thallium data · 2020. 12. 11. · -3.2-2.6 s7z.dev.-1 o 1 € height (absorbance' apea...
TRANSCRIPT
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THALLIUM DATA
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.•CONT:I>] PEAK HEIGHT <ABSOPBANCEI o' PEAK AREA IABS-SECONDS1 0
READ! 58.4
MEAN* 58-3 3T3.DEV.* 0.2
53.3E-50: READING 3PEATEP THAN HI
59.4 STANDARD 3
TL- 10 os Q tsftuq'lJL)PEAfr HEIGHT (ABSCPBAIMCE; 0PEAK AREA : ABS-SECONDS) 0
PEAD : 51-4 An -7 • / >............... .............y. ti «< /.' ~ LPEAK HEI3HT -' ABSCPBANCE1 0PEAK AREA 1 AE'S-SECINirS 0
READ; 5!. 5
MEAN* 51.4 ST;.DEV.= 3.3
PEAK HEIGHT • ABS^EAMCE- oPEAK AREA (ABS-SECCNES) "
READ! -l.S
PEAK HEI'HT ' ABSCRBANCE ) 0PEAK AREA ( ABS-SECCNrS1 0
PEAD: -2.S
MEAN« -2.1 S7C.DEV.' 0.7
PEAK HEIGHT • A3SORBANCE • 0PEAK AREA .'ABS-3ECONE3) 0
READ: -2.:
PEAK HEIGHT IABSOPBANCEI oPEAK AREA I ABS-SECONDS! 0
READ: -2.5
MEAN» -2.3 3TD.DEV.» 0-2
TL- iooa /$l&/)Jl QfiJL 6PEAK HEIGHT (ABSORBANCE) 0
' PEAK AREA (ABS-SECONDS) 0
' READS 19.5 £jeZ /... ... ....................... __.__/W/.'
PEAK HEIGHT (ABSORBANCE) 0PEAK AREA (ABS- SECONDS) 0
READ: 18.9
MEAN« 19.2 STC.DEV.s 0.4
TI_ 1009 $7//053-O/£PEAK HEIGHT < ABSOPEANCE ) 0PEAK AREA (ABS-SECONDS) 0
llHCMi -2.0
AA.524-375
C;EF,
CHEST iTA!"
AA.5-4.310
^ /i/ /L Jt /
AA *.5"!. 317
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AA- C32- 32 1
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COEF.
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AA.020.018
COEF.
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. 149
AA.233. 145
COEF.
AA.039.063
:AA0. 3380.220
.VAP.« 0.33 .'
JD APD
3.3373. 131
-.,0. 3373, 131
Vtp. = " • " 't.
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•3 . -3060.300
VA? . - 33 . 32 i
:AA3.0060.002
ZAAo.:o4•3.000
VAP.« 10.50 t
ZAA0. 1440.073
t ..-.. ........<T ZAA
0. 1400.076
VAR.3 2. 15 *
ZAA0.0070.002
BC0 . 2660. 133
BCC.2390. 1 19
BC0 . 2350. 12S
BG0. 3293-017
0-3320.021
0. 31"0.017
3.013P. 017
BG0. 1000.071
BG0.0990.069
BG0.0360.060
26
PEAK HEIGHT 'A350P3ANCE '=EAK AREA .'ABS-SECGNSS'
PEAD: -2-3
PEAK HEIGHT 'ABSCPEAMCEIPEAK AREA (ABS-SECONDS!
PEAD : -2.0
1EAN= -2.4 S7Z.DEV.S
3.;?: -:.•:::
OS- T&bAA ZAA
3.026 O.CCe3. 732 7 . 072
zoC . 0243.730
FG3.02S•3.030
TL- 1 O 1
PEAKPEAK
PEAD:
PEAKPEAK
READ:
MEAN-
Tt-
PEAKPEAK
HEIGHT 'APSOPBANCE)AREA (ASS -SECONDS)
-1.9
HEIGHT (ABSOPEANCE)AREA IABS-SECCNDS'
-3.2
-2.6 S7Z.DEV.-
1 O 1 €
HEIGHT (ABSORBANCE'APEA (ABS-SECONDS)
A
0
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0.9
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AA.034. 029
AA. 033.024
AA.034.021
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0-0
COEF.VAR. »
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ZAA.ooe.303
ZAA.C05.032
35. 85 S
ZAA.003.000
00
00
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BG. 334. 326
BC.032.026
BC.033.021
PEAK HEIGHT 'PEAK APEA
READ: -3,6
*!EAN* -3.1 STD.DEV.. 0.5 COEF.VAR,. 20.26 t*********»»«*»«***»«jTU 101S f<___ __ _
AA ZAA BCPEAK HEIGHT (ABSORBANCE) 0.596 0.344 0.232PEAK AREA (ABS-SECONDS) 0.322 0.186 0.137
1U... ........................AA ff ZAA BG
PEAK HEIGHT (ABSORBANCE) 0.381 0.332 0.250PEAK AREA (ABS-SECONDS) 3.322 0.184 0.138
READ: 49.4
(1EAN« 49.6 STD.DEV.- 0.4 COEF.VAR.- C.79 t»**«»»»«»»»*»**««»»«»»*«»»»****«»*»»»»»«»#»«»»*«*»»***»**»»»»****»*«»»*4*»»»»»»»
. AA ZAA BG; PEAK HEIGHT (ABSORBANCE) 0.027 o.oos 0.023!PEAK AREA (ABS-SECONDS) 0.031 0.301 0.030
PEAD: -2.4
AA ZAA BGPEAK HEIGHT (ABSORBANCE) 3.023 3.005PEAK AREA (ABS-SECONDS; 0.02S O.OOG
I*JREAD? -2.7 11R
HEIGHT ABSORBANCE' __AREA 1ABS- SECONDS 3.~f«~" 3.
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PEAK HEIGHT (AESOREANCE'PEAK AREA (ASS-SECONDS'
PEAD: 13.9
PEAK HEIGHT 'ABSCFBANCE!PEAK AREA ( AB3-SECCND5 '•
READ : 13.3
MEANs 13.3 3T7) .
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PEAK HEIGHT (ABSORBANCE1PEAK AREA (ABS- SECONDS)
PEADi -3.3
PEAK HEIGHT (ABSOP3ANCE)PEAK AREA ' AES-SECGNDS i
\D - -3,3
MEAN- -3.3 S77j .
PEAK HEIGHT (A3SCPSAN3.E)PEAK APEA i ABS-SECONDS •
PEAK HEIGHT (ABSCPBANCE)PEAK AREA (ABS-SECONDS'
READ: 17.9
MEAN- 17,3 STO.
TI- 1026 Q&Ji
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ASS-SECONDS'
P.EADl -3.0
PEAK HEIGHT (ABSOPBANCE)PEAK AREA 1 ABS- SECONDS'
READs -3.1
MEAN- -3.0 S77I.**4*« »«»»*•»»»»«»»»**»»*
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AA. 347.031
COEF.VAP.
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JU&Qt&lAA ^.236.152
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AA.032.019
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ZAA0.0040.003
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ZAA3. 12SO.C68
ZAA0. 1270,072
- 4.77
ZAA0.0060.001
ZAA0.0060.002
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ZAA0.3200. 177
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BC0.0330.373
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BC0.0470.033
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BC0. 1130.073
BC0. Illo.oao
BC0.0290.020
BG0.0310.021
t»»»»»»*»»««§»»»»»»»
BG0.2330.126
JPEAD: ' °........... ........y.. ..........
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MEAN* -;,= 3~Z. ?£'/.=
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READ: 24.1
MEAN- 24.7 S~Z.3EV.»
TL. 1033 _/£)/
PEAK HEIGHT <ABSCRBA?*:E:PEAK AREA 'AES-3E:ON2S>
PEAD: -2.4
PEAK HEIGHT 'ABSOPBANCE.PEAK AREA 'ABS-SECONDS1-
READ: -I. I
MEAN- -1." 372. DEV. *
TL, 103-4 -/QA-clisUQPEAK HEIGHT : ABSOPBADCE 'PEAK APEA • ABS-3EC3NCS!
PEAD: -2.3
PEAK HEICHT 'APSOPE'ANCE)PEAK APEA ( ABS- SECONDS '
PEAD: -2.4
r ,0.
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AA035033
AA033033
AA050037
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ZAA5.010•3.001
ZAA0.3107-. 003
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ZAA0.0030.301
DZAA0.0113,00!
B:o. :300.095
BG0.3530.032
BG0.0530.05C
BG0. 0433.056
BG3.0490.033
MEAN- -2.4 STZ.5EV.- 0.1 COEF.VAP.« 3.33 t• *«»»*»«»»»»»»»»»»»*»»»«t»»»»»»«»»»«*HH*»l«»»»**»»«*«*»*»*«*t»**»***»»«»»H»»»*
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' PEAK HEIGHT (ABSOPBANCE' 3.033 0.033 0.030PEAK APEA (ABS-SECONDS 0.047 0.001 0.046
READ: -2.2
AA ZAA BG'' PEAK HEIGHT ' ABSOPBANCE' 0.033 3.009 0.030PEAK AREA (ABS-3ECONE3 0.049 0.002 0.047
< READ: -2.0
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-A/>1HEIGHT (ABSORBANCE)AREA (ABS-SECONDS)
-0.9
HEIGHT (ABSORBANCE)AREA iABS-SECONDS)
-2.3
-1.7
2OO9
STD.DEV.
~/SAHEIGHT (ABSCRBANCE)AREA (ABS-SECONDS)
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HEIGHT (ABSOPBANCE)AREA i ABS-SECONDS;-2.4
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ZAA0.0090.006
ZAA3.C093,000
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ZAA0.0120.002
ZAA-3.0113,001
I
BG0.0440.048
BC0.0460. 052
BC0.0363.077
BG0.0610.072
MEAN- -2.3 3T2.EEV.= 0.1 COEF.VAP.= 5.97 tt»««*t*«*»»«*»*«**»«**«***«»«»««*»«»**«»*»ttt»*«**«»******««*****»**»*»»******»*
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PEAK HEIGHT (ABSOPBANCE) 0.075 O.OC7 0.073PEAK AREA (ABS-SECONDS) 0.095 0.002 0.093
READl -2.0
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READ: -1.3
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PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
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BC0.0900.193
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PEAK AREA (ABS-SECONDS)/^' ^^ Q. 33S " 0.271 0.065
MEAN- 40.3 STD.DEV.' O.S COEF.VAR." 1.38 X
40.3 E-23s READING GREATER THAN HIGHEST STANDARD.itttttnt****** *****************************************************************
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AA AA-8C BCPEAK HEIGHT (ABSORBANCE) 0.7S9 0.749 0.024PEAK AREA (ABS-SECONDS) 0 . 4SS 0.399 0 . 06S
39.2
A A AA-BG BGPEAK HEIGHT (ABSOPBANCE) 0.749 0.729 0.023PEAK AREA (ABS-SECONDS) 0.475 0.412 t O.OS4
(CONTINUED)61. 1
MEAN- SO.2 STD.DEV.« 1,4 COEF.VAR.a 2,27 t
60.2 E-25: READING GREATER THAN HIGHEST STANDARD.****************************»***********t*ntt***********************************
60.1 STANDARD 3************************* ************.****Jt****f *********************************AS 1001 UJS3T1-M "Ht I /oo-/ -<-
AA AA-EC BGPEAK HEIGHT (ABSORBANCE) O.S16 0.394 0.023PEAK AREA (ABS-SECONDS1 0.373 0.306 0.067
45.6
AA AA-BG SGPEAK HEIGHT (ABSORBANCE) 0.603 0.378 0.023PEAK AREA (ABS-SECONDS) 0.376 0.309 0.068
46.0
MEAN" 43.8 STD.DEV." 0.3 COEF.VAR." 0.63 X****»*•»»*•***»*••»***••**••**•»»»»*»***»•»••**»»*•**•»•»»•*••••»•»»»•»»•»*•»**«
AS 1002A A AA-BG BG
PEAK HEIGHT (ABSORBANCE) 0.024 0.008 0.024PEAK AREA (ABS-SECONDS) 0.039 -0.006 0.065
0.3
A A AA-BC BGPEAK HEIGHT (ABSORBANCE) 0.026 0.008 0.024PEAK AREA (ABS-SECONDS) 0.053 -0.010 0.064
-0.3
MEAN-. 0.0 STD.DEV.- 0.4 COEF.VAR.- 99.99 X»*»»*••»•«**••«••*•«#•»»••»»»•»•••*•••»••*•**•*«•**•*•*•*•**•*»•****»*»********«AS 1003 SjUe. soso P ti-a
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.028 0.007 0.027PEAK AREA (ABS-SECONDS) 0.056 -0.010 0.063
-0.3 _____________............................. ^ AA-BC BC " ,
PEAK HEIGHT (ABSORBANCE) 0.029 0.010 0.026PEAK AREA (ABS-SECONDS) 0.032 -0.010 0.061
-0.4
NEAN."""-0~3~ STD.OEV.. J;,,,. ; .. ..J.,,..,AE«I»0\? 7 "? £HE -******-Or"****STD"EV?-*******"r****COEF?VAR?**"|?irr* ^ O t3/TV?... ..-,,....,,.,................*••..•»•*»••»••••*»•••••»»•*••••*•»•**•****»
\ 37.6..................... y. ...........
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
38.2
MEAN' 37.9 STD.DEV,'
AS 1010 -If 1
PEAK HEIGHT IABSORBANCE)PEAK AREA (ABS-SECONDS)
33.0
PEAK HEIGHT (ABSOPBANCE)PEAK AREA (ABS-SECONDS)
37.6
MEAN' 37.3 STD.DEV.'
AS 1 O 1 1 C aJj i
PEAK HEIGHT (ABSOPBANCE)PEAK AREA (ABS-SECONDS)
2.4
PEAK HEIGHT (AESORBANCE)PEAK AREA (ABS-SECONDS)
-0,2
MEAN' 1. 1 STD.DEV. «
AA AA-BC0.513 o,3400.553 0.233
0,4 COEF.VAR. a 1.15 *
AA AA-BG0.612 0. 3410.639 0.254
A A AA-BC0.619 0.3520,542 0.231
0.3 COEF.VAR.* 0.72 1-
AA AA-BG0.098 0.0330.129 0.009
AA AA-BG0.033 0.0110.063 -0.009
1.9 COEF.VAR.' 99.99 *
ASS 1O12 OJS37f-/W (.*4<t>) ^fX-ti-c.
1 O 1 2 (CONTINUED)AA AA-BC
PEAK HEIGHT (ABSORBANCE) 0.609 0.582PEAK AREA (ABS-SECONDS) 0.369 0.300
44.7
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
44.9
MEAN' 44.3 STD.DEV.'
AS 1O13 $Zfc 30J-0
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
-0.3
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
-1. 1
MEAN" -0.7 STD.DEV."
AS 1 O 1 •* Q He. (jrm
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
20.3
PEAK HEIGHT i ABSORBANCE)PEAK AREA (ABS-SECONDS)
20.6
MEAN- 20.3 STD.DEV.-
MEAN- 20.3 STD.DEV.-
---.- E-02» ELECTRONIC*»•••••**••••«••••••«*•«•••••»•••»«
AA AA-BC0.5S2 0.5630.365 0.301
O.I COEF.VAR.' 0.18 t
H-IfoA A AA-BC
0.096 0.0080.059 -0.009
A A AA-BC0.028 0.0060.052 -0.015
0.6 COEF.VAR.- 85.69 t.
<SP£* C ie lOOY. .-CO.A A AA-BG
0.325 0.3010.191 0.132
A A AA-BG0.333 0.3100.196 0.134
0.2 COEF.VAR.' 1.08 t
29.0 COEF.VAR.- 99.99 %
RANGE OF INSTRUMENT EXCEEDED
BG '0.2SO0.397
BC0,2720.335
BC0,2740,391
BG0,0700, 120
BC0.0300.072
BG0.0270.069
BC0.0260.064
BG0. 1140.078
BC0.0240.066
BG0.0260.059
BG0.0260.062
. •
AS 10 IS 7 7 I 10 5"*? -o I I'.AAa Q \ \ \ .1 Afc-Bfc * BG
PEAK HEIGHT (ABSOR1ANCE) 0.7lQr\ » U 0.623 0.179PEAK AREA (ABS-SECONDS) 0.762 0.308 0.234 i
PEAK HEI3HT ( ABSORB/5(«E •"•"' -^ 'PEAK AREA ( ABS-SECOJTCS )
17,3
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
17.3
MEAN" 17.4 STD. DEV. » 0
AS 1 02 1 ~f)j
1 O2 1 (CONTINUED)
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
0.3
PEAK HEIGHT iABSORBANCE)PEAK AREA (ABS-SECONDS)
-0.2
MEAN. 0.3 STD.DEV.' 0
AS 1 O2 1 —OS.
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
2.6
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
3. 1
MEAN" 2.3 STD.DEV.. 0
— O A - *
AS 1022
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
3.3
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
3.8
MEAN- 3.3 STD.DEV.- 0
AS 1 023 QjJ &.
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
3.4
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
2.3
MEAN* 2.3 STD.DEV.. 0
AS 1023 Q^J &-L
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
2.2
PEAK HEIGHT (ABSORBANCE) " >>PEAK AREA (ASS- SECONDS)
AA0. 2760. |30
AA0,2310. 192
.2 COEF.VAR
i : too
AA0.0350.069
AA0.0310.053
.7 . COEF.VAR
AA0.3351.057
AA0.3421. 149
.4 COEF.VAR
AA0.3551.234
AA0.3701.235
,1 COEF.VAR
Z*AA
0. 1710.307
AA0. 1080.222
.8 COEF.VAR
AA0.0830. 173
Io8S2380. 149
0. I 1 l
AA-BG0,2490, 1 13
,. 1.14
AA-BC0-010-0.002
AA-BC0.011-0.009
.' 99.99
AA-BC0,0230.010
AA-BG0.0260.014
.- 13.17
AA-BC0.0290.019
AA-BC0.0320.018
. - 1 . 37
AA-BG0.0280.016
AA-BC0.0250.008
.. 27.99
AA-BC0.0220.008
o.ota0.004
- 0 . 0 350. 078
BG0.0330.079
X
BC0.0230.071
BC0.0300.074
X
BG0.3401.047
BC0.3471.133
X
BGC.3621.213
BG0.3701.267
X
BG0. 1480.291
BG0.0940.214
X
BC0.071 •0.167
0.0360. 141
;
1 PEAK AREA (ABS-SECON^^ *—'
39.3
MEAN' 57.2 STD.DEV.'
MEAN- 57,2 STD.DEV.'
---.- E-02: ELECTRONIC
AS 1 030 ?7« OS'f
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
5.0
AS 1 O3O -OS"
PEAK HEIGHT (ABSORBANCE)PEAK APEA (ABS-SECONDS)
9.2
AS 1 O3O - 0 S
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
32.4
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
41 .2
3.3331 . 196
3.3
30.3
RANGE OF
- OS /AA
0. 1360.302
t : zxaAA
0.2200.259
I - toAA
0,3490 . 773
AA0.6300.831
0.4080.404
COEF.VAR.. 6.36 x
COEF.VAR,* 99.99 X
INSTRUMENT EXCEEDED.
• / O OAA-BC0.0430.027
AA-BC0.1310.036
AA-BC0,4390.215
AA-BG0.5270 . 276
0 . 346 10.792 ^
BC0, 1660.275
BC0.0910.214
BC0 . 3740,550 1
BG0.2160.553
MEAN' 36.3 STD.DEV.- 6.2 COEF.VAR.' 16.97 X
AS\ 1 O3 1
PEAK HEI^MT (ABSORBANCE)PEAK AREA TAM-SECONDS)
50.3 \
AS 1 O3O -0<3
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
23.6
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
23.1
MEAN- 25.9 STD.DEV..*****#»»**»***»»» ***************AS 1031 -0,5
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
42. 1
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
44.6
AA0.8750.909
/- 6AA
0.5310.639
AA0.4570.397
3.9**********»<a* •*-*
AA0.7620.715
AA0.6760.725
AA-BG0 . 7700.342
AA-BC0.3990. 189
AA-BC0.3540. 151
COEF.VAR.. 13. 16 X>***»***»****»*»***»*»<>-4. c s) 6 f %
AA-BC0.6570.282
AA-BC0.5780.299
BC0.3660.567
BC0. 1900.450
BC0 . 2720.446
***************
BG0.2430.433
BC0.2320.425
MEAN- 43.3 STD.DEV.- 1.8 COEF.VAR.- 4.22 X»••»»••*»»••••*»**»»«»»»•»*»»••»»*••••«••••»•»»*•»*•••*••*»**«•••**»*»»»*»«*»*«AS 1032 -OS / '• 2-W
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.195 0.112 0.085PEAK AREA (ABS-SECONDS) 0.266 0.048 0.216
i .....M........................................................................{ AA AA-BC BCJ PEAK HEIGHT (ABSORBANCE) 0.182 0.112 0.076
PEAK AREA (ABS-SECONDS) 0.233 0.046 0.137
( 7.8
MEAN- 8.0 STD.DEV.- 0.2 COEF.VAR.- 2.64 X******»********************»*******»******f»***********f ******************AS 1033 -OS &* ~f* lt-SJ ?•?/-*-<-
AA AA-BG BCPEAK HEIGHT (ABSORBANCE) 0.50S 0.433 0.074PEAK AREA (ABS-SECONDS) , „ 0~3«J n n 0.210 0.173
31.6
AA AA-BC BG
_ 35.3 STD/fTS?-. O>£> /-.g.9 COEF.VAR.. 99.99 * .,t«*»«»*»** ******»**|P'** *•*»*»»«»»«»«»**»»»«*»«»»»«•»«*»•••«.»»•»••»«»«••»»••••» I----- E-02t ELECTRONIC RANGE OF INSTRUMENT EXCEEDED.
»»»#»«»»*»»»»»*»*»*»*»»*»**»«*»*»«*«»*»•«»**»»«*»»«»»»»»»*»»»»»«*»»»*»*»*»»««»»» |AS 2OO3 -O 6 c: 2.O
A A AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.608 0,563 0.058PEAK AREA (ABS-SECONDS) 0.473 0.330 0.143
49. 1
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) O.SI3 0.574 0.046PEAK AREA (ABS-SECONDS) 0.462 0.327 0.133
48.7
MEAN- 48.9 STD.DEV.' 0,3 COEF.VAR.. 0.60 X**»********************************»***_************************** ********** *****AS ZOO-4 -& (, Qifr' djULf I •' Z-°
^AA AA-BG BGPEAK HEIGHT (ABSORBANCE) 0.711 0.666 0.043PEAK AREA (ABS-SECONDS) 0.527 0.401 0.123
39.5
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
59.8
MEAN" 59.6 STD.DEV.'
AS 2OOS —Od>
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
AA0.7120 . 527
0.3
CLu dii.AA
0.6230.440
AA0.6190.441
AA-BC0.6710.404
COEF.VAR.. 0.43 X.O 1 '. £, O
AA-BC0.5830.322
AA-BC0.5800.323
BC0.0470. 123
BG0.0440. US
BC0.0420. 118
MEAN- 48.0 STD.DEV.. 0.2 COEF.VAR.. 0.38 Xt*******************************************************************************AS 2006 8111 O-Tf -0<+ «-\, /-'*fO
AA OM-f AA-BG BG: PEAK HEIGHT IABSORBANCE) 0.289 0.237 0.036
PEAK AREA (ABS-SECONDS) 0.208 0.114 0.094
: 17.7i ................................................................................
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.280 0.246 0.035PEAK AREA IABS-SECONDS) 0.201 0.110 0.091
17.1
MEAN' 17.4 STD.DEV.. 0.4 COEF.VAR.- 2.46 X********************************************************************************AS 2006 Tl4/ I •' V°
SI ~l" •" AA AA-BG BCPEAK HEIGHT (ABSORBANCE) <U<<* " Q.301 0.269 0.036PEAK AREA (ABS-SECONDS) 0.204 0.113 0.092
17.3
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
ts.oMEAN- 16.2 STD.DEV.. 1
AS 2OO6 -t3< C.
PEAK HEIGHT (ABSORBANCE) &"-**'•?PEAK AREA (ABS -SECONDS )
17. 1
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
17.2
AA0.2230.207
.8
AA0.3060. 197
AA0.3020.199
AA-BG0.2010.095
COEF.VAR.- 11.00 X
AA-BC0.2730.110
AA-BC0.2720.111
BG0.1530. 112
BG0.0350.087
BG0.0340.088
MEAN- 17.1 STD.DEV.. 0.1 COEF.VAR,- 0.42 Xt*******************************************************************************AS 2OO?" QMt. 304-0 II-IJ
AA AA-BC BCPEAK HEIGHT (ABSORBANCE)c n { flOO?!**3!2 0.014 0.027PEAK AREA (ABS-SECONDS) H fl I U U £ H455 -0.003 0.077
0.7
1 3.6
MEAN" 3.9 STD.DEV. «
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
27.3
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
28. 1
MEAN" 27.7
AS 2O 1 3
STD.DEV.'
-0 A
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
1 .4
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
0.7
MEAN- 1 . 1 STD.DEV..
0.4
AA0.3540.375
AA0.3380. 330
0.5
AA0. 1220. 179
AA0. 1230. 175
0.5
COEF.VAR.' U. 19 X
AA-BG0.2990. 180
AA-BC0.2890. 136
COEF.VAR.' 1.92 X
AA-BC0.0230.002
AA-BC0,020-0.003
COEF.VAR.. 49.03 X
BC 10.1120.193 '
BC0. 1170, 195
BC0. 1250. 176
BC0. 1270. 178
2O 1 -4 (CONTINUED)
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
1.5
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
1.3
MEAN- 1,4 STD.DEV." 0********* ******** *************»*»*»uAS 201S -0,3 SJ.
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
1.2
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
0.6
MEAN- 0.9 STD.DEV." 0t************************************
AA0. 1010. 166
AA0. 1090. 173
.2**#»«»)
" AA0. 1120. 171
AA0. 1100. 157
.4*•»»**<
AA-BC0.0230.003
AA-BG0.0240.001
COEF.VAR.. 11.39 X»****»******»*»»**»»**<L-*y
AA-BG0.0190.001
AA-BG0.025-0.003
COEF.VAR.. 48.94 X»»*•**«*•**»»**»*»»**»'
BG0. 1040.163
BG0. 1070. 171
***************
BG0. 1140. 171
BC0. 1150. 170
AS 2O 1 6 — O<-fAA AA-BC BC
PEAK HEIGHT (ABSORBANCE) 0.106 0.016 0.106PEAK AREA (ABS-SECONDS) 0.182 -0.003 0.185
0.6
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
0.8
MEAN- 0.7 STD.DEV..
AS 20 i ;*• -oPEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
0.9
PEAK HEIGHT (ABSORBANCE) » rPEAK AREA (ABS-SECONDS) £| \
0.9 . ,
'nutlr 0.9 STD. DEV."
AA0. 1180. 189
0. 1
SAA
0. 1330.200
UOSiS0.0
AA-BC0.014-0.002
COEF.VAR.. 18.57 X
AA-BG0.013-0.001
4. 0.0191 -o.ooi
COEF.VAR.. 1.2B *
BC0.1230. 191
BG0. 1280.201
BC0 * i 3s0 « 203
_..„.-.--— .....§r.. ......PEAK HEIGHT (ABSORBANCE)PEAK AREA I ABS-SECONDS)
46.4
MEAN' 46,1 STD.DEV.'»*»»*»»*»»»»»*»**»»»**»**»»*«»*<AS 2O23 QJJe.
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
-0.4
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
0.2
MEAN. -0.1 STD.DEV.'
