technical memorandum no. 3a for remedial … · "standard methods for the examination of water...
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«: TECHNICAL MEMORANDUM NO. 3AFOR
REMEDIAL INVESTIGATION/FEASIBILITY STUDYCITY DISPOSAL CORPORATION LANDFILL
(DUNN LANDFILL)
(PELA Reference No. 495207)
Appendix G
Results of AnalysesSoil and Ground-Water Samples
Volume 16 of 16
Technical Report
SAMPLES: CA4376-CA4377
April 1991
-RE.LaMoreaux& Associates—
OHM Corporation
Environmental Testingand Certification Corp.
Technical Report
for
WASTE MANAGEMENT, INC.
:iS^
ETCStmp/tNO..l:[:M^ii^\l!X:W^
.$liHW
Richard P. AlbertVice President. Oenertt Manager
This Technical -Report is an INSITE1" service generated by LOOESTflR*" Data Management Software.
-284 Raritan Cenler Parkwav CN 7808 Edison, New Jersey 08818-7 201-225-5600-
ETC
TAJBIL,:E
Case Narrative 1Methodology 3
Volatile Data 6QC Summary Data 7Sample Data 14Standard Data • 37Raw QC Data 62
t
Semivolatile Data 90QC Summary Data 91Sample Data 98Standard Data 140Raw QC Data 181
Pesticide/PCB Data 210QC Summary Data 211Sample Data 215Standard Data 222Raw QC Data 264
Chain of Custody 274
ETC
CASE NARJRATIVE
———ETC———————————————SDG NARRATIVE
This technical report submitted by ETC Corporation contains theanalytical results and required deliverables for WASTE MANAGEMENT,INC. Site 405 samples as identified below:
ETC ID CLIENT ID ETC ID CLIENT IDCA4376 1SLPZ11I CA4377 1SLPZ11I
During the preparation and analysis of these samples, the followingwas observed:
VOLATILES: COV70337);The intact sample or extract required dilution resulting inelevated method detection limits (MDL's).
SEMIVOIATILES; (QC70246);The internal standard area counts for the blank outside QC controllimits was confirmed by the results of a replicate analysis. Datafrom both analyses has been included in this report.
The internal standard area counts for sample CA4377 outside QCcontrol limits was confirmed by the results of a replicateanalysis. Data from both analyses has been included in thisreport.
PESTICIDES/PCBS; (067024$.).;Problems were not observed during the preparation and analysis ofthis batch.
Release of the data contained in this hardcopy data package hasbeen authorized by the following signature.
Gregory G. Morrison / /' DateLaboratory Manager
ETC
METHODOLOGY
——ETC———————————-_______INTRODUCTION
Environmental Testing and Certification Corp.284 Raritan Center Parkway, CN 7808
Edison, New Jersey 08818-7808(201) 225-6700
This report contains analytical results in tabular form for your sample. It includescomprehensive data for each analytical process. Associated quality control data is alsopresented, including OC batch results for the laboratory blank, spiked blank, matrix spikeand a replicated sample spike, as well as results from surrogate compound analyses.Quality control data for instrument performance is also included. Other appendices mayinclude data system printouts and chain of custody records.
Analytical Methodology
ETC utilizes a wide variety of methodologies and ERA approved procedures which arelisted below. Analytical results and Quality Assurance protocols are based upon theapproriate guideline dependent upon the level of deliverable requested.
"Methods of Organic Chemical Analysis of Municipal and IndustrialWastewater", Federal Register Vol. 49, No. 209, October 26, 1984;
Test Methods for Evaluating Solid Waste", SW-846 Third Edition, September1986, USEPA;
"Standard Methods for the Examination of Water and Wastewater" 1985,14th, 15th and 16th Edition;
"Methods for Chemical Analysis of Water and Wastes" March 1983, EMSL,ERA 600 4-79-020;
Organic Analysis: Multi-media, Multi-Concentration-IFB-CLP, SOW February1988;
Inorganic Analysis: Multi-media, Multi-Concentration IFB-CLP, SOW July1987;
Dioxin Analysis: Soil/Sediment/Water Matrix; Multi-Concentration, SelectedIon Monitoring with Jar Extraction Procedure; IFB WA86-K357.
"Methods for the Determination of Organic Compounds in Drinking Water"December 1988, EPA-600/4-88/039;
"Handbook for Analytical Quality Control in Water and WastewaterLaboratories", EPA-600/4-79-019, March 1979;
"National Enforcement Investigation Center Policies and ProceduresManual,EPA-330/9/78/001-R, Revised May 1986.
4
——ETC ———————————————————————ETC Network Laboratories are certified to perform analytical analyses upon samplescollected throughout the United States. It may be required that this environmental databe reported with reference to a certified laboratory. The Laboratory IdentificationNumbers for ETC Corp., Edison NJ Laboratory are summarized below for yourinformation and reference. Please contact your Program Manager should you requirecertification verification for an ETC Network Laboratory.
Certification Summary. January 1990
State Agency
Alabama Department of Environmental Management
Arizona Department of Environmental Quality
California Department of Health Services
Connecticut Department of Health Services
Florida Department of Healthand Rehabilitative Services
Illinois Environmental Protection Agency
Kansas Department of Health and Environment
New Hampshire Department of Environmental Services
New Jersey Department of Environmental Protection
New York Department of Public Health
Oklahoma Water Resources Board
Pennsylvania Department of Environmental Regulation
South Carolina Department of Healthand Environmental Control
Tennessee Department of Health and EnvironmentalLaboratory Services
Utah Department of Health
Virginia Department of General Services
Wisconsin Department of Natural Resources
40280
322
162
0511
E87074& 87262
100224
E-148&E1122
198948-B
12257
10586
8703
68-323
94002
02915
E-91
00113
999464070
ETC
VOLATILE DATA
ETC
QC SUMMARY
26SOIL UOLATILE SURROGATE RECOUERY
Lab Name: ETCNJ I Laboratory Contract:
Lab Code: Case No.: SAS No.:
Leve 1 : CLOU/MED >LOUI
SDG No -
010203040506070809101112131415161718192021222324252627282930
1 EPA1 SAMPLE NO.
1 UBLK011 A43761 A43771 A4377MS1 A4377MSD1 UBLK021 A4377111
1
SI( TOL ) *
9910310110110310099
S2(BFB)#
10299999898
10198
S3(DCE)#
94939594929998
OTHER ITOTOUT-- =0000000
page 1 of
51 (TOD = Toluene-d852 (BFB) = Bromofluorobenzene53 (DCE) = l,2-Dichloroethane-d4
QC LIMITS(81-117)(74-121)(70-121)
# Column to be used to flag* Values outside QC l i m i t sD Surrogates d i l u t e d out
recovery values
FORM I I UOA -2 1/87 Rev.
3BSOIL UOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOUERY
Lab Name: ETCNJ I Laboratory Contract:
Lab Code: Case No.: SAS No.: SDG No.:
M a t r i x Spike - EPA Sample No.: A4377 Le ve 1 : (LOUJ/MED) LOU)
111 COMPOUND
1 1 , 1-Dich loroethene1 Tr i ch 1 o roe t hene1 Benzene1 To 1 uene1 Ch 1 orobenzene1
1 SPIKE1 ADDED1 lug/Kg)
= = = 1 = = = = = = = = =15000. 00015000. 00015000. 00015000. 00015000. 0001
SAMPLECONCENTRATION
(ug/Kg )
0. 0000. 0000. 000o. uoo0. 000
MS 1CONCENTRATION!
tug/Kg) 1= = = = = = = = = = = = = | =5389.504 15509.875 15350.920 15423.779 15630.871 1
1
MS%REC #
108110107108113
1 QC 1ILIMITSI1 REC. 11 = = = = = = |159-172 1162-1371166-142 1159-139 1160-13311 1
111 COMPOUND
1 1 f 1-D i ch 1 o roe t hene
1 Benzene1 To 1 uene1 Ch lorobenzene
SPIKEADDEDCug/Kg )
5000. 0005000. 0005000. 0005000.0005000. 000
MSDCONCENTRATION
(.ug/Kg )
5358. 0245486.3725345.6155440 . 4445658.587
MSD*
REC #
107110107109113
HRPD #
10000
QC LIMITSRPD 1 k'EC .
