acz laboratories, inc.recycle4colorado.ipower.com/energyfuels/2014/2013... · acz 10 type analyzed...

--- -

ACZ Laboratories, Inc. 2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493

Inorganic QC Summary

Energy Fuels Resources (USA) Inc. ACZ Project ID: L12392

Alkalinity as CaC03 SM2320B - Titration

ACZ 10 Type Analyzed PCN/SCN QC Sample Found Units Rec Lower Upper RPO Limit Qual

WG345123

WG345123PBW1 PBW 06/06/13 16:19

WG345123LCSW2 LCSW 06/06/13 16:33 WC130601- 820.0001

L 12399-04DUP DUP 06/06/13 18:26

WG345123LCSW5 LCSW 06/06/13 20:10 WC130601- 820.0001

WG345123PBW2 PBW 06/06/13 20:18

WG345123LCSW8 LCSW 06/06/13 23:50 WC130601- 820.0001

WG345123PBW3 PBW 06/06/13 23:59

WG345123LCSW11 LCSW 06/07/13 3 33

WG345123PBW4 PBW 06/07/13 342

WG345123LCSW14 LCSW 06/07/13 7:01

Aluminum, dissolved

WC130601- 820.0001

WC130601- 820.0001

M200.71CP

479

u 754.1

mg/L

mg/L

499.6 mg/L

784,5 mg/L

2.2 mg/L

767.9 mg/L

U mg/L

789.3

2.3

795.6

mg/L

mg/L

mg/L

92

95.7

93.6

96.3

97

-20

90

90

-20

90

-20

90

-20

90

20

110

110

20

110

20

110

20

110

4.2 20


WG345759

WG3457591CV

WG345759ICB

WG345759PQV

WG345759SIC

WG345759LFB

L 12392-01AS

L 12392-01ASD

WG345759CCV1

WG345759CCB1

WG345759CCV2

WG345759CCB2

WG345759CCV3

WG345759CCB3

ICV 06/17/1314:40 11130510-1 2

ICB 06/17/13 14:46

PQV 06/17/1314:50 11130613-5 ,150165

SIC

LFB

AS

ASD

06/17/131453 11130614-1 200.370165

06/17/1314:59 11130617-2 1.0011

06/17/1315:05 11130617-2 1 0011

06/17/1315:08 11130617-2

CCV 06/17/13 15:30 11130514-2

CCB 06/17/13 15:33

CCV 06/17/13 16:08 11130514-2

CCB 06/17/1316:11

CCV 06/17/13 16:30 11130514-2

CCB 06/17/13 16:33

Arsenic, dissolved M200.8 ICP-MS

u u

2,039

u .156

mg/L

mg/L

mg/L

206.6 mg/L

1.025 mg/L

1.027 mg/L

1.037 mg/l

1.027 mg/L

U mg/L

1.014 mg/L

U mg/L

1 013 mg/L

U mg/L

102

103.9

103.1

102.4

102.6

103,6

102.7

101 .4

101 ,3

95

-0.09

70

85

85

85

90

-0.09

90

-0.09

90

-0.09

105

0.09

130

200

115

115

115

110

0.09

110

0.09

110

0.09

0.97 20

ACZ ID Type Analyzed PCN/SCN QC Sample Found Units Rec Lower Upper RPD Limit Qual

ICV 06/12/13 14:29 MS130416-2 .05

ICB 06/12/1314:32

CCV 06/12/13 15:19 MS130510-4 1001

CCB 06/12/13 15:23

WG345415

WG3454151CV

WG3454151CB

WG345415CCV1

WG345415CCB1

WG345415LFB

L 12392-02AS

LFB

AS

ASD

06/12/1315:26 MS130508-1 .05005

06/12/1315:36 MS130508-1 .05005

L 12392-02ASD 06/12/1315:39 MS130508-1 .05005

WG345415CCV2 CCV 06/12/13 16:00 MS130510-4 .1001

WG345415CCB2 CCB 06/12/1316:03

WG345415CCV3 CCV 06/12/13 16:40 MS130510-4 .1001

WG345415CCB3 CCB 06/12/13 16:43

WG345415CCV4 CCV 06/12/13 17:03 MS130510-4 .1001

WG345415CCB4 CCB 06/12/13 17:07

REPIN.01 .06.05.01

.05184 mg/L

U mg/L

1052 mg/L

U mg/L

.04849 mg/L

,0043 .0573 mg/L

0043 .05579 mg/L

,1028 mg/L

U mg/L

.101 mg/L

U mg/L

.1032 mg/L

U mg/L

103.7 90 110

-0.0006 0.0006

105.1 90 110

96 9

105 9

102.9

-0.0006 0.0006

85

70

70

115

130

130

102 7 90 110

-0.0006 0.0006

100 9 90 110

-0 0006 0.0006

103.1 90 110

-0 0006 0.0006

2-67 20

Page 7 of29

- -




Barium, dissolved M200.7 ICP


WG345759

WG3457591CV

WG3457591CB

WG345759PQV

WG345759SIC

WG345759LFB

L 12392-01AS

L 12392-01 ASD

WG345759CCV1

WG345759CCB1

WG345759CCV2

WG345759CCB2

WG345759CCV3

WG345759CCB3

Boron, dissolved

ICV

ICB

PQV

SIC

LFB

AS

ASD

CCV

CCB

06/17/13 14:40

06/17/13 14:46

06/17/13 14:50

06/17/13 14:53

06/17/13 14:59

06/17/13 15:05

06/17/13 15:08

06/17/13 15:30

06/17/13 15:33

11130510-1

11130613-5

11130614-1

11130617-2

11130617-2

11130617-2

11130514-2

CCV 06/17/13 16:08 11130514-2

CCB 06/17/1316:11

CCV 06/17/13 16:30 11130514-2

CCB 06/17/13 16:33

M200.71CP

2

015

.1

.5

.5

.5

.012

.012

2 0205

u .0151

.0976

.5071

.514

.514

1-023

u 1.02

u 1.028

u

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

101

100.7

97_6

101 _4

100 4

100 4

102.3

102

102.8

95

-0.009

70

80

85

85

85

90

-0.009

90

-0.009

90

-0.009

105

0_009

130

120

115

115

115

110

0 009

110

0_009

110

0.009

0 20


WG345759

WG3457591CV

WG3457591CB

WG345759PQV

WG345759SIC

WG345759LFB

L 12392-01AS

L 12392-01ASD

WG345759CCV1

WG345759CCB1

WG345759CCV2

WG345759CCB2

WG345759CCV3

WG345759CCB3

ICV 06/17/13 14:40 11130510-1

ICB 06/17/13 14:46

PQV 06/17/13 14:50 11130613-5

SIC 06/17/13 14:53 11130614-1

LFB 06/17/13 14:59 11130617-2

AS 06/17/13 15:05 11130617-2

ASD 06/17/13 15:08 11130617-2

CCV 06/17/13 15:30 11130514-2

CCB 06/17/13 15:33

CCV 06/17/13 16:08 11130514-2

CCB 06/17/1316:11

CCV 06/17/13 16:30 11130514-2

CCB 06/17/13 16:33

2

,05005

.1001

5005

.5005

.5005

Cadmium, dissolved M200.8 ICP-MS

33

.33

2.037

u .057

.095

52

822

.828

1.023

u 1.02

u 1.022

u

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

101 .9

113.9

94.9

103.9

98.3

99.5

102.3

102

102.2

95

-0.03

70

80

85

85

85

90

-0.03

90

-0.03

90

-0.03

105

0.03

130

120

115

115

115

110

0.03

110

0.03

110

0.03

0.73 20


WG345415

WG3454151CV

WG3454151CB

WG345415CCV1

WG345415CCB1

WG345415LFB

L 12392-02AS

ICV 06/12/1314:29 MS130416-2

ICB 06/12/13 14:32

CCV 06/12/13 15:19 MS130510-4

CCB 06/12/1315:23

LFB 06/12/1315:26 MS130508-1

AS 06/12/13 15:36 MS130508-1

L 12392-02ASD ASD 06/12/13 15:39 MS130508-1

WG345415CCV2 CCV 06/12/13 16:00 MS130510-4

WG345415CCB2 CCB 06/12/13 16:03

WG345415CCV3 CCV 06/12/1316:40 MS130510-4

WG345415CCB3 CCB 06/12/13 16:43

WG345415CCV4 CCV 06/12/1317:03 MS130510-4

WG345415CCB4 CCB 06/12/13 17:07

REPIN.01 ,06.05.01

.05

.1002

.0501

.0501

.0501

.1002

.1002

.1002

u u

.0511 mg/L 102.2 90 110

U mg/L -0.0003 0.0003

,1028 mg/L 102.6 90 110

U mg/L -0.0003 0.0003

.04797 mg/L 95.7 85 115

.04701 mg/L 93.8 70 130

.04766 mg/L 95.1 70 130 1.37 20

.1019 mg/L 101.7 90 110

U mg/L -0.0003 0.0003

09992 mg/L 99.7 90 110

U mg/L -0.0003 0,0003

09973 mg/L 99.5 90 110

U mg/L -0.0003 0, 0003

Page 8 of 29


Energy Fuels Resources (USA) Inc.

