thru: mike zickler, tatl, region lu-ff— td d #9010-11from: luis loarca, tat region iii subject:...

* 5 Underwood CourtDetroit, NJ 08075 1.609-461-4003

TECHNICAL ASSISTANCE TEAM FOR EMERGENCY RESPONSE REMOVAL AND PREVENTIONERV CONTRACT 68-WO-OQ36

MEMORANDUM

TO: Glen Lapsley, EPA Region IIIEnforcement and Title III Section

THRU: Mike Zickler, TATL, Region l U - f f — TDD #9010-11v PCS #1198

FROM: Luis Loarca, TAT Region IIISUBJECT: Snow Hill lane Sample Reoults

DATE: January 3, 1991Enclosed you will find the analytical results for Snow Hill LaneSite, as you requested yesterday, (January 2).

Sample Label Sample Location

W-l FIELD BLANKW-2 325 Cedar Hill Lane residency, non-

filtered i/ir.,-H-3 325 Cedar Hill Lane residency, .filteredw-4 upstream, non-filtered AW-5 Downstream, non-filteredH-6 GE drumW-8 Uptream, filteredW-9 Downstream, filteredS-l Soil backgroundS-2 Neville drumS-3 Monsanto drums-4 Soil around Neville drumS-5 Soil around Monsato drumS-6 Soil around the Rohm & Haas drumS-7 Offsite soil backgroundS-8 Soil around the GE drumS-9 Rohm & Haas DrumS-10 Soil Background on Snow Hill Lane

W0005MAJOR PROGRAMS DIVISIONIn Auociadon with Foster Wheeler Envireiponse, Inc., Retourct Applications, Inc., C.C, Johnson Mulhotra, RC,ind RE. Swrlcra Auodatet

the. pa,g<L Wmd in thi* faamr. i* not O.A ne.ndable. o*. Itaibte. mit U *.* due to AubAtanda/id aoto/i o/i conditional tht original

Bridgeport Environmental Inc. ucti»«umiyii«iuiw.iariM fM(____________________________________________________H 08S55 IJlP.O.Box 247 609/467.0380510 Heron Drive Suite 107Bridgeport, NJ 08014-0247

HESTON

PROJECT: SNOW HILL LANE

DATE RECEIVED: NOVEMBER 11, 1990

REPORT NO: E627S - E6288

BRIDGEPORT ENVIRONMENTAL, INC.

RICHARD W. LINCH ,nnnnftLABORATORY MANAGER lUUUUO

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SAMPLE JdCATION AND IDENTIFICATION

ANALYSIS NO CLIENT ID

E6275 W-l

E6276 • W-2

E6277 W-3

E6278 N-4

E6279 W-5

E6280 W-6

E6281 s-2

E6282 S-3

E6283 S-4

E6284 S-5

E6285 S-6

E6286 S-7

E6287 S-8

E6288 s-9

woo?O

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I ?•S3

& H'isi^

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COMP.

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Iss

llDOOB

METHODOLOGY' SUMMARY

PURGEABLES U.S.E.P.A. Method 624 - This is « purge andcrap Gas Chromatagraph/Masa Spectrometer (GC/MS)method applicable to the determination of thecompounds listed in the U.S.E.P.A. Manualentitled " Test Procedures for tha Analysis ofOrganic Pollutants".

Ac RF5996 GC/MS was used with a capillary column.

Method detection Units are as stated,

Soil samples are prepared for analysis aa prescribedin Method 8240 frsw 3H846.

ACID EXTRACTABLESBASE NEUTRALS D.S.E.F.A. Method 625 - This method covers

the determination of a number of organic compoundsthat an partitioned in an organic solvent and••enable to gas chroaatography. Thii it a gaichromatography/mass ipectrometer (GC/MS) methodapplicable to the determination of the compound!listed in the D.S.E.P.A. Manual entitled "leitProcedures for the Analysis of Organic Pollutants".

/

A HP5970 was used with a DB-S FSCC.

Method detection limits are as stated.

Soil samples were prepared for analysis asprescribed in Method 3550 from SH846.

PESTICIDES/PCB's U.S.E.P.A. Method 608 - This method covers thedetermination of pesticides and PCS' a in samplesby uittr*. ztlbn/concentractlon with organic solventsand subsequent qualification/quantification byGas Chromatography. The gas chromatograph utilizesan electron capture .detector (ECD) which isapplicable for the determination of the compounds listedfor this method in the U.S.E.P.A. Manual entitle"Test Procedures for the Analysis of Organic Pollutants".

Soil samples were prepared as prescribed in Method3SSO from SW846.

100009

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nMETIIODOLOCY SUMMARY

METALS Soil samples Cor metal analysis were run inaccordance with the methods prescribed inSU846, This Includes a nitric acid digestionfollowed by either furnace flame atomicabsorption, Flaneless Atomic Absorption, orInductively Coupled Plasma analysis.

Aqueous samples for metals analysis were runin accordance) with the methods prescribed inMethods for Chemical Analysis of Watur andWastes, EPA-600/4-79-020 March 1979.

PHEHOLS Analysis performed according to U.S.E.P.A.420 (coloxlneccic, Automated 4AAP withDistillation). Samples that are high insolids are predlstllled according to 420,1(8.1). Sample is reacted with four (A)Amlnoantlpyrine and Alkaline ferrlcyanl.de tofora a red color, which is read at SOSnm.Equipment used; Technlcon Autoanalyzer 1IC.

Analysis performed according to U.S.E.P.A.335.3 (colormetric, automated), Samples highin solids are predlstllled according Cofigure 1, 335-2. All samples pass throughautomated distillation. Sample is reactedwith Chloroaroine T Co produce cyanogenchloride, which developes a red color whencombined with pyrldina/barblturlc acidreagent; which is read at 570nm, Equipment:used: Technicon Autoanalyzer I1C,

PETROLEUMHYDROCARBONS Aqueous 'samples were analyzed following Method

418.1 as prescribed in Methods for ChemicalAnalysis of Water and Wastes, EPA-600/4-79-020March 1979,

Soil samples were extracted in accordance with *•'»'"*"the methods prescribed in SW-846 andsubsequently analyzed as scored above,

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LABORATORY CHRONICLE

RECEIPT/REFRIGERATION _____________ 11/11/90

ORCANICSEXTRACTION

1. Acids

2. Base/Neutrals

3. Pestlcidea/PCB'B/Berbicldea 11/13/90 - 11/19/90

4. Petroleum Hydrocarbons_______*____________

ANALYSIS

1. Volatlles_______________!{_•_____________

2. Acids ________ HA

3. Base/Neutrals

4. Pestlcldes/PCB'a/Herbicides UW9Q - 12/4/90

5. Petroleua Hydrocarbons______NA___________

6. Total Organic Carbon________^ _______

Sectlon SupervisorT.uvlew & Approval

INORGANICS

1. Metals_________________ii/Ti/on - ii/9n/qn

2. Cyanides__________________11/13/90________

3. Phenols_________._______HA

OTHER ANALYTES

Section SupervisorReview & Approval__

Quality Control Supervisor 100011Review & Approval____________g UA________*

—^ If fractions are re-extracted and re-analyzed because initial endeavorsdid not _eet quality control acceptance criteria, Include dates for both.

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RESDT.T SUMMARY

0

100012

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CERTIFICATE OF ANALYSIS

SAMPLE ID: K6275

CMENT ID: w-1

SAMPLE DATE: 11/9/90

"PALS MDL(_g/L) RESDLT(-g/L)

b.Ol N.D.

1,00013

J

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SAMPLE ID: £6276

CLIENT ID: W-2


METALS MDL(_g/L) RESULT (ag/I.)LEAD 0.01 N.D.

u

100014

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SAMPLE ID: E6277

CLIENT ID: tf-3


METALS HDL(Dg/L) -ESOLT(Bg/L)

LEAD 0.01 0.015

. 100015

O

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CERTIFICATE OF ANALYSIS———————

SAMPLE ID: E6278

CLIENT ID: H-4


METALS , HDL(-g/L) RESOLT(nE/L)

LEAD 0.01 N.D.

100016 ^•' U

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CERTIFICATE OP ANALYSIS

SAMPLE ID: E6279

CLIENT ID: W-5

SIMPLE DATE: 11/9/90

METALS MOL(mg/L) RESULT(ag/L)LEAD 0.01 N.D.

O 100017

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HAZARDOUS SUBSTANCE LIST(aqueoua)

SAMPLE ID: E62BO

CLIENT ID: H-6


METALS MDL (mil) RESDLT (_g/L)ALUMUm 0.10 0.11ANTIMONY 0.005 N.D.ARSENIC 0.005 N.D.BARIUM 0.50 N.D.BERYLLIUM 0.01 N.D. ,CADMIUM 0.01 N.D.CALCIUM 0.05 34.9CHROMIUM 0.01 N.D.COBALT 0.05 N.D.COPPER , 0.01 3.39 (~~\IRON 0.05 0.50LEAD 0.05 1>UMAGNESIUM 0.05 2.71MANGANESE 0.01 0.39MERCURY 0.0005 0.028NICKEL 0.05 N.D.POTASSIUM 0.10 9.69SELENIUM 0.005 N.D.SILVER 0.01 . N.D.SODIUM 0.05 12.3THALLIUM 0.10 N.D.VANADIUM 0.05 . N.D.ZINC 0.01 1.45

CYANIDE 0.10 N.D.

100018

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LabNam: Bridgeport Environiantal, Inc. I Saiplo Hurter Ibig No i N/A I E6260 I

ORGANICS ANALYSIS DATA SHEET »..,-........—.«(Pago 3)

Pesticides/PCBs ><

Conctntration: (toT) Itediui ( Circla Dng ) GPC Clianup _ Vis J Ho xDal« Extricttd/PrejISfcd; 11/13/90 Sepiratory Funnel Extraction _/ YogCite Analyzadi 12/03/90 Continuous Liquid-Liquid Extraction _ YetCore/Oil Factor! IdOiL/frlPircent toitture; N/A

C.A.S.Huibir

12674-11-211104-26-211141-16-;55469-21-912672-29-611097-69-111096-62-;

Arochlor-1016, ,flrochlor-1221. ,Arochlor-1232. ,Arochlor-1242, ,Arochlor-1248, ,

Arochlor-1260, ,

13 U13 UHU13 U13 U13 U13 U•J

Fori 1 7/85

100019

xj

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HAZARDOUS SUBSTANCE LIST

SAMPLE ID: E6281

CLIENT ID: S-2


METALS MDL (ag/kg) RESULT (an/kg)

ALUMINUM 5.00 2640ANTIMONY 0.13 2.57ARSENIC 0.13 9.53BARIUM 12.5 N.D.BERYLLIUM 0.50 N.D.CADMIUM 0.50 N.D.CALCIUM 2.50 13900CHROMIUM 0,50 1860COBALT 2.50 „_„_COPPER ' 0.50 186000 0IRON 2.50 1MOOOLEAD 2.50 6530MAGNESIUM 2.50 M600MANGANESE 0.50 404MERCURY 0.05 legNICKEL 2.50 66<4POTASSIUM 5.00 1030SELENIUM 0.13 30<0SILVER 0.50 H<1)_SODIUM 2.50 2550THALLIUM 2.50 „_„_VANADIUM 2.50 . U3ZINC 0.50 19700

100020CYANIDE 0.10 39.0

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r Lab HIM ! Bridgeport Environmental, Inc. I Saiple Nuwor ICaiaNo I N/A I E6261 I

ORGANICS ANALYSIS DATA SHEET «•••-• •-•——«(Page 3)

PeJticides/PCBs ••

Concantrationi (to* nediim ( Circle Ono ) GPC Cleanup _ Yas __ NoData Extracted/Prepared! 11/13/90 Sepiratory Funnel Extraction _YesData Analytadi 12/04/90 Continuous Liquid-Liquid Extraction _ YeaConc/Dil Factor) 10,08/lOnLPercent toiiture: 3.9

C.A.S,Nurier

12674-11-2 Arochlor-1016. ..... 2700011104-26-2 Arochlor-1221. ..... 13000 U11141-16-; Arochlor-1232. ..... 17000 U53469-21-9 Arochlor-1242, . . , , , 13000 U12672-29-6 Arochlor-1248. ..... 13000 U11097-69-1 Arochlor-1254, ..... $000011096-B2-5 Arochlor-1260. ..... 17000 U

Fori 1 7/B5

100021O

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HAZARDOUS SUBSTANCE LIST(solid)

SAMPLE ID: E6282

CLIENT ID: S-3


METALS MDL (_g/kg) RESULT (ag/kg)

ALUMIKDH 5.00 460

ANTIMONY 0.13 N.D.ARSENIC 0.13 8.36BARIUM 12.5 N.D.BERYLLIUM 0.50 N.D.CADMIUM 0.50 1.19CALCIUM 2.50 467CHROMIUM 0.50 12.6COBALT 2.50 N.D.COPPER ' 0.50 86.4 BON 2.50 26500 ^LEAD 2.50 526MAGNESIUM 2.50 163MANGANESE 0.50 189MERCURY 0.05 0.088NICKEL 2.50 77.!POTASSIUM 5.00 148SELENIUM 0.13 0.13SILVER . 0.50 N.D.SODIUM 2.50 507THALLIUM 2.50 N.D.VANADIUM 2.50 27.2ZINC 0.50 2300

CYANIDE 0.10 4.01

100022O

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Lab New i Bridgeport Environnental, Inc. I Staple Nuiber IGate No ! M I E6262 I

ORGANICS ANALYSIS DATA SHEET ,———...—.,(Page 7)

Pejticidea/PCBs '•/••••s.

Concentration! (fcm) Ifediui ( Circle One ) GPC Cleanup _ Yat j VaData Extracted/Prepared! 11/13/90 Separator)) Funnel Extraction _YeiData Analyzed! 12/04/90 Continuona Liquid-Liquid Extraction _ YetCone/Oil Factor: 10,07/lOiLPercent Koiilurei 2.!

