tti environmental incorporated 1253 n. church street

A Service Disabled Veteran Owned Small Business

TTI Environmental Incorporated 1253 N. Church Street Moorestown, New Jersey 08057 Tel: 856-840-8800 Fax: 856-840-8815

Providing Sound Environmental Solutions For Business & Industry

www.ttienv.com

June 27, 2013 Mr. Christopher Eyre TD Bank, N.A. 2059 Springdale Road Cherry Hill, New Jersey 08003 Reference: Phase II Investigation

Alan R. Cantrell Block 538, Lots 13-18 45 Juliustown Road Browns Mills, Pemberton, Burlington County, New Jersey

TTI Project No. 12-1272 TD Project No. 12-006370-03-1 Dear Mr. Eyre: TTI Environmental, Inc. (TTI) is pleased to provide you with this Phase II Investigation for the above referenced facility. For your ease of review, the report is organized in the following manner:

1.0 Background 2.0 Technical Overview

3.0 Site Assessment Summary 4.0 Recommendations & Conclusions

1.0 BACKGROUND

TTI completed a Phase I Environmental Site Assessment (Phase I) of the above referenced property on September 26, 2012. The purpose of the assessment was to identify historical, existing or potential areas of environmental concern. The Phase I was conducted in accordance with the American Society for Testing and Materials Standard Practice for Environmental Site Assessments: Phase I Environmental Site Assessment Process. Figure 1.0 depicts the location of the subject site on a USGS topographic map. The following recognized environmental conditions (RECs) requiring further investigation were identified:

• Abandoned In Place Heating Oil UST • Surficial Staining • Former Dry Cleaning Operation

A summary of the Phase I conclusions regarding these areas of concern is provided below.

TD Bank, N.A. TTI Project No. 12-1272 June 27, 2013 of 9

1.0 BACKGROUND (CONTINUED) 1.1 Abandoned In Place Heating Oil UST

According to Alan Cantrell, the property owner, the site formerly utilized a No. 2 heating oil UST of unknown capacity. The UST is currently abandoned in place on the southeast exterior of the subject building. Pemberton Township construction records indicate a tank removal occurred in 2006 by a contactor identified as Mr. John Donelson. No additional information was provided to TTI regarding the abandonment event. USTs represent and area of concern as a failure or leak in the system can impact subsurface soil and water. It is TTI’s opinion that this environmental consideration is a recognized environmental condition (REC). TTI recommended further investigation of this REC.

1.2 Surficial Staining

TTI observed staining on the concrete floor within the subject building in the vicinity of the oil burner and associated return/feed lines. Granular Oil-Dry was used as an absorbent in and around the staining. TTI did not observe any actively leaking petroleum; however, the observed staining was in close proximity to a nearby wall-floor seam. In addition, the amount and duration of the staining is unknown. It is TTI’s opinion that this environmental consideration is a recognized environmental condition (REC). TTI recommended further investigation of this REC.

1.3 Former Dry Cleaning Operation

Mr. Cantrell indicated that the portion of the subject building occupied by the tobacco shop formerly operated as an offsite dry cleaning operation. As part of this assessment, TTI submitted a request to review records from the Pemberton Township Tax Assessor’s Office and Construction Departments. TTI received information from the Assessor’s office include the site’s property record card, ownership information, historic use, etc. According to the records provided, the former dry cleaning operation was located on site in 1973. Dry cleaners represent an environmental concern as the release of hazardous dry cleaning materials could cause soil and/or groundwater contamination. At this time, TTI cannot confirm that the operation did not engage in onsite dry-cleaning operations. In addition, TTI suspects the dry cleaner could have operated on site. It is TTI’s opinion that this environmental consideration is a recognized environmental condition (REC). TTI recommended further investigation of this REC.


2.0 TECHNICAL OVERVIEW TTI personnel involved in the collection of samples were Ms. Kristin Kaeser, TTI Environmental

Project Supervisor (NJDEP Certification No. 236270) and Mr. Max Demianovich, TTI Environmental Assistant Project Manager.

2.1 Ground Penetrating Radar (GPR) Survey

Prior to field sampling activities, TTI conducted oversight of a GPR survey of the subject site in the vicinity of the abandoned in place UST. The survey was conducted to evaluate the potential presence and/or evidence of historic underground storage tanks at the property. The survey results were also utilized to guide the sample location points. The GPR survey was performed by Enviroprobe Service, Inc. of Moorestown, NJ (Enviroprobe). To complete this investigation, Enviroprobe utilized a Radiodetection RD1000 cart-mounted Ground Penetrating Radar (GPR) unit with a 250 MHz antenna, a Radiodetection 8000T10 multi-frequency transmitter, a Radiodetection 8000 receiver, and a Fisher TW-6 metallic locator. Areas of interest were marked out using spray paint. Upon completion of this survey, one (1) anomaly was identified in the area of the suspected UST. The anomaly was approximately five (5) feet by eight (8) and located approximately three (3) feet below grade. The size and location of this anomaly appeared consistent with an abandoned in place UST between 1,000 gallons and 1,500 gallons in capacity. A copy of the geophysical investigation report prepared by Enviroprobe pertaining to the subject site GPR survey is included herein as Appendix A.

2.2 Soil Sampling Methodology

The soil borings for this Phase II Investigation were installed using a direct push hydraulic sampling unit. Soil samples were collected using dedicated plastic sleeves in the unit’s macro core sampling device. A concrete core drill was utilized to facilitate interior sampling as necessary. Soil cores were continuously field screened using a Photoionization detector (PID) for organic vapor concentrations. Soil selected for chemical analysis from each core was transferred from the sampling device into laboratory supplied sample containers. Samples were shipped to the designated laboratory in ice packed coolers under chain-of-custody documentation.


2.0 TECHNICAL OVERVIEW (CONTINUED)

2.3 Groundwater Sampling Methodology

Groundwater sampling activities were conducted in general conformance with N.J.A.C. 7:26E – Technical Requirements for Site Remediation and the NJDEP Field Sampling Procedures Manual, August 2005. Two (2) temporary well points were placed using a GeoProbe direct push hydraulic unit in order to assess groundwater quality in the historic dry cleaner area. The well point consisted of a 1.5 inch diameter PVC casing and screen. The well point was removed from the ground within 48 hours of installation and the probe holes filled with native soil, sand, and bentonite. Both well points were advanced to a total depth of approximately 12 feet below grade and completed using 10 feet of PVC screen. Groundwater samples were collected using disposable, single use bailers. Each bailer was allowed to travel to the bottom of the temporary well point prior to sample collection. The groundwater samples were transferred directly into laboratory supplied sample containers and transported to the laboratory in ice packed coolers under Chain of Custody documentation.

2.4 Analytical Methodology

Samples collected for analysis were submitted to Alpha Analytical of Westborough, Massachusetts (NJDEP Certification No. MA935). The following methodologies were used: Soil

• EPH Category 1 • Volatile Organic Compounds via EPA Method 5035

Groundwater

• Volatile Organic Compounds via EPA Method 8260B

2.5 Non-Conformance Issues

Volatile Organics

The WG609456-3 Method Blank, associated with L1308954-01 and -02, has a TIC concentration above the reporting limit. The results of the original analysis are reported and are qualified with a "B" for any associated sample concentrations that are less than 5x the blank concentration for this TIC. NJ Extractable Petroleum Hydrocarbons (Total)

The WG609036-5 Laboratory Duplicate RPD (56%), performed on L1308954-05, is outside the acceptance criteria. The elevated RPD has been attributed to the non-homogeneous nature of the sample utilized for the laboratory duplicate. None of these nonconformance issues have impacted the quality of the data. The final laboratory report (L1308954) is attached is attached as Appendix B.


3.0 SITE ASSESSMENT SUMMARY

Limitations: TTI’s investigation was limited due to the presence of subgrade utilities in the vicinity of exterior sample locations. Additionally, the UST being investigated was abandoned in place; as such, sampling directly below the tank centerline was not feasible. Finally, the location of the surficial staining sample location was limited due to the presence of stockpiled material and interior shelving units. The location of all sample points and anomalies identified during the GPR survey are depicted on Figure 2.0. 3.1 Abandoned In Place Heating Oil UST

TTI performed an investigation of the abandoned in place heating oil UST using the NJDEP’s Technical Guidance for the Investigation of Underground Storage Tank Systems v1.0 dated April 12, 2012 for guidance. Based on the suspected capacity of the UST (between 1,000 and 1,500 gallons) one (1) sample was collected from each side of the tank for a total of four (4) soil samples. The sample depths were selected at the suspected invert of the tank and/or based on positive bias (olfactory/visual observation and PID screening). A total of two (2) of these samples were submitted for EPH Category 1 analysis. The selection of samples UST-3 and UST-4 for analysis was based on a petroleum odor detected during borehole advancement. Each sample was collected from the half foot interval directly above the observed soil-groundwater interface. A summary of the results is provided below in Table 1.0.

Table 1.0: UST Investigation Soil Analytical Data (mg/kg) Sample

Location Depth (ft) Date PID EPH

Result NJDEP Further Action

Criteria

UST-3 8-8.5 05/16/2013 ND 375 1,000 mg/kg – Further

Action Criteria

5,100 mg/kg = Remedial Criteria UST-4 7.5-8 05/16/2013 ND ND

ppm = parts per million; ND = None detected; EPH (Extractable Petroleum Hydrocarbon Category 1); PID = photoionization detector A review of the data indicates that no EPH category 1 results were detected above the NJDEP further action criteria of 1,000 mg/kg. As such, no samples were selected for contingent analysis.

3.2 Surficial Staining

TTI performed a subsurface investigation in the vicinity of surficial staining observed near the site’s current oil fired boiler. Subsurface soils were sampled after exposure via concrete core drilling. The sample was collected from the half foot interval directly below the building’s concrete slab floor and submitted for EPH Category 1 analysis. A summary of the results is provided in Table 2.0 on the following page.


3.0 SITE ASSESSMENT SUMMARY (CONTINUED)

3.2 Surficial Staining – Continued

Table 2.0: Surficial Staining Investigation Soil Analytical Data (mg/kg) Sample

Location Depth (ft) Date PID EPH

Result NJDEP Further Action

Criteria

I-1 0.5-1.0 05/16/2013 ND 40.8

1000 mg/kg – Further Action Criteria

5100 mg/kg = Remedial

Criteria mg/kg = milligrams per kilogram; ND = None detected; PID = photoionization detector; EPH (Extractable Petroleum Hydrocarbon Category 1); A review of the data indicates that no EPH category 1 results were detected above the NJDEP further action criteria of 1,000 mg/kg. As such, no samples were selected for contingent analysis.

3.3 Former Dry Cleaning Operation

TTI installed two (2) borings to investigate this REC. A soil sample was collected from each borehole at the half foot interval directly above the observed soil/water interface. The samples were submitted for Volatile Organic Compound (VOC) analysis. The borings were advanced to a total depth of 12 feet below grade. Groundwater was encountered at approximately 7.5 to eight (8) feet below grade. A summary of the soil results is provided below in Table 3.0.

