Company Name Madina Trading & Contracting Est. - Mechanical Division

KEY INFORMATION QUESTIONS ANSWERS

File Reference File Details KH/Excel/Welding/BH/WPS011

Test Conducted On Date of Test 16 - JUN - 98

Reviews & Approvals Prepared By KEITH HARMERDepartment ENGINEERINGDate Prepared 12 - JULY - 98Reviewed By R. VAIRAMANIDepartment QA / QCDate Reviewed 12 - JULY - 98Approved By S.E. LANGLEYDepartment BUREAU VERITASDate Approved 12 - JULY - 98

Welder Details Welder ID MW00078Employee No. 00078Name V.K. MOHANLocation of Test MADINA WORKSHOP, SALWA, QATAR.

Original PQR Details WPS No. 011Revision No. 000Supporting PQR 011Welding Process GTAW & SMAWElectrode Polarity -Ve & +VePQR Position 6GPositions Qualified ALL

Welding Details Weld Direction UPHILLMaximum Bead Width 3 x Core DiaMulti / Single Pass MULTIPASSManual / Automatic MANUAL

Technique Technique STRING / WEAVESingle/Both Sides SINGLEMultiple/Single Electrode SINGLEOscillation MANUALOther NOT APPLICABLE

Joint on Qualification Test Joint Type BUTT WELDMethod of Preparation FLAME CUT &/OR GRINDIncluded Angle 37.5 Deg +/- 2 DegMaterial Thickness 11.0 mmRoot Gap 2.5 - 3.0 mmRoot Face 1.0 - 2.0 mmBacking NONE

Base Metal Details Material Specification API5LType or Grade GRADE BHeat Number J738201From - P No. 1To - P No. 1Diameter of Test Coupon 6"Other NONE

Welding Consumables Electrode Brand ESAB & LINCOLNSize of Filler Metal 2.4 mm, 2.5 mm & 3.25 mmSFA / AWS No 5.18 & 5.1

Classification ER70S-3 & E7018Type of Flux NOT APPLICABLEOther NONE

Inert Gas Details Gas Type ARGONGas Flow Rate 10 LTR/MINGas Mixture 99.99%Oriface / Cup Size 10mmBacking Gas NOT APPLICABLEBacking Flow Rate N/ABacking Gas Mixture N/A

Preheat Details Pipe to Pipe AMBIENTPipe to Fittings AMBIENTFitting to Fitting AMBIENTSpare Line 1Spare Line 2

Interpass Temperature Interpass Temperature NOT TO EXCEED 150 °C

PWHT Details Temperature NOT APPLICABLETime NOT APPLICABLEEquipment Type NOT APPLICABLEOther NOT APPLICABLELine 5

PQR Material Details (QW 403) Qualified ANY METAL ASSIGNED TOCode/Testing Standard ASME IXOther Codes/Standards NOT APPLICABLEP No. / Group No. P1 - GROUP No. 1

Plate & Pipe Ranges ASME IX 4.75 - 22.0 mm (ASME IX) OTHERS NOT APPLICABLEDiameter ALLPQR Filler Metal F Nos. F6 & F4PQR Filler Metal A Nos. A1Interpass Cleaning Method GRINDING & BRUSHINGMethod of Back-Gouging NOT APPLICABLETungsten Type 2% THORIATEDTungsten Size 2.4 mm

WPSPASS WELDING ELECTRODE CURENT TYPE ACTUAL WPS ACTUAL WPS TRAVEL TRAVEL ACTUAL INTERNUMBER ELECTRODE DIA (mm) & POLARITY AMPS AMPS VOLTS VOLTS SPEED SPEED KJ/mm Temp°CPass No. 1 GTAW - ER70S-3 2.4 mm Direct -Ve 101.0 90 - 110 12.0 11 - 13 75 70 - 100 0.97 AmbientPass No. 2 GTAW - ER70S-3 2.4 mm Direct -Ve 132.0 120 - 140 14.0 13 - 15 90 70 - 100 1.23 95Pass No. 3 SMAW - E7018 2.5 mm Direct +Ve 93.0 90 - 110 23.0 22 - 25 80 75 - 140 1.60 116Pass No. 4 SMAW - E7018 2.5 mm Direct +Ve 97.0 90 - 110 24.0 22 - 25 120 75 - 140 1.16 145Pass No. 5 SMAW - E7018 2.5 mm Direct +Ve 96.0 90 - 110 23.0 22 - 25 130 75 - 140 1.02 120Pass No. 6 SMAW - E7018 3.25 mm Direct +Ve 121.0 120 - 140 24.0 22 - 25 135 120 - 140 1.29 130Pass No. 7 SMAW - E7018 3.25 mm Direct +Ve 92.0 120 - 140 23.0 22 - 25 130 120 - 140 0.98 133Pass No. 8 SMAW - E7018 3.25 mm Direct +Ve 93.0 120 - 140 24.0 22 - 25 130 120 - 140 1.03 130