C.A.S.Nuaber

12674-11-2 Arochlor-1016. , , . . , 13000 U11104-28-2 Arochlor-1221, ..... 13000 U11141-16-; Arochlor-1232. , , , , , 17000 U53469-21-9 Arochlor-1242. ..... 13000 U12672-29-6 Arochlor-1248. , . , . , 17000 U11097-69-1 Arochlor-1254. ..... 3500011096-82-; Arochlor-1260. , . . , , 13000 U

Fori 1 7/fl5

100023

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HAZARDOUS SUBSTANCE LIST(aolld)

SAMPLE ID: g6283

CLIENT ID: S-4


METALS HDL (ng/kg) RESULT (mg/kg)

ALUMINUM 5.00 7B10ANTIMONY 0.13 0.26ARSENIC 0.13 18.1BARIUM 12.5 679BERYLLIUM 0.50 0.86CADMIUM 0.50 11.0CALCIUM 2.50 10400CHROMIUM 0.50 1710COBALT 2.50 42.0COPPER ' 0.50 , 224000HON 2.50 199000LEAD 2.50 6220MAGNESIUM 2.50 15000MANGANESE 0.50 1270MERCURY 0.05 76.0NICKEL 2.50 112POTASSIUM 5.00 456SELENIUM 0.13 18.9SILVER • 0.50 , N.D.SODIUM 2.50 714THALLIUM 2.50 N.D.VANADIUM 2.50 , 46.6ZINC 0.50 13100

CYANIDE 0.10 62.0100024

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Lab Na*e t Bridgeport Environmental, Inc. i Saiplo Nuiber ICaaeNo : N/A I E6283 I

ORGANICS ANALYSIS DATA SHEET t................*(Paga 3)

Peiticides/PCBs ••

Concentration! (\M) Ifediui ( Circle Una ) 6PC Cleanup _ Yea i/mData Extracted/Prepared! 11/13/90 Separator^ Funnel Extraction _ YeaData Analyzed! 12/04/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor! 10.09/lOiLPercent ttoiature! 19.9

C,A,S,Nuiber

12674-11-2 Arochlor-1016, , , , , , 13000 U11104-28-2 Arochlor-1221. ..... 17000 U11141-16-; Arochlor-1272. ..... 13000 UH469-21-9 Arochlor-1242, ..... 13000 U12672-29-6 Arochlor-1248, ..... 17000 U11097-69-1 flrochlor-125'4. . , . . , 3300011096-82-; Aroctilor-1260. ..... 17000 U

'•-J

Fori 1 7/85

0 ' 100025

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HAZARDOUS SUBSTANCE LIST ^(solid) ' '

SAMPLE ID: E6284

CLIENT ID: S-5


METALS MDL (ag/kg) RESULT (ag/kg)

ALUMINUM 5.00 8300ANTIMONY 0.13 N.D.ARSENIC 0.13 11.6BARIUM 12.5 103BERYLLIUM 0.50 0.68CADMIUM 0.50 N.D.CALCIUM 2.50 545CHROMIUM 0.50 111COBALT 2.50 16.0COPPER ' . 0.50 209 0'IRON 2.50 50400LEAD 2.50 941MAGNESIUM 2.50 783MANGANESE 0.50 649MERCURY 0.05 1.30NICKEL 2.50 15.4POTASSIUM 5.00 447SELENIUM 0.13 1.53SILVER . 0.50 H-DSODIUM 2.50 630THALLIUM 2.50 N-D-VANADIUM 2.50 < 55>2ZINC 0.50 142

CYANIDE 0.10 100026 *-60

o

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Lab Kant I Bridgeport Enviroimntel, Inc. I Saiple Nurier ICase No i N/A I E6284 I

ORGANICS ANALYSIS DATA SHEET ..................(Paga 7)

Pe«ticido8/PC8s ••

Concinlrationi (!OM> hediui .( Circle One ) GPC Cleanup „ Yea _/DifData Extrected/PrepTfed! 11/13/90 Separator^ Funnel Extraction _YesData Analyzed! 12/04/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor: 10.01/lOiLPercent Itoisture: 24,8

C.A.S.Nuiber

12674-11-2 Arochlor-1016, , , . . . 13000 U11104-28-2 Arochlor-1221, ..... 13000 U11141-16-; Arochlor-1232, ..... 13000 U53469-21-9 flrochlor-1242, ..... 13000 U12672-29-6 Ai'Ochlor-1246. ..... 17000 U11097-69-1 Arochlor-1254, ..... 14000011096-62-; Arochlor-1260. ..... 17000 U

Fori 1 7/6;

100027

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SAMPLE ID: E6285

CLIENT ID: g-o


METALS MDL (ag/kg) RESULT (ng/kg)

ALUMINUM 5.00 13800ANTIMONY 0.13 „_„ARSENIC 0.13 16.4BARIUM 12.5 230

CADMIUM 0.50BERYLLIUM 0.50 u „n.u.

N.D.CALCIUM 2.50 996CHROMIUM 0.50 54<9COBALT 2.50 1?]9COPPER ' 0.50HON 2.50USAD 2.50MAGNESIUM 2.50MANGANESE 0.50MERCURY 0.05NICKEL 2.50POTASSIUM 5.00SELENIUM 0.13

HON 2.50 299003280

MAGNESIUM 2.50

MERCURY 0.05 0>261M

POTASSIUM 5.00 6710>51

SILVER , 0.50 „ -SODIUM 2.50 620THALLIUM 2.50 N QVANADIUM 2.50 -j jZINC 0.50 ' 19j

100028CYANIDE 0.10 1.07

H the. page, filmed in thiA frame. iA not aA ne.ado.bte.,on legible. aA thiAlabe.1, it iA due. to AubAtundand colon on condition oft the. oniginal page..

Lab Nam i Bridgeport Environnntal, Inc. I Saiplo Nurtor ICase No i N/A I E62B5 I

ORSANICS ANALYSIS DATA SHEET «•-•••——-••••»(Page 7)

Pesticidia/PCBs '•x-C\

Concentration! (UMJ Nedlu*. ( Circle One ) CPC Cleanup _ Yea ,/NoDate Extracted/ProjnTedi 11/13/90 Soparatory Funnel Extraction „ YesDale Analyzed! 12/04/90 Continuous Liquid-Liquid Extraction _ YeaCone/Oil Factor! 10,15/10-.Percent toisturei 27,;

C.A.S, ug/L orNuiber

12674-11-2 Arochlor-1016. . . , . , 17000 U11104-28-2 Arochlor-1221. , , , . . 17000 U11141-16-; Arochlor-1232. , , , . . 13000 U;7469-21-9 Arochlor-1242. ..... 13000 U12672-29-6 Arochlor-1248, , . . . , 13000 U11097-69-1 flrochlor-1254, ..... 29000011096-82-; Arochlor-1260. ..... 17000 U

For* 1 7/B;

100029

J

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SAMPLE ID: E6286

CLIENT ID: S-7


METALS HDL (ag/kg) RESULT (ag/kg)

ALUMINUM 5.00 1900ANTIMONY 0.13 N.D.ARSENIC 0.13 0.84BARIUM 12.5 N.D.BERYLLIUM 0,30 N.D.CADMIUM 0.50 N.D.CALCIUM 2.50 177CHROMIUM 0.50 630COBALT 2.50 N.D.COPPER ' 0.50 2.21IRON 2.50 1900LEAD 2.50 5.99MAGNESIUM 2.50 122MANGANESE 0.50 4.09MERCURY 0.05 N.D.NICKEL 2.50 N.D.POTASSIUM 5.00 132SELENIUM 0.13 0.15SILVER . 0.50 < N.D.SODIUM 2.50 281THALLIUM 2.50 N.D.VANADIUM 2.50 , 9.16ZINC 0.50 3.88

CYANIDE 0.10 N.D.

100030

H the. page, med in thiA frame. iA not aA ne.adablt.on Itgiblt aA.thiAlabe.1, it iA due to AubAtandand colon on condition orf the oniginal page.

Lab KtM i Bridgeport Environmental, Inc. I Saiple Nuiber ICase No i N/A I E62B6 I

GRGANICS ANALYSIS DATA SHEET »-.....—.—..,(Page 3)

Pasticidea/PCBs >•

Concentration! I'toT) Itediui ( Circle One ) CPC Cleanup _ Yes j NoDate Extractid/PreTnrod! 11/19/90 Separatory Funnel Extraction _ YesDate Analyzed! 12/04/90 Continuous Liquid-Liquid Extraction YesCone/Oil Factor! 10.15/10-.Percent Itoisturoi 1.7

C.A.S,Nuiber

12674-11-2 Arochlor-1016. ..... 250 U11104-28-2 Arochlor-1221. ..... 250 U11141-16-; Arochlor-1232. ..... 250 U53469-21-9 Arochlor-1242. ..... 250 U12672-29-6 Arochlor-1246. ..... 250 U11097-69-1 Arochlor-1254, ..... 250 U11096-62-; Arochlor-1260. ..... 250 U

Fr,rn 1 7/85

100031

U the page filmed in thiA frame. iA not AA ntadablt.on ttgible, aA thiAlabtl, U 4.A due to 4u6^tanda/td colon on condition oi the oniginal page.



SAMPLE ID: E6287

CLIENT ID: S-8


METALS MDL (ag/kg) RESULT (ng/kg)

ALUMINUM 5.00 11500ANTIMONY 0.13 N.D.ARSENIC 0.13 9.90BARIUM 12.5 146BERYLLIUM 0.50 N.D.CADMIUM 0.50 N.D.CALCIUM 2.50 1394CHROMIUM 0.50 28.2COBALT 2.50 9.12COPPER ' 0.50 60.3IMH 2.50 16700LEAD 2.50 237MAGNESIUM 2.50 1310MANGANESE 0.50 732MERCURY 0.05 1.00NICKEL 2.50 12.3POTASSIUM 5.00 1210SELENIUM 0.13 1.14SILVER 0.50 H.D.SODIUM 2.50 342THALLIUM 2.50 N.D.VANADIUM 2.50 44.8zrac o.so 101

CYANIDE 0.10 , 4.70

100032

11 the.-pa'gir'i'ilme.d in thiA frame iA not aA ntadabtt on ttgible. aA thiAlabzl, it iA due to .substandard co*o« on condition o< the o*,ig,oia,_ page.

I.—..........—ILab NIM i Bridgeport Environitntal, Inc. I Ssiple Nuiber IUse No i N/A I E6287 I

ORGANICS ANALYSIS DATA SHEET '-———•—•-•(Page 3)

Pesticides/PCBa '•

Concentration! (toi,/ Itediun ( Circle One ) GPC Cleanup _ Yea _fNoData Extracted/Prepared! 11/13/90 Saparatory Funnel Extraction _ YesDate Analyzed! 12/04/90 Continuous Liquid-Liquid Extraction _YeaConc/Dil Factor: 10,08/10-.Percent Itoiaturei 20,3

C.A.S. ug/L orNuiber

12674-11-2 Arochlor-1016, ..... 250 011104-28-2 Arochlor-1221. ..... 250 U11141-16-; Arochlor-1272. ..... 250 U53469-21-9 Arochlor-1242, ..... 250 U12672-29-6 Arochlor-1248, ..... 250 U11097-69-1 flrochlor-1254, ..... 76011096-62-; Arochlor-1260. ..... 250 U

Fon 1 7/8;

100033

li the page, itmtd in thiA frame iA not aA ntadabl.t..on ttgiblt, a.labtl, it iA due to substandard colon on condition o< the oniginal page.



SAMPLE ID: £6288

CLIENT ID: s-9


METALS MDL (ag/kg) RESULT (ag/kg)

ALUMINUM 5.00 13000ANTIMONY 0.13 3.55ARSENIC 0.13 1.95BARIUM 12.5 70.8BERYLLIUM 0.50 N.D.CADMIUM 0.50 11.0CALCIUM 2.50 108000CHROMIUM 0.50 8950COBALT 2.50 53.5COPPKK ' 0.50 236IRON 2.50 51700 ^LEAD 2.50 4460MAGNESIUM 2.50 13700MANGANESE 0.50 322MERCURY 0.05 0.86NICKEL 2.50 21.7POTASSIUM 5.00 3350SELENIUM 0.13 1.20SILVER • 0.50 N.D.SODIUM 2.30 893THALLIUM 2.50 N.D.VANADIUM 2.50 43.1ZINC 0.50 1730

CYANIDE 0.10 15.0

00034 o

U the. page filmed in thiA frame. iA not aA ntadabtc. on :itgib.lt aA\thiA-.tabtl, it iA due to substandard colon on condition o& t/ie original 'page.

Lab HIM I Bridgeport Environmental, Inc. I Saiple Nurier ICase No I N/A I E62B6 I

ORGANICS ANALYSIS DATA SHEET ..................(Page 7)

Paaticidis/PCBs ••

Concentration! (ioTyttadiu* ( Circle One ) GPC Cleanup _ Yea j/hData Extracted/Prepared! 11/13/90 Separatory Funnel Extraction _ YeaData Anilyzedi 12/04/90 Continuous Liquid-Liquid Extraction YesCone/Oil Factor! 10.31/10iLPercent Mature: 44,2

C.A.S.Nutter

12674-11-2 Arochlor-1016, ..... 13000 U11104-28-2 Arocblor-1221. ..... 13000 U11141-16-; Arochlor-1232, ..... 13000 U53469-21-9 Arochlor-1242. ..... 13000 U12672-29-6 Arochlor-1248, ..... 17000 U11097-69-1 flrochlor-1254, . , . , , 22000011996-62-; Arochlor-1260. ..... 17000 U

Fon 1 7/85

•J

100035

U the. page Yarned in thiA framt iA not aA ne.adable...on ltgibtt.uA,thiAlabe.1, -it iA due to substandard co^or or co«d^t*on o< the oniginal page., ''

DATA PACKAGE

100036

I<_the page *-ed ^n th/s <rane iA not aA readab/_e_.or ttgiblt., aA thiA,labtl, it 4.A due to substawrfard co^or or eond.it.iort o{ the or^gina^ page.