Table 3.0: Former Dry Cleaning Operation Soil Analytical Data (mg/kg)

Sample Location Depth (ft) Date PID

Targeted VOC Result

VOC Tentatively Identified Compound

Result

DC-1 7.0-7.5 05/16/2013 ND ND 0.0457

DC-2 7.5-8.0 05/16/2013 ND ND 0.1274

mg/kg = milligrams per kilogram; ND = None detected; PID = photoionization detector; VOC = (Volatile Organic Compound

A review of the data indicates that no targeted VOCs were detected. Additionally, tentatively identified compounds (TICs) for each sample were detected at a concentration of less than one (1) mg/kg.


3.0 SITE ASSESSMENT SUMMARY (CONTINUED)

3.3 Former Dry Cleaning Operation – Continued

At the conclusion of soil sampling, each bore hole was converted to a temporary well point to facilitate ground water sampling (DC-1 was converted to TWP-1 and DC-2 was converted to TWP-2). Each well point was purged to clear via a peristaltic pump prior to sampling. The samples were submitted for Volatile Organic Compound (VOC) analysis. A summary of the groundwater results is provided below in Table 4.0.

Table 4.0: Former Dry Cleaning Operation Groundwater Analytical Data (ug/L)

Sample Location Date

Targeted VOC Result

VOC Tentatively Identified Compound

Result

TWP-1 05/16/2013 ND ND

TWP-2 05/16/2013 ND 52

ug/L = micro grams per liter; ND = None detected; VOC (Volatile Organic Compound

A review of the data indicates that no targeted VOCs were detected. Additionally, tentatively identified compounds for TWP-2 were detected at a concentration of 52 ug/L. This value is below the groundwater remedial standard for total tentatively identified compounds of 500 ug/L.


4.0 CONCLUSIONS AND RECOMMENDATIONS

TTI’s Phase II investigation evaluated the potential environmental impact from an abandoned in place heating oil UST, surficial staining, and a former dry cleaning operation. The investigation was conducted in general conformance with NJDEP requirements. With regard to this Phase II, TTI concludes the following: Abandoned In Place Heating Oil UST: UST-3 produced an EPH result of 375 mg/kg at 8.0 – 8.5 feet below grade. Based on the fact that the EPH Category 1 result was not above the NJDEP further action criteria of 1,000 mg/kg and no signs of impact to groundwater were observed, i.e. sheen/product in groundwater, groundwater odor, etc., TTI is recommending no further action or investigation with regard to this recognized environmental condition. Surficial Staining: Soil sampling in the vicinity of observed interior surficial staining produced an EPH Category 1 result of 40.8 mg/kg. This result is below the NJDEP EPH Category 1 further action criteria of 1,000 mg/kg. As such, TTI is recommending no further action or investigation with regard to this recognized environmental condition. Former Dry Cleaning Operation: TTI’s soil/groundwater investigation identified no targeted or tentatively identified VOCs above applicable NJDEP standards. As such, TTI is recommending no further action or investigation with regard to this recognized environmental condition.


4.0 CONCLUSIONS AND RECOMMENDATIONS Thank you for allowing TTI to provide you with professional environmental consulting services. If you should have any questions or require additional information, please feel free to contact us at any time.

Sincerely,

TTI ENVIRONMENTAL, INC.

Max Demianovich

Assistant Project Manager

Kristin M. Kaeser

Environmental Project Supervisor

Figure 1.0: Site Location Diagram Figure 2.0: Sample Location Diagram Appendix A: Geophysical Investigation Report Appendix A: Alpha Analytical Laboratory Report L1308954 \\TTISERVER00\Public\TTI\TD Bank, NA\2012 Projects\12-1272 P2 Browns Mill\12-1272.P2.Letter Report.docx

FIGURE 1.0

REGIONAL SITE LOCATION MAP BROWNS MILLS QUAD, 1997

45 Juliustown Road Block 538, Lots 13-18 Browns Mills (Pemberton), Burlington County, NJ

SCALE As Shown

DRAWN BY USGS

DATE 06/2013

PROJECT 12-1272

APP’D BY MD

DRAWING NO. 1.0

TTI Environmental, Inc. www.ttienv.com

FIGURE 2.0:

SAMPLE LOCATION DIAGRAM

45 Juliustown Road Block 538, Lots 13-18 Browns Mills (Pemberton), Burlington County, NJ

SCALE As Shown

DRAWN BY USGS

DATE 06/2013

PROJECT 12-1272

APP’D BY MD

DRAWING NO. 1.0

TTI Environmental, Inc. www.ttienv.com

Appendix A: Geophysical Investigation Report

GEOPHYSICAL INVESTIGATION REPORT

PERFORMED AT:

45 Juliustown Rd.Browns Mills, NJ 08015

PREPARED FOR:

Max Demianovich TTI Environmental, Inc.1253 North Church Rd.Moorestown, NJ 08057

PREPARED BY:

Ken LindesGeophysical Technician

Enviroprobe Service, Inc.908 N. Lenola Road

Moorestown, NJ 08057(856) 858-8584(800) 596-7472

May 25, 2013

Enviroprobe Service, Inc. 2

1.0 INTRODUCTION

Enviroprobe Service, Inc. (Enviroprobe) is an environmental investigation services firm which provides monitoring well installation (HSA), Geoprobe (DPT) drilling services and Environmental & Engineering Geophysics (EEG) services to the environmental consulting and engineering community.

Enviroprobe conducted a subsurface geophysical investigation at the subject property within client-specified areas of concern. Due to conditions and objectives, the investigation utilized a Radiodetection RD1000 cart-mounted Ground Penetrating Radar (GPR) unit with a 250 MHz antenna, a Radiodetection 8000T10 multi-frequency transmitter, a Radiodetection 8000 receiver, and a Fisher TW-6 metallic locator.

Ground penetrating radar (commonly called GPR) is a geophysical method that has been developed over the past thirty years for shallow, high-resolution, subsurface investigations of the earth. GPR uses high frequency pulsed electromagnetic waves (generally 10 MHz to 2,000 MHz) to acquire subsurface information. An EM wave is propagated downward into the ground by a transmitting antenna. Where abrupt changes in electrical properties occur in the subsurface, a portion of the energy is reflected back to the surface. This reflected wave is detected by a receiver antenna and transmitted to a control unit for real time processing and display. The penetration depth of the RD1000 unit varies from several inches to tens of feet according to site-specific conditions. The penetration depth decreases with increased soil conductivity. The penetration depth is the greatest in ice, dry sands, and fine gravels. Clayey, highly saline or saturated soils, areas covered by concrete, foundry slag, or other highly conductive materials greatly reduce GPR penetration. GPR is a method that is commonly used for environmental, engineering, archaeological, and other shallow investigations.

The Radiodetection (RD) transmitter and receiver are commonly used for pipe and cable locating. The multi-frequency transmitter can be directly connected, clamped, or used to induce a signal in a target line while the multi-frequency receiver is used to measure the signal from energized lines.

The Fisher TW-6 metallic locator is designed to find pipes, cables and other metallic objects such as underground storage tanks (USTs). The TW-6 transmitter generates an electromagnetic field that induces electrical currents in the subsurface. These currents produce a secondary electromagnetic field that is measured by the TW-6 receiver. One surveyor can carry both the transmitter and receiver together to search for underground metallic objects, although the TW-6 response can also be affected by the electrical properties of non-metallic materials in the subsurface.

2.0 SCOPE OF WORK

On May 16, 2013, a geophysical technician from Enviroprobe Service Inc. was mobilized to the subject property to perform a geophysical investigation. The purpose of


this investigation was to detect possible USTs, designate underground conduits/utilities, and investigate proposed boring locations within all accessible exterior portions of the subject property. The ground surface of the survey area consisted of paved, concrete, landscaped, and natural soil surfaces.

3.0 SURVEY RESULTS

The survey was conducted using a cart-mounted GPR unit, a Fisher TW-6 metallic locator, and a RD unit. The RD unit was used to trace common utilities from sources in and around the survey area. The RD receiver was also used in the passive mode to search for live underground electrical power cables and other utilities emitting 60Hz electromagnetic signals. When possible, the locations of utilities were confirmed with the GPR. Whenever possible and necessary, the manhole covers in and around the survey area were opened and the manholes were visually inspected for underground utilities. A GPR survey was also performed in a grid pattern in at least two orthogonal directions to search for underground utilities. Designated utilities were marked on-site with spray paint using the following colors; blue – water and white – vent line.

The GPR and TW-6 were used in a grid pattern over all client-specified areas of the property. Based on the results of the GPR and TW-6 surveys, a metallic anomaly consistent with an UST was identified adjacent the eastern side of the main building. This rectangular anomaly measured approximately 5 ft by 8 ft and was located at a depth of approximately 3 ft. The approximate extent of this anomaly was designated on-site with white spray paint.

Proposed boring locations were investigated with the GPR, TW-6, and RD receiver. When possible, an area of approximately 10 ft by 10 ft surrounding each boring location was scanned. In some cases, obstructions prevented an investigation of the entire 10 ft by 10 ft area. All designated anomalies were marked on-site with spray paint.

4.0 LIMITATIONS

The client-selected areas of the property had obstructions including debris, landscaping, and walls. These objects prevented a thorough investigation of the spaces beneath and immediately adjacent to them.

Due to surface conditions and subsurface content, the GPR signal penetration was estimated at 4.0 feet in the majority of the survey area. This penetration was reduced in areas of concrete cover.

The TW-6 survey was kept up to 6 feet away from above ground objects containing metals depending on the sizes, shapes and positions of the metal objects. The TW-6 survey was not effective in areas with reinforced concrete.


Due to the dielectric properties of the subsurface, plastic polymer and fiberglass utilities may not have been detected.

All field services were conducted in compliance with the industry standard of care guidelines found in ASCE 38-02 (Level B).

5.0 WARRANTIES

The field observations and measurements reported herein are considered sufficient in detail and scope for this project. Enviroprobe Service, Inc. warrants that the findings and conclusions contained herein have been promulgated in accordance with generally accepted environmental engineering methods. There is a possibility that conditions may exist which could not be identified within the scope of this project and were not apparent during the site activities performed for this project.

Enviroprobe represents that the services were performed in a manner consistent with that level of care and skill ordinarily exercised by environmental consultants under similar circumstances. No other representations to Client, express or implied, and no warranty or guarantee is included or intended in this agreement, or in any report, document, or otherwise.

Enviroprobe Service, Inc. believes that the information provided in this report is reliable. However, Enviroprobe cannot warrant or guarantee that the information provided by others is complete or accurate. No other warranties or guarantees are implied or expressed.

GPR data is subject to signal anomalies and operator interpretation. The GPR data is intended to provide the locations of areas of concern requiring additional investigation or the approximate location of underground structures and utilities. Great care must be utilized when excavating and/or drilling around underground structures and utilities since GPR data can only be used for estimation purposes and GPR data is subject to misinterpretation. Enviroprobe can not guarantee that utilities, post-tension cables, and/or rebar will not be incurred during drilling, cutting, coring, or excavating activities.

This report was prepared pursuant to the contract Enviroprobe has with the Client. That contractual relationship included an exchange of information about the property that was unique and between Enviroprobe and its client and serves as the basis upon which this report was prepared. Because of the importance of the communication between Enviroprobe and its client, reliance or any use of this report by anyone other than the Client, for whom it was prepared, is prohibited and therefore not foreseeable to Enviroprobe.