AS 2O2-<4. BJLk-
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
19.3
PEAK HEIGHT (ABSORBANCE)PEAK AREA I ABS-SECONDS)
20.4
MEAN" 20.1 STD.DEV..
AS 2O2S ^ t f f
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
44.9
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
49.5
AA0.6600.388
0.3»»*»»«»*«*»»(3 QSO F
AA0.0230.064
AA0.0270.064
0.4
Ccwi S fitAA
0.2580.202
AA0.2540.204
0.4
AA0.7100.932
AA0.7611.013
AA-BC0.5400.31 1
COEF.VAR.' 0.63t******************
// -17AA-BC0.010-0.010
AA-BG0.008-0.006
COEF.VAR,. 99.99
C -Z.-0 i 1 oo /.AA-BC0.2370. 129
AA-BG0.2320. 133
COEF.VAR." 2.04
k*a AA-BG0.2720.301
AA-BG0.3120.333
BC0.0230.077
X******************
BG0.0260.074
BC0.0230.070
X
BG0.0290.073
BC0,0260.071
X
BG0.4600.631
BC0.4760.681
MEAN. 47.2 STD.DEV.. 3.2 COEF.VAR.' 6.80 Xt******************************************************************************.AS 2O26 f_o 711 055 -Of / ' 10
2O26 (CONTINUED)
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
S.?
AS 2O26 — 0 "> '
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
17.3
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
19.4
MEAN. 18.4 STD.DEV,. 1
AA0,2090.238
AA0.3070.332
AA0.3540.363
.5*******
AA-BC0.0960.053
AA-BG0. 1650. Ill
AA-BC0.1900. 126
COEF.VAR.. 8.19 X**»**•**•***••*•*.»»
BC0. 1200.184
BG0. 1520.221
BG0.1630.237
AS 202 " —09 £2 < «-T "*:AA AA-BC BG
PEAK HEIGHT (ABSORBANCE) 0.542 0.393 0.160PEAK AREA (ABS-SECONDS) 0.537 0.304 0.234
43.2
AA AA-BG BCPEAK HEIGHT (ABSORBANCE) 0.530 0.407 0.151PEAK AREA (ABS-SECONDS) 0.534 0.303 0.231
43.2
MEAN- 43.2*•»•»»•»*•»*******•AS 20!
STD.DEV.. Q D «.*} O^QEF.VAR.. 0.12 X•••••••••»»**%i»*»«t*|j>*fc5»j*f»«5S»**»**»*»»»»**«—yo f • " ~>
1.8 STD . Dlfer . 7.6 COEF.VAR.. 90.19 X.•***««*********»«»***»***fi*»«****»>***********»**»***. tj, ***********************
- Cfe>J ¥4 -AS 2033 cjsa-rr-i'-t cv&; <?4-,AA AA-BG BG
PEAK HEIGHT (ABSORBANCE) 0.492 0.473 0.028PEAK AREA (ABS-SECONDS) " 0.369 0.290 0.080
43.2
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.484 0.463 0.023PEAK AREA (ABS-SECONDS) 0.374 0.299 0,075
44.5
MEAN" 43.9 STD.DEV.. 0.9 COEF.VAR.' 2.05 X»»»*»»*»****»»**«*»••»•**»*»»**»»**»**»*»**»*****»***»»«*»»**»**»«*•*»»*•*»»»*»»AS 203*4 —(3 I ' J.
AA AA-BG BCPEAK HEIGHT (ABSORBANCE) 0.608 0.405 0.209PEAK AREA (ABS-SECONDS) 0.631 0.342 0.289
50.9
AA AA-BC BGPEAK HEIGHT (ABSORBANCE) 0.652 0.431 0,232PEAK AREA (ABS-SECONDS) 0.638 0.363 0.319
54.7
MEAN" 52.8 STD.DEV.. 2.7 COEF.VAR.. 5.12 Xt*******************************************************************************AS 2O3S —/ V / •' A
A A AA-BG BCPEAK HEIGHT (ABSORBANCE) 0.578 0.336 0.244PEAK AREA (ABS-SECONDS) 0.607 0.273 0.332
41. 1
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.394 0.348 0.246PEAK AREA (ABS-SECONDS) 0.617 0.279 0.338
41.S
MEAN' 41.4 STD.DEV.- 0.3 COEF.VAR.. 0.80 Xt*******************************************************************************AS 3OO3 —/S /•'«•?
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.720 0.472 0.248PEAK AREA (ABS-SECONDS) 0.778 0.413 0.363
61. 1
AA AA-BC BGPEAK HEIGHT (ABSORBANCE) 0.706 0.471 0.247PEAK AREA (ABS-SECONDS) 0.756 0.395 0.361
58.6
MEAN' 59.9 STD.DEV.. 1.8 COEF.VAR.. 3.04 Xt*******************************************************************************AS 3OO-4 — I (a f ' A
._. ,_ AA AA-BC BC3%f,' .~ it PEAK HEIGHT (ABSORBANCE) 0.797 0.514 0.293
PEAK AREA (ABS-SECONDS) 0.847 0.397 0.450
58.8
A A AA-BG BGPEAK HEIGHT (ABSORBANCE) 0.846 0.360 0.299PEAK AREA (ABS-SECONDS) 0.362 0.414 0,449
61.2
MEAN- 60.0 STD.DEV." 1.8 COEF.VAR." 2.92 Xt*******************************************************************************AS 300S ~/-7 t:+tA
AA AA-BC BGPEAK HEIGHT (ABSORBANCE) 0.816 0.539 0.290PEAK AREA (ABS-SECONDS) 0.827 0.420 0.407
62.2
AA AA-BC BGPEAK HEIGHT (ABSORBANCE) 0.801 0.527 0.281PEAK AREA (ABS-SECONDS) 0.813 0.413 0.403
61.5
MEAN* 61.9 STD.DEV." O.S COEF.VAR." 0.73 Xt*******************************************************************************AS 3003 ~ / "7 /•' V
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.430 «. !.<!}• 286 0.202PEAK AREA (ABS-SECONDS) B O4$lf\ .1 L H &203 0.289
30.6
._-?:?.......-...~MEAN" 0.3 STD.DEV.' 0.7 COEF.VAR.. 33.96 Xt*******************************************************************************AS 3O 1 O C*i S 3 "7 J*- / tf Ct/fe/' T ' .-**-<_
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.537 0.564 0.028PEAK AREA (ABS-SECONDS) Q.364 0.285 0.079
42.5
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
42.0
MEAN" 42.3 STD.DEV.'
AS 3011 SJUc. 3oSaPEAK HEIGHT (ABSORBANCE)PEAK AREA 'ABS-SECONDS)
0,3
PEAK HEIGHT • ABSORBANCE)PEAK AREA (ABS-SECONDS)
-1.2
MEAN" -0,4 STD.DEV.'
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
18.7
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
19.0
MEAN" 13.9 STD.DEV..*»»»•**«*»»»»*»»»*»»*«»»**»•*»*«»*
AA0.5720.351
0.4 COEF,
1= tl-thAA
0.02S0.063
AA0.0230.061
t.O COEF.
sric cz.o;AA
0.2400.194
AA0.2420. 197
0.2 COEF.***************
AA-BG0.5300.231
VAR.= 0.96 X
AA-BC0.009-0.003
AA-BG0.006-0.015
VAR." 99.99 %
<?S'*V'. •"-.AA-BC0.2190.121
AA-BG0.2220. 123
VAR.. 1.22 %• **»*»»*»*****»*»<
BC0.0230.080
BC0.0250,073
BG0.0250.076
BG0.0260.073
BC0.0260.074
»***•****»»•*»•
3O13 (CONTINUED)AA AA-BG BG
PEAK HEIGHT (ABSORBANCE) 0.902 0.392 0.529PEAK AREA (ABS-SECONDS) 1.114 0.398 0.716
59.0
AA AA-BG BGPEAK HEIGHT (ABSORBANCE) 0.956 0.422 0.544PEAK AREA (ABS-SECONDS) 1.195 0.434 0.761
V, i 64.2
MEAN" 61.6 STD.DEV." 3.7 COEF.VAR.. 5.95 X«»*»•»•«*»»«»«•»••»*»****«»»**•»»*»«**»**«»»»•»**»»*»»»*»»•»**«»«»»»•»***»•»»»»»AS 301-* GJSaTf-'V OH/ fty.^u.
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.590 0.533 0.076PEAK AREA (ABS-SECONDS) 0.454 0.316 0.137
47.1
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.578 0.548 0.036PEAK AREA (ABS-SECONDS) 0.375 0.288 0.088
42.9
MEAN" 45.0 STD.DEV.- 2.9 COEF.VAR.. 6.53 Xt*******************************************************************************MEAN- 45.0 STD.DEV." 63.7 COEF.VAR." 99.99 Xt*******************************************************************************
---.- E-02: ELECTRONIC RANGE OF INSTRUMENT EXCEEDED.»•»**«•«*»»»««»«»*•»»»*»»»»»•»•»»»»**»»•»*»»*•»«»*»»»*»*»*•»»»***•»»**»»»***»•»»MEAN- 45.0 STD.DEV.. 63.7 COEF.VAR.. 99.99 X
-•-.- E-02i ELECTRONIC RANGE OF INSTRUMENT EXCEEDED.t**************************************************************************.*****AS 301S f7 lto*1~ o I 1-*
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 1.110 0.742 —0.37,2 n ^ i jPEAK AREA (ABS-SECONDS) 1.032 0.523 fl R01S$3 O <£ H
l*? ' 77. t
32.4
MEAN" 32.6 STD.DEV.. 0.4 COEF.VAR." 1.22 Xt*******************************************************************************AS 3O2O ~rSi ' ' *r
AA AA-BC BGPEAK HEIGHT (ABSORBANCE) 0.666 0.388 0.287PEAK AREA (ABS-SECONDS) 0.591 0.235 0.356
35.3
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.640 0.361 0.285PEAK AREA (ABS-SECONDS) 0.602 0.235 0,366
35.3
MEAN" 35.3 STD.DEV.' 0.1 COEF.VAR,' 0,15 Xt*******************************************************************************AS 3O2 1 —Oi <2~i "7*1* C £SV (I y. 7. -"*-
AA AA-BG BCPEAK HEIGHT (ABSORBANCE) 0.901 0,643 0.279PEAK AREA (ABS-SECONDS) 0.733 0.423 0.360
62.6
AA AA-BG BGPEAK HEIGHT (ABSORBANCE) 0.949 0.682 0.289PEAK AREA (ABS-SECONDSI 0.795 0.433 0.362
64. 1
MEAN' 63.4 STD.DEV.. 1.1 COEF.VAR.. 1.69 X********************************************************************************
63.4 E-25: READING GREATER THAN HIGHEST STANDARD.»»*****»*******•***********«*******»***»»»*»**»»»«*»»*»***»**»****»»**»*********AS 3O22 -Ol t '• M
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.926 0.372 0.357PEAK AREA (ABS-SECONDS) 0.864 0.373 0.486
36. 1
AA AA-BC BGPEAK HEIGHT (ABSORBANCE) 0.980 0.611 0.370PEAK AREA (ABS-SECONDS) 0.903 0.399 0.307
»»»*»•**»»***».»»*»»**»********»»»»*»»**»*•*»****»»»»*»*
..........................................................| MEAN. 57.6 STD. DEV. - 2.1 COEF.VAR.. 3.63 X, **********»*******»******»»»*»•**»»***».»»*»»**»********»
AS 3023 -0<+ CUlg, dLu /.'</
3O23 (CONTINUED)A A AA-BC BG
PEAK HEIGHT (ABSORBANCE) 1.024 0.645 0.388PEAK AREA (ABS-SECONDS) 0.902 0.399 0.504
59. 1
AA AA-BC BGPEAK HEIGHT (ABSORBANCE) 1.083 0.692 0.398PEAK AREA (ABS-SECONDS) 0,916 0.410 0.506
60.7
MEAN" 59.9 STD.DEV.. 1.1 COEF.VAR.. 1.90 X*****************AS 3O2-4**»•»**••»••*****•***»*»**»•»»«•***>**•***»**»*»***»»*»»»**»*******»»»*»»*******
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.141 0.051 0.099PEAK AREA (ABS-SECONDS) 0.187 0.028 0.139
S.2
A A AA-BG BGPEAK HEIGHT (ABSORBANCE) 0,038 0.009 0.040PEAK AREA (ABS-SECONDS) 0.084 -0.006 0.090
0.2
MEAN" 2.7 STD.DEV." 3.3 COEF.VAR.. 99.99 X«»»»»»»*•**»»*»*»»»»«»«*»»»»*«**.»*»»*»»»»»»»»»*»»»*•*»•»»*»»»*»*»»»»»**»*»»•»»»«AS 3O2-4 CL*J( JbJUk.
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.025 0.008 0.026PEAK AREA (ABS-SECONDS) 0.067 -0.003 0.071
0.4
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.02S 0.008 , r" 0.028PEAK AREA (AM-SECONDS) 0.067 _ n \-fl\tftf? ilH 0.073
-•.2
--. - .,w ^ ri - . u". aoO 0.297 0.263PEAK AREA (ABS-SECONDSf_/ 0.543 0.137 • 0.336 ——.- ^ _„
^ »!*«- A--?- ~ ^
28.3 ' " '" -t '
MEAN- 29.9 STD.DEV.. 2.3 COEF.VAR.. 7.84 X********************************************************************************AS 3 O 2 9 ~~O6 c2*-i CttjJt I '. fa
AA AA-BG BGPEAK HEIGHT (ABSORBANCE) 0.538 0.288 0.253PEAK AREA (ABS-SECONDS) 0.333 0.182 0.352
27.5
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.344 0.234 0.263PEAK AREA (ABS-SECONDS) 0.534 0.177 0.336
26,9
MEAN" 27.2 STD.DEV,. 0.4 COEF.VAR.' 1.58 X********************************************************************************AS 3O30 <jjS37f-C~f C *+<o) fj /• •"•-<-
AA AA-BG BGPEAK HEIGHT (ABSORBANCE) 0.603 0.332 0.063PEAK AREA (ABS-SECONDS) 0.444 0.304 0.139
43.4
A A AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.536 0.330 0.031PEAK AREA (ABS-SECONDS) 0.364 0,277 0.037
41.4
MEAN" 43.4 STD.DEV." 2.3 COEF.VAR.. 6.31 X************************************ ********************************************AS 3O31 -0*7 /-*f
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.337 0.238 0.234PEAK AREA (ABS-SECONDS) 0.519 0.178 0.341
27.0
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.613 0.338 0.230PEAK AREA (ABS-SECONDS) 0.383 0.211 0.372
31.8
MEAN- 29.4 STD.DEV.' 3.4 COEF.VAR.. 11.62 X********************************************************************************AS 3O32
-O f I .' <•/
3O32 (CONTINUED)A A AA-BC BC
PEAK HEIGHT (ABSORBANCE) 0.478 0.233 0.225PEAK AREA (ABS-SECONDS) 0.463 0.160 0.305
24.4
A A AA-BG BCPEAK HEIGHT (ABSORBANCE) 0.431 0.238 0.217PEAK AREA (ABS-SECONDS) 0.430 0.132 0.293
23.2
MEAN- 23.8 STD.DEV.- 0.3 COEF.VAR.. 3.49 X****»***********************************'AS 3033 —0? /: </
AA AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.369 0.316 0.238PEAK AREA (ABS-SECONDS) 0.336 0.201 0.339
30.3
A A AA-BC BCPEAK HEIGHT (ABSORBANCE) 0.601 0.334 0.268PEAK AREA (ABS-SECONDS) O.SSO 0.210 0.340
31.7
MEAN- 31.0 STD.DEV.. 0.9 COEF.VAR.. 3.06 Xt*******************************************************************************AS 3O3-» -TO '•' '-r
AA AA-BC BGPEAK HEIGHT (ABSORBANCE) 0.448 0.223 0.230 fPEAK AREA (ABS-SECONDS) 0.334 0.163 0.391 O 9 U U
HEIGHT (ABSORBANCE) 0.364 0.178 0.224WEAK AREA (ABS-SECONDS) 0.484 0.108 0.376
if.*
MEAN
AS
PEAKPEAK
PEAKPEAK
MEAN
.------- —— ------------ -y13.9 STD.. DEV. « ^
303S ~l i 1.
HEIGHT (ABSORBANCE)AREA
46.3
(ABS-SECONDS)
HEIGHT (ABSORBANCE)AREA
30.3
.
(ABS-SECONDS)
48.6 STD.DEV.'
0.7
•300
00
2.5
AA,767.784
AA.310.335
COEF.VAR. .
AA0,0.
AA0.0.
COEF.VAR.'
3.57
-BC446314
-BG473339
5. 14
%
0.0.
0.0.
X
BC325470
BC337496
AS -4003 -13. i : 3AA AA-BC BC
PEAK HEIGHT (ABSORBANCE) 0.525 0.245 0.289PEAK AREA (ABS-SECONDS) 0.692 0.172 0.519
26. 1
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
22.2
MEAN" 24.2 STD.DEV..
AS -4OO-4 — U
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
18.8
AS -4OO-** - 13
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
31.3
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
31.6
AA0.474O.S22
2.3
( : -fAA
0.3700.521
AA0.3320.718
AA0.5530.713
AA-BC0.2190. 143
COEF.VAR.. 11.59 X
AA-BG0. 1680. 121
AA-BC0.2670.203
AA-BG0.2830.210
BG0.2530.477
BG0.207-0.400
BC0.2840.310
BC0.2740.508
MEAN- 31.4 STD.DEV.- 0.2 COEF.VAR.. 0.56 Xf*******************************************************************************AS -4OOS CLAJI &-Uc.
AA AA-BC BGPEAK HEIGHT (ABSORBANCE) 0.052 0.014 0.044PEAK AREA (ABS-SECONDS) 0.102 -0.006 0.103
0.2
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
0.6
MEAN" 0.4 STD.DEV.-t*******************************AS -4OO6 CJJ3
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
42.2
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
42.7
MEAN- 42.4 STD.DEV..********************************
AA0.0270.077
0.2 COEF.VAR.*********************
AA0.5480.364
AA0.5780.362
0.4 COEF.VAR.»»»»•»•*»»»«»*•»»•»»«
AA-BC0.0070.004
« 55.10 X.**********•*<
AA-BC0.3290.283
AA-BC0.5600.286
« 0.83 X••»*•**•*•*••<
BC0.0300.030
>**»**»•******»
BG0.0280.082
BG0.0270.076
»•••••*•»»**»**
MERCURY DATA
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r1 PEAK HEIGHT (ABSORBANCE)fj PEAK AREA ! ABS-SECONDS)
j READ! -0.007j .....................................
PEAK HEIGHT (ABSORBANCE), PEAK AREA (ABS-SECONDS)
I READ) 0.009
MEAN" 0.001 STD.DEV.* 0.0
0.000 AUTOZERO
sePEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
READ» 0.065
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
READ: 0.061
MEAN" 0.063 STD. DEV. = 0.0
20.0 STANDARD 1
SE
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
i
*
READ: 39.3
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
READ! 33.5
MEAN" 39.0 STD.DEV.. 0*»*»****«*>***********»*«*****>*«****
39.0E-50i READING GREATER THAN
»»«•••«*»«*»»»«»»•«»*»*•»•*•»*«»»***»39.8 STANDARD 2
i************************************SE
PEAK HEIGHT (ABSORBANCE)i PEAK AREA (ABS-SECONDS)
I READi 39.8
(CONTINUED)
PEAK HEIGHT (ABSORBANCE)1 PEAK AREA (ABS-SECONDS)
1 READi 60.6
AA0.1010. 163
AAO.C900. 144
12 COEF.VAP.
AA0 . 2070.213
AA0.2030.203
02 COEF.VAR.
AA0.3120.280
AA0.2980.266
.7 COEF.VAR.****************
HIGHEST STANDARD•*****»»»*»»>**»
•*»»**•*»**»»**»
AA0.3900.347
AA0.4090.343
ZAA0.0780.040
ZAA0.0730.056
» 99.39 X
ZAA0. 1720. 113
ZAA0. 1600 . I 09
« 3.97 X
ZAA0,2570. 172
@ZAA0.2440. 169
' 1 . 83 X***********
»**»»**»*«*
*«»*»*»*»**
ZAA0.3210.233
@
ZAA0.3320.235
BG0.0880.123
BG0.078o.oes
SOO.C640. 100
EG0.0380.094
BC0.0670.107
BC0.0580.097
*»»***»»*»****»*
****»**•**<*»***
»**»»»*»»**»»»**
BG0.0770.113
BC0.0800.103
MEAN- 60.2 STD.DEV.. 0.6 COEF.VAR.. 0.99 X**»*•*»•«***«***«»****»*«********t**********************************************
60.2E-SO> READING GREATER THAN HIGHEST STANDARD
»•««•»«*•*»»»»*»»»••*»*»»*«*»*»»»««»»*««*»«»»»«»»*»«»»«»••*»»»«•»•»»**«*••««»*•»
10.3256
PEAK HEIGHT (ABSOPBANCE! 0.350PEAK AREA <ABS-3ECONCS> C , 353
PEADs -0.011
AA ZAA 50PEAK HEtCHT 'ABSORBANCE) 0.112 C.236 C.023PEAK AREA ( ABS-SECCNDS ) 0.095 7.:-l2 O.C3?
READ: 0,002
MEAN* -0.004 STD.CEV.. 0.510 "EF.ViR.= 99.99 t#***»*****#**»***»»#*»********### **************** *******************************
0.000 AUTCrEPO
•IA ;AA scPEAK HEIGHT 'ABSOPBANCE) 0.244 0.239 3,:49PEAK AREA (ABS-SECONDS) 0.169 0.103 0.061
READ: 0.0-3
AA ZAA BCPEAK HEIGHT 'ABSCPEANCE) 0.243 0.194 0.032PEAK AREA ' ABS-SECONDS > 0.155 0.102 0.064
PEAD i 0.067
MEAN" 0.070 STD.DEV.. O.C04 COEF.VAP.s 5,65 X******************************************* **»»4*»**»»*******»*****«»****»**»»*«
20.0 STANDARD 1t*******************************************************************************
AA ZAA BCPEAK HEIGHT (ABSOPBANCE) 0.393 0.325 0.075PEAK AREA (ABS-SECONDS) 0,248 0.174 • 0.075
•"*
, READ: 39.6
i AA :AA BCPEAK HEIGHT (ABSORBANCE) 0.373 0.307 0.071
' PEAK AREA (ABS-SECONDS) 0.244 0.164 0-080
J READ) 36-9
MEAN- 38.3 ST3.DEV.- 1.9 COEF.VAR.. 4.92 St*******************************************************************************
38.3E-50! READING GREATER THAN HIGHEST STANDARD
********************************************************************************39.6 STANDARD 2
****************************************************************** ******n**mtSE
AA ZAA BCPEAK HEIGHT (ABSORBANCE) 0.490 0.405 0.090PEAK AREA (ABS-SECCN3S) 0.303 0.219 0.085
READi 74.3
(CONTINUED)AA ZAA BC
PEAK HEIGHT t ABSORB AftICE) 0.47T 0.39* 0>333PEAK AflEft (ABS-SECONBS) 0.310 0.218 C.SSI
READ: 34.2
MEAN- 54.3 STD.DEV.. 0.1 COEF.VAR.. 0.14 *t**********************************•»*•****«»»»**»*«*»***»***•***»**»***««*****«
54.3E-30: READING GREATER THAN HIGHEST STANDARD
»**»»*»»»«»»»*«»»»*»•«»*»«»»•*•»»«»**»*•»«*»»«»»»*»»»»»*»«»»•«»»»*»»«*»»•«»»**»*
\Q3257
1 PEAK HEI3HT (ABSORBANC_KTJ PEAK AREA 'ABS-SECONC^'
| READ: 23,0
' MEAN- 20.2 STD.DEV
SE 1 O 1 O
3C>5&
P£ftlc -'EIGHT •' ABSOPEAPw-E 'PEAK APEA~iABS-3E:2N3S!
READ: -.4
PEAK iJEIGHT 'ABSOPBANCE'PEAK APEA ( ABS-SEC3NDS'
PEAD: 5.4
MEAN= s.9 STD.DEV
3WOSSE 1O11
PEAK HEIGHT (ABSORBANCE!PEAK AREA (ABS-SECONDS)
READ: 47.7
PEAK HEIGHT (ABSCRBANCE)• PEAK AREA ( ABS-SECONDS I
READ! 46.0
MEAN- 46.9 3TZ.DEV
SE 1 O 1 2 _/V
PEAK HEIGHT (ABSORBANCE!PEAK APEA (ASS-SECONDS'
PEAK HEIGHT ' ABSORBANCE)PEAK AREA ( ABS-SECONDS 1
READ! 42.2
j MEAN- 44.4 STO . DEV
|sE ioi3 -Qdt/i PEAK HEIGHT CABSOPBAVCES' PEAK AREA «ABS-SECOiyES'
; PEAK HEIGHT (ABSORBANCE)i PEAK AREA (ABS-SECONDS'
j READ; 53.4
] MEAN- 53.7 S7Z.DEV
| SE ioi-» CQjLhJi.1 PEAK HEIGHT (ABSORBANCE!• PEAK AREA (ABS-SECONDS)
READ: 3.7
5/7 1.323 0.3071 -693 J. 103
. * 3.9 COEF.VAP.- 13.55
i~* ' 3 f • " •* o '2
3.414 j.iss
3.112 0.3940-1 43 0.356
O.T rOEF.vap.. 10.-- »
AA ZAA0.314 0.1380.563 0.187
AA ZAA0.329 0.1310.377 3.132
.. 1.2 CCEF.VAR.= 2.54 t
0 . 330 -3.1-30.503 0.133
AA ZAA0.332 0.2010.339 0.169
.. 3.1 COEF.VAR.. 6.97 1
I *\ S AA ZAA{/,' 2.J 0,379 0.214
0,634 0.20*
.AA ZAA.j.sra o.t550.531 3-221
.. 3.8 COEF.VAR.' S.79 T
&*-£' AA ZAA0.138 0.0960.163 0.047
uora1 , 390
PC
0. =55
rC-0.0493.033
300.2150 • 376
BC0.2110.396
BC0.2050.419
BC0.2280.419
BC0.2340.430
BC•3.247
•C0.0620.116
.AR.1.Q.3!
I PEAK HEIGHT ' ABSORBANCE • PEAK AREA (ABS-SECONDS)
j READ! 5.6
PEAK HEI3HT (ABSOPBANCE)PEAK AREA 1 ABS-SECONDS '
PEAD: 5.0
MEAN- 3.3 3~D. DEV.. 0 .
-O7&SE 1 O 1 9
PEAK HEIGHT (ABSORBANCE'PEAK AREA (ABS-SECONDS)
PEAK HEIGHT 'ABSORBANCE)PEAK AREA (ABS-SECONDS)
READ: 27.8
MEAN- 27.3 STD.DEV.. 0.
SE 1O2O — /O 8 A
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
• PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS!
READi 28.6
MEAN- 28.1 ST3.DEV.. 0.
SE 1021 JJOSC) /6&2/K.PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
READ: 3.8
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS!
., READS 3.3
t<i
•MEAN- 3,6 3T3.EEV.- 0.
