wmi monthly progress report (cover letter included)

1 (05V —30Waste Management of North America. Inc.Midwet.' Rtn-onTwo Westsro?!.' Corpci^te Cri*er • Suite 1000P.O. Be" 7 C 7 j

7c^^9c?: " """1 January 7, 1991Mr. Jae Lee, Remedial Project ManagerRemedial Enforcement and Response BranchMI/WI Section, 5HR-11U.S. Environmental Protection Agency, Region V230 S. Dearborn StreetChicago, Illinois 60604

Ms. Terry EvansonRemedial Project Coordinator Hagen Farm SiteWisconsin Department of Natural ResourcesP. O. Box 7921Madison, Wisconsin 53707-7921

RE: HAGEN FARM SITEMONTHLY PROGRESS REPORT FOR DECEMBER 1990.

Dear Mr. Lee and Ms. Evanson:

In accordance with Section IX, paragraph E of the Hagen Farm AdministrativeOrder by Consent, please find attached three (3) copies of the monthly progressreport for December 1990.

Please contact me if you have any questions.

Sincerely,

Dee BrncichRemedial Projects ManagerWaste Management of North America

DBrjsattachment

cc: Gerard Hamblin-WMNA (report only)Greg Asbury-Warzyn (report only)Timothy C. Wright-The Jesup Group (report only)Rich O'Hara-WMNA-EMD (report only)Ann Straw-WMNA-Legal (report only)Bill Schubert-WMNA (report only)Oliver J. Janney-The Jesup Group, Inc. (report only)Rich Kogler-WMWI (report only)Don Otter-WMWI (report only)Jane LeCapitaine-WMWI (report only)files (8.0 w/attachment, 2.1, 2.3 w/o attachment)

MONTHLY STATUS REPORTDECEMBER 1990

SITE NAME/ACTIVITY:Hagen FarmStoughton, WisconsinRemedial Investigation/Feasibility Study

PREPARED BY:Dee BrncichWaste Management of North AmericaTwo Westbrook Corporate CenterP. O. Box 7070Westchester, IL. 60153

Greg E. AsburyWarzyn Engineering, Inc.One Science CourtMadison, Wisconsin 53705

DATE:January 7,1991

PERIOD:December 1990

PROGRESS MADE THIS REPORTING PERIOD:

During December 1990 the following project activities were conducted:

The groundwater pump test was initiated on Thursday, December 13,1990 and immediately terminated due to the use of PVC glue in the pipejoints connecting the carbon units together.

The groundwater pump test was re-initiated at 12:451 p.m. on December14, 1990 following completion of replumbing activities.

The groundwater pump test was performed for approximately 32 hoursand then permanently terminated at 10:05 p.m. on December 15, 1990due to the apparent breakthrough of the largest carbon column availableat the site.

Drilling activities continued on the downgradient plume characterizationsoil borings.

The Monthly Agency Status Report for November was submitted for^ Agency review.

DATA TRANSMITTED WITH REPORT:

Pumping Test-water quality results (does not include results formanganese, and TCL semi-volatiles at 25.0 hours [See Table 3-WorkPlan Addendum]). RAW data submitted with full report to follow.

Contaminant Characterization Investigation-water quality results (doesnot include results from borings TB-5 or TB-6).

ANTICIPATED PROBLEMS AND RECOMMENDED SOLUTIONS:None

DOCUMENTS SUBMITTED:

None

UPCOMING ACTIVITIES PLANNED:

Complete downgradient soil borings to characterize groundwater qualityat distance and depth.

Summarize the results of the groundwater pump testing.

PERSONNEL CHANGES:

None

TRAVEL MEETINGS:

None

CONTRACT LABORATORY:

Round 4 groundwater monitoring well survey will be conducted at thecompletion of the current field construction program.

SCHEDULE:Attached is a project schedule listing for near-term activities showingthe current breakdown of anticipated dates.

HAGENFAKMRI/FSNEAR-TERM SCHEDULE

January February ' March

3.23

33

Activity

Hydrogeologic Investigation WaterLevels

Contaminant Characterization

Evaluate Pump Test DataTVfiatflhflifv AnfllvsiR

1 2 3 4 1 2 3 4 1 2 3 4X

^ Sofl Boring Construction

Field Sample Analysis/Interpretation

EPA/WDNR Concurrence

Monitoring Well Construction

Round 4 Sampling

* Indicates a non-schedulable activity

Pagel

Explanation of Sample DescriptionsFor the Pumping Test Water Quahty Results

Sample Description

HF-RW1

Step Test After 15000 #CU

HF-PTBT-3.5Q

HF-PTOT-0.1

HF-PTBT-1.0

HF-PTBT-5.N

HF-PTBT-5NDUP

HF-PTBT-5FB

HF-PTBT-10N

HF-PTA15-25Q&N

Explanation

Hagen Farm-recovery well (BeforePumping Test)

Sample taken from effluent of 15000 Ibcarbon unit

Hagen Farm-Pumping Test-BeforeTreatment-3.5 hours from start of test

Hagen Farm-Pumping Test-BeforeTreatment 0.1 hours from start of test



Hagen Farm-Pumping Test-BeforeTreatment Field Blank taken 5.0 hoursfrom start of test - duplicate sample

Hagen Farm-Pumping Test-beforeTreatment Field blank taken 5.0 hoursfrom start of testHagen Farm-Pumping Test-beforeTreatment-10.0 hours from start of test

Hagen Farm-Pumping Test-After 15,000 Ib.carbon units-25.0 hours from start of test

HF-PTA2-25Q&N Hagen Farm-Pumping Test-After 2,000 Ib.carbon units - 25.0 hours from start of test

Sample Description

HF-PTBT-32.5

HF-PTBA15-32.5

HF-PTA2-32.5

HF-PTA2-32.5DUP

Explanation

Hagen Farm-Pumping Test-BeforeTreatment-32^ hours from start of test(immediately prior to termination of test)

Hagen Farm-Pumping Test-After 15,000 Ib.carbon unit-32^ hours from start of test(immediately prior to termination of test).

Hagen Farm-Pumping Test-After 2,000 Ib.carbon units-32.5 hours from start of test(immediately prior to termination of test).

Hagen Farm-Pumping Test-After 2,000 Ib.carbon units-32.5 hours from start of test(immediately prior to termination of test) -Duplicate,

TK/mpb[mpb-112-76]13452.80-MD

MADISONONE SCIENCE COURT

P.O. BOX 5385MADBON. Wl 5370$

mRZYN FAX (606) 23 1-4777

ANALYTICAL LABORATORY RESULTSWI LAB CERTIFICATION IDS: 113138300

Project: Hagen Farms

Location: Town of Dunkirk, Wisconsin

Project #: 13452.85Date Sampled: 11/30/90Ck'dijuJ App'd:Date Issued: lf/*«/?o

Lab No.Sample Description

ArsenicBariumCadmiumChromium, TotalIronLeadMagnesium \Mercury

2033-001HF-RW1

0.0740.46<0.0002<0.000225.2<0.00350.7<0.0002

Results are reported in mg/L. .

Method Reference: EPA-600, "Methods for Chemical Analysis of Water andWastes", March, 1984.


P.O. BOX 5585MADISON. Wl 53705

FAX <fiC8) 23 1-4777

ANALYTICAL LABORATORY RESULTSWI LAB CERTIFICATION ID#: 113138300



Project I: 13452.85Date Sampled: 11/30/90Ck'd:jw App'd:Date Issued:


Alkalinity, BicarbonateAlkalinity, TotalBiochemical Oxygen DemandChemical Oxygen DemandConductivity 0 25-C (umhos/cm)Nitrogen, Nitrate+NitritePhosphorus, TotalSolids, Total DissolvedSolids, Total Suspended

2023-001HF-RW1

6276272787

1140<0.10 (1)0.24

64742

Results are reported in mg/L unless otherwise stated.

(1) Elevated detection limit necessary to overcome interference.


mRZYN


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(608) W-4W7FAX C606) 23M777




Project I: 13452.85Date Sampled: 11/30/90Ck'd: jfiiXAppDate Issued:


Total Organic Carbon

2023-001HF-RW1

18

Results are reported in mg/L.


Method 415.1: Total Organic Carbon

IBSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO

Lab Name: COMPUCHEM.RTP__________

Lab Code: COMPU Case No.: 22001

Matrix: (soil/water) WATER

Sample wt/vol: 1000 (g/mL) ML

Level: (low/med) LOW

% Moisture: not dec. ___ dec. ___

Extraction: (SepF/Cont/Sonc) SEPF

GPC Cleanup: (Y/N) E_

Contract: 248901

SAS No.: _ _____

HF-RW1

SDG No.:

Lab Sample ID: 385139____

Lab File ID: GH085139A06

Date Received: 12/01/90

Date Extracted: 12/03/90

Date Analyzed: 3-2/10/90

Dilution Factor: 1.0____

CAS NO. COMPOUND'CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

108-95-2——————Phenol_________________111-44-4——————bis (2-Chloroethyl) Ether___95-57-8———————2-Chlorophe'nol ________541-73-1—————l;3-Dichlorobenzene______106-46-7—————1,4-Dichlorobenzene______100-51-6——————Benzyl Alcohol___________95-50-1———————1,2-Dichlorobenzene______95-48-7———————2-Methylphenol__________39638-32-9————bis(2-Chloroisopropyl)Ether106-44-5——————4-Methylphenol___________621-64-7——————N-Nitroso-Di-n-Propylamine__67-72-1——————Hexachloroethane_____'98-95-3———————Nitrobenzene____________78-59-1———————Isophorone____________•_88-75-5————————2-Nitrophenol____________105-67-9—————2,4-Dimethylphenol______65-85-0——————Benzoic Acid___________111-91-1——————bis(2-Chloroethoxy)Methane__120-83-2—————2,4-Dichlorophenol______120-82-1——————1,2,4-Trichlorobenzene____91-20-3———————Naphthalene______:______106-47-8—————4-Chloroaniline_________87-68-3———————Hexachlorobutadiene______59-50-7———————4-Chloro-3-Methylphenol___91-57-6———————2-Methylnaphthalene______77-47-4———————Hexachlorocyclopentadiene__88-06-2———————2,4,'6-Trichlorophenol_____95-95-4————————2,4,5-Trichlorophenol_____91-58-7———————2-Chloronaphthalene______88-74-4———————2-Nitroaniline__________131-11^-3——————Dimethyl Phthalate_______208-96-8——————Acenaphthylene___________606-20-2——————2,6-Dinitrotoluene_______

102010103101010101010101010103

1001010103101010101020201010101010

FORM I SV-1 1/87 Rev.

