear and curvilinear motion. D’Alembert’s principle, work, power and energy. Impulse and momentum.

2. Kinetics of rigid bodies : Equations of motion. Translation. Fixed axis rotation. Problems involving frictions.

(A) STRENGTH AND ELASTICITY MATERIALS : 1. Simple stresses and strains. Hook’s law. Elastic limit. Ultimate stress. Factor of safety. Lateral strain. Poisoon’s ratio. Stress concentration idea. Temperature stress. Simple shear, Elastic modulii relations. TERM WORK : Practical and drawings : Experiments and ten graphic statics problems based on the above syllabus. TEXT BOOKS/REFERENCES : 1. Applied Mechanics by S.B. Junnarkar and H.J. Shah, Charotar Pub.

2. Engineering Mechanics by Merium and Kraige, John Wiley & Sons. 3. Vector Mechanics by Beer and E.R. Johnstons, McGraw-Hill Book Co. 4. Engineering Mechanics by Huges and Martin, E.L.B.S. and Macmillan. 5. Engineering Mechanics by R.S. Kumar.

Applied Mathematics II PARTIAL DIFERENTIATION : Function of Two variables- Definition, limit, continuity and partial Derivatives, Chain rule. Euler’s Therem, Implicit functions. Differentials, Applications of Partial derivatives, (Tangent Plane and Normal line, Approximation, Maxima and Minima. Lagrange’s Multiplier’s method) Jacobians and transformations. VECTOR CALCULUS Reorientation, Scalar and vector field. Gradient of a scalar function. Directional Derivative, Devergence and curl of a vector field and their applications. ANALYTICAL GEOMETRY Reorientation, Curvilinear coordinates (polar, cylindrical and spherical) Cone, cylinder, conicoids, surfaces and solids of revolutions. Tangent planes and normal lines to above surfaces (by calculus method) Tracing of curves : cardiod, cycloid, leminiscate, spiral, four level rose. MATRICES : Rank of a matrix, solution of homogeneous and non-homogeneous systems of linear equations. Eigen values and Eigen vectors of a matrix. Cayley-Hamilton theorem. Special matrices Hermitian, skew hermitian, orthogonal and unitary matrices. LAPLACE TRANSFORMS : Laplace Transforms of elementary functions, Inverse Laplace Transforms, Linearity property, First and second shifting theorem. Laplace Transforms of derivatioves and integrals, Applications of Laplace Transform in solving ordinary differential equations. TEXT/REFERENCES 1. Advanced Engineering Mathematics by Erwin Kreyszig. (6th Edition) Johnwilley & Sons. 2. Text Book of Engineering Mathematics – Dhanpat Rai & Sons, Delhi by Srivastava –

Dhavan 3. Differential Calculus by Shantinarayan S. Chand & Co. New Delhi. 4. Advanced Calcus by Willfred Kaplan – Addison Weseley Publ. Company, Inc. 5. Advanced Engineering Mathematics – C.R. wylie, Mc. Graw – Hill, Inc.

(old syllabus)

Basic Metallurgy 1. Scope of Metallurgy Various fields of metallurgical engineering, metallurgical industries in India and their future. 2. Occurance of important areas, minerals: Sources of metals Basic outline of the principle of production of iron and steel, copper, aluminium, zinc, lead. 3. Metallurgical Fuels and furnaces, common refractories and their classification, Pyrometry-various methods used for measurement, recording and control of temperature. 4. Metlalurgical microscope, optical systems, resolution & magnification. Polishing & etching macro & micro examination. 5. Phase Rule Study of simple binary diagrams, different types, Iron-carbon phase diagram, Use of phase diagram as a basis for introduction to the heat treatment of metals & alloys. 6. Introduction to foundry metallurgy, moulding, melting and casting methods. 7. Methods of metal forming-Rolling, forging, extrusion, wire drawing, tube drawing and powder metallurgy. 8. Metal joining - welding, soldering, brazing. 9. Testing of metals and alloys, hardness, tensile strength, ductility measurements. Introduction to NDT technques. REFERENCES 1. Elements of Metallurgy by D. Swarup. 2. Principles of metallographic laboratory practice by G.L. Kehl. 3. Elements of physical metallurgy by A.G. Gu. 4. Introduction to Metallurgy by A.R. Bailey 5. Materials Science and Processes : S.K. Hajra Choudhury, Indian Book Distributing CO., Calcutta.

(Effected from July 2015)

SECOND SEMESTER OF B.E. I Basics of Metallurgy

Met : 1202 Theory : 100 Marks L : 3 Hrs. Total : 100 Marks T : 1 Hr 1. Scope of Metallurgy

Various fields of metallurgical engineering, metallurgical industries in India and their future.

2. Occurrence of important areas, minerals: Sources of metals Basic outline of the principle of production of iron and steel, copper, aluminium, zinc,

lead 3. Metallurgical Fuels and furnaces, common refractories and their classification, Pyrometry-various methods used for measurement, recording and control of temperature 4. Metallurgical microscope, optical systems, resolution & magnification. Polishing &

etching macro & micro examination 5. Phase Rule Study of simple binary diagrams, different types, Iron-carbon phase diagram, Use of

phase diagram as a basis for introduction to the heat treatment of metals & alloys 6. Introduction to foundry technology, moulding, melting and casting methods 7. Methods of metal forming-rolling, forging, extrusion, wire drawing, tube drawing and

powder metallurgy 8. Metal joining - welding, soldering, brazing TEXTS / REFERENCES: 1. Elements of Metallurgy by D. Swarup. 2. Principles of metallographic laboratory practice by G.L. Kehl. 3. Elements of physical metallurgy by A.G. Gu. 4. Introduction to Metallurgy by A.R. Bailey 5. Materials Science and Processes : S.K. Hajra Choudhury, Indian Book Distributing

CO., Calcutta. Revised syllabus of B.E.-I – 2015

Engineering Drawing II 1. Solid Geometry : Projection of simple solids such as prism, pyramid, cylinder and cones. 2. Section of solids by different plans and their conventions, partial and revolved sections. 3. Interpenetration of simple solids such as cylinder and cones, development of surface of simple solids. 4. Machine drawing and sketching, machine parts and engine components such as a cylinder plston, stuffing box, crosshead, connecting rod, crank, eccentric, valve pipe joints, ball and roller bearing etc.

English I. Oral Communication : (Listening/Speaking) a. Listening to Indian/Native pronunciation Common Errors in prenunciation b. Listening for gist and specific details c. Note Taking d. Presentation skills/Expressing views/Facing an interview e. Speaking Siskills : Fluency/Pronunciation/Expression f. Group Discussion II. Written Communication : (Reading/Writing) a. Reading Comprehension : Skipping/Scanning b. Understanding the logic of sentences : Use of reference devices c. Summerising different types of texts : Precis/Note Making d. Business Correspondence e. Writing Reports f. Writing Proposals III. Study Skills a. Dictionary Skills b. Information Transfer : From visual to verbal IV. Grammar and Vocabulary a. Contextualized Grammer b. Sentence Structure c. Error Analysis/Using appropriate vocabulary d. Word Formation Processes : Affixation/Conversion/Compounding/Derivation Prescribed Text : English for All : Nilanjana Gupta (Coordinating Editor) Macillan India Ltd. 1998. REFERENCE BOOKS 1. Trimble and Trimble : English for Science and Technology : Discourse Approach. 2. English for Engineers and Technelogists : A skills approach Humanities and Social Sciences Division, Anna University, Chennai. 3. English Grammar for Today : Leech, Deuchar and Hoogenarad Macmillan 1984. 4. Communication in English for Technical Students : Curriculum Development Centre Technical Teacher’s Training Institute, Calcutta. Orient Longman. 5. Longman Dictionary of Contemporary English, Longman, 1978.

Applied Chemistry 1. Chemical Kinetics, first, second and third order reactions. 2. Phase rule and its applications to binary and ternary systems. 3. Properties of molecules in relation to structure : Surface tension, viscosity, refractive index, optical rotation. 4. Crystal structure, applications of X-ray to crystal structure. 5. Chemistry of beryllium, radium, thorium, uranium and platinum metals, rare gases. 6. Water for industrial and boiler feed purpose, demineralization of water. 7. Fuels, proximate and ultimate analysis of fuels, rocket fuels. 8. A. Corrosion and passivity. B. Applications of the law of marks action to homogeneous equlibria. 9. Ostwald’s dilution Law. Advanced Principles of Metallurgy : (a) Solvent extraction (b) Microbial methods (c) Chelation and (d) Liquid ion exchangers. 10. Petrochemicals and their applications. Manufacturing of following petrochemicals: (a) Synthesis gas (b) Methanol (c) Olefines 11. Introductory polymer chemistry. Definition of monomers, polymers, Mn1 MW etc. Classification of polymers, Chemistry of important polymers. PRATICALS: Based on the above

Syllabus of B. E. – II

(Metallurgical and Materials Engineering)

METALLURGICAL THERMODYNAMICS 1. Definition, Applications, Advantages, Limitations Law of thermodynamics,

Basic terms used, kind of systems, The stgate of a system, Equation of state, Properties of a system.

2. Reversible and irreversible changes, Equilibrium, Isothermal and Adiabatic change, energy and first law, Energy : a state property, Energy change in terms of partial derivatives. The concept of thermodynamic equilibrium.

3. Heat capacity, Specific heat, Heat capacities at constant volume/pressure in terms of energy and relation between them. Dependence of heat capacity on heat capacity on temperature, Enthalpy and enthalpy change for a substance, Heat balance.

4. Heat of reaction, Exothermic and endothermic reaction, Calculation of heat of reaction, Enthalpy change in different types of reactions Hess’ Law, Kirchoff ’s law equation.

5. Second law of thermodynamics and the concept of entropy, Entropy change for reversible and irreversible process. Entropy changes with change of state and for a chemical reaction. Combine expressions of 1st and 2nd laws, Maxwell’s relations.

6. Free energy : Helmholtz’s, Free energy of reaction, free energy as a criterion of equilibrium. The partial derivatives. The third law of thermodynamics and Nernst heat theorem.