SE 1022 /OjM/ jC. ;QjQjLPEAK HEIGHT (ABSOPBANCE)PEAK AREA ( ABS-SECONDS)
READ! 24.8 iif-... ... ..... ... ------------- ---.-.//O,
PEAK HEIGHT (ABSORBANCE)PEAK AREA (ABS-SECONDS)
READ: 22.1
0.271
AA0.2440.271
4 C2EF
•f
AA0.4370.297
AA0.4390. 304
8 COEF
AA0.4700.307
AA0.4320.309
7 COEF
0. 1270. 171
AA0. 1230. 146
2 COEF
<W-<0.2720.233
'/~AMU)LAA
0.2390.226
o. -.540.053
ZAA0. 1300.051
. VAP. = S. 19 *
ZAA•3.3600. 120
jQV&lUjft0.3560.124
.VAR.. 2.90 t
ZAA0 . 3740. 123
'ZAA0.3330. 126
.VAP.. 2.39 "i
) ZAA0.0920.043
ZAA0.0930.346
. VAR . . 6 . 49 I
') ZAA0.2120. 114
k i . ..........U ZAA0.2020. 103
.. — ....._. -TV A J
0. 1960.217
BC0. 1910.220
4<tf 34
BC0. 1330.1-7
BC0. 1620. 131
BC0. 1660. 184
BC0.1290. 183
0.0480. 123
BG0.0400. 100
BC0.0640. 121
BC0.0700.121
C.Q. ..........MEAN- 23.4 STD.DEV.- 1.9 COEF.VA*.t> B.febO*" **»»•«••««»»•»••»«»»•»•»•*»»««*•••*»«*•»»«•»»*«»»«« »«f»V»»»« I************************_K __. « r*. * —* i* „ * f ft —. '
HPEAK HEIGHT (ABSORBANCE)
' PEAK AREA (ABS-SECONDS)
PEAD! 36.3
PEAK HEICHT ! ABSORBANCE iPEAK AREA I ABS-SECONDS1
PEADl -»0.2
MEAN- 33.3 ST3.DEV.*
S E 1 O 2 S _ C^A C.IPEAK HEIGHT (ABSORBANCE1.PEAK ARE* < ABS -SECONDS)
READ: 3.5
PEAK HEIGHT ;AESCREANCE)PEAK AREA (ASS-SECONDS'
READ; 7.3
MEAN. 2-2 STO.TJEV.-
SE 1 029
PEAK HEIGHT (ABSOPBANCE;PEAK AREA (ABS-SECOMDS)
READ: 35. S
PEAK HEIGHT '. ABSORB ANCE!PEAK AREA >. ABS-SECONDS ;
READ: 38.1
MEAN- 36.9 3TC.DEV.-
SE 1O3O _y^4
PEAK HEIGHT (ABSOPBANCE)PEAK AREA (ABS-SECONDS)
READ! 21.7
' PEAK HEIGHT (ABSORBANCE)j PEAK AREA (ABS -SECONDS!
READi 19.7
AA0.4780.517
AA0.4633.410
2.6
' AA0.1-30. 137
AA0. 1~30.1"6
0.5
AA0. r-50 , 267
0?3460. 151
1JjC£l>£qu
073720. 163
COEF.VAR.* S.79 *
ZAA•3 . I 370.062
ZAA
C . CSO
C3EF.VAP.- 3.5-» t.
ZAA0.3120. 148
BC0,2220.363
BC0. 1100.248
BC0.0390. 124
BG0.0600. 115
5C0.0690. 118
l\^f- AlOA(&i<sAA 0 ZAA
0.357 0.3020.2-0 0.136
i.r
AA0.3030.391
AA0.2630.327
COEF.VAR.- 4.65 *.
ZAA0.2170. 104
ZAA0. 1940.098
BC0.0730. 114
BG0. 1230.287
BC0. Ill0.229
MEAN- 20.7 STD.DEV.- 1.4 COEF. VAP. - 7.00 t*•*•*»***•*****«*»»*•»»*•»***»*«**«**»****»*•***»»****•**»*»*»**•»***»•*»***•*»*SE 1O31 —lOAsJj^A\ (Uf*&*nf> AA ZAA BG
• PEAK HEIGHT (ABSCRBANCE) 0.263 0.195 0.110PEAK AREA (ABS-SECONDS) 0.323 0.103 0.222
' READ! 21.5
S PEAK HEIGHT (ABSOPEANCE)' PEAK AREA (ABS -SECONDS:
READ: 20.9
._Ov/...39AA
0.2420.326
..-.-.---..ZAA0. 1840.102
BG0. 1040.224
Ml 103260
i*PEAK WHISHT i ABSORBANCE) 0.446 0.380 074(PEAK AREA I ABS-SECONDS) 0.263 0.195 o!o69
PEAD: 50.1
mEAN* 49.4 37". DEV.«
S E 2 O O ," "7/V/OS"PEAK HEIGHT 'AESCPEANCEJPEAK AREA t ABS-SECONDS)PEAD: 19.4
PEAK HEI3HT 1 ABSOPBANCE'PEAK AREA (ABS-SECONDS!
READ: 14.3
MEAN" 1~. 1 3TS.DEV."
SE 2O OS — /5~/4PEAK HEIGHT (ASSOPBANCE)PEAK AREA ( ABS-SECCNDS)
READ: 13.5
PEAK HEIGHT IABSOREANCE)PEAK AREA (ABS-SECONDS)
READ: 15.3
MEAN- 14.5 3TS.DEV.-
SE 2OO9
PEAK HEIGHT I ABSORB ANCE ( PEAK APEA (ABS-SECONDS)
1. 0
00
30
3.2
00
00
1.4
00
COEF.
AA. z 3r. 23r
AA,23?. 302
COEF.
AA. 194.325
AA.213.331
COEF,
AA.220.407
y'AP.S 2. OS
ZAA0. 1210.097
ZAA0.164 .0.083
VAR.. 13.74
ZAA0. 1340.073
ZAA0. 1350 . 085
. VAR.« 9.77
ZAA0. 1230.071
Y.
BC0. 0940. 190
EC0. 1020.219
r.
BC0, 1050.247
BC0. 1130.246
T.
BG0. 1610.333
READ: 11.3
PEAK HEIGHT (ABSOPBANCE)PEAK AREA (ABS-SECONDS)
" READ: 7.3
1 MEAN- 9.3 ST3.DEV."
I SE 2OO9 S\(Q
\ PEAK HEIGHT (ABSORBANCE)I PEAK AREA (ABS-SECONDS)
* READ: 11.1
; PEAK HEISHT 'ABSORBANCE)! PEAK AREA I ABS-SECONDS!
• READi S.C
j MEAN- 9.5 STD.DEV..' ***********************************
0.0.
2.5
0.0.
0.0.
2.2»»**i
AA231404
AA272543
AA234435
*****
ZAA0. 1500.060
COEF.VAR.. 25.81 X
ZAA0. 1590.071
ZAA0. 1360.061
COEF.VAR.. 23. 13 X»**•*»**«*»•«*»*«****•<
BC0. 1690.344
BC0.2160.472
BC•3.2380.424
20 1 OAA ZAA BC
PEAK HEIGHT (ABSORBANCE! 0.253 0.130 0.236, PEAK AREA (ASS-SECONDS) 0.469 0.072 0.397
READi 11.5
AA ZAAPEAK HEIGHT (ABSORBANCE) 0.250 0.§BPEAK AREA (ABS-SECONDS! 0.428 O.TOf* " 0.367 j
1^ *™ PEAK HEIGHT : ABSORBANCE i <XZG* 0 O / .3 -, aPEAK AREA (ABS-SECONDS) 0.192 0.124 0.068
READ: 0.074
AA ZAA BG;; PEAK HEIGHT (ABSORBANCE) 0.227 0.138 0.032PEAK AREA IABS-SECONDS! 0.170 0.110 0.060
! READ! 0.039
MEAN- 0.066 ST3.DEV.. 3,010 COEF.VAP.= 15.3- %* ********************************************************************************
20.0 STANDARD 1*******«********»»*«*»*********4********44444***4**44******44»444»**44**4***4»4*SE
AA ZAA BCPEAK HEIGHT (ABSORBANCE) 0.360 0.302 0,073PEAK AREA (ABS-SECONDS) 0.248 -3.171 0.077
PEAD: 36.4 / /7 )
AA 3AA BGPEAK HEIGHT IABSORBANCE) 0,340 0.283 0.067PEAK AREA (ABS-SECONDS' 0.23S 0.1~4 0.064
READ: 37.1
MEAN" 36.T 373.DEV.- 0.3 70EF.VAR.= 1.40 *4***********4*»»»»**»*44*»*4****»*»4*4***»»44»4**»***4»*4*»***4*4*444*»**»*4»*»*
36.7E-30: READING GREATER THAN HIGHEST STANDARD
***>***»******»*****»***»**»***»*4*»»4*»*******»**»»»*»****»»**»»*»»************
39.3 STANDARD 2***»«******»»******»*******»****»**********»***»*»*»******<.»**** *«»»»******»****
AA ZAA BGPEAK HEIGHT (ABSORBANCE) 0.457 0.330 0.083PEAK AREA (ABS-SECONDS) 0.314 0.238 0.077
READ: 50.2
(CONTINUES'AA ZAA BG
PEAK HEIGHT (ABSORBANCE) 0.428 0.353 0.090PEAK AREA (ABS-SECONDS/ 0.309 0.233 0.076
READ: 38.8
MEAN- 59.3 STZ.DEV.. 1,0 COEF.VAR.- 1,66 t********************************************************************************
39.3E-30! READING GREATER THAN HIGHEST STANDARD
»**»*•»*•****«*»*******»»*»»**»**»*»»»*»***»»*4*****4**»»*«»********»»*»»*»*»*»»
39.8 STANDARD 3»****••*»•****»»**»»•**»»**»•«»»***********»***»»*»********»*4*»***»»*»****>»**»
SE 2005S QC_^^- AA ZAA BG
PEAK HEIGHT (ABSORBANCE) 0.371 0.306 0.071PEAK AREA (ABS-SECONDS) 0.232 0.187 0.365
READi 44.1
AA ZAA BCi PEAK HEIGHT (ABSORBANCE) 0.350 0.290 0.070•PEAK AREA (ABS-SECONDS) 0.250 0.183 0.067
• READ! 42.8
MEAN- 43.5 ST2.DEV.- 0.9 COEF.VAR.- 2.11 tt***********************t*******************************************************
&R103262
-0.003 O &\
0.000 STD.DEV.. O.o04*,.*************************************.**** ..«..........„0.000 AUTOZERO
«»»*»*»***»«******#******»»**»»*«»*«*»»**»*««»**»**«»*»«**»«»»»«»»»***»**»**lt__SE
AA ZAA BCPEAK HEIGHT ( AESOREANCE) 0.139 0.159 0,041PEAK AREA (ABS-SECONDS) 0.123 0.093 0.033
READ: 0.030
AA ZAA BCPEAK HEI3HT 'ABSORBANCE) 0.188 0.153 0.046PEAK AREA (ABS-SECONDS! 3.137 0.395 0.041
READ: 0.030
MEAN- 0.030 37r.DEV.= 0.300 COEF.VAR.. 0.32 *
20.0 STAN2APD 1*************************************************************************** ******SE
AA zaA BCPEAK HEIGHT (ABSORBANCE' 0.296 3.233 0.052PEAK APEA SABS-SECONDS) 0.198 0.143 0.049
READ: 41.4 (J l)
AA ZAA BCPEAK HEIGHT (ABSOPEANCE) 0.299 0.241 0.058PEAK AREA (ABS-SECONDS) 0.139 0.138 0.051
READ! 37,0
MEAN- 39.2 S7C.DEV.- 3.1 COEF.VAR.. 8.00 X********************t***********************************************************
39.2E-50: READING GREATER THAN HIGHEST STANDARD
t*******************************************************************************39.8 STANDARD ^
********************************************************************************SE
AA ZAA BCPEAK HEIGHT (ABSOPBANCE) o.4ia 0.344 0.073PEAK AREA (ABS-SECONDS) 0.257 0.132 0.064
READ: 59.9 /2f\
(CONTINUED)AA ZAA BC
PEAK HEIGHT (ABSORBANCE) 0.398 0.326 0.072PEAK AREA (ABS-SECONDS) 0-258 0.199 0,060
READ! 62.4
MEAN- 61.1 373.DEV.» 1.8 CQEF.VAR.. 2.93 Xt************************************************************!******************
61.1E-50i READING GREATER THAN HIGHEST STANDARD
i********************************************************************************60.4 STANDARD 3
**»****»*«***«*»****»***»**,»»*»»»***v»**»*« *»»«»*»«*»»*•»»*»*»*»*«**»*•»»»«*»»«*»
AA ZAA BCj PEAK HEIGHT (ABSORBANCE) 0.353 0.296 0.071'PEAK AREA (ABS-SECONDS) 0.234 0.174 0.060
PEAK HEIGHT (ABSORBANCE)k PEAK AREA (ABS-SECONDS)
Q32w«3t2 0.072 jlo.iao o.oso ^m
1*»•**»****«****«»*»**»****»«»*»«*****»*»**»****»«»*»"- »*««**«»*«.»*«««»«««»,«,»**»»»««,*«,»,«2009 <_,A 6 S4?)
I* ^ 0*** -r4 ZAA scPEAK HEIGHT (ABSORBANCE) IS 0.235 0.153 o issPEAK AREA (ABS-SECONDS) ' 0.401 0.063 0.333
READ: 7. l
AA -AA BCPEAK HEIGHT (ABSCRBANCEJ 0.229 0.144 3.174PEAK AREA (ABS-SECONDS) 0.399 C.057 0.342READ: 4.3
MEAN- 5.9 STB. DEV.- 1,7 COEF.. VAR. = 27.39 1********************************************************************************SE 2010 -i~7A
AA ZAA BCPEAK HEIGHT (ABSORBANCE1 0.229 0.160 0.146PEAK ARE^ (ABS-SECONDS) 0.341 0.353 0.273
READ: • 7. 1
AA ZAA BCPEAK HEIGHT ;ABSORBANCE) 0.233 0.153 0.143PEAK AREA IABS-SECONDS: 0.331 0.054 0.265READ: 7.7
MEAN= 7.4 3TZ.DEV.* 0.4 COEF. VAP, = 3,77 T.
SE "yoYY"""" "?' ' I AA ZAA BG
PEAK HEIGHT' (ABSORBANCE' 0.255 o.isa o.ies
PEAK AREA (ABS-SECONDS) 0.415 0.060 0.353
AA ZAA BCPEAK HEIGHT (ABSORBANCE) 0.231 0.139 0.137PEAK AREA ( ABS-SECONDS ) 0.407 0.062 0.345
READ: 6.8
MEAN- 6.5 STD. DEV.- 0.5 COEF, VAR.. r.oi X********************************************************************************
-(%ASE 2012
AA ZAA BGPEAK HEIGHT (ABSORBANCE) 0.359 0.258 0.148PEAK AREA (ABS-SECONDS) 0.413 0.121 0.294
AA ZAA BCHEIGHT (ABSORBANCE) 0.374 0.274 O.MS
PEAK AREA I ABS-SECONDS) 0.420 0.116 0.304READ i 23.3
MEAN- 29.3 STD.DEV.- 1.3 COEF.VAR.- 4.57 tf*******************************************************************************SE 2013 -PEAK HEIGHT (ABSORBANCE) 0.371 0.268 0.144PEAK AREA (ABS-SECONDS) 0.401 0.125 0.276
READ! 32. 11
I
AA «AA BGPEAK HEIGHT (ABSORBANCE) 0.360 0.259 0.142PEAK AREA (ABS-SECONDS! 0.393 0.117 0.275
„'•* . READ! 28.9
MEAN- 30.5 ST3.DEV.- 2.3 COEF.VAR. •
RADIAN ANALYTICAL SERVICESQUALITY CONTROL DATA SUMMARY
Form IX^H ——
Cl lent ID lA ft fow iWorkorder $f / / Q*)
Sample ID No.,mS£jJmQ$'$- (J
CoSub
ICP SERIAL DILUTIONS
Parameter
- n
A
'
Initial SampleConcentration (1)
<7SL
Serial Dilution1Result (S)3(0
mp i 1 edmittedMatr ix /QfrQieL.
Units fl-/«]L^ • J
^Difference2
</»3
jftk luted sample concentration corrected for J'f_f dil'ution.2. ®rcent Difference =lLzS.ix 100
IMR - Not requ i red
103265
Fore VIQ. C. Report No
DUPLICATES
LAB NAME KtoLai CASc NO.
DATEEPA SampleLab SampleUnits fvy
87- I!No.ID No
053,
8?//6f3-
Matrix '&6L&, ^ <T
Cosocur.c
Metals:1. Aluminum
Control Limit J Samole(S) Duolicate(D) P.P--
2. Ar. t icon v3. Arsar.icA. Esriutc5. Beryllium6. Caesium7. Caiciua8. Chroaiua9. Cobalt10. Coorser11. Iron12. Lead13. Maenesium14. Manganese15. Mereurv16. Nickel17. Potassium18. Selenium19. Silver20. Sodium21. Thallium22. Tin23. Vanadium24. Zinc
Other:
r?pD«: ao%
^P/XLiO1?*
n
I*
I.
1// 1
43
<o.ns~
n.iaQ
tr>.-a%
9. 1
43
<n.DS"
O.bl
<0.3X
»
10
D
1r>
l.3~
tic.
\Cyar.ide* Out of ControlTo be added at a later date. 2 RPD - [|S - D|/((S * D)/2)J x 100- Non calculable RPD due to value(s) less than CRDL
B - 12
V s
Fere VI
Q. C. Report No. ~DUPLICATES
LAB NAME jAiAj CASE NO. g?- / /Sample No. ___
Lab Sample ID No.Units // />M/- _
Matrix
Cpapo-jr.s | Control Limit J j Sacple(S) | Duplicated ) J RPD-
Metals:1. Alusinuc2. Ar.timonv
3. Arsenic4. Barium5. Beryllium
6. Cadmium7. Calcium8. Chromium9. Cobalt10. Cooler11. Iron12. Lead13. Maznesium
14. Maneanese15. Mercury16. Nickel17. Potassium18. Selenium19. Silver20. Sodium21. Thallium22. Tin23. Vanadium24. ZincOther:
RPD<*o9o
krotzott,
J?PD <90%
flpDcao*?.,
• <O.OQ1-
fl.no*
A.ooS"
< 0. Of)2>
<o.ao3.
fl.pn*
\ 'O.OOG
<o.oo$
«
N£,
0
tfc
AC.
\Cvar.ide* Out of Control . _ _ _ _ - - -To be aaded at a later date. 2 RPD - [|S - D|/((S * D)/2)J x 100- Non calculable RPD due to value(s) less than CRDL
B - 12 RRS03267
V -
Fcrc VIQ. C. Report No. -052
DUPLICATES*
LAB NAME jQtU>U&/* ______ CA-St NO. . //EPA Sample No.
DATE Lab Sample ID No.Units U<L-
-TT
Corns3-ur.c | Control Limit1 t Sample(S) | Duciicate(D) I RPD-
Metals :1 . Aluminum2. Ar.timonv
3. Arsenic4. Barium5. Beryllium6. Cadmium7. Calcium8. Chromium9. Cobalt10. Cooper
Iron12. Lead13. Maenesiun1 4. Maneanese15. M-rcurv16. Nickel
17. Potassium
18. Selenium19. Silver20. Sodium21. Thallium22. Tin23. Vanadium24. Zinc
Other:
f?PD <
*\
30 "7.
f
thfil
< 0.001
< o.oos
<o.ooq
0.-V&
o.erfi *
o.on *
n.-v*,
<O.Ole
<0.OO/
eo.otn
<O.OO
a. is
C.o'S?*
<o .on*
0.33
1
/Vc,
A/C,A/c.
filC,
ff.a-
A/C
A c
c»-
Cva-ide
"ut of ControlTo be aaded at a later date. 2 RPD - [|S - D|/((S -t- D),'2)J x 100- Non calculable RPD due to value(s) less than CRDL
value. < S~«
B - i 2 RR103268
Form IVQ. C. Report No.
ICP INTEKFEBENCL CHECK SAMPLELAB NAME )&U£uL*O CASE NO. 37- li
Check Sample 1.0. £/V? /DATE • Cheek Sample Source•""•"—"•"— — —— —— - Units
CompoundMetals :1 . Aluminum2. Anciaony3. Arsenic4. Barlua5. Berylliua6 • CadoiuB7. Calciua8. Chroaiua9. Cobalt10. Copper11. Iron12. Lead13. Magnesium14. Manganese12. Mercury16. Nickel17. Potassium18. Selenium19. Silver20. Sodium21. Thallium22. Tin23. Vanadium24. ZincOther :
ControlMean
f>. V77n.SMil
n.eiSKf.
r>.<SZl
c.qtt
O.Qtele
l.OCfe
Limits1Scd. Dev.
A.OOIn.OD**
to.oDto
fJ.ttAtt
ff.ODfa
ff.Afita
0.00*1
True2Initial
Observed
/v</tfI n.r.9-
O.1SL
O.tf,
0.1O
oat
O.tt
_——<•»—<ZR
lf)len
loo
(03,
q*
lot
5?
FinalObserved
1
1e.4* \O.'gT-
A.4SL 1
AW^ 1
DAD
DflK
O.K
r
\2R
JOI
<??
100
11
iqp
(Dl
W
1 Mean value based on n •—j
True value of EPA ICP Interference Check Sample or contractor standard.
B - 10
Form IIIQ. C. Report No. _0]
BLANKS
LAB NAME If LoU M ______ CASE NO. %?- // OS^DATE _____________________ UNITS
Matrix
PreparationCompoundMetals:1 . Aluminum2. Antimony3. Arsenic4. Barium5. Beryllium6« CAdStLus7. Calcium3 • Chromium9. Cobalt10. Cooper11. Iron12. Lead13. Magnesium14. Manganese13. Mercury16. Nickel17. Potassium18. Selenium19. Silver20. Sodium21. Thallium22. tin23. Vanadium24. ZincOther:
Cyanide
InitialCalibrationBlank Value
O.00b *
•
Continuing CalibrationBlank Value
1 2 3 4
(0.00& <0.00f <0 005 (D.OOS'
\
Preparation Blank j1 2
<-0.ooS
*
.
l
4
1
—— 1
B - 9SRI03270
Form IIIQ. C. Report No.
BLANKS
LAS NAME &1AJL/!U*-. _______ CASE NO. ??•-// 053DATE ____________________ UNITS Lt&
ffMati
PreparationCompound
Metals :1 . Aluminum2. Antimony3. Arsenic4. Barium5. Beryllium6. Cadmium7. Calcium3. Chromium9, Cobalt10. Cooper11. Iron12. Lead13. Magnesium14. Manganese15. Mercury16. Nickel17. Potassium18. Selenium19. Silver20 . Sodium21. Thallium22. Tin23. Vanadium24. ZincOther:
Cvanide
InitialCalibrationBlank Value
<D.Oto
< 0.003.
<t>.r>o\€ O . O0_3
1 _)* QfJ
C0.DI
O./J62L
O. OOO*>*
<0.03L
to.oos<o.on<\
< 0.003
C'D.QQk•
•iat <§££. flyaH "•Continuing Calibration
Blank Value1
00.0k
<D.OO
<0.00l
09/503
<O.OtK
<<2/?J
(0,00 3k.
A.oAfla*<A0a.
< 'O.ooS<o.nrx
< 0.60 3
<o.oa<f-
2 3
<. h. Ola
< O.OO3.
<O-OOI
<o.oc&
<t.OOa(
(0.6)
fo.ooi.
< 0.0001,
<0.02-
<040S
W.OO*
<0, 003
<Q.OO(e
< 0.003-
'
Q.OOO3L
<O.OOS
<4.0D±
4
<U/V33
\
AQUJUHAA- S4l<d
Preparation Blank1 2
<0.6b
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ZHZTXAL AND COlttXNUZJIG CALI3JUXXON VEXUTCAJIOW3LA* NAttl lS&6UJLM~ OSX W.
SOU M.DATIS ___________________ wmsCojKMundttecals:1. Altsstnam2. Antimony3. Arsenic4. Barium3. Berylliumw. e*<*«*__i7. Calcium1. Osra-aLu-9. Cabalt10. Cooper11.' Iron12. Lead13. Magnesium1 4. MancjnaeaeL5. Hercnry16. Nideel17. Potassium18. Selenium19. Silver20. Sodium21. thalliua22. tin23. Vanadium24. ZincOther:
Cysa.de
laitiatrue Value
0.0SO
il Calib.Found
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too
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11
1111
A. MS
a
90
Method4
1
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Initial Calibration Source * Conclnu-ac Calibraeioo Source jf&vu. OA3 Control Limits: Mercury and tin- 30-120; All Other Compounds ' 90-UO4 Indicate Aaalycieal Heehed C««d: F - IC7/Flaae AA; F - Furnace.
B - 8
ui HAM &jidMuv
OA2Z ____________
AMD coKzunnuic c.rjm.TioM
Hetals:
2. Aaelsmnr3. ArsenicA. Barium3. Beryllium6. CadBtiai7. Calcium8. Cbmeltm9. Cobalt10. Capper11. Iran12. Lead13. Hacnestiu—14. Maa-ane*eL5. Merenry16. Nickel17. PotassiumU C _ _ 1 __^4 •«->>
19. Silver20. Sodium21. thallium22. tia23. Vanadium24. Zinc.Other:
Cyanide
True Value
n. 100
Found
n.ffft
a
48
True Value
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1 Initial Calibration Source * Caneinuiaj Calibration Source3 Centre. Uaiu: narearf and Tin. 30-120; Ail Ochtr Caa-outuU '90*1104 Indicate Aaalycical Method Osed: P - IQP/Flaaa AA; F - Furnace
B -6R103Z73
ATOMIC ABSORPTION SPECTROPHOTOMETRY QUALITY CONTROL SUMMARY
A Date
Standard Cal Ibratlon ID,Itlal QC Cheek Contlnulna QC Cheek
Cone. £__ Height Measured Theo. __ Re&. Measured Theo. __ Rec0 ,010 _5/ 5fl 702. SO SD 100ZO , 0854O ,153(oO , ZZO
Corr. Coef .______/__)Slope ,OOW
Int. ,O/Z_
Sample No. Sample
SD ~W /DO——— —— ——
Oup 1 fcates
Result Duplicate Result fRPD
-£>3 3.0 <3.£ O-/O <3.£> <3.O &~/7A *3.C> <3-O O
Spikes
Spike t SampleSample No. Result3W/QS3-6I ZS
-Cft 2-t"O'^A 25-Ol ZO
Sample Result Spike Added % Recovery<3.0 -ZS ICO<3-C> 2S 8^*3.O 2S IOO<3.O (&b 20 loO
-OS 13 <3.0 (&ti 2.0 95~/8 L (p 0. 2# (/?£) 1.1 tf*-/-l°l /.? <0.t% ('rf ./. f 5"
ATOMIC ABSORPTION SPECTROPHOTOMETRY QUALITY CONTROL SUMMARY
Element tJ^ Analyst n /u <L____ Date u - /<f "df 7
Standard Cal Ibratton Initial QP Check Continuing Qg Check
Cone. £__, Height Measured Thee. i, Ree. Measured Thee.
. __£__ ..______. -
Corr. Goaf.
Slope - QQ7Int. "• Oo8?
Dup 1 Icates
Sample No. Sample Results<4~~ Q A DH fS . y
Dupl Icate Result SRPD_fo
-n<^ «5/ /7 -2/f 7 ao
*7 // <•
5"1/- Qfe O,j *?A-TSAi *?.?
