zive electrochemical workstations · designing the solution for electrochemistry ... (*1) the...
TRANSCRIPT
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ZIVZIVEE Electrochemical WorkstationsElectrochemical Workstations
ZIVE SP1ZIVE SP1ZIVE SP1ZIVE SP1
Designing the Solution for ElectrochemistryPotentiostat/Galvanostat І Battery Cycler І Fuel Cell Test Station+82-2-578-6516 І [email protected] І www.zivelab.com І www.fctest.com
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FeaturesZIVE SP1ZIVE SP1
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FeaturesZIVE SP1ZIVE SP1
• Economical high quality potentiostat/galvanostat/impedance analyzer• Compact size with full functions & Smart LCD display• Wide current range(1A to 1nA) for various applications• Wide current range(1A to 1nA) for various applications• Supports fourteen(14) kind of EIS techniques• Current interrupt IR measurement/IR compensation• Pulse charge/discharge test available• Bipolar pulse capability• High speed data sampling time
- 50usec/sample in burst mode- 1msec/sample in normal mode1msec/sample in normal mode- 2usec/sample in fast sweep mode
• Internal 350,000 data point storage• Multichannel configuration available• Software packages
- Energy software package (BATe)- EIS software package (EISe)- Electrochemical analysis software package(EASe)y p g ( )- Corrosion software package (CORe)
• Free software package
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AppearanceFront ViewFront View
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AppearanceLCD Display – DC ModeLCD Display DC Mode
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AppearanceLCD Display – EIS ModeLCD Display EIS Mode
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AppearanceRear ViewRear View
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System Configuration
• System setup with multiple ZIVE SP1s• Connecting by USB hub
• System setup with one or more ZIVE product family• Connecting by USB hub
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When communication fails…
• When communication error occurs between ZIVE SP1 and PC the data will• When communication error occurs between ZIVE SP1 and PC, the data will be stored on the device memory.
• The data will be transferred to the PC after PC is restored.
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Strong Point (Hardware)
• Wide current range• Wide current range: Max. 1 Amp: Suitable for various application
• 3 measurement/control voltage range &/ g g10 measurement/control current range
• Independent operation by DSP with FPGA
• Built-in FRA : Impedance measurements available: No other device is needed.
• Compact size and light weight• Compact size and light weight: Small footprint: Suitable for field application
• Big memory capacityg y p y: 350,000 data point can be stored.
• One auxiliary voltage measurement available
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Available Techniques
• Potentiostatic• Galvanostatic• Double step potentiostatic• Double step galvanostatic• OCP measurement• Potential sweep• Current sweep• Cyclic voltammetry• Fast potential sweep• Potentiostatic Ru measurement • Galvanostatic Ru measurement
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Available Techniques
• Potentiostat EIS• Galvanostatic EIS• Pseudo galvanostatic EIS• OCP* EIS• Potentiodynamic PEIS• Galvanodynamic GEIS• Poteniodynamic HFR• Galvanodynamic HFR • Potentiostatic HFR monitor• Galvanostatic HFR monitor• Multisine potentiostatic EIS • Multisine galvanostatic EIS• Intermittent potentiostatic EIS • Intermittent galvanostatic EIS
(*1) The system measures open circuit potential before each frequency change and applies AC sinewave on this potential.
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Available Techniques
a) Battery test technique- CC/CV test for cycle life test of lithium battery - CC/CC tet for cycle life test of NiCd or NiMH battery - Discharging test- EVS(electrochemical voltage spectroscopy)- Variable scan rate CV- Potentiostatic IV curve- Galvanostatic IV curve- Steady state CV- PITT(Potentiostatic intermittent titration technique) test- GITT(Galvanostatic intermittent titration technique) test- Pulse mode is available for GSM & CDMA profile.