= = = = = = | = = = = = =22 159-172O A \ £. *~} 1 "^ "7
21 166-14221 159-13921 160-133
1
# Column to be used to flag recovery and RPD values with an asterisk
* Ualues outside of l i m i t s
°PD: 0 out of 5 outside l i m i t sSpike Recovery: 0 out of 10 outside limits
Commen t s:
FORM I I I UOA -2 1/87 Rev.
4AUOLATILE METHOD BLANK SUMMARY
Lab Name: ETCNJ
Lab Code: Case No.:
Lab F i l e ID: >D1138
Date Analyzed 08/31/90
Matrix: (soil/water) SOIL
Instrument ID: GC/MS D
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:
Con t rac t :
SAS No.: SDG No.:
Lab Sample ID: UBLK01
Time Analyzed: 2100
Le^e1:tlow/med) LOW
1 EPA1 SAMPLE NO.!=,===„«===«=
Oil A4376021 A4377031 A4377MS041 A4377MSD05 106 107108 109110111 112 113 114115 116 117118 119 120121 122 123 124125 126 127128129 1301
LABSAMPLE ID
CA4376UCA4377UCA4377USCA4377UR
LABFILE ID
>D1140>D1141>D1142>D1143
TIMEANALYZED
2240233000200111
-ommen t s :
page 1 ofFORM IU UOA 1/87
10
4AVOLATILE METHOD BLANK SUMMARY
Lab Name: ETCNJ
Lab Code: Case No.:
Lab F i l e ID: >D1149
Date Analyzed 09/01/90
Mat r i x : (soil/water) SOIL
Instrument ID: EC/MS D
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:
Con t rac t :
SAS No.: SDG No.:
Lab Sample ID: U8LK02
Time Analyzed: 2249
Leve1:(low/med) LOW
I EPAI SAMPLE NO.
Oil A437702!03 I04!05 I06 I07!08!09 I10 111 112 113 114115 116117118 119 120 121 122 123 124125 126127128 129 1301
LABSAMPLE ID
CA4377U2
LABFILE ID
>D1152
TIMEANALYZED
0119
Commen t s:
page 1 ofFORM IU UOA 1/87 Rev.
11
5AUOLATILE ORGANIC GC/MS TUNING AND MASSCALIBRATION - BROMOFLUORObENZLNE CBFB)
Lab Name:ETCNJ I Laboratory
Lab Code: Case No.:
Lab F i l e ID: :D1132
Instrument ID: GC/MS D
Con t rac t :
SAS No.: SDb No.:
BFB Injection Date:08/31/90
BFB Injection Time:15 >1
Matrix:CsoiI/water) SOIL Leve 1 : ( 1 ow/med ) LOU) Co 1 umn : C pack/cap J PACK
m/e
50759596173174175176177
I1 ION ABUNDANCE CRITERIA
1 15.0 - 40.0* of mass 951 30.0 - 60 . 05< of mass 951 Base peak, 10054 r e l a t i v e abundance1 5.0 - 9 . 0% of mass 951 Less than 2 . 0* of mass 1741 Greater than 50.056 of mass 951 5.0 - 9.0% of mass 1741 Greater than 95. OS, but less than 101. OS of mass 1741 5.0 - 9. 054 of mass 1761
5i RELATIVEABUNDANCE
19.57.
100.7.0.
90.6 .88.6 .
52080 t64 (2 C4 I
0.0)1
7.1)197.3)17.3)2
1-Oalue is 54 mass 174 2-Ualue is H mass
THIS TUNE APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS:
0102U304050607080910111213141516171819202122
EPASAMPLE NO.
USTD50USTD200USTD150USTD100USTD20UBLKOlA4376A4377M4377MSA4377MSD
LABSAMPLE ID
QC70337USQC70337USQC70337USQC70337USQC70337USQC70337UCA4376UCA4377UCA4377USCA4377UR
LABFILE ID
>D1133>D1134>D1135>D1136>D1137>D1138>D1140>D1141>D1142>D1143
DATEANALYZED
08/31/9008/31/90U8/31/9008/31/9008/31/9008/31/9008/31/9008/31/9009/01/9009/01/90
TIMEANALYSED
1600173818281919201021 UO2240233000200111
page of FORM U UOA I/, Rev.
5AUOLATILE ORGANIC GC/MS TUNING AND nASSCALIBRATION - BROMOFLUOROBENZLNE (6FBJ
Lab Name : ETCNJ
Lab Code:
Lab F i l e ID: ^
Instrument ID: GC/MS D
I Laboratory
Case No. :
Cont rac t :
SAS No . : SDG No . :
BFB Injection Date: O^/
BFB Injection Time: / °) :
M a t r i x : (soi I/water) SOIL Leve1: C1ow/medJ LOW Co 1umn: Ipack/cap)PACK
m/e
50759596173174175176
ION ABUNDANCE
15.030.0Base5.0-LessGreat5.0-Gr ea t
177 1 5.0 -1
- 40. OX
CRITERIA
of mass 95- 60 . OX of mass 95peak, 19. OX o
than 2.e r than9 . OX o
er than9. OX o
OOX ref massOX of50. OX
f mass95. OX
f mass
lative abundance95
mass 174of mass 95174, but less than 101176
1 X RELATIUE1 ABUNDANCE
1 20.1 56.1 100.1 7.1 0.1 94.1 6.
OX of mass 174 1 91 .1 6.1
10030 (19 (7 t7 (
0.
7.97.7.
0)1
3)14)14)2
1-Ualue is X mass 174 2-Ualue is X mass 176
THIS TUNt APPLIES TO THE FOLLOWING SAMPLES, MS, hSD, BLANKS, AND STANDARDS:
1 ERA1 SAMPLE NO.|. »«. = »».„.„
Oil USTD5002 1 UBLK0203 1 A437704105 106 107108 109 110 111 112 113 114115 116 117118 119 120 121 122 1
LABSAMPLE ID
QC70337USQC70337U2CA4377U2
LABFILE ID
>D1147>D1149>D1152
DATEANALYZED
09/01/9009/01/9009/02/90
TIMEANALYSED
210722490119
page of FORM U UOA Rev.
ETC
SAMPLE DATA
14
1AUOLATILE ORGAN ICS ANALYSIS DATA SHEET
Lab Name: ETCNJ
Lab Code : Case No . :
M a t r i x : (soil/water) SOIL
Sample wt/vol: .0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. *K ( 8~
Column: (pack/cap) PACK
Cont ract:
SAS No.:
ERA SAMPLE NC
IIA4376I_____
**
SDG No.:
Lab Sample ID: CA4376U
Lab File ID: >D1140
Dat e Recei ved :
CAS NO. COMPOUND
Date Analyzed: 08/31/90
Dilution Factor: 100
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG U
74-87-3---------CH lorome thane______________I 100074-8 3-9------- --Bromome thane________________I 1UOO75-01-4-- —— — — Uinyl Chloride______________I 100075-00-3--—— -- — Chlo roe thane_______________I 100075-09-2----- —— -Methylene Chloride_________15006 7-64-1---------Ace tone_____________________1420075-15-0- —— - — --Carbon Disulf ide___________150075-35-4---------l,l-Dich loroethene_________I 50075-34-3————————1,1-Di chlo roe thane_________1500540-59-0——----1,2-Dichlorethene (total)__150067-66-3-- — -----Chloroform_________________1500107-06-2 — — ——— 1,2-Di chlo roe thane_________150078-93-3- ——— ——— 2-Butanone_________________12000071-55-6-- ————— -1,1,1-Tr i chlo roe thane______150056-23-5- —— - ——— Carbon Tet rach 1 or ide_______I500108-05-4- —————— Uinyl Acetate______________I 100075-27-4--------~Bromodichloromethane________I 50078-87-5---------l,2-Dich loropropane_________150010061-01-5-- — --cis-1,3-Dichloropropene_____I 50079-01-6-- — - — --Trich loroethene____________1500124-48-l--------Dibromoch lorome thane_______I 50079-00-5 ——— - ——— 1,1,2-Tr i chlo roe thane______150071-43-2 ———————— Benzene________________________150010061-02-6------trans-l,3-Dichloropropene__150075-25-2 ———————— Bromoform__________________1500108-10-1--------4-Me thy 1-2-Pentanone________I 1000591-78-6 ——————— 2-Hexanone__________________11000127-18-4----- —— Tet rach loroethene__________150079-34-5- ——————— 1,1,2,2-Tetrachloroethane__1500108-88-3 ————— --Toluene____________________1500108-90-7--------Ch lorobenzene______________I 500100-41-4———————Ethyl benzene__________________1500100-42-5 —— — — -Styrene_____________________15001330-20-7——————Xylene (total )___________1500____________________________________________ I_____
IUIUIUIUIUIIUIUIUIUIUIUIIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI
FORM I UOA I/87] §e
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ETC
Lab Code: Case No.:
Contract:
SAS No.:
EPA SAy?L.I NO.