7. Fugacity, Activity, Standard states for activity, Equilibrium constant, Equations for predictions of feasibility of reactions and for calculation of the equilibrium condition, Le chatelier principle.

8. Gibb’s-Helmholtz equation, Van’t Hoff equation, The clausius-Clapeyron euation and its applications, solutions : Atom fraction, mole fraction, Partial molal quantity, General interrelations.

9. Ideal and non-ideal solutions, Raoult’s law and Henry’s law, positive and negative deviation, Sievert’s law, Chemical potential, criterion to assess the feasibility of reaction, Gibbs phase rule.

10. Free energy – composition and temperature-composition diagrams and their corlation, metastable phase. Ellingham diagrams: its important features for metal-oxide system- in tutorial numerical based on all above imp. Topics to be covered.

TEXTS/REFERENCES

1. Physical Chemistry of Metals- L.S. Darken and R.W. Gurry, McGraw Hill Pub.

2. Problems in Metallurgical Thermodynamics and Kubetics – G.S Upadhyay and R.K Dube, Pergamon Press, 1977.

3. Text book of Materials and Metallurgical Thermodynamics – A. Ghosh. 4. An Intro. Chemical Metallurgy – R.H. Parkar

Fuels and Energy Sources in Metallurgy

1. Various forms of energy including non-conventional source. Solar energy, Wind energy, Tidal energy & Bio-mass and their applications in different fields. 2. Definition of Fuel and its importance. Indian coals washing methods. 3. Coking coal, Testing of of coking properties, carbonisation of coal. 4. Coke ovens, Recovery of by-products, industrial carbonization. 1. Classification, Classification and composition of gases, Classification of coal, Manufacturing of producer gas, Water gas, Carburetted water gas and Blast furnace gas, Catalytic process & hydrogenation. 2. Natural gas, cracking and reforming of natural gas, use of natural gas in Metallurgy. Laser and its applications. 3. Plasma, plasma state and characteristics, method of production & its application. (Ferrous and Non-ferrous Metallurgy). Nuclear energy, Nuclear fussion, Fussion and other reactions. 4. Energy conservation and recovery, energy aspects of certain metallurgical units and processes. Combustion. REFERENCE\TEXT : 1. Introduction to fuesl by J.C. Macral 2. The efficient use of fuels by H.M.Su 3. Fuels by Brame & Kiing 4. Fuels by Sharma & Chandra mohan

MINERAL DRESSING

1. Introduction, Occurrence of metallic minerals in nature, Role of beneficiation in extractive metallurgy, Mineral dressing as physical separation. Important properties of minerals as criteria for separation. Terms used in mineral beneficiation. 2. Liberation and its significance, comminution, crushing, type of crushers. The laws of comminution. Grinding, dry and wet grinding. 3. Grinding media, theory of tumbling grinding mills, grinding circuits. 4. Sizing, screens, industrial screening, size analysis representation. Size distribution. 5. Motion of solid in fluid. Stokes and Newton’s law. , Free setting and hindered settling, equal settling particles, classifiers. Sizing and sorting classifiers. Hydrocyclone. 6. Gravity separation, concentration criteria. Tabling, wilflly table. Jigging, jigs, heavy media separation. Sedimentation. Dewatering techniques. Thickener. Filtration and drying. 7. Flotation. Physico chemical principles. Surface properties, contact angle. Adsorption. Flotation chemicals. Differential flotation. Machines. 8. Process variables in flotation. Roughing, concentration. Scavenging. Study of flow sheet for important minerals. 9. Magnetic and electrostatic separation. Application of computer in mineral dressing.

MATERIAL & STRUCTURES-I THEORY 1. Types of beams and loads-Diagram of bending moment and shearing force in cantilever and simply supported beams under static loads-analytically as well as graphically with varying and distributed loads, Effect of couples. 2. Theory of simple bending : Distribution of normal stress due to bending, moment of resistance, Beam of uniform strength, Flitched beam, Built up section under bending. Distribution of shear stress : Principle stresses in beam, Curvature, slope and deflection of cantilever and simply supported beams including overhang beams, Carriage springs. 3. Resolution of stresses : Ellipse and circle of stresses, Principal planes, Principal stresses and strains, Mohr’s stress and strain circle for various applications of compound stress, Resilience of sudden, impact and shock loading. 4. Eccentric loading : Tension or compression combined with bending, Middle third rule, Wind pressure on walls and chimney, Water pressure on dam. Simple strut theory – Euler’s and Rankine’s Formula. 5. Stresses in thin cylinders subjected to internal pressure, Cylindrical shell with hemispherical ends, Spherical shell, Riveted joints, Various types of failures, Design of riveted connections. 6. Torsion of circular shafts of uniform sections. Tensional resilience. Distribution of torsional stress – Angle of twist, Power transmissions from shafts. Combined Bending and Torsion including theories of failure. Helical spring under Axial force. 7. Elementary theory of Reinforced cement concrete : Theory of bending as applied to rectangular beams and assumptions made, Relation between amount of reinforcement and position of neutral axis, Economic percentage of steel, Moment of Resistance of beams, Over and under balanced sections, Designs of beams and slabs. TERM WORK This will be presented by the candidate in the form of a laboratory journal and file consisting of graphic statics problems. LABORATORY WORK A minimum of ten experiments on testing of materials under tension, compression, shear, torsion, impact and hardness. GRAPHIC STATICS A minimum of ten exercise based on above items of the syllabus including graphical solution of forces in truss members. TEXT BOOKS/REFERENCES 1. Mechanics of Structures Vol.1 by S.B. Junnarkar and H.J. Shah. 2. Introduction to Mechanics of Solids by I.P. Kapila and S.N. Agnihotri. 3. Elementary Strength of Materials by S. Timonshenko. 4. Strength of Materials by R.S. Khurmi, S. Chand & Co. Ltd. 5. Strength of Materials by Ramamrutham. 6. Strength of Materials by R. C. Patel , T.D. Bhagia & B.M. Patel.

ELECTRICAL ENGINEERING FUNDAMENTALS (A) ELECTRIC CIRCUITS 1. D.C. Circuits : Review of Ohm’s law. Kirchoff’s law. Series parallel connections. Solution of simple d.c. circuits. 2. A.C. Circuits : Sinusoidal e.m.f. and currents. R.M.S. and average value. Phaser representation. Voltage current relations in purely resistive, inductive and capacitive circuits and their combination. Power and power factor. Poly phase system : Voltage and current relation and power in balanced 3 phase system. (B) ELECTRICAL MACHINES 3. D.C. Generators : Principle of working. Types of generators. Their characteristics and applications. D.C. Motors : Principle of working. Types of generators. Their characteristics and applications. 4. Transformers : Review of Faraday’s law and Lenz’s law. Self and mutual induction. Principle of working of transformer. e.m.f. equation. Uses of transformer. Induction motor : Principles of working and applications. 5. Alternators : Principle of working and applications. Syn. Motor : Principle of working. Special features and its applications (C) FUNDAMENTALS OF ELECTRONICS 6. Qualitative Semiconductor Theory : Conductors. Semiconductors and Insulators. Intrinsic and extriosic semiconductors. Conduction in p-n, p-n-p and n-p-n junctions. Their characteristics. Zener diode. Photo-diode and display devices. TERM WORK : About 8 to 10 Experiments based on the above syllabus. TEXTS/REFERENCES 1. Applied Electricity by H. Cotton. 2. Electrical Technology by B.L. Theraia. 3. Advance Electrical Technology by H. Cotton. 4. Problems in Electrical Engg. by Parker Smith.

APPLIED MATHEMATICS-III Multiple integrals : Reorientation of concept of integrals. Line integrals double and triple integrals, evaluation techniques. Change of order of integration, integrals in polar and cylindrical coordinates, transformation of multiple integrals. Application of double and triple integrals for evaluation of area. Volume, mass. · Vector Calculus : Surface integrals, Green’s theorem, Gauss divergence theorem, Stoke’s theorem, Applications of integral theorems. · Improper integrals : Convergence of improper integrals, Error functions. · Fourier series : Fourier expansion of periodic functions with period 2 (Fourier series of even and odd functions, half-range series. Fourier series of functions with arbitrary period, conditions of convergence of Fourier series. · Tensors : Space of N-dimensions, Transformation of co-ordinates, summation convention. Contravariant and co-variant vectors (tensors of first order), tensors of second order (Kroneker delta), Tensors of higher rank, Invariant or scalar. Algebraic operations with tensors. Addition and substraction of tensors, contraction, product of tensors, Inner product, symmetric tensor, skew-symmetric tensor, quotient law. · Second order Partial differential equaitons: Second order partial differential equations, models leading to 2nd order PDE’s, boundary value problems involving 2nd order PDE’s and their solution by methods of separation of variables. Heat, Wave & Laplace Equns. & their solution by method of separation of variables and using Fourier series. · Introductory Statistics, regression and correlation : Reoreintation, measures of central tendency, measures of dispersion, correlation, rank correlation, regresion, curve fittings, method of least squares. · Sampling Techniques and Testing of Hypothesis : Population and samples, Different methods of sampling. Probability distribution and their properties, Binomial, possion, Normal distribution and their properties, estimation of parameters cofidence intervals, Testing of hypothesis, decisions. REFERENCES : 1. Advanced Engineering Mathematics – Erwin Kreyszig. John Willey & sons. 2. Introduction to partial differential equations – Donald Greenspan, McGraw-Hill Book Company. 3. Advanced Engineering Mathematics – C.R. Wylie, McGraw-Hill Book Company. 4. Properties of solids – George G. Koerber, Prentice-Hall. 5. Mechanical Metallurgy, S.I. Metric Edition – George E. Duter, McGraw-Hill Book Company, 1988.

