activity 01 finding the relative atomic mass of an unknowm metal by gas collection

1
1/30 © Pearson Education Ltd 2008 This document may have been altered from the original Practical activities have been checked for health and safety advice by CLEAPSS. All users will need to review the risk assessment information and may need to adapt it to local circumstances. Student Worksheet Activity 1: Finding the relative atomic mass of an unknown metal by gas collection Objective Be able to collect a gas from a reaction. Be able to measure the volume of a gas. Be able to calculate relative atomic mass. Equipment/materials 1.00 moldm –3 hydrochloric acid, HCl Weighing bottle Unknown metal, X Spatula Conical flask Delivery tube 250cm 3 measuring cylinder Bowl Mass balance 25cm 3 measuring cylinder Stand and clamp Safety Wear eye protection. Unknown metal is flammable. Hydrogen gas is flammable. No naked flames Highly flammable Procedure 1. Set up your apparatus as shown in the diagram. You must fill the measuring cylinder with water, cover the open end and place this under water in the bowl provided. 2. Place between 0.15g and 0.20g of the unknown metal in the conical flask. 3. Measure out 25.0cm 3 hydrochloric acid (HCl) and add this directly to the conical flask as quickly as possible, connecting the delivery tube to the flask immediately afterwards. 4. Ensure that all of the metal has reacted. 5. Collect the gas and record the final volume of hydrogen. Data Molar gas volume is 24000cm 3 at 298K and 101kPa (RTP) Equation for reaction: X + 2HCl XCl 2 + H 2 Analysis of results Calculate the amount, in mol, of hydrogen collected. Calculate the amount, in mol, of unknown metal, X, used. Calculate the relative atomic mass, A r , of X. Suggest an identity for X based on your value of A r and its observed reactivity. From the examiner… Record your weighings and gas volume measurement before you begin your calculations. Explain each line of your calculation as shown in the Analysis of Results section above. Consider how many significant figures to use within the calculation. Consider how many significant figures to use in your final answer. Questions 1. State a major procedural error for this experiment. 2. Suggest a modification which would reduce this major procedural error. 3. Calculate amounts in moles (using your value of A r for X) to show that the acid was in excess. 4. How would you modify the procedure if metal X was provided in lump form? 5. How could this experiment be modified to find the relative atomic mass of lithium? Diagram

Upload: a0938746599273927

Post on 28-Nov-2015

191 views

Category:

Documents


7 download

DESCRIPTION

Activity 01 Finding the Relative Atomic Mass of an Unknowm Metal by Gas Collection

TRANSCRIPT

Page 1: Activity 01 Finding the Relative Atomic Mass of an Unknowm Metal by Gas Collection

1/30 © Pearson Education Ltd 2008

This document may have been altered from the original

Practical activities have been checked for health and safety advice by CLEAPSS. All users will need to review the risk assessment information and may need to adapt it to local circumstances.

Student Worksheet

Activity 1: Finding the relative atomic mass of an unknown metal by gas collection

Objective • Be able to collect a gas from a reaction. • Be able to measure the volume of a gas. • Be able to calculate relative atomic mass.

Equipment/materials • 1.00 moldm–3 hydrochloric acid, HCl • Weighing bottle • Unknown metal, X • Spatula • Conical flask • Delivery tube • 250cm3 measuring cylinder • Bowl • Mass balance • 25cm3 measuring cylinder • Stand and clamp

Safety • Wear eye protection. • Unknown metal is flammable. • Hydrogen gas is flammable. • No naked flames

Highly flammable

Procedure 1. Set up your apparatus as shown in the diagram. You

must fill the measuring cylinder with water, cover the open end and place this under water in the bowl provided.

2. Place between 0.15g and 0.20g of the unknown metal in the conical flask.

3. Measure out 25.0cm3 hydrochloric acid (HCl) and add this directly to the conical flask as quickly as possible, connecting the delivery tube to the flask immediately afterwards.

4. Ensure that all of the metal has reacted. 5. Collect the gas and record the final volume of

hydrogen.

Data Molar gas volume is 24000cm3 at 298K and 101kPa (RTP) Equation for reaction: X + 2HCl XCl2 + H2

Analysis of results • Calculate the amount, in mol, of hydrogen collected.

Calculate the amount, in mol, of unknown metal, X, used.

• Calculate the relative atomic mass, Ar, of X. • Suggest an identity for X based on your value of Ar

and its observed reactivity.

From the examiner… • Record your weighings and gas volume

measurement before you begin your calculations. • Explain each line of your calculation as shown in the

Analysis of Results section above. • Consider how many significant figures to use within

the calculation. • Consider how many significant figures to use in your

final answer.

Questions 1. State a major procedural error for this experiment. 2. Suggest a modification which would reduce this major procedural error. 3. Calculate amounts in moles (using your value of Ar for X) to show that the acid was in excess. 4. How would you modify the procedure if metal X was provided in lump form? 5. How could this experiment be modified to find the relative atomic mass of lithium?

Diagram