Calcium, dissolved M200.71CP


ACZ Project ID: L12392


WG345759

WG3457591CV

WG3457591CB

WG345759PQV

ICV

ICB

06/17/1314:40 11130510-1

06/17/13 14:46

PQV 06/17/13 14:50 11130613-5

WG345759SIC SIC 06/17/13 14:53 11130614-1

WG345759LFB LFB 06/17/1314:59 11130617-2

L 12392-01AS AS 06/17/13 15:05 11130617-2

L12392-01ASD ASD 06/17/1315:08 11130617-2

WG345759CCV1 CCV 06/17/13 15:30 11130514-2

WG345759CCB1 CCB 06/17/13 15:33

WG345759CCV2 CCV 06/17/13 16:08 11130514-2

WG345759CCB2 CCB 06/17/1316:11

WG345759CCV3

WG345759CCB3

CCV 06/17/13 16:30 11130514-2

CCB 06/17/13 16:33

Carbon, total organic (TOC) SM5310B

100

201.08

67.95918

67.95918

67.95918

50

50

50

62.7

62.7

99.33 mg/L

U mg/L

1.07 mg/L

198.5 mg/L

69.12 mg/L

128 7 mg/L

128.6 mg/L

50.33 mg/L

U mg/L

49.82 mg/L

U mg/L

49.81

u mg/L

mg/L

99.3

107

98.7

101 .7

97,1

97

100.7

99.6

99.6

95

-0.6

70

1

85

85

85

90

-0.6

90

-0.6

90

-0.6

105

06

130

200

115

115

115

110

0.6

110

0.6

110

0.6

0.08 20


WG344901

WG3449011CV1

WG3449011CB1

. WG345633

WG345633CCV1

WG345633CCB1

WG345633PQV

WG345633LFB

L 12293-02DUP

L 12294-01AS

ICV

ICB

06/06/1314:07 Wl130425-2

06/06/13 14:07

CCV 06/14/13 11 :52 W1130605-5

CCB 06/14/1311:52

PQV 06/14/1311 :52 Wl130613-1

LFB 06/14/1311:52 Wl130506-1

DUP 06/14/13 11:52

AS 06/14/1311:52 Wl130506-1

WG345633CCV2 CCV 06/14/1311:52 Wl130605-5

WG345633CCB2 CCB 06/14/13 11 :52

WG345633CCV3 CCV 06/14/13 11:52 Wl130605-5

WG345633CCB3 CCB 06/14/13 11 :52

WG345633CCV4 CCV 06/14/13 11 :52 Wl130605-5

WG345633CCB4 CCB 06/14/13 11 :52

100

50

5

50

50

50

50

50

Cesium, dissolved M200.8 ICP-MS

6.7

6.9

100.1

u

50.9

u 5.9

52.7

8.9

55.4

52.4

u 50.8

u 52.8

u

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

100.1

101 .8

118

105.4

97

104.8

101 .6

105.6

90

-3

90

-3

70

90

90

90

-3

90

-3

90

-3

110

3

110

3

130

110

110

110

3

110

3

110

3

28 2 20


WG345415

WG3454151CV

WG3454151CB

WG345415CCV1

WG345415CCB1

WG345415LFB

L 12392-02AS

L 12392-02ASD

WG345415CCV2

WG345415CCB2

WG345415CCV3

WG345415CCB3

ICV 06/12/1314:29 MS130416-2

ICB 06/12/1314:32

CCV 06/12/1315:19 MS130510-4

CCB 06/12/13 15:23

LFB 06/12/13 15:26 MS130508-1

AS 06/12/1315:36 MS130508-1

ASD 06/12/1315:39 MS130508-1

CCV 06/12/1316:00 MS130510-4

CCB 06/12/1316:03

CCV 06/12/1316:40 MS130510-4

CCB 06/12/13 16:43

.05

.1

.05

.05

.05

.1

.1

u u

.05217 mg/L

U mg/L

.1032 mg/L

U mg/L

.04894 mg/L

.04898 mg/L

.04981 mg/L

.1028 mg/L

U mg/L

.1019 mg/L

U mg/L

104.3 90 110

-0.0006 0.0006

103.2 90 110

-0.0006 0,0006

97.9 85 115

98 70 130

99.6 70 130 1.68 20

102.8 90 110

-0.0006 0.0006

101.9 90 110

-0.0006 0.0006

RA

REPIN.01.06.05.01 Page 9 of 29

ACZ Laboratories, Inc. 2773 Downhill Drive Steamboat Springs, CO 80487 (BOO) 334-5493