PRINCIPLES OF EXTRACTIVE METALLURGY

Definitions: Ore, Minerals, Metals, etc. Scope of extractive metallurgy, Drying, Calcining, Sintering, Roasting, Smelting, Distillation, Fire refining. Hydrometallurgy, Steps involved, Importance. Merits of pyro and hydrometallurgy. Electrometallurgy, Electro winning. Electro refining. Applications. Fundamentals of unit Process, Unit operations. Review of chemical equilibrium. The basic concept of free energy change. Requirements for prediction and calculation of a chemical reaction. Ellingham diagram in detail for metal oxides. Activities in concentrated solution and in industrial liquid metallic solution 1wt/std. State. Henrian solution activity and activity coeff. (Problems based on few above selected topics are solved in tutorial classes.). Reaction kinetics. Factors affecting Homogeneous and heterogeneous reactions. Effect of conc. Of reacting substances on rate of a reaction. Order and molecularity of a reaction, reaction and concentration of reactant of 1st, 2nd, and nth order. Determination of order and velocity constant of a reaction. Reversible reactions. The effect of temperature on rates of reactions. Arrhenius equation, Role of activation energy. Theory of absolute reactions. Rates, Applicability of reaction kinetics to metallurgical systems. Extraction of metals from oxide and sulphide ores. Reduction of oxide ores by Carbon Hydrogen metallothermic reduction ( Al, Si, Mg, Ca. etc). Electrolysis at low pressure and high pressure. Conversion into halides and subsequent extraction. Reduction of sulphide ores by reduction, smelting and mattesmelting. (Discussion of all above topics with at least specific examples in each case.) Refining of impure metals. Introduction chemical, electrochemical and physical methods i.e. fire refining. Refining via volatile comp. Electrolysis, Distillation. Zone refining, Materials and heat balance. Flow diagram. Techniques and procedure of material balance. Techniques and methods of heat balance.

COMPUTATIONAL – TECHNIQUES (A) C Programming : · Algorithms, effective procedures in problem solving, flowcharts, pseudo-code. · C Preliminaries : Data types, constants, variables, type specification statements, operators and expressions, Library functions simple C programms. · Control Structures : Importance and types of structures, structured programming, if else, while, do-while, for, switch structure, go to, continue and break statement. · Arrays, pointers, functions, text processing and programms using the above features. (B) Numerical Analysis and Application Programming · Finite differences, Newton’s interpolation formula, Lagrange’s formula. · Numerical integration, Trapezoidal Rule, Simpson’s Rule. · Solution of equations of one variable : Bisection method, Regula-falsi, Newton – Raphson Method. · Solution of system on linear equations : Gauss Seidel, Jacobi, Gauss-elimination Methods. · Numerical solution of differential equation : Euler’s Method, Modified Euler Method, Runge-Kutta method. · Finite difference methods for ordinar differential equations. REFERENCES 1. Sudhir Kareker Programming in C. 2. Kernigham B.W. and Ritchie D.M. : The C programming Language, 2nd Edition. 3. Numerical Methods for Scientific & Engineering Computation by M.K. Jain, S.R.K. Iyengar, R.K. Jain – Willey Eastern Ltd. 4. Computer Oriented Numerical Methods – S.S. Sastry, Prantice-Hall of India. 5. Introduction to Numerical Analysis – S.S. Sastry, Prantice-Hall of India.

ANALYTICAL TECHNIQUES IN METALLURGY 1. Introduction to techniques in quantitative analysis Physicochemical method of analysis. Basic principle and methods of colorimetry. 2. Absorptiometry Spectrophotometery Electro-gravimetric analysis. 3. Titrometry, Potentiometric titration. Columbometric titration. Ampstiomatric and conductiometric, Titration. 3. Nuclear Magnetic Resource principle, analytical applications. 4. Thermal Analysis, thermogravimetry Differential thermal analysis. 5. Differential scanning calorimetry. Thermodilatometry. 6. Analysis of cast iron. Steel, Stainless steel, Brass Bronze etc. by chemical and physico chemical methods. TERM WORK Experiments of Wet. Analysis and Instrumental Analysis based on chemical and physico chemical methods. TEXT/REFERENCES 1. A Text Book of Metallurgical Analysis, B.C. Agrawal, S.P. Jain, Khanna. 1. Instrumental Methods of Analysis – G.W. Ewing, Mc-Hill. 2. A Text of Qualitative/Anatilative Analysis – A.1 Yogel Lonsgman. 3. Metallurgical Analysis – V.G. Iyer, Kohinoor. 4. An Introduction to Metallurgical Analysis – S.K. Jain Vikas. 5. Introduction to Thermal Analysis – M.E. Brown. 6. Undergraduate Instrumental Analysis – James W. Robinson.

TRANSPORT PHENOMENA 1. Modes of heat transfer. Conduction of heat through solid. Steady and unsteady state. Temperature profile. Fouriou law of heat conduction. General equation of heat conduction in Cartaian co-ordinate. Spherical co-ordinate & Cylindrical. One diamensional steady state heat flow through composite walls. 2. Radial heat conduction through bollow composite cylinders and spheres. Convective heat transfer. Free and forceed convection. Application of dimensional analysis to Effective boundry layer. Convective mass transfer coefficient. 3. Laws of diffusion. Diffusivity. Steady state one dimensional mass diffusion through stationary media. Counter current diffusion. Unidirectional diffusion. Solid state diffusion. 4. Radiative heat transfer. Reflection adsorbtion and transmission of radiation. Definition of Nack body Plank’s Law. Wien’s distribution law. 5. Heat transfer between two bodies by radiation Labert’s law. View factor. 6. General features of fluid flow. Viscosity. Classification of fluids. Newtonian. Non-Newtonion. Viscous-non viscous. Lamilar curbulant. Compressible incompressible. Steady unsteady fluid flow. Macroscopic energy balance. Verturimeter. Oritices, capilary flow meter. Pilot tube. Nozzle Buckimglram theoram. 7. Rotameter. Friction factor. Dimensionalanalysis supplied to fluid flow. Flow through pipes bends. Flow around spherical particle-bed of solids. Equation of continuity Naijer stokes equation. Bed and particle fluidzation. TEXT/REFERENCES 1. Elements of Heat and Mass Transfer – Prof. R.C. Parel, Acharya Book. 2. Fundamentals of Momentum. Heat and Mass Transfer : J.R. Welty, C.E. Wicks and R.E. Wilson Wiley. 3. Principles of Extractive Metallurgy – A. Ghosh and H.S. Ray. 4. Chemical Engineering – J.M. Coulson and J.F. Richardson. Mc.Hill ELDS. 5. Engineering in Process Metallurgy – RLL Guthrie Oxford. 6. Rate Phenomena in Process Metallurgy – J.Z. Szekely and N.J. Themelis, Wiley Inter-Science.

MACHINE DESIGN & DRAWING

1. Designing : Design procedure. Need for designing synthesis. Material selection. Engineering materials. Important mechanical – properties of materials. Streee concentration. Factor of safety. Types of loads and Stresses. Basic design calculations. Contact stresses. Fatigue loading & calculation based on various criteria. Theory of failure. 2. Operational & Permanent joints : Design of operational joints like – cotter, knuckle, Turn back etc. Design of riverted and welded joint for Structure and pressure vessel. 3. Machine parts subjected to ecoestiric load & columns : Ecoectric loading on rivets of bolts. Columns & starts. Buckling – load End fixing conditions. Column subjected to ecoentric load. 4. Shafts, Keys and Couplings : Shaft : Design consideration. Materials for shafts, Loading, various factors affecting design of shafts. Keys : Types of keys and design criteria. Couplings : Design of various types of couplings like Muff coupling. Flange coupling. Flexible coupling. Elastomer type coupling. Metallic Grid (Steel Flex) coupling. Oldflam coupling etc. 5. Springs : Materials & manufacturing, Pre-stressing. Design of helical compression & Tensile springs, composite spring, contial spring. Torsion spring. Flat spiral spring & Leaf spring. 6. Levers : Design procedure. Design various levers like – Bellcrank, rocker arm etc. Design of various types of Handless & Foot levers. 7. Computer aided drafting & design : Importance of CAD. Design process. The application of computers for design. Product cycle of CAD. Introduction of software and Hardware. Term work is based on theory. At least 4 half imperial sheet with design 10 reports. REFERENCES 1. Machine Design Vol.1 – Patel, Sikh, Rajput & Pandya, C. Jamnadas & Co. 2. Mahcine Design Vol.2 – Patel, Sikh, Rajput & Pandya, C. Jamnadas & Co. 3. Elements of Machine Desing – Spott., Prentice Hall.

PLASTIC DEFORMATION OF METALS

Crystal imperfections. Point defects, Line defects and surface defects. Slip phenomena. Slip systems. Theoretical strength of a perfect crystal. Slip by dislocation movement concept of critical resolved shear stress. Burgers vector and the dislocation loop. Dislocation in F.C.C (including formation of stacking fault.) B.C.C and H.C.P., Stress fields and energies of dislocations. Jogs. Dislocation: Forces. Multimplication of dislocations. Techniques of observation of dislocation. Dislocation point defects interactions. Dislocation pile up. Twinning as a mode of deformation. Deformation of single and polycrystalline materials. Strain hardening of single crystals. Grain boundaries. Strengthening from grain boundaries. Hall-patch equation. Low-angle boundaries. Surface tension of the grain boundary. Strain-hardening of polycrystalline metals. Relation between single and polycrystalline stress-strain curve. Yield point phenomenon. Strain-ageing behaviour. Solid-solution hardening. Strengthening due to second phase particles. Annealing of cold-worked metals, Recovery, Recrystallisation and grain growth. Tensile test, Hardness tests and impact tests. Types of fracture in metals. Theoretical cohesive strength of metals. Griffith theory of brittle fracture. Theory of ductile-brittle transition temperature. Elementary concept of fracture mechanics. Fatigue test. Theory of fatigue. Effect of metallurgical variables and temperature. Creep test, Creep curve. Stress-rupture test. Creep mechanisms. High temperature alloys. Effect of some metallurgical variables. Presentation of engineering creep data. TEXT/REFERENCE: 1. Mechanical Metallurgy – G.E. Dieter, M.C. Graw-Hill. 2. Physical Metallurgy Principles –R.E. Reed-Hill, DlVan-Nostrand Company. 3. Deformation and Fracture Mechanics of Engineering Materials – Richard W. Hortzberg, John Wiley & Sons. 4. Structure and Properties of Materials, Vol. III, Mechanical Behaviour, John Wulff, H.W. Hayde, W.I. Moffatt, Wiley Eastern Private Ltd.

