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Parson’s 2011Rolls-Royce University Technology Centre in Materials
The Influence of Compressive Residual Stress on a
Hot Corrosion Process Within the Gas Turbine
Grant Gibson 1, Jonathan Leggett 2 and Karen Perkins 3
1,3 Rolls-Royce University Technology Centre,
Materials Research Centre, School of Engineering,
Swansea University, SA2 8PP. United Kingdom
2 Rolls-Royce plc, P.O. Box 31, Derby, DE24 8BJ. United Kingdom
Acknowledgements – Cranfield University, Loughborough University and Metal Improvement Company
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Company Background
Rolls-Royce Product Locations
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Company Background
Civil Aerospace Portfolio
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Introduction
Efficiency requirements
Set by the customer and Governments
Emissions targets
Set by Governments
Turbine entry temperatures have increased
Hot components spend more time at temperature
Leading to high temperature corrosion
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Key Conclusions
Shot peening changes the rate of hot corrosion
Non shot peened specimens corroded less than shot peened specimens
Optimisation of shot peening for high temperature corrosion and
corrosion-fatigue desireable in the gas turbine engine
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Area of Focus
Hot Section Components
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Hot Corrosion
Corrosion rate also depends on deposition rate and composition of salt
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Corrosion Pits
Pits forming in components may ultimately compromise integrity
CONVEX SIDE
General view of corrosion
scales
Corrosion pit with crack
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Typical Pitting Mechanism
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Shot Peening
Variety of methods
Introduce a compressive stress close to the surface of the component or
specimen
Shot peening is a cold work process using small shots of metal, glass or ceramic
Used industry wide to improve fatigue and corrosion-fatigue response
Little evidence in published literature with regard to hot corrosion
http://www.metalimprovement.com/shot_peening.php
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Application of Shot Peening in the Gas Turbine
Hot components are shot peened for fatigue improvements
Stress relaxation
Loughborough University have shown that shot peening imparts a permanent
layer of mis-orientated grains into the surface of hardware
Shot peened layer can be redefined as the region of strain hardened material
Results from RR1000 and service show no fatigue deficit when corrosion is within
the shot peened layer
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Shot Peening
Ln
(A
ltern
ati
ng
str
es
s –
Go
od
ma
n c
orr
ec
ted
)
Ln (Nf Number of Cycles to Failure)
Parson’s 2011Rolls-Royce University Technology Centre in Materials
NASA and General Electric
Pre-corroded under high salt flux at 704°C, then air fatigue tested at
704°C
60-98% reduction in fatigue life
The Effects of Hot Corrosion Pits on the Fatigue Resistance of a Disk
Superalloy, T.Gabb, J. Telesman, B. Hazel and D.P. Mourer, 2008
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Surface Roughness and Depth Measurements
EBSD tool
Measurement of strain hardened layer
Directly proportional to the level of permanent grain mis-orientation
Green region indicates local grain to
grain mis-orientation
Surface of material
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Shot Peening and Corrosion Trials
Shot peening improves fatigue response in pre-pitted specimens
Very little information in literature regarding shot peening and hot
corrosion
Investigations have begun to attempt to optimise shot peening for high
temperature corrosion and corrosion-fatigue in nickel based alloys
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Shot Peening Matrix
Range of shot peening intensities and shot sizes used
Material – 720Li nickel based superalloy
Notation Intensity / AShot Type /
HCoverage / %
GA0 - - -
GA1-3 1-3 110 200
GA3-5 3-5 110 200
GA6-8 6-8 110 200
GA8-10 8-10 110 200
GB70 6-8 70 200
GB110 6-8 110 200
GB170 6-8 170 200
GB230 6-8 230 200
GB330 6-8 330 200
ø=5
10
All dimensions
in mm
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Surface Roughness and Depth Measurements
Depth of strain hardening
increases with intensity and
shot size
Surface roughness increases
with intensity, less so with
shot size
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Surface Roughness and Depth Measurements
Initial un-corroded samples highlighted 6-8A, 330H, 200% coverage
Most desireable
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Surface Roughness and Depth Measurements
Type II hot corrosion trials undertaken at Cranfield University
98% Na2SO4 – 2% NaCl
300 hours, 50 hour recoats
A
B
C
Datum
24 measurementsA – Thickness of oxide
B – Pit Depth
C – Internal Corrosion Depth
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Depth and Surface Roughness Measurements
0
5
10
15
20
25
30
35
0 20 40 60 80 100 120
Max
imu
m S
ect
ion
Lo
ss i
n M
icro
ns
afte
r 3
00
Ho
urs
Depth of Strain Hardened Material in Microns
Depth of Strain Hardening Against Maximum Section Loss in Microns
Unpeened
6-8A 230H
1-3A 110H
6-8A 110H
6-8A 110H
6-8A 170H
6-8A 330H
6-8A 70H
8-10A 110H
3-5A 110H6-8A, 230H, 200%
coverage identified as optimised
corrosion protection condition
6-8A, 330H, 200%
coverage one of the worst
Unpeened
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Depth and Surface Roughness Measurements
0
5
10
15
20
25
30
35
0 0.5 1 1.5 2 2.5
Max
imu
m S
ect
ion
Lo
ss i
n M
icro
ns
afte
r 3
00
Ho
urs
Surface Roughness in (SA) in Microns
Surface Roughness Against Maximum Section Loss in Microns
Unpeened
6-8A 230H
1-3A 110H
6-8A 110H
6-8A 110H
6-8A 170H
6-8A 330H
6-8A 70H
8-10A 110H
3-5A 110H
6-8A, 330H, 200%
coverage one of the worst
6-8A, 230H, 200%
coverage identified as optimised
corrosion protection condition
Unpeened
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Key Conclusions
Corrosion features within the shot peened layer show no debit in fatigue response
Shot peening affects the corrosion rate
Initial trials identified 6-8A 330H 200% coverage as optimised condition
Corrosion trials showed that 6-8A 230H 200% had the lowest section loss of all
the matrix of peening conditions
Parson’s 2011Rolls-Royce University Technology Centre in Materials
Future Work
Air fatigue trials at 700°C have been undertaken on a smaller matrix of conditions
Results show that the best shot peening condition for corrosion gave a similar
fatigue response to that of the standard peening condition
Investigation of a duplex peening process to assess the role of depth and surface
roughness on corrosion, fatigue and corrosion-fatigue performance
Corrosion-fatigue trials to be undertaken later this year at Swansea University on
the reduced matrix of conditions