I - Inorganic ac Summary


Chloride SM4500CI-E


WG345779

WG3457791CB ICB 06/17/13 14:51

WG3457791CV ICV 06/17/13 14:51 Wl130131-1

WG345779CCV1 CCV 06/17/1315:06 Wl130211-1

WG345779CCB1 CCB 06/17/13 15:06

WG345779LFB1 LFB 06/17/1315:06 Wl130201-8

WG345779CCV2 CCV 06/17/1315:07 Wl130211-1

WG345779CCB2 CCB 06/17/1315:07

WG345779CCV3 CCV 06/17/1315:08 Wl130211-1

WG345779CCB3 CCB 06/17/13 15:08

WG345779CCV4 CCV 06/17/1315:14 Wl130211-1

WG345779CCB4 CCB 06/17/1315:14

WG345779LFB2 LFB 06/17/13 15:15 Wl130201-8

WG345779CCV5 CCV 06/17/1315:15 Wl130211-1

WG345779CCB5 CCB 06/17/13 15:15

WG345779CCV6 CCV 06/17/1315:16 Wl130211-1

WG345779CCB6 CCB 06/17/13 15:17

DUP 06/17/13 15:23 L 12334-02DUP

WG345779CCV7

WG345779CCB7

WG345779CCV8

WG345779CCB8

CCV 06/17/1315:23 Wl130211-1

CCB 06/17/13 15:23

CCV 06/17/1315:24 Wl130211-1

CCB 06/17/13 15:24

WG345779CCV9 CCV 06/17/1315:32 Wl130211-1

WG345779CCB9 CCB 06/17/13 15:32

L 12334-01AS AS 06/17/1315:35 10XCL

WG345779CCV10 CCV 06/17/1315:35 Wl130211-1

WG345779CCB10 CCB 06/17/13 15:35

WG345779CCV11 CCV 06/17/1315:49 Wl130211-1

WG345779CCB11 CCB 06/17/1315:49

WG345779CCV12 CCV 06/17/1315:50 Wl130211-1

WG345779CCB12 CCB 06/17/13 15:50

Chromium, dissolved M200.71CP

54.945

50

30

50

50

50

30

50

50

50

50

50

30

50

50

50

790

850

u 58.2

52.1

u 30.9

52.6

u 52.6

u 52.9

u 31 .3

52.5

u 52.5

u 797

52.3

u 52.5

u 52.3

u 846

52

u 52

u 51 .8

u

mg/L

mg/L 105.9

mg/L 104.2

mg/L

mg/L 103

mg/L 105.2

mg/L

mg/L 105.2

mg/L

mg/L 105.8

mg/L

mg/L 104.3

mg/L 105

mg/L

mg/L 105

mg/L

mg/L

mg/L 104.6

mg/L

mg/L 105

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

104.6

-13.3

104

104

103.6

-3

90

90

-3

90

90

-3

90

-3

90

-3

90

90

-3

90

-3

90

-3

90

-3

90

-3

90

90

-3

90

-3

90

-3

3

110

110

3

110

110

3

110

3

110

3

110

110

3

110

3

110

3

110

3

110

3

110

110

3

110

3

110

3

0.9 20


WG345759

WG3457591CV

WG3457591CB

WG345759PQV

WG345759SIC

WG345759LFB

L 12392-01AS

L12392-01ASD

WG345759CCV1

WG345759CCB1

WG345759CCV2

WG345759CCB2

WG345759CCV3

WG345759CCB3

ICV 06/17/1314:40 11130510-1

ICB 06/17/13 14:46

PQV 06/17/1314:50 11130613-5

SIC 06/17/13 14:53 11130614-1

LFB 06/17/1314:59 11130617-2

AS 06/17/13 15:05 11130617-2

ASD 06/17/13 15:08 11130617-2

CCV 06/17/13 15:30 11130514-2

CCB 06/17/13 15:33

CCV 06/17/1316:08 11130514-2

CCB 06/17/1316:11

CCV 06/17/1316:30 11130514-2

CCB 06/17/13 16:33

2

.05

.1

.5

.5

.5

u u

1.968 mg/L

U mg/L

.05 mg/L

.094 mg/L

.502

.492

.496

1

u .991

u .987

u

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

98.4

100

94

100.4

98.4

99.2

100

99.1

98.7

95

-0.03

70

80

85

85

85

90

-0.03

90

-0.03

90

-0.03

105

0.03

130

120

115

115

115

110

0.03

110

0.03

110

0.03

0.81 20

M3

REPIN.01.06.05.01 Page 10 of 29



Copper, dissolved M200.71CP




WG345759

WG3457591CV

WG3457591CB

WG345759PQV

WG345759SIC

WG345759LFB

L 12392-01AS

L 12392-01ASD

ICV 06/17/13 14:40 11130510-1

ICB 06/17/13 14:46

PQV 06/17113 14:50 11130613-5

SIC 06/17/13 14:53 11130614-1

LFB

AS

06/17/13 14:59 11130617-2

06/17/1315:05 11130617-2

ASD 06/17/1315:08 11130617-2

WG345759CCV1 CCV 06/17/1315:30 11130514-2

WG345759CCB1 CCB 06/17/1315:33

WG345759CCV2 CCV 06/17/13 16:08 11130514-2

WG345759CCB2 CCB 06/17/1316:11

WG345759CCV3 CCV 06/1 7/13 16:30 11130514-2

WG345759CCB3 CCB 06117/13 16:33

Fluoride SM4500F-C

2

05

.1

.5

.5

.5

u u

1.958 mg/L

U mg/L

.05 mg/L

.1 mg/L

97.9

100

100

.503

.492

.496

.991

mg/L 100.6

u .989

u .993

u

mg/L 98.4

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

99.2

99.1

98.9

99.3

95

-0 03

70

eo 85

85

65

90

-0.03

90

-0.03

90

-0.03

105

0.03

130

120

115

115

115

110

0.03

110

0.03

110

0.03

0.81 20


WG345355

WG3453551CV

WG3453551CB

WG345407

WG345407CCV1

WG345407CCB1

WG345407PQV

WG345407LFB1

L12329-01AS

L12329-01DUP

ICV

ICB

06/11/1310:47 WC130606-

06/11 /1310:51

CCV 06/11/13 16:03 WC130606-

CCB 06/11/13 16:08

PQV 06/11/1 3 16:11 WC130610-

LFB 06/11/1316:14 WC130313-

AS 06/11/1316:21 WC130313-

DUP 06/11/13 16:24

WG345407CCV2 CCV 06/11/1316:50 WC130606-

WG345407CCB2 CCB 06/11/13 16:57

WG345407CCV3 CCV 06/11/1317:33 WC130606-

WG345407CCB3 CCB 06/11/1317:40

WG345407LFB2 LFB 06/11/1317:59 WC130313-

WG345407CCV4 CCV 06/11/1316:22 WC130606-

WG345407CCB4 CCB 06/11/13 16:30

WG345407CCV5 CCV 06/11/1319:02 WC130606-

WG345407CCB5 CCB 06/11/1319:10

WG345407CCV6 CCV 06/11/1319:46 WC130606-

WG345407CCB6 CCB 06/11/13 19:54

WG345407CCV6 CCV 06/11/13 20:03 WC130606-

WG345407CCB6 CCB 06/11/13 20:11

2.002

2.002

.5005

5.005

5.005

2.002

2.002

5.005

2.002

2.002

2.002

2 002

u u

1.96

u

1.86

u .44

4.61

4.69

u 1.93

u 1.97

u 4.67

1.96

u 2.02

u 2

u 2.01

u

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

97.9

92.9

87.9

92.1

93.7

mg/L 96.4

mg/L

mg/L 98.4

mg/L

mg/L 93.3

mg/L 97.9

mg/L

mg/L 100.9

mg/L

mg/L 99.9

mg/L

mg/L 100.4

mg/L

95

-0.3

90

-0.3

70

90

90

90

-0.3

90

-0.3

90

90

-0.3

90

-0.3

90

-0.3

90

-0.3

105

0.3

110

0.3

130

110

110

110

0.3

110

0.3

110

110

0.3

110

0.3

110

0.3

110

0.3

0 20 RA

REPIN.01.06.05.01 Page 11 of 29



Iron, dissolved M200.7 ICP


-- - -- -



WG345759

WG3457591CV

WG3457591CB

WG345759PQV

WG345759SIC

WG345759LFB

L 12392-01AS

L 12392-01ASD

ICV 06/17/1314:40 11130510-1 2

ICB 06/17/13 14:46

PQV 06/17/13 14:50 11130613-5 .05007

SIC 06/17/13 14:53 11130614-1 200,33007

LFB

AS

ASD

06/17/13 14:59 11130617-2

06/17/13 15:05 11130617-2

06/17/1315:08 11130617-2

WG345759CCV1 CCV 06/17/13 15:30 11130514-2

WG345759CCB1 CCB 06/17/13 15:33

WG345759CCV2 CCV 06/17/13 16:08 11130514-2

WG345759CCB2 CCB 06/17/1316:11

WG345759CCV3 CCV 06/17/13 16:30 11130514-2

WG345759CCB3 CCB 06/17/13 16:33

Lead, dissolved M200.8 ICP-MS

u u

2.007 mg/L

U mg/L

.048 mg/L

191.9 mg/L

1.023

1.015

1.015

mg/L

mg/L

mg/L

1.019 mg/L

U mg/L

1.009 mg/L

U mg/L

1.008 mg/L

U mg/L

100A

95.9

95.8

102.3

101.5

101.5

101 _9

100_9

100_8

95

-0.06

70

1

85

85

85

90

-0.06

90

-0.06

90

-0.06

105

0.06

130

200

115

115

115

110

0.06

110

0.06

110

0_06

0 20


WG345415

WG3454151CV

WG3454151CB

WG345415CCV1

WG345415CCB1

WG345415LFB

L 12392-02AS

L 12392-02ASD

ICV 06/12/13 14:29 MS130416-2 .05

ICB 06/12/13 14:32

CCV 06/12/13 15:19 MS130510-4 .25025

CCB 06/12/13 15:23

LFB

AS

ASD

06/12/13 15:26 MS130508-1 .05005

06/12/13 15:36 MS130508-1 .05005

06/12/13 15:39 MS130508-1 ,05005

WG345415CCV2 CCV 06/12/13 16:00 MS130510-4 ,25025

WG345415CCB2 CCB 06/12/13 16:03

WG345415CCV3 CCV 06/12/1316:40 MS130510-4 ,25025

WG345415CCB3 CCB 06/12/13 16:43

WG345415CCV4 CCV 06/12/1317:03 MS130510-4 .25025

WG345415CCB4 CCB 06/12/1317:07

Magnesium, dissolved M200.71CP

u u

,05277 mg/L

U mg/L

2572 mg/L

U mg/L

.04885 mg/L

.04969 mg/L

,05018 mg/L

2564

u .2543

u .2551

u

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

105.5 90 110

-0.0003 0.0003

102.8 90 110

97.6

99.3

100.3

-0.0003 0,0003

85

70

70

115

130

130

102.5 90 110

-0.0003 0,0003

101.6 90 110

-0.0003 0.0003

101 .9 90 110

-0.0003 0,0003

0.98 20

ACZ 10 Type Analyzed PCN/SCN QC Sample Found Units Rec Lower Upper RPD Limit Qual

WG345759

WG3457591CV

WG3457591CB

WG345759PQV

WG345759SIC

WG345759LFB

L 12392-01AS

L 12392-01ASD

WG345759CCV1

WG345759CCB1

WG345759CCV2

WG345759CCB2

WG345759CCV3

WG345759CCB3

REPIN.01 .Q6.0?,01

ICV 06/17/13 14:40 11130510-1

ICB 06/17/13 14:46

PQV 06/17/1314:50 11130613-5

SIC 06/17/13 14:53 11130614-1

LFB 06/17/1314:59 11130617-2

AS 06/17/1315:05 11130617-2

ASD 06/17/1315:08 11130617-2

CCV 06/17/13 15:30 11130514-2

CCB 06/17/1315:33

CCV 06/17/1316:08 11130514-2

CCB 06/17/13 16:11

CCV 06/17/1316:30 11130514-2

CCB 06/17/13 16:33

100

1 0007

201.1407

49 99941

49 99941

49.99941

50

50

50

72.3

72.3

98.98 mg/L

U mg/L

1.12 mg/L

205.8 mg/L

48.94 mg/L

118.8

118.9

49.55

u 48,92

u 48.85

u

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

99

111.9

102.3

97.9

93

93.2

99.1

97.8

97.7

95

-0.6

70

1

85

85

85

90

-0.6

90

-0.6

90

-0.6

105

0.6

130

200

115

115

115

110

0.6

110

06

110

06

0.08 20

Page 12 of 29

• I

lnorgamc QC Summary



Manganese, dissolved M200.71CP


WG345759

WG3457591CV ICV 06/17/13 14:40 11130510-1 2 1,9818 mg/L 991 95 105

WG3457591CB ICB 06/17/13 14:46 u mg/L -0.015 0.015

WG345759PQV PQV 06/17/1314:50 11130613-5 .025 .0248 mg/L 99,2 70 130

WG345759SIC SIC 06/17/13 14:53 11130614-1 50.025 47 69 mg/L 95 3 1 200

WG345759LFB LFB 06/17/13 14:59 11130617-2 .5 5164 mg/L 103 3 85 115

L 12392-01AS AS 06/17/1315:05 11130617-2 .5 u .5035 mg/L 100.7 85 115

L12392-01ASD ASD 06/17/13 15:08 11130617-2 .5 u .507 mg/L 101.4 85 115 0,69 20

WG345759CCV1 CCV 06/17/13 15:30 11130514-2 1 013 mg/L 101 3 90 110

WG345759CCB1 CCB 06/17/13 15:33 u mg/L -0.015 0.015

WG345759CCV2 CCV 06/17/13 16:08 11130514-2 1 9999 mg/L 100 90 110

WG345759CCB2 CCB 06/17/1316:11 u mg/L -0.015 0 015

WG345759CCV3 CCV 06/17/13 16:30 11130514-2 9983 mg/L 99.8 90 110

WG345759CCB3 CCB 06/17/13 16:33 u mg/L -0,015 0 015

Mercury, dissolved M245.1 CVAA


WG344958

WG3449581CV ICV 06/06/13 1 0:18 11130522-4 .005025 ,00484 mg/L 96.3 90 110

WG3449581CB ICB 06/06/13 10:20 u mg/L -0.0006 0.0006

WG344959

WG344959CCV1 CCV 06/06/13 11:14 11130522-4 005025 .00482 mg/L 95,9 90 110

WG344959CCB1 CCB 06/06/13 11:17 u mg/L -0.0002 0.0002

WG344959LRB LRB 06/06/13 11:19 u mg/L -0.00044 0.00044

WG344959LFB LFB 06/06/13 11 :21 11130515-2 .002002 .00192 mg/L 95.9 85 115

WG344959CCV2 CCV 06/06/13 11 :42 11130522-4 .005025 .00491 mg/L 97.7 90 110

WG344959CCB2 CCB 06/06/13 11 :44 u mg/L -0.0002 0.0002

L 12288-02LFM LFM 06/06/13 12:06 11130515-2 002002 u .00176 mg/L 87.9 85 115

WG344959CCV3 CCV 06/06/13 12:08 11130522-4 005025 .00488 mg/L 97.1 90 110

WG344959CCB3 CCB 06/06/13 12:11 u mg/L -0 0002 0.0002

L 12288-02LFMD LFMD 06/06/13 12:13 11130515-2 .002002 u .00182 mg/L 90,9 85 115 3.35 20