1CSEMIVOIATILE ORGANICS ANALYSIS DATA SHEET

Name: COMPUCHEM,RTP__________

EPA SAMPLE NO,

Code: COMPU Case No.: 22001

tetrix: (soil/water) WATER

Sample wt/vol: .000 (g/mL) ML

**evel: (low/med) LOW

t Moisture: not dec. ___ dec. ___

Sxtraction: (SepF/Cont/Sonc) ?EPF

5PC Cleanup: (Y/N) H_ pH: ___

Contract: 248901

SAS No.: _____

HF-RW1

SDG No.:


Lab File ID: GH085139A06

Date Received: 12701/90


Date Analyzed: 12/10/90


CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

99-09-2———————3-Nitroaniline_________83-32-9——————Acenaphthene___________51-28-5——————2,4-Dinitrophenol______100-02-7——————4-Nitrophenol__________132-64-9——————Dibenzofuran___________121-14-2——————2,4-Dinitrotoluene______84-66-2———————Diethylphthalate________7005-72-3—————4-Chlorophenyl-phenylether_86-73-7———————Fluorene______________"100-01-6—————4-Nitroaniline_________534-52-1——————4,6-Dinitro-2-Methylphenol_86-30-6——————N-Nitrosodiphenylamine (1),101-55-3—————4-Bromophenyl-phenylether_118-74-1——————Hexachlorobenzene_______87-86-5———————Pentachlorophenol_______85-01-8———————Phenanthrene___________120-12-7——————Anthracene_____________84-74-2———————Di-n-Butylphthalate_____206-44-0—————Fluoranthene__________129-00-0—————Pyrene_______________85-68-7———————Butylbenzylphthalate_____91-94-1——————3,3' -Dichlorobenzidine___56-55-3——————Benzo (a) Anthracene______218-01-9——————Chrysene_______________117-81-7——————bis (2-Ethylhexyl) Phthalate117-84-0——————Di^n-Octyl Phthalate____'_205-99-2——————Benzo'(b) Fluoranthene_____207-08-9——————Benzo(k)Fluoranthene_____50-32-8———————Benzo (a) Pyrene__________193-39-5——————Indeno (l, 2,3-cd) Pyrene___53-70-3———————Dibenz(a,h)Anthracene____191-24-2——————Benzo (g ,h, i) Perylene_____

2010401010101010101030101010201010101010101010101010101010101010

(1) - Cannot be separated from Diphenylamine

FORM I SV-2 1/87 Rev

SUMMARY OF ORGANIC QUALIFIER DEFINITIONS

Laboratory Qualifiers

U Tne_mater1al was analyzed for, but not detected.

J Indicates an estimated value. This flag 1s used either whenestimating a concentration for tentatively Identified compounds wherea 1:1 response 1s assumed, or when the quality control criteria arenot met.

B This flag 1s used when the analyte 1s found In the associated blank aswell as 1n the sample. It Indicates possible blank contamination andwarns the data user to take appropriate action. This flag must beused for a tentatively Identified compound as well as for a positivelyIdentified target compound.

C (For Pest1c1de/PCB data). The associated value was confirmed usingdual column verification.

E The compound was quantItated above the linear calibration range.

D The compound was quant Itated from an analysis at a secondary dilutionfactor.

X The associated value was quant Itated manually.

I The tentatively Identified compound Is an 1somer1c-type of thecompound reported.

C The tentatively identified compound refers to a class of compounds,

A The tentatively identified compound Is an aldol-type compound.

Data Validation Qualifiers

U The material was analyzed for, but was not detected. The associatednumerical value 1s the sample quantltatlon limit.

UJ The material was analyzed for, but was not detected. The associatednumerical value 1s an estimated quantity because quality controlcriteria were not met.

0 The associated numerical value 1s an estimated quantity.

R The data are unusable (compound may or may not be present).Resampling"and/or reanalysis 1s necessary for verification.

[jlv-601-11]

SUMMARY OF INORGANIC QUALIFIER DEFINITIONS

Laboratory Qualifiers

U The*material was analyzed for, but was not detected.

K The associated value was greater than or equal to the Instrumentdetection limit, but less than the contract required detection limit.

E Indicates the value reported 1s estimated due to the presence of anInterference.

M Duplicate Injection precision for furnace analyses was not met.

* Duplicate analysis 1s not within control limits.

+ Correlation coefficient for the MSA Is less than 0.995.

S The associated value was determined by the method of standardadditions.

N Indicates the spike sample recovery Is not within control limits.

W Post-digestion spike for Furnace AA analysis 1s out of control limits(85-115X), while sample absorbance Is less than 50X of the spikeabsorbance.

Data Validation Qualifiers

U The material was analyzed for, but was not detected above the level ofthe associated value. The associated value 1s either the samplequantltatlon limit or the sample detection limit.

UJ Sample was analyzed, but not detected. The associated value 1s anestimated quantity because quality control criteria were not met.

R The data are unusable (compound may or may not be present).Resampling and/or reanalysls 1s necessary for verification.

J The associated numerical value Is an estimated quantity becausequality control criteria were not met.

[jlv-601-11]


P.O. BOX 5385MAD CON, WI 53705

FAX(608)23M777

Volatile Organic Compound ResultsWI Lab Certification IDS: 113138300Project: Hagen FarmsLocation: Town of Dunkirk, WisconsinCi: 13452.85

Page * Of %Ck*d:jwJ App'dDate

Compound

ReportableDetectionLimit(UG/L)

2024-001(1)HF-RW111/30/90

Benzene°romodichloromethaneomoform

BromomethaneCarbon TetrachlorideChlorobenzeneChlorodibromomethaneChloroethane2-Chloroethylvinyl Ether1.2-Dichlorobenzene1.3-Di chlorobenzene1.4-Di chlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroetheneci s-1,2-Di chloroethenetrans-1.2-Dichloroethene1.2-Dicnloropropanecis-l,3-Dich1oropropenetrans-1,3-Di chloropropeneV,hy1 Benzene

Siethylene Chloride1,1,2,2-Tetrachloroeth aneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenesMethyl Ethyl Ketone (MEK)Methyl Isobutyl Ketone (MIBK)TetrahydrofuranStyrene *"° ,

20020010001000200200200600500020020020020020060060060020020020020010002002002002002005000600600600

400020004000200

XXXXXXXXXXXXXXXXXXXX1250XXXXXXXXX11300

XX14100X


P.O. BOX 5385MADISON. WI 53705

C6C8) HI-4747FAXCfiC6)23M7T7

Volatile Organic Compound ResultsWI Lab Certification ID*: 113138300Project: Hagen FarmsLocation: Town of Dunkirk, WisconsinCf: 13452.85

Page Of "**Date Issued:

X * Analyzed, but not detected.(1) Sample chromatogram contains unidentified compounds.Method Reference: SW846, "Test Methods for Evaluating Solid

Waste", September, 1986. Methods 8010and 8020 with modifications. •


P.O. BOX 5385MADISON, Wl 53705

ANALYTICAL LABORATORY RESULTSWI LAB CERTIFICATION ID#: 113138300

Project: Hagen Farms Project #: 13452.85Date Sampled: 12/12/90

Location: Town of Dunkirk, Wisconsin Ck'd:<na ApDate Issued:

Lab No. 2093-001Sample Step Test AfterDescription ISOOOff CU

Arsenic 0.041Barium 0.02Cadmium <0.0002Chromium, Total 0.0005Lead <0.003Mercury <0.0002

Results are reported in ntg/L.


mRZYN


P.O. BOX 5385MADISON, VI »705

<&» 231-4747FAX (606) 231-4777

Volatile Organic Compound ResultsWI Lab Certification IDS: 113138300Project: Hagen Farm SiteLocation: Dunkirk, WisconsinC#: 13452.85

Compound

BenzeneBromodi chloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzene .ChlorodibfomomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1, 2-Di chlorobenzene1.3-Dichlorobenzene1.4-Dichlbrobenzene1.1-Dichlproethane1.2-Dichloroethane1.1-Dichloroethenecis-l,2-Dichloroethenetrans-l,2-Dichloroethene1.2-Dichloropropanecis-l,3-D1chloropropenetrans-l,3-DichloropropeneEthyl BenzeneMetnylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-TrichloroethaneTrjchloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenes -*StyreneMethyl ethyl ketoneMethyl isobutyl ketoneTetrahydrofuranX • Analyzed, but not detected.

Page » Of >Ck?d:JU^App'dDate Issued: i/3/9l

ReportableDetectionLimit(ug/D

1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.003.0010.010.010.010.0

2093-001Step TestAfter15000? CU12/13/90

XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX,xXXXXX

2093-002TripBlank12/12/90

XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX

Method Reference: SW846, "Test Methods for Evaluating Solid Waste ,September, 1986. Methods 8010 and 8020with modifications.

IXORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: COMPUCHEM,RTP__________

Lab Code: COMPU Case No.: 22145

Matrix: (soil/water) WATER

Sample wt/vol: 1000 (g/mL) ML

Level: (low/med) LOW

% Moisture: _____ decanted: (Y/N) N

Concentrated Extract Volume: 1000(ul)

Injection Volume: l.Ofull

G^_ Cleanup: (Y/N) N pH:

CAS NO. COMPOUND

Contract: 248901

SAS No.: _____

2093-001

SDG No.:


Lab File ID: GJ089062B06

Date Received: 1-2/17/90


Date Analyzed: 12/21/90


CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

108-95-2 ————111-44-4 ————oe:_e;"7_o__. _ __

541-73-1 ————106-46-7 ————

95-50-1 —————95-48-7 —————1QtZ.tO *>*) Q _JSoJo— J^ y— ——106-44-5 ————f ^ ^ ^ * ^621—64—7 ————o/ /î— JL— — —yo— yo— j— — ~" — •—78-59-1 —————oo— /D— o— — • — —105-67-9 ————65-85-0 —————111-91-1 ————

01-20—3 —————^ **- «* w w

106-47-8 ————a*? /;o ô / oo— J— — — — —59-50-7 —————91-57-6 —————^^ A » Jl.77-47-4 —————

95-95-4 —————on RO—-; — __88-74-4 —————131-11-3 ————

606-20-2 ————

—— Phenol—— bis (2-Chloroethyl) Ether—— 2-Chlorophenol

f O UJL^llÛJtUUCilACSilC

t -» <^^^>J.lXVJ J. UUC»l4C<dlIS

—— Benzyl Alcohol—— 1 , 2-Dichlorobenzene—— 2 -Methylphenol—— bis (2-Chloroisopropyl) Ether _—— 4 -Methylphenol—— N-Nitroso-Di-n-Propylamine __—— Hexachloroethane