Reliance or use by any such third party without explicit authorization in the report does not make said third party a third party beneficiary to Enviroprobe contract with the Client. Any such unauthorized reliance on or use of this report, including any of its


information or conclusions, will be at the third party's risk. For the same reasons, no warranties or representations, expressed or implied in this report, are made to any such third party.

Appendix B: Alpha Analytical Laboratory Report L1308954

L1308954

TTI Environmental, Inc.

12-1272

Not Specified

Client:

Project Name:

Project Number:

05/28/13

Eight Walkup Drive, Westborough, MA 01581-1019

Lab Number:

Report Date:

508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com

1253 North Church Street

Moorestown, NJ 08057

Max DemianovichATTN:

ANALYTICAL REPORT

Certifications & Approvals: MA (M-MA086), NY (11148), CT (PH-0574), NH (2003), NJ NELAP (MA935), RI (LAO00065), ME (MA00086),PA (68-03671), USDA (Permit #P-330-11-00240), NC (666), TX (T104704476), DOD (L2217), US Army Corps of Engineers.

(856) 840-8800Phone:

The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in itsentirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.

Serial_No:05281316:15

Page 1 of 75

L1308954-01

L1308954-02

L1308954-03

L1308954-04

L1308954-05

L1308954-06

L1308954-07

L1308954-08

L1308954-09

L1308954-10

L1308954-11

Alpha Sample ID

DC-1

DC-2

UST-1

UST-2

UST-3 8-8.5

UST-4 7.5-8

I-1

TWP-1

TWP-2

UST-3 6.5-7

UST-4 6.5-7

Client ID

PEMBERTON, NJ

PEMBERTON, NJ

PEMBERTON, NJ

PEMBERTON, NJ

PEMBERTON, NJ

PEMBERTON, NJ

PEMBERTON, NJ

PEMBERTON, NJ

PEMBERTON, NJ

PEMBERTON, NJ

PEMBERTON, NJ

Sample Location

Not Specified

12-1272

Project Name:Project Number:

Lab Number: Report Date:

L130895405/28/13

05/16/13 10:15

05/16/13 10:40

05/16/13 10:54

05/16/13 11:02

05/16/13 11:22

05/16/13 11:31

05/16/13 10:42

05/16/13 11:50

05/16/13 12:13

05/16/13 11:18

05/16/13 11:32

Collection Date/Time

Serial_No:05281316:15

Page 2 of 75

Not Specified

12-1272

Project Name:

Project Number:

Lab Number:

Report Date:L1308954

05/28/13

Case Narrative

The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation

or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report.

Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet all of the requirements of

NELAC, for all NELAC accredited parameters. The data presented in this report is organized by parameter (i.e. VOC, SVOC, etc.). Sample

specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list for each individual sample,

followed by the Laboratory Batch Quality Control at the end of each parameter. If a sample was re-analyzed or re-extracted due to a

required quality control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is

designated with an "R" or "RE", respectively. When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the

associated samples for each element are noted in the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific %

recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report. Performance criteria for CAM and RCP methods

allow for some LCS compound failures to occur and still be within method compliance. In these instances, the specific failures are not

narrated but are noted in the associated QC table. This information is also incorporated in the Data Usability format for our Data Merger tool

where it can be reviewed along with any associated usability implications. Soil/sediments, solids and tissues are reported on a dry weight

basis unless otherwise noted. Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the

back of the report.

In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria for CAM and RCP methods allow for some

quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the

associated QC table. The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed

along with any associated usability implications.

Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical

Standards requested on the Chain of Custody.

HOLD POLICY

For samples submitted on hold, Alpha's policy is to hold samples free of charge for 30 days from the date the project is completed. After 30

days, we will dispose of all samples submitted including those put on hold unless you have contacted your Client Service Representative and

made arrangements for Alpha to continue to hold the samples.

Please contact Client Services at 800-624-9220 with any questions.

Serial_No:05281316:15

Page 3 of 75

Case Narrative (continued)

Not Specified

12-1272

Project Name:

Project Number:

Lab Number:

Report Date:L1308954

05/28/13

Report Submission

This final report replaces the partial report issued earlier today, and includes the results of all requested

analyses.

All non-detect (ND) or estimated concentrations (J-qualified) have been quantitated to the limit noted in the

MDL column.

Volatile Organics

The WG609456-3 Method Blank, associated with L1308954-01 and -02, has a TIC concentration above the

reporting limit. The results of the original analysis are reported and are qualified with a "B" for any associated

sample concentrations that are less than 5x the blank concentration for this TIC.

NJ Extractable Petroleum Hydrocarbons (Total)

The WG609036-5 Laboratory Duplicate RPD (56%), performed on L1308954-05, is outside the acceptance

criteria. The elevated RPD has been attributed to the non-homogeneous nature of the sample utilized for the

laboratory duplicate.

I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report.

Authorized Signature:

Title: Technical Director/Representative Date: 05/28/13

Serial_No:05281316:15

Page 4 of 75

ORGANICS

Serial_No:05281316:15

Page 5 of 75

VOLATILES

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Page 6 of 75

FF

1,2-Dibromo-3-chloropropane

1,4-Dioxane

1,2-Dibromoethane

Methylene chloride

1,1-Dichloroethane

Chloroform

Carbon tetrachloride

1,2-Dichloropropane

Dibromochloromethane

1,1,2-Trichloroethane

Tetrachloroethene

Chlorobenzene

Trichlorofluoromethane

1,2-Dichloroethane


Bromodichloromethane

trans-1,3-Dichloropropene

cis-1,3-Dichloropropene

Bromoform

1,1,2,2-Tetrachloroethane

Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene

trans-1,2-Dichloroethene

Trichloroethene

1,2-Dichlorobenzene

Parameter Result Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Volatile Organics by GC/MS-5035 - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

0.0063

0.13

0.0050

0.0063

0.0019

0.0019

0.0013

0.0044

0.0013

0.0019

0.0013

0.0013

0.0063

0.0013

0.0013

0.0013

0.0013

0.0013

0.0050

0.0013

0.0013

0.0019

0.0013

0.0063

0.0025

0.0025

0.0025

0.0013

0.0019

0.0013

0.0063

05/28/13

DC-1Client ID:05/16/13 10:15Date Collected:05/17/13Date Received:

PEMBERTON, NJSample Location:

L1308954-01Lab ID:

Field Prep: Not SpecifiedMatrix: SoilAnalytical Method:Analytical Date:Analyst:

1,8260C05/20/13 15:47BN 88%Percent Solids:

MDL

0.0010

0.022

0.00022

0.0025

0.00022

0.00047

0.00026

0.00029

0.00039

0.00038

0.00018

0.00044

0.00015

0.00018

0.00014

0.00029

0.00015

0.00016

0.00052

0.00022

0.00015

0.00014

0.00018

0.00099

0.00043

0.00018

0.00040

0.00026

0.00027

0.00019

0.00023

Serial_No:05281316:15

Page 7 of 75

1,3-Dichlorobenzene

1,4-Dichlorobenzene

Methyl tert butyl ether

p/m-Xylene

o-Xylene

cis-1,2-Dichloroethene

Styrene

Dichlorodifluoromethane

Acetone

Carbon disulfide

2-Butanone

4-Methyl-2-pentanone

2-Hexanone

Bromochloromethane

Isopropylbenzene

1,2,3-Trichlorobenzene


Methyl Acetate

Cyclohexane

Methyl cyclohexane

1,1,2-Trichloro-1,2,2-Trifluoroethane


ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

0.0063

0.0063

0.0025

0.0025

0.0025

0.0013

0.0025

0.013

0.045

0.013

0.013

0.013

0.013

0.0063

0.0013

0.0063

0.0063

0.0050

0.025

0.0050

0.025

05/28/13



L1308954-01Lab ID:

Field Prep: Not Specified

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

J

J

J

J

J

J

J

J

J

J

0.0068

0.0050

0.0072

0.0037

0.0078

0.0036

0.0030

0.0027

0.0031

0.0028

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

Tentatively Identified Compounds

MDL

0.00023

0.00030

0.00013

0.00041

0.00034

0.00019

0.00039

0.00028

0.0039

0.0025

0.00045

0.00031

0.00024

0.00025

0.00021

0.00021

0.0010

0.00096

0.0014

0.0016

0.00034

Serial_No:05281316:15

Page 8 of 75

Parameter Result Dilution FactorQualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

1,2-Dichloroethane-d4

Toluene-d8

4-Bromofluorobenzene

Dibromofluoromethane

124

94

116

107

70-130

70-130

70-130

70-130

Acceptance CriteriaSurrogate % Recovery Qualifier

05/28/13



L1308954-01Lab ID:


MDL

Serial_No:05281316:15

Page 9 of 75


1,4-Dioxane

1,2-Dibromoethane

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.00024

ND

ND

ND

ND

ND

ND

ND

ND

ND

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

0.0055

0.11

0.0044

0.0055

0.0016

0.0016

0.0011

0.0038

0.0011

0.0016

0.0011

0.0011

0.0055

0.0011

0.0011

0.0011

0.0011

0.0011

0.0044

0.0011

0.0011

0.0016

0.0011

0.0055

0.0022

0.0022

0.0022

0.0011

0.0016

0.0011

0.0055

05/28/13



L1308954-02Lab ID:

Field Prep: Not SpecifiedMatrix: SoilAnalytical Method:Analytical Date:Analyst:

1,8260C05/20/13 16:15BN 80%Percent Solids:

MDL

0.00087

0.019

0.00020

0.0022

0.00020

0.00041

0.00023

0.00025

0.00034

0.00033

0.00015

0.00038

0.00013

0.00016

0.00012

0.00025

0.00013

0.00014

0.00046

0.00019

0.00013

0.00012

0.00016

0.00086

0.00037

0.00016

0.00035

0.00023

0.00023

0.00017

0.00020

Serial_No:05281316:15

Page 10 of 75

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone


2-Hexanone

Bromochloromethane

Isopropylbenzene



Methyl Acetate

Cyclohexane

Methyl cyclohexane



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

0.0055

0.0055

0.0022

0.0022

0.0022

0.0011

0.0022

0.011

0.040

0.011

0.011

0.011

0.011

0.0055

0.0011

0.0055

0.0055

0.0044

0.022

0.0044

0.022

05/28/13



L1308954-02Lab ID:


Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

J

J

J

J

J

J

J

J

J

J

J

0.0046

0.0093

0.0054

0.015

0.013

0.014

0.015

0.012

0.018

0.0064

0.0028

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1


MDL

0.00020

0.00027

0.00011

0.00036

0.00030

0.00016

0.00034

0.00024

0.0034

0.0022

0.00039

0.00027

0.00021

0.00022

0.00018

0.00018

0.00087

0.00084

0.0012

0.0014

0.00030

Serial_No:05281316:15

Page 11 of 75



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954


Toluene-d8



124

105

107

107

70-130

70-130

70-130

70-130


05/28/13



L1308954-02Lab ID:


Unknown

Unknown

Unknown

J

J

J

0.0036

0.0051

0.0032

mg/kg

mg/kg

mg/kg

1

1

1


MDL

Serial_No:05281316:15

Page 12 of 75

1,2-Dibromoethane



ND

ND

ug/l

ug/l

1

1

Qualifier Units RL

Microextractables by GC - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

0.011

0.011

05/28/13

TWP-1Client ID:05/16/13 11:50Date Collected:05/17/13Date Received:


L1308954-08Lab ID:

Field Prep: Not SpecifiedMatrix: WaterAnalytical Method:Analytical Date:Analyst:

1,801105/25/13 00:12SR

Extraction Date: 05/24/13 13:00

MDL

0.003

0.004

Serial_No:05281316:15

Page 13 of 75

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Volatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

2.5

2.5

2.5

0.50

1.0

0.50

1.5

0.50

2.5

2.5

0.50

2.5

0.50

0.50

0.50

2.0

0.50

0.50

2.5

2.5

2.5

2.5

1.0

2.5

0.50

2.5

0.50

2.5

2.5

2.5

2.5

05/28/13



L1308954-08Lab ID:


1,8260C05/23/13 00:21PD

MDL

0.70

0.70

0.70

0.16

0.30

0.19

0.50

0.18

0.70

0.70

0.16

0.70

0.19

0.16

0.14

0.65

0.19

0.19

0.70

0.70

0.70

0.70

0.33

0.70

0.18

0.70

0.17

0.70

0.70

0.70

0.70

Serial_No:05281316:15

Page 14 of 75

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

1,4-Dioxane

Methyl cyclohexane



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

2.5

2.5

2.5

2.5

5.0

5.0

5.0

5.0

5.0

5.0

2.5

2.0

2.5

2.5

2.5

2.5

2.0

10

250

10

2.5


Toluene-d8



79

89

96

103

70-130

70-130

70-130

70-130


05/28/13



L1308954-08Lab ID:


No Tentatively Identified Compounds ND ug/l 1


MDL

0.70

0.70

0.70

0.70

1.0

1.0

1.0

1.0

1.0

1.0

0.70

0.65

0.70

0.70

0.70

0.70

0.65

0.70

76.

0.29

0.70

Serial_No:05281316:15

Page 15 of 75

1,4-Dioxane


ND ug/l 1

Qualifier Units RL

Volatile Organics by GC/MS-SIM - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

3.0

05/28/13



L1308954-08Lab ID:


1,8260C-SIM(M)05/23/13 00:21PD

MDL

0.76

Serial_No:05281316:15

Page 16 of 75

1,2-Dibromoethane



ND

ND

ug/l

ug/l

1

1

Qualifier Units RL

Microextractables by GC - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

0.011

0.011

05/28/13



L1308954-09Lab ID:


1,801105/25/13 00:43SR

Extraction Date: 05/24/13 13:00

MDL

0.003

0.004

Serial_No:05281316:15

Page 17 of 75

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

2.5

2.5

2.5

0.50

1.0

0.50

1.5

0.50

2.5

2.5

0.50

2.5

0.50

0.50

0.50

2.0

0.50

0.50

2.5

2.5

2.5

2.5

1.0

2.5

0.50

2.5

0.50

2.5

2.5

2.5

2.5

05/28/13



L1308954-09Lab ID:


1,8260C05/23/13 16:52PD

MDL

0.70

0.70

0.70

0.16

0.30

0.19

0.50

0.18

0.70

0.70

0.16

0.70

0.19

0.16

0.14

0.65

0.19

0.19

0.70

0.70

0.70

0.70

0.33

0.70

0.18

0.70

0.17

0.70

0.70

0.70

0.70

Serial_No:05281316:15

Page 18 of 75

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

1,4-Dioxane

Methyl cyclohexane



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

2.5

2.5

2.5

2.5

5.0

5.0

5.0

5.0

5.0

5.0

2.5

2.0

2.5

2.5

2.5

2.5

2.0

10

250

10

2.5

05/28/13



L1308954-09Lab ID:


Propene

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

NJ

J

J

J

J

J

J

J

J

20

3.3

13

1.3

1.4

4.8

1.9

3.7

2.6

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1


MDL

0.70

0.70

0.70

0.70

1.0

1.0

1.0

1.0

1.0

1.0

0.70

0.65

0.70

0.70

0.70

0.70

0.65

0.70

76.

0.29

0.70

Serial_No:05281316:15

Page 19 of 75



SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954


Toluene-d8



92

87

90

101

70-130

70-130

70-130

70-130


05/28/13



L1308954-09Lab ID:


MDL

Serial_No:05281316:15

Page 20 of 75

1,4-Dioxane


ND ug/l 1

Qualifier Units RL

Volatile Organics by GC/MS-SIM - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

3.0

05/28/13



L1308954-09Lab ID:


1,8260C-SIM(M)05/23/13 16:52PD

MDL

0.76

Serial_No:05281316:15

Page 21 of 75

Method Blank AnalysisBatch Quality Control

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

05/20/13 10:411,8260CAnalytical Method:

Analytical Date:

05/28/13

Analyst: BN


1,4-Dioxane

1,2-Dibromoethane

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



2-Chloroethylvinyl ether

Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





1,1-Dichloropropene

Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.00020

ND

ND

ND

ND

ND

ND

ND

RL

0.0050

0.10

0.0040

0.0050

0.0015

0.0015

0.0010

0.0035

0.0010

0.0015

0.020

0.0010

0.0010

0.0050

0.0010

0.0010

0.0010

0.0010

0.0010

0.0050

0.0040

0.0010

0.0010

0.0015

0.0010

0.0050

0.0020

0.0020

0.0020

0.0010

0.0015

J

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

UnitsQualifier

Volatile Organics by GC/MS-5035 - Westborough Lab for sample(s): 01-02 Batch: WG609456-3

MDL

0.00079

0.017

0.00018

0.0020

0.00018

0.00037

0.00021

0.00023

0.00031

0.00030

0.00062

0.00014

0.00035

0.00012

0.00015

0.00011

0.00023

0.00012

0.00013

0.00046

0.00041

0.00017

0.00012

0.00011

0.00015

0.00078

0.00034

0.00014

0.00032

0.00020

0.00021

Serial_No:05281316:15

Page 22 of 75


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954


Analytical Date:

05/28/13

Analyst: BN

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Dibromomethane

1,4-Dichlorobutane

1,2,3-Trichloropropane

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Ethyl methacrylate

Acrolein

Acrylonitrile

Bromochloromethane

Tetrahydrofuran

2,2-Dichloropropane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

0.0010

0.0050

0.0050

0.0050

0.0020

0.0020

0.0020

0.0010

0.010

0.010

0.010

0.0020

0.010

0.036

0.010

0.010

0.010

0.010

0.010

0.010

0.025

0.0040

0.0050

0.020

0.0050

0.0050

0.0010

0.0050

0.0010

0.0010

0.0050

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

UnitsQualifier


MDL

0.00015

0.00018

0.00018

0.00024

0.00010

0.00032

0.00027

0.00015

0.00016

0.0010

0.00022

0.00031

0.00022

0.0031

0.0020

0.00036

0.00048

0.00024

0.00019

0.00076

0.0092

0.00024

0.00020

0.00038

0.00022

0.00017

0.00032

0.00021

0.00020

0.00020

0.00056

Serial_No:05281316:15

Page 23 of 75


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954


Analytical Date:

05/28/13

Analyst: BN

o-Chlorotoluene

p-Chlorotoluene

Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

n-Propylbenzene



1,3,5-Trimethylbenzene


trans-1,4-Dichloro-2-butene

Ethyl ether

Methyl Acetate

Ethyl Acetate

Isopropyl Ether

Cyclohexane

tert-Butyl Alcohol

Ethyl-Tert-Butyl-Ether

Tertiary-Amyl Methyl Ether

Methyl cyclohexane


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

0.0050

0.0050

0.0050

0.0010

0.0010

0.0050

0.0010

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0040

0.020

0.0040

0.020

0.10

0.0040

0.0040

0.0040

0.020

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

UnitsQualifier


Unknown J0.0034 mg/kg


MDL

0.00016

0.00015

0.00042

0.00017

0.00019

0.00077

0.00012

0.00017

0.00079

0.00014

0.00057

0.00045

0.00026

0.00076

0.00082

0.00014

0.0011

0.00091

0.00042

0.00058

0.0013

0.00027

Serial_No:05281316:15

Page 24 of 75


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954


Analytical Date:

05/28/13

Analyst: BN

Parameter Result RLUnitsQualifier



Toluene-d8



109

99

105

105

70-130

70-130

70-130

70-130

Surrogate %Recovery QualifierAcceptance

Criteria

MDL

Serial_No:05281316:15

Page 25 of 75


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954


Analytical Date:

05/28/13

Analyst: PD

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.5

2.5

2.5

0.50

1.0

0.50

1.5

0.50

2.5

2.5

0.50

2.5

0.50

0.50

0.50

2.0

0.50

0.50

2.5

2.5

2.5

2.5

1.0

2.5

0.50

2.5

0.50

2.5

2.5

2.5

2.5

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

Volatile Organics by GC/MS - Westborough Lab for sample(s): 08 Batch: WG610254-3

MDL

0.70

0.70

0.70

0.16

0.30

0.19

0.50

0.18

0.70

0.70

0.16

0.70

0.19

0.16

0.14

0.65

0.19

0.19

0.70

0.70

0.70

0.70

0.33

0.70

0.18

0.70

0.17

0.70

0.70

0.70

0.70

Serial_No:05281316:15

Page 26 of 75


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954


Analytical Date:

05/28/13

Analyst: PD

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

tert-Butyl Alcohol

1,4-Dioxane

Methyl cyclohexane


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.5

2.5

2.5

2.5

5.0

5.0

5.0

5.0

5.0

5.0

2.5

2.0

2.5

2.5

2.5

2.5

2.0

10

10

250

10

2.5

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier


No Tentatively Identified Compounds ND ug/l


MDL

0.70

0.70

0.70

0.70

1.0

1.0

1.0

1.0

1.0

1.0

0.70

0.65

0.70

0.70

0.70

0.70

0.65

0.70

0.90

76.