WG344959CCV4 CCV 06/06/13 12:25 11130522-4 005025 .00489 mg/L 97.3 90 110

WG344959CCB4 CCB 06/06/13 12:27 u mg/L -0.0002 0.0002

REPIN.01.06.05.01 Page 13 of 29


Inorganic QC I

Summary


Molybdenum, dissolved M200.71CP


WG345759

WG3457591CV ICV 06/17/13 14:40 11130510-1 2 2.006 mg/L 100.3 95 105

WG3457591CB ICB 06/17/13 14:46 u mg/L -0.06 0.06

WG345759PQV PQV 06/17/13 14:50 11130613-5 .1 .101 mg/L 101 70 130

WG345759SIC SIC 06/17/13 14:53 11130614-1 .2 .182 mg/L 91 80 120

WG345759LFB LFB 06/17/13 14:59 11130617-2 .5 .497 mg/L 99.4 85 115

L 12392-01AS AS 06/17/1315:05 11130617-2 .5 u .5 mg/L 100 85 115

L12392-01ASD ASD 06/17/13 15:08 11130617-2 .5 u .503 mg/L 100.6 85 115 0.6 20

WG345759CCV1 CCV 06/17/13 15:30 11130514-2 1.019 mg/L 101.9 90 110

WG345759CCB1 CCB 06/17/13 15:33 u mg/L -0.06 0.06

WG345759CCV2 CCV 06/17/13 16:08 11130514-2 1.008 mg/L 100.8 90 110

WG345759CCB2 CCB 06/17/1316:11 u mg/L -0.06 0 06

WG345759CCV3 CCV 06/17/13 16:30 11130514-2 1.005 mg/L 100.5 90 110

WG345759CCB3 CCB 06/17/13 16:33 u mg/L -0.06 0 06

Nickel, dissolved M200.71CP


WG345759

WG3457591CV ICV 06/17/13 14:40 11130510-1 2 1.991 mg/L 99.6 95 105

WG3457591CB ICB 06/17/13 14:46 u mg/L -0.03 0.03

WG345759PQV PQV 06/17/13 14:50 11130613-5 .05 .055 mg/L 110 70 130

WG345759SIC SIC 06/17/13 14:53 11130614-1 .1 .096 mg/L 96 80 120

WG345759LFB LFB 06/17/13 14:59 11130617-2 .5 .505 mg/L 101 85 115

L 12392-01 AS AS 06/17/13 15:05 11130617-2 .5 u .495 mg/L 99 85 115

L 12392-01ASD ASD 06/17/1315:08 11130617-2 .5 u .495 mg/L 99 85 115 0 20

WG345759CCV1 CCV 06/17/1315:30 11130514-2 1.012 mg/L 101 .2 90 110

WG345759CCB1 CCB 06/17/13 15:33 u mg/L -0.03 0.03

WG345759CCV2 CCV 06/17/1316:08 11130514-2 .998 mg/L 99.8 90 110

WG345759CCB2 CCB 06/17/1316:11 u mg/L -0.03 0.03

WG345759CCV3 CCV 06/17/13 16:30 11130514-2 .996 mg/L 99.6 90 110

WG345759CCB3 CCB 06/17/13 16:33 u mg/L -0.03 0.03

REPIN.01.06.05.01 Page 14 of 29

- ---



Energy Fuels Resources (USA) Inc. ACZ Project 10: L12392

Nitrate/Nitrite as N M353.2 - H2S04 preserved


WG345694

WG3456941CV

WG3456941CB

WG345703

WG345703CCV1

WG345703CCB1

WG345703LFB1

L 12392-01AS

L12392-02DUP

WG345703CCV2

WG345703CCB2

WG345703CCV3

WG345703CCB3

ICV

ICB

06/14/13 20:25 Wl130411-3

06/14/13 20:26

CCV 06/14/13 23:03 Wl130614-1

CCB 06/14/13 23:04

LFB

AS

06/14/13 23:06 Wl130215-3

06/14/13 23:08 Wl130215-3

DUP 06/14/13 23:10

CCV 06/14/1323:17 Wl130614-1

CCB 06/14/13 23:18

CCV 06/14/13 23:31 Wl130614-1

CCB 06/14/13 23:33

WG345703LFB2 LFB 06/14/13 23:40 Wl130215-3

WG345703CCV4 CCV 06/14/13 23:45 Wl130614-1

WG345703CCB4 CCB 06/14/13 23:47

WG345703CCV5 CCV 06/14/13 23:56 Wl130614-1

WG345703CCB5 CCB 06/14/13 23:57

2416

2

2

2

2

2

2

2

2

.83

2.07

Nitrogen, ammonia M350.1 -Automated Phenate

2.469 mg/L

U mg/L

1.967

u 1,989

3.006

mg/L

mg/L

mg/L

mg/L

2.09 mg/L

2.005 mg/L

U mg/L

1.993 mg/L

U mg/L

2.018

1.978

u 1.988

u

mg/L

mg/L

mg/L

mg/L

mg/L

102 2

98.4

99.5

108.8

100.3

99.7

100.9

98.9

99.4

90

-0_06

90

-0 06

90

90

90

-0.06

90

-0.06

90

90

-0.06

90

-0.06

110

0.06

110

0.06

110

110

110

0.06

110

0.06

110

110

0.06

110

0.06

20


WG345741

WG3457 411CV

WG3457411CB

WG345741LFB1

L 12288-01AS

L 12288-02DUP

ICV

ICB

LFB

06/17/1312:54 Wl121105-5

06/17/1312:55

06/17/13 12:56 Wl121218-3

AS 06/17/13 12:58 Wl121218-3

DUP 06/17/13 13:01

WG345741CCV1 CCV 06/17/1313:07 Wl121218-1

WG345741CCB1 CCB 06/17/1313:08

WG345741CCV2 CCV 06/17/1313:21 Wl121218-1

WG345741CCB2 CCB 06/17/13 13:22

WG345741LFB2 LFB 06/17/1313:29 Wl121218-3

WG345741CCV3 CCV 06/17/13 13:34 Wl121218-1

WG345741CCB3 CCB 06/17/1313:35

WG345741CCV4 CCV 06/17/1313:49 Wl121218-1

WG345741CCB4 CCB 06/17/13 13:50

WG345741CCV5 CCV 06/17/13 13:59 Wl121218-1

WG345741CCB5 CCB 06/17/13 14:00

WG345741CCV6 CCV 06/17/1314:05 Wl121218-1

WG345741CCB6 CCB 06/17/13 14:06

REPIN.01.06.05.01

1.003

2

2

2

2

2

2

u u

1.1 mg/L

U mg/L

1 005 mg/L

.983

u mg/L

mg/L

109.7

100.5

98.3

2.113 mg/L 105.7

U mg/L

2.044 mg/L 1 02.2

U mg/L

1.032 mg/L 103 2

2.091 mg/L 104.6

U mg/L

2.03 mg/L 101.5

U mg/L

2.045 mg/L 1 02.3

U mg/L

2.041 mg/L 102,1

u mg/L

90

-0.15

90

90

90

-0.15

90

-0.15

90

90

-015

90

-0.15

90

-0.15

90

-0.15

110

0,15

110

110

110

0.15

110

0.15

110

110

0.15

110

0.15

110

0.15

110

0.15

0 20 RA

Page 15 of29



Potassium, dissolved M200.71CP




WG345759

WG3457591CV

WG3457591CB

WG345759PQV

WG345759SIC

WG345759LFB

L 12392-01AS

L 12392-01ASD

WG345759CCV1

WG345759CCB1

WG345759CCV2

WG345759CCB2

WG345759CCV3

WG345759CCB3

ICV

ICB

PQV

SIC

LFB

AS

ASD

CCV

CCB

06/17/13 14:40

06/17/13 14:46

06/17/13 14:50

06/17/13 14:53

06/17/13 14:59

06/17/13 15:05

06/17/13 15:08

06/17/13 15:30

06/17/13 15:33

11130510-1

11130613-5

11130614-1

11130617-2

11130617-2

11130617-2

11130514-2

CCV 06/17/13 16:08 11130514-2

CCB 06/17/13 16:11

CCV 06/17/13 16:30 11130514-2

CCB 06/17/13 16:33

Residue, Filterable (TDS) @180C SM2540C

20

1_5

1.5

99.97161

99.97161

99.97161

10

10

10

111

11 .1

20.11

u 1.68

1.65

98.17

108.9

109 2

10 21

u

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

10 12 mg/L

U mg/L

10.14 mg/L

U mg/L

100.6

112

110

98.2

97,8

98,1

102.1

101 .2

101.4

95

-0.9

70

80

85

85

85

90

-0.9

90

-0.9

90

-0.9

105

09

130

120

115

115

115

110

0.9

110

0.9

110

0.9

0.28 20


WG344805

WG344805PBW PBW 06/03/1313:30

WG344805LCSW LCSW 06/03/13 13:31 PCN42166

L12393-01DUP DUP 06/03/1313:45

Residue, Non-Filterable (TSS) @105C SM2540D

260

930

u 258

934

mg/L

mg/L

mg/L

99.2

-20

80

20

120

0.4 10


WG344869

WG344869PBW PBW 06/04/13 10:20

WG344869LCSW LCSW 06/04/13 10:21 PCN42166 160

L12396-02DUP DUP 06/04/1310:40

Selenium, dissolved M200.8 ICP-MS

u

u 153

u

mg/L

mg/L

mg/L

95.6

-15

80

15

120

0 10

ACZ 10 Type Analyzed PCN/SCN QC Sample Found Units Rec Lower Upper RPD Limit Qual