Al J* 1— J. UJJUildiVvAiC

—— Isophorone—— 2 -Nitrophenol—— 2 , 4-Dimethylphenol

j?uiii£iuxv nv»xu—— bis ( 2 -Chloroethoxy) Methane __—— 2 , 4-Dichlorophenol

f £ / ** Ai. ^>IlXOJtwJJ6Il£cllQ

—— Naphthalene—— 4-Chloroaniline—— Hexachlorobutadiene—— 4-Chloro-3-Methylphenol—— 2-Methylnaphthalene—— Hcxachlorocyclopentadiene—— 2 , 4 ', 6-Trichlorophenol—— 2 , 4 , 5-Trichlorophenol—— 2-Chloronaphthalene—— 2-Nitroaniline—— Dimethyl Phthalate

«ii->»-.4nj[-m <»ii_y ûiif^—— 2 , 6-Dinitrotoluene

. 6201010101010101010101010101010

10010101010101010101020201010101010

Juuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

FORM I X-l 3/90

99-09-2———————3-Nitroaniline83-32-9———————Acenaphthene51-28-5———————2,4-Dinitrophenol100-02-7———'——4-Nitrophenol132-64-9——————Dibenzofuran121-14-2——————2,4-Dinitrotoluene84-66-2———————Diethylphthalate7005-72-3—————4-Chlorophenyl-phenylether86-73-7———'————Fluorene100-01-6——————4-Nitroaniline534-52-1——————4,6-Dinitro-2-Methylphenol86-30-6———————N-Nitrosodiphenylamine (1)101-55-3——————4-Bromophenyl-phenylether118-74-1——————Hexachlorobenzene87-86-5———————Pentachlorophenol85-01-8———————Phenanthrene120-12-7——————Anthracene84-74-2———————Di-n-Butylphthalate206-44-0——————Fluoranthene129-00-0——————Pyrene85-68-7———————Butylbenzylphthalate91-94-1———————3,3'-Dichlorobenzidine56-55-3———————Benzo( a) Anthracene218-01-9——————Chrysene117-81-7——————bis (2-Ethylhexyl) Phthalate117-84-0——————Di-n-Octyl Phthalate205-99-2——————Benzo(b) Fluoranthene207-08-9——————Benzo (k) Fluoranthene50-32-8———————Benzo (a) Pyrene193-39-5——————Indeno (1,2,3-cd) Pyrene53-70-3———————Dibenz(a,h)Anthracene191-24-2——————Benzo(g,h,i)Perylene

20104010101010101010301010-10 '201010101010101010101010io1010101010

uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

FORM I X-2 3/90

METHOD REFERENCE

To determine the concentration of Semi-Volatile organic compounds in aqueousmatrix CompuChem employs the methods as outlined in SW-846 for sample preparation(Method 3S10) and analysis (Method 8270). These methods are approved forobtaining data to satisfy the requirement of 40CFR part 261, Identification andListing of Hazardous Waste.

METHOD SUMMARY

Surrogates are added to an aliquot (usually 1-liter) of aqueous sample. The sampleIs extracted at a pH of greater than 11 and then at a pH of less than 2 using aseparatory funnel. The solvent used is methylene chloride. The extracts are driedand concentrated for analysis.

Analysis is performed by separation of the components by gas chromatographyfollowed by qualitative and quantitative identification by mass spectrometry usinginternal standard technique.



(606) 23I.-4747FAX C6C6) 2JM777

Volatile Organic Compound ResultsWI Lab Certification IDS: 113138300Project: Hagen Farm RI/FSLocation: Town of Dunkirk, WisconsinC#: 13452.85

Page 1 Of *Ck?d:$WApp'dDate Issued:

Compound

ReportableDetectionLimit

2099-001(1}HF-PTBT-3.5Q12/14/90

BenzeneBromod1chloromethaneBromoformBromomethaneCarbon TetrachlorldeChlorobenzeneChlorodlbromomethaneChloroethane2-Chloroethylvlnyl EtherChloroformChloromethane1.2-D1chlorobenzene1.3-D1chlorobenzene1.4-Dlchlorobenzene1.1-D1ch1oroethane1.2-D1chloroethane1.1-D1chloroethene .cis-lt2-D1chloroethenetrans-l,2-D1chloroethene1.2-D1cnloropropanec1s-l,3-D1chloropropenetrans-l,3-D1chloropropeneEthyl BenzeneMetnylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trlchloroethane1.1.2-TrlchloroethaneTrlchloroetheneTrlchlorofluoromethaneVinyl ChlorideXylenes

1001001001001001001001001000100100100100100100100100100100100100100100500100100100100100100100100300

XXXXXXXXXXXXXXXXXXXXXX668XXXXXXXXX

8130

Tetrahydrofuran 5000 11800

mRZYN


P.O. BOX 5585MADISON, v\ SJTOS

<6C8) 231-4747FAX (608)231-4777

Volatile Organic Compound ResultsWI Lab Certification IDS: 113138300Project: Hagen Farm RI/FSLocation: Town of Dunkirk, Wisconsin«: 13452.85

PageCkfd:Date Issued

(1) Sample chromatogram contains unidentified compounds.X - analyzed, but not detected.

Method reference: SW846, "Test Methods for Evaluating SolidWaste", September, 1986. Methods 8010and 8020 with modifications.

WiRZYN


P.O. BOX 5385MADISON, wi 53705

FAX (608) Z3M777

Volatile Organic~Compound ResultsWI Lab Certification IDS: 113138300Project: Hagen Farm SiteLocation: Town of Dunkirk, WisconsinCf: 13452.85

Paqe 1 Of1*Ck d:jw App'dDate Issued:.iJ

Compound

ReportableDetectionLimit(ug/L)

2104-001HF-PTBT-0.112/14/90

BenzeneBromochloromethaneBromodi chloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethanel,2-Dibromo-3-Chloropropane1, 2-D1chlorobenzene1.3-Dichlorobenzene1.4-Di chlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroetheneci s-1,2-Di chloroethenetrans-l,2-Dichloroethene1.2-Dicnloropropaneci s-1,3-Dichioropropenetrans-l,3-Dich1oropropeneEthyl BenzeneMethylene Chloride1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trichloroethane1.1.2-Trichloroethane ;;Trichloroethene •Tri chlorof1uoromethaneVinyl ChlorideXylenesStyrene yMethyl ethyl ketone (MEK)Methyl isobutyl ketone (MIBK)Tetrahydrofuran

250250250250250•25025025025025002502505002502502502502502502502502502502502501250250250250250250250250250250750

250625025002500

XXXXXXXXXXXXXXXXXXXXXXXX958XXXXXX3CXXX

11100

XXX

14900


P.O. BOX 5565MADISON, WI 53705

(6C8) 2JM747FAX <60B)2J 1-4777

Volatile Organic"Compound ResultsWI Lab Certification ID#: 113138300Project: Hagen Farm SiteLocation: Town of Dunkirk, WisconsinC#: 13452.85

Page * Of bCkfd:.*Date Issued

Compound

BenzeneBromodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodibromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-Di chlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-1,2-Dichloroethenetrans-l,2-Dichloroethene1.2-Dichloropropanecis-l,3-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trichloroethane1.1.2-TrichloroethaneTrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenesStyreneMethyl ethyl ketone (MEK)Methyl isobutyl ketone (MIBK)Tetrahydroftiran


SO,SO,SO,5050.50,50,50.050050.050,50,50,50.50.50.50,50.50,50,50,50.50.025050.050.050,50.50.50,50,50.01500

5001250050005000

2104-002HF-PTBT-1.012/14/90

XXXXXXXXXXXXXXXXXXXXXX

1020XXXXXXXXX

10500

XXX

14300

2104-003HF-PTBT-5.N12/14/90

XXXXXX 'XXXXXXXXXXXXXXXX778XXXXXXXXX

8220

XXX

12000

mRZYN


P.O. BOX 5J85MADISON. Wl 53705

FAX C6C6) Z3M777

Volatile Organic Compound ResultsWI Lab Certification IDS: 113138300Project: Hagen Farm SiteLocation: Town of Dunkirk, WisconsinC*: 13452.85

Page 3 Of <•Ck*d:jw ApDate Issued

Compound

ienzeneBromodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorod i bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-Dichlorobenzene1.3-Di chlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-1,2-Dichloroethenetrans-1,2-DichloroetheneJ,2-Dichloropropanecis-l,3-Dichioropropenetrans-l,3-DichloropropeneEthyl BenzeneMetnylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1,1,1-Tri chloroethane

" 1,1,2-Tri chloroethaneTrichloroetheneTrichlorofluoromethaneVinyl ChlorideXylenesStyreneMethyl ethyl ketone (HEK)Methyl isobutyl ketone (MIBK)Tetrahydrofuran


50.050.050,50.50,50.50,50.050050.050,50,50.50.50,50,50,50.50,50,50,50.50.025050.050.050,50,50,50,50.50.1500

5001250050005000

2104-004HF-PTBT-10N12/14/90

X.XXXXXXXXXXXXXXXXXXXXX

683XXXXXXXXX

7450

XXX

11200

2104-005HF-PTBT-5NDUP12/14/90WKMCHKV


844XXXXXXXXX

9020

XXX

12500

WJRZYN



CfiOU 251-4747FAX<6CB)23M777

Volatile Organic Compound ResultsWI Lab Certification IDS: 113138300Project: Hagen Farm SiteLocation: Town of Dunkirk, WisconsinC#: 13452.85

e i Ofd:;rvxJ

Date Issued

Compound

BenzeneBromochloromethaneBromodi chloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodibromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethanel,2-Dibromo-3-Chlorqpropane1.2-Di chlorobenzene1.3-Dichlorobenzene1,4 -Di chlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-l,2-Dichloroethenetrans-l,2-Dichlorbethene1.2-Di chloropropanecis-l,3-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMetnylene Chloride1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethanetetrachloroetheneToluene1.1.1-Trichloroethane1.1.2-Trichloroethane •'** .TrichloroetheneTrichlorofluoromethaneVinyl ChlorideXylenes

'•*StyreneMethyl ethyl ketone (MEK)Methyl isobutyl ketone (MIBK)Tetrahydrofuran


1.001.001.001.001.001.001.001.001.0010.01.001,002.001.001*001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.00.1.001.001.004.001.0025.010.010.0

2104-006HF-PTBT-5FB12/14/90

XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX

mRZYN

MADISONONE SCIENCE COL'RT

P.O. BOX 5565MADISON, vi SJTCJ

<6C8) 231-4747FAX (608) Z3M777

Volatile Organic Compound ResultsWI Lab Certification ID?: 113138300Project: Hagen Farm SiteLocation: Town of Dunkirk, WisconsinC#: 13452,85

Page f OfCk d:^»«^>Date Issued: h-J-

Compound


2104-007TRIPBLANK12/12/90

BenzeneBromochloromethaneBromodi chloromethaneBromoformBromomethaneCarbon Tetrachl'orideChlorobenzeneChlorodibromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethanel,2-Dibromo-3-ChToropropane1.2-01Chlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Di chloroethane1.2-Dichloroethane1.1-Dichloroethenecis-1,2-Dichloroethenetrans-l,2-Dichloroethene1.2-Dicnloropropanecis-l.S-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,1,2-Tetrachloroethane1,1,2,2-Tetrachl oroethaneTetrachloroetheneToluene1.1.1-Trichloroethane .,1.1.2-Trichloroethane "s /TrichloroetheneTrichlorofluoromethaneVinyl ChlorideXylenes

^StyreneMethyl ethyl ketorie (MEK)Methyl isobutyl ketone (MIBK)Tetrahydrofuran

1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003.00

1.0025.010.010.0

XXXX.XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX

MADISONONE SCIENCH CO CRT

P.O. BOX 5355MADISON. >T1 53705

<6C8> 231-4W7FAX (606) 2JM 777

Volatile Organic Compound ResultsWI Lab Certification ID?: 113138300Project: Hagen Farm SiteLocation: Town of Dunkirk, WisconsinCl: 13452.85

Page t Of 6Ck'dyw*7 App'd:Date Issued:jt/z«

X - analyzed, but not detected.