Syllabus of B. E. – III

(Metallurgical and Materials Engineering)

NON FERROUS EXTRACTIVE METALLURGY

1. Indian scenario of ores and mineral deposits and production facility for non-ferrous metals such as Cu,Zn,Pb,Al,Sn,Ni,Mg,Ti. 2. Copper:Ores & Minerals, Pyrometallurgical extraction,concentration, roasting and smelting,converting refining, Hydrometallurgy of Copper. 3. Comparitive study of electrowining and electrorefining of copper & behaviour of impurities.Parallel and Series systems. 4. Nickel: Ores & Minerals.Pyrometallurgical extraction,Refining. 5. Aluminium: Ores and minerals. Pyro and hydro Metallurgical processes of extraction. Preparation of alumina from bauxite.Preparation of electrode.Manufacture of carbon electrode,Hall & Heroult's process,Anode effect,Aluminium refining by Hoop's process. 6. Magnesium:Ores and minerals,method s of production of MgO and MgCl2,Pyrometallurgical extraction of magnesium.Electrolytic extraction,Refining of electrolyte. 7. Zinc: ores & minerals,Pyrometallurgical extraction of zinc,methods of distillation,Hydrometallurgical extraction of zinc. 8. Lead: Ores & Minerals,Pyrometallurgical extraction of lead ,Pyrometallurgical refining of lead bullion, Continuous lead refining,Seperation and extraction of Ti-metal. 9. Tin:Ores & Minerals and extraction of tin from its ores,Properties uses of important non-ferrous metals Recovery of precious metals from secondary resources such as anode mud,zinc dross,red mud and zinc electrolyte. Term Work:Tutorials / Assignments based on above syllabus. Text / Refrences. 1.Extractive Metallurgy:J.Newton.Willey 2.Metallurgy of Non Ferrous metals -W.H.Dennis,Ditman. 3.Extraction of Non Ferrous metals -H.S.Ray, R.Shridhar and K.P.Abraham 4.General Metallurgy-B.Kuznetov,Peace pubs.Moscow 5.Hydrometallurgy-S.Venkatachalam,Norsa Pub,Bombay.

IRON MAKING

1. Iron Making historical,Iron & steel industries in India,Occurence and distribution of raw

materials,Valuation of Iron ores.Metallurgical coal resources in India,flux and its evaluation.

2. Burden preparation,Burden calaculation,Burden Qualities,Methods of bebficiation,agglomeration,sintering process, variables and machines. 3. Types of sinter,Pelletization process,Theory of bonding,Mechanism of ball formation,disc and drum pelletizer,Induration of pellets,cold bonding technique,testing of agglomerates. 4. Physiochemical principles of blast furmace,Blast furnace reactions,Thermodynamics of Iron oxide reduction 5. Reaction in stack,Direct & Indirect reductio. Slag-metal reactions,Desiliconisation,Desulpaharization. 6. Constructional features of blast furnace, profile, refractories, accessories,charging mechanism,Bell and Belless charging systems. 7. Development in blast furnace process,Fuel Injection, oxygen injection, high-top pressure,high temperature blast, their effect in coke-ratioandmetal-impurity distribution in slag and metal. 8. Alternative methods of iron making,Reduction smelting,Direct reduction processes and Fludised bed process, mini- blast furnace,electrothermal process. 9. Blast furnace opertion,operational troubles and minimization,blast furnace control,Blast furnace gas,gas cleaning and utilization. Term Work: Experiments and Problems based on above syllabus. Text / Refrences. 1. Introduction to Modern Iron making -R.H.Tupkary,Khanna Pub.,Delhi. 2. Introduction to Physical chemistry of iron and steel making -R.G.Ward,ELBS. 3.The making,shaping and treating of Steel.-H.M.Gannon,U.S.S.Pub.Pittsburgh. 4.Principles of blast furnace Iron Making- A.K.Biswas,SBA Pub,Calcutta 5.Blast Furnace Iron making-J.J.Gupta and Amit Chaterjee,SBA Pub.,Calcutta.

MECHANICAL METALLURGY

1. Princples of metal working. Flow curve. True strain, True stress. Yielding criteria for Ductile metals. Octahedral shear stress and shear strain. Invariants of stress and strain. 2. Theories of plasticity, Flow and Deformation theories, Two dimensional plastic flow. 3. Classification of forming processes, Mechanics of metal working. Flow stress deformation 4. Effect of temperature, Strain rate and metallurgical structureon forming process. Friction and lubrication, Workability, Residual stress, Cold work anneal cycle. 5. Forging : Classification of forging. Drop and press forging. Forging equipment. Calculation of forging pressure and loads. Metallurgical variables associated with forging. Forging Defects. 6. Rolling of metals : Theory and practice. Different types of machines and accessories. Elementary roll pass design. Rolling of blooms, slabs. Merchant mill. Rolling of rails and structures. Flat products and wheel. Lay out of different mills for rolling of above products. Theories of cold and hot rolling. Defects in rolled products. 7. Direct and Indirect extrusion. Variables in extrusion. Flow patterns in direct and indirect extrusion through unsymmetrical multiple dies. 8. Impact extrusion. Hydrostatic extrusion. Tube forming. Production of seamless tubes by rolling and extrusion. Tube drawing. Wire drawing. Dry and Wet wire drawing. Wire drawing equipment. 9. Theory and practice of wire drawing. Variables in wire drawing. Other conventional methods of working such as deep drawing. Strech forming. 10. Spinning, Piercing, Swagging, Embossing, Coining, Shearing, Bending, High rate forming methods. Superplasticity, Defects oin wrought products. Causes and remedy. TEXT / REFERENCE 1. Mechanical Metallurgy - G.E.Dieter. 2. Introduction to Principles of Metal Working - G.W. Rowe, Edward 3. Mechanical Treatment of Metals - R.N. Parkins. 4. Making, Shaping and Treatment of Steels - H.M. Gannon, USS. Pittsburgh. 5. Engineering Metallurgy II - R.A. Higgins.

INDUSTRIAL CERAMIC MATERIALS 1) Fundamental ascepts of ceramics. Their difference from metallic and organic materials. Traditional and modern ceramics, classification od modern ceramics as oxide and non-oxide ceramics as well as classification based on their application. 2) Ceramic raw materials, Methods of Ceramic Powder processing, Pressing, Casting and plastic forming processes and brief review of other forming processes. Sintering / Firing of ceramics. Other modified classification processes. 3) Structural Ceramics : Properties and uses of Oxides and non-Oxide structural ceramics such as alumina, aluminium nitride,boron nitride, tungsten carbide,titanium carbide,silicon carbide,Sialon. 4) Electronic Ceramics : Properties and applications as Piezoelectric materials,ferrites,electroptical materials as pressure,gas and moisture detectors,etc. Ceramic dielectrics. 5) Ceramic cutting tools : Properties and applications of ceramic cutting tools such as alumina tools, boron nitride tools, Si3N4, Sialon etc. 6) Glasses and optical Fibres : Basic and application of various types of glasses namely Silica glass, Vycor glass,Opal-Glass. Application of glass fibres in composite materials and telecommunications, some aspects of crystallized glasses. 7) Ceramic Coatings : Techniques,parameters and applications of plasma / spray coatings for coating materials like WC, Cr3C, Al2O3, Stabilized Zirconia, etc. Similar studies on flame spray coatings. 8) Refractories : Classifications, properties such as PCE, RUL, Spalling, thermal properties, Chemical properties,Testing of refractories, Phase diagrams of Al2O3 -SiO2, etc 9) Applications of refractories in Iron making and Steel making, foundries,Special refractories. Text / Refrence : 1) Modern Ceramic Engineering :- David W Richerson Marcel Dekker,Inc., New Yoek [1982] 2) Introduction to fine Ceramics :- Applications in Engineering. Noborn Ichinose by John Wiley & sons Ltd, Newyork [1987] 3) Advanced Ceramics :- P.Ramkrishnan, Oxoford & IBH Publ.Co. P. Ltd., New Delhi.

FURNACE TECHNOLOGY 1) Classification and uses of furnaces in metallurgy based on technology,structure and heat generation. 2) Fundamentals of heat engineering of furnaces. Heat transfer laws, Review of steady state,conduction. 3) Transeint conduction, cartesian,cylindrical and spherical co-ordinates,solution for simple geometry and boundry conditions. 4) Convective heat transfer and radiative heat transfer. 5) Flow of gases in furnaces,ducts,drafts,chimney. Sample calculations, waste heat recovery, regenerators and recuperators,principle and design,Blast furnace stove. 6) Elements of furnace design,Refractories,materials for constructions, Fuel burning devices for solid/liquid/gaseous fuel,design of roof and hearth. 7) Principle of electric heating,Resistance heating elements, principles of induction heating,core and coreless furnaces, various types,comparison,Typical calculations. 8) Study of few important metallurgical furnaces,Special furnaces,Plasma heating,Optical furnaces, Uses of laser. 9) Temperature Measurement and control,calculations on heat transfer and fluid flow. Simple furnace design. TERM WORK : It includes drawing of burners and furnaces,calculations on heat transfer and fluid flow,simple furnace design. TEXT/REFERENCE : 1) Combustion Engineering, A.K.Shaha,Oxford and IBH Publ. Co. Calcutta,1974 and Fuel Technology 2) Metallurgical Furnaces, V.KKrivanchiv and B.Markov,MIR Publ. Moscow,1977. 3) Metallurgical Engineering, Schuman Principles Vol 1 4) The General Theory of M.A.Glinkov and G.M. Glinkov, MIR Publ.Moscow,1978 Furnace

ENGINEERING ECONOMICS

L - 4 Hrs. Theory : 100 Marks 1. Demand Analysis: Demand function – Demand Curve – Relationship between Demand Function

and Demand Curve, Measures of responsiveness, Determination and Uses of Elasticity of Demand.

