aanalyst 600
DESCRIPTION
AAnalyst 600. ES Hwang Inorganic Product Specialist PerkinElmer Korea. Features Dedicated THGA furnace High sensitivity segmented solid-state photodiode detector Simultaneous measurement of sample and reference beams Transversely heated graphite furnace - PowerPoint PPT PresentationTRANSCRIPT
AAnalyst 600AAnalyst 600
ES HwangES Hwang
Inorganic Product SpecialistInorganic Product Specialist
PerkinElmer KoreaPerkinElmer Korea
AAnalyst 600…AAnalyst 600…
FeaturesFeatures• Dedicated THGA furnaceDedicated THGA furnace• High sensitivity segmented High sensitivity segmented
solid-state photodiode solid-state photodiode detectordetector
• Simultaneous measurement Simultaneous measurement of sample and reference of sample and reference beamsbeams
• Transversely heated graphite Transversely heated graphite furnace furnace
• Longitudinal Zeeman effect Longitudinal Zeeman effect background correction background correction
BenefitsBenefits THGA furnace reduces THGA furnace reduces
interferences in difficult matricesinterferences in difficult matrices Exceptional analytical performance Exceptional analytical performance
and detection limitsand detection limits Highest Long-term StabilityHighest Long-term Stability Minimized interferences and Minimized interferences and
memory effectsmemory effects Shorter analysis time (fast furnace Shorter analysis time (fast furnace
programs)programs) Best possible background Best possible background
correction with no light losscorrection with no light loss
… … the best dedicated THGA furnace systemthe best dedicated THGA furnace system
AAnalyst 600 AAnalyst 600 AA SpectrometersAA Spectrometers
AAnalyst 600 AAnalyst 600 Revolutionary Optical SystemRevolutionary Optical System
AAnalyst 600 AAnalyst 600 Unique FeaturesUnique Features
First AA spectrometerFirst AA spectrometer • Integrated furnaceIntegrated furnace
Zeeman-THGA graphite furnaceZeeman-THGA graphite furnace
AAnalyst 600 AAnalyst 600 Unique FeaturesUnique Features
First AA spectrometerFirst AA spectrometer• 8-8-lamp holderlamp holder
Automatic lamp selection and adjustment Automatic lamp selection and adjustment • Built-in power suppliesBuilt-in power supplies
Hollow cathode lampsHollow cathode lamps Electrodeless discharge lamps Electrodeless discharge lamps
AAnalyst 600AAnalyst 600Highly Versatile Furnace AutosamplerHighly Versatile Furnace Autosampler
User Benefits:User Benefits: Automatic generation Automatic generation
of reference solutionsof reference solutions Automatic multiple Automatic multiple
injectionsinjections Automatic dilutionAutomatic dilution Automatic injection Automatic injection
into a preheated tube into a preheated tube Variable pipetting Variable pipetting
speedspeed Ease-of-operationEase-of-operation
AAnalyst 600 AAnalyst 600 Revolutionary Optical SystemRevolutionary Optical System
Real time double beam system Real time double beam system
High sensitivity segmented solid-state photodiode High sensitivity segmented solid-state photodiode detectordetector• User Benefits:User Benefits:
Exceptional analytical performanceExceptional analytical performance Highest Long-term StabilityHighest Long-term Stability
AAnalyst 600 AAnalyst 600 Customized Solid-State DetectorCustomized Solid-State Detector
Highest quantum efficiency Integrated low noise CMOS
charge amplifier array Exceptional signal-to-noise ratio
AAnalyst 600 AAnalyst 600 Quantum Efficiency of DetectorsQuantum Efficiency of Detectors
photomultiplier
solid state detector
AAnalyst 600 AAnalyst 600 Furnace (THGA) Instrument Detection LimitsFurnace (THGA) Instrument Detection Limits
THGA Instrument detection limits (IDL) / pgTHGA Instrument detection limits (IDL) / pg
ElementElement PMT PMT PhotodiodePhotodiode
AsAs 9 9 66
CrCr 1.5 1.5 0.40.4
CuCu 5 5 44
MnMn 2 2 1.51.5
PbPb 3 3 3 3
TlTl 7.5 7.5 77
AAnalyst 600 AAnalyst 600 Automatic Lamp SelectorAutomatic Lamp Selector
8-Lamp holder Built-in power
supplies for hollow cathode and electrodeless discharge lamps
Automatic alignment, element, wavelength and slit selection
AAnalyst 600 AAnalyst 600 Unique Overall ConceptionUnique Overall Conception
Total system control Total system control via via AA WinLab32 software for AA WinLab32 software for highest versatility and simplest operating highest versatility and simplest operating convenienceconvenience• Atomizer controlAtomizer control• Lamp and lamp current controlLamp and lamp current control• THGA controlTHGA control• Accessory controlAccessory control
AAnalyst 600 AAnalyst 600 Unique Software ConceptionUnique Software Conception
Automatic system setup from stored user’s methodsAutomatic system setup from stored user’s methods• Direct from Direct from WorkspaceWorkspace
MethodMethod Sample informationSample information Individual screen design, window selection Individual screen design, window selection etcetc..