Method reference: SW846. "Test Methods for Evaluating SolidWaste*, September, 1986. Methods 8010and 8020 with modifications.

WJRZYNONE SCIENCE COURT"

P.O. BOX 5365MADISON. VI 53705

FAXC606)23M7J7

Volatile Organic Compound Results Page I Of3

VI Lab Certification ID?: 113138300 Ck7d:^WAp|Project: Hagen Farm RI/FS Date IssuedLocation: Town of Dunkirk, WisconsinC#: 13452.85

Compound


2100-001 2100-002HF-PTA15 HF-PTA2-25Q -25Q12/15/90 12/15/90

BenzeneBromodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1»2-Di chlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroetheneci s-1,2-Dichloroethenetrans-l,2-Dichloroethene1.2-Dicnloropropanecis-l,3-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMetnylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneTo!uene1.1.1-Tri chloroethane1.1.2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl ChlorideXylenes

1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.003.00


1.89XXXXXXXXX

12 .8

XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX

Tetrahydrofuran 10.0 101

WARZYNONE SCIENCE COURT

P.O. BOX 5i85MADISON. Wl 53XJ5

«C6) 231-4747FAX C6C8) 231-4777

Volatile Organic .Compound Results Page *• Of3

VI Lab Certification IDS: 113138300 Ck7d:*WAp|Project: Hagen Farm RI/FS Date Issued:Location: Town of Dunkirk, WisconsinC#: 13452.85

Compound


2100-003HF-PTTRIPBLANK12/15/90

BromodlchloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-Dichlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-01chloroethane1.2-Dichloroethane1.1-Di chloroethenecis-1,2-Dichloroethenetrans-1.2-Dichloroethene1.2-Dichloropropanecis-l,3-Dichloropropenetrans-1,3-PichloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneTo!uene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenes

1.001.001.001.001.001.00•1.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.003.00


Tetrahydrofuran 10.0

WARZYNONE SCIENCE COURT

P.O. BOX 5J85MADISON, wi 33705

<606> 23M747F4X<fi08>23M777

Volatile Organic-Compound ResultsWI Lab Certification IDS: 113138300Project: Hagen Farm RI/FSLocation: Town of Dunkirk, WisconsinCS: 13452.85

e 2> Ofd: vJ

Date Issued

X'- analyzed, but not detected.

Method reference: SW846. "Test Methods for Evaluating SolidWasteV September, 1986. Methods §010and 8020 with modifications.


P.O. BOX 5385MADISON, Wl 53705

(608) 231 -4747FAX (&»> Z51-4777




Project f: 13452.85Date Sampled: 12/15/90Ck'dr'-wj App'd:Date Issued:


ArsenicBariumCadmiumChromium, TotalLeadMercury

2103-001HF-PTBT-25N

0.0510.26<0.00020.0004<0.003<0.0002

2103-002HF-PTA2-25N

0.0150.18<0.00020.0002<0.003<0.0002

Results are reported in mg/L.


WiRZYN



(6C8) 23M747FAX (60B) 251-4777

Volatile Organic Compound ResultsWI Lab Certification ID*: 113138300Project: Hagen Farm SiteLocation: Town of Dunkirk, WisconsinC#: 13452.85

Page ' Of /Ck7d:^W App'd:Date Issued:i/3/<)l

Compound


2103-001HF-PTBT-25N12/15/90

BenzeneBromodi chloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-Di chlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroetheneci s-1,2-Di chloroethenetrans-l,2-Dichloroethene1.2-Dichloropropanecis-l,3-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneTo!uene1.1.1-Tri chloroethane1.1.2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl ChlorideXylenesMethyl Ethyl Ketone (MEK)Methyl isobutyl Ketone (MIBK)Styrene.TetrahydrdTuran

50.050.050.050.050.050.050.050.050050.050.050.050.050.050.050.050.050.050.050.050.050.050.025050.050.050.050.050.050.050.050.01500

125050050.05000

XXXXXXXXXXXXXXXXXXXXXX449XXXXXXXXX5780

XXX7780


P.O. BOX 5585MADISON, Tl 53705

(600 231.4747FAX (60S) 231-4777

Volatile Organic Compound ResultsVI Lab Certification I0#: 113138300Project: Hagen Farm SiteLocation: Town of Dunkirk, WisconsinC#: 13452.85

Page * OfCk*d:Date Issued: i/s/<ii

Compound


2103-002HF-PTA2-25N12/15/90

BenzeneBromodichloromethaneBromoformBromomethaneCarbon TetrachlorldeChlorobenzeneChlorodlbromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-01chlorobenzene1.3-01chlorobenzene1.4-Di chlorobenzene1.1-Dlchloroethane1.2-Dlchloroethane1.1-01chloroetheneds-l,2-D1chl oroethenetrans-l,2-D1chloroethene1.2-Dlcnloropropanec1s-l,3-D1chloropropenetrans-l,3-D1chloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trlchloroethane1.1.2-TrlchloroethaneTrlchloroetheneTr1chlorof1uoromethaneVinyl Chloride " tXylenesMethyl Ethyl Ketone (MEK)Methyl Isobutyl Ketone (MIBK)Styrene ^Tetrahydrofuran

1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001,001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.004.00

25.010.01.0020.0


XXXX

HAD [SONONE SCIENCE COURT

P.O. BOX 5385MADISON, VI 53TO5

(606) 2J1-4747FAX (606) 231-4777

Volatile Organic Compound Results Page3 Of/WI Lab Certification IDS: 113138300 Ckrd:**/APIProject: Hagen Farm Site Date IssuedLocation: Town of Dunkirk, WisconsinC#: 13452.85

Compound


2103-003HF-PTA15-25N12/15/90

BenzeneBromodichloromethaneBromoformBromomethaneCarbon TetrachlorldeChlorobenzeneChlorodlbromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane *1.2-D1chlorobenzene1.3-Dlchlorobenzene1.4-D1chlorobenzene1.1-01chloroethane1.2-D1chloroethane1.1-D1chloroethenecis-l,2-D1chloroethenetrans-1,2-D1chloroethene1.2-D1chloropropanecis-l",3-D1chloropropenetrans-l,3-D1chloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tr1chloroethaneTrlchloroetheneTrlchlorofluoromethane.sVinyl Chloride "^ /XylenesMethyl Ethyl Ketone (MEK)Methyl Isobutyl Ketone (MIBK)Styrene ,Tetrahydrofuran

00000000

1.001.001.001.0010,01.001.001.001.001.001.00.00.00.00

1111.001.001.001.001.005.001.001.001.001.001.001.001,001,003.00

25.010.01.0050.0

XXXXXXXXXXXXXXXXXXXXXX1.37XXXXXXX

- XX13.6

XXX87.6



(608) 251-4747FAX (608) 731-4777

Volatile Organic Compound Results Page 4 Of/VI Lab Certification ID#: 113138300 CkTd:ju*.Project: Hagen Farm Site Date IssuedLocation: Town of Dunkirk, Wisconsin«: 13452.85

Compound

BenzeneBromodi chlorometh aneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-D1chlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-l,2-Dichloroethenetrans-K2-Dichl oroethene1.2-Dicnloropropanecis-l,3-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethanetetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTrichlorof1uoromethaneVinyl Chloride -v ,,XylenesMethyl Ethyl Ketone (MEK)Methyl isobutyl Ketone (HIBK)StyreneTetrahydrofuran


1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.003.00

25.010.01.0010.0

2103-004TRIP BLANK12/12/90


WARZYN


P.O. BOX 5385MADISON, \ffl 53705

FAX(608)23M777

Volatile Organic Compound ResultsWI Lab Certification IDS: 113138300Project: Hagen Farm SiteLocation: Town of Dunkirk, WisconsinC#: 13452.85

PageCkrd:Date Issued

X - Analyzed, but not detected.

Method Reference: SW846. "Test Methods for Evaluating SolidWaste'1, September, 1986. Methods 8010and 8020 with modifications.


P.O. BOX 5365MADBON, wi 55705

FAX (6C6) ZJM777

Volatile Organic Compound ResultsWI Lab Certification ID#: 113138300Project: Hagen Farm RI/FSLocation: Town of Dunkirk, WisconsinCl: 13452.85

Page J OfCk'd ^Date Issued:i*/

Compound


2117-001HF-PTBT-32 512/i5/90

BenzeneBromodi chloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-Dichlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-1,2-D1chloroethenetrans-1.2-Dichloroethene1.2-Di cnloropropanecis-l,3-Dichloropropenetrans-l,3-D1chloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenes ** ;StyreneMethyl ethyl ketone (MEK)Methyl isobutyl ketone (MIBK)Tetrahydr^furan

25025025025025025025025025002502502502502502502502502502502502502502501250250250250250250250250250750

250625025002500


412XXXXXXXXX

4850

XXX

7840

MADISONONE SCIENCE COURTP.O. BOX 5385

MADISON. Wl «?05<6C8) 231 •4747

FAX (608)231-4777

Volatile Organic Compound ResultsWI Lab Certification IDS: 113138300Project: Hagen Farm RI/FSLocation: Town of Dunkirk, WisconsinCf: 13452.85

Page * OfCk*d:Date Issued

Compound

BenzeneBromodi chloromethaneBromoformBromomethaneCarbon TetrachlorldeChlorobenzeneChlorodlbromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-D1chlorobenzene1.3-D1chlorobenzene1.4-Dlchlorobenzene1.1-Dichloroethane1.2-Dichloroethaneltl-D1chloroethenewcis-l,2-Dichloroethenetrans-l;2-D1chloroethene112-Di cnloropropanecis-l,3-D1chloropropenetrans-l»3-DichloropropeneEthyl BenzeneMetnylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trlchloroethane1.1.2-TrlchloroethaneTrichloroethene