2. Cost and Output : Short Run Average Cost Curve – Divisibility and Adaptability – Break – Even Analysis – Elements of Manufacturing Costs.

3. Market Structure and The Theory of Prices 4. Pricing Practices : Cost – Plus Pricing – Marginal / Incremental Analysis in Pricing – Multiple

Product Pricing. 5. Depreciation: Factors Governing Depreciation – Methods of Depreciation, Tax Considerations. 6. Theory of Capital : Meaning of Capital and Investment – Productivity of Capital Goods, Supply

of Capital Resources – Time Preference – Demand for Capital Resources, Roundabout Production Process – Measurement of Capital.

7. Cost of Capital : 8. Interest and Annuity Relationship with their Applications, Simple Interest, Compound Interest,

Present Worth, Annuities, Equivalence, Comparision of Alternatives. 9. Economic Analysis of Projects in the Public Sector and Benefit Cost Analysis. TEXTS / REFERENCE 1. Principles of Engineering Economic Analysis – John A. White, Marvin H. Agee and Kenneth E

Case Chapter 3 to 7 2. Managerial Economics – Eugene F Bringham and James L Papas, The Dryden Press, Hinsdale,

LLLinois, Chapter 4,8,10,11,13 and Appropriate Sections. 3. Cost Engineering Analysis – William R. Park, John Wiley and Sons, Chapter 2 to 8,10,11. 4. Managerial and Engineering Economy George A. Taylor, East West Indian Edition, Chapters 2

to 9,12,18 5. Economic Theory and Operations Analysis – W J Baumol, Prentice Hall of India, Chapters 18,19 6. Economics – Paul A Samuelson 7. Introduction to managerial Economics – Chirstopher I Savage and John R Small, Chapters

4,6,8,9 8. Elements of Cost Benefit Analysis – E J Mishan

FOUNDARY TECHNOLOGY

1. Introduction : Importance of Foundary Industry in Modern Industrial scenario,Advantages and limitations of casting method.Classification of Foundaries, Different sections in Foundary and their functions. 2. Patterns : Types, Brief discussion on pattern making materials,consideration in selection of pattern materials, colour code,Pattern allowances, core-boxes,types of core boxes. 3. Moulding and core making materials, Ingrediants of common type of moulding and core making sands, their properties and behaviour.Testing of sands & clay. 4. Classification of Moulding processes and casting processes,Brief description of all processes such as green sand,dry sand, loam, floor,pit and Machine moulding. 5. Shell Moulding,CO2 Silicate process,Investment Casting process,Permanent moulding process Gravity and Pressure die casting,centrifugal casting process. 6.Melting of cast iron, Mechanical features of cupola, operational steps and principles of cupola operation,Advanced practicles in the cupola operation.Melting of aluminium and copper based alloys including mould treatments such as dressing , grain refining and modification. 7. Elements of gating system : Classification, Basic considerations in gatting design,Gating ratio, Gating practise for ferrous and non-ferrous alloys,Pouring equipments. 8. Risering practise, Functions of riser, Directional and progressive solidification,Centreline feeding resistance , Riser efficiency,Riser design considerations,Risering curves, Cain's,N.R.L. and Modulus method, Feeding distance, Feeding aids, blind and atmosphereic risers, Defects in castings, causes and remedies. Term Work : Experiments and Tutorials based on above syllabus. Text/Reference : 1. Principles of Metal Casting - Heine and Rosentall 2. Foundry Technology - Beelay 3. Foundry Technology - M.Lal 4. Foundry Technology - P.L.Jain 5. Foundry Technology - Goel and Sinha

PHYSICAL METALLURGY I Met : 3208 Theory : 100 Marks L : 4 Hrs. TW/Viva : 100 Marks Pr. : 6 Hrs. Total : 200 Marks 1. Study of various types of Phase Diagrams, Binaru and Ternary. 2. Solidification jof Metals and Alloys,Nucleation and growth phenomena. Constitutional supercooling,Eutectic solidification. Rules of formation of various types of solid solutions. Intermediate phases, Intermetallic compounds. 3. Iron-carbon system, Fe-Fe3C diagram. Effect of alloying elements. Isothermal and continuous cooling transformation diagrams, Hardenability. 4. Fundamentals of heat treatments of Steels. Annealing, Homogenisation. Spheroidising, Normalising, Quenching media, Austempering, Martempering, Hardening and Tempering. 5. Surface modification Techniques with or without change of surface chemistry. 6. Cast irons: Classification according to graphite morphology and matrix structure. 7. Microscopy: Abbe's criterion for image formation, resolving power, numerical aperture, empty magnification, construction of simple and compound microscopes, Important lens defects and their correction. 8. Principles of bright field, dark field contrast, oblique illumination, phase contrast, interference and polarized light microscopy. 9. Metakkography - Macrography, Fractography, Photomicrography, Elements of quantitative metalography and Image processing. Term Work : Experiments and Problems based on above syllabus. Text/Reference : 1. Physical Metallurgy Principles - R.E. Reed Hill [East - West] 2. Principles of Metallographic Laboratory Practice - G.E. Kehl and H.Davis[Mc.Hill] 3. Phase Diagrams in Metallurgy - F.N.Rhines. 4. Engineering Physical Metallurgy - Y.Lakhtin[MIR Publications] 5. Physical Metallurgy Vol I-I.A.Gulyaev[MIR Publications] 6. Physical Metallurgy for Engineers-D.S.Clark and W.R. Varney[CBS] 7. Modern Physical Metallurgy - R.E.Smallman[ELBS] 8. Heat Treatment Principles and Techniques - T.V.Rajan, C.P.Sharma and A. Sharma [Prentice Hall]

POWDER METALLURGY MET : 3207 Theory : 100Marks L : 4Hrs TW/Viva : 50Marks Pr : 2Hrs Total : 150Marks 1) Introduction : Historical and modern developments in P/M. Advantages limitations and applications of P/M. 2) Characteristics of metal powder in terms of particle size , shape and size distribution, Characteristics of powder mass such as apparent density, tap density, flow rate, friction conditions. Properties of green compacts and sintered compacts. 3) Important methods of metal powder manufacturing like machining, milling, atomization, electrodeposition, reduction from oxide, carbonyl process, production of alloy powders, New development. 4) Powder conditioning, fundamentals of powder compaction, density distribution in green compacts, types of compaction presses, compaction tooling and role of lubricants. 5) Single and double die compaction, isostatic pressing, hot pressing. 6) Powder rolling, powder forging, powder extrusion and explosive forming technique. 7) Definition of sintering, stages of sintering, effect of variables on sintering, sintering atmospheres and sintering furnaces. 8) Mechanism of sintering, liquid-phase sintering, infiltration process. 9) Study of sintered bearings, cutting tools, and metallic filters. 10) Study of friction and antifriction parts and electrical contact materials. TERM WORK : Experiments and assignments based on above syllabus. TEXT/REFERENCES : 1) Powder Metallurgy :- W.D.Jones 2) Introduction to Powder Metallurgy :- A.K.Sinha 3) Principles of Powder Metallurgy :- T.Shukerman 4) Handbook of Powder Metallurgy :- H.H.Hausner

STEEL MAKING 1. Priciples of Steel makingprocess, Steel making as oxidation process. Wrought iron making, Thermodynamics of refining, Types of slags - Acid, Basic, Dry and Wet slags. 2. Raw materials for steel making, Pneumatic aqnd Hearth processes, Oxygen steel making and LD Process, Selection of steel making process. 3. LD plant layout, Jet - material interaction, Vessel and lance design, Multinozzle lances. 4. Modification in oxygen blowing processes, LD-AC and bottom blown oxygen processes, Combined blowing, Steel making in rotating vessels, Kaldo and Rotor process, Continous steel making. 5. Physical chemistry of carbon removal, Active and Inactive sites, Mechanism of oxygen transport, P,Si,Mn,S distrubition. 6. Deoxidation, Selection of deoxidizer and deoxidation practise, e.g. Simple and Complex, Mechanism of deoxidation. 7. Electric Arc Furnace process [ AC & DC ], single and double slag practise, Raw materials, classification, Chromiun - Carbon equilibrium, Rustless process, Argon Oxygen decarburisation, Vaccum oxygen decarburisation, Use of sponge iron in steel makin, advantages and limitations, Induction Furnace. 8. Gases in steel, Vaccum degassing, Ladle stream degassing, Degassing in bulk and by part, Secondary steel making, ASEA-SKF process, VAD process 9. Casting pit practise, teeming, ingot mould, Types of ingots, Ingot structures, Ingot defects and remedies. 10. Continous casting, principlrs, machines, Types, metallurgical aspects, Integrated steel plants, Alloy steel making and mini-steel plants in India. TEXT / REFERENCE 1) Introduction to Modern Steel Making :- R.H.Tupkary, Khanna Publ. Delhi. 2) Steel Making :- V.A.Kudim, MIR Publishers,Moscow. 3) Electrometallurgy of Steel :- E.P.Edneral, MIR Publ; Moscow & Ferro.Alloys Vol I & II 4) Making,Shaping and :- H.M.Gannon, USS Pub. Pittsburg. Treating of steel 5) Introduction to Physical :- R.G.Ward, ELBS. Chemistry of Steel Making

METALLURGICAL INSTRUMENTATION

ELN 3208 Theory : 100 Marks Pr./TW/Viva : 50 Marks Total Marks : 150 Marks Unit-1: Operational Amplifiers as a module & basic signal processing circuits like Inverting, Non-inverting Amplifier, Instrumentation Amplifier, Difference Amplifier Unit-2: Introductions to digital circuits, Microprocessors & system – Block diagram descriptions & operation, ADC, DAC & Interfacing. Unti-3: Resistance heating, Introduction heating, Electric heating Unit-4: Contact & Non contact measurements sensors for pressure, Temperature & Flow, humidity. Unit-5: Displays & Recording devices Unit-6: Applications – On based controllers, PID Controller for temp. – Different Electronic control applications in Wire Drawing in Arc Furnaces & Miscellaneous applications. Books : 1. Linear Integrated Circuits by Coughlin & Driscoll. 2. Engineering Electronics by Ryder. 3. Digital Electronics by Malvino

Syllabus of B. E. – IV

(Metallurgical and Materials Engineering)

PHYSICAL METALLURGY – II

MET 4101 Theory : 100 Marks L 4 hrs. Pr./TW/Viva : 100 Marks Pr. 6 hrs. Total : 200 Marks 1. Mechanism and kinetics of pearlite to austenite transformation. Grain growth of

austenite and factors affecting it. 2. Mechanism and kinetics of transformation of austenite to pearlite. TTT and CCT

diagrams. Mechanism and kinetics of bainitic transformation, variables affecting the transformation.