ASDG No.:
Matrix: (soil/water) SOIL.
Sample vt/vol:.*? &> _____(g/mL)_§;_
Level: (low/ned)
% Moisture: not dec.
Column: (pack/cap)
Lab Sample ID:
Lab File ID: 7orf
Date Received: _j£
Date Analyzed: P
CAS NO. COMPOUND
Dilution Factor:
CONCENTRATION UNITS:(ug/L or ug/Kg) MStluG
Tetrahydrofuran_
FORM I VOA 1/87 Rev.
16
IEVOLATILE ORGAN ICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name:ETCNJ I Laboratory
Lab Code: Case No.:
M a t r i x : (soil/water) SOIL
Sample wt/vol: .1 (g/mLJ G
Le^el: (low/med) LOU
% Moisture: not dec. 18
Column: (pack/cap) PACK
Number TICs found: 2
Lon tract:
SAS No.:
EPA SAMPLE NO.
IIA4376I ____
SDG No.:
Lab Sample ID: Crt4376V
Lab Fi \e ID: >D1140Cy/23,/9
Date Received: 09/OS/1'?
Date Analyzed: 08/31/90
D i l u t i o n Factor: 82.0
CONCENTRATION UNITS:lug/L or ug/Kg) UG/Kb
CAS NUMBER
01.02.
COMPOUND NAME
UnknownUnknown
RT
21.2015.^8
EST . CONL
60U600
Q
JJ
FOKIM I UOA-T 1C 1/87
M
TOTAL ION CHROMPTOGRflMFi le >D1
78000-
60000-
50000-
48888-
30000-
30000-
10000-
0-
140 35.0-360.0 amu
. i . .
. B4376,, CR4376V ,QV70337,Sir
400 t 600 | 800 ; 1000
i §I j !•? I
ji:
7 9
4 e :
s § H 1i | 12) 1
l iI :i
15
1 ' I12
5 ^
S|
<4
1
iv ^Jl.
t ^ 2g «n
|I I
3
IWl8
16 Z9 34 38 33 36 40
Data File: >D1140::SSName: A4376,,Misc: CA4376U ,QU70337,S:M4,0.05,, 1:100 DL
Id File: ID0259::U1Title: XUOA13, IFB, PP/UOALast Calibration: 900901 17:25
Operator ID: EK1710Quant Time: 900901 17:27Injected at: 900831 22:40
Quant Output File: ~D1140::AQ
18
Operator ID:Output File:Data Fi le:Name : A4376 , ,Nisc: CA4376U
EK1710~D1140::AQ>D1140::SS
,QU70337,S:M4,
QUANT REPORT
Quant Rev: 7 Quan t TimeInjected at
D i l u t i o n Factor
1:100 DL
Page 1
900901 17:27900831 22:40
1. 00000
ID File: ID0259::U1T i t l e : XUOA13, IFB, PP/UOALast Calibration: 900901 17:25
Compound R.T. Scan* Area Cone Units
1)7)9)15)18)20)21)36)41)43)45)46)48)
*Bromoch lorome thaneMe-t- h v \ erre — L!I lui iUi -*- .y • • • ~t ~ ' T • ~ • * w ^Acetone I/ .Te t rahyd ro fu ran */1 ,2-Dichloroethane-D4 (SURR)
*1 ,4-Di f luorobenzeneMethyl ethyl ketone^/
*Ch Iorobenzene-d5Toluene-DS CSURR)
p-Bromof 1 uorobenzene (SURR)
mto Xmlenng —
11.
9.12.14.22.14.27.25.27.32.34.36.
62093367532061219333684714
266175207293341539343668635671809Q r- c
B9B
3875637121028371757788915960812205
117999174658
983342324•550*
250.20.211.276.231.250.1017.250.256.6.
248.4.
i n .
00
47766000040052121609R<r,
NGklf~"
NGNGNGNGNGNGNGNGNGklf"*
Nr;
97939510093979482957690O JL
91
* Compound is ISTD
19
REFERENCE STRNDORO SPECTRUMFile >C4697Bpk Rb 9999
10000-
j"-1— i—
Targat Reference SpectraNRM NOH
43s-
44 46 48 58 52
Scan 1667. 48 tain.
[-100
. . . . . . . . . I54 56 56
SOMPLE SPECTRUM <BRCKSROUND SUBTRRCTED)File >D1140 R4376, ,Bpk Rb 746
43I
506-•.
Q
X
42/s[
44
44 46
CR4376V .QV78337, 3:04,8. 8 Scan 297SUB 9-33 Kin.
58-
1
-100.•-PI
48 ' 50 ' 52 ' 54 ' 56 ' 58
SRMPLE SPECTRUM (UNRLTERED)File >D1140 04376, ,Bpk Ob 746
43:
500
^
42/
'
44
144 46
CR4376V ,QV70337,S:M4,0.0 Scan 2079.33 Min.
58
|
-100
-Pi48 ' 50 ' 52 ' '54 ' 56 ' 58
Data File: >D1140::SS Quant Output File: ~D1140::AQName: A4376,,Misc: CA4376U ,QU70337,S:M4,0.05,, 1:100 DLQuant Time: 900901 17:27 Quant ID File: ID0259::U1Injected at: 900831 22:40 Last Calibration: 900901 17:25
Compound No: 9Compound Name: AcetoneScan Number: 207Retention Time: 9.33 min.Quant Ion: 43.0Area: 10283Concentration: 211.47 NGq-value: 95
20
REFERENCE STftNDflRD SPECTRUMFile >CS010Bpk Rb 9999
10000-j i'
^ . i40
Tarset Reference SpectraNRFt NOn
43
72
1 \50 ' 60 ' 70 ' 80
Scan13.06
90 100
309tun .
-109
LSflMPLE SPECTRUM (BRCKGROUND SUBTRRCTED)File >D1140 R4376, ,Bpk Rb 4503
43
4000-•
gt
42 51
. . \ ,40 S0
CR4376V ,aV70337,S:M4,0.0 Scan 343SUB 14.61 Bin.
65
1 7357 63 / 10£Mf,.....',),!...,)...,,.,,.,,.,.,.,,,,,,,,,,,,,.'',,-
-100
69 70 80 90 100
SflMPLE SPECTRUM CUNRLTERED)File >01140 R4376, ,Bpk Rb 4503
43
4000-
-42
""
51
, , 1 ,40 50
CR4376V ,QV70337,SiM4,0.0
65
= 7 «J , 7\ -M" 1 160 70 80 90
Scan 34314.61 min.
161
-1B0
100
Data File: >D1140::SS Quant Output File: ~D1140::AQName: A4376,,Misc: CA4376U ,QU70337,S:M4,0.05,, 1:100 DLQuant Time: 900901 17:27 Quant ID File: ID0259::U1Injected at: 900831 22:40 Last Calibration: 900901 17:25
Compound No: 21Compound Name: Methyl ethyl ketoneScan Number: 343Retention Time: 14.61 mm.Quant Ion: 72.0Area: 12205Concentration: 1017.04 NGq-value: 94
REFERENCE STPNORRO SPECTRUMFil« >DBMS T«rs«t R«f«r«nc« Sp«c tr* Scan 251Bpk Ob 9999 CLP NRM NOM 251.00 Min.