• User Benefits:User Benefits: Analytical reliability Analytical reliability Ease-of-operationEase-of-operation Time-savingTime-saving
Bringing a new level of productivity to high-performance AA
WinLab32 for AAWinLab32 for AA
AA WinLab32 - Features and BenefitsAA WinLab32 - Features and Benefits
Improve productivityImprove productivity• Data Reprocessing *Data Reprocessing *• WinLab32 Offline *WinLab32 Offline *• Priority samples *Priority samples *• Append to Analysis List *Append to Analysis List *• Edit CalibrationEdit Calibration• Recall CalibrationRecall Calibration• Furnace Method Development wizard *Furnace Method Development wizard *
Improve ease of use and reduce trainingImprove ease of use and reduce training• Tool tips (available in 6 languages) *Tool tips (available in 6 languages) *• Wizards *Wizards *• Analysis List *Analysis List *• AS-93 parameters integrated *AS-93 parameters integrated *
* New features not present in 16-bit AA WinLab
AA WinLab32 - Features and BenefitsAA WinLab32 - Features and Benefits
Reduce training and supportReduce training and support• Common look and feel with WinLab32 for ICP-OESCommon look and feel with WinLab32 for ICP-OES• CD Document PackCD Document Pack
Improve stability and data accessibilityImprove stability and data accessibility• Access database *Access database *
Method and data securityMethod and data security• Password protection *Password protection *• Multiple user levels *Multiple user levels *• Data check sums to detect changes *Data check sums to detect changes *• 21 CFR Part 11 Compliant21 CFR Part 11 Compliant
* New features not present in 16-bit AA WinLab
WinLab32 for AA WorkspaceWinLab32 for AA Workspace
Toolbar
Automated Analysis
Results
Status Monitor
Common look and feel with WinLab32 for ICP for easy cross platform trainingCommon look and feel with WinLab32 for ICP for easy cross platform trainingCommon look and feel with WinLab32 for ICP for easy cross platform trainingCommon look and feel with WinLab32 for ICP for easy cross platform training
Calibration
Data ReprocessingData Reprocessing
Recalculation of analytical data Recalculation of analytical data • Correct SIF errorsCorrect SIF errors• Change calibration functionChange calibration function• Delete replicate(s)Delete replicate(s)
Performed using the raw dataPerformed using the raw data Samples can be reprocessed in any sequenceSamples can be reprocessed in any sequence Original data are preservedOriginal data are preserved Analytical log can be printedAnalytical log can be printed Reprocessed data are identified Reprocessed data are identified
Data ReprocessingData Reprocessing
Select samples in the order you want them
reprocessed.