3. Martensitic transformation-classification, characteristics, mechanism, variables and kinetics for ferrous systems.

4. Martenstic transformation in non-ferrous systems such as In-Th, Fe-Ni and Cu-Al system. Special features such as stabilization and effect of plastic deformation.

5. Mechanism and kinetics of tempering in steel, secondary hardening, temper-brittleness. 6. Order-disorder phenomenon, carbide precipitation in stainless steel, sigma phase

formation. 7. Characteristics of formation of fine precipitates in ferrous and non-ferrous systems. 8. Phase transformation in copper, aluminum, nickel, titanium base alloys. 9. Heat treatment and applications of Non-ferrous alloys. Term Work : Experiments and problems based on above syllabus. TEXT / REFERENCES: 1. Physical Metallurgy Principles – Robert E. Reed-hill, Affiliated East-West Press, New

Delhi. 2. Fundamentals of Physical Metallurgy – John D. Verhoeven, John Wiley & Sons, New

York. 3. Engineering Metallurgy – Part 1 and 2 – Raymond A. Higgings, The English Language

Book Society and Hodder & Staughton, U.K. 4. Introduction of Physical Metallurgy – Sindey H. Avner, McGraw – Hill, New Delhi. 5. Physical Metallurgy Vol. I & II – A Gulyaev, MIR Publishers, Moscow. 6. Heat Treatment – Principles & Techniques – T.V. Rajan, C.P. Sharma and Ashok

Sharma, Prentice Hall of India, New Delhi.

NON-DESTRUCTIVE TESTING OF MATERIALS MET 4102 Theory : 100 Marks L 4 hrs. Pr./TW/Viva : 50 Marks Pr. 2 hrs. Total : 150 Marks 1. Fundamentals of and introduction to non-destructive testing. Scope and limitations of

NDT Visual examination methods. Different visual examination aids. 2. Leak and pressure testing of industrial components. Various methods of pressure and

leak testing underlying principles of these testing systems. 3. Dye penetrant and magnetic particle methods of NDT. 4. Ultrasonic methods of NDT-Basic principles of wave propagation, types of waves,

methods of UT, their advantages and limitations. Various types of transducers. Calibration methods, use of standard blocks.

5. Characterization of defects in castings, forgings, rolled and welded products by UT. Thickness determination by ultrasonic method. Study of A,B and C scan presentations.

6. Radiographic testing of metallic components. X-ray and Gamma-Ray radiography. Their principles, methods of generation. Industrial radiography techniques. Types of films, screens and penetra-meters. Interpretation of radiographs. Real time X-ray radiography.

7. Electrical methods of NDT-Conductivity & resistivity methods and their applications. Eddy current testing.

8. Thermal methods of NDT. 9. Study of advanced methods of NDT like acoustic emission, holography, tomography,

MRI etc. Term Work: Experiments / tutorials based on above syllabus. TEXT / REFERENCES: 1. Practical Non-destructive Testing – Baldev Raj, T. Jayakumar & M. Thavasimuthu,

Norosa Publishing House, New Delhi. 2. Non-destructive testing, Warren J. McGonnagle, Gordon Breach, Science Publishers Ltd. 3. Ultrasonic Testing of Materials, J. Krautkramer & Herbert Krautkramer, Narosa

Publishing House, New Delhi. 4. Treaties on Non-destructive testing, Vol. 1,2 & 3 Edited by Dr. E.G. Krishnadas Nair,

NDT Centre, Hal, Bangalore. 5. Non-destructive testing, R. Hatmshaw. 6. Ultrasonic Methods of Testing Materials, Leszek Filipezynski, Zdzislaw Pawlowski &

Jerzywehr, Butterworths, London.

ELECTROMETALLURGY AND CORROSION MET 4103 Theory : 100 Marks L 4 hrs. Pr./TW/Viva: 50 Marks Pr. 2 hrs. Total : 150 Marks 1. Electrolytic and electrochemical cells : Electrolysis, Faraday’s Law, current efficiency,

energy efficiency, decomposition voltage, over voltage, throwing power, covering power of electrolyses.

2. Electroplating, pre-electroplating preparations, electroplating of metals like copper, nickel, chromium.

3. Principles of alloy plating: Applications like electrogalvanizing, electro aluminizing, anodizing, electropoloshing, etching.

4. Corrosion of metals: Electrochemical principles applied to corrosion such as electrode potential, E.M.F. series, Nearnst equation.

5. Polarization: types, Tafel’s equation, limiting current density, exchange current density, passivity.

6. Types of Corrosion: Uniform, galvanic, pitting, crevice corrosion, filiform corrosion, intergrannular corrosion, knife-line attack, selective leaching.

7. Stress Corrosion: erosion corrosion, tretting corrosion. Calvitation damage, corrosion fatigue, hydrogen damage and embrittlement.

8. Corrosion Prevention Methods: Material selection & design, cathodic protection, Use of inhibitors etc.

Term Work : Experiments based on above syllabus. TEXT / REFERENCES: 1. Corrosion Engineering – Mars G. Fontana and Norbert D. Green, McGraw-Hill, New

Delhi. 2. Eletrodeposition and Corrosion Processes – J.M. West, D. Van Nostrand Company Ltd.,

London. 3. An Introduction to Electrometallurgy – Satya Narayan & Rajendra Sharan, Standard

Publishers & Distributors, New Delhi.

PRINCIPLES OF METAL JOINING MET 4104 Theory : 100 Marks L 4 hrs. Pr./TW/Viva: 50 Marks Pr. 2 hrs. Total : 150 Marks 1. History, Importance of Metal Joining Processes : Theory of Metal joining, barriers of

welding, classification of welding processes. 2. Fusion welding: Joint design and edge preparation, methods and selection, nature of heat

sources, physics of arc, electrical characteristic of arc, machine characteristics. 3. Metal transfer, forces acting on the arc, different modes of metal transfer, heat flow in

metals, prediction of heating and cooling rates. 4. Gas-metal and slag-metal reactions, evolution of gases, formation of porosity, inclusions

in weld metal, weld pool solidification, residual stresses, weld cracking, solidous and sub-solidous, dilution.

5. Fusion welding: SMAW – ‘unction of coatings, based on slag metal, gas metal reactions, classification of coating types, formulation of continuous welding by coated electrodes, SAW, electroslag welding.

6. GTAW, GMAW, FCAW, Plasma Welding, type of guns. 7. Electron beam welding: Laser beam welding, gas welding, cutting methods. Solid phase

welding, cold pressure welding, hot pressure welding, friction welding, explosive welding, ultrasonic and diffusion welding.

8. Resistance welding: Contact resistance, spot, seam projection, resistance butt, flash butt etc. Soldering and brazing, theory, types of alloy systems, methods of heating type of joints, adhesive joining.

9. Weldability of carbon and low allow steels. Hydrogen embrittlement, Brittle fracture, weldability of stainless steels, weldability tests, weldability of non-ferrous systems.

10. Quality control in welding, procedure for control of material, establishment of correct welding procedure, qualification of operators, testing and inspection during and after welding. Welding defects.

Term Work: Experiments based on above syllabus. TEXT / REFERENCES: 1. The Metallurgy of Welding, Brazing and Soldering – J.F. Lancaster, George Alien and

Unwin Ltd., London. 2. Introduction to Welding and Brazing – D.R. Milner & R.L. Apps. Pergamon Press,

London.

ADVANCED FERROUS METALLURGY (Elective –I) MET 4105 Theory : 100 Marks L 1 hr. Total : 100 Marks 1. Thermodynamics and kinetics of iron oxide reduction. Kinetics of solid – solid and

solid-gas reactions. 2. Problems of Indian Steel Plants. High temperature properties of Iron-bearing materials. 3. Modern developments in blast furnace, charging system and coal injection, equipment

and theoretical considerations. Mini blast furnace. 4. Methods of sponge iron production and their importance under Indian conditions. Uses as

feed material for Iron and Steel Industries. Reduction smelting processes. 5. Pre-treatment of hot metal. Physico-chemical aspects of pre-treatment processes. Status

of hot metal treatment in India. 6. Electric arc furnace steel making. Design of EAF-AC, DC electric arc. Latest trends in

EAF design and operation. 7. Secondary steel making processes. Alloy steel making in EAF using secondary refining.

Continuous casting. 8. Roll of synthetic slags. Electroslag refining. Slag-metal reaction in iron and steel

making. 9. Ferro-alloy production. Application of plasma technology. TEXT / REFERENCES:

1. International Symposium on Blast Furnace Iron Making, Jamshedpur, Nov. 1985, organized by the Indian Institute of Metals and the Tata Iron & Steel Company Ltd.

2. Workshop on Production of Liquid Iron using coal, Eds. H.S. Ray et al, Allied Publishers Ltd., New Delhi, 1994.

3. Principles of Secondary Processing & Casting of Liquid Steel – Ahindra Ghosh, Oxford & IBH, New Delhi.

4. Electrometallurgy of steel and ferro-alloys, Vol. I & II, F.P. Edneral, MIR Publishers, Moscow.

ENERGY ECONOMY AND WASTE MANAGEMENT (Elective –I)

MET 4106 Theory : 100 Marks L 4 hrs. Total : 100 Marks 1. Energy sources for industrial applications. Economic value of energy conservation.

