turbidimetry

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Determination of Sulphate Content in Water Sample Collected from different places using TURBIDIMETER

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Determination of Sulphate Content in

Water Sample Collected from different

places using TURBIDIMETER

Introduction

Group MembersBharath KumarVinit ShahdeoIpsit GambhirArchit RoyAditya SharmaVinod KumarShivam ShuklaAmogha Bhardwaj

Group Photo

TurbidimetryIt is the process of measuring the loss of

intensity of transmitted light due to the

scattering effect of particles suspended in it

Water Sample

Collection

VIT Lake

Tap Water

Sewage Water

DrinkingWater Girls Hostel

VelloreCity

Procedure

Experimental PartSome of the reagents and apparatus used for the estimation of sulphate ions using turbidimetry are:

1.Potassium Sulphate2.Sodium Chloride3.Barium Chloride4.Glycerol5.Pure Alcohol(Ethanol)6.Nephelometer/Turbidimeter

Procedure1.Preparation of Standard Sulphate Solution:

dissolve 0.4535g of dry potassium sulphate in distilled water and make the volume to 250 ml.

Then this solution has the concentration of 1.0mg/ml2.Preparation of Barium Chloride Solution:

Pass the finely powdered crystals of barium chloride weighing 5g in the 100ml of distilled water3.Preparation of Conditioning Reagent:

50ml glycerol+30ml conc.HCL+300ml distilled water+100mlof 95%ethanol+75g of NaCl

1.Take seven 50ml volumetric flasks and label them accordingly, and the first one is for the blank solution preparation2.Transfer 1,2,3,4 and 5 of the standard sulphate solution in the flask number 2,3,4,5 and 63.To each flask add 30ml of conditioning reagent solution4.Add 10ml of barium chloride solution to each flask and make the volume to 50ml. Allow flask to stand for 5 minutes5.The flask marked 1 will have allasunder 3 and 4 but except 26.Use the flask labelled as 7 for the unknown solution.

Preparation of suspended particles

Photo Gallery

Vinod

Amogha

Bharath

Ipsit

Archit

Shivam

Vinit Shahdeo

Aditya

Conclusion

Results Derived From the Experiment:

Blank solution: 0 ppm1ml Sulphate solution: 124 NTU2ml Sulphate solution: 168 NTU3ml Sulphate solution: 251 NTU4ml Sulphate solution: 343 NTU5ml Sulphate solution: 376 NTU

Tap Water: 239 NTU59 ppmLake Water: 298 NTU73.4ppmSewage water: 332 NTU89.6ppmVellore City: 320 NTU69ppmDrinking Water: 28 NTU4.7ppm

Graph

(Values in ppm are inferred from the model graph of the standard solution)

Thank You

Created By: Vinit ShahdeoFor more: vinitshahdeo.blogspot.in