Status display
Change sample information in these
columns
Furnace Method Development WizardFurnace Method Development Wizard
Define FurnaceSteps to cycleTemperatures
Define SolutionsTo Analyze
Analyze Solutions and Display Results
Align Autosampler Tip WizardAlign Autosampler Tip Wizard
Auto dilution by systemAuto dilution by system
Priority SamplePriority Sample
Samples can be added without interrupting current analyses
Exporting Data to LABWORKSExporting Data to LABWORKS
Export data to LABWORKS
WinLab32 Enhanced Security OptionWinLab32 Enhanced Security Option
Enhancement to WinLab32 for AA (Enhancement to WinLab32 for AA (andand ICP) ICP) Significant set of new featuresSignificant set of new features
• Audit trailsAudit trails• File versioningFile versioning
Enable compliance with new regulationsEnable compliance with new regulations• 21 CFR Part 11 - Pharmaceutical21 CFR Part 11 - Pharmaceutical• 40 CFR Part 3 - Environmental (proposed)40 CFR Part 3 - Environmental (proposed)• OthersOthers
Primarily for highly regulated laboratoriesPrimarily for highly regulated laboratories• Users actions are restrictedUsers actions are restricted• Increased storage space requirementsIncreased storage space requirements• Additional information entry requirementsAdditional information entry requirements• Requires more system housekeepingRequires more system housekeeping
AAnalyst 600 AAnalyst 600 Total Range Graphite Furnace AATotal Range Graphite Furnace AA
THGA-type furnace with Zeeman-effect background THGA-type furnace with Zeeman-effect background correctioncorrection
User Benefits:User Benefits: Selection of the best system for individual Selection of the best system for individual
requirements and budgetsrequirements and budgets High performance, near interference-free trace High performance, near interference-free trace
analysis with STPF conceptanalysis with STPF concept
AAnalyst 600AAnalyst 600Integrated THGA Furnace SystemIntegrated THGA Furnace System
AAnalyst 600AAnalyst 600Zeeman THGA FurnaceZeeman THGA Furnace
Transversely heated graphite furnace Transversely heated graphite furnace
Longitudinal Zeeman effect background correction Longitudinal Zeeman effect background correction
User Benefits:User Benefits: Exceptional detection limitsExceptional detection limits Minimized interferences and memory effectsMinimized interferences and memory effects Best possible background correctionBest possible background correction Mimimum sample preparation timeMimimum sample preparation time Shorter analysis time (fast furnace programs)Shorter analysis time (fast furnace programs)
AAnalyst 600 AAnalyst 600 Integrated THGA SystemIntegrated THGA System
THGA Concept: more THGA Concept: more than 2500 systems in than 2500 systems in use use
Longitudinal Zeeman-Longitudinal Zeeman-Effect: highly resolved Effect: highly resolved background background compensation without compensation without light losslight loss
DC furnace power DC furnace power supplysupply
Closest approach Closest approach to the "ideal system" to the "ideal system"
AAnalyst 600 AAnalyst 600 Integrated THGA SystemIntegrated THGA System
0.000
0.025
0.050
0.075
0.100
0.125
0 1 2 3 4 5 6 7 8
Time / s
Ab
sorb
ance
AA-BG
BG
Atomic and background signals
for Ba, 20uL, 25 ug/L
AAnalyst 600AAnalyst 600 Zeeman Zeeman versus versus DD2 2 Background CorrectionBackground Correction
Background correction independent of wavelengthBackground correction independent of wavelength
True double-beam with only one optical pathTrue double-beam with only one optical path
Baseline noise at least 2x lowerBaseline noise at least 2x lower
Optical resolution Optical resolution is 100x better is 100x better
Char. mass typically 10 and 20 % poorer than with DChar. mass typically 10 and 20 % poorer than with D22 (the (the
mm00 for the worst case, Cu, is 50% poorer) for the worst case, Cu, is 50% poorer)
Zeeman-effect background correction gives superior Zeeman-effect background correction gives superior detection limits in real samplesdetection limits in real samples
AAnalyst 600 AAnalyst 600 Highly Versatile Furnace AutosamplerHighly Versatile Furnace Autosampler
High-capacity, interchangeable sample traysHigh-capacity, interchangeable sample trays88 88 or 146 sample positionsor 146 sample positions
Full AA WinLab32 control including multi-taskingFull AA WinLab32 control including multi-tasking
User Benefits:User Benefits: Automatic generation of reference solutionsAutomatic generation of reference solutions Automatic multiple injectionsAutomatic multiple injections Automatic dilutionAutomatic dilution Automatic injection into a preheated tube Automatic injection into a preheated tube Variable pipetting speedVariable pipetting speed Ease-of-operationEase-of-operation
AAnalyst 600AAnalyst 600Flow Injection - Furnace CouplingFlow Injection - Furnace Coupling
Optional accessory for coupling FI-MHS with furnace Optional accessory for coupling FI-MHS with furnace AAAA
Software controlled automatic operationSoftware controlled automatic operation
User Benefits:User Benefits: Detection limits in range of ng/LDetection limits in range of ng/L Time-savings by automatic on-line operationTime-savings by automatic on-line operation Less interferences since matrix components are Less interferences since matrix components are
removed in the FI systemremoved in the FI system
AAnalyst 600 AAnalyst 600 Automatic Slurry SamplingAutomatic Slurry Sampling
Optional ultrasonic probe integrated in the Optional ultrasonic probe integrated in the autosampler autosampler
Automatic introduction of solid samples as slurriesAutomatic introduction of solid samples as slurries
Full software controlFull software control
User Benefits:User Benefits: Reduced sample preparation and analysis timeReduced sample preparation and analysis time Reduced potential for contaminationReduced potential for contamination Easy operationEasy operation
What else can PerkinElmer offer?What else can PerkinElmer offer?