P"'.I

SAMPLE ID: E6275

CLIENT ID: w-1

SAMPLE DATE: .11/9/90

METALS MDL(_g/L) RESDLT(ag/L)

LEAD 0.01 N.D.

100037•N y

H the. page filmed in thiA frant iA not aA ntaddbt.t.jn ligibtt aA Alabtl, 4.t iA due to substandard colon on condition o< the. oniginat page.


SAMPLE ID: £6276

CLIENT ID: H-2


HDL(Bg/L) RESULT(ag/L)

0.01 N.D.

100038

U the. page, ilmtd in thiA frame. iA not aA ntadabl.t J>n Itgiblt aA thiAlabel, 4.t IA due to AubAtandand colon on condition o< the oniginal page.


SAMPLE ID: E6277

CLIENT ID: H-3


METALS MDL(ng/L) RESULT(Bg/L)

LEAD 0.01 0.015

0 100039

H the. pagt^itmtd in thiA frame. iA not aA ntadable.. on Itgibte,, aA *labtl, it iA due to substandard color or co«dit*on otf the oniginat page.


0SAMPLE ID: £6278

CLIENT ID: w-4


METALS , NDL(ag/L) Rj_SDLT(ag/L)

LEAD 0.01 N.D.

0

100040

o

H the. page, filmed in thiA frame. iA not aA ntadable,.,or Itgiblt a ^ . A - 'labtl, it iA due to substandard color or condition ot the oniginal page.

CERTIFICATE OF ANALYSIS——————————

SAMPLE ID: E6279

CLIENT ID: W-5


METALS HDL(»g/L) RESULT(ag/L)LEAD 0.01 N.D.

100041s-_-X

U the. pagt \|il-ed in thiA frame. iA not aA readable or ttgible, aA thiAlabe.1, *t 4.A due to substandard color or condition o< the original page.


HAZARDOUS SUBSTANCE LIST(aqueous)

SAMPLE ID: E6280

CLIENT ID: W-6


METALS MDL (ng/L) RESULT (dg/L)ALUMINUM 0.10 0.11ANTIMONY 0.005 N.D.ARSENIC 0.005 N.D.BARIUM "' 0.50 N.D.BERYLLIUM 0.01 N.D. ,CADMIUM 0.01 N.D.CALCIUM 0.05 34.9CHROMIUM 0.01 N.D.COBALT 0.05 N.D.COPPER .- 0.01 3.39IRON 0.05 0.50LEAD 0.05 1-1*MAGNESIUM 0.05 2.71MANGANESE 0.01 0.39MERCURY 0.0005 0.028NICKEL 0.05 N.D.POTASSIUM 0.10 9.69SELENIUM 0.005 N.D.SILVER 0.01 N.D.SODIUM 0.05 12.3THALLIUM 0.10 N.D.VANADIUM 0.05 N.D.ZINC 0.01 1.45

CYANIDE 0.10 N.D.

100042

lo" the page \jilmed in thiA frame. iA not aA readable ..or legible aA thiAlabel, it is due to substandard color or condition o< the original page.

Lab Haie i Bridgeport Environmental, Inc. I Sseple Nsnbtr ICaieHo i N/A I E6280 I

ORGANICS ANALYSIS DATA SHEET .........——...(Page 3)

Peslicides/PCBs ..

Concentration! (urn) Itediim ( Circle One ) GPC Cleanup _ Yes _/No *Data Extrected/Prejnffad! 11/13/90 Saparatory Funnel Extrection _/YesData Analyzed! 12/03/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor; lOOt/hlPercent Itoialurai N/A

C.A.5,Nuiber

12674-11-2 Arochlor-1016. .11104-28-2 Arochlor-122111141-16-; Arochlor-1232, .53469-21-9 Arochlor-124212672-29-6 Arochlor-1248,11097-69-1 Arochlor-125411196-82-5 Arochlor-1260,

Fori 1 7/8;

100043

U tht page, filmed in thiA frame. iA not aA readable,or legible, as thiAlabel, U AS due to substandard color or condition orf the original page.

I *>DU I 13 AniTilt'

ijuoa 1 ("bur; I. I,iiist1^. Oti(; I) i l>'»i> ;f<f>tn-r' I niJLll i. iol&dl«'& UDS ti't H*'' 11r':,.,rl i rll.lll ..'i-l'.'l . :':•!-• i,1 IV'/u j

CI.OUUD unhni-nXcin unl M

..',;• I.M.. ' -..;ts ».'iSM4m>-« t^.iviv t'-hw.^ . •:.-• . . -.!•>-«

..,.i.i , .4.|«/~-4 |.....;,'.

..... . . . . -I.-.. ;.|.i;r.:.:i

ov/.llrtli DC IU.IUXH) uni nown

n

100044• \J

H the <page \jilmed in this <rame is not as readable Kor legible, as. this-label, it is due to substandard color on condition O|j the original page.

ub vc»- .";>i.''. UK, ;-., .

.on en IviM-

L'tifjri'.,'lillflP3t!l i

: 100045: V~^_____ ;I ! ii M iH/a

ia,» - ! ^ **"x x

Itf the p_age Mi^med in this <rame is not as readable or legible as thislabel, U x.s due to substandard color or condition o/| the original page.

CERTIFICATE OP ANALYSIS

HAZARDOUS SUBSTANCE LIST(oolW)

SAMPLE ID: E6281

CLIENT ID: S-2


METALS MDL (pg/kg) RESULT (ng/kg)

ALUMINUM 5.00 2640ANTIMONY 0.13 2.57ARSENIC 0.13 9.53BARIUM 12.5 N.D.BERYLLIUM 0.50 N.D.CADMIUM 0.50 H.D.CALCIUM 2.50 13900CHROMIUM 0.50 1860COBALT 2.50 N>D>COPPER " 0.50 186000IRON 2.50 moonLEAD 2.50 6J30MAGNESIUM 2.50 14600MANGANESE 0.50 404MERCURY 0.05 __QNICKEL 2.50 66-4POTASSIUM 5.00 1030SELENIUM 0.13 30,0SILVER , 0.50 H-J)tSODIUM 2.50 2550THALLIUM 2.50 N>D<VANADIUM 2.50 113ZINC 0.50 19700

CYANIDE 0.10 39.0100048

O

U the. page Yarned in this frame, is not as readab!e~or <«gi6le, as,t/iis ~ .label, 4.t *s due to substandard color or condition 04* the original page.

Lab Nan ! Bridgeport Envirnniental, Inc. I Seqilt Nuiber ICaaaNo i N/A I E6281 I

OR6ANICS ANALYSIS DATA SHEET <——-—•—«<P«ge 7)

Pesticides/PEs ..

Concentration! (utiyKediui t Circle One I EPC Cleanup _ Yes __ NoData Extracted/Prepared! 11/17/90 Separatory Funnel Extrection _ YesData Analyzed! 12/04/90 Continuous Liquid-Liquid Extraction _YasConc/Dll Factor! 11.08/lOiLPercent Matures 3.9

C.A.S.Huifaer

12674-11-2 Arochlor-1016, ..... 2700011104-28-2 Arochlor-1221. ..... 13000 U11141-16-; Arochlor-1272. ..... 17000 U53469-21-9 Arochlor-1242. ..... 17000 U12672-29-6 Arochlor-1248. ..... 17000 U11097-69-1 flrochlor-1254. ..... $000011196-02-; Arochlor-1260. ..... 17000 U

Fon 1 7/85

100047

U the. pagt tilmd in thiA frame iA not aA readable .or legib.le as thiAlabel, *t 4.A due to substandard color or condition otf the original page.

vttf i *},»r (,, .•

< .:.» mr. . /~\.

"l,VU-jrirtl1d Mnif

r , .n n n », ..rn<nann• ,,,!. i . -j ii'Mrtnii..,-,-r,1: •• !.»•'_

*. ' i uO'in.1 jniTiOtvn

43i(j'.ir'i t'-iiiiCM.^Vh.1 Hlic f Hi.nl. Uh

,.'.-.,£ * -.

i )4l/hlN jiluni nown

0 , vuuC' Un Known

in aiot):'

in? tuiin-WiT ').!))

4,111 «inic«'H« irwpi•Mil

1000.8

Mil ii«iw»iwnw n

Iii the page filmed in thiA front iA not aA readab|e..,or legible as thislabel, it is due to substandard color or condition OA/the original page.

l.ov vC liSu '(

.. .::, i . . • '''(''"PI .','•.

,,IIMI. r'.i "in.'ui - -i

mhitii'.'i'tU ., , ;.--ti&wnseOOoi. uncnown:,.VJPV rt -WiL'

Lino*n»/iV.4SQ1 li-bHt:

i&V| ;.f . V >t,n;i UnhnctHiiiiUEitarnii

..u-U^iiaUMV ;ii>t.nt)nn.'w./f.in ftltlrjr.

i. el !tr'iVi,00 Uni-'llfiwfi

s-.'ilUHiii.'Ji.- '.'iil'n.Nii

• i.'.v.-..,' nfi"

. . '.''.'iXip-'i,.

'- ;}0 •".. . ."f 'vt" H-, .. .,ir..'n«.t- .-,'.' ''•'(! • •', V.i.Ov)*!!

<'• ~~""fa,m, . .. ...

100049

i'i the page (il-ed in thiA framt iA not as' readable,,or,;;|egi6|e as. tI'abel, it is due to substandard color or condition o_ the original page.



SAMPLE ID: B6282

CLIENT ID: S-3


METALS KPL (pg/ke) RESOLT

100050

ALUMINUM 5.00 «0AHTDIOHT 0.13 H-D.ARSENIC 0-13 8.36BARIUM 12.5' S-D>BERILH0M 0.50 H D.CADMIUM 0.50 1.19CALCIUM 2.50 467CHROMIUM 0.50 12.6COBALT 2.50 N.D.COPPER v< 0.50 86.4 fjHON 2.50 26500LE_D 2.50 526MAQJESIUM 2.50 163MANGANESE 0.50 189MERCURY 0.05 0.088NICKEL . 2.50 77.1POTASSIUM " '" 5.00 148SELENIUM 0.13 0.13SILVER 0.50 N.D.SODUM 2.50 507THALLIUM 2.50 N.D.VANADIUM 2.50 • 27.2ZINC . 0.50 2300

CTANtOE 0.10 *-°l

o

H the. page, filmed in this frame. iA not aA reodabl.e .or legible as thislabel, 4.t is due to substandard color or condition o^ the original page.

n I................I

Lab Hi* i Bridgeport Environmental, Inc. I Saaple Nu*er I""' Cue (to i N/A I E6282 I

ORGANICS ANALYSIS DATA SHEET «--————-'(Page 7)

Pesticides/FCBs ,.

Concentration! (S) Hud in ( Circle One ) EPC Cleanup „ Yes VoDate Extracted/Prepared! 11/17/90 Seperatory Funnel Extraction _, YesDate Analyzed! 12/04/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor! 10.07/lOiLPercent Moisture! 2.;

C.A.S.Nuaber

12674-11-2 Arochlor-1116. ..... 17000 U11104-28-2 Arochlor-1221. ..... 17000 U11141-16-; Arochloi-1272. ..... 17000 U5J469-2H Arochlor-1242. ..... 17000 U12672-29-6 Arnchlor-1240. ..... 17000 U11097-69-1 Arochlor-1254. ..... 7500011096-B2-; Arochlor-1260. ..... 17000 U

Fori 1 7/8;

J 100051

H the. page. Mi^me •'.« this tframe is not as ntadable...,on. te,giblt aA..thiAlabel, it is due to substandard color or condition oi the. original page.

111?. . . i?0 IWtlWO I 'IU1.II i 111 ISO lit; tt«C U* l'"U .•• -.- -. • *"io,' : ''l.il , .'IM.!,.'!'''! If.';: •"' 1 !l t

".'•... :'.'.i.i.'.1.':

.-l-'/S. ENDrVlN ^

-Mil HUM

>-u» itniciui crtxiiE

100052,.11.11! D11IIK lUDIWt

l._the page Mi^ttd in this <rame is not as readable, on "legible as thislabel, *t 4.A due to substandard color or condition o| the original page.

••:•.__• i •T.IV; '-•«- ." ; :•• Minnac t GFPEdr i liliunion NDV ?o J ' > i . .:• 'ti :•;:<- •-i I'i'Jv .'iveluid i UtTI;Q[ l lOtiXtuVi M6v Ji'i lf^d )

• • . •• -."jt..".'" ,1.1-t.iont I . (.HAM ii ip t (.ii.ii •

. M. A t'.-oiU I,F Concn Namir"'.i.r.'r .' i .ooooufl»ij 7viiftV,!//_n Unknown'';1'-: ..ctijOOOtfrO 1 7,7 : 125 unhngnn»<'i /I ( , .Ji;rji> i,i* i.. ti't? i , OiVOO unknawri

.. Ja.( li.BU'M'ftt-B ' ft-SHPiiSI1! ^./^-iOVt'-i UncJflfip/P-tiHU

i .'.."V ,.. :••;. »4.«..i|Ti»2u-& -U3tibtl 6-Wtt'.*>'. v ; ,c«,iOi>MHto /'/:O.O.'ILILI jni;nuwn

Vi.1" I .UMiiXio*!1' 130.17 tSOOu UntmoHitH. v;.' I. i.i_"o -H MpDUcriior

' • • . • ' • . , v"iX'u+M i i't/i7!i,g.'ljti Uni.'nawnj "- -' _ i i , vvOOOu^i,' fc^oVU , i,ui,iO i <•' mir_wn

13.a -:

--.'i.t.'Chlor

i, M.n."'if?-i.i *v<>61 H iOUM.II",! /Minonn! ' .!iV',i-il ', iijil'.iu • •'"

".' i i . '. I'j '•""-'. j. '.-'.I I'MlHII'll

M iHiM.ii.i uiit (town

s ;i i* » 9

100053

Id the page Yarned in this tfraine is not ,as reddabl.e.,or legible, as this.label, it is due to substandard color or condition o< the original page.