WG345415

WG3454151CV

WG3454151CB

WG345415CCV1

WG345415CCB1

WG345415LFB

L 12392-02AS

L 12392-02ASD

WG345415CCV2

WG345415CCB2

WG345415CCV3

WG345415CCB3

WG345415CCV4

WG345415CCB4

ICV 06/12/1314:29 MS130416-2 05

ICB 06/12/13 14:32

CCV 06/12/1315:19 MS130510-4 _25025

CCB 06/12/13 15:23

LFB

AS

06/12/13 15:26 MS130508-1 .05005

06/12/1315:36 MS130508-1 .05005

ASD 06/12/1315:39 MS130508-1 .05005

CCV 06/12/13 16:00 MS130510-4 .25025

CCB 06/12/13 16:03

CCV 06/12/13 16:40 MS130510-4 .25025

CCB 06/12/13 16:43

CCV 06/12/13 17:03 MS130510-4 .25025

CCB 06/12/13 17:07

,05135 mg/L

U mg/L

,245 mg/L

U mg/L

,04843 mg/L

,0143 .0681 mg/L

,0143 ,06635 mg/L

2526 mg/L

U mg/L

.2481

u .2526

u

mg/L

mg/L

mg/L

mg/L

102 7 90 110

-0.0003 0.0003

97,9 90 110

96.8

107.5

-0.0003 0,0003

85

70

115

130

104 70 130 2.6

100.9 90 110

-0.0003 0.0003

99.1 90 110

-0.0003 0,0003

100,9 90 110

-0.0003 0,0003

20

RA

REPIN.01.06.05.01 Page 16 of 29



Silica, dissolved M200.71CP




WG345759

WG3457591CV

WG3457591CB

WG345759PQV

WG345759SIC

WG345759LFB

L 12392-01AS

L 12392-01ASD

WG345759CCV1

WG345759CCB1

WG345759CCV2

WG345759CCB2

WG345759CCV3

WG345759CCB3

ICV 06/17/13 14:40 11130510-1

ICB 06/17/13 14:46

PQV 06/17/13 14:50 11130613-5

SIC 06/17/13 14:53 11130614-1

LFB

AS

ASD

06/17/13 14:59 11130617-2

06/17/13 15:05 11130617-2

06/17/13 15:08 11130617-2

CCV 06/17/13 15:30 11130514-2

CCB 06/17/1315:33

CCV 06/17/13 16:08 11130514-2

CCB 06/17/1316:11

CCV 06/17/13 16:30 11130514-2

CCB 06/17/13 16:33

Sodium, dissolved M200.71CP

42.8

2.1428

2.1428

21.428

21_428

21_428

21.4

21.4

21,4

16.1

161

42.94

u 2 22

2.19

22 26

37.51

37.47

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

21 72 mg/L

U mg/L

21 ,49 mg/L

U mg/L

21.42 mg/L

U mg/L

100.3

103 6

1022

103.9

99.9

99.7

101 .5

100 4

100.1

95

-1.2

70

80

85

85

85

90

-1.2

90

-1.2

90

-1.2

105

1.2

130

120

115

115

115

110

1.2

110

1 2

110

1 2

0.11 20


WG345759

WG3457591CV

WG3457591CB

WG345759PQV

WG345759SIC

WG345759LFB

L 12392-01AS

L 12392-01ASD

WG345759CCV1

WG345759CCB1

WG345759CCV2

WG345759CCB2

WG345759CCV3

WG345759CCB3

Sulfate

ICV 06/17/13 14:40 11130510-1

ICB 06/17/13 14:46

PQV 06/17/13 14:50 11130613-5

SIC 06/17/13 14:53 11130614-1

LFB 06/17/13 14:59 11130617-2

AS 06/17/13 15:05 11130617-2

ASD 06/17/13 15:08 11130617-2

CCV 06/17/13 15:30 11130514-2

CCB 06/17/13 15:33

CCV 06/17/13 16:08 11130514-2

CCB 06/17/1316:11

CCV 06/17/13 16:30 11130514-2

CCB 06/17/13 16:33

100

1.5

1 5

100.0416

100.0416

100 0416

50

50

50

SM4500 S04-D

86.2

86.2

100.28 mg/L

U mg/L

1.57 mg/L

1.57 mg/L

98.16 mg/L

182 6

183.1

50.35

u 50.07

u 50.45

u

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

100.3

104.7

104.7

98,1

96.4

96.9

100.7

100.1

100.9

95

-0.9

70

80

85

85

85

90

-0.9

90

-0.9

90

-0.9

105

0.9

130

120

115

115

115

110

0.9

110

0,9

110

0,9

0 27 20


WG344992

WG344992PBW PBW 06/05/13 16:33

WG344992LCSW LCSW 06/05/13 16:35 WC130501-

L12446-03DUP DUP 06/05/1317:00

REPIN.01.06.05.01

100

1730

u 111

1701

mg/L

mg/L

mg/L

111

-30

80

30

120

1 7 20

Page 17 of 29


' Inorganic QC Summary


Sulfide as 5 SM4500S2-D

ACZ ID Type Analyzed PCNISCN QC Sample Found Units Rec Lower Upper RPD Limit Qual

WG344884

WG3448841CV

WG3448841CB

WG344884LFB

WG344884CCV1

WG344884CCB1

WG344884CCV2

WG344884CCB2

ICV 06104113 14:40 WC130603-

ICB 06104/13 14:42

LFB 06/04/13 14:45 WC130603-

CCV 06/04/13 15: 15 WC 130603-

CCB 06/04/13 15:18

CCV 06/04/1315:50 WC130603-

CCB 06/04/13 15:53

L12393-02AS AS 06/04/13 16:05 WC130603-

L12393-02DUP DUP 06/04/1316:08

WG344884CCV3 CCV 06/04/13 16:10 WC130603-

WG344884CCB3 CCB 06/04/13 16:13

32266

.224

,168

.168

224

168

Uranium, dissolved M200.8 ICP-MS

u u

336

u 245

172

u .17

u .033

u ,169

u

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

104,1

109.4

102.4

101.2

14 7

100,6

90

-0 .06

80

90

-0.06

90

-0.06

75

90

-0.06

110

0.06

120

110

0 06

110

0.06

125

110

0,06

0 20


WG345415

WG3454151CV

WG3454151CB

WG345415CCV1

WG345415CCB1

WG345415LFB

L 12392-02AS

L 12392-02ASD

WG345415CCV2

WG345415CCB2

WG345415CCV3

WG345415CCB3

WG345415CCV4

WG345415CCB4

ICV

ICB

06/12/13 14:29 MS130416-2

06/12113 14:32

CCV 06/12/1315:19 MS130510-4

CCB 06/12/13 15:23

LFB

AS

ASD

06/12/13 15:26 MS130508-1

06/12/13 15:36 MS130508-1

06/12/13 15:39 MS130508-1

CCV 06/12/13 16:00 MS130510-4

CCB 06/12/13 16:03

CCV 06/12/1316:40 MS130510-4

CCB 06/12/13 16:43

CCV 06/12/13 17:03 MS130510-4

CCB 06/12/1317:07

Vanadium, dissolved M200.71CP

.05

,05

05

,05

.1

.05275 mg/L

U mg/L

.1018

u mg/L

mg/L

,04865 mg/L

.0776 .1262

.0776 .1276

.1018

u .1015

u .1011

u

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

105.5 90 110

-0.0003 0,0003

101 8 90 110

97.3

97.2

100

-0,0003 0,0003

85

70

70

115

130

130

1018 90 110

-0,0003 0.0003

1015 90 110

-0.0003 0.0003

101 1 90 110

-0.0003 0.0003

1.1 20

ACZ ID Type Analyzed PCNISCN QC Sample Found Units Rec Lower Upper RPD Limit Qual