0.29

0.70

Serial_No:05281316:15

Page 27 of 75


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954


Analytical Date:

05/28/13

Analyst: PD




Toluene-d8



83

88

94

97

70-130

70-130

70-130

70-130


Criteria

MDL

Serial_No:05281316:15

Page 28 of 75


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

05/22/13 13:561,8260C-SIM(M)Analytical Method:

Analytical Date:

05/28/13

Analyst: PD

1,4-Dioxane

Parameter Result

ND

RL

3.0ug/l

UnitsQualifier

Volatile Organics by GC/MS-SIM - Westborough Lab for sample(s): 08 Batch: WG610255-3

MDL

0.76

Serial_No:05281316:15

Page 29 of 75


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

05/23/13 14:041,8260C-SIM(M)Analytical Method:

Analytical Date:

05/28/13

Analyst: PD

1,4-Dioxane

Parameter Result

ND

RL

3.0ug/l

UnitsQualifier

Volatile Organics by GC/MS-SIM - Westborough Lab for sample(s): 09 Batch: WG610273-3

MDL

0.76

Serial_No:05281316:15

Page 30 of 75


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954


Analytical Date:

05/28/13

Analyst: PD

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.5

2.5

2.5

0.50

1.0

0.50

1.5

0.50

2.5

2.5

0.50

2.5

0.50

0.50

0.50

2.0

0.50

0.50

2.5

2.5

2.5

2.5

1.0

2.5

0.50

2.5

0.50

2.5

2.5

2.5

2.5

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier


MDL

0.70

0.70

0.70

0.16

0.30

0.19

0.50

0.18

0.70

0.70

0.16

0.70

0.19

0.16

0.14

0.65

0.19

0.19

0.70

0.70

0.70

0.70

0.33

0.70

0.18

0.70

0.17

0.70

0.70

0.70

0.70

Serial_No:05281316:15

Page 31 of 75


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954


Analytical Date:

05/28/13

Analyst: PD

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Methyl cyclohexane


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.5

2.5

2.5

2.5

5.0

5.0

5.0

5.0

5.0

5.0

2.5

2.0

2.5

2.5

2.5

2.5

2.0

10

10

2.5

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier


No Tentatively Identified Compounds ND ug/l


MDL

0.70

0.70

0.70

0.70

1.0

1.0

1.0

1.0

1.0

1.0

0.70

0.65

0.70

0.70

0.70

0.70

0.65

0.70

0.29

0.70

Serial_No:05281316:15

Page 32 of 75


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954


Analytical Date:

05/28/13

Analyst: PD




Toluene-d8



87

91

98

84

70-130

70-130

70-130

70-130


Criteria

MDL

Serial_No:05281316:15

Page 33 of 75


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

05/24/13 23:261,8011Analytical Method:

Analytical Date: Extraction Date: 05/24/13 13:00

05/28/13

Analyst: SR

1,2-Dibromoethane


Parameter Result

ND

ND

RL

0.010

0.010

ug/l

ug/l

UnitsQualifier

Microextractables by GC - Westborough Lab for sample(s): 08-09 Batch: WG610498-1

MDL

0.003

0.004

Serial_No:05281316:15

Page 34 of 75


1,4-Dioxane

1,2-Dibromoethane

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



2-Chloroethylvinyl ether

Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





1,1-Dichloropropene

Bromoform

88

98

99

98

90

94

88

90

95

103

100

85

96

104

100

89

96

102

94

89

89

88

106

100

104

91

94

87

92

95

106

105

86

97

101

101

89

97

106

95

89

95

68-130

65-136

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-139

70-130

70-130

70-130

70-130

70-130

70-130

70-130

0

8

1

6

2

0

1

2

0

3

5

1

1

3

1

0

1

4

2

1

6

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPD RPD Limits

Volatile Organics by GC/MS-5035 - Westborough Lab Associated sample(s): 01-02 Batch: WG609456-1 WG609456-2

Lab Control Sample AnalysisBatch Quality Control

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

05/28/13

Qual Qual Qual

Serial_No:05281316:15

Page 35 of 75


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Dibromomethane

1,4-Dichlorobutane

1,2,3-Trichloropropane

102

90

95

95

71

114

102

114

85

87

89

96

96

96

91

91

89

88

97

101

103

106

91

96

96

69

116

100

114

86

87

89

91

97

98

95

96

90

90

99

104

109

70-130

70-130

70-130

70-130

52-130

57-147

67-130

50-151

65-135

70-130

70-130

70-130

70-130

70-130

66-130

70-130

70-130

70-130

70-130

70-130

68-130

4

2

2

1

2

2

2

0

1

1

0

6

0

2

4

5

1

2

2

3

6

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

05/28/13

Qual Qual Qual

Serial_No:05281316:15

Page 36 of 75

Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Ethyl methacrylate

Acrolein

Acrylonitrile

Bromochloromethane

Tetrahydrofuran

2,2-Dichloropropane

1,3-Dichloropropane


Bromobenzene

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

o-Chlorotoluene

94

86

129

90

119

96

84

96

96

69

86

90

83

87

103

94

82

99

97

95

97

98

83

129

89

118

101

90

101

100

76

89

92

74

87

107

96

93

99

96

93

102

70-130

30-146

54-140

59-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

66-130

70-130

69-130

70-130

70-130

70-130

70-130

70-130

70-130

5

4

0

0

1

5

6

5

4

9

3

1

11

0

4

2

13

0

1

2

5

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

05/28/13

Qual Qual Qual

Serial_No:05281316:15

Page 37 of 75

p-Chlorotoluene

Hexachlorobutadiene

Isopropylbenzene

p-Isopropyltoluene

Naphthalene

n-Propylbenzene





trans-1,4-Dichloro-2-butene

Ethyl ether

Methyl Acetate

Ethyl Acetate

Isopropyl Ether

Cyclohexane

tert-Butyl Alcohol

Ethyl-Tert-Butyl-Ether

Methyl cyclohexane


99

81

91

93

89

97

81

86

96

98

99

113

93

77

91

84

85

91

88

93

100

84

90

93

95

97

91

90

97

98

105

119

97

89

94

82

92

94

88

91

70-130

67-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

67-130

51-146

66-130

59-142

67-130

70-130

70-130

50-139

1

3

1

0

7

0

12

4

1

0

6

5

4

14

4

3

8

3

1

2

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

05/28/13

Qual Qual Qual

Serial_No:05281316:15

Page 38 of 75

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene

99

96

106

104

106

100

91

98

96

89

85

95

90

95

91

84

86

88

70-130

70-130

70-130

63-132

70-130

63-130

70-130

70-130

75-130

11

12

11

14

11

9

8

13

9

20

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery



Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 08 Batch: WG610254-1 WG610254-2


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954


Toluene-d8



107

107

104

103

70-130

70-130

70-130

70-130

108

108

104

104

Surrogate Qual%Recovery Qual%RecoveryLCS LCSD

05/28/13

AcceptanceCriteria

Qual Qual Qual

Serial_No:05281316:15

Page 39 of 75


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

106

102

101

99

80

98

87

83

101

93

86

98

112

89

90

96

93

104

96

96

94

89

90

88

89

78

87

76

76

90

83

79

88

97

80

79

85

88

90

83

80

82

62-150

70-130

67-130

67-130

70-130

70-130

54-136

67-130

70-130

70-130

70-130

64-130

39-139

55-140

55-138

61-145

70-130

70-130

70-130

70-130

70-130

17

13

14

11

3

12

13

9

12

11

8

11

14

11

13

12

6

14

15

18

14

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

05/28/13

Qual Qual Qual

Serial_No:05281316:15

Page 40 of 75


p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

tert-Butyl Alcohol

1,4-Dioxane

100

93

94

112

92

96

68

88

75

100

80

120

97

88

84

95

102

93

88

77

0

90

85

86

101

85

82

59

75

70

103

75

93

93

80

71

87

90

88

76

80

0

63-130

70-130

70-130

70-130

70-130

36-147

58-148

51-130

63-138

59-130

57-130

70-130

70-130

41-144

70-130

70-130

70-130

70-130

70-130

70-130

56-162

11

9

9

10

8

16

14

16

7

3

6

25

4

10

17

9

13

6

15

4

NC

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

05/28/13

Qual Qual

Q Q

Qual

Q

Serial_No:05281316:15

Page 41 of 75

Methyl cyclohexane


1,4-Dioxane

78

96

100

66

82

118

70-130

70-130

70-130

17

16

17

20

20

25

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery



Volatile Organics by GC/MS-SIM - Westborough Lab Associated sample(s): 08 Batch: WG610255-1 WG610255-2


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954


Toluene-d8



88

87

93

106

70-130

70-130

70-130

70-130

90

89

85

98


05/28/13

AcceptanceCriteria

Qual Qual

Q

Qual

Serial_No:05281316:15

Page 42 of 75

1,4-Dioxane

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene

124

97

93

104

110

106

94

87

110

95

115

90

90

101

100

103

87

79

90

89

70-130

70-130

70-130

70-130

63-132

70-130

63-130

70-130

70-130

75-130

8

7

3

3

10

3

8

10

20

7

25

20

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


Volatile Organics by GC/MS-SIM - Westborough Lab Associated sample(s): 09 Batch: WG610273-1 WG610273-2



Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

05/28/13

Qual Qual Qual

Serial_No:05281316:15

Page 43 of 75


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

112

104

107

98

80

94

81

86

104

93

92

97

93

97

87

94

105

110

95

93

94

103

100

96

95

74

93

81

78

97

84

80

93

87

85

80

90

91

100

92

92

91

62-150

70-130

67-130

67-130

70-130

70-130

54-136

67-130

70-130

70-130

70-130

64-130

39-139

55-140

55-138

61-145

70-130

70-130

70-130

70-130

70-130

8

4

11

3

8

1

0

10

7

10

14

4

7

13

8

4

14

10

3

1

3

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

05/28/13

Qual Qual Qual

Serial_No:05281316:15

Page 44 of 75


p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Methyl cyclohexane


99

94

96

113

93

100

70

88

82

114

84

119

98

81

88

99

100

97

106

109

107

90

84

88

112

85

100

55

81

72

95

68

113

87

75

81

100

95

87

93

85

98

63-130

70-130

70-130

70-130

70-130

36-147

58-148

51-130

63-138

59-130

57-130

70-130

70-130

41-144

70-130

70-130

70-130

70-130

70-130

70-130

70-130

10

11

9

1

9

0

24

8

13

18

21

5

12

8

8

1

5

11

13

25

9

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

05/28/13

Qual Qual

Q

Qual

Q

Q

Q

Serial_No:05281316:15

Page 45 of 75

1,2-Dibromoethane


100

100

-

-

70-130

70-130

-

-

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery



Microextractables by GC - Westborough Lab Associated sample(s): 08-09 Batch: WG610498-2


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954


Toluene-d8



90

85

88

110

70-130

70-130

70-130

70-130

88

83

92

105


05/28/13

AcceptanceCriteria

Qual Qual Qual

Serial_No:05281316:15

Page 46 of 75

1,2-Dibromoethane ND 0.249 101 - - 70-130 - 20

ParameterNative Sample

MS Found

MS%Recovery

MSD Found

MSD %Recovery RPD

RPD Limits

Microextractables by GC - Westborough Lab Associated sample(s): 08-09 QC Batch ID: WG610498-3 QC Sample: L1308960-01 Client ID: MS Sample

0.246

MS Added

Matrix Spike AnalysisBatch Quality Control

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

05/28/13

RecoveryLimitsQual Qual Qual

Serial_No:05281316:15

Page 47 of 75

PETROLEUM HYDROCARBONS

Serial_No:05281316:15

Page 48 of 75

FF

Total EPH


375 mg/kg 1

Qualifier Units RL

NJ Extractable Petroleum Hydrocarbons (Total) - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

27.2

Chloro-Octadecane

o-Terphenyl

88

93

40-140

40-140


05/28/13

UST-3 8-8.5Client ID:05/16/13 11:22Date Collected:05/17/13Date Received:


L1308954-05Lab ID:

Field Prep: Not SpecifiedMatrix: Soil Extraction Method:Analytical Method:Analytical Date:Analyst:

103,NJDEP EPH05/21/13 16:28AR

EPA 3546Extraction Date: 05/18/13 13:09

85%Percent Solids:

MDL

27.2

Serial_No:05281316:15

Page 49 of 75

Total EPH


ND mg/kg 1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

27.8

Chloro-Octadecane

o-Terphenyl

84

78

40-140

40-140


05/28/13

UST-4 7.5-8Client ID:05/16/13 11:31Date Collected:05/17/13Date Received:


L1308954-06Lab ID:


103,NJDEP EPH05/21/13 19:59AR


84%Percent Solids:

MDL

27.8

Serial_No:05281316:15

Page 50 of 75

Total EPH


40.8 mg/kg 1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

23.9

Chloro-Octadecane

o-Terphenyl

87

86

40-140

40-140


05/28/13

I-1Client ID:05/16/13 10:42Date Collected:05/17/13Date Received:


L1308954-07Lab ID:


103,NJDEP EPH05/21/13 17:59AR


96%Percent Solids:

MDL

23.9

Serial_No:05281316:15

Page 51 of 75


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

05/21/13 14:51103,NJDEP EPHAnalytical Method:

Analytical Date:Extraction Method: EPA 3546Extraction Date: 05/18/13 13:09

05/28/13

Analyst: AR

Total EPH

Parameter Result

ND

RL

23.3mg/kg

UnitsQualifier

NJ Extractable Petroleum Hydrocarbons (Total) - Westborough Lab for sample(s): 05-07 Batch: WG609036-1

Chloro-Octadecane

o-Terphenyl

76

72

40-140

40-140


Criteria

MDL

23.3

Serial_No:05281316:15

Page 52 of 75

Total EPH

Nonane (C9)

Decane (C10)

Dodecane (C12)

Tetradecane (C14)

Hexadecane (C16)

Octadecane (C18)

Eicosane (C20)

Heneicosane (C21)

Docosane (C22)

Tetracosane (C24)

Hexacosane (C26)

Octacosane (C28)

Triacontane (C30)

Dotriacontane (C32)

Tetratriacontane (C34)

Hexatriacontane (C36)

Octatriacontane (C38)

Tetracontane (C40)

94

70

78

79

83

90

90

91

93

92

91

91

89

92

92

90

89

89

87

90

65

73

73

75

84

86

88

90

89

88

89

86

89

89

86

85

84

82

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

4

7

7

8

10

7

5

3

3

3

3

2

3

3

3

5

5

6

6

25

25

25

25

25

25

25

25

25

25

25

25

25

25

25

25

25

25

25

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


NJ Extractable Petroleum Hydrocarbons (Total) - Westborough Lab Associated sample(s): 05-07 Batch: WG609036-2 WG609036-3


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

05/28/13

Qual Qual Qual

Serial_No:05281316:15

Page 53 of 75

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


NJ Extractable Petroleum Hydrocarbons (Total) - Westborough Lab Associated sample(s): 05-07 Batch: WG609036-2 WG609036-3


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

Chloro-Octadecane

o-Terphenyl

94

93

40-140

40-140

89

88


05/28/13

AcceptanceCriteria

Qual Qual Qual

Serial_No:05281316:15

Page 54 of 75

Total EPH

Nonane (C9)

Decane (C10)

Dodecane (C12)

Tetradecane (C14)

Hexadecane (C16)

Octadecane (C18)

Eicosane (C20)

Heneicosane (C21)

Docosane (C22)

Tetracosane (C24)

Hexacosane (C26)

Octacosane (C28)

Triacontane (C30)

Dotriacontane (C32)

Tetratriacontane (C34)

Hexatriacontane (C36)

Octatriacontane (C38)

Tetracontane (C40)

375.

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

724

3.87

4.68

5.58

8.47

8.60

8.16

7.76

7.87

7.46

7.07

6.94

6.72

6.94

6.91

6.76

6.80

6.87

6.85

129

51

62

74

112

114

108

103

104

99

94

92

89

92

92

90

90

91

91

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

40-140

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50


MS Found

MS%Recovery

MSD Found

MSD %Recovery RPD

RPD Limits

NJ Extractable Petroleum Hydrocarbons (Total) - Westborough Lab Associated sample(s): 05-07 QC Batch ID: WG609036-4 QC Sample: L1308954-05 Client ID: UST-3 8-8.5

271

7.54

7.54

7.54

7.54

7.54

7.54

7.54

7.54

7.54

7.54

7.54

7.54

7.54

7.54

7.54

7.54

7.54

7.54

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

05/28/13


Serial_No:05281316:15

Page 55 of 75


MS Found

MS%Recovery

MSD Found

MSD %Recovery RPD

RPD Limits


MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

05/28/13

Chloro-Octadecane

o-Terphenyl

40-140

40-140

Surrogate % RecoveryAcceptance

CriteriaQualifier

91

92

% Recovery QualifierMS MSD


Serial_No:05281316:15

Page 56 of 75

Total EPH 375. 210 mg/kg 56 50

Units RPDParameter Native Sample Duplicate Sample RPD Limits


Not Specified

12-1272

Project Name:

Project Number:

L1308954Lab Number:

Report Date:

Lab Duplicate AnalysisBatch Quality Control

Chloro-Octadecane

o-Terphenyl

82

83

40-140

40-140


Criteria

05/28/13

88

93

%Recovery Qualifier

Qual

Q

Serial_No:05281316:15

Page 57 of 75

INORGANICS&

MISCELLANEOUS

Serial_No:05281316:15

Page 58 of 75

FF


Parameter ResultDilution Factor

Matrix: Soil


L1308954-01Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

Field Prep:

DateAnalyzed

AnalyticalMethod Analyst

Not Specified

General Chemistry - Westborough LabSolids, Total 88.1 % 10.100 05/20/13 09:46 30,2540G MO

Date Prepared

-

05/28/13

MDL

NA

Serial_No:05281316:15

Page 59 of 75

FF



Matrix: Soil


L1308954-02Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

05/28/13

MDL

NA

Serial_No:05281316:15

Page 60 of 75

FF

UST-3 8-8.5Client ID:05/16/13 11:22Date Collected:05/17/13Date Received:


Matrix: Soil


L1308954-05Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

05/28/13

MDL

NA

Serial_No:05281316:15

Page 61 of 75

FF

UST-4 7.5-8Client ID:05/16/13 11:31Date Collected:05/17/13Date Received:


Matrix: Soil


L1308954-06Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

05/28/13

MDL

NA

Serial_No:05281316:15

Page 62 of 75

FF

I-1Client ID:05/16/13 10:42Date Collected:05/17/13Date Received:


Matrix: Soil


L1308954-07Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

Not Specified

12-1272

L1308954

Field Prep:

DateAnalyzed


Not Specified


Date Prepared

-

05/28/13

MDL

NA

Serial_No:05281316:15

Page 63 of 75

Solids, Total 83.0 83.6 % 1 20

Units RPDParameter Native Sample Duplicate Sample RPD Limits

General Chemistry - Westborough Lab Associated sample(s): 01-02,05-07 QC Batch ID: WG609228-1 QC Sample: L1308924-01 Client ID: DUP Sample

Not Specified

12-1272

Project Name:

Project Number:

L1308954Lab Number:

Report Date:

Lab Duplicate AnalysisBatch Quality Control

05/28/13

Qual

Serial_No:05281316:15

Page 64 of 75

*Values in parentheses indicate holding time in days

L1308954-01A

L1308954-01B

L1308954-01C

L1308954-01D

L1308954-01E

L1308954-01F

L1308954-01G

L1308954-02A

L1308954-02B

L1308954-02C

L1308954-02D

L1308954-02E

L1308954-02F

L1308954-02G

L1308954-03A

L1308954-04A

L1308954-05A

L1308954-06A

L1308954-07A

L1308954-08A

L1308954-08B

L1308954-08C

L1308954-08D

L1308954-08E

L1308954-08F

L1308954-09A

L1308954-09B

5 gram Encore Sampler



Vial MeOH preserved split

Vial Water preserved split


Plastic 2oz unpreserved for TS




Vial MeOH preserved split



Plastic 2oz unpreserved for TS

Amber 250ml unpreserved





Vial HCl preserved

Vial HCl preserved

Vial HCl preserved

Vial Na2S2O3 preserved



Vial HCl preserved

Vial HCl preserved

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

2.7

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

A AbsentCooler

Custody SealCooler Information

Not Specified

12-1272

NJ-8260HLW(2)

NJ-8260HLW(2)

NJ-8260HLW(2)

NJ-8260HLW(14)

NJ-8260HLW(14)

NJ-8260HLW(14)

TS(7)

NJ-8260HLW(2)

NJ-8260HLW(2)

NJ-8260HLW(2)

NJ-8260HLW(14)

NJ-8260HLW(14)

NJ-8260HLW(14)

TS(7)

HOLD()

HOLD()

NJEPH-TPH-CAT1(14),TS(7)



8260-SIM(14),NJ-8260(14)

8260-SIM(14),NJ-8260(14)

8260-SIM(14),NJ-8260(14)

8011(14)

8011(14)

8011(14)

8260-SIM(14),NJ-8260(14)

8260-SIM(14),NJ-8260(14)

Project Name:

Project Number:

L1308954Lab Number:

Report Date:

Sample Receipt and Container Information

Container ID Container Type Cooler pHTempdeg C Pres Seal

Container Information

Analysis(*)

05/28/13

Were project specific reporting limits specified? YES

Reagent H2O Preserved Vials Frozen on: 05/18/2013 01:01

Serial_No:05281316:15

Page 65 of 75

*Values in parentheses indicate holding time in days

L1308954-09C

L1308954-09D

L1308954-09E

L1308954-09F

L1308954-10A

L1308954-11A

Vial HCl preserved






A

A

A

A

A

A

N/A

N/A

N/A

N/A

N/A

N/A

2.7

2.7

2.7

2.7

2.7

2.7

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Not Specified

12-1272

8260-SIM(14),NJ-8260(14)

8011(14)

8011(14)

8011(14)

HOLD()

HOLD()

Project Name:

Project Number:

L1308954Lab Number:

Report Date:

Container ID Container Type Cooler pHTempdeg C Pres Seal

Container Information

Analysis(*)

05/28/13

Serial_No:05281316:15

Page 66 of 75

Report Format: DU Report with "J" Qualifiers

GLOSSARY

Project Name:

Project Number:

Lab Number:

Report Date:

L1308954Not Specified

12-1272 05/28/13

Acronyms

EDL

EPA

LCS

LCSD

LFB

MDL

MS

MSD

NA

NC

NI

RL

RPD

SRM

Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis of PAHs using Solid-Phase Microextraction (SPME).Environmental Protection Agency.

Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes.Laboratory Control Sample Duplicate: Refer to LCS.

Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes.Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any adjustments from dilutions, concentrations or moisture content, where applicable.Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. Matrix Spike Sample Duplicate: Refer to MS.

Not Applicable.

Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit.Not Ignitable.

Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL includes any adjustments from dilutions, concentrations or moisture content, where applicable.Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precisionof analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report.Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples.

-

-

-

-

-

-

-

-

-

-

-

-

-

-

Terms

Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum.

Data Qualifiers

A

B

C

D

E

G

H

I

-

-

-

-

-

-

-

-

Spectra identified as "Aldol Condensation Product".

The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte at less than five times (5x) the concentration found in the blank. For MCP-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ-Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit.Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted analyses.Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations of the analyte.Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument.

The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should be considered estimated.The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.

The RPD between the results for the two columns exceeds the method-specified criteria; however, the lower value has been reported

1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the originalmethod.