5 5 3 - a .2 75y «i z.-o- /& <?• '
*?7*fo
<a-o-7-3
5"^0
-?7- 7
Spikes
Spike t SampleSample No. Result Sample Result Spike Added % RecoveryVTHQStJ-rM ______
•xs0 /
/-o/S"
01 <•?<? 3-? AS
-07 ^5
•RRI03275
ATOMIC ABSORPTION SPECTROPHOTOMETRY QUALITY CONTROL SUMMARY
Element ____________ Analyst _____2_1____ Date //'/_?' 87
Standard Gal Ibratlen Initial flC, Check Continuing
Cone. Pk Height Measured Thee. i Rec. Measured \s~) /)(/& 4 7 .5) Qtf V7
20 ,11 1 V84O ,171 <+l6sO • 234 V 7
Corr. Coef. 'VVT7 ,...z5—Slope ,__/QQ3 __Int. -.P S
Dup 1 Icates
Sample No. Sample Result Duplicate Result2/7//G5</-02_ <5.O ^^-0
-04 <5.0 <«5.0
1 QC Cheek
Oieo. J Rec3) f7«L^
j ^g7 9 0
JRPD0O
3/y/£53-£>3 <5.0 <S.O O-OV S.O <S.O 0
Sp ikes
Spike t SampleSample No. Result Sample Result Spike Added27//Q5< 0/ <SO *3>O 2O
$ RecoveryO
~Of <JTO < S-0 ZO Ot/:«o -03 2 4 <:5.ft 2S %
%' OS" S.O < S.O 2S &*'(r.a\ o ^ *5 <0 2°V_J ' / - -*l _X S-- • L-< •*•-. ,__J /ZO-OS <O.S <0>5 2.0 ^-O-5 <^0-5 <O-5 2.0
M/inswi 2 <5,o 2so
RR103276
L fATOMIC ABSORPTION SPECTROPHOTOMETRY QUALITY CONTROL SUMMARY
Element rA Analyst r>AX_c_____ Date M - /g~f 7
Standard Gal Ibratlen Initial g Cheek Continuing qc Cheek
Cone. EX Height Measured Thee. £ Rec. Measured Thee,/-. aav/ ?? (SO <?8 /at/ 700
aao .<3?,3 /> (oW / 0 jf
Corr. Coef..Slope « ^^/-oc-TInt. ~ -oocra, /.oo3
Dup 1 icates
- » 7sTllQS^" ^b « D /« ^_^£j______ ^_____7 S^ 0 O o_________T3C.. o S1 QQ t> ___j
Spikes
^10 O (J » • T- ** O
__3___I5
y?^a a
Sample No. Sample Result Duplicate Result {RPDuk f .*/ f._g ___I
Spike t SampleSample No. Result Sample Result Spike Added % Recovery
COM »OM«TI01
?CB QC SUMMARY
ZN 8.03 0.0345 0.033 0.033 5.2
SAMPLE NO. 43 CAL BLANK
WEIGHT 1 GRAMS VOLUME 1 ML
22:34:26 20-NOV-87 43 CAL BLANK
MV INT RAW CONC CONCEN OIL CORR RSD
<AG 12.75 -0.0034 U-0.003 < 0.009 < 0.009<AL 12.05 -0.0461 U-0.046 < 0.200 < 0.200AS 6.20 0.1110 U 0.111 < 0.300 < 0.300AU 4.36 0.0342 U 0.034 < 0.200 < 0.200<B 6.49 -0.0077 0-0.008 < 0.600 < 0.600BA 10.92 0.0022 0 0.002 < 0.009 < 0.009BE 6.57 0.0000 U 0.000 < 0.001 < 0.001<BI 3.18 -0.0274 0-0.027 < 0.800 < 0.800<CA 10.73 -0.0135 U-0.013 < 0.060 < 0.060<CD 4.17 -0.0017 U-0.002 < 0.003 • 0.003<CO 6.27 -0.0074 0-0.007 < 0.010 < 0.010<CR 7.04 -0.0006 0-0.001 < 0.009 < 0.009<CO 26.84 -0.0010 0-0.001 < 0.010 < 0.010<FE 5.64 -0.4775 0-0.478 < 0.030 < 0.030<IN 4.09 -0.0027 0-0.003 < 0.200 < 0.200<K 7.52 -0.0843 0-0.084 < 0.300 < 0.300<LI 11.24 -0.0001 0-0.000 < 0.020 < 0.020<MG 8.30 -0.0017 0-0.002 < 0.100 < 0.100<MN 7.17 -0.0003 0-0.000 < 0.003 < 0.003MO 6.85 0.0242 0 0.024 < 0.050 < 0.050<NA 12.01 -0.5484 0-0.548 < 0.080 < 0.080<NI 5.50 -0.0044 0-0.004 < 0.020 < 0.020<P 2.92 -0.1873 0-0.187 < 0.300 < 0.300PB 8.24 0.0024 0 0.002 < 0.050 < 0.050<PT 5.15 -0.0303 0-0.030 < 0.200 < 0.200S 18.47 0.0392 0 0.039 < 5.000 < 5.000<SB 9.43 -0.0055 0-0.006 < 0.060 < 0.060<SE 9.23 -0.0282 0-0.028 < 0.300 < 0.300<SI 8.87 -0.0082 0-0.008 < 0.300 < 0.300<SN 5.86 -0.1000 0-0.100 < 0.500 < 0.500<SR 37.02 -0.0001 0-0.000 < 0.003 < 0.003TE 14.08 0.1247 0 0.125 < 0.200 < 0.200TI 9.93 0.0071 0 0.007 < 0.050 < 0.050<TL 4.28 -0.0234 0-0.023 < 0.090 < 0.090<U 7.96 -0.1132 0-0.113 < 0-500 < 0.500•. y :•. \~. •:. :•-">. ••-•> v.7 ': ' :";-w 4 .' a , : : ' : ' - : • , ; : ~
ZN h >4
DONE ON 20-NOV-87
0.87042.11970.3159
'Si'0343
904U 0.240
•:!
;rS •' •;•»iss0.413
* 0.196< 0.0090.845 0.5
600
SAMPLE NO. 41 CCCS-1f )WEIGHT 1 GRAMS VOLUME 1 ML
22:29:36 20-NOV-87 41 CCCS-1
MV INT RAW CONC CONCEN DIL CORR RSD
AG 13.13 0.0194 * 0.019 * n niq , ,
" : <«: | < ;:,?:?! - ; « :.
:B8S:S : :j j
<..»» < :S .S.9:SS S:ISS ' f:o>» • : i :
ii;s S w 's .-Isil !• HS Hi 0
500 <. 0
r if 11 :l f» iJttf .°:!.°?; •S.-.'Sf <•;•«•103Z80
_ _——,—— - — -- - — _•_•_ mp __, • _^ , —— — « « • * —• - ———-; i ••a» a>' p aiIK 4.23 0.1918 0 0.043 < 18.18K 14.34 17.5604 12.66 1151 6LI 36.77 1.0220 1.022 92.91 0MG 67.75 29.5292 29.43 2676 0MN 225.14 2.1196 2.116 192.3 0.2MO 7.11 0.0374 0 0.010 •: 4.545 < 0.050NA 45.41 12.7695 9.609 873.5 0.3NI 22.71 1.0176 1.010 91.81 0.7P 6.16 8.2820 2.785 253.2 2.0PB 13.74 1.2983 1.242 112.9 2.0PT 5.92 0.6610 U 0.131 •, 18.18 <- 0.200S 150.55 S.8341 * 8.108 * 7.37.1 0.5SB 14.40 0.7678 0.631 57.40 6.2SE 12.77 1.4576 * 1.173 * 106.6 2.4SI 70.73 9.4320 9.311 846.5 0.2>3N 13.09 10.4097 * 1.123 * 102.1 9.4SR 480.74 1.0041 1.003 91.22 0.2TE 14.56 0.1425 U 0.082 •: 18.18 < 0.200TI 19.13 0.8344 0.834 75.86 0.3TL 3.53 0.9435 0.897 81.51 2.7U 8.99 1.3160 * 0.591 * 53.75 7.9V 16.86 1.0185 1.018 92.59 0.3W 4.55 0.1227 U-0.046 < 9.091 < 0.100Y 12.26 0.0575 0.058 5.228 1.4ZN 74.44 1.9773 1.935 175.9 0.1
SAMPLE NO. 39 053-17A OIL
WEIGHT 1.01 GRAMS VOLUME 400 ML
22:24:41 20-NOV-87 39 053-17A DIL
MV INT RAW CONC CONCEN DlL CORR RSD
<AG 12.73 0.0028 0 0.003 < 3.564 < 0.009AL 57.40 12.5160 12.52 4957 0.7AS 6.16 0.0555 0-0.047 < 118.8 < 0.300AU 4.57 0.2152 0 0.056 < 79.21 < 0.200B 6.57 0.0232 0-0.127 < 237.6 < 0.600BA 19.15 0.1360 0.136 53.87 1.4BE 7.30 0.0033 0 0.000 < 0.396 < 0.001BI 3.20 -0.0391 U-0.055 < 316.8 < 0.800CA 38.87 5.1136 5.114 2025 0.4CD 4.55 0.0164 * 0.009 * 3.427 46.9CO 6.65 0.0134 * 0.012 * 4.699 24.2CR 7.36 0.0115 * 0.009 * 3.705 11.7CO 30.87 0.0639 0.062 24.43 0.3FE 954.62 33.9751 33.98 13455 0.6IN 4.12 0.0621 U 0.029 < 79.21 < 0.200K 8.20 2.0221 * 0.800 * 317.0 14.7LI 11.92 0.0159 0 0.016 < 7.921 < 0.020MG 18 10 4 8650 4.846 1919 0.4MN 36.65 0.2829 0.282 111.7 0.8MO 6.54 -0.0003 0-0.005 < 19.80 < 0.050NA 14.34 -1.5914 0-2.656 < 31.68 < 0.080NI 6.18 0.0199 0 0.018 < 7.921 < 0.020P 3.42 1.5958 * 0.569 * 225.4 661.8PB 8.61 0.0895 * 0.080 * 31.66 29.5PT 5.26 0.1184 0 0.021 < 79.21 < 0.200S 47.89 1.2843 0 1.145 < 1980. < 5.000SB 9.70 0.0620 U 0.032 < 23.76 < 0.060<SE 9.23 0.0949 0 0.095 < 118.8 < 0.300SI 13.55 0.6329 * 0.567 * 224.7 2.0SN 7.18 1.9676 0 0.022 < 198.0 < 0.500SR 45.63 0.0186 0.018 7.207 0.5 . A n O QTE 13.86 -0.0534 0-0.059 < 79.21 < 0 ftefeo \ U «J t. VTT 11.58 -n n=,RR n-o nc.o /• 1 o Rn x oV\en
47.5519 47.55 4708 0 . 6~V/ In f) H0.3051 U-0.082 < 29 70 < 0.30(X *
Air 184.03AS 6.40AO 4.66 0.2520 0-0.003 < 19.80 < 0.200B 6.90 0.1518 U-0.254 < 59.41 < 0.600BA 42.61 0.5225 0.522 51.73 0.5BE 9.53 0.0118 U 0.000 < 0.099 < 0.001BI 3.30 0.0703 U-0.004 < 79.21 < 0.800CA 119.47 22.2550 22.26 2203 0.2CD 4.87 0.0290 * 0.010 * 0.992 22.7CO 7.29 0,0447 * 0.039 * 3.870 2.0CR 8.52 0.0813 0.074 7.297 3.4CO 42.30 0.3148 0.308 30.48 0.7FE 3565.97 127.6403 127.6 12638 0.4IN 4.14 0.0784 U-0.043 < 19.80 < 0.200K 10.21 7.1228 3.894 385.5 2.6LI 13.91 0.0966 * 0.097 * 9.566 0.4MG 45.21 18.3289 18.25 1807 0.3MN 121.23 1.1070 1.104 109.3 0.4MO 6.99 0.0295 U 0.008 < 4.950 < 0.050NA 20.66 1.3310 0-1.290 < 7.921 < 0.080NI 7.89 0.1230 0.120 11.88 5.5P 4.68 4.6742 2.446 242.1 1.6PB 9.49 0.2977 0.255 25.20 5.4PT 5.49 0.3112 U 0.022 < 19.80 < 0.200S 133.35 7.5692 * 7.113 * 704.3 . 0.3SB 9.95 0.1000 U 0.010 < 5.941 < 0.060SE 9.69 0.2720 U 0.234 < 29.70 < 0.300SI 26.28 2.5916 2.537 251.2 0.4SN 10.97 7.3797 U 0.043 < 49.50 < 0.500SR 69.80 0.0734 0.073 7.203 0.3TE 14.29 0.0675 U 0.022 < 19.80 < 0.200TI 16.01 0.4653 0.465 46.07 0.2TL 4.51 0.0325 U-0.004 < 8.911 < 0.090U 8.17 0.2766 U-0.265 < 49.50 ; 0.500V 9.78 0.1007 0.101 9.968 14.3W 4.27 -0.0015 0-0.135 <-' 9.901 < 0.100Y 11.92 0.0490 0.049 4.852 0.8ZN 39.71 0.9538 0.929 91.97 0.6
SAMPLE NO. 37 053-18A PD SPK
WEIGHT 1.03 GRAMS VOLUME 100 ML
22:19:41 20-NOV-87 37 053-18A PD SPK
MV INT RAW CONC CONCEN OIL CORR RSD
A-l ?" ?.' •' ' •'•• .-.-!. 'L'.- ..4AL c:.?. :" .••••-- •"--• • - -j..AO 4 •• * 4 .7 •: -. .r..-B A .'." ri? i '• •'; 4 'BA .-"? .K' ' 4,' 7 ; 4.'U : 3.^.2 - . i . iBE L'49.10 •;. ii'i.'.jl i..SU6 citi.Ul U.2BI 3.46 0.2579 U 0.168 < 77.67CA 168.05 32.5878 32.59 3164CD 27.42 0.9156 0.882 85.67CO 25.86 0.9434 0.937 90.95CR 23.46 0.9800 0.970 94.20CO 83.25 1.2139 1.206 117.1FE 4155.07 148.7703 148.8 14444IN 4.34 0.2405 0 0.101 < 19.42K 14.15 17.0883 12.16 1181LI 36.79 1.0227 1.023 99.29MG 68.08 29.6915 29.60 2874MN 229.27 2.1598 2.156 209.3MO 7.06 0.0344 0 0.008 < 4,854NA 42.79 11.5587 8 587 833.7
SAMPLE NO. 34 053-15A
WEIGHT 1.01 GRAMS VOLUME 100 ML
22:12:15 20-NOV-87 34 053-15A
MV I NT RAW CONC CONCEN OIL CORK RSD
AG 12.84 0.0093 * 0.009 * 0.920 151.6AL 309.59 82.2898 82.29 8148 0.3AS 6.76 0.6831 U 0.073 < 29.70 < 0.300AU 4.85 0.3256 U-0.009 < 19.80 '- n . 200B 7.07 0.2161 0-0.257 ,. 59.41 < 0.600BA 94.52 1.3777 1.378 136 4 0.2BE 10.45 0.0153 U 0.001 < 0.099 < 0.001BI 3.39 0.1758 U 0.080 «. 79.21 < 0.800CA 198.93 39.1555 39.16 3877 0.2CD 4.96 0.0324 * 0.009 * 0.905 41.5CO 7.65 0.0619 0.055 5.447 1.8CR 9.03 0.1124 0.101 10.05 0.8CO 34.56 0.1449 0.137 13.56 1.3FE 4368.12 156.4122 156.4 15486 0.2IN 4.23 0.1459 U 0 . 000 < 19.80 '•. 0.200K 11.82 11.1781 -.828 676.1 2.6LI 15.17 0. 1476 148 14 62 14MG 60.31 25.8333 .5.74 2548 0 2MN 413.22 3.9522 • 949 390.9 0.2MO 7.02 0.0317 U C.001 < 4.950 < 0.050NA 24.30 3.0148 0-0.084 < 7.921 < 0.080NI 8.34 0.1505 0.147 14.59 4.6P 5.34 6.2786 4.402 435.9 1.7PB 9.51 0.3016 * 0.225 * 22.30 11.7PT 6.44 1.0961 0 0.163 < 19.80 < 0.200S 118.81 6.4999 * 5.490 * 543.6 0.6SB 10.40 0.1676 0 0.015 < 5.941 < 0.060SE 10.04 0.4055 * 0.361 * 35.76 8.5SI 28.12 2.8753 2.808 278.1 0.4SN 12.24 9.1901 0 0.169 < 49.50 < 0.500SR 109.30 0.1628 0.162 16.04 0.1TE 14.30 0.0694 0-0.015 < 19.80 < 0.200TI 15.36 0.3884 0.388 38.46 0.7TL 4.68 0.0725 0 0.010 < 8.911 < 0.090U 8.25 0.3772 0-0.258 < 49.50 < 0.500V 9.92 0.1193 0.119 11.81 2.9W 4.44 0.0725 0-0.092 < 9.901 < 0.100Y 12.91 0.0735 0.073 7.274 0.5ZN 49.39 1.2392 1.206 119.4 0.3
WF.:.JtiT • :.-. ;?• A-;, v-. >;.:?Mfr ;. '..•
22:14:44 20-NOV-87 35 053-16A
MV INT RAW CONC CONCEN DIL CORR RSD
AG 12.89 0.0123 * 0.012 * 1.091AL 231.81 60.7697 60.77 5378AS 6.62 0.5305 0 0.008 < 26.55AU 4.72 0.2770 U-0.006 < 17.70B 7.11 0.2316 0-0.281 < 53.10BA 31.78 0.3440 0.344 30.45BE 10.79 0.0166 0 0.001 < 0.088 < 0.001 n n oBI 3.40 0.1954 0 0.085 < 70.80 < 0.#Q8 1 ft / Q «5a A AT* nn a? AAAR 07 AA ne^-s n B v\ I *J *•*'CA 473.00 97.4445 97.44 8623
Y 11.34 0.034 ..___ - ————w——~_~——-____.ZN 22.97 0.4606 0.448 43788~ 0. 5~
SAMPLE NO. 32 053-13A
WEIGHT 1.11 GRAMS VOLUME 100 ML
22:07:13 20-NOV-87 32 053-13A
MV INT RAW CONC CONCEN OIL CORR RSD
<AG 12.76 0.0044 U O.C04 •: 0.811 < 0.009AL 171.28 44.0224 44.02 3966 0.1AS 6.33 0.2358 U-0.079 <. 27.03 < 0.300AU 4.62 0.2363 U-0.005 < 18.02 < 0.200B 6.87 0.1415 U-0.110 < 54.05 < 0.600BA 78.91 1.1204 1.120 100.9 0.1BE 8.43 0.0076 * 0.001 * 0.124 9.2BI 3.26 0.0234 0-0.012 < 72.07 < 0.800CA 216.27 42.8420 42.84 3860 0.2CD 4.68 0.0215 * 0.009 * 0.802 35.4CO 6.69 0.0155 * 0.012 * 1.125 33.6CR 8.23 0.0643 0.060 5.415 1.4CO 34.54 0.1444 0.140 12.63 0.8FE 1927.19 68.8596 68.86 6204 0.1IN 4.10 0.0405 0-0.027 < 18.02 < 0.200K 8.94 3.9022 2.157 194.3 5.2LI 13.20 0.0676 * 0.068 * 6.091 1.9MG 25.18 8.3820 8.341 751.4 0.3MN 74.53 0.6520 0.650 58.59 0.2MO 6.89 0.0232 0 0.007 < 4.505 < 0.050NA 22.13 2.0089 * 0.364 * 32.83 0.9NI 6.95 0.0664 * 0.064 * 5.759 1.3P 4.86 5.1140 3.602 324.5 3.7PB 8.95 0.1697 * 0.130 * 11.70 3.6PT 5.38 0.2148 0 0.033 < 18.02 < 0.200S 243.07 15.6379 * 14.97 * 1349 0.8SB 9.97 0.1025 0 0.018 < 5.405 < 0.060SE 9.60 0.2361 0 0.201 < 27.03 < 0.300SI 21.52 1.8592 1.829 164.8 0.5SN 8.55 3.9209 0-0.044 < 45.05 < 0.500SR 92.07 0.1238 0.123 11.08 0.1TE 13.89 -0.0450 0-0.086 < 18.02 < 0.200TI 13.42 0.1589 * 0.159 * 14.32 0.9TL 4.45 0.0196 0-0.014 < 8.108 < 0.090U 8.12 0.2179 U-0.112 < 45.05 < 0.500V 9.64 0.0821 * 0.082 * 7.396 12.8W 4.10 -0.0784 0-0.149 < 9.009 < 0.100Y 12.43 0.0615 0.062 5.542 1.0ZN 22.59 0.4495 0.433 38.97 0.7
SAMPLE NO. 33 053-14A
WEIGHT 1.02 GRAMS VOLOME 100 ML R R Q 3 2 O H
HB»'.rmv/ *
_ rob*' " < 5.408 < o!o6oA''_p 0$0.3349 0 0.297 < 27.03 < O.SOCr
SI 29.12 3.0286 2.997 270.0 0.2SN 8.71 4.1544 U-0.018 < 45.05 < 0.500SR 95.64 0.1319 0.131 11.80 0.4TE 14.43 0.1078 0 0.054 < 18.02 < 0.200TI 14.76 0.3170 0.317 28.56 1.8TL 4.57 0.0461 0 0.004 < 8.108 < 0.0900 8.14 0.2473 0-0.096 < 45.05 < 0.500^f 9.99 0.1279 0.128 11.52 3.8W 4.17 -0.0473 0-0.122 < 9.009 < 0.100Y 13.88 0.0971 0.097 8.748 2.1ZN 23.65 0.4805 0.461 41.55 0.6
SAMPLE NO. 30 053-11A
WEIGHT 1 GRAMS VOLOME 100 ML
22:02:23 20-NOV-87 30 053-11A
MV INT RAW CONC CONCEN OIL CORK RSD
<AG 12.73 0.0028 0 0.003 < 0.900 < 0.009AL 138.53 34.9611 34.96 3496 0.4AS 6.23 0.1248 0-0.115 < 30.00 < 0.300AO 4.51 0.1916 0-0.036 < 20.00 < 0.200B 6.71 0.0785 0-0.088 < 60.00 < 0.600BA 73.46 1.0308 1.031 103.1 0.2BE 7.67 0.0047 * 0.001 * 0.120 9.0BI 3.32 0.0938 0 0.075 < 80.00 < 0.800CA 195.60 38.4465 38.45 3845 0.4CD 4.49 0.0140 * 0.005 * 0.489 123.9CO 6.56 0.0092 0 0.007 < 1.000 < 0.010CR 7.95 0.0474 * 0.045 * 4.451 10.8CO 33.16 0.1142 0.112 11.16 1.4FE 1109.64 39.5356 39.54 3954 0.2IN 4.10 0.0459 0 0.007 < 20.00 < 0.200K 9.02 4.1045 2.208 220.8 2.8LI 12.99 0.0592 * 0.059 * 5.924 1.5MG 27.18 9.3739 9.351 935.1 0.5MN 75.73 0.6637 0.663 66.26 0.3MO 6.68 0.0089 0-0.003 < 5.000 < 0.050NA 18.41 0.2912 0-0.866 < 8.000 < 0.080NI 6.76 0.0550 * 0.052 * 5.189 1.8P 4.47 4.1530 2.842 284.2 1.1PB 8.89 0.1547 * 0.124 * 12.36 7.2PT 5.35 0.1928 0 0.007 < 20.00 < 0.200S 249.45 16.1073 * 15.50 * 1550 1.0SB 9.69 0.0605 0-0.007 < 6.000 < 0.060SE 9.55 0.2168 0 0.185 < 30.00 < 0.300SI 26.75 2.6645 2.647 264.7 0.1SN 7.42 2.3059 U 0.037 < 50.00 < 0 500SR 117.22 0.1807 0.180 18.00 0.3TE 14.03 -0.0066 0-0.037 < 20.00 < 0.200TI 13.84 0.2078 * 0.208 * 20.78 1.2TL 4.43 0.0151 0-0.012 < 9.000 < 0.0900 8.09 0.1844 0-0.030 < 50.00 < 0.500V 9.44 0.0566 * 0.057 * 5.660 4.3W 4.07 -0.0917 0-0.132 < 10.00 < 0.100Y 12.39 0.0607 0.061 6.070 0.5ZN 19.54 0.3594 0.347 34.72 0.7
0.0540 0-0 7614 <19- - - _ _ . - _ ~ <•>*. & <* >J . 200 >< t9.80 6.0774 4.129 400.9 2.4 /•" /I 0
LI 13.00 0.0596 * 0.060 * 5.791 1.1 yMG 27.91 9.7382 9.697 941.5 0.3MN 58.55 0.4962 0.495 48.02 0.4MO 7.04 0.0326 0 0.013 < 4.854 <. 0.050NA 19.64 0.8612 0-0.789 '. 7.767 < 0.080NI 6.88 0.0622 * 0.059 * 5.718 5.5P 5.38 6.3763 4.790 465.0 0.0PB 9.14 0.2136 * 0.159 * 15.42 6.0PT 5.30 0.1515 U 0.004 < 19.42 < 0.200S 116.65 6.3410 * 5.913 * 574.1 0.8SB 10.09 0.1211 0 0.009 ; 5.825 < 0.060CE 9.80 0.3144 0 0.277 : 29.13 -- 0.30051 29.13 3.0301 3.000 291.3 0.5SN 8.64 4.0448 0 0.062 •, 48.54 < 0.500SR 97.98 0.1372 0.137 13 26 0.4TE 14.09 0.0112 0-0.047 < 19.42 < 0.200TI 14.50 0.2859 0.286 27 76 0.9TL 4.50 0.0317 0-0.014 •- 3.738 < 0.090U 8.11 0.2012 0-0.130 •: 48.54 < 0.500V 9.87 0.1119 0.112 10.37 0.9W 4.21 -0.0281 0-0.099 < 9.709 < 0.100Y 12.90 0.07.31 0.073 7.101 0.7ZN 24.94 0.5187 0.499 48.46 0.7
SAMPLE NO. 28 053-09A PD DUP(D)WEIGHT 1 GRAMS VOLUME 100 ML
21:57:20 20-NOV-87 28 053-09A PD DUP
MV I NT RAW CONC CONCEN DIL CORR RSD RFJ AV
<AG 12.74 0.0036 U 0.004 <. 0.900 < 0 009AL 191.59 49.6426 49.64 4964 0.6 jp iAS 6.32 0.2219 0-0.125 < 30.00 < 0 300AU 4.65 0.2494 0-0.010 .'20.00 < 0 200B 6.77 0.1003 0-0.151 < 60.00 < 0*600BA 71.38 0.9965 0.996 99.65 0.7 8 \ i-n 343.BE 8.41 0.0075 * 0.001 * 0.130 51.7 2i'o O U 5 -BI 3.29 0.0664 0 0.031 < 80.00 < 0 800CA 125.98 23.6389 23.64 2364 0 .' 4 5 4 24"'9 507.CD 4.53 0.0153 0 0.003 < 0.300 < 0 003C0 6-?3 0.0174 * 0.014 * 1.443 4*0 13 i 452<CR 8.22 0.0637 0.060 5.958 4 3 i-'o cCO 34.85 0.1513 0.147 14.7? o.l ^'4 14FE 1924.54 68.7647 68.76 6876 05 ot fl7JJ'IN 4.12 0.0567 0-0.010 < 20 00 < 0 200 t.796.K 9.38 5.0067 3.212 321.2 4.2 22 1 ^61 037-LI 12.80 0.0517 * 0.052 *5.168 49 U4 J-J?JMG ^5.86 a. 7165 8.676 867.6 03 - 8^ flO^oTMN 56. U2 0.4716 0.470 47.00 0.5 ? - 475091MO 7.08 0.0352 U 0.018 < 5.000 < 0 050 'NA 20.75 1.3742 U-0.269 < 8.000 < o'oSONI 6.68 0.0499 * 0.047 * 4.692 2.7 19 7 <sP 5.23 6.0179 4.457 445.7 04 42 4«5PB 9.02 0.1861 * 0.141 * 14.10 13 l 83PT 5.19 0.0606 U 0.050 <20.00 < 0*200 'S 112.58 6.0417 * 5.643 * 564.3 o!s 1 7SB 9.95 0.1005 U 0.006 <6.000 <0060ff 9-73 0.2861 U 0.251 < 30.00 < 0.300SI 26.32 2.5978 2.568 256.8 OJ$nr 12.6 274. 025^SN 8.59 3.9781 U 0.019 < 50 . 00 -_ l ft *» S^O 'T? ?5'?n n'm^ °'119 H- 8&H \ " fl.1 11.2 12.555]TE 14.10 0.0150 0-0.032 < 20.00 < 0 200
0.9085AO 4.34 0.1259 0-0.021 < 0.200 < 0.20{B 8.90 0.9250 * 0.925 * 0.925 0.6BA 67.65 0.9350 0.935 . 0.935 0.2BE 243.67 0.8995 0.899 0.899 0.1BI 3.33 0.1055 0 0.101 < 0.800 < 0.800CA 59.04 9.4027 9.403 9.403 0.1CD 26.86 0.8936 0.879 0.879 0.4CO 24.93 0.8981 0.898 0.898 0.8CR 22.17 0.9025 0.901 0.901 0.1CO 69.15 0.9043 0.904 0.904 0.2FE 267.14 9.3162 9.316 9.316 0.2
•TIN 4.07 0.0162 U 0.016 < 0.200 < 0.200K 11.76 11.0264 9.198 9.198 0.3LI 34.08 0.9131 0.913 0.913 0.3MG 26.22 8.8987 3.896 3.896 0.3MN 100.34 0.90.35 0.903 0.903 0.1MO 6.56 0.0010 U-0.004 < 0.050 < 0.050NA 37.12 8 9382 8.283 8.283 0.2NI 20.43 0.8800 0.879 0.879 0.4P 4.05 3.1350 U-0.688 < 0.300 < 0.300PB 12.10 0.9127 0.906 0.906 1.1PT 5.41 0.2396 0 0.001 < 0.200 < 0.200S 27.20 -0.2372 0-0.505 '5.000 • •: 5.000SB 16.12 1.0265 0.988 0.988 1.6SE 12.03 1.1702 * 0.866 * 0.866 9.4SI 9.41 -0.0036 0-0.062 < 0.300 < 0.300SN 6.90 1.5626 * 1.012 * 1.012 7.9SR 447.03 0.9277 0.927 0.927 0.2TE 13.93 -0.0.337 0-0.035 < 0.200 < 0.200TI 12.19 0.0130 0 0.013 < 0.050 < 0.050TL 8.29 0.8891 0.882 0.882 4.50 8.68 0.9262 * 0.791 * 0.791 4.0V 16.11 0.9217 0.922 0.922 0.2W 4.08 -0.0858 0-0.095 < 0.100 < 0.100<Y 9.85 -0.0018 0-0.002 < 0.009 < 0.009ZN 37.13 0.8779 0.863 0.863 0.3
SAMPLE NO. 26 QCMS( )WEIGHT 1 GRAMS VOLOME 100 ML
21:52:24 20-NOV-87 26 QCMS