SAMPLE ID: B6283

CLIENT ID: S-4


METALS MBL fag/kg) RESDT.T (_g/kg)

ALUMINUM 5.00 7810ANT-MONT < 0.13 0.26ARSENIC 0.13 18.1BARIDH 12.5 679BERYLLIUM 0.50 0.86CADMIUM 0.50 11.0CALCIUM 2.50 10400CHROMIUM 0.50 1710COBALT 2.50 42.0COPPER " 0.50 224000IROH 2.50 199000 v—/LEAD 2.50 6220MACHESIUM 2.50 15000MANGANESE 0.50 1270MERCDKT 0.05 76.0NICKEL 2.50 112POTASSIUM 5.00 456SELENIUM 0.13 18.9SILVER . 0.50 N.D.SODIUM 2.50 714THALLIUM 2.50 N.D.VANADIUM 2.50 46.6ZINC . 0.50 13100

CTANIDE 0.10 100054 M'°

o

11 the page filmed in this frame iA not aA readable ,or legible as this ,label, 4.t ^.A due to substandard color or condition orf the original page.

Lab Neie i Bridgeport Environmental, Inc. I Simile NutberCaaeNo ! N/A I E6287

ORGANICS ANALYSIS DATA StEET <•——————(Page 7)

Pesttaides/PCBs1 ..

Concentration: (urn/ ttediui ( Circle One ) GPC Cleanup _ YesDate Extracted/Prepared! 11/17/90 Stparatory Funnel Extraction _ YesDate Analyzed! 12/04/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor: 10.19/1W.Parcanl tloialurei 19.9

C.A.S.Nuibar

12674-11-2 Arochlor-1016. ..... 17000 U11104-28-2 Arochlor-1221. ..... 17000 U11141-16-; Arochlor-1272. ..... 17000 U57469-21-9 Arochlor-1242, ..... 1)000 U12672-29-6 Arochlor-1243. ..... 17000 U11097-69-1 firochlor-1254. ..... 7700011196-82-5 Arochlor-1260. ..... 17000 U

For* 1 7/ft

100055

I^the page filmed in this framt iA not aA readable ,or legible as thislabel, *t AS due to substandard color or condition orf the original page.

...,,,•„„•„.) .l»t oils1' T Jao'. •; ".:•;'.; " u:i; :•»«.•.; v o..:.' /fci<wi' T ,;»5 .'

J .670 .1,1.-; „( .it.1' r .:&£ J-;•»«* .'**••' 1 .196 'J

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.£.. 1 .,:... . "'"" .;

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.MI .,.'.

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*'.' MittnoU i .I; i i i "..' i M'jOl IJo. On l^SX

ijuuuufl i u ,.< , >>i '00 DnKnoHfiU'XiOOntO OiO'Xttt Linivnflwnooooi;"3'«'0 OiCf'H'* Jnrnown

w&bJlcr-'i ulNUANUy'JiCVn-'i AI ,2160 _*-tJHt*7.,-ti'lB"'* /U , M^b Hf PTACI H .flR.''.'BVo-1 JI.4732 D-BHKi6u:*)ff-'i ':,"[>,- M. MI iii"ronooo+o I'l.ooud : in Knowni.'VCi;ii:i(itii .t'.niyf1 Mni.nown.iiJ-t-'i :. i.Ui'in fi,i'-(ni:iiU'M i.-'-i.'.".'U'H'BHi ,-,Ht,nX' i I'M nown;,.''iO-'iO" 4 r.HI/*j** t

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i;iii,inorfi',. i,i,.'n.'i>i'i t.,ni noHM

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, -1. ./ ;. ,»• f M • , i m^ri i ji ,t iic.nn

uuiinn ^

..'','i:,in nwntmi wuni

100056

ml

Ij the page Yilpned in this frame, is not as readable ...or legible, as. thislabel, it is due to substandard color or condition of, the original page.

•IITver l

•Y&_r . iwiyip/.r MOV -i; 1irt'iiv-r.sr.t .c..-i. - £_= i."» i • •• hfrtriijO i J''*i_fiT . triiOtiCU Nov V.u 1

.r.i.'rHnl. SlHNt'rtllfJ I Hblih i

H" mncn ' itafflR-

, . ...- 1 •' .'.•»•» iy I ,'d617 . -000 Unk nnwn

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l^walir ._r.i'.-i. unt nounllVti'*t>.ui;i Unl:nOHh

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I to,vi •—————————————

O. ______ 100057

ITiii

' U_the page \jil-ed in this <rame is not as rea-able or legible as thislabel, it AS due to substandard color or condition 04* the original panriginal page.



SAMPLE 10: E6284

CLIENT ID: S-5


METALS HDL (ro/kg) RESULT (»s/kg)

AUnONDM 5.00 8300ANTIMONY 0.13 H.D.ARSENIC 0.13 11.6BARIDH 12.5 103BERYLLIUM 0.50 0.68CADMIUM 0.50 H.D.CALCIUM 2.50 545CHROMIUM 0.50 111COBALT 2.50 16.0COFFER * 0.50 209DON 2.50 50400LEAD 2.50 941MAGNESIUM 2.50 783MANGANESE 0.50 649MERCDRT 0.05 1.30NICKEL 2.50 15.4POTASSIUM 5.00 447SELENIUM 0.13 1.53SILVER , 0.50 H.D.SODIUM 2.50 630THALLIUM 2.50 H.D.VANADIUM 2.50 55. 2ZINC . 0.50 ' 142

CIAHIDE 0.10 4.60

100058

Id the page filmed in this frame, is not as ntadablt.j>n l,t,£iblt, aA A-:-label, At AS due to substandard color or condition o< thf/ original page.

\' i Lib HJK ! Bridgeport Environenntal, Inc. I Saiplft Hu-er I-' C«>aNo i N/A I E42B4 I

OflGflNICS ANALYSIS DATA SHEET »••••»-————»(Page 3)

Pesticidos/PCBs

Concentration! /LoV)/t1ediu« ( Circle One I EPC Cleanup _V« _/DoData Extrected/Pre^aiedi 11/13/?0 Separatory Funnel Extraction _ VetDue Analyzed: 12/04/90 Continuous Liquid-Liquid Extraction _ Ve«Cone/Oil Factor: 10,01/10-.Percent toisturei 24.8

C.A.S.Huaber

12674-11-2 Arochlor-lOU. ..... UOOO U11104-28-2 Arochlor-1221. ..... 1)000 U11U1-16-5 Arochler-1232. ..... 13000 U53W-21-9 Arochlor-1242. ..... 13000 U12672-29-6 Arochlor-124B. ..... 13900 U1U97-69-1 Arochlor-1254, ..... 14000011094-82-5 Arochlor-1260. ..... 13000 U

Fon 1 7/8$

100059

Ji».f» ^^ ^^me_ *n f1*-4 a***"* i-4 not as readable or legible as tfcijilabel, At AS due to substandard color or condition oi the original page",

U., .«** Ill" «UI M>flCII-11.-J3LX" I ->.|:l;;. i.K'1. hu.tlBWI- I . IVDI? I •>«'., ,1.

. .1:. A-' • . ' -• iio&nr.U I ."tn..| !• ' . -I-;. wOC "."I l'/-< .:-'! ..l.'.-M'.. M.: '.'-' It" I'ldnori I I1JLI1 L IJini. I*'.: Due .'-* In

• ..:»..('.; :.•>>. " I'.-.' .'it'tnaa i rtuLii i ioi'ii-tn; IKJC &i !•?>'. .

:.';..r.ii,«. ihYiiiWii).r<n :u i: .ni.v li-

'.i'"" i .'..''0'. i.."iii..i»H

:.i.V.I0.1u-»

J .. .•. .i.a'/.nn.-«.«(. ....- .

ii.m m/roHi

_HZ1- •s»u.en

11,IM Dwiumi iiimiirx

23,;)- >H,HI ItUINWIDnOlI.II

I< the page filmed in thiA frame iA not aA ntadabljt...on legible, as.this-label, it is due to substandard color or condition of, the original page.

. - •• '• ••••nnpfi t ui'-'.-»i ' .iiuniiu:,- 'tat • ',"-i;.'. _•_•(.• '.i 17'Vu Kfrtnoii i orpcsT r imc^ios NOV v.o 19i-ii. .tfff , .1 I-,'".1 In ihetl i i.->"'-SI . irmi'liutt Nnv ';Ci 1-W

ii' L l l U t l C n t 1 .WOUL.if! HAM i

r.oivr (<»tmi»

:. i«. i V'.i /" 1 .OC'OUDp rO 1S093,tWOO Unlinom

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- 1 3''i

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V.V6-1

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. • • * ;'i

. IJI.M lOtjn M'I 1 liHijft,.- , _ til -0 'int. ni)Nn

,>XjriODr>TO |S5,T!i.4".7!i Uni.-nnMn

. ,".".'."v*'.i •i/i?') in.. 1 .'.'.- ..i ii-.nnHtt

:;,J:;: _,»,«._,* s:,'-1 ;. i'!i;i*:li)"t ,/,,u/ Lifiarift .il• OO'.'-xio f.' i 1,'Ob VC • -Sui,' Jm nount •(f.v'i.-i '.niii'tn/Lnnufiii

li,'OC".'0»i'U i5D",jQ_;.jV"Ci UnhnoMn

:3.?ii U'Jr'i;; v • LuWOOr-fO lian372.0iM*ni Unknowni",*--.; i*:;-!-; i i,ixit'irxwt-o ".U7171 ,J)000 unlnown

• •-. '-'4 l.!J7D4Se»4 HbD/S&

..1,6r_ -'i iM«Df)-^ Hiftriuiivf.nlat*

100061

I^ the page filmed in this <rawe is not as readabl.e,,or legible.as..thislabel, it is due to substandard color or condition of, the original page.



SAMPLE ID: E628S

CLIENT ID: s-6


METALS MDL (eg/kg) RESULT (ng/fcg)

ALUMINUM 5.00 13800ANTIMONY 0.13 N.D<AKSENIC 0.13 ifi.4BARIUM 12.5 230BERYLLIUM 0.50 H.D.CADMIUM 0.50 H.D,CALCIUM 2.5C 996CHROMIUM 0.50 54.9COBALT 2.50 19.9COWER " 0.50 248 /"">,DON 2.50 29900LEAD 2.50 328QMAGNESIUM 2.50 1310MANGANESE 0.50 744MERCURY 0.05 0,26NICKEL 2.50 16.1POTASSIUM 5.00 £71SELENIUM 0.13 0.51SILVER , 0.50 NiD.SODIUM 2.50 6ZOTHALLIUM 2.50 N.D.VANADIUM 2.50 • 72.7ZINC 0.50 193

CYANIDE 0.10 1.07

o1C0062

U the, page, filmed in this frame, is not aA readable or legible as this -,label, At AS due to substandard color or condition o< the original page.'

Lab Ham i Bridgeport Environiental, Inc. I Staple Nueber ICase* i N/A I E«B5 I

ORGANICS fWLVSIS DATA SHEET «—-———--•(Page Jl

Pe«ticidea/PC8j-*.

Concentration! (uijtlodiui (Circle One) ETC Cleanup „ Yes i/HoDate ExtracttdifrcjUfedi 11/11/90 Separatory Funnel Extraction _YesData Analyzed! 12/04/70 Continuous Liquid-Liquid Entraction „ YetCone/Oil Factor: 10.15/10-.Pircent Itoislure: 27.$

C.fl.S, ug/l orNuater "

12674-11-2 flrochlor-1016. ..... 1)000 U11104-28-2 Arochlor-1221. ..... 13000 U11141-16-5 drochlor-12)2. ..... 13000 U5J465-21-9 Arochlor-1242. ..... 13000 U12672-29-6 flrochlor-1248. ..... 13000 U11097-69-1 flrochlor-1254. ..... 27000011096-82-5 ftrochlor-1260. ..... 13000 U

Fon 1 7/8;

100063

H the. page filmed in this frant iA not aA readable ..or legible as thislabel, it AS due to substandard color or condition bij the original page.

*,'ist i -K'ntmr

i T;U"; » vrij.'!;'.1 He* 01 I1/I rJt.ll I* iftlljGlIl L";; 0>| . /

•-,. i. Latoi

,'.',:. ;•/•••• i ,'.'. . U£ 1 U1. v 7,2{,U -c,

".•I"!!! 1'

*.;Si. Kivss v 1.2UO

.,.• f i] tit -.... ... y,,. . _ .,.,« .

•;• X= .«:?!T ?!.»«

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in. l! r...Ki\ ..VilliH. ..•./.l.TV.I.l'j

r«K fiummn MmJI;.,JOOQTO li.OOOO uninortr.

OUl9Jrt-H -lu.d-K./ D-t'MC;.M7|."» H8PTACHLIW

Cw'liUt* ''o!°uuO uSlnilln

."'i!'l"/u.- iM.i-Mi, ''"-"i.'i.u

i;i. ci'i'iiBP1 • ri,..ot.</ .'r.i.ii'jmifc'.'i/i!'tf*-'i "4.*. J.. 'd Ut'iJ/tMiU •!