-

Footnotes

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Report Format: DU Report with "J" Qualifiers

Project Name:

Project Number:

Lab Number:

Report Date:


12-1272 05/28/13

Data Qualifiers

M

NJ

P

Q

R

RE

-

-

-

-

-

-

due to obvious interference.

Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte.

Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where the identification is based on a mass spectral library search.The RPD between the results for the two columns exceeds the method-specified criteria.

The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing CalibrationStandard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoverieswhen the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are lessthan 5x the RL. (Metals only.)Analytical results are from sample re-analysis.

Analytical results are from sample re-extraction.

J

ND

-

-

Estimated value. The Target analyte concentration is below the quantitation limit (RL), but above the Method Detection Limit (MDL) or Estimated Detection Limit (EDL) for SPME-related analyses. This represents an estimated concentration for Tentatively Identified Compounds (TICs).Not detected at the method detection limit (MDL) for the sample, or estimated detection limit (EDL) for SPME-related analyses.

Serial_No:05281316:15

Page 68 of 75

Alpha Analytical performs services with reasonable care and diligence normal to the analytical testinglaboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analyticalshall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liablefor any incidental, consequential or special damages, including but not limited to, damages in any wayconnected with the use of, interpretation of, information or analysis provided by Alpha Analytical.

We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,containers, sampling procedures, holding time and splitting of samples in the field.

LIMITATION OF LIABILITIES

1

30

103

Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates I - IIIA, 1997.

Standard Methods for the Examination of Water and Wastewater. APHA-AWWA-WPCF. 18th Edition. 1992.

Analysis of Extractable Petroleum Hydrocarbon Compounds (EPH) in Aqueous and Soil/Sediment/Sludge Matrices. New Jersey Department of Environmental Protection, Site Remediation Program, (Version 1.1), Document # NJDEP EPH 10/08, Revision 3, August 2010.

Project Name:

Project Number:

Lab Number:

Report Date:


12-1272

REFERENCES

05/28/13

Serial_No:05281316:15

Page 69 of 75

Certificate/Approval Program Summary Last revised December 19, 2012 - Westboro Facility

The following list includes only those analytes/methods for which certification/approval is currently held.

For a complete listing of analytes for the referenced methods, please contact your Alpha Customer Service Representative.

Connecticut Department of Public Health Certificate/Lab ID: PH-0574. NELAP Accredited Solid Waste/Soil. Drinking Water (Inorganic Parameters: Color, pH, Turbidity, Conductivity, Alkalinity, Chloride, Free Residual Chlorine, Fluoride, Calcium Hardness, Sulfate, Nitrate, Nitrite, Aluminum, Antimony, Arsenic, Barium, Beryllium, Cadmium, Calcium, Chromium, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Nickel, Selenium, Silver, Sodium, Thallium, Zinc, Total Dissolved Solids, Total Organic Carbon, Total Cyanide, Perchlorate. Organic Parameters: Volatile Organics 524.2, Total Trihalomethanes 524.2, 1,2-Dibromo-3-chloropropane (DBCP) 504.1, Ethylene Dibromide (EDB) 504.1, 1,4-Dioxane (Mod 8270). Microbiology Parameters: Total Coliform-MF mEndo (SM9222B), Total Coliform – Colilert (SM9223, Enumeration and P/A), E. Coli. – Colilert (SM9223, Enumeration and P/A), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform-EC Medium (SM 9221E). Wastewater/Non-Potable Water (Inorganic Parameters: Color, pH, Conductivity, Acidity, Alkalinity, Chloride, Total Residual Chlorine, Fluoride, Total Hardness, Silica, Sulfate, Sulfide, Ammonia, Kjeldahl Nitrogen, Nitrate, Nitrite, O-Phosphate, Total Phosphorus, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Strontium, Thallium, Tin, Titanium, Vanadium, Zinc, Total Residue (Solids), Total Dissolved Solids, Total Suspended Solids (non-filterable), BOD, CBOD, COD, TOC, Total Cyanide, Phenolics, Foaming Agents (MBAS), Bromide, Oil and Grease. Organic Parameters: PCBs, Organochlorine Pesticides, Technical Chlordane, Toxaphene, Acid Extractables (Phenols), Benzidines, Phthalate Esters, Nitrosamines, Nitroaromatics & Isophorone, Polynuclear Aromatic Hydrocarbons, Haloethers, Chlorinated Hydrocarbons, Volatile Organics, TPH (HEM/SGT), CT- Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH. Microbiology Parameters: Total Coliform – MF mEndo (SM9222B), Total Coliform – MTF (SM9221B), E. Coli – Colilert (SM9223 Enumeration), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform – A-1 Broth (SM9221E), Enterococcus - Enterolert. Solid Waste/Soil (Inorganic Parameters: pH, Sulfide, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Thallium, Tin, Vanadium, Zinc, Total Cyanide, Ignitability, Phenolics, Corrosivity, TCLP Leach (1311), SPLP Leach (1312 metals only), Reactivity. Organic Parameters: PCBs, PCBs in Oil, Organochlorine Pesticides, Technical Chlordane, Toxaphene, CT-Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH, Dicamba, 2,4-D, 2,4,5-T, 2,4,5-TP(Silvex), Dalapon, Volatile Organics (SW 8260), Acid Extractables (Phenols) (SW 8270), Benzidines (SW 8270), Phthalates (SW 8270), Nitrosamines (SW 8270), Nitroaromatics & Cyclic Ketones (SW 8270), PAHs (SW 8270), Haloethers (SW 8270), Chlorinated Hydrocarbons (SW 8270). ) Maine Department of Human Services Certificate/Lab ID: 2009024. Drinking Water (Inorganic Parameters: SM9215B, 9222D, 9223B, EPA 180.1, 353.2, SM2130B, 2320B, 2540C, 4500Cl-D, 4500CN-C, 4500CN-E, 4500F-C, 4500H+B, 4500NO3-F, EPA 200.7, EPA 200.8, 245.1, EPA 300.0. Organic Parameters: 504.1, 524.2.) Wastewater/Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 350.1, 351.1, 353.2, 410.4, 420.1, SM2320B, 2510B, 2540C, 2540D, 426C, 4500Cl-D, 4500Cl-E, 4500CN-C, 4500CN-E, 4500F-B, 4500F-C, 4500H+B, 4500Norg-B, 4500Norg-C, 4500NH3-B, 4500NH3-G, 4500NO3-F, 4500P-B, 4500P-E, 5210B, 5220D, 5310C, 9010B, 9040B, 9030B, 7470A, 7196A, 2340B, EPA 200.7, 6010B, 6010C, 200.8, 6020, 245.1, 1311, 1312, 3005A, Enterolert, 9223B, 9222D. Organic Parameters: 608, 624, 625, 8081A, 8081B, 8082, 8082A, 8330, 8151A, 8260B, 8260C, 8270C, 8270D, 3510C, 3630C, 5030B, ME-DRO, ME-GRO, MA-EPH, MA-VPH.) Solid Waste/Soil (Inorganic Parameters: 9010B, 9012A, 9014, 9030B, 9040B, 9045C, 6010B, 6010C, 6020, 6020A, 7471A, 7471B, 7196A, 9050A, 1010, 1030, 9065, 1311, 1312, 3005A, 3050B. Organic Parameters: ME-DRO, ME-GRO, MA-EPH, MA-VPH, 8260B, 8270C, 8270D, 8330, 8151A, 8081A, 8081B, 8082, 8082A, 3540C, 3546, 3580A, 3630C, 5030B, 5035.) Massachusetts Department of Environmental Protection Certificate/Lab ID: M-MA086. Drinking Water (Inorganic Parameters: (EPA 200.8 for: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,Tl) (EPA 200.7 for: Ba,Be,Ca,Cd,Cr,Cu,Na,Ni) 245.1, (300.0 for: Nitrate-N, Fluoride, Sulfate); (EPA 353.2 for: Nitrate-N, Nitrite-N); (SM4500NO3-F for: Nitrate-N and Nitrite-N); 4500F-C, 4500CN-CE, EPA 180.1, SM2130B, SM4500Cl-D, 2320B, SM2540C, SM4500H-B. Organic Parameters: (EPA 524.2 for: Trihalomethanes, Volatile Organics); (504.1 for: 1,2-Dibromoethane, 1,2-Dibromo-3-Chloropropane), EPA 332. Microbiology Parameters: SM9215B; ENZ. SUB. SM9223; ColilertQT SM9223B; MF-SM9222D.)