4210008-
;& , r , ,-r^-, , , . ,- r-r . , . , -.--, . , . r-r- ,.,,-,-
43 78
48 44 46 52 56 68 64 68
-100
-072
SPMPLE SPECTRUM (BPCK6ROUND SUBTRPCTED)FileBpk
>D1140 P4376, , CP4376V .QV70337 ,S :M4 ,0 .0 Sc*n 293Pb 597 SUB 12.67 min.
42
J '460H 39{-"
J)
43
1 .
[-100
4e ' ' ' 44 ' ' '4e' ' '52' ' ' ?6 ' ' 's'e' ' '$V ' 'e'e' ' ' izSPMPLE SPECTRUM CUNPLTERED)Fi l* >01140 P4376, ,Bpk Pb 597
42
400^9
(3 i43
1 148 ' 44 ' 48
CR4376V ,QV70337,SiM4,0.0 Scan 29312.67 m i n .
Fee
52 ' 56 ' 60 ' 64 ' 68 ' 72
Data File: >D1140::SS Quant Output File: ~D1140::«QName: A4376,,Misc: CA4376U ,QU70337,S:M4,0.05,, 1:100 DLQuant Time: 900901 17:27 Quant ID File: ID0259::U1Injected at: 900831 22:40 Last Calibration: 900901 17:25
Compound No: 15Compound Name: TetrahydrofuranScan Number: 293Retention Time: 12.67 min.Quant Ion: 42.0Area: 7175Concentration: 276.76 NGq-^alue: 100
22
File >D1140 S4376,Epk Sb 9999
10000-
800*-
600£-
400CV-
''RPi CV-
'"J.,.,,File Ht:49KBpk Rb 9999
leeee-seeo-iea*-4000-
2000-
27\
cJ ____ 1
, CS437c.',' .QV73337 ,3 :M4 ,0 .05 . , icir, 51oSUE NPM 21 .20 mm.
41 rr
!
57""
-100
-80
-60
.i j i' £1 7 (-? i"i
• I ^tl "40 SS 126 ID£' 200
1-Bute-ne * c in 800.00 mm.
41
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-40
-2(<
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Data File: >D1140::S3Name: £43 76,,Misc. Date: LM4376U , C" .'"0777 , S : (14 , 0 . 05 , , 1:100 DLPT ( m i n i : 21 . 20Scan: ?13Area: 47979 Rank: 4Sem i -qi.an t i t a t i ve Cone ', unco r r ec t ed -1 : 30.06 NGSern i-quan t i t a t i'./e Cone ( c o r r e c t e d ): 601.22 ug/l- gC a l c u l a t e d usinq Istd: 1 , 4-D i f 1 uo r obenrene (51 22.24 min u t e s
1. i-Butene 56 C4HS
Sample f i l e : >D1140 Spectrum #:" e a r c h speed: 2 T i l t i n g option: S
5 17No. of ion ranqes searched:
P r o b . CAS # CDt-i $ ROOT K DK tt-LG TILT
11* 106°8':' °9S NBS49k' 25 54 2 0 65
23
Ti l * 51)1140Bpk flb 9999
1 IC00-
isoao-
90.*-
rea^
eaee-
seo*
4600-
3000-
2000-
10 FiFt
'",
fl4376
4
39
i
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65
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E7
i
i 58
in 3fci, m i n . |
:"*^100
_QIJ
-70
-r 0
L-,
|ao
he
-3a
r
^
Data F i l e : >D1140::SSN^me: A4376 , ,Misc. Data: CH47-76O , Q'.i^O??"7 , $ : M4 , 0 . O1? , , 1:100 DI-PT ' mm) : 15 .53bear: ?6bHrea: 70156 Rank: 5Sem i-quant i t at ive Cone ( unco r rec t ed ): 2'5.96 NGSem i -quan t i t a t i >.>e Cone C corrected ) : 599.27 uq.--'l qC a l c u l a t e d using Istd: Er ornoch 1 o rome thane |9 11.66 mi nut'
t-io PBtl h i t s for t h i s scan.
24
1AVOLATILE ORGAN ICS ANALYSIS DATA SHEET
ERA SAMPLE NO.
IIA4377
Lab Name: ETCNJ Con t rac t :
Lab Code: Case No.: SAS No.: SDG No.:
Matri x : (soil/water) SOIL Lab Sample ID: CA4377U
Sample wt/vol: .0 Cg/mL) 6 Lab File ID: >D1141
Level: (low/med) LOUI Date Received:
?i Moisture: not dec. "frit? <c\
Column: (pack/cap) PACK
CAS NO. COMPOUND
Date Analyzed: 08/31/90
Di lut ion Factor: 1UU
CONCENTRATION UNITS:lug/L or ug/Kg ) LJG/KG
I74-87-3---------Ch lorome thane______________I 100074-83-9---------Bromome thane________________I 100075-01-4- — - ———— Uinyl Chloride______________I 100075-00-3---------Ch lo roe thane________________I 100075-09-2- ————— --Methylene Chloride_________15006 7-64-1---------Ace tone_____________________I 580075-15-0---------Carbon Disulf ide___________I 50075-35-4- — ------1,1-Dich loroethene_________150075-34-3---------l,l-Dich lo roe thane__________I 500540-59-0----- — -1,2-Dichlorethene (total)__I 50067-66-3- ——— -- — Chloroform__________________1500107-06-2--------l,2-Dich lo roe thane_________I 50078-93-3- — -- — --2-Butanone_________________13100071-55-6--- — ----1,1,1-Trichloroe thane_______150056-23-5- — -- — --Carbon Te t rach 1 or ide________1500108-05-4- — - — --Uinyl Acetate_______________I 100075-27-4---------Bromodichloromethane________I 50078-87-5---------l,2-Dich loropropane________150010061-01-5---—-cis-l,3-Dichloropropene____150079-01-6---------Trich loroethene____________I 500124-48-l--------Dibromochloromethane_______I 50079-00-5- — —— ——1,1,2-Tr ich loroethane______150071-43-2- —————— -Benzene____________________150010061-02-6------trans-l,3-Dichloropropene___I 50075-25-2---------Bromof orm___________________I 500108-10-1 ——————— 4-Methyl-2-Pentanone________I 1000591-78-6 —— —— --2-Hexanone__________________I 1000127-18-4- — ———— Tet rach loroethene__________150079-34-5- — —— — -1,1,2,2-Tetrachloroe thane___1500106-88-3 ——————— Toluene____________________1500108-90-7----- — -Chlorobenzene______________1500100-41-4--------Ethyl benzene_______________1500100-42-5 — — ——— Styrene____________________15001330-20-7- ——— — Xylene (total )____________1500
Q
IUIUIU!UIUIIUIUIUIUIUIUIIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI LIIUIUIUIUIUI
FORM I OOA ev.
Lab Name:
Lab Code:
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
___________ Contract:____
Case No.: _____ SAS No.:
EPA SAXFLI NO.
,44377
Matrix: ( soil/water )
Sample wt/vol : ~O
Level: (low/med)
% Moisture: not dec. •' 6
Column: (pack/cap)
(9/aL).
CAS NO. COMPOUND
Tetrahydrofuran
SDG No. :
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor: /
CONCENTRATION TWITS.:(ug/L or uo/Kcr)
FORM X VOX 1/87 Rev.
26
IEUOLAT1LE ORGAN1CS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
Lab NamerETCNJ I Laboratory
Lab Code: Case No. :
natrix: (soil/water) SOIL
Sample wt/vol: .1 (g/mL) G
Level: Clow/med) LOW
% Moisture: not dec. 16
Column: (pack/cap) PACK
Number TICs found: 2
Con t rac t :
SAB No.:
ERA SAMPLE NO.
IIA4377I_____
SDG. No. :
Lab Sample ID: CA4377U
Lab File ID: >D1141o?/t3/<?*
Date Received: • OSMUOV9U
Date Analyzed: 06/31/90
D i l u t i o n Factor: 84.U
CONCENTRATION UNITS:tug/L or ug/Kg) UG/Kb
CAS NUMBER
01. 110-54-302.