, Tr1chlorofluoromethane"~V1nyl ChlorideXylenesStyreneMethyl ethyl ketone (MEK)Methyl isobutyl ketone (MIBK)Tetrahydrofuran


1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.003.00

1.0025.010.010.0

2117-002HF-PTA15-32.512/15/90

XXXXXXXXXXXXXXXX 'XXXXXX1.45XXXXXXXXX15.7

XXX

100


P.O. BOX 5J65MADISON, vi 53705

<6C8) 25M7"FAX (6C8) 25M777

Volatile Organic Compound ResultsWI Lab Certification IDS: 113138300Project: Hagen Farm RI/FSLocation: Town of Dunkirk, WisconsinC#: 13452.85

Page 3Ck*d:Date Issued

Compound

BenzeneBromodi chloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1»2-Di chlorobenzene1.3-Di chlorobenzene1.4-Dichlorobenzene1.1-D1chloroethane1.2-Dichloroethane1.1-Dichloroethenecl s-1,2-Dichloroethenetrans-1,2-D1chloroethene1.2-Dichloropropanecis-l,3-Dichloropropenetrans-1,3-DichloropropeneEthyl BenzeneMetnylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTrichlorofluoromethaneVinyl ChlorideXylenes "* ,•StyreneMethyl ethyl ketone (MEK)Methyl isobutyl ketone (MIBK)Tetrahydrofuran


1,001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.004.00

1.0025.010.010.0

2117-003 2117-004HF-PTA2 HF-PTA2-32.5 -32.5 DUP12/15/90 12/15/90

XXXXXXXX

•XXXXXXXXXXXXXXXXXXXXXXXXX

XXXX


XXXX



<6C8) »M747FAX C6C8) »I-4777

Volatile Organic Compound ResultsWI Lab Certification ID*: 113138300Project: Hagen Farm RI/FSLocation: Town of Dunkirk, WisconsinC#: 13452.85

^ OfCk7d:aWApp'Date Issued:

Compound

BenzeneBromodi chloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-Dichlorobenzene1.3-Di chlorobenzene1.4-D1chlorobenzene1.1-Dlchloroethane1.2-D1chloroethane1.1-Dichloroethenecis-1,2-D1chloroethenetrans-1.2-Di chloroethene1.2-Dicnloropropanecls-1,3-Di chloropropenetrans-l,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trichloroethane1.1.2-Tr1chloroethaneTr'i chl oroetheneTrichlorofluoromethaneVinyl ChlorideXylenes '* •StyreneMethyl ethyl ketone (MEK)Methyl isobutyl ketone (MIBK)Tetrahydro/uran


1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.003.00

1.0025.010.010.0

2117-005TRIPBLANK12/15/90



P.O. BOX 5J85MADISON, wi 53705

(ffiS) 231-<7<7FAX<6CB)23M777

Volatile Organic Compound ResultsWI Lab Certification ID#: 113138300Project: Hagen Farm RI/FS Date Issued:Location: Town of Dunkirk, WisconsinCf: 13452.85


Method reference: SW846, "Test Methods for Evaluating SolidWaste*, September, 1986. Methods 8010and 8020 with modifications.

Explanation of Sample Descriptionsfor the Contaminant Characterization Investigation

Water Quality Results

Description

HF-GWDTB01-22HF-GWDTB01-91HF-GWDTB01-37HF-GWDTB01-57HF-GWDTB01-79HF-GWDTB01-97HF-GWDTB01-117HF-GWDTB01-137

HF-GWDTB02-27HF-GWDTB02-37HF-GWDTB02-57HF-GWDTB02-74HF-GWDTB02-78HF-GWOTB02-94HF-GWDTB02-97HF-TB01HF-FB01

HF-GWOTB03-27HF-GWDTB03-47HF-GWDTB03-67HF-GWDTB03-87HF-GWOTB03-92HF-GWDTB03-107HF-GWDTB03-127HF-GWDTB03-147HF-FB02HF-FB03HF-TB02

HF-GWDTB04-47HF-GWOTB04-60HF-GWDTB04-75HF-GWDTB04-92HF-GWDTB04-104HF-GWOTB04-122HF-GWOTB04-134HF-GWDTB04-93HF-TB04

Explanation

HagenHagenHagenHagenHagenHagenHagenHagen

HagenHagenHagenHagenHagenHagenHagenHagenHagen

HagenHagenHagenHagenHagenHagenHagenHagenHagenHagenHagen

HagenHagenHagenHagenHagenHagenHagenHagenUagen

FarmFarmFarmFarmFarmFarmFarmFarm

FarmFarmFarmFarmFarmFarmFarmFarmFarm

FarmFarmFarmFarmFarmFarmFarmFarmFarmFarmFarm

FarmFarmFarmFarmFarmFarmFarmFarmFarm

- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater

- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater

.-------

-------

TestTestTestTestTestTestTestTest

TestTestTestTestTestTestTest

BoringBoringBoringBoringBoringBoringBoringBoring

BoringBoringBoringBoringBoringBoringBoring

11tlflfl11fl1111

1212121212#212

- 22- 22- 37- 57- 79- 97- 117

feetfeetfeetfeetfeetfeet

Duplicate

feet- 137 feet

- 27- 37- 57- 74- 78- 94- 97

feetfeetfeetfeetfeetfeetfeet

- Trip Blank 11- Field Blank

- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Field Blank- Field Blank

11--------



1313131313131313

- 27- 47- 67- 87- 87- 107- 127- 147

feetfeetfeetfeetfeetfeetfeetfeet

Duplicate

1213

- Trip Blank 12

- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater

--------



141414#414#414#4

- 47- 60- 75- 92- 104- 122- 134- 134

feetfeetfeetfeetfeetfeetfeetfeet Duplicate

- Trip Blank #4

[sss-101-98b]

WJRZYN

MADISONONE SCIENCr COLUT

P.O. BOX 53S5MADISON, wi 53705

<6C8) 2)1-47X7FAXC6C8)23M777

VOLATILE ORGANIC COMPOUND RESULTSWI LAB CERTIFICATION IDS: 113138300PROJECT: HAGEN FARM RIFSLOCATION: STOUGHTON, WISCONSINC#: 13452.89

PAGE 1 OF *CK'D^wJAPP'D:DATE ISSUED:*!*

COMPOUND

REPORTABLEDETECTIONLIMIT

1946-001 1946-002HF-GWDTB01-22 HF-GWDTB01-9111/12/90 11/12/90

BENZENEBROMOCHLOROMETHANEBROMODICHLOROMETHANEBROMOFORMBROMOMETHANECARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANEl,2-DIBROMO-3-CHLOROPROPANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE,1,1-DICHLOROETHANE1,2-DICHLOROETHANE1.1-DICHLOROETHENECIS-1,2-DICHLOROETHENETRANS-1.2-DICHLOROETHENE1.2-DICHLOROPROPANECIS-1,3-DICHLOROPROPENETPANS-1,3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1,2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE .,1.1.2-TRICHLOROETHANE '* .TRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENES

1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.00'1.001.001.003.00

XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX

BMQL

XXXXXXXXXXXXXXXXXXXXXXXXXXXX•XXXXXXX

BMQL

TETRAHYDROFURAN 20.0

mRZYN

MADISONONE SCIENCE COIKT

P.O. BOX 5J65MADISON. Wl 53705

<6C81 251-4747FAX (6C8) 251-4777

VOUTILE. ORGANIC COMPOUND RESULTSWI LAB CERTIFICATION ID?: 113138300PROJECT: HAGEN FARM RIFSLOCATION: STOUGHTON, WISCONSIN«: 13452.89

PAGECK'DDATE ISSUED

IMPOUND

BENZENEBROMOCHLOROMETHANEBROMODICHLOROMETHANEBROMOFORMBROMOMETHANE

. CARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DIBROMO-3-CHLOROPROPANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE

^4,1-DICHLOROETHANE1,2-DICHLOROETHANE1.1-DICHLOROETHENECIS-1,2-DICHLOROETHENETRANS-1.2-DICHLOROETHENE1.2-DICHLOROPROPANE

. CIS-1.3-DICHLOROPROPENETRANS-1,3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1,2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE .v1.1.2-TRICHLOROETHANETRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENES

REPORTABLEDETECTIONLIMIT(UG/L)

1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003.00

1946-003HF-GWDTB01-3711/12/90


MADISONONE SCIENCE COU'XT


<6C8> 231-4747FAX C6C8) 231-4777

VOLATILE ORGANIC COMPOUND RESULTSWI LAB CERTIFICATION ID*: 113138300PROJECT: HAGEN FARM RIFSLOCATION: STOUGHTON, WISCONSINCl: 13452.89

PAGE 3 OF JCK'D: APP'DDATE ISSUED:

BMQL - DETECTED, VALUE BELOW METHOD QUANTITATION LIMIT.X - ANALYZED, BUT NOT DETECTED.

,ETHOD REFERENCE: SW846, "TEST METHODS FOR EVALUATING SOLIDWASTE", SEPTEMBER, 1986. METHODS 8010AND 8020 WITH MODIFICATIONS.

WARZYN'

MADISONONE SOENCZ COCST


<6C8> 231-4747FAXC6CB)23M777

VOLATILE ORGANIC XOMPOUND RESULTS PAGE 1 OF £WI LAB CERTIFICATION IDS: 113138300 CK'D:*wJAPIPROJECT: HAGEN FARM RIFS DATE ISSUED:LOCATION: STOUGHTON, WISCONSINC#: 13452.89

•OMPOUNO


1952-001HF-GWDTB01-5711/13/90

BENZENEBROHOCHLOROHETHANEBROHODICHLOROMETHANEBROMOFORM -BROHOMETHANE .CARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DIBROMO-3-CHLOROPROPANE1.2-DICHLOROBENZENE1.3-DICHLORQBENZENE1.4-DICHLOROBENZENE

v >,1-DICHLOROETHANEM.2-DICHLOROETHANE

1.1-DICHLOROETHENECIS-1,2-DICHLOROETHENETRANS-1,2-DICHLOROETHENE1.2-DICHLOROPROPANECIS-1,3-DICHLOROPROPENETRANS-1,3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1,2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANE

- TETKACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE .,1.1.2-TRICHLOROETHANE *'TRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENES

1.00000000

1.001.001.001.001.0010.01.00

00000000

1.001.001.001.001.001.001.001.00

.1.001.005.001.001.001.001.001.001.001.001.001.003.00

XXXXXXXXXXXXXXXXXXXXXXXXXXXXX\XXXXX

TETRAHYDROFURAN 20,0

MADISON


(6CS) 2J1-4747FAX(6C6)23M777

VOLATILE ORGANIC"COMPOUND RESULTS PAGE OF WI LAB CERTIFICATION ID*: 113138300 CK'D: JuwAPP'D:PROJECT: HAGEN FARM RIFS DATE ISSUED:LOCATION: STOUGHTON, WISCONSINC#: 13452.89

BMQL - DETECTED, VALUE BELOW METHOD QUANTITATION LIMIT.X « ANALYZED, BUT NOT DETECTED.