TENSILE TESTDimensions UTS Fracture Comments

Mark No. Type mm Area mm2 UTL kN N/mm2 Position Location516 Cross-weld 11.0 x 19.1 210.1 101.7 484.0 Parent Mat'l Nil 517 Cross-weld 10.3 x 19.0 195.7 97.0 496.0 Parent Mat'l Nil

BEND TESTFormer Dia Comments

Mark No. Type Bend Angle mm Result Location518 Face Bend 180° 4 t Acceptable Nil 519 Face Bend 180° 4 t Acceptable Nil 520 Root Bend 180° 4 t Acceptable Nil 521 Root Bend 180° 4 t Acceptable Nil

CHARPY IMPACTLocation Dimensions Temperature Absorbed Energy Average Comments

Mark No. mm °C Joules, J524 W C L 10 x 10 -29 106 33 27 55 Nil525 H A Z 10 x 10 -29 156 194 204 181 Nil

TEST RESULTS

Visual Examination SATISFACTORYSurface NDT NOT APPLICABLERadiography SATISFACTORYTensile Test SATISFACTORY

Bend Test SATISFACTORYMacro Examination SATISFACTORYFillet Weld Fracture Test NOT APPLICABLECharpy Vee Notch Code ASTM E23Charpy Vee Notch Test SATISFACTORYOther Tests HARDNESS - OKOVERALL TEST RESULT ACCEPTABLE

mm2

4 t4 t4 t4 t

TEST SPECIFICATION - Interpass Temperature kN N/mm2 Position Location

Parent Mat'l

TEST SPECIFICATION - Interpass TemperatureLocation

Acceptable 1 - 2 o'clock Acceptable 7 - 8 o'clock Acceptable 4 - 5 o'clock Acceptable 10-12 o'clock

### Madina Trading & Contracting Est. - Mechanical Division

WELDING PROCEDURE SPECIFICATION - No. 011

WPS Details Welding Consumables PQR Material Details

WPS No. : 011 Electrode Brand : ESAB & LINCOLN Material (QW 403) QualifiedRevision No : 000 SFA / AWS No : 5.18 & 5.1 ANY METAL ASSIGNED TOSupporting PQR : 011 Classification : ER70S-3 & E7018 P1 - GROUP No. 1Welding Process : GTAW & SMAW Type of Flux : NOT APPLICABLE Plate & Pipe DetailsElectrode Polarity : -Ve & +Ve Gas Type : ARGON Thickness : 4.75 - 22.0 mm (ASME IX) PQR Position : 6G Gas Flow Rate : 10 LTR/MIN Thickness : NOT APPLICABLEPositions Qualified : ALL Backing Gas : NOT APPLICABLE Diameter : ALL

PQR Details Preheat Details Deg C PWHT Details

Weld Direction : UPHILL Pipe to Pipe : AMBIENT Temperature : NOT APPLICABLEMax Bead Width : 3 x Core Dia Pipe to Fittings : AMBIENT Time : NOT APPLICABLEMulti / Single Pass : MULTIPASS Fitting to Fitting : AMBIENT Equipment : NOT APPLICABLEManual Automatic : MANUAL Other : NOT APPLICABLETechnique : STRING / WEAVEOscillation : MANUAL Interpass Temperature : NOT TO EXCEED 150 °C

Joint On Qualification Test Qualified Weld Preparations - Qualified Joint Configuration