COMPOUND NAME
HexaneUnknown
RT
21. 1915.53
EST. CONC
560890
-
Q
JJ
FORM I UOA-TIC 1/87 K'ev.
27
TOTPL ION CHROHPTOBRPMFile >D1141 35.0-860.0 »mu. B43". ,
TIC
70000-
60000-
peeee-
40008-
30000-
20000-
10000-
CP4377V ,QV70337,S:r
600
7 9
' 1
15JL. ^Ji
16 88 3£ 36 40
Data File: >D1141::SSName: A4377,,Misc: CA4377U ,QU70?37,S:M4,0.05,, 1:100 DL
Id File: ID0259::U1Title: XUOA13, IFB, PP/UOALast Calibration: 900901 17:25
Operator ID: EK1710Quant Time: 900901 17:28Injected at: 900631 23:30
Quant Output File: ~D1141::AQ
28
QUANT REPORT Page
Quant Rev: 7Operator ID: EK1710Output File: ~D1141::AQData File: >D1141::SSName: A4377,,Misc: CA4377U ,QU70337,S: M4/frr* -, , 1:100 DL
ID File: ID0259::UlTitle: XYOA13, IFB, PP/UOALast Calibration: 900901 17:25
Quant Time:In jected at:
Dilution Factor:
900901 17:28900831 23:30
1.00000
Compound R.T. Scan# Area Cone Units
1)7)9)15)18)20)21)36)41)42)43)45)46)48)
•Bromoch loro me thaneMethylene .ihloi ideAcetone \/Tet rahydrof urarn/l,2-Dichloroethane-D4 (SURR)
*1 ,4-Di f luorobenzeneMethyl ethyl ketone /
*Chlorobenzene-d5Toluene-DB (SURR)
Ghlui uUeii^mil!-p-Bromof luorobenzene (SURR)
11.618. 089.33
12.7014.4822.2414.6027.2125.9626.1227.3232.6734.5036.17
267176208295341541344669637641672810857900
388523484140399548798321638011901412144817715424412856
10140228583534
250.00 NG18.98 NG288.00 NG367.39 NG236.79 NG250.00 NGHMJ.OO MG//'250.00 NG252.80 NG6.64 NG5.91 NG
248.63 NG4.89 NG
10.62 NG
9497931009299
25" 9585969779917493
* Compound is ISTD
29
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QUANT REPORT
Operator ID: MGRMS QuantOutput File: /SD1152::AQData File: >D1152::U1Name: A4377,,Misc: CA4377U2 ,QU70337,S:M4,0 . 025,,
ID File: ID0259::UlTitle: XYOA13, IFB, PP/UOALast Calibration: 900902 15:34
Compound
7 Quant Time:In jected at:
Di lut ion Factor:
Page 1
900902 15:42900902 01:19
1.00000
1:200 DL
R.T. Scan* Area Cone Units
1)9)15)18)20)21)36)41)45)
*Bro mo chlorome thaneAcetoneTe t rahydrof uranl,2-Dichloroethane-D4 CSURR)
*1 ,4-Di f luorobenzeneMethyl ethyl ketone
*Ch Iorobenzene-d5Toluene-08 (SURR)p-Bromof luorobenzene (SURR)
11.9.12.14.22.14.27.25.32.
621459492453219772
266202291340540341668636810
41796803856038610217095211351127870184532106517
250.146.191.244.250.847.250.247.245.
008772210068002539
NGNGNGNGNG .NG NGNGNG
9594100949893849489
» Compound is ISTD
31
REFERENCE STflNDflRD SPECTRUMFile >C4697 T»rs«t R«f«r«nc« Sp«c tr*Bpk flb 9999 NRH NOD
43leeee-
e- , . i . i . i . i . i • i . i . i • i . i . i •
^
44 46 48 60 52 54
Scan 1667.48 Kiln.
kiee
L56 ' 58
SRMPLE SPECTRUM <BPCK6ROUND SUBTRPCTED)Fila >D1141 P4377, ,Bpk Pb 993
431000-
•42
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y
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58
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SPMPLE SPECTRUI1 <UNPLTERED>Fil« >D1141 P4377,,Bpk Pb 993
431000-
.
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441
i i " i i '44 46
CP4377V ,QV70337,S iM4,0.0 Scan 2089.33 Bin.
58|
-100
-fi48 50 5£ 54 56 58
Data File: >D1141::SS Quant Output File: ~D1141::AQName: A4377,,Misc: CA4377U ,QU70337,S:M4,0.05,, 1:100 DLQuant Time: 900901 17:28 Quant ID File: ID0259::U1Injected at: 900831 23:30 Last Calibration: 900901 17:25
Compound No: 9Compound Name: AcetoneScan Number: 208Retention Time: 9.33 min.Quant Ion: 43.0Area: 14039Concentration: 288.00 NGq-value: 93
32
REFERENCE STANDARD SPECTRUMFile >C£010 T«ra«t Reference Spectra Scan 309Bpk fib 9999 NRM MOM 13.06 Kin.
4310000-
•
0-
*~^
72
i. ......................... A.. ................................
-106
•
-048 58 60 76 80 90 108
SAMPLE SPECTRUM (BACKGROUND SUBTRACTED)File >D1152 A4377, , CA4377V2 ,QV70337,SsM4 ,0. Scan 341Bpk Ab 6646 SUB 14.53 «in.
65•,
4000-
f^ '
43^~
42\40
51
I I I' 50 60
67i"" 72 102
1-100•
70 ' 80 ' 90 ' 100SAMPLE SPECTRUM (UNALTERED)File >D1152 A4377..Bpk Ab 6648
•.
4800;
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CA4377V3 ,QV78337,S :M4 ,0 . Scan 34114.53 Bin.
6543
42\
40 '
5157
... , . ' !_ Jj
67^ 7£ 182
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-a,, 1.^4 W i-|-i-|. ir,-r, T- r- ,,T „,,,-,„, ,,,,.,,,,, j- r y, , , ,_r, j , „
50 60 70 80 90 100
Data File: >D1152::U1 Quant Output File: "D1152::AQName: A4377,,Misc: CA4377U2 ,QV70337,S: (14, 0 . 025 ,, 1:200 DLQuant Time: 900902 15:42 Quant ID File: ID0259::U1Injected at: 900902 01:19 Last Calibration: 900902 15:34
Compound No: 21Compound Name: Methyl ethyl ketoneScan Number: 341Retention Time: 14.53 min.Quant Ion: 72.0Area: 11351Concentration: 847.68 NG
93
33
REFERENCE STANDARD SPECTRUMFile >DBMS Target Reference SpectraBpk Rb 9999 CLP NRM NOM
4£10000-
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f^
148 44 48 52 56 60 64 68
Scan 251251.00 (tin.
72
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iz 76 88
SAMPLE SPECTRUM (BACKGROUND SUBTRACTED)Tile >D1141Bpk Ab 763
500-
:39V
A4377,, CA4377V .OV70337 ,S :H4 ,0 .0 Scan 295SUB 18.70 (tin.