REFERENCE: SW846, "TEST METHODS FOR EVALUATING SOLIDWASTE*f SEPTEMBER, 1986. METHODS 8010AND 8020 WITH MODIFICATIONS.

MADISONONE SCIENCE COLTTT

P.O. BOX 5385MADISON, Wl 5J705

(6C8) 23M747FAX (6C6) 2J1-4777

VOLATILE ORGANIC COMPOUND RESULTSWI LAB CERTIFICATION IDS: 113138300PROJECT: HAGEN FARM RIFSLOCATION: STOUGHTON, WISCONSINCl: 13452.89

PAGE ' Of CK'D:4Uu'APP'DDATE ISSUED :

COMPOUND


1957-001HF-GWDTB01-7911/14/90

BENZENEBROMOCHLOROMETHANEBROMOOICHLOROMETHANEBROMOFORMBROMOMETHANE

• CARBON TETRACHLORIDECHLOROBENZENECHLOROOIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DIBROMO-3-CHLOROPROPANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE

v 1,1-DICHLOROETHANE^-a,2-DICHLOROETHANE

1.1-DICHLOROETHENECIS-1,2-DICHLOROETHENETRANS-1.2-DICHLOROETHENE1.2-DICHLOROPROPANECIS-1,3-DICHLOROPROPENE

. TRANS-1,3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1,2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE1.1.2-TRICHLOROETHANE -vTRICHLOROETHENETRICHLOROFLUOROHETHANEVINYL CHLORIDEXYLENES

TETRAHYDROftjRAN

1.001.001.00i;ooi.ooi.ooi.ooi.ooi.oo10.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001,001.001,001.001.003.00

250

XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX

923

MADISONONE SOENCe COURT

P.O. BOX S3S5MADISON, W 5J70S

<6C8) 231-4747FAX(6C8)23M777

VOLATILE ORGANIC COMPOUND RESULTSWI LAB CERTIFICATION IDS: 113138300PROJECT: HAGEN FARM RIFSLOCATION: STOUGHTON, WISCONSIN«: 13452.89

PAGE*- OF5CK'D** **' APP'D"DATE*ISSUED:*/*-

OMPOUND

BENZENEBROMOCHLOROMETHANEBROMODICHLOROMETHANEBROMOFORMBROMOMETHANE .CARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANEl,2-DIBROMO-3-CHLOROPROPANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE

v 1,1-DICHLOROETHANEMf2-DICHLOROETHANE

1.1-DICHLOROETHENECIS-1.2-DICHLOROETHENETRANS-1.2-DICHLOROETHENE1.2-DICHLOROPROPANECIS-1, 3-DICHLOROPROPENETRANS-1.3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1, 2-TETRACHLOROETHANE1,1,2 , 2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE .,1.1.2-TRICHLOROETHANE " .TRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENES


1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.00-1.001.001.003.00

1957-002HF-GWDTB01-9711/14/90


TETRAHYDROFURAN 50.0 157


MADISON, wi 55705<6C» 2JM747

FAX (6C8) 291-4777

VOLATILE ORGANIC COMPOUND RESULTS PAGE:* OF^WI LAB CERTIFICATION ID?: 113138300 CK'D APP'D:PROJECT: HAGEN FARM RIFS DATE ISSUED: n/LOCATION: STOUGHTON, WISCONSINC#: 13452.89


Si THOD REFERENCE: SW846, "TEST METHODS FOR EVALUATING SOLIDWASTE*, SEPTEMBER, 1986. METHODS 8010AND 8020 WITH MODIFICATIONS.

P.O. BOX 5535MADISON. V[ 53705

<6C8) 2JM747FAX(6C8)2JM777

Volatile Organic Compound ResultsWI Lab Certification ID#: 113138300Project: Hagen Farms RI/FSLocation: Stoughton, WisconsinCf: 13452.98

Page! Of3Ckfd:jW App'dDate Issued: u

Compound


2047-001HF-GWOTB01-11712/6/90

Bromodi chloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChlorbethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-01chlorobenzene1.3-Dichlorobenzene1.4-Dlchlorobenzene1.1-Dichloroethane1.2-DichToroethane1.1-Dichloroetheneci s-1,2-Di chloroethene

\_/trans-l,2-Dichloroethene1.2-Dicnloropropanecis-1,3-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenesTetrahydrofuran

1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001,001.001.001.001.001.003.0020.0

XXXXXXXX .XXXXXXXXXXXXXXXXXXXXXXXXXX

WJRZYNi*.O. DUA «oJ

MADISON. Wl 53705C6C8) 2JM747

FAXC606)23M77?

Volatile Organic Compound ResultsWI Lab Certification IDS: 113138300Project: HagenTarms RI/FSLocation: Stoughton, Wisconsintt: 13452.98

PageCk*dDate Issued: \T_-ZC-

Compound


2047-002HF-GWDTB01-13712/6/90

BenzeneBromodi chloromethane

BromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromometh aneChloroethane2-Chloroethylvinyl Ether

• ChloroformChloromethane1.2-Dichlorobenzene1.3-Di chlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroetheneci s-1,2-Di chloroethenetrans-l,2-Dichloroethene1.2-Di chloropropane

^ cis-lf3-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMetnylene Chloride1,1,2,2-Tetrachl oroethaneTetrachloroetheneTo!uene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenesTetrahydrofuran

10.010.010.010.010.010.010.010.010010.010.010.010.010.010.010.010.010.010.010.010.010.010.050.010.010.010.010.010.010.010.010.030.0200

XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX


P.O. BOX 5585MAD CON. WI 53705

(6C8) 23M747FAX <6CB) 23M777

Volatile Organic-Compound ResultsWI Lab Certification ID#: 113138300Project: Hagen Farms RI/FSLocation: Stoughton, WisconsinC*: 13452.98

Page 3 Of 3Ck*dDate




P.O. BOX 5J65MADISON, Wl 53TO

(fiC8) 2)1-4747FAX C6C8) 251-4777

VOLATILE ORGANIC COMPOUND RESULTSWI LAB CERTIFICATION ID#: 113138300PROJECT: HAGEN FARM RIFSLOCATION: STOUGHTON, WISCONSINC#: 13452.89

PAGE 1 OF CZ-CK'D:jdWAPPDATE ISSUED:

COMPOUND.= »==r«CX=

N—<-• *

BENZENEBROMOCHLOROMETHANEBROMODICHLOROMETHANEBROMOFORMBROMOMETHANE

- CARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DIBROMO-3-CHLOROPROPANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENEM-DICHLOROETHANE

^,2-DICHLOROETHANE1.1-DICHLOROETHENECIS-1,2-DICHLOROETHENETRANS-1.2-DICHLOROETHENE1.2-DICHLOROPROPANECIS-1,3-DICHLOROPROPENETRANS-1.3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1,2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE1.1.2-TRICHLOROETHANE -vTRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENES

TETRAHYDROFtlRAN


1964-001HF-GWDTB02-2711/15/90

1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003.00

20,0


mRZYN

MADISON'ONE SCIENCE COURT

P.O. BOX 53-85MADISON. Wl 53705

(60S) 23M747FAX(6C8)25M777

VOLATILE ORGANIC COMPOUND RESULTS PAGE OF *WI LAB CERTIFICATION ID?: 113138300 CK'D w APP'D:PROJECT: HAGEN FARM RIFS DATE ISSUED:LOCATION: STOUGHTON, WISCONSINtt: 13452.89


METHOD REFERENCE: SWS46, "TEST METHODS FOR EVALUATING SOLIDWASTE6, SEPTEMBER, 1986. METHODS 8010AND 8020 WITH MODIFICATIONS.

WiRZYN


P.O. BOX 5J85MADBON, Wl 53705

(6C8) HH747FAX (606) 23M777

VOLATILE ORGANIC COMPOUND RESULTSWI LAB CERTIFICATION ID*: 113138300PROJECT: HAGEN FARM RI/FSLOCATION: STOUGHTON, WISCONSINC#: 13452.89

PAGE l OF 3CK'D:JWAPP'DDATE ISSUED: »

"OMPOUND

BENZENEBROMOCHLOROMETHANEBROMODICHLOROMETHANEBROMOFORMBROMOMETHANECARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DIBROMO-3-CHLOROPROPANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE

v>,l-DICHLOROETHANEM.2-DICHLOROETHANE

1.1-DICHLOROETHENECIS-1.2-DICHLOROETHENETRANS-1.2-DICHLOROETHENE1.2-DICHLOROPROPANECIS-1 ,3-DICHLOROPROPENETRANS-1 ,3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1,2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRlCHLOROETHANE .,1.1.2-TRICHLOROETHANE " .TRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENES


1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003.00

1971-001HF-GWDTB02-37

11/16/90





(6C8) »l-47«7FAX(6CB)23M777

VOUTILE ORGANIC-COMPOUND RESULTSWI LAB CERTIFICATION IDS: 113138300PROJECT: HAGEN FARM RI/FSLOCATION: STOUGHTON, WISCONSINC#: 13452.89 •

PAGE *- OFCK'D:4vDATE ISSUED

COMPOUND


- 1971-002HF-GWDTB02-57

11/16/90

BROMOCHLOROMETHANEBROMODICHLOROMETHANEBROMOFORMBROMOMETHANECARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANE 'CHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DIBROMO-3-CHLOROPROPANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE1.1-DICHLOROETHANE1.2-DICHLOROETHANE1.1-DICHLOROETHENECIS-1,2-DICHLOROETHENETRANS-1,2-DICHLOROETHENE1.2-DICHLOROPROPANECIS-1,3-DICHLOROPROPENETRANS-1,3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1f2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE1.1.2-TRICHLOROETHANETRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENES

1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003.00



WARZYN

MADISONONE SC1ENCI COURTP.O. 3OX 5J3S

MAD BOS. wi 5J705(6CS) 23M747

FAX(6CS)23M777

VOLATILE ORGANIC COMPOUND RESULTS PAGE * OF3WI LAB CERTIFICATION ID#: 113138300 CK'Dt^APP'D:PROJECT: HAGEN FARM RI/FS DATE ISSUED: a|tt.LOCATION: STOUGHTON, WISCONSINC#: 13452.89


REFERENCE: SW846, "TEST METHODS FOR EVALUATING SOLIDWASTE*, SEPTEMBER, 1986. METHODS 8010AND 8020 WITH MODIFICATIONS.