MV INT RAW CONC CONCEN DIL CORR RSD
AG 25.04 0.7493 0.749 74.93 1.0AL 143.61 '36.3685 36.37 3637 0.2AS 6.37 0.2705 0-0.079 < 30.00 < 0.300AO 4.73 0.2783 U 0.048 < 20.00 < 0.200B 7.21 0.2715 0-0.187 < 60.00 < 0.600BA 289.16 4.5843 4.584 458.4 0.3BE 9.87 0.0131 0-0.001 < 0.100 < 0.001BI 3.60 0.4259 0 0.335 < 80.00 < 0.800CA 896.93 187.6068 187.6 18761 0.0CD 9.35 0.2051 0.165 16.51 0.6CO 7.45 0.0523 * 0.046 * 4.563 12.6CR 34.56 1.6476 1.638 163.8 0.1CO 468.35 9.6691 9.661 966.1 0.2FE 4189.64 150.0106 150.0 15001 0.1IN 4.19 0.1135 U-0.027 <20.00 < 0.200K 12.39 12.6283 7.538 753.8 1.5LI 11.71 0.0076 0 0.008 < 2.000 < 0.020MG 70.26 30.7745 30.68 3068 0.2MN 203.55 1.9092 1.906 190.6 JJ .A A rt 9 O 7JMO 7.36 0.0539 0 0.033 < 5.000 ft M .f)d0 U £ O 'NA 353Q P 1 171 R • 1 / K . e i/» e ^ t
SAMPLE NO. 23 CAL BLANK( )WEIGHT 1 GRAMS VOLOME 1 ML
21:44:59 20-NOV-87 23 CAL BLANK
MV INT RAW CONC CONCEN OIL CORR RSD
<AG 12.78 -0.0002 U-0.000 < 0.009 <. 0.009<AL 12.09 -0.1430 0-0.143 < 0.200 <. 0.200AS 6.11 0.0069 U 0.007 <, 0.300 < 0.300AU 4.33 0.0989 U 0.099 < 0.200 v 0.200B 6.56 -0.0540 0-0.054 < 0.600 < 0.600BA 10.93 -0.0020 0-0.002 •• 0.009 t 0.009BE 6.58 0.0005 U 0.001 < 0.001 < 0.001<BI 3.18 -0.0195 0-0.020 < 0.800 < 0.300CA 10.92 -2.2473 U-2.247 < 0.060 < 0.060<CD 4.12 -0.0025 0-0.002 •. 0.003 < 0.003<CO 6.27 -0.0127 0-0.013 < 0.010 < 0.010<CR 6.93 -0.0066 0-0.007 < 0.009 < 0.009CO 26.91 -0.0236 U-0.024 < 0.010 < 0.010<FE 5.75 -0.2177 U-0.218 < 0.030 < 0.030IN 4.13 0.0594 U 0.059 < 0.200 < 0.200
<K 7.39 -0.4489 U-0.449 < 0.300 < 0.300<LI 11.17 -0.0099 0-0.010 < 0.020 < 0.020<MG 3.28 -0.1788 0-0.179 < 0.100 < 0.100MN 7.39 0.0010 0 0.001 < 0.003 < 0.003MO 6.82 0.0107 U 0.011 < 0.050 < 0.050<NA 12.37 -5.0853 0-5.085 < 0.080 < 0.080<NI 5.54 -0.0038 0-0.004 < 0.020 c 0.020<P 2.94 -0.0712 0-0.071 < 0.300 : 0.300<PB 8.23 -0.0165 0-0.016 < 0.050 - 0.050<PT 5.13 -0.0138 0-0.014 < 0.200 < 0.200S 19.36 -1.2440 0-1.274 < 5.000 •, 5.000<SB 9.46 -0.0417 0-0.042 < 0.060 < 0.060<SE 9.13 -0.0141 0-0.014 < 0.300 < 0.300<SI 8.83 -0.1641 0-0.164 < 0.300 < 0.300<SN 5.81 -0.1763 0-0.176 < 0.500 < 0.500<SR 36.97 -0.0042 0-0.004 < 0.003 < 0.003TE 14.14 0.0881 0 0.088 < 0.200 < 0.200TI 9.91 -0.0189 0-0.019 < 0.050 < 0.050<TL 4.20 -0.0378 0-0.038 < 0.090 < 0.090<0 8,02 -0.0042 0-0.004 < 0.500 < 0.500<V 9.14 -0.0056 0-0.006 < 0.020 < 0.020W 4.00 -0.0044 0-0.004 < 0.100 < 0.100<Y 9.94 0.0014 U 0.001 < 0.009 < 0.009<ZN 6.85 -0.0278 0-0.028 < 0.006 < 0.006
SAMPLE NO. 24 BLANK (3050) 11-18(B)WEIGHT i GRAMS VOLUME i ML
21:47:25 20-NOV-87 24 BLANK (3050) 11-18
MV I NT RAW CONC CONCEN DIL CORR RSD
<AG 12.68 -0.0077 0-0.008 < 0.009 < 0.009<AL 12.17 -0.0148 0-0.015 < 0.200 < 0 200AS 6.11 0.0173 U 0.017 < 0.300 < 0.300AO 4.36 0.0329 0-0.100 < 0.200 < 0.200B 6.51 0.0000 0 0.000 < 0.600 < 0.600BA 10.90 0.0018 0 0.002 < 0.009 < 0.009<BE 6.42 -0.0006 0-0.001 < 0.001 < 0.001
- BI 3.24 0.0391 0 0.039 < 0.800 < 0.800r& 1*A R-J O R57R n PUR A R K S q t
ZN 47.52 1.1707 0.854 ; 0.854 0.4
SAMPLE NO. 22 CCCS-2( )WEIGHT 1 GRAMS VOLOME 1 ML
SAMPLE NO. 21 CCCS-1( )WEIGHT 1 GRAMS VOLUME 1 ML
21:40:09 20-NOV-87 21 CCCS-1
MV INT RAW CONC CONCEN OIL CORR RSD
AG 13.15 0.0222 * 0.022 * 0.022 4.5AL 12.66 0.0148 0 0.015 < 0.200 < 0.200AS 11_.10 5.2013 5.201 5.201 0.2AO 4.40 0.1265 U-0.005 < 0.200- < 0.200B 19.17 4.8128 4.813 4.813 0.9BA 322.73 5.1347 5.135 5.135 0.3BE 1366.17 5.1554 5.155 5.155 0.3BI 3.42 0.2657 U 0.266 < 0.800 < 0.800CA 11.77 -2.0651 U-2.065 < 0.060 < 0.060CD 135.50 5.1641 5.096 5.096 0.3CO 112.22 5.1149 5.115 5.115 0.5CR 91.05 5.0526 5.049 5.049 0.4CU 255.26 4.9900 4.990 4.990 6.3<FE 9.60 -0.0797 U-0.080 < 0.030 t 0.030IN 4.24 0.1459 U 0.146 < 0.200 < 0.200
<K 7.49 -0.1960 0-0.196 < 0.300 < 0.300LI 137.18 5.0910 5.091 5.091 0.3MG 9.13 0.2418 * 0.242 * 0.242 3.5MN 530.71 5.1003 5.100 5.100 0.4MO 6.67 0.0010 0-0.001 < 0.050 < 0.050<NA 12.97 -4.8096 0-4.810 < 0.080 < 0.080NI 88.99 5.0339 5.033 5.033 0.3P 9.11 15.0115 U-2.640 < 0.300 < 0.300PB 8.39 0.0212 U 0.021 < 0.050 < 0.050PT 6.95 1.4900 * 0.272 * 0.272 6.2S 20.41 -1.1668 0-1.805 < 5.000 < 5.000SB 10.22 0.0718 0-0.024 < 0.060 < 0.060SE 24.15 5.7674 4.685 4.685 1.5SI 9.37 -0.0800 0-0.130 < 0.300 < 0.300SN 6.11 0.2525 U 0.220 < 0.500 < 0.500SR 2249.55 5.0071 5.007 5.007 0.4TE 14.16 0.0947 0 0.095 < 0.200 < 0.200TI 9.97 -0.0110 0-0.011 < 0.050 < 0.050TL 27.54 5.2531 5.253 5.253 0.60 11.98 4.9832 4.951 4.951 0.5V 48.64 5.1152 5.115 5.115 0.1W 4.38 0.1626 * 0.163 * 0.163 8.0Y 10.29 0.0101 * 0.010 * 0.010 21.4ZN 183.07 5.1647 5.100 5.100 0.6
RRI03Z89
0.836__ _ _ _ _ _ _.__—. — .._,„». U.OJO Z.W ^^SB 12.11 1.1355 * 0.846 * 0.846 3.9 If '{ L IASI 44.73 5.3607 5.303 5.303 0.4 _£" *&'vSN 7.09 1.6579 * 0.936 * 0.936 2.7SR 503.84 1.0532 1.052 l.C'2 0.4TE 14.02 0.0"534 0 0.052 < 0 0 < 0.200TI 10.19 0.0142 0 0.014 < 0 • n < 0.050TL 8.30 0.8929 0.886 O.^S 0.5U 8.81 0.9891 * 0.758 * 0 ^58 2.0V 16.12 0.9001 0.900 0.900 1.2W 4.02 0.0030 U-0.007 < 0.100 < 0.100Y 10.00 0.0028 U 0.003 < 0.009 < 0.009ZN 37.97 0.8893 0.875 0.875 0.3
SAMPLE NO. 19 053-06B DIL( )WEIGHT 1 GRAMS VOLUME 4 ML
21:35:14 20-NOV-87 19 053-06B DIL
MV INT RAW CONC CONCEN DIL CORR RSD
AG 12.85 0.0044 U 0.004 < 0.036 < 0.009AL 12.39 -0.0590 U-0.059 < 0.800 < 0.200AS 6.11 0.0069 U 0.006 < 1.200 < 0.300AU 4.35 0.1067 0-0.037 < 0.800 < 0.200B 6.85 0,0592 0 0.059 < 2.400 < 0.600BA 13.17 0,0348 * 0.035 * 0.139 0.6<BE 6.50 0.0002 0 0.000 < 0.004 < 0.001<BI 3.12 -0.0938 0-0.094 < 3.200 < 0.800CA 115.85 20.0694 20.07 80.28 0.7CD 4.28 0.0038 * 0.003 * 0.013 165.4<CO 6.27 -0.0127 0-0.013 < 0.040 < 0.010<CR 7.02 -0.0010 0-0.001 < 0.036 < 0.009CO 27.16 -0.0181 0-0.018 < 0.040 < 0.010<FE 18.73 0.2479 0.248 0.991 0.0IN 4.09 0.0297 0 0.030 < 0.800 < 0.200K 8.20 1.5998 * 0.491 * 1.962 7.5LI 11.35 -0.0028 0-0.003 < 0.080 < 0.020MG 16.55 3.9310 3.931 15.72 1.2MN 19.95 0.1233 0.123 0.492 0.7MO 6.55 -0.0069 0-0.009 < 0.200 < 0.050NA 32.26 4.1086 4.109 16.43 1.7NI 5.70 0.0057 0 0.004 < 0.080 < 0.020<P 2.98 0.0265 0 0.027 < 1.200 < 0.300PB 8.31 0.0031 0 0.003 < 0.200 < 0.050PT 5.20 0 0413 0-0.020 < 0.800 < 0.200S 79.62 3.1874 0 2.858 < 20.00 < 5.000<SB 9.36 -0.0572 0-0.057 < 0.240 < 0.060<SE 9.15 -0.0051 0-0.005 < 1.200 < 0.300SI 18.07 1.2581 * 1.258 * 5.033 1.0<SN 5 83 -rt 1477 0-0.148 < 2.000 < 0.500SR 71.52 0.0740 0.073 0.294 0.8TE 13.86 0.0103 0 0.010 < 0.800 < 0.200TI 9.90 -0.0197 0-0.020 < 0.200 < 0.050<TL 4.37 0.0015 0 0.002 < 0.360 < 0.090<0 7.97 -0.0629 0-0.063 < 2.000 < 0.500<V 9.13 -0.0060 0-0.006 < 0.080 < 0.020W 3.89 -0.0532 0-0.053 < 0.400 < 0.100<Y 9.92 0.0009 0 0.001 < 0.036 < 0.009ZN 7.29 -0.0148 0-0.015 < 0.024 < 0.006
56. 01IN 4.14 0.0703 0 0.070 < 0.200 < 0.200K 10.39 7.1221 4.211 4.211 0.4LI 11.71 0.0120 0 0.012 < 0.020 < 0.020MG 40.77 15.9626 15.96 15.96 0.2MN 56.89 0.4893 0.483 0.483 0.3MO 6.56 -0.0065 U-0.010 < 0.050 < 0.050NA 89.35 30.4904 29.96 29.96 0.6NI 5.77 0.0103 U 0.005 < 0.020 < 0.020P 3.01 0.0998 U 0.024 < 0.300 < 0.300PB 8.33 0.0079 U 0.008 < 0.050 , 0.050PT 5.33 0.1487 U 0.001 < 0.200 < 0.200S 260.43 16.4344 * 15.31 * 15.31 0.9SB 9.65 -0.0137 U-0.034 •< 0.060 < 0.060<SE 8.96 -0.0783 U-0.078 < 0.300 % 0.300SI 45.25 5.4407 5.389 5.389 0.3SN 6.08 0.2096 LI-0.049 < 0.500 <. 0.500SR 174.52 0.3073 0.306 0.306 0.4TE 14.08 0.0712 U 0.071 < 0.200 < 0.200TI 10.07 -0.0000 U-0.000 < 0.050 < 0.050<TL 4.34 -0.0053 0-0.005 < 0.090 v 0.090<0 8.05 0.0377 0 0.038 < 0.500 < 0.500<V 9.16 -0.0022 0-0.002 < 0.020 <. 0.020W 3.91 -0,0444 0-0.046 < 0.100 < 0.100Y 10.08 0.0049 U 0.005 < 0.009 < 0.009ZN 8.27 0.0140 * 0.012 * 0.012 5.8
.11
SAMPLE NO. 17 053-07B PD SPK( )WEIGHT 1 GRAMS VOLUME 1 ML
21:30:16 20-NOV-87 17 053-07B PD SPK
MV INT RAW CONC CONCEN DIL CORR RSD
AG 27.63 0.9005 0.900 0.900 0.8AL 44.94 8.9478 8.927 8.927 0.4AS 7.00 0.9362 * 0.859 * 0.859 6.6AU 4.53 0.1764 U-0.016 < 0.200 < 0.200B 9.44 1.0601 * 0.898 * 0.898 0.6BA 68.89 0.9528 0.953 . 0.953 0.6BE 240.93 0.8891 0.888 0.888 0.5BI 3.37 0.1993 0 0.195 < 0.800 < 0.800CA 390.20 78.4194 78.42 78.42 0.5CD 26.41 0.8741 0.860 0.860 0.4CO 23.89 0.8397 0.839 0.839 0.6CR 21.39 0.8632 0.861 0.361 0.3CO 67.79 0.8739 0.873 0.873 0.6FE 278.55 9.5672 9.567 9.567 0.6IN 4.14 0.0675 0 0.059 < 0.200 < 0.200K 13.91 16.0336 12.55 12.55 0.7LI 33.07 0.8766 0.877 0.877 0.6MG 48.53 19.3159 19.81 19.81 0.5MN 163.95 i.b265 1.526 1.526 0.5MO 6.69 0.0025 0-0.003 < 0.050 < 0.050NA 75.46 24.0725 23.41 23.41 0.8NI 19.84 0.8597 0.855 0.855 0.5P 4.21 3.0235 0-0.698 < 0.300 < 0.300PB 12.01 0.8757 0.869 0.869 3.7PT 5.70 0.4572 0 0.066 < 0.200 < 0.200S 212.09 12.9294 * 11.69 * 11.69 0.6SB 15.51 0.8662 0.819 0.819 4.1
Q SE 12.04 1.1073 * 0.824 * 0.824 4.8SI 44.18 5.2751 5.217 5.217 0.6SN 7.13 1.7151 * 0.998 * 0.998 7.2SR 495.03 1.0333 1.032 1.032TE 14.22 0.1115 U 0.110 < 0.200
1<BE 6.39 -0.4002 U-0.000 < .001 cBI 3'34 0.1680 U 0.167 < r, son n annCA 360.75 72.1566 72.16 ?_ ?6 ' o'f<CD 4.12 -0.0024 U-0.002 - o 003<CO 6.32 -0.0103 U-0.010 < o'S 0 < oCR 7.06 0.0012 U 0.000 < 0 009 - SCU 27.99 o.OOOl U-0.000 , 0 010 : o0FE 39.98 l.niOl 1.010 ' i S 0 ' 07IN 412 0.0540 U 0.054 J 0 2 0 0 '0200K 10.04 6,2363 3.916 T qje ' °'o°°LI 11.96 0.0220 * 0.022 * 0 02? \1
.5:S.7 8-?:l!?S5 "1,11 ' •« ;
. e i _•SB 9.55 -0.0282 0-0.047 < o 060 - O'If „•:!! -J:SI1 "?:?•} « : =f -ii si ; i ; I
:{ -o°:.°;U SI:.0?? J S.-gj 1:.a 4:,°SJ g4:.°S .< 0°:?o2S J :.s:jsj jsrj «
SAMPLE NO. 15 053-05B
WEIGHT 1 GRAMS VOLUME 1 ML
21:25:24 20-NOV-87 15 053-05B
MV INT RAW CONC CONCEN DIL CORR RSD
AG 12.89 0.0069 U 0.007AL 12.71 0.0286 U 0.015As 6.10 0.0000 0-0.016Au 4.48 0.1580 0-0.020B 7,65 0.3692 U 0.213RA 13.12 O.U64 0.116
<BE H.44 -U.OOUU 0-0 000B! 3.27 0.0821 U 0.081CA 399,07 80.3052 80.31CD 4.24 0.0025 0-0.001
<CO 6.29 -0.0119 0-0 012CR 7.07 0.0022 0 0,001CO 28.05 0.0015 0 0.001FE 65.02 1.9081 _ 908IN 4.26 0.1675 0 0 167K 10.16 6.5572 3.862" 11-72 0.0123 0 0.012MG 37.87 14.5220 14.52MN 52.97 0.4452 o 445
SAMPLE NO. 12 053-02B( )WEIGHT 1 GRAMS "" VOLUME 1 ML
21:18:04 20-NOV-87 12 053-02B
MV INT RAW CONC CONCEN DIL CORR RSD
AG 13.05 0.0166 * 0.017 ""* 0.017 38.8AL 12.84 0.0655 U 0.053 < 0.200 < 0.200AS 6.12 0.0173 U 0.006 c 0.300 < 0.300AU 4.53 0.1777 U-0.015 < 0.200 < 0.200B 7.32 0.2419 U 0.088 < 0.600 < 0.600BA 15.66 0.0759 0.076 0.076 0.6<BE 6.42 -0.0001 U-0.000 < 0.001 < 0.001BI 3.29 0.1055 U 0.105 < 0.800 < 0.800CA 365.75 73.2200 73.22 73.22 0.2CD 4.22 0.0014 U-0.002 < 0.003 •; 0.003<CO 6.30 -0.0115 0-0.011 < 0.010 < 0.010CR 7.13 0.0056 U 0.004 < 0.009 < 0.009CO 28.53 0.0121 * 0.012 * 0.012 8.3FE 25.49 0.4903 0.490 0.490 2.8
<IN 4.04 -0.0135 0-0.014 < 0.200 < 0.200K 9.80 5.6467 3.366 3.366 2.2LI 11.48 0.0024 0 0.002 < 0.020 < 0.020MG 32.31 11.7567 11.76 11.76 0.5MN 74.44 0.6544 0.654 0.654 0.3MO 6.59 -0.0040 0-0.007 < 0.050 < 0.050NA 59.51 16.7025 16.19 16.19 0.5NI 6.18 0.0347 * 0.029 * 0.029 5.0P 3.14 0.4256 0-0.319 < 0.300 < 0.300PB 8.28 -0.0047 0-0.005 < 0.050 <. 0.050PT 5.39 0.2038 0 0.020 < 0.200 < 0.200S 214.88 13.1343 * 12.06 * 12.06 0.6<SB 9.46 -0.0417 0-0.042 < 0.060 < 0.060<SE 9.11 -0.0192 0-0.019 < 0.300 < 0.300SI 55.51 7.0194 7.018 7.018 0.4SN 5.95 0.0286 0-0.016 < 0.500 < 0.500SR 113.70 0.1696 0.168 0.168 0.3TE 13.97 0.0394 0 0.039 < 0.200 < 0.200TI 10.13 0.0071 0 0.007 < 0.050 < 0.050<TL 4.30 -0.0136 0-0.014 < 0.090 < 0.0900 8.10 0.1006 0-0.083 < 0.500 < 0.500<V 9.20 0.0026 0 0.003 < 0.020 < 0.020W 3.99 -0.0104 0-0.011 < 0.100 < 0.100<Y 9.93 0.0012 0 0.001 < 0.009 < 0.009ZN 8.11 0.0094 * 0.007 * 0.007 6.1
SPECTRO TEMPERATORE = 40.490 30.000 TO 40.000SAMPLE NO. 13 053-03B( )WEIGHT 1 GRAMS VOLOME 1 ML
21:20:32 20-NOV-87 13 053-03B
MV INT RAW CONC CONCEN DIL CORR RSD
<AG 12.80 0.0014 0 0.001 < 0.009 < 0.009AL 12.53 -0.0212 0-0.034 < 0.200 < 0.200AS 6.14 0.0347 0 0.024 < 0.300 < 0.300AU 4.34 0.1041 0-0.072 < 0.200 < 0.200B 7.08 0.1479 0-0.005 < 0.600 < 0.600BA 15.50 0.0732 0.073 0.073 0.2<BE 6.38 -0.0002 0-0.000 < 0.001 < 0.001 « r>Q OBI .3.28 0.0938 00.093 < 0.800 < 0 . 800 ft D i Q 0 C- " "'CA 345.76 68.9685 68.97 68.97 0.3 H*v
r 1SPECTRO TEMPERATORE = 40.620 30.000 TO 40.000SAMPLE NO. 10 3711053-013(Q)WEIGHT 1 GRAMS VOLUME 1 ML
21:13:01 20-NOV-87 10 8711053-01B
MV INT RAW CONC CONCEN DIL CORR RSD
AG 12.95 0.0105 * 0.011 * 0.011 24.5AL 20.46 2.1747 2.175 2.175 0.8AS 6.17 0.0659 U 0.023 •-' 0.300 < 0.300AU 4.56 0.1909 0-0.022 < 0.200 <: 0.200B 7.55 0.3293 U 0.076 < 0.600 < 0.600BA 18.77 0.1270 0.127 0.127 0.2BE 6.78 0.0013 U 0.000 < 0.001 < 0.001BI 3.36 0.1954 U 0.138 c 0.800 < 0.800CA 432.44 87.4031 87.40 87.40 0.4<CD 4.21 0.0012 U 0.001 < 0.003 < 0.003<CO 6.37 -0.0079 0-0.008 < 0.010 < 0.010CR 7.19 0.0092 U 0.007 c 0.009 < 0.009CU 45.35 0.3812 0.380 0.380 0.5FE 415.51 14.4798 14.48 14.48 0.6IN 4.10 0.0324 U 0.019 < 0.200 <. 0.200K 10.80 8.1675 4.683 4.683 2.5LI 11.62 0.0081 U 0.008 < 0.020 -' 0.020MG 48.50 19.8010 19.79 19.79 0.5MN 58.33 0.4974 0.496 0.496 0.5MO 7.31 0.0434 U 0.039 < 0.050 < 0.050NA 65.96 19.6835 18.94 18.94 0.8NI 6.38 0.0472 * 0.039 * 0.039 7.4P 3.76 1.9322 0-0.093 < 0.300 < 0.300PB 8.75 0.1060 * 0.106 * 0.106 2.2PT 5.35 0.1680 U 0.015 < 0.200 •: 0.200S 262.19 16.6136 * 15.38 * 15.38 0.7SB 9.69 -0.0072 0-0.032 < 0.060 < 0.060<SE 9.12 -0.0167 0-0.017 < 0.300 < 0,300SI 71.63 9.4992 9.442 9.442 0.4SN 6.60 0.9624 0-0.058 < 0.500 < 0.500SR 200.67 0.3665 0.365 0.365 0.6TE 13.71 -0.0337 0-0.034 < 0.200 < 0.200TI 10.52 0.0532 * 0.053 * 0.053 4.4<TL 4.31 -0.0113 0-0.011 < 0.090 < 0.0900 8.09 0.0880 0-0.024 < 0.500 < 0.500
<V 9.20 0.0022 0 0.002 < 0.020 < 0.020W 4.12 0.0488 0 0.034 < 0.100 < 0.100Y 10.17 0.0070 0 0.007 < 0.009 < 0.009ZN 19.16 0.3350 0.330 0.330 0.6
SPECTRO TEMPERATURE = 40.580 30.000 TO 40.000SAMPLE NO. 11 053-01B PD DUP(D)WEIGHT 1 GRAMS VOLUME 1 ML
21:15:31 20-NOV-87 11 053-01BPDDUP Q Q\*
MV INT RAW CONC CONCEN DIL CORR a Q \ VRST& " RPD AVG
SR 4G 64 0.0031 U O.UG3 0.003 -. 0.003TE 16.30 0.7489 * 0.228 * 0.223 12.9TI 10.13 0.0308 U 0.031 C 0,050 < 0.050TL 6.20 0.4109 U 0.052 < 0.090 < 0.090U 8.70 0.8089 0-0.524 < 0.500 < 0.500V 13.38 0.5.406 0.418 0.413 1.0W 4.90 0.4569 * 0.269 * 0.269 2.6Y 10.04 C.0011 U 0.001 < O.OU9 •- 0.009ZN 47.74 1.2047 0,889 u.889 0.9
£''tif
SAMPLE NO. 8 BLANK .6010) 11-13(B)WEIGHT 1 GRAMS VOLUME 1 ML
21:08:01 20-NOV-87 8 BLANK (60101 11-18
MV INT RAW CONC CONCEN DIL CORR RSD
<AG 12.78 -0.0018 U-0.002 < 0.009 < 0.009AL 12.60 0.1061 0 0.106 < 0.200 < 0.200AS 6.10 0.0139 U 0.014 •; 0.300 ' 0.300AU 4.42 0.0565 U-0.077 v 0.200 •- 0.200B 6.70 0.0733 U 0.073 < 0.600 ; 0.600BA 11.06 0.0044 U 0.004 < 0.009 v 0.009<BE 6.44 -0.0005 U-0.000 < 0.001 ••• 0.001<BI 3.20 -0.0078 0-0.008 < 0.800 c 0.800CA 21.48 2.2729 2.273 2.273 0.6<CD 4.18 -0.0014 U-0.001 «; 0.003 < 0.003CO 6.54 0.0056 U 0.006 < 0.010 < 0.010<CR 7.04 -0.0006 U-0.001 < 0.009 < 0.009CU 27.98 0.0240 * 0.024 * 0.024 1.9<FE 11.82 -0.2559 U-0.256 < 0.030 < 0.030<IN 4.06 -0.0270 U-0.027 < 0.200 < 0.200K 7.78 0.5564 U 0.036 < 0.300 < 0.300LI 11.42 0.0070 U 0.007 < 0.020 < 0.020MG 8.64 0.1672 * 0.167 , * 0.167 14.9MN 7.30 0.0010 U 0.001 < 0.003 < 0.003MO 6.68 0.0132 U 0.011 < 0.050 < 0.050NA 23.37 4.7017 4.702 4.702 0.1NI 5.62 0.0032 U 0.002 < 0.020 < 0.020P 3.00 0.0000 U-0.075 < 0.300 < 0.300PB 8.30 0.0157 U 0.016 < 0.050 < 0.050<PT 5.15 -0.0303 U-0.030 < 0.200 < 0.200S 37.07 1.4073 U 1.349 < 5.000 < 5.000SB 9.79 0.0490 U 0.041 < 0.060 < 0.060
i <SE 9.16 -0.0526 0-0.053 < 0.300 < 0.300j SI 10.22 0.1990 0 0.149 < 0.300 < 0.300
<SN 5.93 -0.0048 0-0.005 < 0.500 < 0.500SR 38.99 0.0044 * 0.004 * 0.004 2.8
__ TE 13.83 0.0534 0 0.053 < 0.200 < 0.200U TI 10.07 0.0237 0 0.024 < 0.050 < 0.050
<TL 4.36 -0.0053 0-0.005 < 0.090 < 0.090<0 8.OS -0.0419 U-0.042 < 0,500 < 0.500<V 9.18 -0.0035 U-0.003 < 0.020 < 0.020W 4.01 0,0606 U 0.061 < 0.100 < 0.100<Y 9.88 -0.0027 0-0.003 < 0.009 < 0.009ZN 7.80 0.0277 * 0.028 * 0.028 7.0
S 65.64 3.5079 U 3.345 < 5.1)00 -. 5.0uOSB 16.83 1.1050 1.083 1.083 1 3SE 12.48 1.2228 * 0.892 * 0.892 1.8SI 20.79 1.8249 1.770 1.770 0.7SN 5.95 0.0191 0-0.007 •; 0.500 v. 0.500SR 37.10 O.OOXU 0-0.000 -c 0.003 c 0.003<TE 13.60 -0.0103 0-0.010 < 0.2UO <- . 200TI 18.53 1.0253 1.025 1.025 0.3TL 8.63 0.9616 0.962 0.962 0.8
<-U 8.02 -0.0377 0-0.038 < u.5t)U •; 0.500V 16.81 0.9860 0.936 0.986 u.9W 3.96 0.0384 0 0.037 -. u.lOu o.lUO<Y 9.91 -0.0020 0-0.002 < 0.^09 , 'i.OO*ZN 41.25 1.0134 1.000 l.fHiti 06
SAMPLE NO. tf CAL BLANK( )WEIGHT 1 GRAMS VOLOME 1 ML
SAMPLE NO. 6 CAL BLANK( IWEIGHT 1 GRAMS VOLOME 1 ML
21:03:06 20-NOV-87 6 CAL BLANK
MV INT RAW CONC CONCEN DIL CORR RSD
<AG 12.73 -0.0048 U-0.005 < 0.009 - 0.009<AL 11.97 -0.0692 U-0.069 < 0.200 -. 0.200AS 6.10 0.0139 0 0.014 < 0.300 •; 0.300AO 4.29 0.0066 0 0.007 < 0.200 < 0.200B 6.51 0.0013 U 0.001 < 0.600 < 0.600BA 10.86 0.0012 0 0.001 < 0.009 < 0.009<BE 6.43 -0.0005 0-0.001 < 0.001 < 0.001<BI 3.17 -0.0391 0-0.039 < 0.800 < 0.300<CA 10.76 -0.0085 0-0.009 < 0.060 < 0.060<CD 4.17 -0.0020 U-0.002 < 0.003 < 0.003<CO 6.26 -0.0076 0-0.008 < 0.010 < 0.010<CR 6.89 -0.0092 0-0.009 < 0.009 < 0.009<CU 26.74 -0,0033 U-0.003 < 0.010 < 0.010<FE 6.96 -0.4303 0-0.430 < 0.030 < 0.030<IN 4.07 -0.0135 0-0.014 < 0.200 < 0.200<K 7.46 -0.2445 0-0.244 < 0.300 < 0.300• LI : i . l H -'r ^O'-H t)-0,.?n.1 • 0. •'.•;",) -; •'-CO
NI "- "•' / t.'iv) :i i.i. u 1 I '.i .);;'• • ; .,p :' - -- "'!f.H I l - - i l <0h . ,, n,,'..', , „"."