4841/ 78
/ 831 \
hi 00;•
1 46 4V ' 4'e1 ' 'rfe ' '5V ' '6V ' «V ' 'e' ' ii ' >V ' 'eV ' "SAMPLE SPECTRUM (UNALTERED)File >D1141Bpk Ab 783
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04377,, CA4377V .QV78337 ,S :M4 ,0 .0 Scan 295
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48 44 48 58 56 60 64 68 78 76 60
Data File: >D1141::SS Quant Output File: "D1141::AQName: A4377,,Misc: CA4377U ,QU70337,S:M4,0.05,, 1:100 DLQuant Time: 900901 17:28 Quant ID File: ID0259::U1Injected at: 900831 23:30 Last Calibration: 900901 17:25
Compound No: 15Compound Name: TetrahydrofuranScan Number: 295Retention Time: 12.70 min.Quant Ion: 42.0Area: 9548Concentration: 367.39 NGq-value: 100
34
! File Mil 141 84377, ,Epk fib 9999
41
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Data File: 5D1141::SSName: A4377,,Misc Data: CA4377U ,Q"703?7 ,S : M4 , 0 . 05 , , 1:100 DI-RT Cm in >: 21 . 19Scan: 514Area: 46474 Rank: 4Bern i - q u a n t i t a t i v e Cone Cuncorrected 1 : 28.04 NGSemi-quantitative Cone ( corrected ): 560.76 ug-'kgCalculated using Istd: 1,4-Dif1uorobenzene @ 22.24 minutes
1. Hexane2. Pentane, 2-me thy 1-
86 C6H1486 C6H14
Sample file: >D1141 Spectrum #:= a r c h speed: 2 T i l t i n g option: S
514No. of ion ranges searched: 46
Prob. CAS # CON ^ ROOT
52* 110543 6971 NBS49K20* 10"7S35 4260 NBS49K
K DK #FLG TILT
7826
CON C ! P I"
5860
22 71
1854
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STANDARDS DATA
37
6hUOLATILE ORGAN1CS INITIAL CALIBRATION DATA
Lab Name:ETCNJ I Laboratory Contract:
Lab Code: Case No.: SAS No.: SDG No.:
Instrument ID:GC/MS D Calibration Date(s ) 08/31/90 08/31/9U
Matrix:(soiI/water) SOIL Leve1: (Iow/med) LOW Co 1umn: (pack/cap) PACK
Mm RRF for SPCC ( #) - 0.300 10.250 for Bromoform) Max JiRSD for CCC(») = 30.0*
ILAB FILE ID: RRF20 =>D1137IRRF100=>D1136 RRF15 0= >D1 1351
RRF50 =>D1133RRF200«>D1134
1 1 1 1 1 1 11 COMPOUND IRRF20 IRRF50 1 RRF100 1 RRF150 1 RRF2U 0 1
1 Ch 1 o rome t hane ••\ Bromome t hane
t .35511 .3121
lUinvl Chloride * .69611 Ch 1 o roe t haneiMethvlene Chloride1 Ace t oneICarbon Disulfide
.490 11.316 1.355 1
3.430 11 1 . 1-Dich loroethene * 1.11911 1 ,1-Dichloroethane # 2.32711 1,2-Dichlorethene (total) __ 1 1.2261IChlorofo-rm * 2.68311 1 ,2-Dichloroethane1 2-Bu t anone1 1 ,1 ,1-TrichloroethaneICarbon Te t rach lor i deI'Jmvl AcetateIBromodlchlo rome thane1 1 ,2-Dich loropropane *1 c is-1 ,3-Dich lorop ropene ___1 Tr ich loroethene1 D i bromoch 1 o rome thane1 I ,1 ,2-Trichloroethane1 Benzene1 trans-l,3-Dichl oropropene __1 Bromo form :!4-Methvl-2-Pentanone1 2 - He x a n o n e1 Tet rach loroethene
2.1671. 019 1.7881.665 1.399 1.6171.310 1.409 1.3941.440 1.3041.8981.3841.289 1.383 1.318 1.588 1
11,1 /2, 2-Tetrachl oroe thane _ * .508 1IToluene * .8211IChlorobenzene * 1.06811 Et hulbenzene * .56911 S t v r e n e1 Xvlene (total )
1 To 1 uene-d8iBromofluorobenzene1 1 ,2-Dichloroethane-d41
1.2671.725 1
1.4541.8471
2. 095 11
FORM
.418 1
.3671
.818 1
.555 11.2641 1.356 1
3.8121 31. 116 1 12.2881 21.2661 12.6201 21.9621 2. 0191.7471.662 1.450 1.576 1.286 1.3841.3671.389 1.262 1.8271.3541.255 1.3171.2541.562 1.449 1.7571
1. 008 1.556 1
1.203 1 1.696 1
1.401 1 1.8371
2. 062 1 2\
UI UOA
.3571
.3051
.732 1
.4941
.0931
.316 1
.430 1
. 071 1
. 1671
. 193 1
.5201
. 0291
. 019 1
.7241
.659 1
.379 1
.6041
.289 I
.398 1
.3591
.445 1
.2791
.799 1
.381 1
.322 1
.3271
.246 1
.5471
.473 1
.739 1
.979 1
.536 1
.2071
.675 1
.455 1
.8541
. 199 11
.3701
.273 1
.762 1
.503 11. 131 1.278 1
3.726 11. 076 12.208 11.21012.54212. 021 1. 019 1.7141.659 1.436 1.5941.2821.401 1.351 1.4341.263 1.7801.381 1.319 1.3101.245 1. 545 1.458 1.742 1.978.542
1.203.681
1.451.842
2.259
.371 1;257I.731 1.498 1
1. 100 1.263 1
3.66411. 066 12. 132 11.20412.453 11.870 1. 0171.6841.6471.418 1.562 1.2641.380 1.343 1.3941.2321.7561.3471.281 1.2741.2041.536 1.409 1.723 1.939 1.515 1
1. 133 1.648 1
l.:452 1. is i
2.i32 11
1111
RRF 1
.3741
.303 1
.748 1
.508 11. 181 1.3141
3.613 11. 090 12. 22411/220 12.563 12. 010 1. 019 1.731 1.658 1.416 1.590 1.286 1.3941.363 1.421 1.268 1.812 1.370 1.293 1.322 1.253 1.555 1.459 1.756 1.995 1.5441
1.2031.685 1
1.443 1.840 1
2. 16911
RS
61465e13423235451635356964912163754344
114
1D 1= = 1.8*. 1 1. 1*.3 1.71.6 1.6 1.4*./•#.3 1.5*. 4 1.3 1.3 1. 1 1.81.8 1.7*. 0 1.41.41. 71.71.71.5*.21.2 1.71.e#. 0*
.8*
. 0
. 1
.6
.6
. 0
1/87 Rev.
38
6AVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Naa«:.Lab Cod«:
In»truB«nt 10:
Contract:,SAS No. :Ca>« No.:
p Calibration Dat«(s):SZX« No. :
Matrix: (»oil/watar) s*>>i~ Level: (iow/m«d) Le><^ Column: (pacJc/cap)Min RR? for SPCC(I) • 0.300 (0.250 for Broaofon) Max tRSO for CCC(*) »LAB FILE ID:RRF100- >
RRT20 •RRT130-"
RRF50 •RW200-"
COMPOUKD
Tetrahydrofuran.
2-Dichloro«than«-d4
RRF20•mmmm*.n i
RRT50 IRRT100IRRT150
FORM vt VGA'
RRT200mm^mm. <5-5t
RRF"?W
RSS
6 . ;
1/87 Rev.