WG345759

WG3457591CV

WG3457591CB

WG345759PQV

WG345759SIC

WG345759LFB

L12392-01AS

L 12392-01ASD

WG345759CCV1

WG345759CCB1

WG345759CCV2

WG345759CCB2

WG345759CCV3

WG345759CCB3

ICV 06/17/13 14:40 11130510-1

ICB 06/17/13 14:46

PQV 06/17/13 14:50 11130613-5

SIC 06/17/13 14:53 11130614-1

LFB 06/17/1314:59 11130617-2

AS

ASD

06/17/13 15:05 11130617-2

06/17/13 15:08 11130617-2

CCV 06/17/1315:30 11130514-2

CCB 06/17/1315:33

CCV 06/17/1316:08 11130514-2

CCB 06/17/1316:11

CCV 06/17/1316:30 11130514-2

CCB 06/17/13 16:33

2

025

_1

_5

_5

_5

1

.021

.021

2.0125 mg/L

U mg/L

.0275 mg/L

.0891 mg/L

.5024 mg/L

.5194

.5204

1.02

u 1.011

u 1.011

u

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

100.6

110

89.1

100.5

99.7

99.9

102

101.1

101 .1

95

-0.015

70

80

85

85

85

90

-0.015

90

-0.015

90

-0.015

105

0.015

130

120

115

115

115

110

0.015

110

0.015

110

0.015

0.19 20

M2

RA

REPIN.01.06.05.01 Page 18 of 29



Zinc, dissolved M200.71CP



ACZ ID Type Analyzed PCN/SCN QC Sample Found Units Rec Lower Upper RPD limit Qual

WG345759

WG3457591CV ICV 06/17/13 14:40 11130510-1 2 1.957 mg/L 97.9 95 105

WG3457591CB ICB 06/17/13 14:46 u mg/L -0.03 0,03

WG345759PQV PQV 06/17/13 14:50 11130613-5 .05 049 mg/L 98 70 130

WG345759SIC SIC 06/17/13 14:53 11130614-1 .1 .096 mg/L 96 80 120

WG345759LFB LFB 06/17/13 14:59 11130617-2 .5 .495 mg/L 99 85 115

L 12392-01AS AS 06/17/1315:05 11130617-2 .5 u .483 mg/L 96.6 85 115

L12392-01ASD ASD 06/17/1315:08 11130617-2 .5 u 489 mg/L 97.8 85 115 1.23 20

WG345759CCV1 CCV 06/17/1315:30 11130514-2 1 007 mg/L 100.7 90 110

WG345759CCB1 CCB 06/17/1315:33 u mg/L -0.03 0,03

WG345759CCV2 CCV 06/17/1316:08 11130514-2 995 mg/L 99.5 90 110

WG345759CCB2 CCB 06/17/1316:11 u mg/L -0.03 0.03

WG345759CCV3 CCV 06/17/13 16:30 11130514-2 991 mg/L 99.1 90 110

WG345759CCB3 CCB 06/17/1316:33 u mg/L -0.03 O,Q3

REPIN.01.06.05.01 Page 19 of 29

ACZ Laboratories, Inc. 2773 Downhill Drive Steamboat Springs, CO 80487


(800) 334-5493

Inorganic Extended Qualifier Report


ACZ ID WORKNUM PARAMETER METHOD QUAL DESCRIPTION

L 12392-01 WG345633 Carbon, total organic (TOG) SM5310B

WG345779 Chloride SM4500CI-E

WG345407 Fluoride SM4500F-C

WG345741 Nitrogen, ammonia M350.1 -Automated Phenate

WG344869 Residue, Non-Filterable (TSS) @1 05C SM2540D

WG344884 Sulfide as S SM4500S2-D

SM4500S2-D

L 12392-02 WG345633 Carbon, total organic (TOC) SM5310B

WG345779 Chloride SM4500CI-E

WG345407 Fluoride SM4500F-C

WG345741 Nitrogen, ammonia M350,1 -Automated Phenate

WG344869 Residue, Non-Filterable (TSS) @1 05C SM2540D

WG344884 Sulfide as S SM4500S2-D

SM4500S2-D

REPAD.15.06.05.01

RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation(< 10x MDL).

M3 The spike recovery value is unusable since the analyte concentration in the sample is disproportionate to the spike level The recovery of the associated control sample (LCS or LFB) was acceptable,

RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation (< 1 Ox MDL).

RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation(< 10x MDL}.

RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation(< 1 Ox MDL),

M2 Matrix spike recovery was low, the recovery of the associated control sample (LCS or LFB) was acceptable,



M3 The spike recovery value is unusable since the analyte concentration in the sample is disproportionate to the spike level. The recovery of the associated control sample (LCS or LFB) was acceptable.




M2 Matrix spike recovery was low, the recovery of the associated control sample (LCS or LFB) was acceptable.


Page 20 of 29


Report Header Explanations

Batch

Error(+/-)

Found

Limit

LCL

A distinct set of samples analyzed at a specific time

Calculated sample specific uncertainty

Value of the QC Type of interest

Upper limit for RPD, in%.

Lower Control Limit, in% (except for LCSS, mg/Kg)

Calculated sample specific Lower Limit of Detection LLD

PCN/SCN

PQL

A number assigned to reagents/standards to trace to the manufacturer's certificate of analysis

Practical Quantitation Limit

QC True Value of the Control Sample or the amount added to the Spike

Rec

RER

RPD

Amount of the true value or spike added recovered, in % (except for LCSS, mg/Kg)

Relative Error Ratio, calculation used for Dup. QC taking into account the error factor.

Relative Percent Difference, calculation used for Duplicate QC Types

UCL

Sample

Upper Control Limit, in % (except for LCSS, mg/Kg)

Value of the Sample of interest

QC Sample Types

DUP

LCSS

LCSW

Sample Duplicate

Laboratory Control Sample - Soil

Laboratory Control Sample - Water

QC Sample Type Explanations

MS/MSD

PBS

PBW

Matrix Spike/Matrix Spike Duplicate

Prep Blank- Soil

Prep Blank - Water

Blanks

Control Samples

Duplicates

Matrix Spikes

Verifies that there is no or minimal contamination in the prep method procedure.

Verifies the accuracy of the method, including the prep procedure.

Verifies the precision of the instrument and/or method.

Determines sample matrix interferences, if any.

ACZ Qualifiers (Qual)

H Analysis exceeded method hold time.

Method Prefix Reference

M EPA methodology, including those under SDWA, CWA, and RCRA

SM Standard Methods for the Examination of Water and Wastewater.

D ASTM

RP DOE

ESM DOE/ESM

Comments

(1) Solid matrices are reported on a dry weight basis.

(2) Preparation method: "Method" indicates preparation defined in analytical method.

(3) QC results calculated from raw data. Results may vary slightly if the rounded values are used in the calculations.

(4) An asterisk in the "XQ" column indicates there is an extended qualifier and/or certification

qualifier associated with the result.

For a complete list of ACZ's Extended Qualifiers, please click: http://WNYV.acz.com/public/exlqualliSt.pdf