-.•..i,'i.ii;i L. j,..: M.. .iinnnrtiiVlQ-4 -0 •.;•,'.'«.( ENBI'dt) hl.LH

,;(f463 -4 '»•.! 7. 30 UNDOaUUFrtN

,vwo «* fa.oouo umnQ«nCHUv_y

100064

I* *_e P_9^ Mi^wed in this <rane is not as readable .or legible as thislofted, it AS due to substandard color or condition o'< the original page.

1 Tvti* i j.tnibit

MriOCl I f.f-'l .Si', . l£l>,"l|l<!i H'jV "'* t'*Bi'i /

• ,i,'. -.'*'? i, ^vuiiittu -II1?1/'/. 1U/!} Unknown•;,7aC _*"t '-n :,OOi.njLi(t+C< 39 334, tJiyj' UnKHONn

: .796 a.-no^tci-s i-ttHC. ,OIX»OPBK> (tlS^.OOdO unrnown

i *;vi '.v. 'j ifiiMinHiiAlarm

I, . '.;••'! .-.r., r'.norirt t*lplt'Mv.}\«., i.'v'.».;'w.' .'i')>j;:t'i'i..ni.''>'' um nown',.; -.!.'-• .'n.i'in i -rv.i.i,.>]')-.- 11

u.a •o

'.i .at,; -• >j'i_;sw-H n.".noi:vcnior'.. 'M.-i.ii'c«' •- "."-t^.< .c.-i; ••<?! 'nun. .'.'I.'.''.'.'!. ".' '|M*'' '' . >,!'.'• ' UN I nOH1"!

100065

I< the page filmed in this frame. iA not aA readable ,or. legible, a>./th.<>label, At AS due to substandard color or condition o(, the original page.


HAZARDOUS SUBSTANCE LIST(uolld) _

SAMPLE ID: E6286

CLIENT ID: S-7


KETALS HDL (-g/kg) RESULT (ng/kg)

AUnOMUH 5.00 1900AMTDtONI 0.13 H.D.ARSENIC 0.13 0.84B-UDH 12.5 H.D.MimilM 0.50 N.D.CiDHIDM 0.50 H.D.CALCICM Z.50 177CHROMIUM 0.50 630COBALT 2.50 R.D.COWER *' 0.50 2.21IBOH 2.50 1900 V_>LEAD 2.50 5.99MACHESniH 2.50 122MAHGANESE 0.50 4.09HEBCDRT 0.05 H.D.NICKEL 2.50 N.D.POTASSIUM 5.00 132SELENIUM 0.13 0.15SILVER , . 0.50 N.D.SODIUM 2.50 281THALLIUM 2.50 N.D.VAHADIUM 2.50 9.16ZINC . 0.50 3.88

CTAHIDE 0.10 N.D.

. 1COOB6

n the page filmed in this frame. iA not aA readable or legible a.* thislabel, At is due to substandard color or condition o< the original page.

Lab NaM i Bridgeport Environuntal, Inc. I Stiplo rtaber ICase No i N/A I K286 I

OREftNICS ANALYSIS MTA SHEET «•-—•——••—-»(Page 3)

Pesticides/PCBs

Concentration! (Cm} ttediui ( Circle Ono ) GPC Cleanup _ Yea JflbDate Entracted/PreHfMi 11/19/90 Separatory Funnel Extraction _ YesData Analytedi 12/04 0 Continuout Liquid-Liquid Extraction _ YesConc/Dil Factor! 10,15/lOiLPercent Itoiature! 1.1

C.A.S.Nualier

12674-11-2 Arochlor-lOU, ..... 250 U11104-28-2 ftrochlor-1221, ..... 250 U11141-16-5 rVochlor-1232. ..... 250 U53469-21-9 ftroctilor-1242. ..... 250 U12672-29-6 Arochlor-1248, ..... 250 U11097-69-1 (Vochlor-1254, ..... 250 U11196-82-5 Arochlor-1260, ..... 250 U

Fon 1 7/85

100087

If, the page \jil-ed in this framt iA not aA readable or ,',e'gib|e as thislabel, At is due to substandard color or condition of, the original page.

:M ; '•••.,'. 11 L I/M i*|iV in. r,'t IIV- Ji-.oH i hJh.it ._-t_._;__i ,-uc ..'t I'/'*M ,iiiarj ' ."JUII i Vl)l')'l|i,l Udfi M'l 17TI.. J

»;•/»«!>— H-W*.t-.|_....l -IHIMNfi

"U.Wl D-BMCILI" nci»c,*.

i .•.-.... I.--I.HLv. J.IH

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".'•" .••l:n—" .'...'ij' ..fL'tril.'.)-! 1T-ii!"'.' ."!*!•""»-* liKBflP. rtuinil'fl'!.'

_.-. in.'./".•« •- 1 /U.^uii- MtA/it'n'tJHtL't-N.tihJ.-OI.=.tiici»wt '

rr-],ui I-IKC••!.!(] :-!af

!;.»,!« .'(WBIW-II

U 0 -

O ! 100068",• -i "~~"l;

• Ipj the pag«. Mi^med i« this ijra-e is not as readable,or legible as thislabel, it is due to substandard color or condition otj the original page.

..;. i.*i_*.4 _" i .; i. .• i M ;,;: fit !•".• wijtno(j i i_,7"t.pr l i-.rsvilu iittc o»i IS^O J

..-.«:-.'. • • . _.. •;. .f.r '••' i';:.- htUiaa i infest L .. -ib'/ilO Due ufl r/y.' ; /*~\-•;rt i _ . , . i i , . _c_ t.i'i ivvv Pi'tnou i wrusi [ fcvi-»viio »nc 0*1 r^o > I l

1 i .-;.'.'.. .i.ANLAKU i fnif.!1) ;

i. U cviini "c1 Crjncn l.air.ir

, . ."vvOs N> "l'uV?( iti'.'a uni.. .i,<ji.« uiu «<t5ci,!ii.ii.'iij , un K

'I1)

1,1 'if l H; '.nOOOU t )' Oil* 1 ,'

i 4 i1 t C

100069

' .'.*_' Pafl(: •''me(' *" *«*•* <*a""e ^ no* <«•* readab|e.,or legible, as this* »label, At AS due to substandard color or condition o< the original page.



SAMPLE ID: £6287

CLIENT ID: s-8

SAMPLE DATE; 11/9/90

METALS HDL (as/kg) RESULT (_g/kg)

ALUWWm 5.00 11500ANTIMONY 0.13 N.D.ARSENIC 0.13 9.90BARIUM 12.5 146BERYLLIUM 0.50 N.D.CADMIUM 0.50 N.D.CALCIUM 2.50 1394CHROHIUH 0.50 28.2COBALT 2.50 9.12r'PER '« 0.50 60.3_.-/N 2.50 16700LEAD 2.50 237HACHESIUH 2.50 1310MAHGAHESE 0.50 732MERCDKY 0.05 1.00NICKEL 2.50 12.3POTASSIUM 5.00 1210SELENIUM 0.13 1.14SILVER , 0.50 N.D.SODIUM 2.50 342THALLIUM 2.50 N.D.VANADIUM 2.50 44.8ZINC 0.50 101

CYANIDE 0.10 4.70

o100070

If, tht page, filmed in thiC frame is not as rea-able^cr legible,as .this-label, it is due to substandard color or condition of] the. original page.

I.-......——..* _Lab Neie i Bridgeport Environiental, Inc. I Saaple Hunter I . iCeaaNo i H/A I E62B7 I

ORGflNICS ANALYSIS DATA SHEET ,......— .......f(Page 3)

Pealicid«-/PC8s

Concentration: (jS) fedim ( Circle One ) ETC Cleanup „ Yee _C"NoData Extracted/Prepared! 11/13/90 Separator^ Funnul Extraction _ YesDate Analyzed! 12/04/90 Continuous Liquid-Liquid Extraction _ YeaCone/Oil Factor: 10.t8/10iiPercent Itoiiturai 28.3

C.A.S. ua/L orNuaber

12674-11-2 flrochlor-1016. . . , . , 250 U11104-28-2 Arochkr-1221. ..... 250 U11141-16-5 Arochior-1232. ..... 250 U5J469-21-9 Arochlor-1242. , .... 250 U12(72-29-6 Arochlor-1248. ..... 290 U11097-69-1 Arochlor-1254. ..... 76011196-82-5 Arochlor-1260, . . , . , 250 U

Fori 1 7/65

100071

U the page, filmed in thiA framt iA not aA readable tor legible as this.-label, At AS due to AubAtandand color or condition o< the. original page.

' -';:.' .'"• . • V Me-thud I **u-li ii IV • -i .' :''"'. "'yt'iflrt i "H.'l.i I

stv«Mt, .-.'f'-iilifUiL' I flM-ft 1 . N'lNUftl.l.v

.'i"iiin;< uni.-nriNn:, iVir ij- jui tiwr,

I3?!SV»IC ft lii Ifi.lNi,Mi«f;

-l.'. .oV I"lliVMl>l>- iH'.Mu'Jll

.;.._--1l, lvbrtC

.,,-/.•,,- .\i.l)li)<J..-.tM.Hn.' Lnt r.ami, ...>.i> jni nJrtii

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. ''l.-ilJ- •;-. 'MLt'-ll

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i/'iSr.l1.J.-. li.:r. .>..;..'.'l-.!il;li -I)«.r,ii.JHnrr-iw,..'UMOWN..j, ;v, v. .'fw-n cwniii nuoEHYBi;

. .••;.i/''0c..»v .'.'•'.'...i., ..jiilrujwn«...'i- • .'; ••:uu..» ill.KiL.uanit slUU'Mi.'.,ii-. ..••;,., , .S3,.VM* ilp..i,M.hO;.|!)Wil i.Nl.-;.J."i...::. • ...i-il/L'-'i l'L-!'Hi..VI:lli.iF

— }.I14 li'MIC•ss'::::i'::_i«ii t-mC.JiS'l.lll IIWIN,-*££L-

.".'"-S5"'1'" *t"*Ml." "Will

5'C;..........;>i.li' fWH—»i,7HNnniii

2U.A " '•>.

• '>'" 100072

H the page, \ilmtd in thiA frame iA not aA ntadabl.e....on legible,as...this-"••<label, it iA due to substandard color or condition 04 the origAnal page.

• '..».' , . ..'• .....i.'!. UM; v" ."•.' . iii'.Mcic. i i_i'l..'_i i .V-it-'M'.v i*i»C O'i i •)'*'> i '. I

. t': 11

.'..." .a.o-.:.'. i. "ill -••

I

" ' '.V'U l'//il6l .l.'l.'il.i iJIM fllltlhujOOUtftO ;'&37ft ''f(i.00ni:i unuMQHii

wfjwu H.I "fy/ji'j.soCiC' um.-nonn.•I'-.io-a : ,u;_'j H-i'n_.'/VV>B-*» -..rcflmti'lf1 Mi_.:ii._:«f-:i -i.svv? i.-hw

i if't .1 ., ... : nuut-chiuiliiiuws •>.• ij -I!// ILIA 1.1 i nmtjwfi.•i-i at"-'* ^.nnri'..'/i.-i'.1"1 HfMirmnlnr *n

.0:.- .'/u*1.' »i ',"''. ; ./.,",_; •'.-(' _iM'

. •..>'.!.'»• ' ' ' _i.'_''tnu'-l., «i

!.'ji:i;ivi'4r'.' i lutlul. /ino urtrnownl.**7!lftH-4 JW.7B9K iTL/BE.M. iS^SBfl-1* 1'Kfiui'vcnlar

!•< the page \jil-ed in this <rane is not as readable,,.<M legible. as..thislabel, it is due to substandard color or condition of, the original.page.

CERTIFICATE Of ANALYSIS


SAMPLE ID: E6288

CLIENT ID: S-9


METALS MDL to/kg) RESULT (_g/kg)

ALOMINDM 5.00 13000ANTIMONY . 0.13 3.55ARSENIC 0.13 1.95BARIUM 12.5 70.8BERYLLIUM 0.50 N.D.CADMIUM 0.50 11.0CALCIUM 2.50 108000CHROMIUM 0.50 8950COBALT 2.50 53.5r™PER '' 0.50 236. ..-,N 2.50 51700LEAD 2.50 4460MAGNESIUM 2.50 13700MANGANESE 0.50 322MERCURY 0.05 0.86NICKEL 2.50 21.7POTASSIUM 5.00 3350SELENIUM 0.13 1.20SILVUR , 0.50 , N.D.SODIUM 2.50 893THALLIUM 2.50 N.D.VANADIUM 2.50 43.1ZINC 0.50 1730

CYANIDE 0.10 15.0

100074

If, the page filmed in this frame, is not as readable .or legible as this' ''label, At AS due to substandard color or condition of, the original page.

Lab Hate i Bridgeport Environmental, Inc. I Saaple NuaberCase No i N/A I £4268

ORSANICS ANALYSIS DATA SHEET • —— — ---- —(Page 3)

Pesticides/PCBs

Concentration! (Wjlfcdiui ( Circle One I GPC Cleanup „ Yea j_DoData E«tracted/Pre)nredi 11/13/90 Septratory Funnel Extraction „ YesDate Analyzed: 12/04/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor: 10.31/10aLPercent Itoiature: 44.2

C.A.S.Huefcor

12674-11-2 Arochlor-1016, ..... 13000 U11104-28-2 Arochlor-1221. ..... 13000 U11141-16-$ Arochlor-1232, ..... 13000 U53469-21-9 ftrothlor-1242. ..... 13000 U12672-29-6 Arochlor-1248. ..... 13000 U11097-69-1 Arocblor-1254. ..... 22000011096-82-$ Arochlor-1260. ..... 13000 U

Fori 1 7/8$

100075s~~*-(J

U the. page, filmed in this rframe is not as readable jtn legible as thislabel, At AS due to substandard color or condition o< the original page.