Sample Preparation SolutionsSample Preparation Solutions• Multiwave 3000 Multiwave 3000 • High Pressure Asher (HPA)High Pressure Asher (HPA)
Flow Injection Technology (FIAS)Flow Injection Technology (FIAS)• For sample pre-treatmentFor sample pre-treatment• Hydride generationHydride generation
Stand-alone Mercury systems (FIMS)Stand-alone Mercury systems (FIMS) Sample Introduction SystemsSample Introduction Systems
• AutodilutorsAutodilutors• Laser Ablation systemsLaser Ablation systems
World class service and supportWorld class service and support
Inorganic sample preparation….Inorganic sample preparation….
Multiwave 3000Multiwave 3000• Reduced digestion timesReduced digestion times• Superior digestion qualitySuperior digestion quality• Time-saving Time-saving • Easy operationEasy operation• Maximum safetyMaximum safety
High Pressure AsherHigh Pressure Asher• Complete sample Complete sample
mineralizationmineralization• Minimum organic residueMinimum organic residue• No elemental lossesNo elemental losses• No contaminationNo contamination
……a clear solution for sample preparation !a clear solution for sample preparation !
Multiwave 3000Multiwave 3000
HPA systemHPA system
FIAS – Flow Injection SystemsFIAS – Flow Injection Systems
2 2 ModelsModels• FIAS 100 (1 valve, 1 pump)FIAS 100 (1 valve, 1 pump)• FIAS 400 (1 valve, 2 pumps)FIAS 400 (1 valve, 2 pumps)
Automated sampling for Automated sampling for Flame AAFlame AA• DilutionDilution• Add reagents or modifiersAdd reagents or modifiers• Matrix removalMatrix removal• PreconcentrationPreconcentration
Improved sample handlingImproved sample handling• Small sample volumesSmall sample volumes• High solids samplesHigh solids samples
Hydride generationHydride generation• Determination of As, Se, Te, Determination of As, Se, Te,
Be, Sb, SnBe, Sb, Sn
FIAS 100 systemFIAS 100 system
FIAS 400 systemFIAS 400 system
Flow Injection Mercury SystemsFlow Injection Mercury Systems
FIMS 400FIMS 400• Determines Mercury via Determines Mercury via
Cold Vapor AA (CVAA)Cold Vapor AA (CVAA)
• Small footprintSmall footprint
• Fully automatedFully automated
• Easy to operateEasy to operate
• Stand alone systemStand alone system
• Cost effectiveCost effective
• Now with WinLab32 for AA Now with WinLab32 for AA softwaresoftware
AAnalyst 600 AAnalyst 600 ConclusionsConclusions
Not just another AA!Not just another AA!
No compromises!No compromises!
Easiest, simplest AA furnace Easiest, simplest AA furnace
Full automationFull automation
Full range of accessoriesFull range of accessories
Power of AA WinLab32 softwarePower of AA WinLab32 software
Ultimate in performanceUltimate in performance
The AA instrument to take you beyond 2000...The AA instrument to take you beyond 2000...