### Angle : 37.5 Deg +/- 2 DegThickness : 11.0 mm (t)Root Gap : 2.5 - 3.0 mm (rg)Root Face : 1.0 - 2.0 mm (rf)Backing : NONE TEST POSITION 6GPipe Dia : 6" Root Gap : 2.5 - 3.0 mm Root Face : 1.0 - 2.0 mm

Pass Welding Electrode Electrode Current Type Amps Volts Travel Speed Number Welding Class Diameter & Polarity (a) (v) mm / min

Pass No. 1 GTAW - ER70S-3 2.4 mm Direct -Ve 90 - 110 11 - 13 70 - 100Pass No. 2 GTAW - ER70S-3 2.4 mm Direct -Ve 120 - 140 13 - 15 70 - 100Pass 3 to 5 SMAW - E7018 2.5 mm Direct +Ve 90 - 110 22 - 25 75 - 140Pass 6 to < SMAW - E7018 2.5 mm Direct +Ve 120 - 140 22 - 25 120 - 140

ASME Notes Additional Notes

1. PQR Base Matl. P Nos & Group Nos : P1 - GROUP No. 12. PQR Filler Metal F Nos. : F6 & F43. PQR Filler Metal A Nos. : A14. Interpass Cleaning Method : GRINDING & BRUSHING5. Tungsten Type : 2% THORIATED

PREPARED BY REVIEWED BY APPROVED BYNameName : KEITH HARMER Name : R. VAIRAMANI Name : S.E. LANGLEY

Sign : Sign : Sign :

Dept : ENGINEERING Dept : QA / QC Dept : BUREAU VERITAS

Date : 12 - JULY - 98 Date : 12 - JULY - 98 Date : 12 - JULY - 98

KH/Excel/Welding/BH/WPS011

Madina Trading & Contracting Est. - Mechanical Division

PROCEDURE QUALIFICATION RECORD

PQR : 011 REV : 000 Sheet : 1 of 2

Company Name : Madina Trading & Contracting Est. - Mechanical Division

Original Procedure Qualification Record No : 011 Date : 16 - JUN - 98

Original WPS No. : 011 Welder ID : MW00078

Welding Process : GTAW & SMAW Name : V.K. MOHAN

Type (Manual / Automatic / Semi-Automatic) : MANUAL Location : MADINA WORKSHOP, SALWA, QATAR.

JOINTS (QW - 402)

###

################## Angle : 37.5 Deg +/- 2 Deg

Thickness : 11.0 mm (t)Root Gap : 2.5 - 3.0 mm (rg)Root Face : 1.0 - 2.0 mm (rf) TEST POSITION 6GBacking : NONE Root Gap : 2.5 - 3.0 mm Root Face : 1.0 - 2.0 mm

BASE METAL (QW - 403) POSTWELD HEAT TREATMENT (QW - 407)

Material Specification : ASME SA 106 Temperature : NOT APPLICABLEType or Grade : GRADE B Time : NOT APPLICABLEHeat Number : J738201 Equipment Type : NOT APPLICABLEFrom P No. : 1 To P No. : 1 Other : NOT APPLICABLEThickness of Test Coupon : 11.0 mmDiameter of Test Coupon : 6"

FILLER METAL (QW - 404) GAS (QW - 408)

SFA Specification : 5.18 & 5.1 Percent CompositionAWS Specification : ER70S-3 & E7018 Type Gas(es) Mixtures Flow RateFiller Metal F No. : F6 & F4 Shielding ARGON 99.99% 10 LTR/MINWeld Metal Analysis A No. : A1 Trailing - - -Size of Filler Metal : 2.4 mm, 2.5 mm & 3.25 mm Backing - - -Weld Metal Thickness : 11.0 mm Other - - -Other : NOT APPLICABLE

POSITION (QW - 405) ADDITIONAL NOTES

Position of Groove : 6GWelding Progression : UPHILLOther : NOT APPLICABLE

PRE - HEAT (QW - 405)

Pre-Heat Temperature : AMBIENTInterpass Temperature : NOT TO EXCEED 150 °CEquipment Type : NOT APPLICABLEOther : NOT APPLICABLE