• -.-a ••'.•. . t iti.ii.- t*c •"• ;i'*"oH-'ia i »: :L T I i 'j'.'t'li'uOl I'-JT i."i j-fi".'"'.rfiO I MM '; j i' .iJ1'i',",i| IV.-- i.'.l ','?!'•

„•;•'_•;_• -iT:. J ... .'"'/irK'iV |'i i.'LlPri! 1 , '.'OlliyOlf H.'VC-

ii.i!KV,t. rVlDflPB ( hrifh t \ tlflWJALLr ALTERRD

'mlao» -•.. iCiOiMXwi.i o.ooiiv'' Unknown

0 1 0 00 Uni.noNni>,!,;'n.'C' Uni.lKiwfi/5. IB'A" hL'r*im:H!.i . ,.oi)0 Jnt'nnun

I-*."611 ii«i)ijiiiJt,fr'«r4I UK. mi v. <H;...H4<niimirUi'L'IIP

100075

I< the page filmed in this <rame is not as readable or legible aslabel, At AS due to substandard color or condition of, the original page.

i.i.-rnnn i Cl'l-i;.' t iivitm H1* hue <,'•» 1770 .'"JMoiJ I LM-'Utii '. Hfcl'l'. tli. hire O'l l'i"fo j

( 5V!J7, ai:.i' uni nown{-^Sll ,Ou.uO Unnnonn2 WO. d US unl 'nowri

Unt.-nouriioQt«cnlar

• V - .n'. .on. i ;..S'lj,_,..,,-.- lliunrlul., >.'i» • . .ir.V'l?"" fe'tnnou] t.in •;

- . . .•.••f.r...... •• ':.O*K'2. _?Si;« Mm nywn

:". ' <'* '.(t?--.'«••'( :niicniuH»n tun .win

i-ir:/'1. ... i 'wfl-4 "" nor'.,),'.»: n («»)> j iHSBIiiiOii'.ni unt;nonn

T(1,0 «—

3.. i

"^

/I E T . 100076/ 11,11?

Id the page filmed in this iSrame is not as readable .or legible, as.thislabel, it is due to AubAtandand colon on condition of, the original page,

Q C RESULTS

100077

U the page filmed in this <rame is not as readable or legible as thislabel, it AS due to substandard color or condition oij the original page.

QUALITY ASSURANCE DATA

ANALYSIS NO: E6275 BATCH NO: H331

MATRIX: Aqueoua

HETAL AHOIIHT OF SPIKE I RECOVERY X DUPLICATE SPIKE RECOVERY

LEAD 50 ppb 101 100

100078

li the paga \jilmed in this ^rame is not as readable or legible as this.label, it is due to substandard color or condition ojj the original page.

QUALITY ASSURANCE PATA

ANALYSIS NO: E6276 BATCH NO: M331

MATRIX: Aqueous

HETAL AMOUNT OF SPIKE Z RECOVERY Z DUPLICATE.SPIKE RECOVERY

LEAD SO ppb 103 108

100079

If, the page filmed in this frame iA not aA readable .or legible as this nlabel, it is due to substandard color or condition of, the original page.'

QUALITY ASSURANCE PATA

ANALYSIS NO: E6277 BATCH NO: M331

MATRIX: Aqueous

METAL AMOUNT OF SPIKE I RECOVERY I DUPLICATE .SPUE RECOVERY

LEAD 50 ppb 116 92

1000SO

•;' 'U the page \Jilmed in this frame is not as readable ...or legible, a,i .this„ label, it is due to substandard color or condition of, the original page.

QUALITY ASSPRANCE DATA

ANALYSIS NO: E6278 BATCH BO: H331

MATRIX: Aqueous

METAL AMOUNT OF SPIKE X RECOVERY Z DUPLICATE .SPUE RECOVERY

LEAD 50 ppb 111 111

o100081

If, the page filmed in thiA frame iA not aA neadab.'jl-pn ttgible as..this-label, it AS due to substandard color or condition oi the original page.



ANALYSIS NO. E6286 { I

BATCH NO. M330

MATRIX: Solid

METAL AMOUNT OF SPIKE (ug) Z 'SPIKE RECOVERY Z DUPLICATE RECOVERY

ALUMINUM 10000 100 98

ANTIMONY 50 96 83

ARSENIC 50 101 101

BARIUM 1000 108 113

BERYLLIUM 1000 104 109

CADMIUM 1000 95 99

CHROMIUM 1000 102 109

COBALT 1000 102 106

COPPER 1000 113 116 _

IRON 10000 98 96

LEAD 10000 101 101

MANGANESE 1000 97 104

MERCURY 1.00 97 97

NICKEL 1000 100 104

SELENIUM 50.0. 115 111

THALLIUM 50 99 _Q4

VANADIUM 1000 104 116

10000 96 100

100082

If, the page filmed in this frame iA not aA readable..or legible, as this »label, it is due to substandard color or condition of, the original page.



nBATCH NO: M 33°

MATRIX: Solid

METAL METHOD BLANK (BE/,.) AMOUNT OF SPIKE (ug/L) X SPIKE RECOVERY

ALUMINUM «'D- 1000° 10S

ANTIMONY »•">• 50 103

ARSENIC »•»• 50 10Z

BARIUM »•»• 100° 103

BERYLLIUM "-D- 100° "

(aaoDM »-D- 100° 90

CHROMIUM "•"• 100° "

COBALT '. "•"• 100° 9B».D. 1000 98

I.D. 10000 102

H.D. 10000 106

IJARGANESE "•"• 100° 103

MERCURY "•"• * *"'

»•»• 100° 98

SELENIUM "• ' "

THALLIUM "•»• 50 8Z

VANADIUM ••»• 100° 99

"•D< 500° 98

O " • • 100083

Id the page Mi^med in this <rane is not as readable jn legible, as thislabel, At AS due to substana"ard color or condition of, the original1 page.

H •• ? ' , _ * _ , /Tca * I " - C

S

n•q

'I

fRinMi?ac

1

100p84

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iy

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1

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tf

9

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1

sH

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P H

^H S S"igo§

1

11 tt

S5£

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2EWATER PESTICIDE SURROGATE RECOVERY

>b NameiBridgeport Environmental, Contract : N/A

sb Code; NJ 08555 Case Ho.: N/A SAS No.: N/A SDG No.: N/A

1 ERA1 SAMPLE NO.

01IPBLK 266-202I_E628Q ____031 MSQ4I MSD051061071OBI091101111121131141151161171181191201211221231241251261271291291301

SI 1 OTHER(HBB)*I

135__U2_11990

BB) • Hexabromobenzene

. ———— ,

ADVISORYQC LIMITS(24-154)

# Column used to flag recovery values

* Values outside of QC li m i t s

D Surrogates diluted out

.go 1 of 1_____ FDRh II PEST-1____________ 1/87 Rev.

If, the page filmed in this frame iA not aA readable .or legible as thislabel, it iA due to substandard color or condition oi the original page.

2FSOIL PESTICIDE SURROGATE RECOVERY

»b NameiBridgeport Environmental, Contract : N/A

tb Code: NJ 08555 Case No.: N/A SAS No.: N/A SDG No.: N/fl

jvel: (low/mod) LOW

I EPAI SAMPLE NO.

Oil PBLK 288-502lmPBLK 292-1.,03|_E62B1 ____041 E6282 ____05I_E6283 ____061 E8284 ____07I_,E6285 ____081 E6286 _____09I_E6287 ____101 E6288 ____

121 MSD131141151161171181191201211221 ___231241251261271 ___281291301

SI I OTHER(HBB)#I

109JL14_D_D_D_D_D

ADVISORYPC LIMITS

51 (HBB) - Hexabromcbenzene (20-150)

4 Column used to flag recovery values

* Values outside of OC limits

D Surrogates diluted out (J

»» Surrogate recovery cannot be calculated due tocoelution of PCB 1260 and HBB peaks.

age 1 of 1FORM 11 PEST-2 1/87 Rov.

I(i the page filmed in this tframe is not aA readable..or,.legible.as,tfcis.label, it is due to substandard color or condition of, the original page.

3F

! JUEOUS PCS MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

NameiBridgeport Environmental, Contract:N/A

Codes M 08555 Case No.: N/A SAS No.: N/A SDG No.: N/A

rix Spike - EPA Sample No.: E34S5 ''Level! (low/med) LOU

COMPOUND

rochlor 1016,., _„...,.rochlor 1221 . . .. „roohlor 1232:rochlor 1242rochlor 1242.rochlor 124B _rochlor 1254in lor 1260, ,..,,

COMPOUND

.rochlor 1016 , ,„„., ,

.rochlor 1221 ,

.rochlor 1232,,,, ,,,, , ,. l,rochlor 1242irochlor 1248.. . ., „ ,. ,,.rochlor 1254irochlor 1260 ,

SPIKEADDED(ug/L)

N/A50

N/AN/AN/AN/AN/AN/A

1 SAMPLE1 CONCENTRATION

<ug/L)

O.Q0.00.00.00.00.00.00.0

SPIKEADDED'(ug/Kg)

N/A50N/AN/AN/AN/AN/A •

MSDCONCENTRATION

(ug/Kg)

N/A74N/AN/AN/AN/A

MSCONCENTRATION

(ug/1)

N/A52

N/AN/AN/AN/AN/AN/A

MSDX

REC ft

N/A147N/AN/AN/AN/AN/A

SRPD ft

N/A34

N/AN/AN/AN/A_N/A_

MS1 H

REC ft

N/A104N/AN/AN/AN/AN/A_N/A_

QC LRPD

QCLIMITS

REC.

MITSREC.

lolumn to ba used to flag recovery and RPD values with an asterisk

'•lues outaida of qc limits

): 0 out of 6 outside limits 1000 7.ke Recovery: 0 out of 12 outside l i m i t s 4.UUU-M

1MENTS: BA 266.

FORM 111 9/90 Rev.

/_J/e SJ9;. 1""* *" _*** ^flme no* " ««<<««e ox legible as thislabel, it AS due to substandard color or condition orf the origin«/Jag£(

*- <<; »« jugs : SK! i HISS W S

.••MMini flTONimni) i ARM i

*„. K B-PRI «• ""•"« •""u l lAOMttO 9MIW.WOO UnVnoxnv ', ooo,,g MM9.0COO UnhnoHO

' «S«.S6!3 UnknQHnI.7W.9S7S UnHnsm

SSS:SSIl(aol7""s"

Ml! i 111T ' "iWWi«0 S5BS9I.MOO

,w; S T !"1r*

i ». SWW.BW

MWS.WW Unkno-n . •.

X-x'

. h.' ft S

|«_

N ti M H NC U t f »s ': f t f

« Ft it ! nc it

100088

li the page \pjilmed in this <rawe is not as readable ,or legible, as thislabel, it iA due to AubAtandand colon on condition o. the original page.

.'l'i'JWU rtvml !t i:«»9«nant N|,«o«r i I Tvp» I Unwilt

uctum'tV/ilM.* mm '•'•' ' "":' 111'""!! ' ""l." c ISiSSiW nufl 0= I99D )HI 4Hunt Minimi.-. '««l v.1 iv"" niiitiinl i niK.il I UiJSlJV nun gi' i'i'/i, Jn i iMidiv* nuii u.i iwv finthoo i null I I OHiOuu*. mm us uw Jl>l \i I .uiMXnnXiO PMIutimi I.OOiMU»««iO

i I rcKNAl. STflNUflhU I (WEfl I

.1 nr.. K EllBFiT RF PICMRAna N...

153750 1UfaUSJ? 1

IS'.B "

.449 III33I T

.7*0 . 40117 T145. /ISS705 T

'.1S6 ««' T 4.I4W4S9 94G7B T 4.497;K 40412 1 9.011:M :»llMl :7U4i'l 1.415Iv-i si.'!!.'. '>.•>!>.'

IO.QI111,371

UnknpnnUnknpnnUnknnnnUul'minli

M>u6.>li'/ti UnHnpwn131:31.4688 Unknpnn40147.3031 Unknpnn

.OOOOO.tO 133703,6330 Unknpnn

.OOOOOntO 301303.9373 Unknpnn,930561-4 A-BHC.iMmiXicitrj 'l',i4llS.I,'.'50 Unknpnn

3.5641.BIG

,90640*-4 19,0903 HEPTACHUQR. IBOIB.-4 17,3078 D-BHC.1Q742I-4 9, 8479 (1LDRIN.ODOOOQtO 3f.lll.'J/M) UnhnQnn.»IJ07i-4 J.A'17 HBPTW!Ml.l)» Win I ISi :. I.NIIU-I

PP-DD6»Ut-4 DIEUOnlN

tut IttlOlt 13. 85! 2, 384781-4 6.3751 CNDRIN16,976 3.3143M-1 OOU/tHCU-l I19.843 i,7t337.-« PP-CPI31,313 ;,36490>-4 ENDRIN HLOEHrDE

U8D 100707 23.830 S,91330t-4 39.7611 ENDOSUkFdN UUUFftTE473 71Q733 T 31.969 S, 649791-4 19U.IS93 HEX«6llOnDUtHJENli.'ai;117 2B9902 1.00000«»0 VOW!, 0009 Unknonn . ,

».1J; 4,6ll}4«-4 nCTHOXVCHUOR

3 ,« «»»-'"•«•» «"j ' l 4'f'i>

N T ) N M

t«,i +

,9,1 •

it.i •

II )>,« i

100069 !

IlS the page Yi^med in this <rame is not as readab|e.,or legible as this-label, it AS due to substandard color or condition of, the original page.