P.O. BOX 5385MADISON, wi 537Q5

<608> 23M747FAX (6C6) 231-4777

VOLATILE ORGANIC COMPOUND RESULTS PAGE*WI LAB CERTIFICATION ID#: 113138300 CKMPROJECT: HAGEN FARM RIFS DATE ISSUEDLOCATION: STOUGHTON, WISCONSIN«: 13452.89

^COMPOUND


1977-001 1977-002HF-GWDTB02-78 HF-FB0111/19/90 11/19/90

BENZENEBROMODICHLOROMETHANEBROMOFORMBROMOMETHANECARBON TETRACHLORIOECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE.2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE1,1-DICHLOROETHANE

^yl,2-DICHLOROETHANE1.1-DICHLOROETHENECIS-1.2-DICHLOROETHENETRANS-1,2-DICHLOROETHENE1.2-DICHLOROPROPANECIS-1,3-DICHLOROPROPENETRANS-1.3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1,2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE1.1.2-TRICHLOROETHANETRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENES

1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003.00



TETRAHYDROfURAN 20.0


MADISON, VI 53705(6C8J ZJM747

FAX (6C8) 2514777

VOLATILE ORGANIC-COMPOUND RESULTS PAGE* OFWI LAB CERTIFICATION IDS: 113138300 CK'DwPROJECT: HAGEN FARM RIFS DATE ISSUEDLOCATION: STOUGHTON, WISCONSINCl: 13452.89

COMPOUND

BENZENEBROMODICHLOROMETHANEBROMOFORMBROMOMETHANECARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENC1.1-DICHLOROETHANE1.2-DICHLOROETHANE1.1-DICHLOROETHENE *

-1 ,2-DICHLOROETHENETRANS-1, 2-DICHLOROETHENE1.2-DICHLOROPROPANECIS-1, 3-DICHLOROPROPENETRANS-1 ,3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1 , 1 , 1 , 2-TETRACHLOROETHANE1 , 1 ,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE1.1.2-TRICHLOROETHANETRICHLOROETHENETRICHLOROFLUOROMETHANE - ,VINYL CHLORIDEXYLENES


1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001,001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003,00

1977-003HF-TB0111/19/90




P.O. BOX 3585MADISON, Wl 55T05

VOLATILE ORGANIC COMPOUND RESULTS PAGE 3WI LAB CERTIFICATION I0#: 113138300 CK'D: APP'D:V1CGPROJECT: HAGEN FARM RIFS DATELOCATION: STOUGHTON, WISCONSINC#: 13452.89


REFERENCE: sws46, -TEST METHODS FOR EVALUATING SOLIDWASTEfi, SEPTEMBER. 1986. METHODS 8010AND 8020 WITH MODIFICATIONS.

WAKZYN

. MADISONONE SCIENCE COURT

P.O. BOX 5J85MADISON, Wl 53TO5

(606) 2J1-47H7FAX (606) 23M777

Volatile Organic Compound ResultsWI Lab Certification ID#: 113138300Project: Hagen farm RI/FSLocation: Stougliton, Wisconsin«: 13452.98

Page I Of ICkrd: W App'dDate Issued:i-j

Compound


2069-001HF-GWDTB02-7412/11/90

BenzeneBromochloromethaneBromod1chloromethane

v JSromoformBromomethaneCarbon TetrachlorldeChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethanel,2-Dibromo-3-Chloropropane1, 2-D1chlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-1,2-Di chloroethenetrans-1,2-Dichloroethene1t2-D1chloropropane^ cis-l,3-Dichloropropenetrans-1,3-Di chloropropeneEthyl BenzeneMethylene Chloride1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trichloroethane1.1.2-Trichloroethane

. TrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenesTetrahydrofuran

1*001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.00000000

1.001.001.001.005.001.001.001.001.001.001.001.001.001.003.00

10.0


X * analyzed, but not detected.Method reference: SW846, "Test Methods for Evaluatin<

Waste", September, 1986. Methods 1and 8020 with modifications.

I Solidtoio

Volatile Organic Compound ResultsWI Lab Certification ID3: 113138300Project: Hagen Farm RI/FSLocation: Town-"of Dunn, WisconsinCl: 13452.98

• Page l Ofpk rf *•Date Issued'



FAX(6C6)23M777

Compound


2062-001(1)HF-GWDTB02-9412/10/90

BenzeneBromochl oromethane3romodi chl oromethane

BromomethaneCarbon TetrachlorideChl orobenzeneChl orodibromomethaneChl oroethane2-Chloroeth/l vinyl EtherChloroformChl oromethanel,2-Dibromo-3-Chloropropane1 , 2-Di chl orobenzene1,3-Dichl orobenzene1 , 4-Di chl orobenzene1 , 1 -D1 chl oroethane1, 2-Di chl oroethane1.1-Dichloroethenecis-1, 2-Dichloroethenetrans-1, 2-Di chl oroethene1.2-Dichloropropanecis-1, 3-Dichloropropenetrans-1 ,3-Dichl oropropeneEthyl BenzeneMetnylene Chloride1,1,1 , 2-Tetrachl oroethane1,1,2, 2-Tetrachl oroethaneTetrachl oroetheneTo! uene1 , 1 , 1-Tri chl oroethane1 , 1 , 2-Tri chl oroethaneTrichloroetheneTri chl orof 1 uoromethaneVinyl ChlorideXyl enes

1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.000000

1.001.005.001.001.001.001.001.001.001.001.001.003.00




P.O. BOX 5385MADBON. -m 53705

«C8> Wl-4747FAX (608) 23M777

Volatile Organic Compound Results Paqe Of *-WI Lab Certification ID#: 113138300 £k d: App'd:Project: Hagen Farm RI/FS Date Issued:Location: Town of Dunn, WisconsinC#: 13452.98

X « analyzed, but not detected.(1) Sample chromatogram contains unidentified compounds.Method reference: SW846, "Test Methods for Evaluating Solid

Waste*, September, 1986. Methods 8010and 8020 with modifications.

WARZYN


P.O. BOX 5385. MADISON. WI 53705

(608) 23M747FAX<6C8)23M777

VOLATILE ORGANIC COMPOUND RESULTSWI LAB CERTIFICATION ID#: 113138300PROJECT: HAGEN FARM RIFSLOCATION: STOUGHTON, WISCONSINC#: 13452.89

COMPOUND

PAGE t OF 'DATE ISSUED: ,i,»-


1982-001HF-GWDTB02-9711/20/90

1.00BROMODICHLOROMETHANEBROMOFORMBROMOMETHANECARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE1.1-DICHLOROETHANE1.2-DICHLOROETHANE1.1-DICHLOROETHENECIS-1.2-DICHLOROETHENE

WTRANS-1,2-DICHLOROETHENE1.2-DICHLOROPROPANE 'CIS-1,3-DICHLOROPROPENETRANS-1,3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1,2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE1.1.2-TRICHLOROETHANETRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENESTETRAHYDROFURAN

1.001.001.001.001.00J.OO1.0010.01.001.001.001.001.001,001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003.00

20.0


X « ANALYZED, BUT NOT DETECTED.

METHOD REFERENCE: SW846, "TEST METHODS FOR EVALUATING SOLIDWASTE", SEPTEMBER, 1986. METHODS 8010AND 8020 WITH MODIFICATIONS.



(60S 7J1-4W7FAX (6063 231-4777

Volatile Organic Compound ResultsWI Lab Certification ID#: 113138300Project: Hagen Farms - RI/FSLocation: Town of Dunkirk, WisconsinC#: 13452.98

Page ICkYd :

OfApp'd:

Date Issued:rt//t/54v

Compound


2002-001 2002-002HF-GWDTB03-67 HF-FB0211/27/90 11/27/90

v janzene^IJromodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodibromomethaneChloroethane2-Chloroethylvinyl Ether1.2-Di chlorobenzene1.3-Di chlorobenzene1.4-Di chlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroetheneci s-1,2-Di chloroethenetrans-1.2-Dicnloroethene1.2-Di cnloropropane:i s-1,3-Di ch1oropropenerans-1,3-Di chl oropropeneEthyl BenzeneMetnylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-TrichloroethaneTrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenes

1.001.005.005.001.001.001.003.0025.01.001.001.001.001.003.003.003.001.001.001.001.005.001.001.001.001.001.001.003.003.003.00

XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX

XXXXXXXXXXXXXXXXXXXXX6.76XXXXXXXXX


MAXHSONONE SCIENCE COURT

P.O. BOX 5385MADBON, wi 53705

FAX<606)23M777


e 2- Ofd:j*«v

Date Issued:t*//*/>>

Compound


2002-003HF-GWDTB03-8711/27/90

Benzene, omodi chloromethaneX^omoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodibromomethaneChloroethane2-Chloroethylvinyl Ether1.2-Di chlorobenzene1.3-Di chlorobenzene1.4-Di chlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecls-1,2-Di chloroethenetrans-1.2-Dichloroethene1.2-Di chloropropanecis-1,3-Di chloropropene*rans-l,3-Dichloropropene

v/hyl BenzeneHetnylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTri chlorofluoromethaneVinyl ChlorideXylenes

1.001.005.005.001.001.001.003.0025.01.001.001.001.001.003.003.003.001.001.001.001.005.001.001.001.001.001.001.000000

3.00





<606> 23M747FAX (60S) 23M777


3 Of-

Compound


2002-004HF-GWDTB03-9211/27/90

Benzene, -omodi chloromethaneroraoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodibromomethaneChloroethane2-Chloroethylvinyl Ether1.2-Dichlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-l,2-Dichloroethenetrans-1.2-Dichloroethene1.2-D1cnloropropanecis-l,3-Dichloropropene>ans-l,3-Di chloropropene

v thyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trichloroethane1.1.2-Tri chloroethaneTrichloroethene.Trichlorof1uoromethaneVinyl ChlorideXylenes

1.001.005.005.001.001.001.003.0025.01.001.001.001.001.003.003.003.001.001.001.001.005.001.001.001.001.001.001.003.003.003.00



W^RZYN



<&») 231-4747FAX(6C6)23M777

Volatile Organic Compound ResultsWI Lab Certification ID#: 113138300Project: Hagen farms - RI/FSLocation: Town of Dunkirk, WisconsinCl: 13452.98

Page H OfCk?d:-jwDate Issued:)1/'*/

Compound

Benzenev^romodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorod i bromomethane

. Chloroethane- 2-Chloroethylvinyl Ether1.2-Di chlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-l,2-Dichloroethenetrans-1.2-Di chloroethene1.2-Dichloropropanecis-1,3-Di chloropropene