KH/Excel/Welding/BH/WPS011

Madina Trading & Contracting Est. - Mechanical Division

PROCEDURE QUALIFICATION RECORD

PQR : 011 REV : 000 Sheet : 2 of 2

TECHNIQUE (QW - 410)

String or Weave Bead : STRING / WEAVE Single/Both Side : SINGLEOrifice / Cup Size : 10mm Maximum Weave : 3 x Core DiaInterpass Cleaning Method : GRINDING & BRUSHING Joint Type : BUTT WELDMethod of Back Gouging : NOT APPLICABLE Method of Preparation : FLAME CUT &/OR GRINDOscillation : NOT APPLICABLE Code/Testing Standard : ASME IXMultiple/Single Pass : MULTIPASS Other Applicable Codes : NOT APPLICABLE

Pass Welding Electrode Electrode Current Type Amps Volts Heat Input Travel Interpass Number Welding Class Diameter & Polarity (a) (v) Kj / mm mm / min Temp°C

Pass No. 1 GTAW - ER70S-3 2.4 mm Direct -Ve 101.0 12.0 0.97 75 AmbientPass No. 2 GTAW - ER70S-3 2.4 mm Direct -Ve 132.0 14.0 1.23 90 95Pass No. 3 SMAW - E7018 2.5 mm Direct +Ve 93.0 23.0 1.60 80 116Pass No. 4 SMAW - E7018 2.5 mm Direct +Ve 97.0 24.0 1.16 120 145Pass No. 5 SMAW - E7018 2.5 mm Direct +Ve 96.0 23.0 1.02 130 120Pass No. 6 SMAW - E7018 3.25 mm Direct +Ve 121.0 24.0 1.29 135 130Pass No. 7 SMAW - E7018 3.25 mm Direct +Ve 92.0 23.0 0.98 130 133Pass No. 8 SMAW - E7018 3.25 mm Direct +Ve 93.0 24.0 1.03 130 130

TENSILE TEST TEST SPECIFICATION - ASME IXMark No. Type Dimensions Area UTL UTS Fracture Comments/Location

mm mm2 kN N/mm2 Position

516 Cross-weld 11.0 x 19.1 210.1 101.7 484.0 Parent Mat'l Nil 517 Cross-weld 10.3 x 19.0 195.7 97.0 496.0 Parent Mat'l Nil

BEND TEST TEST SPECIFICATION - ASME IXMark No. Type Bend Angle Former Diameter Result Comments/Location

518 Face Bend 180° 4 t Acceptable Nil 519 Face Bend 180° 4 t Acceptable Nil 520 Root Bend 180° 4 t Acceptable Nil 521 Root Bend 180° 4 t Acceptable Nil

CHARPY IMPACT TEST SPECIFICATION - ASTM E23Mark No. Location Dimensions Absorbed Energy Average Temperature °C Comments

mm Joules, J J

524 W C L 10 x 10 106 33 27 55 -29 Nil 525 H A Z 10 x 10 156 194 204 181 -29 Nil

TEST HOUSE LABORITORY : MTS INTERNATIONAL HOLDING Test No. AD-81427 Rev'n 0WITNESSED BY : BUREAU VERITAS, INTERNATIONAL REGISTER, ABU DHABI, U.A.E.

Visual Examination : SATISFACTORY Fillet Weld Fracture Test NOT APPLICABLESurface NDT : NOT APPLICABLE Charpy Vee Notch Test SATISFACTORYRadiography : SATISFACTORY Other Tests HARDNESS - OKTensile Test : SATISFACTORY OVERALL TEST RESULT ACCEPTABLEBend Test : SATISFACTORY We certify that the statements in the record above areMacro Examination : SATISFACTORY correct in accordance with the standard indicated above.

PREPARED BY REVIEWED BY APPROVED BY Name : KEITH HARMER Name : R. VAIRAMANI Name : S.E. LANGLEY

Sign : Sign : Sign :

Dept : ENGINEERING Dept : QA / QC Dept : BUREAU VERITAS

Date : 12 - JULY - 98 Date : 12 - JULY - 98 Date : 12 - JULY - 98

KH/Excel/Welding/BH/WPS011