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Non-Potable Water (Inorganic Parameters:, (EPA 200.8 for: Al,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,Tl,Zn); (EPA 200.7 for: Al,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,Tl,V,Zn); 245.1, SM4500H,B, EPA 120.1, SM2510B, 2540C, 2340B, 2320B, 4500CL-E, 4500F-BC, 426C, SM4500NH3-BH, (EPA 350.1 for: Ammonia-N), LACHAT 10-107-06-1-B for Ammonia-N, SM4500NO3-F, 353.2 for Nitrate-N, SM4500NH3-BC-NES, EPA 351.1, SM4500P-E, 4500P-B,E, 5220D, EPA 410.4, SM 5210B, 5310C, 4500CL-D, EPA 1664, SM14 510AC, EPA 420.1, SM4500-CN-CE, SM2540D. Organic Parameters: (EPA 624 for Volatile Halocarbons, Volatile Aromatics),(608 for: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT,Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs-Water), (EPA 625 for SVOC Acid Extractables and SVOC Base/Neutral Extractables), 600/4-81-045-PCB-Oil. Microbiology Parameters: (ColilertQT SM9223B; Enterolert-QT: SM9222D-MF.) New Hampshire Department of Environmental Services Certificate/Lab ID: 200307. NELAP Accredited. Drinking Water (Inorganic Parameters: SM 9222B, 9223B, 9215B, EPA 200.7, 200.8, 300.0, SM4500CN-E, 4500H+B, 4500NO3-F, 2320B, 2510B, 2540C, 4500F-C, 5310C, 2120B, EPA 332.0. Organic Parameters: 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM9222D, 9221B, 9222B, 9221E-EC, EPA 3005A, 200.7, 200.8, 245.1, SW-846 6010C, 6020A, 7196A, 7470A, SM3500-CR-D, EPA 120.1, 300.0, 350.1, 350.2, 351.1, 353.2, 410.4, 420.1, 426C, 1664A, SW-846 9010B, 9010C, 9030, 9040B, 9040C, SM2120B, 2310B, 2320B, 2340B, 2540B, 2540D, 4500H+B, 4500CL-E, 4500CN-E, 4500NH3-H, 4500NO3-F, 4500NO2-B, 4500P-E, 4500-S2-D, 4500SO3-B, 5210B, 5220D, 2510B, 2540C, 4500F-C, 5310C, 5540C, LACHAT 10-204-00-1-A, LACHAT 10-107-06-2-D, 3060A. Organic Parameters: SW-846 3510C, 3630C, 5030B, 8260C, 8270D, 8330, EPA 624, 625, 608, SW-846 8082A, 8081B, 8015C, 8151A, 8330, 8270D-SIM.) Solid & Chemical Materials (Inorganic Parameters: SW-846 6010C, 6020A, 7196A, 7471B, 1010, 1010A, 1030, 9010C, 9012B, 9014, 9030B, 9040C, 9045C, 9045D, 9050, 9065, 9251, 1311, 1312, 3005A, 3050B, 3060A. Organic Parameters: SW-846 3540C, 3546, 3050B, 3580A, 3620D, 3630C, 5030B, 5035, 8260C, 8270D, 8270D-SIM, 8330, 8151A, 8015B, 8015C, 8082A, 8081B.) New Jersey Department of Environmental Protection Certificate/Lab ID: MA935. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9222B, 9221E, 9223B, 9215B, 4500CN-CE, 4500NO3-F, 4500F-C, EPA 300.0, 200.7, 200.8, 245.1, 2540C, SM2120B, 2320B, 2510B, 5310C, SM4500H-B. Organic Parameters: EPA 332, 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM5210B, EPA 410.4, SM5220D, 4500Cl-E, EPA 300.0, SM2120B, 2340B, SM4500F-BC, EPA 200.7, 200.8, 351.1, LACHAT 10-107-06-2-D, EPA 353.2, SM4500NO3-F, 4500NO2-B, EPA 1664A, SM5310B, C or D, 4500-PE, EPA 420.1, SM510ABC, SM4500P-B5+E, 2540B, 2540C, 2540D, EPA 120.1, SM2510B, SM2520B, SM15 426C, 9222D, 9221B, 9221C, 9221E, 9222B, 9215B, 2310B, 2320B, 4500NH3-H, 4500-S D, EPA 350.1, 350.2, SW-846 1312, 7470A, 5540C, SM4500H-B, 4500SO3-B, SM3500Cr-D, 4500CN-CE, EPA 245.1, SW-846 9040B, 9040C, 3005A, 3015, EPA 6010B, 6010C, 6020, 6020A, 7196A, 3060A, SW-846 9010C, 9030B. Organic Parameters: SW-846 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3510C, EPA 608, 624, 625, SW-846 3630C, 5030B, 8011, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 1,4-Dioxane by NJ Modified 8270, 8015B, NJ EPH.) Solid & Chemical Materials (Inorganic Parameters: SW-846, 6010B, 6010C, 6020, 6020A, 7196A, 3060A, 9030B, 1010, 1010A, 1030, 1311, 1312, 3005A, 3050B, 7471A, 7471B, 9010C, 9012B, 9014, 9038, 9040B, 9040C, 9045C, 9045D, 9050A, 9065, 9251. Organic Parameters: SW-846 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3540C, 3546, 3580A, 3620C, 3630C, 5030B, 5035L, 5035H, NJ EPH.) New York Department of Health Certificate/Lab ID: 11148. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9223B, 9222B, 9215B, EPA 200.8, 200.7, 245.2, SM5310C, EPA 332.0, SM2320B, EPA 300.0, SM2120B, 4500CN-E, 4500F-C, 4500NO3-F, 2540C, SM 2510B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: SM9221E, 9222D, 9221B, 9222B, 9215B, 5210B, 5310C, EPA 410.4, SM5220D, 2310B-4a, 2320B, EPA 200.7, 300.0, SM4500CL-E, 4500F-C, SM15 426C, EPA 350.1, SM4500NH3-BH, EPA 351.1, LACHAT 10-107-06-2, EPA 353.2, SM4500-NO3-F, 4500-NO2-B, 4500P-E, 2540C, 2540B, 2540D, EPA 200.8, EPA 6010B, 6010C, 6020, 6020A, EPA 7196A, SM3500Cr-D, EPA 245.1, 7470A, SM2120B, LACHAT 10-204-00-1-A, 4500CN-CE, EPA 1664A, EPA 420.1, SM14 510C, EPA 120.1, SM2510B, SM4500S-D, SM5540C, EPA 3005A, 3015, 9010C, 9030B. Organic Parameters: EPA 624, 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 625, 608, 8081A, 8081B, 8151A, 8330, 8082, 8082A, EPA 3510C, 5030B.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010A, 1030, EPA 6010B, 6010C, 7196A, 7471A, 7471B, 9012B, 9014, 9065, 9050A, EPA 1311, 1312, 3005A, 3050B, 9010C, 9030B, 9040C, 9045D. Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8015B, 8015C, 8081A, 8081B, 8151A, 8330, 8082 8082A, 3540C,

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3546, 3580A, 5030B, 5035A-H, 5035A-L.) North Carolina Department of the Environment and Natural Resources Certificate/Lab ID : 666. (Inorganic Parameters: SM2310B, 2320B, 4500Cl-E, 4500Cn-E, 9014, Lachat 10-204-00-1-X, 1010A, 1030, 4500NO3-F, 353.2, 4500P-E, 4500SO4-E, 300.0, 4500S-D, 5310B, 5310C, 6010C, 6020A, 200.7, 200.8, 3500Cr-B, 7196A, 245.1, 7470A, 7471B, 1311,1312. Organic Parameters: 608, 8081B, 8082A, 624, 8260B, 625, 8270D, 8151A, 8015C, 504.1, MA-EPH, MA-VPH.) Drinking Water Program Certificate/Lab ID: 25700. (Inorganic Parameters: Chloride EPA 300.0. Organic Parameters: 524.2) Pennsylvania Department of Environmental Protection Certificate/Lab ID : 68-03671. NELAP Accredited. Drinking Water (Inorganic Parameters: 200.7, 200.8, 300.0, 332.0, 2120B, 2320B, 2510B, 2540C, 4500-CN-CE, 4500F-C, 4500H+-B, 4500NO3-F, 5310C. Organic Parameters: EPA 524.2, 504.1) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1312, 3005A,3015, 3060A, 200.7, 200.8, 410.4, 1664A, SM2540D, 5210B, 5220D, 4500-P,BE, 245.1, 300.0, 350.1, 350.2, 351.1, 353.2, 420.1, 6010C, 6020A, 7196A, 7470A, 9030B, 2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 3500Cr-D, 426C, 4500CN-CE, 4500Cl-E, 4500F-B, 4500F-C, 4500H+-B, 4500NH3-H, 4500NO2-B, 4500NO3-F, 4500S-D, 4500SO3-B, 5310BCD, 5540C, 9010C, 9040C. Organic Parameters: EPA 3510C, 3630C, 5030B, 625, 624, 608, 8081B, 8082A, 8151A, 8260C, 8270D, 8270D-SIM, 8330, 8015C, NJ-EPH.) Solid & Hazardous Waste (Inorganic Parameters: EPA 350.1, 1010, 1030, 1311, 1312, 3005A, 3050B, 3060A, 6010C, 6020A, 7196A, 7471B, 9010C, 9012B, 9014, 9040B, 9045D, 9050A, 9065, SM 4500NH3-BH, 9030B, 9038, 9251. Organic Parameters: 3540C, 3546, 3580A, 3620C, 3630C, 5035, 8015C, 8081B, 8082A, 8151A, 8260C, 8270D, 8270D-SIM, 8330, NJ-EPH.) Rhode Island Department of Health Certificate/Lab ID: LAO00065. NELAP Accredited via NJ-DEP. Refer to MA-DEP Certificate for Potable and Non-Potable Water. Refer to NJ-DEP Certificate for Potable and Non-Potable Water. Texas Commisson on Environmental Quality Certificate/Lab ID: T104704476. NELAP Accredited. Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664, 200.7, 200.8, 245.1, 245.2, 300.0, 350.1, 351.1, 353.2, 410.4, 420.1, 6010, 6020, 7196, 7470, 9040, SM 2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 2540D, 426C, 4500CL-E, 4500CN-E, 4500F-C, 4500H+B, 4500NH3-H, 4500NO2B, 4500P-E, 4500 S2¯D, 510C, 5210B, 5220D, 5310C, 5540C. Organic Parameters: EPA 608, 624, 625, 8081, 8082, 8151, 8260, 8270, 8330.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1311, 1312, 9012, 9014, 9040, 9045, 9050, 9065.) Virginia Division of Consolidated Laboratory Services Certificate/Lab ID: 460195. NELAP Accredited. Drinking Water (Inorganic Parameters: EPA 200.7, 200.8, 300.0, 2510B, 2120B, 2540C, 4500CN-CE, 245.2, 2320B, 4500F-C, 4500NO3-F, 5310C. Organic Parameters: EPA 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 200.7, 200.8, 245.1, 300.0, 3005A, 3015, 1312, 6010B, 6010C, 3060A, 353.2, 420.1, 6020, 6020A, SM4500S-D, SM4500-CN-CE, Lachat 10-204-00-1-X, 7196A, 7470A, 9010B, 9040B, 2310B, 2320B, 2510B, 2540B, 2540C, 3500Cr-D, 426C, 4500Cl-E, 4500F-B, 4500F-C, 4500PE, 510AC, 5210B, 5310B 5310C, 5540C. Organic Parameters: EPA 3510C, 3630C, 5030B, 8260B, 608, 624, 625, 8081A, 8081B, 8082, 8082A, 8151A, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330, ) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010A, 1030, 3060A, 3050B, 1311, 1312, 6010B, 6010C, 6020, , 7196A, 7471A, 7471B, 6020A, 9030B, 9010B, 9012A, 9014 9040B, 9045C, 9050A, 9065. Organic Parameters: EPA 5030B, 5035, 3540C, 3546, 355B0, 3580A, 3630C, 6020A, 8260B, 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330.) Department of Defense, L-A-B Certificate/Lab ID: L2217. Drinking Water (Inorganic Parameters: SM 4500H-B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: EPA 200.7, 200.8, 6010B, 6010C, 6020, 6020A, 245.1, 245.2, 7470A, 9040B, 9010B, 180.1. 300.0, 332.0, 6860, 353.2, 410.4, 9060, 1664A, SM 4500CN-E, 4500H-B, 4500NO3-F, 4500CL-D, 5220D, 5310C, 2130B, 2320B, 2540C, 3005A, 3015, 9010B, 9056, 7196A, 3500-Cr-D. Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330A, 8082, 8082A, 8081A, 8081B, 3510C, 5030B, MassDEP EPH, MassDEP VPH.) Solid & Hazardous Waste (Inorganic Parameters: EPA 200.7, 6010B, 6010C, 7471A, 6860, 1311, 1312, 3050B, 7196A, 9010B, 9012A, 9040B, 9045C, 3500-CR-D, 4500CN-CE, 2540G, Organic Parameters: EPA 8260B, 8260C, 8270C,

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8270D, 8270C-SIM, 8270D-SIM, 8330A/B-prep, 8082, 8082A, 8081A, 8081B, 3540C, 3546, 3580A, 5035A, MassDEP EPH, MassDEP VPH.) The following analytes are not included in our current NELAP/TNI Scope of Accreditation: EPA 8260B: Freon-113, 1,2,4,5-Tetramethylbenzene, 4-Ethyltoluene. EPA 8330A: PETN, Picric Acid, Nitroglycerine, 2,6-DANT, 2,4-DANT. EPA 8270C: Methyl naphthalene, Dimethyl naphthalene, Total Methylnapthalenes, Total Dimethylnaphthalenes, 1,4-Diphenylhydrazine (Azobenzene). EPA 625: 4-Chloroaniline, 4-Methylphenol. Total Phosphorus in a soil matrix, Chloride in a soil matrix, TKN in a soil matrix, NO2 in a soil matrix, NO3 in a soil matrix. EPA 9071: Total Petroleum Hydrocarbons, Oil & Grease.

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tti environmental incorporated 1253 n. church street

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