<PB 6.14 -n.ui;o4 0-0.U2U ^ G.ObO •- ,) i:60<PT 5.13 -0.0413 0-0.041 < 0.200 < 0*200S 18.51 0.0419 0 0.014 < 5.000 < 5 000SB 9.71 0.0370 U 0.037 < 0.060 < 0 060<SE 9.12 -0.0680 0-0.068 < 0.300 < 0 300<SI 8.84 -0.0133 U-0.013 < 0.300 ' < 0 300<SN 5.85 -0.1143 0-0.114 < 0.500 < 0.500<SR 36.66 -0.0009 U-0.001 < 0.003 < 0 003<TE 13.55 -0.0244 0-0.024 < 0.200 < 0 200<TI 9.83 -0.0047 0-0.005 < 0.050 < 0 050<TL 4.30 -0.0204 0-0.020 < 0.090 < 0 090<U 8.00 -0.0629 0-0.063 < 0.500 < 0 500,<V .9.12 -0.0117 0-0.012 < 0.020 < o'o2W 3.89 0.0059 0 0.006 < 0.100 < Q' '
<FE 13.33 -0.2018 U-0.202 < 0.030 •.' 0.030 '' & I *14.06 -0.0243 0-0.024 < 0 200 < 0.2oSr ^ ' I
K 7.76 0.5143 * 0.514 * 0 514 9.8LI 11.63 0.0155 U 0.016 < 0.020 < 0.020<MG 8.29 -0.0066 0-0.007 < 0.100 < 0.100MN 7.40 0.0019 U 0.002 < 0 003 < 0 003MO 8.12 0.1076 * 0.108 * O.loS 27.1NA 15.27 0.9567 0.957 0.957 4.6NI 5.59 0.0010 U 0.001 < 0.020 < 0.020P 3.01 0.0244 0-0.561 < 0.300 < 0.300PB 8.40 G.G408 U 0.041 -. 0.050 v 0.050<PT 5.11 -0.0578 U-0.058 < 0.200 < 0.200S 25.90 0.5859 U 0.556 < 5.000 •. 5.000>SB 76.66 10.0830 10.08 10.08 2.5SE 11.32 0.7783 0-0.229 < 0.300 < 0.300SI 9.43 0.0769 0-0.007 < 0.300 < 0.300SN 12.81 9.8333 9.833 9.833 1.6SR 37.87 0.0019 U 0.002 < 0.003 < 0.003TE 14.64 0.2812 * 0.281 * G.281 50.6TI 10.04 0.0205 U 0.021 < 0.050 < 0.050<TL 4.31 -0.0181 U-0.018 < 0.090 < 0.090U 8.06 0.0042 U-0.028 < 0.500 < 0.500V 9.34 0.0169 U 0.017 < 0.020 < 0.020W 3.98 0.0488 U 0.049 < 0.100 < 0.100Y 10.06 0.0017 U 0.002 < 0.009 . <- 0.009ZN 7.72 0.0255 * 0.024 ' * 0,024 10.7
SAMPLE NO. 4 EPAICP-7( )WEIGHT 1 GRAMS VOLUME 1 ML
20:56:50 20-NOV-87 4 EPAICP-7
MV INT RAW CONC CONCEN DIL CORR RSD
AG 28.69 0.9627 0.963 0.963 0.8AL 15.66 0.9509 * 0,951 * 0.951 2.4AS 6.11 0.0208 U 0.018 < 0.300 < 0.300AO 4.32 0.0171 0-0.122 < 0.200 < 0.200B 9.20 1.0382 * 1.038 * 1.038 2.0BA 72.36 1.0143 1.014 1.014 0.9
<BE 6.55 -0.0001 0-0.000 < 0.001 < O.OOl'<BI 3.18 -0.0234 0-0.023 < 0.800 < 0.800CA 10.95 0.0326 0 0.033 < 0.060 < 0.060<CD 4.19 -0.0010 0-0.001 < 0.003 < 0.003<CO 6.29 -0.0065 0-0.006 < 0.010 < 0.010•-CR 6.97 -0.1044 U-0.004 < 0.009 . 0.0,19'ilt.! /n • . ,;>... -.:-;! .!(,:;. I;.: ;. •)!>;
FE >•• '-...' -4-.)n ••• ••• 44-, : . ':. . .. •-.IN 4 r, • ' * 7 : u i.;-:-: . , . ,, .. ..;:,.K ! 1 . 4, .-i, ?.>.!•!:; S. ciTil
^LI 'l i A -.1 ot'i'. 4 i i - u .jui•.Wt A •'.". u 11 [.32 n-o.ma .<MN Y . I / -U.UUU..H U-U.UUO •. U.UU3 < U.OU3MO 6.75 0.0178 0 0.018 < 0.050 < 0.050NA 14.22 0.4699 0.470 0.470 2.5<NI 5.51 -0.0038 0-0.004 < 0.020 < 0.020<P 2.98 -0.0570 0-0.057 < 0.300 < 0.300<PB 8.16 -0.0157 0-0.016 < 0.050 < 0.050<PT 5.12 -0.0496 0-0.050 < 0.200 < 0.200S 19.81 0.1380 0 0.136 < 5.000 < 5.000SB 11.86 0.3592 0.350 0.350 13.6<SE 9.05 -0.0975 0-0.098 < 0.300 < 0.300SI 15.06 0.9442 * 0.893 * 0.893 1.9<SN 5.85 -0.1191 U-0.119 < 0.500 < 0.500SR 37.32 0.0006 00.000 < Ol«p3 ft Q 9 CB.?03
-<TE 13.53 -0.0291 0-0.029 < M §00 ^ *-* V" V. 200TT Q O * T r* n r» n A T T n n A O / - n r \ - ; r t x n n c n
<AS 6.05 -0.0381 0-0.038 < 0.300 < 0.30-^AU 4.33 0.0223 0-0.110 < 0.200 < 0.200<B 6.40 -0.0399 0-0.040 < 0.600 < 0.600BA 10.96 0.0028 0 0.003 < 0.009 < 0.009<BE 6.30 -0.0010 0-0.001 < 0.001 < 0.001<BI 3.16 -0.0547 0-0.055 < 0.800 < 0.800<CA 10.69 -0.0227 0-0.023 < 0.060 < 0.060<CD 4.13 -0.0033 0-0.003 < 0.003 < 0.003<CO 6.31 -0.0055 0-0.005 < 0.010 < 0.010<CR 6.94 -0.0066 U-0.007 < 0.009 < 0.009<CU 26.70 -0.0042 0-0.004 < 0.010 < 0.010<FE 14.45 -0.1618 0-0.162 < 0.030 < 0.030<IN 4.04 -0.0405 0-0.041 < 0.200 < 0.200K 7.56 0.0084 U 0.008 < 0.300 < 0.300<LI 11.11 -0.0054 0-0.005 < 0.020 < 0.020<MG 8.18 -0.0613 0-0.061 < 0.100 < 0.100<MN 7.17 -0.0002 U-0.000 < 0.003 < 0.003MO 6.52 0.0026 U 0.003 < 0.050 < 0.050<NA 12.10 -0.5068 0-0.507 < 0.080 < 0.080NI 5.59 0.0014 0 0.000 < 0.020 < 0.020<P 2.98 -0.0570 U-0.057 < 0.300 < 0.300>PB 50.67 10.0008 10.00 10.00 0.6<PT 5.08 -0.0881 0-0.088 < 0.200 < 0.200S 19.49 0.1142 0 0.114 < 5.000 < 5.000<SB 9.22 -0.0375 0-0.038 < 0.060 < 0.060<SE 9.04 -0.1014 0-0.101 < 0.300 < 0.300SI 9.11 0.0282 0 0.028 < 0.300 < 0.300<SN 5.84 -0.1382 0-0.138 < 0.500 < 0.500<SR 36.62 -0.0010 U-0.001 < 0.003 < 0.003<TE 13.45 -0.0534 U-0.053 < 0.200 < 0.200<TI 9.83 -0.0043 0-0.004 < 0.050 < 0.050<TL 4.32 -0.0159 0-0.016 < 0.090 < 0.090<0 7.92 -0.1676 0-0.168 < 0.500 < 0.500<V 9.07 -0.0173 0-0.017 < 0.020 < 0.020<W 3.85 -0.0089 0-0.009 < 0.100 < 0.100<Y 9.88 -0.0028 0-0.003 < 0.009 < 0.009ZN 6.87 0.0003 U 0.000 < 0.006 < 0.006
SPECTRO TEMPERATORE = 40.120 30.000 TO 40.000SAMPLE NO. 2 STD»3()WEIGHT 1 GRAMS VOLOME 1 ML
20:51:58 20-NOV-87 2 STD«3
MV INT RAW CONC CONCEN DIL CORR RSD
AG 13.98 0.0707 0.071 0.071 6.0AL 12.81 0.1632 U 0.163 < 0.200 < 0.200AS 15.83 10.1321 10.13 10.13 0.7AO 29.32 9.8751 9.741 9.741 0.3B 31.67 9.7131 9.713 9.713 0.3BA 613.10 9.9227 9.923 9.923 0.6BE 2606.76 9.8587 9.859 9.859 0.6BI 11.72 9.9883 9.988 9.988 0.9CA 13.86 0.6515 0.652 0.652 1.3CD 259.09 10.0229 9.887 9.887 0.3CO 210.54 9.8787 9.879 9.879 0.3CR 171.00 9.8606 9.855 9.855 0.3CU 475.54 9.8504 9.850 9.850 0.5<FE 10.88 -0.2897 0-0.290 < 0.030 < 0.030IN 16.10 9.7379 9.738 9.738 0.3
>K 58.83 129.6940 129.1 129.1 0.5LI 255.33 9.8813 9.881 9.881 0.7MG 9.73 0.7071 0.707 0.707 4.9MN 1019.70 9.8661 9.866 9.866 0.4•MO 157.06 9.9177 9.916 9.916 0.7
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INSTRUMENT LOG
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HC-IR RAW DATA
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QUALITY CONTROL SUMMARY
E I ement -^ Ana I yst ^ Date
Standard Cal Ibrat ion I n i t i a l QC Check Cont inu ing QC Check
Cone. Pk Height Measured Theo. j_ Rec. Measured Theo. i Rec
13*7Corr. Coef. ' 3 SSlope ________ * )3?int. _______ 135 137
OupI icates
Sample No. Sample Result Duplicate Result £RPD
Spikes
Spike + SampleSample No. Result Sample Result 'Spike Added % Recovery
03305
1
UI
e a1
oo
llH
oo10
filtf* *
i(Atn u.
Cf
vi
8
doDC
r-
)6
o ®
< Q.
spl»**>— 4- 5
*« *•s:iLJjM4j^ 9N C 4-
— N -I85. 2
3 -»
O JlX •»- 4-<*. or~1«4' 2• O CBCM « I*** 4- 3 —~ C -O +-$ U 0 •</) U — >^ o .a —*-• a. <o •*•
^ a__iaM M N
QC SummaryPage 2
2. Inorganic Carbon Mode
Sample. .N2aC03 Run #1 11.30 10.04 88.8
*2 11.30 11.17 98.8#3 11.30 9.04 80.0#4 11.30 11.67 103.3
flRI03307
METHOD
OPERATING MODEMODE MODE SELECTED
ELEMENT MODE: CHN(1) SULFUR<2) OXYGEN(3) 1PRINTER? (Y/N) YAUTOSAVE? (Y/N) YBALANCE? (Y/N) NMANUAL BLANK-AV? (Y/N) NMANUAL K-AV? (Y/N) NCHANGE CRIT? (Y/N) N
0;77Ue
REVIEW RESULTS
n"v< ,H- • ' tj v «.DATA SELECTED - ''_"•* ———-£ ^
CARBON HYDROGEN NITROGEN r ' v •'-1 '• V'-f\[° BLANK O.O1 -0.02 1.1O ' ' \i \
KFACT 8.79 64.SO 1O.36#7 ' NA2C03 *£• WTX 10.04 -O.27 O.72#S^CAC03 KFACT 19.60 64.50 1O.36#9 NA2C03 # WTX 11.17 -0.27 O.72#10 O8711O54-O5A WTX O.05 -O.O1 O.O4#11 8711054-06A WTX O.O5 -O.O1 O.07#12 8711053-09A WTX O.O7 -0.01 0.3O .. / rj>~±#13 8711053-10A WTX 0.15 -O.O1 -O.O4 H O-"> -> '#14 8711O53-11A WTX O.16 -O.O2 O.29#15 8711053-12A WTX O.O8 -O.OO O.O3#16 6lC BLANK 0.02 -O.O2 O.96#17 NA2C03^C WTX 9.04 -O.23 -O.O1#18 8711O53-13A WTX O.17 -O.OO -O.ll#19 8711053-14A WTX 0.1O -O.OO -O.OO • <nO#20 8711053-15A WTX 0.14 -0.00 -0.08 (A J#21 S711O53-16A WTX1 ' O.36 -O.O1 -0.10#"" 8711053-17A WTX O. 16 -O.OO -0.17- ^* 8711053-17S WTX 6.O7- -O. 14 O.24-f • V. /v >'A'~\
4 8711053-17S2 WTX 7.41 -0.17 O.O1-.A <{..25 NA2CO3 < C WTX 11.67 -O.27 -O.OO
RADIANCORPORATION
Quality Control SummaryJob Number 1050, Mill Creek
Perkin Elmer Elemental AnalyzerTOC in soil assayed by difference analysis (Total Carbon less Total Inorgani'.Carbon).
BLANKSInorganic Carbon Tests Cart_QH_Uy.Blank (Run No. 5) 0.01Blank (Run No. 16) 0.02
Total Carbon Test SeriesBlank #1 0.05Blank *2 0.03
MS/MSP
The organic carbon spike was acetanilde.Sample tt 06585
>le_IE .__ SasiEle. Elks ge fivejcz M>1££ BEE
Matrix Spike (MS) 1.56 70.13 67.55 94%3%
Matrix SpikeDuplicate I.MSD) 1.56 49.25 49.38 97%
1. Total Carbon Mode
%CarbonKHP Run 1*1 47.05 46.49 98.8
*2 47.05 45.77 97.3#3 47.05 45.84 y7 4*4 47.05 46.46 98.7tf5 47.05 48.19 102.4
RR103309
ROY F. WESTOW-REACGSA Raritan Depot, Building 209, Bay F
Woodbridge Avenue, Edison, New Jersey 08817
November 9, 1987
Radian CorporationS501 Mo-Pec Blvd.Austin, Texas 78720-1008
Attn: Robert Richardson
Dear Rob,
As per our conversation on November 6, 1987, six (6) water and nine(9) sediment samples have been shipped to your laboratory foranalysis.The analyses to be performed are as follows:
PP Metals Base/Neutral Acids ExtractablePCB Total Petroluem HydrocarbonVOA TOCGrain Sizing (Sieve & Hydrometer)
The analyses are to be performed according to EPA Federal Register,Methods for Chemical Analysis of Water and Wastes and EPA TestMethods for Evaluating Solid Waste, Sept.,1986 with a ContractLaboratory Program (CLP) type data package. The QA/QC requested is10% matrix spike/matrix spike duplicate (MS/MSD) on all samplesanalysis except Grain Sizing, which will only get a duplicate.The Grain Sizing analysis is the lowest priority to be performed, soif extra sample is needed to perform other tests use the Grain Sizesample jars.
The final report is due 15 working days from receipt of samples inyour lab or December 3,1987.
The data package for the GC/MS should include:
1. Spectra and tabulation of ions for DFTPP for every twelve ortwenty-four hours of analysis.
2. Total ion chromatograms for every blank, standard, sample, andmatrix spike.
3. Spectra for standards of any compounds with sample hits.
^ 3 f
4. Spectra for hits in samples.
5. Response tabulation for each point in the most recently analyzedcalibration range.
6. Response factors for each daily check standard.7. All surrogate and"internal standards must be clearly labeled on
the total ion chromatograms.8. Each data sheet and chromatogram of spectrum must be clearly
labeled with the sample identity and date and time of analysisplus dilution and/or concentration factors.
9. All sample analysis results must be presented in tabulated form-data sheets alone are not acceptable.
10. All surrogate standards recoveries must be presented in tabulatedform. -
11. Sample matrix spikes must be presented in tabulated form.12. Instrument and method detection limit for each parameter.
The data package for gas chromatographic analysis should include:
1. Clearly labeled copies of the most recent calibration range forthe compounds of interest.
2. A list of instrument and method detection limits for eachcompound analyzed.
3. Chromatograms of all samples, daily standards and blanks. Allchromatograms must be clearly labeled with the standard or sampleidentity, date and time and dilution/concentration factors. Onestandard for each parameters must be analyzed for every twelvehours of analysis.
4. All instrument conditions including oven temperature, detectortemperature and type, column, sensitivity and chart speed.
5. Tabulation of sample results.6. Tabulation of any internal and/or surrogate standard results.
Data package for the PP Metals analysis should include:
1. Copies of the analysts notebook that show not only results butstandard curve used.
2. A list of instrument and method detection limits for eachcompound analyzed.
3. Copy of sample digestion method.4. Tabulated matrix spike and duplicate results.5. Tabulated sample results.6. All instrument printouts and notebook pages for standard curve.
The data package for the remaining analyses should include:
1. Copies of all analyst's notebook data.2. Tabulated sample results.3. Tabulated duplicate results.4. Copy of standard curve used.5. Copies of all raw data.
s rirj rSo1.?; sr r:? -- * *>i«. The Price is nocattached chain of custody an"5 return ^alyses' .Please sign theby December 3, 1987. Results sJoulS me Wlth the final reportaddress: results snould be sent to me at the following
ROY F. WESTON - REACGSA Raritan Depot, Bldg 209 RJ»,, «-woodbriage Avenue, E*ilm^ea B ay .^
p*««".5',.rijtqif;sjrs;."5S?bl—concern ing the —^—.Sincerely,
therine Paolino
3 3
REAC SUPPORT ORGANIZATIONGSA RARITAN DEPOTWOODBRIDGE AVENUEBUILDING 209. BAY FEDISON. NJ 08837
MANAGERS \ ^ DESIGNEflS/CONSUI.TANTS PHONE: 201-906-0369
DATE: January 5, 1987
TO: David ChartersU.S. EPA ERT
FROM: Michael A.REAC QA Officer
SUBJECT: MILLCREEK, PENNSYLVANIA ANALYTICAL REPORT STATUS3347-01-01-1050
The purpose of this memo is to document the events which have caused thedelay in the release of the analytical report for sampling conducted atthe Millcreek site on November 3-5, 1987.
Our laboratory services subcontractor, Radian Corporation, failed to sendus a complete data package describing organic analyses procedures.Volatiles were calibrated on two different days by the lab. The VOAcalibration documentation received by REAC was incomplete for both ofthose days. The entire VOA package for sample 6578 was also omitted fromthe labs report. As a result, it was not possible for us to validate VOAdata. In addition, GC/MS tuning data was not supplied in the labs report,which made validation of BNA compound results impossible. This missinginformation was received by REAC today and we will proceed with our dataevaluation.
As of today, all solids TOC data is still undelivered. In reviewing thislab's overall data package, we had also discovered several miscalculationsand have been working with the lab to obtain revised data reportingpages. We anticipate that these remaining issues will be resolved byJanuary 19 and that we will deliver the final report to you by January22. Petroleum hydrocarbon and PCB data is currently approved forrelease. If you desire those results now, please contact Gary Buchanan.
cc: L. WhiteG. BuchananM. MurphyJ. Chang
eh/ski rka/m-05
ARI033I3
JfiN 04 '88 13:38 RhtDIAt, nUSTIN BLDG 4 ._ p.?
To: Kathy Paolino & Rene Cohen
From; Robert RichardsonRadian - Austin, TX
Res Update on project 1041/1050
1041 - TOO instrument vent down Thursday. Looks like samples will be runtoday.
MDL's sent to Marian Fed Ex. She should gat them today.
1050 - TOC's - see above
Volatiles - Ail data requested were in the 13/17 submitted. Theresponse tables for 11/4 and 12/8 were located behind the Sample 01'svolatile data package. To save you time, I will reassemble the package andforward to you tonight. Each part will be clipped separately and have anidentifing cover sheet attached.
Semi'a - We are preparing the DFTPP and Quant Rept's for shipmenttonight with the volatilea package.