£rans-l, 3-Di chl oropropeneEthyl BenzeneMetnylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trichloroethane1.1.2-Tri chloroethaneTrichloroetheneTrichlorofluoromethaneVinyl ChlorideXylenes


1.001.005.005.001.001.001.003.0025.01.001.001.001,001.003.003.003.001.001.001.001.005.001.001.001.001.001.001.003.003.003.00

2002-005 2HF-FB03 H11/27/90 1

XXXXXXXXXXXXXXXXXXXXX

5.85XXXXXXXXX

:002-006(1)IF-TB021/27/90

XXXXXXXX-xXXXXXXXXXXXXXXXXXXXXXX


mRZYN

Volatile Organic Compound Results Page^Of/ rf\/ —— ~WI Lab Certification ID#: 113138300 Ck?d:^juu App'd: |^X


P.O. BOX 5JB5MADISON. Wl 53705

' C608) 231-4747FAX (608) 23M777

Project: Hagen Farms - RI/FS Date Issuedi/tV/z/jLocation: Town of Dunkirk, Wisconsin 'C#: 13452.98

X • analyzed, but not detected.(1) Sample chromatogram contains unidentified compounds.thod reference: SW846, "Test Methods for Evaluating Solid


mRZYN



(606) 231-4747FAX (608) 231-4777

VOLATILE ORGANIC COMPOUND RESULTSWI LAB CERTIFICATION IDI: 113138300PROJECT: HAGEN FARM RI/FSLOCATION: STOUGHTON, WISCONSINC#: 13452.89

PAGE I OF*CK'D:4WAPDATE ISSUED

COMPOUND

V 3ENZENEMJROMODICHLOROMETHANEBROMOFORMBROMOMETHANECARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE1.1-DICHLOROETHANE1.2-DICHLOROETHANE1,1-DICHLOROETHENECIS-1,2-DICHLOROETHENETRANS-1.2-DICHLOROETHENE^,2-DICHLOROPROPANECIS-1,3-DICHLOROPROPENETRANS-1,3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1,2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE1.1.2-TRICHLOROETHANETRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENESTETRAHYDROFURAN

REPORTABLEDETECTIONLIMIT

1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003.0020.0

1998-001(1)HF-GWDTB03-2711/26/90

1998-002(1)HF-GWDTB03-4711/26/90



X - ANALYZED, BUT NOT DETECTED.

METHOD REFERENCE: SW846, "TEST METHODS FOR EVALUATING SOLIDWASTE", SEPTEMBER, 1986. METHODS 8010 AND8020 WITH MODIFICATIONS.

(1) SAMPLE CHROMATOGRAM CONTAINS UNIDENTIFIED COMPOUNDS.

mRZYN


P.O. BOX 5385MADISON, VI 53705

(606) 231-4747FAX (6C8) 13M777

Volatile Organic Compound Results Page l OfWI Lab Certification ID#: 113138300 CkycProject: Hagen Farms - RI/FS Date Issued;Location: Town of Dunkirk, WisconsinC#: 13452.98

Compound


2007-001HF-GWDTB03-10711/28/90

v anzene^tfromodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl Ether1,2-Di bromo-3-Chloropropane1,2-D i chlorobenzene1(3-D1chlorobenzene1,4-Di chlorobenzene1.1-Dichloroethane .1.2-01chloroethane1,1-Dichloroethenecis-1,2-Dichloroethenetrans-l,2-Dichloroethene\2-Dicnloropropane

^-«ds-l,3-Dichioropropenetrans-l,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trichloroethane1.1.2-Tri chloroethaneTrichloroetheneTrichlorofluoromethaneVinyl ChlorideXylenesTetrahydrof uran - * •»

1.001.005.005.001.001.001.003.0025.02.001.001.001.001.001.003.003.003.001.001.001.001.005.001.001.001.001.001.001.003.003.003.00

20.0

XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX





<&») 23M747FAX(606)ZJM777

Volatile Organic Compound ResultsWI Lab Certification IDs?: 113138300Project: Hagen Farms - RI/FSLocation: Town of Dunkirk, WisconsinC#: 13452.98

OfApp'd

Date Issued:

Compound


2007-002HF-GWDTB03-12711/28/90

BenzeneV jromodichloromethane^-Bromoform

BromomethaneCarbon TetrachlorideChlorobenzeneChlorod1bromomethaneChloroethane2-Chloroethylvinyl Ether1,2-DIbromo-3-Chl oropropane1.2-Di chlorobenzene1.3-Dichlorobenzene1.4-Di chlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-l,2-Dichloroethenetrans-1.2-Dichloroethene1.2-D1cnloropropanev:1 s-1,3-Di chl oropropene

^trans-l,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-TrichloroethaneTrichloroetheneTri chlorofluoromethaneVinyl ChlorideXylenesTetrahydrofuran

1.001.005.005.001.001.001.003.0025.02.001.001.001.001.0000000000

1.001.001.001.005.001.001.001.001.001.001.003.003.003.00

20.0

X = analyzed, but not detected.Method reference: SW846, "Test Methods for Evaluating Solid


mRZYN


P.O. BOX 5385MADBON, W] 53705

<€08) 2J1-47X7FAX(6Q6)23M777


Page < Of >CkTd:awu> App'd: »yDate Issued:i*/|T/?0

Compound


2016-001HF-GWDTB03-14711/29/90

yizenex^omodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorod i bromomethaneCM oroethane2-Chloroethylvinyl Ether1.2-Di chlorobenzene1.3-Dichlorobenzene1.4-Dlchlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-l,2-Dichloroethenetrans-1.2-Di chloroethene1.2-D1cnloropropane'•is-l.S-Di chl oropropene•ans-1,3-Di chloropropene'thvl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTrlchldrofluoromethaneVinyl ChlorideXylenesTetrahydrofuran

Vth

1.001.005.005.001.001.001.003.0025.01.001.001.001.001.003.003.003.001.001.001.001.005.001.001.001.001.001.001.003.003.003.00

20.0


X « analyzed, but not detected.Method reference: SW846, "Test Methods for Evaluating Solid


WRZYN



(608) 231X747FAX (608) 25U777

Volatile Organic Compound Results Page ( OfWI Lab Certification ID#: 113138300 Ckrd:<j ,Project: Hagen Farm RI/FS Date IssuedLocation: Stoughton, WisconsinC#: 13452.98 "

Compound


2090-OOim-HF-GWDTB04-7512/13/90

BenzeneBromochloromethaneBromod i chloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethanel,2-Dibromo-3-Chloropropane1.2-Dichlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-l,2-Dichloroethenetrans-1,2-Dichloroethene1.2-Dichloropropanecis-l,3-Dichloropropenetrans-1,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenes

1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003.00




P.O. BOX $383 attMADBON, Wl 53705

<6» 2314747FAX (606) 231-4777

Volatile Organic Compound Results Page'1' Of*WI Lab Certification IDs?: 113138300 Ck*d:**s App'd:Project: Hagen Farm RI/FS Date Issued:izJ^yToLocation: Stoaghton, Wisconsin 'Cl: 13452.98

X - analyzed, but not detected.(1) Sample chromatogram contains unidentified compounds.Method reference: SW846, "Test Methods for Evaluating Solid

Waste*, September. 1986. Methods 8010and 8020 with modifications.


P.O. BOX 5385MADISON. Wl 5J705

C6C8) 231-4747FAX <60B) 231-4777

Volatile Organic Compound ResultsWI Lab Certification ID#: 113138300Project: Hagen Farm RI/FSLocation: Stoughton, WisconsinC#: 13452.98

Of3App'd:

Date Issued:, r/tPag?

Compound

^-BenzeneBromochloromethaneBromodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorod i bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethanel,2-Dibromo-3-Chloropropane1.2-D1chlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane,1-Dichl oroethene

ci s-1,2-Di chloroethenetrans-l,2-D1chloroethene1.2-Di chloropropanecis-l,3-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tri chloroethane ^TrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenes


1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.004.00

2122-001 2122-002 2122-003HF-GWD HF-GWD HF-GWDTB04-134 TB04-93 TB04-12212/18/90 12/18/90 12/18/90


XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX '


Tetrahydro£uran 10.0

WiRZYN


P.O. BOX 5585MADISON, wi JJTOS(608) 25M747

FAX (608) 231-4777


Page *• Of 3Ck'd:-*'*-'App'd:Date Issued: i

Compound

BenzeneBromochloromethaneBromodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodibromomethaneChl oroethane2-Chloroethyl vinyl EtherChloroformChloromethanel,2-Dibromo-3-Chloropropane1 , 2-Dichl orobenzene1,3-Dichlorobenzene1 , 4 -Di chl orobenzene1.1-Dichloroethane1.2-Dichloroethane1,1-Dichloroethenecis-l,2-Dichloroethenetrans-l,2-Dichloroethene1 , 2 -Di cnl oropropanecis-l,3-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMethyl ene Chloride1,1,1 ,2-Tetrachl oroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1,1,1 -Tr i chl oroethane1,1,2-Trichl oroethaneTrichloroetheneTri chl orof 1 uoromethane" * . -Vinyl ChlorideXylenes


2122-004 2122-005HF-GWD HF-GWD 2122-006TB04-104 TB04-92 HF-TB0412/18/90 12/18/90 12/18/90

1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.004.00

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P.O. BOX 5585MADISON, vi 53705

<6tt) 2)1-4747FAX <6C6) 251-4777

Volatile Organic Compound Results Page 3 of3WI Lab Certification ID#: 113138300 Ck'd: App'd:Project: Hagen Farm RI/FS Date Issued: iLocation: Stoughton, Wisconsin«: 13452.98


Method reference: SW846, "Test Methods for Evaluating SolidWaste* , September, 1986. Methods 8010and 8020 with modifications.

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FAX (608) Z3M777


Page I Of *-Ck'diJW-' App'd:Date Issued: 1/3/7 /

Compound

BenzeneBromodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1, 2-Di chlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1,1-Dichloroethenecis-1,2-Di chloroethenetrans-1,2-Dichloroethene1, 2-Di chloropropanec1s-l,3-Dichloropropenetrans-1,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trichloroethane1.1.2-TrichloroethaneTrichloroetheneTrlchlorofluoromethaneVinyl Chloride /-?Xylenes


1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.003.00

2142-001 2142-002HF-GWD HF-GWDTB05-60 TB05-4712/20/90 12/20/90




mRZYN



<&») 23M747PAX C6C8) 231-4777

Volatile Organic Compound ResultsWI Lab Certification IDS: 113138300Project: Hagen Farm RI/FSLocation: Stoughton, WisconsinC*: 13452.98

Paget, Of *Ck7d: W App'd:>iTADate Issued: i


Method reference: SW846, "Test Methods for Evaluating SolidWaste*, September, 1986. Methods 8010and 8020 with modifications.

wmi monthly progress report (cover letter included)

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