39
TOTAL ION CHROrtPTOGROflFile >D1137 35.6-260.e amu. VSTD20
zee
70006-
60886-
50C00-
48888-
38006-
aeeee-
10000-
GlC7e337VS,O.V7e337, Si
16 20 84 ' 26' ' 38 ' "36 '
Data File: >D1137::SS Quant Output File: ~D1137::AQName: USTD20Misc: QC70337US,QU70337;S:M4,5,, 2UL CAL I * I I+XUOA
Id File: ID0259::U1Title: XUOA13, IFB, PP/UOALast Calibration: 900830 08:26
Operator ID: EK1710Quant Time: 900831 20:53Injected at: 900831 20:10
40
QUANT REPORT Page
Operator ID: EK1710Output File: ~D1137::AQData File: >D1137::SSName: VSTD20Misc: QC70337US,QU70337,S:M4,5,,
ID File: ID0259::UlTitle: XUOA13, IFB, PP/YOALast Calibration: 900830 08:26
Compound
Quant Rev: 7 Quant Time:In jected at:
Di lu t i on Factor ',
900831 20:53900831 20:10
1.00000
2UL CAL I+II+XUOA
R.T. Scan* Area Cone Uni ts
1)2)3)5)6)7)8)9)10)11)12)13)14)15)16)17)18)19)20)22)23)23)24)25)26)27)28)29)30)31)32)33)34)35)36)37)38)39)40)41)42)43)44)
•Bromoch loro me thaneMe t hy 1 ch 1 or ideMethyl bromideVinyl ch lor ideCh loroethaneMethylene chlorideAero 1 e inAcetoneAery Ion i t r i leCarbon disulfideTrichlorof luorome thane1,1-Dichloroethylene1,1-DichloroethaneTetrahydrofuran1 ,2-Trans-dichloroethyleneCh lorof orml,2-Dichloroethane-D4 (SURR)1,2-Dich loroethane
*1 ,4-Dif luorobenzene1,1,1-TrichloroethaneCarbon t e t rach lor ideCarbon tet rach lor ideUinyl acetateDich 1 o rob romome thane1 ,2-Dichloropropanec is-1 ,3-DichloropropyleneTrichloroethyleneCh lorod ib romome thanebisCChloro methyl )etherBenzene1,1, 2- Trich loroethanetrans-l,3-Dichloropropylene2-Ch loroethyl vinyl etherBromof orm»Chlorobenzene-d5Me t hy 1- iso-bu ty 1 ketone2-Hexanone1 , 1 ,2 ,2-Tet rach loroethaneTet rach loroethyleneToluene-08 (SURR)To lueneCh lorobenzeneEthylbenzene
11234588899101112121313141422151516161618181919191919192022272224242425262729
.54
.24
.40
.29
.57
.01
.83
.83
.64
.72
.34
.08
.43
.51
.21
.83
.49
.57
.20
.92
.92
.31
.47
.85
.25
.52
.10
.72
.72
.61
.84
.84
.92
.48
. 18
.94
.49
.76
.80
.93
.13
.29
.58
264245477110173194194215217233252287289307323340342539377377387391401437444459475475472478478506546667558598605606635640670729
3931255754903109467703
207012643855805447
5393239953175893658626871928642190823403406916318751468647343431260414027320222266672573828729925558592198192507928351885212370018937157342513229076179857406265284828172
2504228434866
25672392971284981
258761732056625010114966992777185882407287642010125089827570
228427521
.00
. 14
.62
.64
.58
.18
.92
.49
.33
.34
.54
. 15
.79
.06
.30
.93
.21
.22
.00
.15
.34
.19
.60
.89
.73
.72
.91
.90
.23
.43
.93
.46
.13
.87
. 00
.69
.49
.05
.53
.66
.90
.64
.60
NGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNG
97979999969994949999999797100989894959895969897959595949810095929410097849491989896999779
41
QUANT REPORT Page 2
Operator ID: EK1710 Quant Rev: 7 Quant Time: 900831 20:53Output File: ~D1137::AQ Injected at: 900831 20:10Data File: >D1137::SS Dilution Factor: 1.00000Name: USTD20Misc: QC70337US,QU70337,S:M4,5,, 2UL CAL I + I I+XUOA
ID File: ID0259::U1Title: XUOA13, IFB, PP/UOALast Calibration: 900830 08:26
Compound R.T. Scan# Area Cone Units
45)46)47)48)
p-Bromofluorobenzene (SURR)St yrenem-Xy leneo+p-Xy lenes
32.34.34.36.
64478610
808855865897
104759627063536371774
207.61.28.29.
42190381
NGNGNGNG
92959790
* Compound is ISTD
42
TOTBL ION CHROMPTOSRPMfile >D1133 35.e-266.e MU.
eeeeen
70000-
60006-
50000-
40000-
seeee-1
80000-
10000-
QC7e337VS,QV7e337,Sl
6B0 , B00 ,
i • i • i • i • i * i • i • i • i • i • i • i * i • i • i • j • i • i6 IS 16 80 84 28 38 36 40
Quant Output File: ~D1133::AQData File: >D1133::UOName: USTD50Misc: QC70337US,QU70337,S:M4,5,, 5UL CAL I+II+XVOA
Id File: ID0259::U1Title: XUOA13, IFB, PP/UOALast Calibration: 900830 08:26
Operator ID: EK1710Quant Time: 900831 16:43Injected at: 900831 16:00
43
QUANT REPORT Page
Operator ID: EK1710Output File: ">D1133::AQData File: >D1133::UOName: YSTD50Misc: QC70337US,QU70337,S:M4,5, ,
ID File: ID0259::U1Ti t l e : XUOA13, IFB, PP/UOALast Calibration: 900830 08:26
Compound
Quant Rev: 7 Quant TimeIn ject ed a t
Di lut ion Fac tor
900831 16:43900831 16:00
1.00000
5UL CAL I+II+XUOA
R.T. Scan* Area Cone Units
1 )2)3)4)5)6)7)8)9)10)11)12)13)14)15)16)17)18)19)20)21)?2)23)23)24)25)26)27)28)29)30)31 )32)33)34)35)36)37)38)39)40)41)42)
*BromochloromethaneMe t hy 1 ch 1 o r i deMe t hy 1 bromi deDichlorodifluoromethaneUi ny 1 ch 1 or i deCh 1 oroe thaneMethylene chlorideAc ro 1 e inAcetoneAc ry 1 on i t r i leCarbon d isu 1 f ideTr ichlorof luoro me thane1,1-Dichloroethylene1,1-DichloroethaneTe t rahydrof uran1,2-Trans-dichloroethyleneCh 1 orof orml,2-Dic'hloroethane-D4 (SURR)1,2-Dichl oroe thane
*1 ,4-Di f luorobenzeneMethyl ethyl ketone1,1,1-TrichloroethaneCarbon t e t rach lor i deCarbon t et rach lor ideU i ny 1 acetateDichlorobromo me thane1,2-Dichloropropanecis-1 ,3-DichloropropyleneTrichloroethyleneChlorodibromomethanebis(Chloromethyl )etherBenzene1,1,2-Trichloroethanetrans-l,3-Dichloropropylene2-Ch 1 oroe thy 1 vi nyl etherBr omo f o rm*Ch Iorobenzene-d5Me t hy 1 - i so-bu t y 1 ketone2-Hexanone1 , 1 ,2 ,2-Tet rach loroethaneTe t rach lo roe thyleneToluene-08 (SURR)To 1 uene
11.2.3.4.4.5.8.8.8.9.9.
10.11.12.12.13.13.14.14.22.14.15.15.16.16.16.18.18.19.19.19.19.19.19.20.22.27.22.24.24.24.25.26.
60263820315900818958703210455727855163235998983753913158167875679090955021965283839516
26625547578
111173194196214217233253288291309324341344540343379379389393403439446461477476474480480507547668559599607607636641
40389168751484016121133049224255105377160143721385815398010982845166923946543
5111910580183298792631717903303
1282431556911372377259988794910265985630186678422207142152449436087824978438741287464085732747578307236818035197431
250.124.84.9.
128.137.158.
7294.58.
228.270.343.122.201.
6131.158.180.202.149.250.25.
239.32.
239.196.216.179.168.199.196.547.166.189.148.168.225.250.185.164.TL65.-&68 .220.98.
00153348256587718965509385056616450696004941752514652957803155934163512200929593663085
NGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNG
959397
979599939491999597971009798949696929697999797999694981009689931009788979495989596
44
QUANT REPORT
Operator ID: EK1710Output File: ~D1133:: AQData FiIB: >D1133::UOName: USTD50Misc: QC70337US,QU70337,S:M4,5,,
Quant Rev: 7 Quant TimeIn jected a t:
Di lut ion Fact or'
Page 2
900831 16:43900831 16:00
1. 00000
5UL CAL I + I I+XUOA
ID File: ID0259::U1Title: XUOA13, IFB, PP/UOALast Calibration: 900830 08:26
Compound R.T. Scan# Area Cone Units
43)44)45)46)47)48)
ChlorobenzeneEthy Ibenzenep-Bromof luorobenzene (SURR)St yrenem-Xy leneo +p-Xy lenes
272932343436
.33
.62
.72
.54
.86
.14
671730810857865898
1298267158310769915494087894179104
178.52.
204.145.66.71.