Thanks,
Rob R. JAK4 t383S&A
RADIANC O R P O R A T I O N
DATA REPORTFOR
WESTON-REAC
JOB NO. 1050VOLUME 1
t i V10
s &/
8501 Mo-Pac Blvd./P.O. Box 201088/Austin, TX 78720-1088/(512) 454-4797
ARI033I5
CONTENTS
SECTION ITEM
VOLUME 2
5 RAW DATA
TOC
8270
8240
HC-IR
ATOMIC ABSORPTION
LEADTHALLIUM
ARSENICVOLUME 3
5 RAW DATA, CONT.
ATOMIC ABSORPTION, CONT.MERCURY
SELENIUM - 11/18SELENIUM - 11/28
ICPESPCB'S
LAB NOTES
CHROMATOGRAMS
RADIANC O R P O R A T I O N
DATA REPORTFOR
WESTON-REACJOB NO. 1050VOLUME 3
R t o _. i EDEC i o W!
8501 Mo-Pac Blvd./P.O. Box 201088/Austin, TX 78720-1088/(512) 454-4
C O R P O R A T I O N
Date: 01-04-88
Client: Roy F. Weston-ReacContact: Kathy Paolino
Radian ID: 87-11-053Reac Job No: 1050Site: Mill Creek, PA
Item: Resubmittal of Volatiles Data
R i . »: • * £ DJAN 5 19bj
8240 WATER SAMPLES
INCLUDES SURROGATE RECOVERIES
RR1033V9
79-01-6 Trichloroethene <2.0 <2.0 <2.o <2.o75-69-4 Trichlorofluoromethane <2.0 <2.0 <2.0 <2.'o75-70-7 Trichloromethanethiol N\A N\A N\A N\A96-18-4 1,2,3-Trichloropropana N\A N\A N\A N*108-05-4 Vinyl acetate <2 <25 <25 <JP75-01-4 vinyl chloride <2.o <2.o <2.o <2.o1330-20-7 Xylenes <2.0 <2.0 <2.0 <2.0
SURROGATE RECOVERIES (results in % recovery)
d4-l,2-dichloroethaane 96 112 122 120d8-toluene 97 104 101 99p-bromofuorobenzene 98 105 106 100
NOTES AND DEFINITIONS FOR THIS REPORT.N\A -STANDARD WAS NOT AVAILABLE; THE COMPOUND WAS SEARCHED.USING AN NBS LIBRARY OF 42,000 COMPOUNDS.
79-01-6 Trichloroethene 7.1 5.7 3.875-69-4 Trichlorofluoromethane <2.0 <2.0 <2.o75-70-7 Trichloromethanathiol N\A N\A N\A96-18-4 1,2,3-Trichloropropane N\A N\A N\A108-05-4 Vinyl acetate <2 <25 <2575-01-4 Vinyl chloride <2.0 <2.0 <2.o1330-20-7 xylene» <2.0 <2.o <2.o
SURROGATE RECOVERIES (results in % recovery)
d4-l,2-dichloro«thaane 104 108 94d8-toluene 97 91 97p-bromofuorobenzene 94 93 107
NOTES AND DEFINITIONS FOR THIS REPORT.N\A -STANDARD WAS NOT AVAILABLE; THE COMPOUND WAS SEARCHED.USING AN NBS LIBRARY OF 42,000 COMPOUNDS.
\0332i
PageClient: WESTON LABORATORIES 01A 6572 SOIL VOA
RADIAN INTERNAL 02A 6578 SOIL VOARADIAN INTERNAL 03A 6579 SOIL VOA
04A 6580 SOIL VOA
EPA METHOD 8240CAS # COMPOUND RESULTS IN ug/gLab No: A7-11-04101A 02A 03A 04A
67-64-1 Acetone <50 <50 <50 <5075-05-8 Acetonitrile <50 <50 <50 <50107-02-8 Acrolein <10 <10 <10 <10107-13-1 Acrylonitrile <10 <10 <10 <1071-43-2 Benzene <2.0 <2.0 <2.0 <2.075-25-2 Bromoform <2.0 <2.0 <2.0 <2.074-83-9 Bromomethane <2.0 <2.0 <2.0 <2.075-15-0 Carbon Disulfide <2.0 <2.0 <2.0 <2.056-23-5 Carbon Tetrachloride <2.0 <2.0 <2.0 <2.0108-90-7 Chlorobenzene <2.0 <2.0 <2.0 <2.0126-99-8 2-Chloro-1,3-butadiene N\A N\A N\A N\A"124-48-1 Chlorodibromomethane <2.0 <2.0 <2.0 <2.075-00-3 Chloroethane <2.0 <2.0 <2.0 <2.067-66-3 chloroform <2.0 <2.o <2.0 <2.o74-87-3 Chloromethane <2.0 <2.0 <2.0 <2107-05-1 3-Chloropropene <2.0 <2.0 <2.0 <210061-01-5 cis-l,3-Dichloropropene <2.0 <2.0 <2.0 <2.096-12-8 l,2-Dibromo-3-chloropropane <2.0 <2.0 <2.0 <2.0106-93-4 1,2-Dibromoethane <2.0 <2.0 <2.0 <2.075-95-3 Dibromomethane <2.0 <2.0 <2.0 <2.075-27-4 Dichlorobromomethane <2.0 <2.0 <2.0 <2.075-71-8 Dichlorodifluoromethane <10 <10 <10 <1075-34-3 1,1-Dichloroethane <2.0 <2.0 <2.0 <2.0107-06-2 1,2-Dichloroethane <2.0 <2.0 <2.0 <2.075-35-4 1,1-Dichloroethene <2.0 <2.0 <2.0 <2.078-87-5 1,2-Dichloropropane <2.0 <2.0 <2.0 <2.0100-41-4 Ethyl benzene <2.0 <2.0 <2.0 <2.075-21-8 Ethylene oxide N\A N\A N\A N\A97-63-2 Ethyl methacrylate <10 <10 <10 <10591-78-6 2-Hexanone <10 <10 <10 <1074-88-4 lodomethane <10 <10 <10 <1075-09-2 Methylene chloride <50 <50 <so <5078-93-3 Methyl ethyl ketone <50 <50 <50 <5080-62-6 Methyl methacrylate <10 <10 <10 <10108-10-1 4-Methyl-2-pentanone <10 <io ^nQ5-en-i «——._-_-••_ _—_- . *,«»*i.ajiw.iw <10 <10 <10 <1095-50-1 Propanenitrile N\A N\A N\A N\A100-42-5 Styrene <2.0 <2.0 <2.0 <2.0630-20-6 1,1,1,2-Tetrachloroethane <2.0 <2.0 <2.0 <2.079-34-5 1,1,2,2-Tetrachloroethane <2.0 <2.0 <2.0 <2.0127-18-4 Tetrachloroethylene <2.0 <2.0 <2.0 3.0108-88-3 Toluene <2.0 <2.0 <2.0 6.4t110-57-6 Trans-l,4-dichloro-2-butene <25 <25 <25 <25^156-60-5 trans-l,2-Dichloroethene <2.0 <2.0 <2..0 <2.010061-02-6 trans-l,3-Dichloropropene <2.0 <2.0 <2-.0 <2.o71-55-6 1,1,1-Trichloroethane <2.0 <2.0 <2.0 <2.079-00-5 1,1,2-Trichloroethane <2.0 <2.0 oq^0 <2.0
Page 2client: WESTON LABORATORIES OSA essi SOIL VOA
RADIAN INTERNAL 06A 6582 SOIL VOARADIAN INTERNAL 07A 6583 SOIL VOA
OSA 6584 SOIL VOA
EPA METHOD 8240CAS # COMPOUND RESULTS IN ug/g
Lab No: A7-11-041OSA 06A 07A OSA
67-64-1 Acetone <50 <50 <50 <5075-05-8 Acetonitrile <50 <50 <50 <50107-02-8 Acrolein <io <io <io <lo107-13-1 Acrylonitrile <lo <10 <io <io71-43-2 Benzene <2.0 <2.o <2.o <2.o75-25-2 Bromoform <2.0 <2.0 <2.o <2.o74-83-9 Bromomethane <2.0 <2.0 <2.0 <2.075-15-0 Carbon Disulfide <2.0 <2.0 <2.0 <2.056-23-5 Carbon Tetrachloride <2.0 <2.0 <2.0 <2.0108-90-7 Chlorobenzene <2.0 <2.0 <2.0 <2.0126-99-8 2-Chloro-1,3-butadiene N\A N\A N\A N\A124-48-1 Chlorodibromomethane <2.0 <2.0 <2.o <2.o75-00-3 Chloroethane <2.o <2.o <2.o <2.o67-66-3 Chloroform <2.o <2.0 <2.o <2.o74-87-3 Chloromethane <2.0 <2.0 <2.0 <2.o107-05-1 3-Chloropropene <2.0 <2.0 <2.0 <2.010061-01-5 cis-l,3-Dichloropropene <2.0 <2.0 <2.0 <2.o96-12-8 l,2-Dibromo-3-chloropropane <2.0 <2.0 <2.0 <2.0106-93-4 1,2-Dibromoethane <2.0 <2.0 <2.0 <2.075-95-3 Dibromomethane <2.0 <2.0 <2.0 <2.075-27-4 Dichlorobromomethane <2.0 <2.0 <2.0 <2.075-71-8 Dichlorodifluoromethane <10 <10 <10 <1075-34-3 1,1-Dichloroethane <2.0 <2.0 <2.0 <2.0107-06-2 1,2-Dichloroethane <2.0 <2.0 <2.0 <2.075-35-4 1,1-Dichloroethene <2.0 <2.0 <2.o <2.o78-87-5 1,2-Dichloropropane <2.0 <2.0 <2.0 <2.0100-41-4 Ethyl benzene <2.0 <2.0 <2.0 <2.075-21-8 Ethylene oxide N\A N\A N\A N\A97-63-2 Ethyl methacrylate <10 <10 <10 <lo591-78-6 2-Hexanone <10 <10 <10 <1074-88-4 lodomethane <10 <10 <10 <1075-09-2 Methylene chloride <50 <50 <50 <5078-93-3 Methyl ethyl ketone <50 <50 <50 <so80-62-6 Methyl methacrylate <10 <10 <io <lo108-10-1 4-Methyl-2-pentanone <10 <10 <10 <1095-50-1 Propanenitrile N\A N\A N\A N\A100-42-5 Styrene <2.0 <2.0 <2.0 <2.0630-20-6 1,1,1,2-Tetrachloroethane <2.0 <2.0 <2.0 <2.079-34-5 1,1,2,2-Tetrachloroethane <2.0 <2.0 <2.0 <2.0127-18-4 Tetrachloroethylene 2.8 <2.0 <2.0 <2.0108-88-3 Toluene <2.0 <2.0 <2.0 <2.0110-57-6 Trans-l,4-dichloro-2-butene <25 <25 <25 <25156-60-5 trans-i,2-Dichloroethen« <2.0 <2.0 <2.0 <2.010061-02-6 trans-l,3-Dichloropropene <2.0 <2.0 <2.0 <2.071-55-6 1,1,1-Trichloroethane <2.0 <2.0 <2.0 <2.079-00-5 1,1,2-Trichloroethane <2.0 <2.0 <2.0 <2.0
03323
Client: «ZSTOK ,„ SSS5 SOIL VOA
0
EPA METHOD 8240CAS # COMPOUND RESULTS IN ug/gLab No: A7-11-04109A 10A 11A
67-64-1 Acetone <50 <50 <5075-05-8 Acetonitrile <50 <50 <50107-02-8 Acrolein <10 <10 <10107-13-1 Acrylonitrile <10 <10 <1071-43-2 Benzene <2.0 3.0 <2.075-25-2 Bromoform <2.0 <2.0 <2.074-83-9 Bromomethane <2.0 <2.0 <2.075-15-0 Carbon Disulfide <2.0 <2.0 <2.056-23-5 Carbon Tetrachloride <2.0 <2.0 <2.0108-90-7 Chlorobenzene <2.0 <2.0 <2.0126-99-8 2 -Chloro-1, 3 -butadiene N\A N\A N\A124-48-1 Chlorodibromomethane <2.0 <2.0 <2.075-00-3 Chloroethane <2.0 <2.0 <2.067-66-3 Chloroform <2.0 <2.0 <2.074-87-3 Chloromethane <2.0 <2.0 <2.0107-05-1 3-Chloropropene <2.0 <2.0 <2.010061-01-5 cis-l,3-Dichloropropene <2.0 <2.0 <2.096-12-8 l,2-Dibromo-3-chloropropane <2.0 <2.0 <2.0106-93-4 1,2-Dibromoethane <2.0 <2.0 <2.075-95-3 Dibromomethane <2.0 <2.0 <2.075-27-4 Dichlorobromomethane <2.0 <2.0 <2.075-71-8 Dichlorodifluoromethane <10 <10 <1075-34-3 1,1-Dichloroethane <2.o <2.o <2.0107-06-2 1,2-Dichloroethane <2.0 <2.0 <2.075-35-4 1,1-Dichloroethene <2.0 <2.o <2.078-87-5 1,2-Dichloropropane <2.0 <2.0 <2.0100-41-4 Ethyl benzene <2.0 <2.0 <2.075-21-8 Ethylene oxide N\A N\A N\A97-63-2 Ethyl methacrylate <10 <10 <10591-78-6 2-Hexanone <10 <10 <1074-88-4 lodomethane <10 <10 <1075-09-2 Methylene chloride <50 <50 25078-93-3 Methyl ethyl ketone <50 <50 12080-62-6 Methyl methacrylate <10 <io <10108-10-1 4-Methyl-2-pentanone <10 <io <1095-50-1 Propanenitrile N\A N\A N\A100-42-5 Styrene <2.0 <2.0 <2.0630-20-6 1,1,1,2-Tetrachloroethane <2.0 <2.0 <2.o79-34-5 1,1,2,2-Tetrachloroethane <2.0 <2.0 <2.0127-18-4 Tetrachloroethylene <2.0 <2.0 <2.0108-88-3 Toluene <2.0 <2.0 <2.0110-57-6 Trans-l,4-dichloro-2-butene <25 <25 <25156-60-5 trans-l,2-Dichloroethene <2.0 <2.0 <2.010061-02-6 trans-l,3-Dichloropropene <2.0 <2.0 <2.071-55-6 1,1,1-Trichloroethane ,. t A £°U <2<0 ^?«°79-00-5 1,1,2-Trichloroethane j\RiU4d_t> <2.0
RADIANe o • i
MATRIX SPIKE DUPLICATE STUDY VOA (%)
Compound
1, 1-Dichloroethene
Toluene
Chlorobenzene
Benzene
Trichloroethene
6581 WaterA7 11 040-0 2
#1 n
86
112
111
94
83
92
113
111
91
86
ft:RlQ3325
8270 WATER SAMPLES
INCLUDES SURROGATE RECOVERIES
\Q3326
Client: WESTON LABORATORIES OSA 6584 WATERRADIAN INTERNAL 06A 6585 WATERRADIAN INTERNAL 07A SYSTEM BLANK
EPA METHOD 8270 Page 2CAS # COMPOUND RESULTS IN ug/LLab No: A7-11-038
OSA 06A 07A208-96-8 Acenaphthalene <10 <10 <1083-32-9 Acenaphthene <10 <10 <1098-86-2 Acetophenone <10 <10 <1053-96-3 2-Acetylaminofluorene <250 <250 <25092-67-1 4-Aoinobiphenyl <250 <250 <25062-53-3 Aniline <20 <20 <20•120-12-7 Anthracene <io <io <10140-57-8 Aramite N\A N\A N\A56-55-3 Benz(a)anthracene <10 <10 <10108-98-5 Benzenethiol N\A N\A N\A92-87-5 Benzidine <50 <50 <5050-32-8 Benzo(a)pyrene <10 <10 <10205-99-2 Benzo(b)fluoranthene <io <10 <10 ,191-24-2 Benzo(g,h,i)perylene <10 <10 <1065-85-0 Benzole acid <loo <100 <100207-08-9 Benzo(k)fluoranthene <io <10 <10106-51-4 p-Benzoquinone N\A N\A N\Aioo-si-6 Benzyl alcohol <20 <20 <20lll-91-i bis(2-Chloroethoxy)ethane <10 <10 <10111-44-4 bis(2-Chloroethyl)ether <10 <10 <10108-60-1 bis(2-chloroispropyl)ether <10 <10 <10117-81-7 bis(2-ethylhexyl)phthalate <10 <10 <10101-55-3 4-Bromophenyl phenyl ether <10 <10 <1085-68-7 butyl benzyl phthalate <10 <10 <1088-85-7 2-sec-butyl-4,6-dinitrophenol N\A N\A N\A106-48-7 p-Chloroanillne <200 <200 <200510-15-6 Chlorobenzilate N\A N\A N\A110-75-8 2-Chloroethyl vinyl ether N\A N\A N\A59-50-7 p-Chloro-m-cre»ol <10 <10 <1091-58-7 2-Chloronaphthalene <10 <10 <io95-57-8 2-chlorophenol <10 <10 <107005-72-3 4-Chlorophenyl phenyl ether <10 <10 <10218-01-9 Chrysene <10 <10 <1095-48-7 o-Creaol <10 <10 <10106-44-5 p-Cresol <10 <10 <10192-65-4 Dibenzo(a,e)pyrene N\A N\A N\A132-64-9 Dibenzofuran <10 <10 <1053-70-3 Dibenzo(a,h)anthracene <10 <10 <10189-64-0 Dibenzo(a,h)pyrene <10 <10 <10189-55-9 Dibenzo(a,i)pyrene N\A N\A N\A
ftB!03327
Page 4
Client: WESTON LABORATORIES OSA 6584 WATERRADIAN INTERNAL 06A 6585 WATERRADIAN INTERNAL 07A SYSTEM BLANK
EPA METHOD 8270CAS * COMPOUND RESULTS IN ug/L
Lab No: A7-11-038OSA 06A 07A
95-50-1 1,2-Dichlorobenzene <10 <10 <10541-73-1 1,3-Dichlorobenzene <10 <10 <10106-46-7 1,4-Dichlorobenzene <10 <10 <1091-94-1 3,3'-Dichlorobenzidine <20 <20 <20120-83-2 2,4-Dichlorophenol <10 <10 <1087-65-0 2,6-Dichlorophenol <10 <10 <1084-66-2 Diethylphthalate <10 <10 <1060-11-7 p-Dimethylaminoazobenzene <250 <250 <250119-90-4 3,3'-Dimethoxybenzidine <50 <50 <5057-97-6 7,12-Dimethylbenz(a)anthracene <20 <20 <20119-93-7 3,3'-Dimethylbenzidine <50 <50 <50122-09-8 2,2-Dimethylphenethylamine <250 <250 <250105-67-9 2,4-Dimethylphenol <10 <10 <10131-11-3 Dimethylphthalate <10 <10 <10100-25-4 1,4-Dinitrobenzene <100 <100 <100584-52-1 4,6-Dinitro-o-cresol <50 <50 <5051-28-5 2,4-Dinitrophenol <50 <50 <50121-14-2 2,4-Dinitrotoluene <10 <10 <10806-20-2 2,6-Dinitrotoluene <10 <10 <1084-74-2 Di-n-butylphthalate <10 <10 <10117-84-0 Di-n-octylphthalate <10 <10 <10621-64-7 Di-n-propylnitrosamine <10 <10 <10122-39-4 Diphenylamine <10 <10 <10122-66-7 1,2-Diphenylhydrazine <10 <10 <10206-44-0 Fluoranthene <10 <10 <1086-73-7 Fluorene <10 <10 <10118-74-1 Hexachlorobenzene <10 <10 <1087-68-3 Hexachlorobutadiene <10 <10 <1077-47-4 Hexachlorocyclopentadiene <10 <10 <1067-72-1 Hexachloroethane <10 <10 <1070-30-4 Hexachlorophene N\A N\A N\A1888-71-7 Hexachloropropene <10 <lo <10193-39-5 Indeno(l,2,3-c,d)pyrene <10 <10 <1078-59-1 Isophorone <10 <10 <10120-58-1 Isosafrole <100 <100 <10091-80-5 Methapyrilene N\A N\A N\A56-49-5 3-Methylcholanthrene <100 <100 <100101-14-4 4,4Methylnbis(2-chloroanilne) <200 <200 <20066-27-3 Methyl methanesulfonate <20 <20 <2091-57-6 2-Methylnaphthalene <10 <10 <10
0332
2-Fluorobiphenyl2,4,6-Tribromophenol 77 " JJ 78Terphenyl-dl4 ZJ "J 97 "«
70 85 81 81
ZS AND DEFINITIONS FOR THIS REPORT.
2-Fluorobiphenyl 83 74 662,4,6-Tribromophenol 100 110 looTerphenyl-dl4 81 82 69
.ES AND DEFINITIONS FOR THIS REPORT.N\A -STANDARD WAS NOT AVAILABLE; THE COMPOUND WAS SEARCHEDUSING AN NBS LIBRARY OF 42,000 COMPOUNDS.
03330
CORPORATION
MS/MSD RESULTS
0333V
Client: WESTON LABORATORIES OSA 6581 SOILRADIAN INTERNAL 06A 6582 SOILRADIAN INTERNAL 07A 6583 SOIL
08A 6584 SOIL
EPA METHOD 8270 Page 2CAS # COMPOUND RESULTS IN ug/g
Lab No: A7-11-043OSA 06A 07A OSA
208-96-8 Acenaphthalene <1.0 <1.0 <1.0 <1.083-32-9 Acenaphthene <1.0 <1.0 <1.0 <1.098-86-2 Acetophenone <1.0 <1.0 <1.0 <1.053-96-3 2-Acetylaminofluorene <25 <25 <25 <2592-67-1 4-Aminobiphenyl <25 <25 <25 <2562-53-3 Aniline <2.0 <2.0 <2.0 <2.0120-12-7 Anthracene <1.0 <l.o <i.o <l.o140-57-8 Aramite N\A N\A N\A N\A56-55-3 Benz(a)anthracene <1.0 <1.0 1.4 <l.o108-98-5 Benzenethiol N\A N\A N\A N\A92-87-5 Benzidine <5.0 <5.0 <5.0 <5.050-32-8 Benzo(a)pyrene <l.O <l.O 3.1 <l.o205-99-2 Benzo(b)fluoranthene <1.0 <1.0 1.7 <1.0191-24-2 Benzo(g,h,i)perylene <1.0 <1.0 <1.0 <1.065-85-0 Benzoic acid <10 <10 <10 <10207-08-9 Benzo(k)fluoranthene <1.0 <1.0 2.2 <1.0106-51-4 p-Benzoquinone N\A N\A N\A N\A100-51-6 Benzyl alcohol <2.0 <2.0 <2.0 <2.0111-91-1 bis(2-Chloroethoxy)ethane <l.O <1.0 <1.0 <l.O111-44-4 bis(2-Chloroethyl)ether <1.0 <1.0 <1.0 <1.0108-60-1 bis(2-chloroispropyl)ether <1.0 <1.0 <1.0 <1.0117-81-7 bis(2-ethylhexyl)phthalate <l.O <1.0 <1.0 <l.O101-55-3 4-Bromophenyl phenyl ether <1.0 <1.0 <1.0 <1.085-68-7 butyl benzyl phthalate <1.0 <1.0 <1.0 <1.088-85-7 2-sec-butyl-4,6-dinitrophenol N\A N\A N\A N\A106-48-7 p-Chloroaniline <20 <20 <20 <20510-15-6 Chlorobenzilate N\A N\A N\A N\A110-75-8 2-Chloroethyl vinyl ether N\A N\A N\A N\A59-50-7 p-chloro-m-cre»ol <l.o <l.o <i.o <i.o91-58-7 2-Oil or ©naphthalene <1.0 <1.0 <1.0 <1.095-57-8 2-Chlorophenol <l.O <1.0 <l.O <l.O7005-72-3 4-Chlorophenyl phenyl ether <1.0 <1.0 <1.0 <l.o218-01-9 Chrysene <1.0 <1.0 1.3 <1.095-48-7 o-Cresol <1.0 <1.0 <1.0 <1.0106-44-5 p-Cresol <1.0 <1.0 <1.0 <1.0192-65-4 Dibenzo(a,e)pyrene <5.0 <5.0 <5.0 <5.0132-64-9 Dibenzofuran <1.0 <l.O <l.O <l.o53-70-3 Dibenzo(a,h)anthracene <1.0 <l.O <l.o <i.o189-64-0 Dibenzo(a,h)pyrene <1.0 <l.o <l.o <i.o189-55-9 Dibenzo(a,i)pyrene <5.0 <5.0 <5.0 <5.o
Client: WESTON LABORATORIES 09A 6585 SOILRADIAN INTERNAL 10A SYSTEM BLANKRADIAN INTERNAL
EPA METHOD 8270CAS # COMPOUND RESULTS IN ug/g
Lab No: A7-11-04309A 10A
95-50-1 1,2-Dichlorobenzene <1.0 <1.0541-73-1 1,3-Dichlorobenzene <1.0 <1.0106-46-7 1,4-Dichlorobenzene <1.0 <1.091-94-1 3,3'-Dichlorobenzidine <2.0 <2.0120-83-2 2,4-Dichlorophenol <l.o <l.o87-65-0 2,6-Dichlorophenol <1.0 <1.0.84-66-2 Diethylphthalate <1.0 <1.060-11-7 p-Dimethylaminoazobenzene <25 <25119-90-4 3,3'-Dimethoxybenzidine <5.0 <5.057-97-6 7,12-Dimethylbenz(a)anthracene <2.0 <2.0119-93-7 3,3'-Dimethylbenzidine <5.0 <5.0122-09-8 2,2-Dimethylphenethylamine <25 <25105-67-9 2,4-Dimethylphenol <1.0 <1.0131-11-3 Dimethylphthalate <l.O <1.0100-25-4 1,4-Dinitrobenzene <10 <10584-52-1 4,6-Dinitro-o-cresol <5.0 <5.051-28-5 2,4-Dinitrophenol <5.0 <5.0121-14-2 2,4-Dinitrotoluene <1.0 <1.0806-20-2 2,6-Dinitrotoluene <1.0 <1.084-74-2 Di-n-butylphthalate <1.0 <1.0117-84-0 Di-n-octylphthalate <1.0 <1.0621-64-7 Di-n-propylnitrosamine <1.0 <1.0122-39-4 Diphenylamine <1.0 <l.o122-66-7 1,2-Diphenylhydrazine <l.O <1.0206-44-0 Fluoranthene <1.0 <1.086-73-7 Fluorene <l.o <l.O118-74-1 Hexachlorobenzene <1.0 <1.087-68-3 Hexachlorobutadiene <1.0 <1.077-47-4 Hexachlorocyclopentadiene <l.O <1.067-72-1 Hexachloroethane <1.0 <1.070-30-4 Hexachlorophene N\A N\A1888-71-7 Hexachloropropene <1.0 <1.0193-39-5 Indeno(l,2,3-c,d)pyrene <1.0 <l.O78-59-1 Isophorone <1.0 <1.0120-58-1 Isosafrole <10 <1091-80-5 Methapyrilene N\A N\A56-49-5 3-Methylcholanthrene <10 <10101-14-4 4,4Methylnbis(2-chloroanilne) <20 <2066-27-3 Methyl methanesulfonate <2.0 <2.091-57-6 2-Methylnaphthalene <1.0 <1.0
Page 6
Aftl0333"3
,2-Fluorobiphenyl x 74 69 82 842,4,6-Tribromophenol 89 78 51 95Terphenyl-dl4 76 69 76 si
AND DEFINITIONS FOR THIS REPORT.N\A -STANDARD WAS NOT AVAILABLE; THE COMPOUND WAS SEARCHEDUSING AN NBS LIBRARY OF 42,000 COMPOUNDS.