Economics of alternative sources of energy for industrial applications. 2. Requirement of energy in Metallurgical processes. Areas of intensive use and scope for

efficient utilization. Energy spent in extraction / processing of metals and materials. 3. Energy analysis – Review, methodology and conventions. Methods use in energy

analysis. Effect of energy saving measures. Application of thermodynamic principles and energy balance.

4. Perspectives in energy conservations – Alternative routes of extraction of metals for energy saving. Direct reduction v/s Conventional route for steel making. Role of optimal selection of metal processing route. Conservation through protection of materials against decay. Waste heat recovery methods.

5. Case studies in energy conservation in metallurgical industry. Use of energy efficient equipments.

6. Classification of industrial waste. Effect of waste on environment and resources. Economic value of industrial waste. Waste disposal v/s recycling and secondary uses (value added products).

7. Effect on environment due to excessive use of gaseous, liquid and solid resources from earth. Environmental degradation due to minimizing, disposal of lean ores, pollution due to water used. Extraction from leaner ores, recycling of spent metal for energy saving and use of water in industrial processes. Generation of waste during primary processing of ores and beneficiation.

8. Air pollution and control due to toxic and non-toxic gases, fumes, dust etc. during combustion, heating and roasting processes and industrial production, control methods, cleaning of gaseous effluents, recovery of economic value from gases.

9. Generation of solid waste in metallurgical and powder industry. Economic uses of solid waste such of B.F. slag and fly ash & wastes from non-ferrous industry.

10. Water pollution. Methods of treatment of waste water, recovery and recycling of effluents water. Case studies related to waste management in metal related industries. Knowledge of Environmental system, ISo-14000.

TEXT / REFERENCES: Recent books, journals and Periodicals covering above topics are to be followed.

NUCLEAR METALLURGY (Elective –I)

MET 4107 Theory : 100 Marks L 4 hrs. Total : 100 Marks 1. Atomic structure. Fundamental properties. Atomic nucleus. Radio activity. Half life

period and isotopes. 2. Fission, fusion and othernuclear reactions. Critical mass. Nutron cross section.

Multiplication factor and nuclear disintegration. 3. Essential parts of a nuclear reactor. Reactor types. Reactor fuel cycle. 4. Indian atomic power plants. Nuclear power programme in India and future trends. 5. Difference in separation methods as compared to conventional methods. Purity

requirements of nuclear metal. Separation processes – Ion and solvent extraction techniques.

6. Occurrence, extraction, mechanical and physical properties and use of uranium and thorium.

7. Occurrence, extraction, mechanical and physical properties and uses of zirconium, hafnium and plutonium.

8. Methods of production of ultrahigh purity metals and their importance in nuclear metallurgy. Influence of radiation damage on mechanical properties. Scope of beryllium in nuclear plants.

TEXT / REFERENCES: 1. Nuclear Reactor Fuel Elements – Metallurgy and Fabrications – Kaufmann. 2. Proceedings of Seminar on Nuclear Metallurgy, March 1978, IIM, Bombay Chapter and

IE, Maharashtra State. 3. Extraction of Non-ferrous Metals – H.S. Ray, R. Sridhar, K.P. Abraham, Affiliated East-

West Press Pvt. Ltd. 4. Zone Mellign – William G. Pfann, John Wiley & Sons Inc., New York.

COMPOSITE MATERIALS-I MET 4108 Theory : 100 Marks L 4 hrs. Total : 100 Marks 1. Introduction, relevance as modern materials, classification & basic characteristics of

composites. Strengthening mechanism in various types of composite materials. 2. Production and properties of various types of fibre reinforcing materials such as glass,

carbon etc. 3. Treatment and intermediate processing of various fibres, their structure and morphology.

Properties of particulate reinforcements. 4. Classification on the absis of matrix. Types and properties of matrix. 5. Interfaces – Interaction and types of bonding at the interface. Tests for measuring

interfacial strength. 6. Metal matrix composites – scope, properties and applications. Methods of fabrication. 7. Poly er matric composites – scope, properties and applications. Methods of fabrication. 8. Ceramic matrix composite – scope, properties and applications. Methods of fabrication. 9. Mechanical properties of composites – tensile elastic and fatigue properties. Fracture

modes in composites. 10. Plastic deformation, joining and machining of composite materials. Mechanical testing

of composite materiasl. Examples of some critical applications of composite materials. TEXT / REFERENCES: 1. Composite Materials – Lensile – Holliday, Elsevie Publishing Company, Amsterdam. 2. Modern Composite Materials – Lawrence J., Broutman and Richard H. Krock, Addison-

Wesley Publishing Company, California. 3. Advances in Materials & their Applications – edited by P. Ramarao, Wiley Eastern Ltd.,

New Delhi.

NON-FERROUS ALLOYS (Elective –I)

MET 4109 Theory : 100 Marks L 4 hrs. Total : 100 Marks 1. Phase diagrams of various non-ferrous alloys (Al-alloys, Cu-alloys, Ni-alloys, Ti-alloys,

Mg-alloys, Zn-alloys) and strengthening mechanisms in non-ferrous alloys. 2. Alumnium and its alloys: Physical metallurgy of aluminium alloys. Principles of age-

hardening. Ageing processes. Mechanical behaviour. 3. Wrought aluminium alloys and cast aluminium alloys: Compositions, heat treatments,

properties and applications. 4. Copper and its alloys: Compositions, heat treatments, properties and applications. 5. Magnesium and its alloys: Zinc and its alloys, Compositions, heat treatments, properties

and applications. 6. Nickel and its alloys: Ni-Cr alloys, Ni-Al alloys, Ni-Cr-Al alloys, Ni-Cr-Al-Ti alloys:

Compositions, heat treatment, properties and applications. 7. Complex Nickel-base alloys: Solid-solution strengthening of Gamma, solid-solution

strengthening of gamma prime, amount of gamma prime. Anti-phase boundary energy, Lattice mismatch. Coarsening of gamma prime. Oxidation and corrosion resistance. Longtime phase stability. Applications.

8. Titanium and its alloys: Compositions, heat treatments, properties and applications. 9. Fabrication and corrosion behaviour of various non-ferrous alloys. TEXT / REFERENCES: 1. Physical Metallurgy for Engineers – Donald S. Clark, & Wilbur R. Varney, CBS

Publishers & Distributors, New Delhi. 2. Metals Handbook Ninth Edition – Vol.2, Properties and Selection: Non ferrous alloys and

Pure Metals, American Society for Metals, Metals Park, Ohio. 3. Introduction to Physical Metallurgy – Sidney H. Avner, McGraw-Hill Book Company,

New Delhi. 4. Relevant Indian and Foreign Standards. 5. Heat Treatment, Structure and Properties of Non-ferrous Alloys – Charlie R. Books,

1982, ASM.

STRUCTURAL METALLURGY

MET 4210 Theory : 100 Marks L 5 hrs. Pr./TW/Viva: 75 Marks Pr. 4 hrs. Total : 175 Marks 1. Crystal geometry, crystal systems & bravais lattices, laws of rational indices, zones &

zone axis, summitry class & point groups, directions & planes, slip planes & screw axis, atom sizes and coordination.

2. Stereographic projections and its application. Polymorphism – definition, thermodynamic concept of polymorphism and examples.

3. X-rays: generation, properties, electromagnetic radiation, continuous spectrum, characteristic spectrum, absorption filters, detection and safety precautions. X-ray diffraction.

4. The Bragg’s Law, Diffraction methods, X-ray scattering, structure factor and its determination.

5. Crystal structure determination, phase diagram determination. Electron and neutron diffraction.

6. Crystallite size determination. Stress measurement, preferred orientation and chemical analysis by X-rays.

7. Electron microprobe analyzer, X-ray microscopy and field ion microscopy. 8. Scanning electron microscopy. Free-energy composition diagram. 9. Free electron & zone theory of metals. Zone theory of alloy phases. 10. Conductors, semi-conductors and insulators based on free electron & zone theory of

Metals. Ferromagnetism, diamagnetism and paramagnetism. Superconductivity. Term Work: Experiments based on above syllabus. TEXT / REFERENCES: 1. Structure of Metals – Crystallographic Methods, Principles & Data-Charles S. Barrett &

T.B. Massalski, Eurasia Publishing House (Pvt.) Ltd., New Delhi. 2. Theoretical Structural Metallurgy – A.H. Cottrell, The English Language Book Society &

Edward Arnold (Publishers) Ltd., U.K. 3. Elements of X-ray Diffraction – B.D. Cullity, Addison – Wesley Publishing Company

Inc., USA. 4. Physical Metallurgy Principles – Robert E-Ree-Hill, Attiliated East-West Press Private

Ltd., New Delhi.

MATERIAL TESTING AND STANDARDS MET 4211 Pr./TW/Viva : 50 Marks Pr. 2 hrs. Total : 50 Marks Practicals based on following syllabus: 1. Importance of Material Testing. Classification of various type of testing methods.

Selection of testing methods. 2. Importance of calibration of Testing Instruments. Calibration methods and standards.

Following tests / experiments based on methods with active reference to various codes and standard for each test.

3. Hardness testing – Rockwell, Brinell, Vickers, Poldi-Shore sclarescope, Cupping test, Impact testing including subzero, Tensile testing on Monosanto, Coid rolling and study of grain structure. Wire drawing. Fatigue testing. Wear testing. Annealing.

4. Handling of data. Material testing & Interpretation, design of experiments. TEXT / REFERENCES: 1. Inspection of Materials, Vol. II – Destructive Methods, R.C. Andersen, ASM 1988. 2. Testing of Metallic Materials – A.V.K. Suryanarayan, Prentice Hall of India. 3. Workability Testing Techniques, G.E. Dieter, ASM 1984. 4. Relevant codes and standards.

ALLOY STEELS MET 4212 Theory : 100 Marks L 4 hrs. Pr./TW/Viva: 50 Marks Pr. 2 hrs. Total : 150 Marks 1. Plain carbon steel: Review of FFe-Fe2C phase diagram, Classification of steels on the

basis of composition, equilibrium structure and method of manufacturing process. Effect of carbon and inherent impurities on properties of steels. Apllications of plain carbon steels. Limitations of plain carbon steels.