Pulse shape profile can be measured by user's demand.b) Control mode
- Charge : CC, CC-CV, pulse, sine wave- Discharge : CC, CP, CR, pulse, sine wave
c) Cut-off condition- Time, voltage, current, power, auxV etc.- Various battery charge/discharge test is available including
pulse discharge for GSM, CDMA application
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Available Techniques
• Tafel(Tafel experiment)• Rp(Polarization resistance)• RpEc trend• PDYN(Potentiodynamic)• CYPOL(Cyclic polarization resistance)• GDYN(GalvanoDynamic)• Reactivation• Galvanic corrosion• Potentiostatic ECN• Galvanostatic ECN• ZRA mode ECN
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Available Techniques
a) Step techniques- CA(Chronoamperometry)- CC(Chronocoulometry)- CP(Chronopotentiometry)
b) Sweep techniques- LSV(Linear sweep voltammetry)- SDV(Sampled DC voltammetry)- Fast CV- Fast LSV
c) Pulsed techniques- DPV(Differential pulse voltammetry)- SWV(Square wave voltammetry)- DPA(Diff.pulse amperometry)- NPV(Normal pulse voltammetry)- RNPV(Reverse normal pulse voltammetry)- DNPV(Differential normal pulse voltammetry)
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Applicable FieldMarket For the ProductMarket For the Product
Other Application- Coating evaluation- Heavy metal detection- Semiconductor- EDLC- Membrane- Bioelectrochemistry- Material testing etc.g
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SpecificationZIVE SP1ZIVE SP1
System
Cell cable 1 meter shielded type(standard)working, reference, counter, working sense, auxiliary V
ControlDAC
DSP with FPGA2x16bit DAC(50MHz) for bias & scan
Data acquisitionADC
2x16 bit ADCs(500kHZ) for voltage, current1x16bit ADCs(250kHz) for auxiliary readingADC 1x16bit ADCs(250kHz) for auxiliary reading
Calibration Automatic
Filter selection 4ea (5Hz, 1kHz, 500kHz, 5MHz)
Scan rate 0~200V/sec in common mode0~5000V/sec in fast mode
Max. channel no. 8 channels via USB connection
Internal data memory 350,000 points
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SpecificationZIVE SP1ZIVE SP1
Power Amplifier(CE)
Power 12Watt (12V@1A)
Compliance voltage ±12VCompliance voltage ±12V
Max. current ±1A
Control speed selection 4eap
Bandwidth 2MHz
Slew rate 10V/usec
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SpecificationZIVE SP1ZIVE SP1
Potentiostat Mode (Voltage Control)
Voltage Control
Control voltage range ±10V, ±1V, ±100mV
Voltage resolution 16 bit per each range
Voltage accuracy ±1mV, ±0.05% of setting(gain x1)
Max scan range ±10V vs ref EMax. scan range ±10V vs. ref. E
Current Measurement
Current range 10 ranges (auto/manual setting)100nA~1A1nA & 10nA with gain
Current resolution 16 bit30uA, 3uA, 300nA, 30nA, 3nA, 300pA,30uA, 3uA, 300nA, 30nA, 3nA, 300pA, 30pA, 3pA (300fA, 30fA with gain)
Current accuracy ±10pA ±0.1% f.s. (gain x1)>100nA f.s.
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SpecificationZIVE SP1ZIVE SP1
Galvanostat Mode (Current Control)
Current Control
Control current range max. ±1A± full scale depending on selected range± full scale depending on selected range
Current resolution 16 bit30uA, 3uA, 300nA, 30nA, 3nA, 300pA, 30pA, 3pA (300fA 30fA ith i )(300fA, 30fA with gain)
Current accuracy ±10pA ±0.1% f.s. (gain x1)>100nA f.s.