RADIANCO* » O««TI«M
DUPLICATE MATRIX SPIKE DATA, SEMIVOLATILE ANALYSIS (%)
6572 SoilA711043-07
Compound #1 #2
Phenol 59 52
2-Chlorophenol 59 54
1,4-Dichlorobenzene 50 47
N-nitroso-di-n-propylamine 60 55
1,2,4-Trichlorobenzene 48 47
4-Chloro—3-methylphenol 62 57
Acenaphthene 46 44
4-Nitrophenol 50 48
2,4-Dinitrotoluene 44 41
Pentachlorophenol 56 54
Pyrene 83 54
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FIELD DATA SHEETEnvironmental RwponM Team, InvlTC*****.! Protection Agency
w. Edtea. K(201) 521-9660
.ocatton: ____
f.Electors:Lab Number (Cooeec.*'!) Dale Coilectad Time <_« rw)
NO 6572SON. VKOeTATION OROOMDWATEM
Device
>pllt Spoon:yUnder Cup
>eptrtFtorIn.
Soil TypeRec*
SandClaySiltMuckLoamPeat
Upland-DryLowtwtd-OryFtoodplataWetlandQuHy
Slop* >15*
OldWooded IndustrialFwmland Comnwrc
W«_f Tabto Depth
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OBHColor..
Cotor .Odor .Oil: .Dtwica:.
SUMFACC WATIR PREPARATION
Twnp .•lor _ ——————— _ pH
• REAM Width
Depth
V-todty
Ft
FtorIn.
Ft/Sec
LOW DIRECTION.Pool*—— «• RifflM.
Device
SurberManualNetSemeTrewlBucket
SurfaceCteenOH
QarbegeTrMhBubbteaDeedFiart
ind.WeweFtoatSoHda
Bottom % ContainerOozeSandGravelClayRubbteRockShellOrganic
Qlaaa JarPtaatfcJv
AoetatiCorePaper CapTeflon CapFoilCao
Wet IceAmteentDry toe
Oeentng ProcedureLow »H>gf> ConcentretDetergent WaanWater RirweAcetone Rm«eHexane RineeOther Solvent RineeSpecify;
•WAMttCT INFORMATIONLetter Station f
^iCompee* Okvctton
___j
DH
to
«ane«i Between Stattom
le| ,
Ft
lemurk* and Stte DeecnpUoti
U. -AR 103342B
FIELD DATA SHEETEnvironmental Response Teem, Environmental Protection Agency
WoodbrWge Ave., Edison, N J. OM37(201) 321-4680
Location:
Collector*:LabNurnber (Coneec.t'8) Date Collected Time (24 hr)
NO 6578 ISOIL LAND VCQETATION GROUNDWATER
DeviceAugerCoraSplit SpoonCylinder CupSpadeDepth
Ft.orIn.
SoilTyp*RockGravelSandClaySiltMuckLoamPeat
Upland-DryLowtand-OryFtoodplalnWetlandGully
Slope >1S*OS*
Old Field ResidentialWooded IndustrialFarmland Commercial
Cotor.
Water Table Depth
Sample Depth Ft
DBH
Color .Odor.Oil:Device:
SURFACE WATtft SAMPLE PREPARATION
Color ._.. Temp.PH
oTREAM Width
Depth
Velocity
Ft
FtorIn.
Ft/Sec
Pools _____% Riffle*.
Device
PetanenSurberManualNet
TrowiBucket
FLOW DIRECTION W-t lc*
SurfaceCleenOil
GarbageTraahBubble*DeedFiahSewageInd.Waata
Bottom % ContainerOozeSandGravelClayRubbleRockShellOrganic
GlaaaJarPlastic JarMetalAcetate CorePaper CapTeflon CapFoil Cap
Float SoHda , Storage
AmbientDry Ice
Cleaning ProcedureLow—»Hign ConcentrationDetergent WMMWater RIHMAcetone RinseHexane RinseOtrter Solvent RinseSpecify:
TRANSECT INFORMATION___|Compaas Direction Distance Between StationsLetter Stations
Remarks and Site Deecripdon
AR 103342C
FIELD DATA SHEETEnvironmental Response Teem, Environmental Protection Agency
Woodbrtdge Ave., Edison, NJ. OM37(201) 321-6*60
Location:
Collectors:Lab Number (Conaec.fs) Date Collected________ Time (24 hr)
NO 6579SOIL VEGETATION QROUNOWATER
DeviceAugerCoreSplit SpoonCylinder CupSpadeDepth
Ft.orIn.
Soil TypeRockGravelSandClaySiltMuckLoamPeat
Upland-DryLowland-DryFloodpiamWetlandGully
Slope
Old Field ResidentialWooded IndustrialFarmland Commercial
Color.
Water Table Depth
Sample Depth Ft
DBH
Color .OdorOil:Device:
SURFACE WATER SAMPLE PREPARATION
Color. ___,—_____ Temp.Ddor. _________ pH
STREAM Width
Depth
Velocity
Ft.
FtorIn.
Ft/SecFLOW DIRECTION ,
Pools———————% Rifflee.
DeviceKemmererPetersenSurberManual
SemeTrowiBucket
Surface Bottom ContainerClean OozeOU Sand
Garbage GravelTrash ClayBubble* RubbleDeed Fish RockSewage Shell
Ind. Waste OrganicFloat Solida | Storage
Glass JarPlastic JarMetalAcetate CorePaper CapTeflon CapFoil Cap
Wet IceAmbientDry Ice
Cleenmg ProcedureConcen*
Detergent WashWater RinseAcetone RinseHexane RinseOther Solvent RinseSpecify:
tr»**1Bfe
TRANSECT INFORMATION | .Compass Direction Distance Between StationsLatter Station»
Remarks and Site Deecnption
AR 103342D
FIELD DATA SHEETEnvironmental Response Teem, Environment* Protection Agency
Woodbridge Ave. Edison, N J. 06837(201) 321-6660
Colloctorr ___ •ftft|Lab Number (Conaee.e's) Date Coliected Time (24 hr)
NO 6580SOIL LAND VEGETATION QROUNDWATER
DeviceAugerCoraSplit SpoonCylinder CupS partiDepth
Ft.orin.
Soil TypeRockGravelSandClaySiltMuckLoamPaat
Upland-DryLowland-DryFtoodplainWetlandGully
Slope >15*OS*
Old Field ResidentialWooded IndustrialFarmland Commercial
Color.
Water Tsbte Deotn
Sample Depth Ft.
DBH
Color .OdorOil:Device:
SURFACE WATER SAMPLE PREPARATION
Colon ' Temp ,pH
STREAM Width
Depth
Velocity
Ft.
FtorIn.
Ft/Sec
Pools ______% Riffle*.
DeviceKiPatarsenSurberManualNet
Trow*Bucket
FLOW DIRECTION *" IC*
SurfaceCleanOil
GarbageTrashBubblesDeadFiahSewage
ind. WasteFloat Solids
Bottom ContainerOozeSandGravelClayRubbleRockShellOrganic
Glass JarPlastic JarMetalAcetate CorePaper CapTeflon CapFoil CapStorage
AmbientDry Ice
Cleaning ProcedureLoo f High ConcentrationDetergent W««nWater RinseAcetone RinseHexsne RinseOther Solvent RinseSpecify
TRANSECT INFORMATION |Compass Direction Distance Between StationsLatter Station »
to Ft
Remarks and Site OeecnpMon
5W/fc
AR 103342E
FIELD DATA SHEET ., Reeponee Team, Environmental Protectton Agfency~Woodbridge Ave^ Edison, MJ. 06137 . . ,-_
.ocatton:
Collectors:Lab Number (Consec-S's) Date Collected Time (24 hr)
NO 6581 // _ /SOIL LAND VEGETATION GROUNOWATER
DeviceAugerCoraSplit SpoonCylinder CupSpadeDepth
Ft.orIn.
Soil TypeHockGravelSandClaySiltMuckLoamPeat
Upland-DryLowland-DryFloodplainWetlandGully
Slope >ir
Old Field ReetdenualWooded IndustrialFarmland Commercial
Color.
Water Table Depth
Sample Depth Ft
DBH
Color ,OdorOil:Device:
SURFACE WATER SAMPLE PREPARATION
Color ___________ Temp.'lor. ______________ pH
STREAM Width
Depth
Velocity
Ft
Ftorin.
FVSec
FLOW DIRECTION .Pools ______% Riffle*.
DeviceK em mererPetersenSurberManualNetSemeTrow!Bucket
SurfaceCleanOH
GarbageTrsehBubblesDeed FishSewage
Ind. WasteFloat. Soiida
Bottom % ContainerOozeSandGravelClayRubbleRockShellOrganic
Q lass JarPlastic JarMetalAcetate CoraPaper CapTeflon CapFoil CapStorageWet iceAmbientDry Ice
CVeening ProcedureLow—^High ConcentrationDetergent WasnWster RinseAcetone RinseHexane RinseOther Solvent RinseSpecify:
TRANSECT INFORMATION |Compass Direction Distance Between StationsLetter Station s
Ft
Remarks and Site Description
AR 103342F
^ Tessn, Emrtronmeo al ProtectionWoodbrtdge Ave., Edison, N J. 06837
(201) 321-6660
Location:
Collectcf* / ?JL
Lab Number (Conaac.*'s) Date Collected Time (24 hr)
NO 6582 / LS-0SOIL LAND VEGETATION OROUNOWATER
DeviceAugerCoraSplit SpoonCylinder CupSpadeDepth
FtorIn.
Soil TypeRockGravelSandClaySiltMuckLoamPeat
Upland-DryLowland-DryFloodptatnWetlandGully
Slope >ir
Old Field ResidentialWooded IndustrialFarmland Commercial
HerbaceousShrubs ———,—— %Trees : .._«-
DBH
Water Table Depth
Sample Depth
Color.
ColorOdor.Oil:Device:
SURFACE WATER SAMPLE PREPARATION
Color ______________ Temp,PH
STREAM Width
Depth
Velocity
Ft.
FtorIn.
Ft/Sec
Pools —————% Riffle*.
DeviceK em mererPetersenSurberManualNetSeineTrowtBucket
FLOW DIRECTION W* loa
SurfaceCleanOil
GarbageTrashBubble*DeadFiahSewage
Ind. WasteFloat Solida
Bottom ContainerOozeSandGravelClayRubbleRockShellOrganic
Glass JarPlastic JarMetalAcetate CoraPaper CapTeflon CapFoil CapStorage
AmbientDry Ice
Cleaning ProcedureLow—»Hign ConcentrationDetergent WashWater RinseAcetone RinseHexane RinseOther Solvent RinseSpecify:
TRANSECT INFORMATION |Compass Direction Distance Between Stationslatter Station *
Ft
Remarks and Site Deecnption
103342G
Environmental Response Team, Environmental Protection AgeneyWoodbrtdge Ave., Edison, N J. 06637
(201) 321-6660
.ocatton:
Collectors:
UtU, C£ag«i,
Lab Number (Coneec.*'a) Date Collected Time (24 hr)
6583 | \/mf\srsou. VEGETATION GROUNOWATER
Device
DoraSplit SpoonCylinder CupSpadeDeptn
FtorIn.
SoU TypeRockGravelSandClaySiltMuckLoamPeat
Upland-DryLowtand-OryFtoodptatnWetlandGully
Slope >15B
Old Field ResidentialWooded IndustrialFarmland Commercial
Color.
Water Table Depth
Sample Depth
DBH
Color ,OdorOil:Device:
SURFACE WATER SAMPLE PREPARATION
Color. ___________ Temp .or _________ pH ,
„ i REAM Width
Depth
Velocity
Ft
FtorIn.
Ft/Sec
FLOW DIRECTION .Pools______% Riffles.
DeviceKemmererPetersenSurberManualNetSeineTrow)Bucket
Surface Bottom ContainerClean Ooze Gleaa JarOil Sand Plastic Jar
Garbage Gravel MetalTrash Clay Acetate CoraBubblee Rubble Paper CapDeed Fish Rock Teflon CapSewage Shell Foil Cap
Ind. Waste Organic ,____Float. Solids •—St0f*g*Wet ice
AmbientDry Ice
Cleaning ProcedureLow—^High ConcentrationDetergent WssnWster RinseAcetone RinseHexane RinseOther Solvent RinseSpecify:
TRANSECT INFORMATION
Letter Stations Compaaa Direction Distance Between Stations
—— to is Ft
Remarks and Site Deaenption
AR 103342H
FIELD DATA SHEET- - • ., . . ... . .. . ......« -. •Environmental Response Team, Environmental Protection Agency
Woodbridge Ave., Edison, N J. 06637(201) 321-6660
Location:
Collectors:
""P
Lab Number (Conaec.*'s) Date Collectad Time (24 hr)
NO 6584 ff| ffl OSOIL LAND VEGETATION OROUNDWATER
DeviceAugerCoraSplit SpoonCylinder CupSpadiDepth
Ft.orIn.
Soil TypeRockGravelSandClaySiltMuckLoamPeat
Upland-DryLowland-DryFtoodptamWetlandGully
Slope >15*
Old Fieid ResidentialWooded industrialFarmland Commercial
HerbaceousShrubs ____.%Trees _______%
DBH
Water Table Depth
Sample Depth
Color.
Color .OdorOil:Device:
SURFACE WATER SAMPLE PREPARATION
Color: __________ Temp .JOJQC __
W- pH
STREAM Width
Depth
Velocity
Ft
FtorIn.
Ft/Sec
FLOW DIRECTION .Pools——————% Riffles.
DeviceKemmerarPetersenSurberManualNetSeineTrowlBucket
SurfaceCleanOil
GarbageTrashBubbte*Deed FishSewage
I nd. Waste
Bottom ContainerOozeSandGravelClayRubbleRockShellOrganic
Glass JarPlastic JarMetalAcetate CoraPaper CapTeflon CapFoil Cap
Float Solids i StorageWet iceAmbientDry Ice
Cleaning ProcedureLow—»Htgn ConcentrationDetergent WashWster RinseAcetone RinseHexane RinseOther Solvent RinseSpecify
TRANSECT INFORMATIONLetter Station* Compass Direction Distance Between Stations
to Ft
Remarks and Site Deecnptton
Sire* 7
AR 1033421
Environmental Response Teem, Environmental Protection AgencyWoodbridge Ave., Edison, N J. 06637
(201) 321-6660
Location:
Collectors:Lab Number <Conaec.ra) Date Collected Time (24 hr)
NO 6585 /5V #&$&- / oSOIL LAND VEGETATION QROUNOWATER
DeviceAugerCoraSplit SpoonCylinder CupSpadeDepth
Ft.orIn.
Soil TypeRockGravelSandClaySiltMuckLoamPeat
Upland-DryLowland-DryFlood plainWetlandGully
Slope >1S"OS-
Old Field ResidentialWooded industrialFarmland Commercial
Color.
Water Table Depth
Sample Depth Ft
DBH
Color .Odor .Oil:Device:.
SURFACE WATER SAMPLE PREPARATION
Color ——_——____ Tamp ,
oTREAM Width
Depth
Velocity
Ft
FtorIn.
Ft/Sec
FLOW DIRECTION .Pools______% Riffle*.
DeviceKemmererPetersenSurberManualNet
Trow!Bucket
SurfaceCleanOil
GarbageTrashBubble*DeadFlahSewageInd.Wi
Bottom % ContainerOozeSandGravelClayRubbleRockShellOrganic
Glass JarPlastic JarMetalAcetate CoraPaper CapTeflon CapFoil Cap
Float Solids •—StOT19*iceAmbientDry Ice
Cleaning ProcedureLow »Htgn ConcentrationDetergent WasnWater Rins-Aceton* RinseHexane RinseOther Solvent RinseSpecify
TRANSECT INFORMATION
Lener Stations compass Direction Dis
to
itance Between Stattor
is
IS
Ft
Remarks and Site Deacnptton
1Q3342J
i -I , ..'i I I I ^! : S
Vt\i 'si M 's ?j1-1 *l: I i'M^
a r "ft „ i*, - TJ|-",25 i,tD^ |J«i
*><a•:r'; M ^* r -"' ° v» * «^ tliwv« r* k -* A=..
i ^ ^ mmmAR 103342K
si« ! j ^ ..-i^ 4i^.iV
.5hV3>: N I <4 1 l *. u_ [5_ 4: . s, f"«! - JT ,1 - ^ 41^1 n-- •-3 *4*. * ^ ,1M i * ^ -4j . — • • r v ^ I > . A C
^
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<^i--. «'!• H '-* r- 72 tv* :^v *« i" JH1 ^ "
plfJi !»• ~ J ^' >^ *- ^ 7 1/v *~43 "* * ^ ' o - * v B v * - » 7
\{i M;'?^M4 T -lf' 1IN * *" "^ 1^^ ^ ,S - > 3 1 v* •*! ^- >/" ) L_£4^ * ~" u_ £3 •>. . j ^ t\ s" o > strr
AR 103342L
1U„ «5 x0 < N
'-1
.• <>r**S f^ i
r**7<o r?^ < :^ " ?.u c2
APPENDIX C
Photodocumentation
eh/DONEGAN/fInal-report
AR 103342P
AR 103342Q
APPENDIX D
Maps, Site Sketches
eh/DONEGAN/fi nal-report
AR 103342R
EPA/REACRoy F. Weston, Inc.
EPA CONTRACT 68-03-3482
Not to Scale
Approximate Location of Sanpling Sites
Millcreek Site, Millcreek Township, Pennsylvania
AR 103342S
J 135' £30jf-A2.s.i • •»• t1-3 ow' y
AR 103342T
APPENDIX E
Site Health and Safety Plan
eh/DONEGAN/final-report
AR 103342U
WESTON REACHAZARDOUS UASTE SITE INVESTIGATION AND RESPONSE
HfAlTH AND SAFETY PLAN
EPA Assignor: * *- ' -- -- A___ Work Assignment No.Date of Field Activity: °^ 3-U____ Prepared by: HOriginal Safety Plan: Yes >£_ No __ Modification No.
Site Name: (*4»~cc*£€"*• , Lee.*
Site Address: Street No.CltV /*Ml_._.C.j*,tfeV£ >&UA/fH>rW e »J ^ ^ BIH H B BHlBWIBHBiM ^ ^ MM ^ iBMi i B ^ ^ ^ HB
CountyState ffcvA/.ycv/A/iA_____ z^p code
Site Contact: _____________________ Phone ______Directions to Site:£~&
Map Attached: Yes >__ No _Site H1 storv;
Hi*
INCIDENT DESCRIPTION
TYPE: A) Spill __ Air Release __ F1re __ HW Site _i) AsstssMnt __ SamollnQXl Emergency Response
Clean-up/Re«oval __ Other (specify) ______C Urbtn/Rt$1dtnt1tl _ Comntrdal __ Industrial __
Rural __ Rt«ott __PHYSICAL DESCRIPTION
: CA\Size of SUi:.^^^ Terrain: f. / .Y Weather:± w^ — 4 ' ZZf
rd/H&S-FOR«
AR 103342V
Involved In the Release or Incident
Drums ^ No. __ Tanks _____ No. __
Truck ____ License No. ____ Tanker ______ Box
Railroad Car ' Tank No. _______ Box No. _Spill ____ Source ____________ Approximate VolumeOtherANTICIPATED ACTIVITIES
„ ——
l+t. /cr--, J
EXPOSURE HAZARDS
Inhalation X Skin Contact X Ingestlon __ Radioactive __Biological __ Fire ___ Explosion __ Unknown __PHYSICAL HAZARDS
Heat __ Cold X Noise __ Underground Utilities __
Overhead Utilities __ Heavy Equipment __ Sharp Objects __
Pressurized Air __ Cylinders __ Ladders __ Scaffolds __
Unguarded OpenIngs-Wall, Floor __ Liquids 1n Open Containers, Ponds,
Lagoons __SPECIAL HAZARDS_________________________________________
~»/*u
ANTICIPATED LEVEL OF PROTECTION (Circle Ont): A
WHY:
rd/HiS-FORHxv V<. 0<\ \V\\A x^ Q^VS.M. ,
AR 103342W
PHYSICAL HAZARDS OF CONCERN
Hazard Description Location Applicable Precautions
><
.
; ft _ ,'< rt.//,.fre .
-f-Lt,
H - o _ v
rd/H4S-FORM
AR 103342X
HHEMICAL CONTAMINANTS OF CONCERN
TLV I.O.L.H. Source/Quantity Route of Symptoms of Used to^onitContaminant (PPM) (PPM) Characteristics Exposure Acute Exposure Contaminant
"
Ni -A'i
rd/HiS-FORM
AR 103342Y
Was Entry Madt: Yes __L No —
iHL.£ NO ___
A B (C j D Why:
SCBA __ APR *^ Model __ Cart./Can. Type __ Tyvek _
Poly Tyvek __ Saran Tyvek *^ Add Suit __ Rain Gear __
Cotton Coveralls __Gloves: Inner ___^T~Butyl __ N1tr1le *^~ V1ton __ Other
Foot Gear: Safety Shoes __ Outer Boots _f___| Booties __ Other
Descrlotion of Decontamination Used:_______ __________v. (It)
AIR MONITORING Performed by:
Instrument Reading*; CGI/02 Rad Meter OVA QHNOs^ Other
Background ___
Site Location: /font Tr+^J-o&A-A __ Q' / ty*- .Site Location: / 7<*-»X B MJL -ff" f&fsh __ O'/ M*~Site Location: ______________ __ __Site Location: _____________ __ __Wind: Speed __ Direction __ Temp. __ Rel. Hum. __ B.P.Summarize A1r-Monitoring Data ______________________
rd/H&S-FORMAR 103342Z
SAMPLIN6 ~ ~ Performed by: £•&•«>*'— /P-
Sampling Plan (Y or N) ./—No. of Samples: Solid V Liquid _____ Gas __ Other ____
Laboratory: _________.———————————————————————————
Has Lab Been Notified of Potential Hazard Level? Yes __ No __~Analyses: ____________________________________Sampling Comments:
DOCUMENTATION Performed by: <?• &-J*——/f- » ./C. Z-,jLc#r-
Type: Photo * Log Book * Recorder __ Video __PUBLIC IMPACT
Distance to Nearest: Residence ____ School ____ Hospital ____Public Building ____ Other
*/Evacuation: Yes __ No * Nuaber __ By Whom:!
ENVIRONMENTAL IMPACT:
Nearest Waterway: />Vs>Ul-. fl*W Distance:
Condition ' Observed Potential None
Surface Water ContaminationGround Water ContaminationDrinking Water ContaminationA1r ContaminationSoil CoatMlnttlonStressW Veg«tat1onPERSONNgL (Name and Phone, On or Off -Site)S1t§ Manager:S1tt Safety Coordinator:Other REAC Field Personnel:
rd/HiS-FORMAR 103342AA
fflfRSENCY INFORMATION
Emergency Phone Numbers:
Location Phone Notified (Y/N) ContactF1rt -
Pol 1 ceAmbulanceHospital 7-3.- u. zf st (ft*)
Nearest Phone ___________DIRECTIONS TO HOSPITAL: <5o *•*-£ 6cX /I. •* £6* -A.
(AHACH MAP)
>-
ADDITIONAL EMERGENCY PHONE CONTACTS:
CHEMTREC (800) 424-9300TSCA HOTLINE (202) 554-1404RCRA HOTLINE (800) 424-9346CDC (404) 452-4100 (Day), (404) 329-2888 (Night)BUREAU OF ALCOHOL, TOBACCO & FIREARMS (800) 424-9555, (202) 566-7777NATIONAL RESPONSE CENTER (800) 424-8802WESTON MEDICAL EMERGENCY SERVICE (513) 421-3063PESTICIDE INFORMATION SERVICE (800) 424-9346BUREAU OF EXPLOSIVES, A.A. RAILWAYS (202) 835-9500WESTON REAC OFFICE (201) 906-0734 OR 9Ub-U847
Larry White, Weston Program Manager (301) 992-8880 (H)Rich Habrukowlch, Operations Manager (215) 275-1895 (H)Cralg Moylan, Health & Safety Manager (215) 524-1160 (H)
rd/HiS-FORM
AR 103342BB
I have rtad, understood, and agreed with the Information set forth in thisHealth and Safety Plan and will adhere to the protocols specified herein.
USite Manager Slyrtftye ^ Date.
< WSite Safety Coordinator Signature Dateo* w*——caField Team Member Signature. ,, Date
Field Team Member Signature DateP-J&- L,)frS\SL.ay4* - jj/i ______________________
Field Team Member./ Signature " D a t e
HEALTH & SAFETY PLAN APPROVAL
REAC HEALTH/SAFETY MANAGERSignature^ v"——' Date
rd/HiS-FORM
AR 103342CC
fj
LAKE* ERIE'APPROX MEAN LAKE EL.,7 57] <j
•;• =________ „ ,_ _ _. K^ — _1 •
BASS MAP IS A PORTION OF THE U.S.3.S. SWANVILLC, M QUAOTMiSLE (7.5 MMUTE SERB. *57, PHOTDREVI9ED !9€>Va
AR 103342DD
LOCATION MAPMILLCREEK SITE, MILLCREEK TWP.t ________
SCALE: l"« 2000' ~ —i CORPORAnON2_2 ^J A HaHtburton Company
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AR 103342EE
APPENDIX F
Sampling Plan
eh/DONEGAN/flnal-report
103342FF
SAMPLING PLAN FOR MILLCREEK SITE
Sediment samples will be collected from Marshal Is Run and a wetland basinIn the south central portion of the site. Specific sampling equipment andmethodology'employed will be determined onsite following Initialreconnaissance. Variables such as substrate characteristics and depth ofwater will be noted and evaluated with respect to the applicability ofequipment and techniques available. Ekman and ponar dredges will beonsite and utilized if sediments are soft enough to permit efficientoperation. This will most likely be the case in Marshalls Run. Localtopography and site description indicate that flow In this waterbody issluggish and the reach under consideration depositional in nature.Sediments are most likely fine grained.
r
At least a portion of the wetland basin was a forested upland prior to thedischarge of fill north of this area. The substrate most likely containsremnants of the previous vegetative cover, as well as upland soils.Typically, wetlands are depositional environments with soft substrates,however, sufficient time may not have elapsed since the formation of thishydrosystem to allow a significant deposit of fine grained material toaccumulate. As a result, operation of an Ekman or ponar dredge may not bepossible. If this is the case, a hand bucket auger will be employed tocollect sediments.
Water samples will also be collected from Marshalls Run and the wetlandbasin. Marshalls Run will be sampled by utilizing a composite samplingprocedure. A number of subsamples will be collected at various pointsacross a representative cross section of this waterbody. The transitrate, or number of discrete samples collected, will be determined by themixing characteristics of the stream. Depending on the depth of thiswaterbody and other hydrologic characteristic, a kemmerer bottle, depthIntegrating sampler, or hand held sample bottle will be employed tocollect the sample. A similar compositing procedure will be employed ateach sampling point 1n the wetland basin, however, the subsamples will becollected across a vertical rather than horizontal transect.
The selection of sampling locations will be determined following initialsite reconnaissance. A combination of biased and random samples will becollected in this study. Biased locations are those areas where there ishigh likelyhood of encountering positive evidence of contamination.Obvious contaminant plumes as Indicated by staining, discoloration, and/oroil slicks vlll be sampled. In addition to biased samples, random sampleswill be collected. The selection of these locations will be based on astatistically va]_1d protocol such as a grid sampling scheme.Approximately 12 sediment and six water samples will be collected forchemical analysis. All samples will be analyzed for total recoverablepetroleum hydrocarbons, volatile organlcs, base, neutral and acidextractable organlcs, PCBs, and priority pollutant metals. Additionally,analysis of sediments will Include total organic carbon and grain sizeanalysis. All sampling and analytical procedures will follow EPAguidelines.
rd/COMBS/SP-MILLCR
103342GG