3F

SOIL PCS MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

3 NameiBridgeport Environmental, Contract:N/A

3 Code: NJ 08555 Case No.: N/A SAS No.: N/A SDG No.: N/A

trix Spike - EPA Sample No.: E6241 'Level:(low/mod) LOW

COMPOUND

Irochlor 1016Irorihlor 1221Irochlor 1232irochlor 1242irochlor 1242Irochlor 1248irochlor 1254irochlor 1260

COMPOUND

irochlor 1016irochlor 1221frochlor 1232irochlor 1242irochlor 1248trochlor 1254Irochlor 1260

SPIKEADDED(ug/Kg)

N/AN/AN/AN/AN/AN/AN/A

1000

SPIKEADDED(ug/Kg)

N/AN/AN/AN/AN/AN/A

1000

1 SAMPLE1 CONCENTRATION

(ug/Kg)

Q.O0.00.00.00.00.00.00.0

MSDCONCENTRATION

(ug/Kg)

N/AN/AN/AN/AN/AN/A

1300

1 MS[CONCENTRATION

(ug/Kg)

N/AN/AN/AN/AN/AN/AN/A890

MSDN

REC «

N/AN/AN/AN/AN/AN/A130_

SRPD ft

N/AN/AN/AN/AN/AN/A35

1 MS1 XREC *

N/AN/AN/AN/AN/AN/AN/AB9

QC(LIMITS1 REC.

QC LRPD

HITSREC.

Column to be used to flag recovery and RPD values with, an asterisk

Values outside of qc limits

): 0 out of 6 outside limits•.ke Recovery: 0 out of 12 outside lim i t s

1MENTS; BA 288.

luuoyo

FORM III 9/90 Rev.

If, the page filmed in this frame is not as readable or legible as thislabel, At AS due to substandard color or condition of, the original page,

I •-: '• ..'"'.. . ..'il'lli I0u thl HlU»»m«(W. i ':: fvot i &«mp|»> u.' i .1 -•.•::;.:,u'..». i .ii-:i:i we '.c iviij .lotnon i ".ui.ii i IDHSI.I& L'.I- i.; 119(1 jInuprmoni u'ti/ino rue ,c, 1*10 notnoo i nui.1I : ,<,i.>5i46 u«; 05 IWi )>«wt , i:tii>ti,t in. v: ivx- -.nan i HULTI i lotusiM \at os 1990 I

f \ iiiffipl

..lOOi!) Jnl.nph'...0000 jnknpn

( ,. L'HL' Unl.nflnn

T.496 ;.MS77«-«. ,Voi ..^HliViB-l -l.llioo ll-HHC-.lOCi •,:.I79M«-A i.i'HBi-

...i gCW*.'.. •. . ijui.ii.i

6.?- 72757S 1 O.OOOCJOt^O v.OOOO unnnnnnJ.l'lt 735.167 T V.90C .•,331191-4, 35.9S5B ENOD-IB.IS ' 4S«sVi' v I.I.OIWCIMV v.VUMi Unlinp»r

>, . , ..u..l»- likin. 341 A 763 II 1 O.OOOOfmtO v.OOOO Unknpnn11.107 145310 v O.OOOdOtn'i .'..;MUU unhnn.r<

\ I1.US3 :;.B«H7l«-4 ENBR1NU.a;- )S8"3'." " %'.(i4<iMwt(i 0.00'.*.. unKnonr.(::v.v;i v 17.14.055 Vs;?'.''a T O.OOOOOotO 0.0000 unlinonn

14.450 S,160:SO"H fP-l)DT17.231 (I6a4':i« .;i,uC,W"iinii :.,«nv, .jniinpnn

^ :..,':.'.' •LMamv-ii BNURINJl.S7i HHIVI: '

T :t,164 -.1449711-4 !7o,8409I'j.OOOOC'p O C>,M'>;iC> Unhnpnn

.U.060 7.0B667«--

, -<! « U t * «t : i : c s

i ••»•

100091

Ifj the page filmed in this iSrame is not as readable or legible as this-label, At AS due to substandard color or condition of, the original page.

.;ilUc'.>:r. I .LlMlVi !« ,V! \11v :ictncd I nuuT! t IOI4SI46 5«r 03 H90 I\r •.nan-.iHtt .JiS'.H!! !>- o1.' il'':1 fQtnos i rji.ri ; iui4MH6 If: 03 I9»ft :I'.awr.f -. i :'!•• -.1 .iiu' ...' si-*, "ss.ua i .-L.i.n .. KM'i5i4f. .«« u'J 1940 )

rj.i.oOM <*ni nownO.oywo ,unl:nphnO.i.'yC'O 'unknuwn0.0000 Unknpn".js.snvs n-wn

J',,I4J1 D-DHC

n,T/t ;i,-w.'- 0.i.<p."X'...»+o i''.0'.'''Xi unknownft, 645 <*l*?6-» • 0 . .';OCii.H'.'»+0 0.0000 Unknown

i,l')S EJ.!3'7:0>-3 HfpTflt'llLOfis.11;!: -*.ua70 T 0 . 'X'MOaTO 0.0000 Unlinonn7. M,I .:,'..ivi i i.. i,,r. .',:.T«»,O..(I IS9.P/W l"NI)0-iU.^VI .'lif'll I ',. A.'.'WWH> II.I.U.JI.. Ulll M(>nl.9,341 IS'.HV T B, 9V l./4!77e-4 '.'6.425V PI—UkE

7, MB !.«r9:!u-J DIGWRINO.oOOMoK' 0.0000 UnhnonnO.'ivO'WB'O O.ooOO gnlmpm

11.6:3 3,S947le-4 tNDRINo.i|.X"X'V<u 0, 0000 UnKnown

O: V 1C.90:. 3.1f)374p-4 la.uTIt DDP/ENDq-llI6,n'i9 -Aim"! '' u.iWidfmiMn D.oi'ifif. unKncmn

I*,, •»»!.• U.^W^OIt-4 H'"l)IH17.245 U'sCMD «J.OC.OOO«rO U.OOOO Unknpnn

18.437 3,;6i99>-4 tNUFlIN AUOEh^DE:ii60B I'!I347 1 O.uOWOt-f. 0,0000 Unknpnn

V'2,64* 3.:i'7;a«-<. CNDOSULFAN SULFATE:3,10? l:oc043 V ;;,I64 4.l«670it-4 SSS. 6199 HEXflURDNODENIiNE-sE30.014 mi)4994 0.00000»»(i O.OOilO Unknown

51.060 7.0B667P-4 M6THIHYCHI.OR

» s> !PF3 _ M,mu> hi),o«K'1

100092

H the page filmed in thiA frame is not as readable .or legible as thislabel, At AS due to substandard color or condition of, the original page.

BE^ PESTICIDE EMALUATION STANDARDS SUMMARY, sluation of Retention Time Shift for Haxabromobonzeno

ib NameiBridgeport Environmental, Contraot:N/A

ib Code: NO 08555 Case No.: N/A SAS No.: N/A SDB No.: N/A

istrument ID: PE-1 GC Column ID: PRIMARY

ites of Analyses: 12/03/90 10:10 to 12/04/90 20:04

•J

1 EPA 1 LAB SAMPLE1 SAMPLE NO. ID

Oil IPCB 1221/1254021031

PCS 1016/126Q_PBLK 266-2

041 IE628D051 IPBLK 2U8-3061 IPBLK 292-1 _071081091

PCB 1016/1260_PCB 1221/1254_E62B5

101 IE6286111 IE62B1121 IE6282131 IE62B3141 IE6284151 IE62B7161 IE628B1711811912012112212312412512612712BI301311321331341351361371381

DATEANALYZED

_12/Q3/90__12/03/9Q12/07/90

_12/03/90,__12/03/90_,_12/03/9Q_12/04/90

_12/04/90__12/04/90__12/04/90_._12/04/9Q__12/Q4/90__12/04/9Q,,_12/04/90__12/04/90__12/04/90_

TIMEANALYZED

10:1013:0413:47U:2515:0615:4507:3508;2515:3516:1616:5917:3618:131B:5019:2720:04

———— 11

SD„

_o.i_0.2_

_o.i_o.i_0.1

_0.6_0.4_D

_0.1^DD0.6~ D0.2-D

fWJS

i* Values outside of QC limits (2. OS for packed columns.0.3H for capillary columns)

»m

q_*

ge 1 of 1FORM UIII PEST-2

H the page filmed in thiA frame iA not aA readable or legible as thislabel, At AS due to substandard color or condition of, the original page.

. «u_r i :.i.*ir' £« ol mo flotnon i nuuTI . v7ior)i3S DKC gs WO Jnt.:*: '.-t','-' if?i 0" 1'*'"' !«i?r.rK»fi i MUL "J t I'.''|4!J|46 Dur O'i l-'/V't :

., .. i . i-e •'• !• !'• ip'.frtiJ i l..&'t . ^''lllil'/ tbr. '.'v l-''i" J

hltt ! 1 .',"•• I'-'l-'V-*1.1-'!.. UllUtlOl't i .OCiOin.ipi-001.'

,i6S l'Bi6; v l,i*.ui.0>*

S67 ilvJ1; '1 I.V'XKmt107 i-l'Mt; t J.065 A.HSiK'l)-

.ava a»:it • l.ilwut*,1*1 B'.P|J'!I ' iiiaS 4,s i.i ',p->>i3Z «3'4-', " 1 , OOOUUtf .•a>. .'„••£; • .•.,;ii'. •;.ir'i...iu»i'.l; 'a>'lb ' ' ' lixv'iiU'..'s' ^..|i '. ,«."«lnr

llA" I.1.'*.... ..'.".... J1.1 *

3..-. .i""i'. •« ^ .i 'j .'..i''.J3 ••

J 49866S.OOUO19467.21)13

r/Mvioli:920«v.VltJU99S6.6U5I

adSle.iiiiOOMS6.0V034nsi]4. i«30i62'..;6'j?07011!. ?tdutMl'I.VKU

^JMK .!..' ...

:t;:i.;:0«;;..K*n

'iuO.OX'O

'.'nttnoHn

unknown.inKnoNMi;??iunKnpMtiln*lUnknonnU'-liinMiomunK-norih

-.'Hi n onnUni.nOHh

'ibU-ii;.

ri'iii————i.nt i»i

100094

H the page \jilmed in this <rame is not as readable or legible as thislabel, At AS-due to substandard color or condition of, the original pag'e,

t, , .. ,,, : ... !-. ,:,,-; ;'.',o '.no dillum*, tt. " _ t_ i vi»« i ruiinim-

•>*4ifc<:-_;'i i i:t';-iiH five 0.; l?i» ivtnao i ruuft ; .tfctSHt, u*c 05 1*90 JIr.t.-rniont I'l'.-fl-: JVc H-* f.-V, i-flthoa I MUuTI C 1 a 1 86 1 33 &«c i* 1»90 1'_•;-.•• I ..II-.HI was O-i 1 ; '. Hrtt-.hfi.l t MULT I . ..OHUlOl !)t!- '>H I1? 'JO i

i'l' • -.'UA 1 \ MWHUflLLV

n , 1.11,11/1 ' 'jr.i'noHn

CilvJ :'.'iuj!l ' • .iii S.VI'MJD-l !».71,'liS

ilBMMCMLUh R'-'U-UDuI'.i.iUl.n .Jill nOHd

•! , VI1"!.1 Ulll IT

iitiX'OO uni noun!>-,. /H-I; t/Du/BNAD-l !

1 1 H'II..I:OO+ "".,%>«••-«

SUUFftTEM';ir.t)f.uMiiuDJMnNr;'?.&111-tllOXYCHi.Qh

_ ame "" «* ««<<««« or lwible,,as thi*label, At AS due to substandard color or condition ol the rigi'al page

;. Iki.Nh.. ii.'iiniMi.i. . ..i.;.' 1 - .'IMI.UHU... ....-i''

M

l.'.tW -S.063MR-

fl-t'HCLlllU.W

, AUCIilM' HEPTf.uHUOri 6POX1DE

ENDU-I

DICUDrilNCNt/hlll

-Q.S370 UDD/ENDO-IIpr-noreilDOSULFAIt SULFATE

-i.in !•

'ii.in »«,'[*»• 11l I'

. , |II.M) PIIIIH (tlfflltl

jo.a - '. '

'"--——.——j>,» - """ i'O.in imnmraiM'n

100096

timed in this rframe is not as readable or leaifcle OA tki\iue to AubAtandand colon on condition olthe9o"gi"i* e.

• •' Ivfiii i -jAin.ii

. ,' ; :.-.'»..•: p.uni :';,:3t... _-pf? (t* IW 'i -jiao i «iii..n t ;6iC.1i^5 Put '"• i'••:.'. .' ' • - . ; • - f hilt,'?.--1. _». ..-I l<Wij Mif(.'-atl i fllA'M I 2-Ji»ii,'H''| C.»i: i'i»i !"v, .