Voltage Measurement
Voltage range 10V, 1V, 100mV
Voltage resolution 16 bit0.3mV, 30uV, 3uV0.3mV, 30uV, 3uV
Voltage accuracy ±1mV ±0.05% of reading(gain x1)
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SpecificationZIVE SP1ZIVE SP1
EIS(Internal FRA) for System( ) y
Frequency range 10uHz ~ 1MHz
Frequency accuracy 0.01%
Frequency resolution 5000/decade
Amplitude 0.1mV ~ 5V rms (potentiostatic)f ( l )0.1 ~ 70% f.s. (Galvanostatic)
Mode Static EIS:Potentiostatic, Galvanostatic,Pseudogalvanostatic OCPPseudogalvanostatic, OCP
Dynamic EIS:Potentiodynamic, Galvanodynamic
Fixed Frequency Impedance:Potentiostatic GalvanostaticPotentiostatic, Galvanostatic,Potentiodynamic, Galvanodynamic
Multisine EIS:Potentiostatic, Galvanostatic
Intermittent PEIS/GEISIntermittent PEIS/GEIS
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SpecificationZIVE SP1ZIVE SP1
ElectrometerElectrometer
Max. input voltage ±10V
Input impedance 2x1013 Ω ιι 4.5pF
Bandwidth >22MHz
CMRR >114dB
Interface for System
Auxiliary port
Auxiliary voltage input 1 analog input: ±10V
Zero resistance ammeter 100nA ~ 1AZero resistance ammeter 100nA ~ 1A
External booster interface Via booster I/F cable
Sync terminal For channel synchronizing
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SpecificationZIVE SP1ZIVE SP1
SoftwareSoftware
Max. step per experiment 1000
Shutdown safety limits voltage, current, power, AuxV, etc.
Max. sampling rate 20kHz(50usec) in burst mode500kHz(2usec) in fast sweep mode
Max. sampling time unlimitedp g
Sampling condition Time, dV/dt, dI/dt, etc.
Main Systemy
PC communication USB 2.0 high speed
Line voltage 100~240VAC, 50/60Hz, 1Amp
Power adapter 24V, 2.5Amp
Size / Weight 160x330x81mm(WxDxH) / 2.05kg
Max. output power 15Watt
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SpecificationZIVE SP1ZIVE SP1
Smart LCD Display
DC mode Control value, E value, I valueE range, I range
EIS mode Frequency, Magnitude, PhaseE range, I range
Operation status Mode: PST, GST, ZRA, EIS, CC, CV, CP, CRStatus: Cell on Run ErrorStatus: Cell on, Run, Error
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SpecificationZIVE SP1ZIVE SP1
PC RequirementPC Requirement
Operating system Windows XP SP3/7/8/10(32bit/64bit OS)
PC ifi ti P ti 4 RAM 1GB hi hPC specification Pentium4, RAM 1GB or higher
Display 1600x900 high color or higher
USB High speed 2.0g p
General
Dummy cell One external dummy cell included
Impedance data analysis software ZMANTM software
DC data analysis software IVMANTM software
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Ordering Guide
Zi SP1Zive SP1- Comes with following items as standard
a) Cell cable with alligator clips, 1eab) Dummy cell, 1ea) AC/DC d t +24V 2 5A 1
Standard Systemc) AC/DC adapter, +24V 2.5A, 1ead) Power cord, 1eae) USB cable, 1eaf) Install CD, 1ea
Software Package- EIS software package (EISe)- Energy software package (BATe)gy p g ( )- Corrosion software package (CORe)- Electrochemical analysis software package (EASe)
Optional Booster I/F Cable, 1.5m
Optional Items
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Quick Start Guide
① Insert installation CD and click ‘Smart Manager’ ② The Smart Manager installation program will run① Insert installation CD and click Smart Manager button to install Smart Manager program.
② The Smart Manager installation program will run.- Follow the prompts through the rest of the
installation process.- If Microsoft visual C++2010 was not installed on
your PC, it will be installed. Or if VC++2010 wasy ,installed on your PC already, click cancel button.
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Quick Start Guide
③ Click LabView RTE2013 button which is needed ④ Install data analysis software packages③ Click LabView RTE2013 button, which is neededfor data analysis packages.
④ Install data analysis software packages.- Click ZMAN button to install EIS data analysis
software package- Click IVMAN button to install DC data analysis
software packagesoftware package- Click SIM4U button to install cyclic voltammetry
digital simulation software package
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Quick Start Guide
⑤ Plug in the ZIVE instrument’s power cord ⑥ Microsoft Windows will detect ZIVE instrument⑤ Plug in the ZIVE instrument s power cord.- Plug in the USB cable.- Plug in the cell cable.- Switch on the ZIVE instrument.
⑥ Microsoft Windows will detect ZIVE instrument.
l h ’Plug in the potentiostat’s power cord. Plug in the USB cable.
Run Device Manager on control panel.Double click on
Switch on the ZIVE SP1Plug in the cell cable.
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Thank o !Thank you !