REP003.09.12.01

Page 23 of29



Alpha M900.0

-WG345380

WG344957PBW PBW 06/10/13

WG344957LCSW LCSW 06/10/13 RC121002-2 81.06

L12292-01DUP DUP-RER 06/10/13 2,6 2.5 2.1

L 12441-05DUP DUP-RER 06/10/13 1.1 1.5 1.5

L 12294-02MS MS 06/10/13 RC121002-2 81.06 1 2.2 2.4

Beta M900.0

ACZID Type Analyzed PCN/SCN QC Sample Error LLD

WG345380

WG344957PBW PBW 06/10/13

WG344957LCSW LCSW 06/10/13 PCN40563 100

L 12292-01 DUP DUP-RER 06/10/13 4.5 3,8 5

L 12441-05DUP DUP-RER 06/10/13 0.12 2.3 3.6

L 12442-03MS MS 06/10/13 PCN40563 66.67 0.03 3.1 3.8

Lead 210, dissolved EICHROM, OlW01

ACZID Type Analyzed PCN/SCN QC Sample Error LLD

WG345433

L 12392-02DUP DUP-RER 06/11/13 -12 4.5 19

L 12393-02MS MS 06/11/13 RC120601-1 70.61 -2 5.1 20

WG345070LCSW LCSW 06/11/13 RC120601-1 70.61

WG345070PBW PBW 06/11/13

REPRC.01.06.05.01

2.3 1.6 1.2

75 8.4 1,8 92.5

2 2.3 2.1

1 1.7 1.5

63 8,8 2.3 76.5

Found Error LLD Rec

3.5 2.7 3.4

94 7.6 5.4 94

5.2 3.9 5.4

.32 2.3 3.5

66 5.7 3.8 99

Found Error LLD Rec

-9.5 3.8 16

55 5.1 16 80.7

65 5.7 18 92.1

-3.1 4.1 16

Radiochemistry QC Summary


Units: pCi/L

2.4

83 133

0.18 2

0.04 2

83 133 M2

Units: pCi/L

Lower Upper RPD

6.8

70 129

0.13 2

0 06 2

70 129

Units: pCi/L

Lower Upper RPD

0.42 2

55 121

55 121

32

Page 24 of29



Radium 226, dissolved M903.1

-WG345832

WG344950PBW PBW 06/17/13

WG344950LCSW LCSW 06/17/13 RC130227-2 23.92

L12260-01DUP DUP-RER 06/17/13 0.12 0.07 0.05

L 12427 -01DUP DUP-RER 06/17/13 1.5 0.15 0.1

L 12266-01MS MS 06/17/13 RC130227-2 23.92 59 0 81 0.11

Radium 228, dissolved M904.0

-WG345976

WG344949LCSW LCSW 06/18/13 PCN41953 19,02

WG344949PBW PBW 06/18/13

L 12233-02DUP DUP-RER 06/18/13 2.8 1.1 1.3

L 12234-01MS MS 06/18/13 PCN41953 19.02 2 ., 2.6

WG344949LCSWD LCSWD 06/18/13 PCN41953 19.02

WG344949LCSWD LCSWD 06/18/13 PCN41953 19.02

Thorium 230, dissolved ESM 4506

WG346566

WG346220PBW PBW 06/26/13

WG346220LCSW LCSW 06/26/13 RC111214-1 162.12

L 12392-01 DUP DUP-RER 06/26/13 1 0,59 0.76

L12672-01DUP DUP-RER 06/26/13 0.29 0.36 0.69

L 12392-02MS MS 06/26/13 RC111214-1 162.12 1.1 0.49 0.72

REPRC.01.06.05.01

.05 0.06 0.08

23 0.48 0.13 96.2

.13 0.05 0.09

1.6 0.15 0.25

62 0.76 0.07 12.5

15 1.6 1.9 78.9

.62 0.48 0.81

4 0.86 1.8

15 1.2 1.3 68.4

16 1.2 1.2 84.1

16 1.2 1.2 84.1

.17 0.51 0.94

190 52 0.75 117.2

08 0.57 0,66

-.2 0.42 0,89

180 4.7 0,65 110.4

Radiochemistry QC Summary


Units: pCi/L

0.16

43 148

0.12 2

0.47 2

43 148 M2

Units: pCi/L

47 123

1 62

0.86 2

47 123

47 123 20

47 123 6.5 20

Units: pCi/L

1.88

91 126

1.12 2

0.89 2

91 126

Page 25 of29

ACZ Laboratories, Inc. 2773 Downhill Drive Steamboat Springs, CO 80487


(800) 334-5493

RadChem Extended Qualifier Report


ACZ ID WORKNUM PARAMETER METHOD QUAL DESCRIPTION

L 12392-01 WG345380 Gross Alpha M900,0 M2 Matrix spike recovery was low, the recovery of the associated control sample (LCS or LFB) was acceptable.

WG345832 Radium 226, dissolved M903,1 M2 Matrix spike recovery was low, the recovery of the associated control sample (LCS or LFB) was acceptable

L 12392-02 WG345380 Gross Alpha M900,0 M2 Matrix spike recovery was low, the recovery of the associated control sample (LCS or LFB) was acceptable.

WG345832 Radium 226, dissolved M903-1 M2 Matrix spike recovery was low, the recovery of the associated control sample (LCS or LFB) was acceptable.

REPAD.15.06.05.01

Page 26 of29



Metals Analysis

The following parameters are not offered for certification or are not covered by NELAC certificate #ACZ.

Cesium, dissolved M200.8 ICP-MS

Radiochemistry

The following parameters are not offered for certification or are not covered by NELAC certificate #ACZ.

Wet Chemistry

Lead 210, dissolved

Thorium 230, dissolved

EICHROM, OTW01

ESM 4506

,The following parameters are not offered for certification or are not covered by NELAC certificate #ACZ.

Sulfide asS SM4500S2-D

REPAD.05.06.05.01

Certification Qualifiers


Page 27 of29



Sample Receipt


Date Received: 05/31/2013 10:37

Received By: ksj

Date Printed: 5/31 /2013

Receipt Verification

YES

1) Is a foreign soil permit included for applicable samples?

2) Is the Chain of Custody or other directive shipping papers present?

3) Does this project require special handling procedures such as CLP protocol?

4) Are any samples NRC licensable material?

5) If samples are received past hold time, proceed with requested short hold time analyses?

6) Is the Chain of Custody complete and accurate?

7) Were any changes made to the Chain of Custody prior to ACZ receiving the samples?

Samples/Containers

YES

8) Are all containers intact and with no leaks?

9) Are all labels on containers and are they intact and legible?

1 0) Do the sample labels and Chain of Custody match for Sample ID, Date, and Time?

11) For preserved bottle types, was the pH checked and within limits?

12) Is there sufficient sample volume to perform all requested work?

13) Is the custody seal intact on all containers?

14) Are samples that require zero headspace acceptable?

15) Are all sample containers appropriate for analytical requirements?

16) Is there an Hg-1631 trip blank present?

17) Is there a VOA trip blank present?

18) Were all samples received within hold time?

Chain of Custody Related Remarks

Client Contact Remarks

Shipping Containers

Cooler Id Temp (°C) Rad ().lR/Hr) Custody Seal Intact?

3477 2 12 Yes

Was ice present in the shipment container(s)?

Yes - Wet ice was present in the shipment container(s).

Client must contact an ACZ Project Manager if analysis should not proceed for samples received outside of their thermal preseNation acceptance criteria.

REPAD LPII 2012-03

NO NA

NO NA

X

Page 28 of29

-o 0 ...,

~~ u ~

--0

t:

Laboratories, Inc.

·(Surface Water)· GW (Ground Water) · WW (Waste Water) · OW (Drinking Water) · SL (Sludge) · SO (SoW) • OL (Oil) · Other (Specify)

Please refer to ACZ's terms & conditions located on the reverse side of this COC.

FRMAD050.12.12.12 White- Return witl:l sample. Yellow -Retain for your records. Page 29 of 29


Analytical Report

Report to:

Ryan Ellis


225 Union Blvd. ,Suite 600

Lakewood, CO 80228

cc: Jamie Massey

Project ID:

ACZ Project I D: L 12393

Ryan Ellis:

June 27, 2013

Bill to:

Kathy Weinel


225 Union Blvd. ,Suite 600

Lakewood, CO 80228

Enclosed are the analytical results for sample(s) submitted to ACZ Laboratories, Inc. (ACZ) on May 31, 2013. This project has been assigned to ACZ's project number, L 12393. Please reference this number in all future inquiries.

All analyses were performed according to ACZ's Quality Assurance Plan. The enclosed results relate only to the samples received under L 12393. Each section of this report has been reviewed and approved by the appropriate Laboratory Supervisor, or a qualified substitute.

Except as noted, the test results for the methods and parameters listed on ACZ's current NELAC certificate letter (#ACZ) meet all requirements of NELAC.

This report shall be used or copied only in its entirety. ACZ is not responsible for the consequences arising from the use of a partial report.

All samples and sub-samples associated with this project will be disposed of after July 27, 2013. If the samples are determined to be hazardous, additional charges apply for disposal (typically $11/sample). If you would like the samples to be held longer than ACZ's stated policy or to be returned, please contact your Project Manager or Customer Service Representative for further details and associated costs. ACZ retains analytical raw data reports for ten years.

If you have any questions or other needs, please contact your Project Manager.

Tony Antalek has reviewed and approved this report.

Page 1 of 29

ACZ Laboratories, Inc. 2773 Downhill Drive Steamboat Springs. CO 80487 {BOO) 334-5493

Report Header Explanations

A distinct set of samples analyzed at a specific time

Value of the QC Type of interest

Upper limit for RPD, in%.

Lower Recovery Limit, in % (except for LCSS, mg/Kg)

Batch

Found

Limit

Lower

MDL

PCNISCN

PQL

Method Detection Limit. Same as Minimum Reporting Limit, Allows for instrument and annual fluctuations.

A number assigned to reagents/standards to trace to the manufacturer's certificate of analysis

Practical Quantitation Limit, typically 5 times the MDL.

QC True Value of the Control Sample or the amount added to the Spike

Rec

RPD

Upper

Sample

Recovered amount of the true value or spike added, in % (except for LCSS, mg/Kg)

Relative Percent Difference, calculation used for Duplicate QC Types

Upper Recovery Limit, in % (except for LCSS, mg/Kg)

Value of the Sample of interest

QC Sample Types

AS Analytical Spike (Post Digestion) LCSWD Laboratory Control Sample - Water Duplicate

ASO Analytical Spike (Post Digestion) Duplicate LFB Laboratory Fortified Blank

CCB Continuing Calibration Blank LFM Laboratory Fortified Matrix

CCV Continuing Calibration Verification standard LFMD Laboratory Fortified Matrix Duplicate

DUP Sample Duplicate LRB Laboratory Reagent Blank

ICB Initial Calibration Blank MS Matrix Spike

/CV Initial Calibration Verification standard MSD Matrix Spike Duplicate

/CSAB Inter-element Correction Standard- A plus B solutions PBS Prep Blank- Soil

LCSS Laboratory Control Sample - Soil PBW Prep Blank- Water

LCSSD Laboratory Control Sample - Soil Duplicate PQV Practical Quantitation Verification standard

LCSW Laboratory Control Sample- Water SOL Serial Dilution

QC Srnnpli) Typa Expl~natlun~~o

Blanks

Control Samples

Duplicates

Spikes/Fortified Matrix

Standard

Verifies that there is no or minimal contamination in the prep method or calibration procedure.

Verifies the accuracy of the method, including the prep procedure.

Verifies the precision of the instrument and/or method.

Determines sample matrix interferences, if any.

Verifies the validity of the calibration.

ACZ Qualifiers (QIJJ.!I)

B

H

L

u

Analyte concentration detected at a value between MDL and POL. The associated value is an estimated quantity.

Analysis exceeded method hold time. pH is a field test with an immediate hold time.

Target analyte response was below the laboratory defined negative threshold.

The material was analyzed for, but was not detected above the level of the associated value ,

The associated value is either the sample quantitation limit or the sample detection limit.

(1) EPA 600/4-83-020. Methods for Chemical Analysis of Water and Wastes, March 1983.

(2) EPA 600/R-93-1 00. Methods for the Determination of Inorganic Substances in Environmental Samples, August 1993,

(3) EPA 600/R-94-111. Methods for the Determination of Metals in Environmental Samples- Supplement I, May 1994.