^tOOuO unknownt.' , >X>00 Un knottn

«.."•» li'/nftj-i i•«. Md /iAOOftfi 1 t.SOU 2,176730-t ','i., ?C7-J AUSHlN

/ nV' 'i i tiiOOVO'.'Hfij o.Ciyjo unknown.' n'iu4 'i C',iVtJi'iiii.''i;»i.- '"',i.n.'1'iO wfihnuMti

-, f . -1200 • i.'ii.".'i.'.."'ii*i.1 i.iiOUOC' i:nt'.now(i..H".' Ifayrtw t ..'/ij J.uOft**-* -W.^/Oft fli'p7i«.hi.i'in t'rCKtil'r..'. »i, . ifWn- (.svMi'f'Mi11*'!' '.'a vO'>y unt noun

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100098

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8E-N PESTICIDE EVALUATION STANDARDS SUMMARY

I aluation of Retention Time Shift for Hoxabromobonzone

| ab NameiBridgeport Environmental, Contract:N/A

ab Coda: NJ 08555 Case No.! N/A SAS No.: N/A SDG No.: N/A

Natr-m-nt ID: PE-2 GC Column ID: CONFIRMATORY

ates of Analyses: 12/03/90 13:47 to 12/04/90 22:15

1 EPA1 SAMPLE NO.

O i l021031041051061071081091101111121131141151161171181191201211221231241251261271281301311321331341351361371381

1 LAB SAMPLE1 ID

IPCB 1016/1260IPCB 1221/1254PBLK 266-2IE6280PBLK 292-1IPBLK 288-3E6281IPCB 1016/1260.,E62B2PCB 1221/1254E6283E62B4E6285E6286E6287E62BB

DATEANALYZED

12/03/9012/03/9012/03/90

_12/03/90_,_12/Q3/9Q_,_12/03/90__.12/03/9Q__12/04/90__12/04/90_12/04/90_12/04/9012/04/90

_12/04/90__12/04/90__12/04/90_12/04/90_

TIMEANALYZED

13:4714:2314:56,15:2916:0317:1017:5608:3B09:2711:3315:4416:1916:5121:0021:3722:15_

SD

_0. 10.40. 10.0

_0.2_D0.3D0.3DDD0, 10,2D

___

I*

__,

/ « lvalues outside of QC li m i t s (2.OS for packed columns., _nno0.3* for capillary columns) jOOUo"

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100102

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-»,(» _ _.-,.«, 100103

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PEST/HERB/PCB ^^ BLANK SUMMARY

ab NameiBridgeport

ab Code: NJ 08555 Case ^O.i N^ QflS No.s N/A SDG No.: N/A

)b Sample ID: BA266 Uab File ID' BLflNK #2

at rix: (soil/water) WATER Uovel s ( iow/med) LOW

ate Extracted: 11/13/9Q Extraction: ^SepF/Cont/Sonc )SepF

ste Analyzed (1): 12 03 5,0 Pate Analyzed (2): 12/03/90

ime Analyzed (1): Uftj? Time final yz"d (2): 14:56

istrument ID (1): PS>i 'natPunient 1° ^2): PE-2

: Column ID (1): PRIORY SC Column ID (2): CONFIRMATORY

THIS METHOD BkANK AfPUlES TO THE FOLLOWING SAMPLES, MS AND MSDi

DATE I DATE ISAMPLE No- SIMPLE IP I ANALYZED 11 ANALYZED 21

1MMENTS:

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100105

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4CPEST/HERB/PCB METHOD BLANK SUMMARY

ab NameiBridgeport Environmental, Con tract: N/A

ab Code: NJ OB555 Case No.: N/A SAS No.: N/A SDG No.: N/A

sb Sample ID: BA2BB Lab File ID: BLANK #3

atrix: (soil/water) SOIL Level :( low/mod) LOW

ate Extracted: 11/13/90 Extraction: (SopF/Cont/Sonc )Sonc

ite Analyzed (1): 12/03/90 Date Analyzed (2)1 12/03/90

ime Analyzed (1): 15:06 Time Analyzed (2): 17:10

istrument ID (1): PE-1 Instrument ID (2): PE-2

: Column ID (1): PRIMARY GC Column ID (2): CONFIRMATORY

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:

1 EPA1 SAMPLE NO.

Oil021031041051061071081091101111121131141151161171iei191201211221231241251261

LAB 1 DATE 1 DATESAMPLE ID (ANALYZED 11 ANALYZED 2

E5281E52B2E52B3E52B4E52B5E52B7E52BB

_12/04/90__12/04/90_12/04/90

_12/04/90_12/04/90_

_12/04/90__12/Q4/90_,

12/03/90_12/04/90__12/04/90__12/04/90__12/04/90_12/04/90..

_12/04/90_,

JMMENTS:

100106

O-.go 1 of 1

FORM IY PEST 1/87 Rev.

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100107

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4CPEST/HERB/PCB METHOD BLANK SUMMARY

ah NameiBridgeport Environmental, ContractiN/A

ab Code: NJ 08555 Case No.: N/A SAS No.: N/A SDG No.: N/A

ab Sample ID: BA292 Labfilo ID: BLANK #1

atrix:(soil/water) SOIL Levo1;(low/mod) LOW

ato Extracted; 11/19/90 Extraction: (SepF/Cont/Sonc)Sonc

ate Analyzed (1): 12/03/90 Date Analyzed (2): 12/03/90

ime Analyzed (1): 15:46 Time Analyzed (2): 16:03

istrumont ID (1): PE-1 Instrument ID (2): PE-2

: Column ID (1): PRIMARY GC Column ID (2): CONFIRMATORY

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:

1 EPA1 SAMPLE NO.

Oil021031041051061071OBI0911011111211311411511611711BI191201211221231241 ,'251 ''261

LAB 1 DATE 1 DATESAMPLE ID 1 ANALYZED 11 ANALYZED 2

E5286

•"

_12/04/90_ _12/03/90_

100108

3MMENTS:

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If, the page filmed in this frame iA not aA readable .or legible, as. thislabel, it is due to substandard color or condition oij the original page.

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UbKaiai Bridgeport Environmental, Inc. I Saiolt Nuabar ICm No i N/A I PBLK 266-2 I

OR9ANIC5 ANALYSIS DATA SHEET (................t(Page }>

PetticidBS/PCBs ••

Continuation: t \s&j Ifediui ( Circle Una ) GPC Cleanup _Vnj _.NoDale Extracted/Prepared: 11/13/VO Saparatory Funnal Extraction _,YaaData Analyiad: 12/03/50 Cantinuaua Liquid-Liquid Entraclion _ VaaCone/Oil Factor: 100iL/5_.Perctnt tloisturo: N/A

C.A.S.Nuibar iig/Kg

12674-11-2 Arochlor-1016, ..... 1} U11104-28-2 Arochlor-1221. ..... 13 U11141-16-5 flrochlor-1232, , . , , . 13 U5J«?-21-9 Arochlor-1242. ..... 1J U12672-27-6 Arochlor-1248. . , , , . 13 U110??-69-l Arochlor-1254, ..... 1} U110W-62-5 Arochlor-1260, 15 U

Fori 1 7/85

.100110

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Lib HIM : Bridgiport Environmental, Inc. I Saipla Nuafcer ICate No : N/A I PBLK 280-J I

ORCANICS ANALYSIS DATA SHEET t................*(Page 3)

Pesticidea/PCBs ••

Concentration; ^ Low , flediui ( Circle One ) GPC Cleanup _, Yes j. NoData Extracted/Prepared! 11/13/90 Separator^ Funnel Extraction _ YeaData Analyied: 12/03/90 Continuous Liquid-Liquid Extraction _ YeaCone/Oil Factor: 10.00g/10ilPircant Itoisturei N/A

C.A.S. ug/L orNuabir

12674-11-2 Arochlor-1016, , , . , . 250 U11104-28-2 Arochlor-1221, ..... 250 U11141-16-5 Arochlor-1232, ..... 250 U53W9-21-9 Arochlor-1242. ..... 250 U12672-29-6 Arochlor-1248, . , . . , 250 U11097-69-1 Arochlor-1254, ..... 250 U11096-82-5 Arochlor-1260. ..... 250 U

FOM 1 7/85

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100113

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Lab Nan i Bridgeport Environmental, Inc. I Saiola Nuriter ICaaaNo i N/A I PBLK 292-1 I

ORGANICS ANALYSIS DATA SHEET ..................(Page 3)

Pesticides/PCBs ••

Concentration; > _oj> IfediiM ( Circle One ) GPC Cleanup _ Yet _. NoData Extracted/Prepared: 11/19/90 Sepiratory Funnel Extraction _ YeaDate Analyzed; 12/03/90 Continuous Liquid-Liquid Extraction _ YoaCone/Oil Factor: lO.OOg/KM.Percent Matures N/A

C.A.S. ug/L orNuiber /ub7Kr,

12674-11-2 Arochlor-1016. ..... 250 U11104-28-2 Arochlor-1221. ..... 250 U11141-16-5 Arochlor-1232, , , , . , 250 U53469-21-9 Arochlor-1242. ..... 250 U12672-29-6 Arochlor-1240, ..... 250 U11097-69-1 Arochlor-1254, ..... 250 U11096-62-5 Arochlor-1260. ..... 250 U

For« 1 7/85

100114

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Bridgeport Environmental Inc. u.,««iA..ylic,iui»r.wri«, W[,___________________________________________________j_08665__§lP.O.Box 247 609/467-0380510 Heron Orlva Suite 107Bridgeport, NJ 08014-0247

WESTON

PROJECT: SNOW HILL LANE

DATE RECEIVED: NOVEMBER 16, 1990

RETORT NO: E6327-E6330

BRIDGEPORT ENVIRONMENTAL, INC.

RICHARD W. MUCH ALABORATORY MANAGER . i

IV0116

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r-AMPLE LOCATION AND IDENTIFICATION

ANALYSIS HO. CLIENT ID

B 6327 W8

E 6328 N9

B 6329 SI

E 6330 S10

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METHODOLOGY SUMMARY

METALS Soil Samples for- metal analysis ware run inaccording with the methods prescribed in SW846.This includes a nitric acid digestion followedby either Furnace, Flame Atomic absorption,Flameless Atomic Absorption, or InductivelyCoupled Plasma analysis,

Aqueous samples for metals analysis were runin accordance with the methods prescribed inMethods for Chemical Analysis of Hater and Hastes,EPA-600/4-79-020 March 1983.

PHENOLS Analysis performed according to U.S.E.P.A. 420.1(Spectrophotometric, Manual 4AAP with distillation).Phenolic materials react with four (4) Aminoantlpyrineand Potassium Ferrlcyanlde at pH 10, Red coloris read at 510 nm.

-CYANIDE Analysis performed according to U.S.E.P.A. 335.2(Spectrophotometric with distillation). Sampleis reacted with Chloranlne-T to produce Cyanogen,Chloride, CNC1, Red color develops when combinedwith Pyrldlne/Barblturic Acid Reagent; which is redat 578 nm.

Soil samples are prepared for anlysis as prescribedin Method 9010 from SH846.

PETROLEUMHYDROCARBONS Aqueous samples were analyzed following Method 4,18,1

as prescribed in Methods for Ch-mical Analysis ofHater and Hastes, EPA-600/4-79-020 March 1983.

Soil Samples were extracted in accordance with themethods prescribed in SW-846 and subsequentlyanalyzed as stated above.

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LABORATORY CHRONICLE

nRECEIPT/REFRIGERATION______________11/16/90_________________

ORGAHICSEXTRACTION

1. Acids________________'• NA_________________

2. Bane/Neutrals___________HA________________________

3. Pesticides/PCD'a/Berblcides____NA

4. Petiole™ Hydrocarbons________NA

ANALYSIS

1. VolatUes________ NA

2. Acids__________ NA

3. Base/Neutrals______________HA

4. Pesticides/FCB'a/Herbicides_____HA

5. Petroleum Hydrocarbons_______HA

6. Total Organic Carbon_________HA

Section SupervisorReview & Approval_

INORGANICS

t. Metals__________________11/16/90 - 11/19/90

2. Cyanides________________HA___________

3. Phenols_________________HA

OTHER AHALTTES

Section Supervisor I ft n 1 O QReview t Approval ______ ______________________ *VU * *

Quality Control SupervisorReview t Approval

If fractions are re-extracted and re-analyzed because Initial endeavors v-/did not Met quallty'control acceptance criteria, Include dates for both.

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nCERTIFICATE OF ANALYSIS

SAMPLE ID: E 6327

CLIENT ID: "8


METALS MDL (-g/L) RESULT (_g/L)

LEAD 0.01 N.D.

100121O

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SAMPLE ID: E 6328

CLIENT ID: W9

SAMPLE BATE: 11/9/90

METALS HDL (ag/L) RESULT (-g/L)

LEAD 0.01 N.D.

100122

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oCERTIFICATE OF ANALYSIS

SAMPLE ID: B 6329

CLIENT ID: SI


MKIALS MDL (_g/kg) RESULT (-g/kg)

LEAD 2.50 40.0

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SAMPLE ID: B 6330

CLIENT ID: S10


MBTALS MDL (_g/kg) RBSHL't (mg/kg)

LEAD 2.50 25.3

J00124

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QUALITY ASSURANCE DATAHAZARDOUS SDB5TANCE LIST

JJMLYSIS NO. E6190BATCH NO. M331MATRIX: AQUEOUS

METAL AHOUHT OF SPIKE (ug) X SPIKE RECOVERY Z DUPLICATE RECOVERY

ALUMINUM 10000 91 91AHTIHONY 50 113 114

ARSENIC 50 105 101

BARIDM 1000 99 100

BERILLIUH 1000 101 101

CADMIOM 1000 93 93.

CUROMIOM 1000 102 102

COBALT 1000 99 99

'"WEB, 1000 96 97/

IttON 10000 91 91

LEAD 10000 89 90

MANGANESE 1000 98 98

MERCDRX 1.00 101 105

NICKEL 1000 97 97

SELENIUM 50 105! 105

THALLIUM 50 87 87

VAHADIUM 1000 100 100

ZINC 5000 88 88

100125

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BATCH NO: 331

MATRIX: AQUEOUS

METAL METHOD BLAH- (-8/L) AHODHT OF SPIKE (ug/L) X SPIKE RECOVER!

ALUHKUH ND 10000 96

ABTQIONY HD 50 119

AHSEHIC HD 50 105

BARIUM HD 1000 96

BERYLLIUM ND 1000 96

CADMIUM HD 1000 89

CHROMIUM HD 1000 98

COBALT HD 1000 96

COFPE. ND 1000 93

DON ND 10000 98

LEAD HD 10000 98

MANGANESE HD 1000 99

MERCURY HD 1.00 117

NICKEL HD 1000 95

SELENIUM HD 50 104

THALLIUM HD 50 99 •

VANADIUM HD 1000 97

ZHC HD 5000 96

100126

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thru: mike zickler, tatl, region lu-ff— td d #9010-11from: luis loarca, tat region iii subject:...

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