2. Constitution of Alloy Steels: Purpose of using alloying elements, mode of combination of alloying elements in annealed state, classification of alloying elements, various effects of alloying elements additions to steel.

3. Structural steels: Property requirements, methods of improving strength of structural steels, characteristics and applications of mild steels, medium carbon and low-alloy steels, HSLA steels, ball bearing steels, alloy casecarburising steels. Discussion on the basis of AISI specifications.

4. Special Steels: Hadfield Mn-steels, marageing steels, ausforming steels, TRIP steels. 5. Tool Steels: Classification of tool steels, requirements of properties for various types of

tools. Characteristics of high speed steels, annealing, hardening and tempering of high speed steels, role of alloying elements in high speed steels.

6. Water-hardening tool steels, cold work tool steels, hot-work tool steels, shock resisting steels and special prupose tool steels, factors for selection of tool steels.

7. Stainless steels: General features and classification of stainless steels, various types of phase diagrams. Austenitic and duplex stainless steels.

8. Martensitic, ferritic and precipitation hardenable stainless steels. Examples of newly developed compositions of stainless steels & their applications.

9. Creep and heat resisting steels, dual phase steels, wear resistant steels. 10. Standards in alloy steels – Study of a few selected standards. Term Work: Experiments based on above syllabus. TEXT / REFERENCES: 1. Alloying Elements in Steel – Edgar C. Bain, Harold W. Paxton, American Society for

Metals, Metals Park, Ohio. 2. Structure and Properties of Alloys – Robert M. Brick, Robert B. Gordon & Arthur

Phillips, Eurasia Publishing House (Private) Ltd., New Delhi. 3. Phisical Metallurgy – Vol. II – A Gulyaev, MIR Publishers, Moscow. 4. Metallurgy and Heat Treatment of Tool Steels – Robert Wilson, McGraw-Hill Book

Company (U.K.) Ltd. London. 5. Physical Metallurgy for Engineers – Donald S. Clark & Wilbur R. Varney, CBS

Publishers & Distributors, New Delhi. 6. Metals Hand Book Ninth Edition – Vol. 1.

ADVCANCED FOUNDRY ENGINEERING (Elective –II)

MET 4214 Theory : 100 Marks L 4 hrs. Pr./TW/Viva: 50 Marks Pr. 3 hrs. Total : 150 Marks 1. Structure and properties of liquid metals and their relevance to casting practice. 2. Physicochemical properties of liquid metals such as surface tension and viscosity. Effect

of variables on these properties and their control. 3. Liquid density and fluid flow concept, shrinkage phenomena in cast alloys. Their

evaluation and control. Different types of shrinkage cavity formation. 4. Dissolution of gases in liquid metals. Gas-metal systems. Gas-removal practices for

ferrous and non-ferrous alloys. Effect of dissolved gases on castings unsoundness. 5. Metallurgy of cast iron: Gray, white, wear resistant, malleable, S.G. ADI and C.G. cast

irons, their engineering properties and applications. 6. Melting of alloy and special cast irons, melt treatment such as inoculation, Mg treatment

desulphurization mechanism, malleabilization cycle and its control, microstructure of alloy cast irons, their properties and applications.

7. Steel foundry practice – Melting practice, moulding materials, methoding practice with examples.

8. Special mould and core making methods both, organic and inorganic, developments in casting practice such as Rheo, Thixo, Compo-casting etc.

Term Work: Experiments base on syllabus. TEXT / REFERENCES: 1. Principles of Metal Casting – Rechard W. Heine, Carl R. Loper & Philip C. Rosenthal,

Tata McGraw – Hill Publishing Co. Ltd., New Delhi. 2. Fundamentals of Metal Casting – Richard A. Finn, Addison-Wesley Publishing Company

Inc., USA. 3. Fundamentals of Metal Casting Technology – P.C. Mukherjee, Oxford and IBH

Publishing Company Private Ltd., New Delhi. 4. Metallurgical Principles of Founding – V. Kondic, Edward Arnold (Publishers) Ltd.,

London.

CORROSION ENGINEERING (Elective - II) MET 4215 Theory : 100 Marks L 4 hrs. Pr./TW/Viva: 50 Marks Pr. 3 hrs. Total : 150 Marks 1. Thermodynamics of corrosion, pourbaix diagrams. Fe-O-H system. Hydrogen & oxygen

evolution. Kinetics of electrochemical reaction.

2. Activation, concentration and mixed polarizations. Mixed potential theory. Anodic and

cathodic polarizations.

3. Theory of inhibition. Zero charge potential. Electrical double layer. Type of inhibitors.

Some corrosion inhibitor examples.

4. High temperature corrosion. Oxidation corrosion with flue gases. Oxides of carbon,

sulphur containing gases. Sulphidation, corrosion in air, corrosion by molten salts.

5. Cooling water. Quality of natural water. Formation of deposits. Corrosion in power

equipment. Deareation, deoxigenation, corrosion of different alloys and metals in water.

6. Methods of combating corrosion with special reference to metallic and non-metallic

coatings. Improvement in design. Cladding Advances in cathodic and anodic protection

techniques. Corrosion resistant alloys in brief.

7. Corrosion testing methods. Weight loss method and its limitation.

8. Other Practies: Electro chemical methods. Accelerated tests such as potentiodynamic test

and EPR test. AC Impedance Methods. ASTM A262 practices A-E, ASTM tests for

pitting / crevice and galvanic corrosion.

Term Work: Experiments base on syllabus. TEXT / REFERENCES:

1. Corrosion Engineering – Mars G. Fontana and Norbert D. Green, Mcgraw-Hill

International Book Company, New Delhi.

2. Corrosion and Corrosion Control – An Introduction to Corrosion Science & Engineering

– Herbert H. Uhlig. John Wiley & Sons Inc., New York.

3. Corrosion – Vol. 1 & 2 – L.L. Shreir, R.A. Jarman & G.T. Burstein, Butterworth

Heinermann, U.K.

WELDING METALLURGY (Elective - II) MET 4216 Theory : 100 Marks L 4 hrs. Pr./TW/Viva: 50 Marks Pr. 3 hrs. Total : 150 Marks 1. Importance of Metallurgy in Welding. Concept of weldability. Review of classification of

welding processes. 2. Metallurgy of solid phase welding, Effect of variables such as deformation &

temperature. Mechanism of welding in various solid phase welding processes such as cold pressure, ultrasonic friction and diffusion welding.

3. Heat flow equation and its refinements, weld simulation. Effect on microstructure. Effect of preheat and post heat on rate of cooling of weldments.

4. Physical chemistry of slag metal reactions. Trasfer of alloying elements from fluxes. Effect of dilution on chemical composition. Gas absorption and effect of gases on weldments. Gas flow equation for hydrogen. Principles of consumable developments for various fusion welding processes.

5. Epitaxial nucleation. Mode of solidification and segregation. Kinetics of phase transformation in carbon steels, low alloy steels and stainless steels.

6. Mechanism of cracking and embrittlements. Fracture toughness and its testing applied to weldments. Solidification cracking. Liquation cracking. Lamellar tearing. Cold cracking. Reheat cracking and strain age embrittlement. Tests for above.

7. Weldability of non-ferrous alloys especially aluminium, nickel and titanium alloys. 8. Joining metallurgy of the dissimilar metals, clad metals etc. Welding metallurgy of

various types of cast irons. Metallurgy of repair welding. Welding metallurgy of spray coating. Metallurgy of cutting.

Term Work: Experiments base on syllabus. TEXT / REFERENCES: 1. Introduction to Physical Metallurgy of Welding – Kenneth Easterling, Butterworths &

Company (Publishers) Ltd., London. 2. The Metallurgy of Welding, Brazing and Soldering – J.F. Lancaster, geroge Allen and

Unwin Ltd., London.

SELECTION OF MATERIALS AND FAILURE ANALYSIS

MET 4217 Theory : 100 Marks L 4 hrs. Pr./TW/Viva: 50 Marks Pr. 3 hrs. Total : 150 Marks 1. Philosophy of material selection, relationship to available resources, concept of resource

base. Criteria for selection of engineering materials – service requirements, ease of manufacturing, availability of materials and cost effectiveness.

2. Selection for mechanical properties like strength, toughness, stainless, fatigue, creep and temperature resistance.

3. Selection for surface durability like for corrosion resistance, wear resistance. Relationship between material selection and material processing.

4. Identification of required properties. Selection of material based on available property data and optimization to select the best material.

5. Case studies in material selection like materials for bearings, gears, aircraft components etc.

6. Importance of failure analysis and its relationship to material selection, fundamental causes of failure. General practice in failure analysis.

7. Identification and characterization of ductile and brittle type of failures. 8. Identification and characterization of fatigue failures. Tyes of fatigue, corrosion fatigue

and contact fatigue etc. 9. Corrosion and corrosion related failures such as hydrogen embrittlement, stress-corrosion

cracking and high temperature failures. 10. Failure of boiler and related high temperature power plant equipment, tube and piping.

High temperature related degradation studies. Term Work: Experiments base on syllabus. TEXT / REFERENCES: 1. Selection & Users of Engineering Materials – F.A.A. Crane & J.A. Charles, Butlerworth

& Com. (Publishers) Ltd., London. 2. Engineering Materials – Vol. 1 and 2 – Michael F. Ashby & David R.H. Jones, Pergamon

Press, New York. 3. Engineering Materials – Selection and Value Analysis – H.J. Sharp, Elsevier Publishing

Company Inc., New York. 4. Analysis of Metallurgicval Failures – V.J. Colangelo & F.A. Heiser, John Wiley & Sons,

New York. 5. Metals Hand Book – Eighth Edition – Failure Analysis and Prevention, American Society

for Metals, Metals Park, Ohio. 6. Metals Hand Book – Eightgh Edition – Factography, American Society for Metals,

Metals Park, Ohio.