(4) EPA SW-846. Test Methods for Evaluating Solid Waste.

(5) Standard Methods for the Examination of Water and Wastewater.

Comments

(1) QC results calculated from raw data. Results may vary slightly if the rounded values are used in the calculations.

(2) Soil, Sludge, and Plant matrices for Inorganic analyses are reported on a dry weight basis ,

(3) Animal matrices for Inorganic analyses are reported on an "as received" basis.

(4) An asterisk in the "XQ" column indicates there is an extended qualifier and/or certification qualifier

associated with the result.

(5) If the MDL equals the PQL or the MDL column is omitted, the POL is the reporting limit.

For a complete list of ACZ's Extended Qualifiers, please click: ! rltp ://www.:tC)'~C(! IDI!IublitiC.Xt!ruulliSI .p If

Page 6 of 29



Alkalinity as CaC03 SM2320B -Titration




WG345123

WG345123PBW1 PBW 06/06/13 16:19

WG345123LCSW2 LCSW 06/06/13 16:33 WC130601- 820.0001

L 12399-04DUP DUP 06/06/13 18:26

WG345123LCSW5 LCSW 06/06/13 20:10 WC130601- 820.0001

WG345123PBW2 PBW 06/06/13 20:18

WG345123LCSW8 LCSW 06/06/13 23:50 WC130601- 820,0001

WG345123PBW3 PBW 06/06/13 23:59

WG345123LCSW11 LCSW 06/07/13 3:33 WC130601- 820.0001

WG345123PBW4 PBW 06/07/13 3:42

WG345123LCSW14 LCSW 06/07/13 7:01 WC130601- 820.0001

Aluminum, dissolved M200.7 ICP

479

u 754 1

499 6

784.5

2.2

767 9

u 789.3

2.3

795.6

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

92

95.7

93 6

96 .3

97

-20

90

90

-20

90

-20

90

-20

90

20

110

110

20

110

20

110

20

110

42 20


WG345759

WG3457591CV

WG3457591CB

WG345759PQV

WG345759SIC

WG345759LFB

L 12392-01AS

L 12392-01ASD

WG345759CCV1

WG345759CCB1

WG345759CCV2

WG345759CCB2

WG345759CCV3

WG345759CCB3

ICV 06/17/1314:40 11130510-1 2

ICB 06/17/13 14:46

PQV 06/17/1314:50 11130613-5 .150165

SIC 06/17/13 14:53 11130614-1 200.370165

LFB

AS

ASD

CCV

CCB

06/17/1314:59 11130617-2

06/17/13 15:05 11130617-2

06/17/13 15:08

06/17/13 15:30

06/17/13 15:33

11130617-2

11130514-2

CCV 06/17/13 16:08 11130514-2

CCB 06/17/1316:11

CCV 06/17/13 16:30 11130514-2

CCB 06/17/13 16:33

1.0011

1.0011

1.0011

Arsenic, dissolved M200.8 ICP-MS

u u

2.039

u .156

206.6

1.025

1.027

1.037

1.027

u 1.014

u 1.013

u

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

102

103.9

103.1

102.4

102.6

103.6

102 7

101_4

101.3

95

-0.09

70

85

85

85

90

-0.09

90

-0.09

90

-0.09

105

0"09

130

200

115

115

115

110

0.09

110

0.09

110

0.09

0.97 20


WG345415

WG3454151CV

WG3454151CB

WG345415CCV1

WG345415CCB1

WG345415LFB

L 12392-02AS

L 12392-02ASD

WG345415CCV2

WG345415CCB2

WG345415CCV3

WG345415CCB3

WG345415CCV4

WG345415CCB4

REPIN .01 .06.05.01

ICV 06/12/13 14:29 MS130416-2

ICB 06/12/13 14:32

CCV 06/12/1315:19 MS130510-4

CCB 06/12/13 15:23

LFB

AS

ASD

CCV

CCB

CCV

CCB

06/12/13 15:26

06/12/13 15:36

06/12/13 15:39

06/12/13 16:00

06/12/13 16:03

06/12/13 16:40

06/12/13 16:43

MS130508-1

MS130508-1

MS130508-1

MS130510-4

MS130510-4

CCV 06/12/1317:03 MS130510-4

CCB 06/12/13 17:07

.05

.1001

.05005

.05005

.05005

,1001

,1001

,1001

.0043

.0043

.05184 mg/L

U mg/L

.1052 mg/L

U mg/L

.04849

.0573

.05579

.1028

u .101

u .1032

u

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

103,7 90 110

-0.0006 0.0006

105.1 90 110

96.9

105.9

102.9

102.7

100.9

103,1

-0.0006 0.0006

85

70

70

90

-0,0006

90

-0,0006

115

130

130 2.67

110

0.0006

110

0.0006

90 110

-0,0006 0,0006

20

Page 7 of29

- --




Barium, dissolved M200.71CP


WG345759

WG3457591CV

WG3457591CB

WG345759PQV

WG345759SIC

WG345759LFB

L 12392-01AS

L 12392-01ASO

WG345759CCV1

WG345759CCB1

WG345759CCV2

WG345759CCB2

WG345759CCV3

WG345759CCB3

Boron, dissolved

ICV

ICB

06/17/13 14:40 11130510-1

06/17/13 14:46

PQV 06/17/13 14:50 11130613-5

SIC 06/17/13 14:53 11130614-1

LFB 06/17/13 14:59 11130617-2

AS 06/17/13 15:05 11130617-2

ASD 06/17/13 15:08 11130617-2

CCV 06/17/13 15:30 11130514-2

CCB 06/17/13 15:33

CCV 06/17/13 16:08 11130514-2

CCB 06/17/1316:11

CCV 06/17/13 16:30 11130514-2

CCB 06/17/13 16:33

M200.71CP

2

.015

.1

.5

.5

.5

_012

_012

2.0205 mg/L

U mg/L

.0151 mg/L

,0976 mg/L

.5071 mg/L

_514 mg/L

514 mg/L

1.023 mg/L

U mg/L

1.02 mg/L

U mg/L

1 028 mg/L

U mg/L

101

100.7

97.6

101.4

100.4

1004

102.3

102

102.8

95

-0.009

70

80

85

85

85

90

-0 009

90

-0.009

90

-0.009

105

0.009

130

120

115

115

115

110

0 009

110

0 009

110

0.009

0 20


WG345759

WG3457591CV

WG3457591CB

WG345759PQV

WG345759SIC

WG345759LFB

L 12392-01AS

L 12392-01ASD

WG345759CCV1

WG345759CCB1

WG345759CCV2

WG345759CCB2

WG345759CCV3

WG345759CCB3

ICV 06/17/13 14:40 11130510-1

ICB 06/17/13 14:46

PQV 06/17/13 14:50 11130613-5

SIC 06/17/13 14:53 11130614-1

LFB 06/17/13 14:59 11130617-2

AS 06/17/13 15:05 11130617-2

ASD 06/17/13 15:08 11130617-2

CCV 06/17/13 15:30 11130514-2

CCB 06/17/13 15:33

CCV 06/17/13 16:08 11130514-2

CCB 06/17/13 16:11

CCV 06/17/13 16:30 11130514-2

CCB 06/17/13 16:33

2

.05005

.1001

.5005

.5005

.5005

1

Cadmium, dissolved M200.8 ICP-MS

_33

.33

2,037

u ,057

,095

,52

.822

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

.828 mg/L

1.023 mg/L

U mg/L

1,02

u 1.022

u

mg/L

mg/L

mg/L

mg/L

101 .9

113.9

94.9

103.9

98.3

99.5

102.3

102

102.2

95

-0.03

70

80

85

85

85

90

-0.03

90

-0.03

90

-0.03

105

0.03

130

120

115

115

115

110

0,03

110

0.03

110

0.03

0.73 20


WG345415

WG3454151CV

WG3454151CB

WG345415CCV1

WG345415CCB1

WG345415LFB

L 12392-02AS

ICV

ICB

06/12/13 14:29 MS130416-2

06/12/13 14:32

CCV 06/12/13 15:19 MS130510-4

CCB 06/12/13 15:23

LFB 06/12/13 15:26 MS130508-1

AS 06/12/13 15:36 MS130508-1

L 12392-02ASD ASD 06/12/13 15:39 MS130508-1

WG345415CCV2 CCV 06/12/1316:00 MS130510-4

WG345415CCB2 CCB 06/12/1316:03

WG345415CCV3

WG345415CCB3

WG345415CCV4

WG345415CCB4

REPIN.01.06.05.01

CCV 06/12/13 16:40 MS130510-4

CCB 06/12/13 16:43

CCV 06/12/1317:03 MS130510-4

CCB 06/12/13 17:07

,05

1002

.0501

.0501

.0501

.1002

.1002

.1002

u u

,0511

u mg/L

mg/L

.1028 mg/L

U mg/L

.04797 mg/L

.04701 mg/L

.04766 mg/L

,1019 mg/L

U mg/L

_09992 mg/L

U mg/L

09973 mg/L

U mg/L

102.2 90 110

-0.0003 0,0003

102,6 90 110

-0.0003 0.0003

95.7 85 115

93.8 70 130

95.1 70 130 1.37 20

101 .7 90 110

-0.0003 0,0003

99.7 90 110

-0.0003 0.0003

99.5 90 110

-0.0003 0.0003

Page 8 of 29

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