537489279448
NGNGNGNGNGNG
927988969790
Compound is ISTD
45
TOTAL ION CHROMRTOBRPnFile >D1136 35.0-260.0 anu. VSTD100
800 400
QC70337VS,QV70337,S i
3eee
88 38 36 404 8 18 16 80 84
Data File: >D1136::SS Quant Output File: /SD1136::AQName: USTDIOOMisc: QC70337US,Q«J70337,S:M4,5,, 10UL CAL I + IJ+XUOA
Id File: ID0259::UlTitle: XUOA13, IFB, PP/UOALast Calibration: 900830 08:26
Operator ID: EK1710Quant Time: 900831 20:02Injected at: 900831 19:19
46
QUANT REPORT Page
Operator ID: EK1710Output File: ~D1136::AQData File: >D1136::SSName: USTD100Misc: QC70337US,QU70337,S:M4,5,,
ID File: ID0259::U1Title: XUOA13, IFB, PP/UOALast Calibration: 900830 08:26
Compound
Quant Rev: 7 Quant Time:In jected at:
Dilution Factor:
900831 20:02900831 19:19
1.00000
10UL CAL I+II+XUOA
R.T. Scan* Area Cone Units
1)2)3)5)6)7)8)9)10)11)12)13)14)15)16)17)18)19)20)21)22)23)23)24)25)26)27)28)29)30)31)32)33)35)36)37)38)39)40)41)42)43)44)
•Bromoch loro me thaneMethyl ch lor ideMethyl bromideUiny 1 ch lor i deCh 1 oroe thaneMethylene chlorideAero le inAcetoneAery 1 on i t r i leCarbon disulf ideTrichlorofluoro me thane1,1-Dichloroethylene1,1-DichloroethaneTe t rahydrof uran1,2-Trans-dichloroethyleneCh lorof orml,2-Dichloroethane-D4 (SURR)1,2-Dichl oroe thane
*l,4-DifluorobenzeneMethyl ethyl ketone1,1,1-TrichloroethaneCarbon tet rach lor ideCarbon tet rach lor ideUinyl acetateDichlorobromomethane1,2-Dichloropropanecis-l,3-DichloropropyleneTrichloroethyleneCh lorodibromomethanebis (Ch loro methyl )etherBenzene1,1,2-Trichloroethanetrans-l,3-DichloropropyleneBromof orm*Ch Iorobenzene-d5Methyl- iso-butyl ketone2-Hexanone1, 1, 2, 2- Tet rach lor oe thaneTet rachloroethyleneToluene-08 CSURR)To lueneChlorobenzeneEthy Ibenzene
11234588899101112121313141422141515161616IB1819191919191922272224242425262729
.58
.24
.40
.29
.61
.01
.79
.87
.60
.72
.34
.11
.47
.55
.25
.83
.49
.61
.21
.53
.96
.92
.35
.51
.89
.29
.56
.10
.76
.73
.65
.84
.84
.48
.18
.94
.50
.77
.81
.93
.13
.34
.62
265245477111173193195214217233253288290308323340343539341378377388392402438445459476475473478478546667558598605606635640671730
4038928830246105910239919882981521912552127408277073203446864891750271447296382203524888221638731709966573
247747300162253061295322067279888413627912291015235147851273090954901304111099561294148473163787122374141611188284191167253318138668
250212139229245274
14388104452486637235380
1356229834721531025050464634763304553623493914491185322404319567250383319349328228192346101
.00
.10
.85
.35
.04
.76
.13
.57
.22
.73
.10
.24
.86
.19
.19
.13
.46
.04
.00
.96
.65
.44
.20
.37
.06
.74
.76
.51
.92
.33
.19
.32
.87
.05
.00
.58
.65
.31
.34
.81
.95
.56
.65
NGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNG
9697979997969295959997949710098979398978996979996979696939610096909496869692979794969580
47
QUANT REPORT
Operator ID: EK1710Output File: ~D1136::AQData File: >D1136::S3Name: USTD100Misc:
Quant Rev: 7 Quant Time:In jected at:
Di lut ion Factor;USTD100QC70337US,QU70337,S:M4,5,, 10UL CAL I+II+XVOA
Page 2
900831 20:02900831 19:19
1.00000
ID File: ID0259::UlTitle: XUOA13, IFB, PP/UOALast Calibration: 900830 08:26
Compound R.T. Scan* Area Cone Units
45)46)47)48)
p-Bromof luorobenzene (SURR)St yrenem-Xy 1 eneo+p-Xy 1 enes
32.34.34.36.
69478207
809855864896
110473312474171450349503
209291129138
.08
.46
.90
.77
NGNGNGNG
91949691
* Compound is ISTD
48
TOTAL ION CHROHflT06RPttFile >D1135 35.8-260.0 amu. U.C70337VS ,O.V7e337 ,S
1000
Quant Output File: ~D1135:: AQData File: >D1135::SSName: USTD150Misc: QC70337US,QU70337,S:M4,5,, 15UL CAL I+II+XUOA
Id File: ID0259::U1Title: XUOA13, IFB, PP/UOALast Calibration: 900B30 08:26
Operator ID: EK1710Quant Time: 900831 19:11Injected at: 900831 18:28
49
QUANT REPORT Page
Operator ID: EK1710Output File: ~D1135:: AQData File: >D1135::SSName: USTD150disc: QC70337US,QU70337,S:M4,5,,
ID File: ID0259::U1Title: XUOA13, IFB, PP/UOALast Calibration: 900830 08:26
Compound
Quant Rev: 7 Quant Time:In jected at :
Di lut ion Fac tori
900831 19:11900831 18:28
1.00000
15UL CAL I+I1+XUOA
R.T. Scan* Area Cone Units
1)2)3)4)5)6.X7)8)9)10)11)12)13)14)15)16)17)IB)19)20)°1 ),2)23)23)24)25)26)27)28)29)30)31)32)33)34)35)36)37)36)39)40)41)42)
*BromochloromethaneMe t hy 1 ch lor i deMethyl bromideDich lorod i f luoro me thaneUiny 1 ch lor ideO?i l.Q*1? Q>t*i.*riVPi'fcMethylene chlorideAero 1 e i nAcetoneAc ry Ion i t r i leCarbon disulfideTrichlorofluorome thane1,1-Dichloroethylene1,1-DichloroethaneTetrahydrofuran1,2-Trans-dichloroethyleneCh lorof orml,2-Dichloroethane-D4 (SURR)1,2-Dich lor oe thane
*l,4-DifluorobenzeneMethyl ethyl ketone1,1,1-TrichloroethaneCarbon tet rach lor ideCarbon tet rach lor ideUinyl acetateDich lo rob romome thane1 ,2-Dich loropropanec is-1 ,3-Dich loropropyleneTrichloroethyleneCh lorodibromomethaneb is ( Ch 1 orome thy 1 )e t herBenzene1 ,1 ,2-Tr ichloroethanetrans-1 ,3-Dich loropropylene2-Ch loroe t hy 1 viny 1 etherBromof orm*Ch Iorobenzene-d5Me t hy 1 - iso-bu t y 1 ketone2-Hexanone1,1,2,2-TetrachloroethaneTet rach loroethyleneToluene-08 (SURR)To luene
11.582.243.404.174.29"5 ."*y~/8.058.838.879.569.72
10.3411.1212.4712.5113.2513.8714.4914.6122.2514.5315.9615.9616.3516.5116.8918.2918.5619.1419.7619.7619.6519.8819.8820.9722.5227.2222.9824.5424.8124.8525.9826.17
26524547477
lit)174194195213217 '233253288289308324340343540341378378388392402438445460476476473479479507547668559599606607636641
406674511533290421092910614191380142282833395342182454569315745131237269420210171476123101379186124652717949810425
38450346723354730234615319821151804215783188997233780743434198161418762051998420717183813425012487598636184649219477194798298951
250.00 NG329.63 NG187.88 NG24.59 NG
358. 08 NG374.43 NG426.53 NG
21434.34 NG138. 16 NG691.22 NG793.08 NG982.00 NG354.51 NG582.25 NG
19561.08 NG453.57 NG525.35 NG221.31 NG463.22 NG250.00 NG77.00 NG686.98 NG94.07 NG714.23 NG570.04 NG670.67 NG530.49 NG527.58 NG573.50 NG657.69 NG1754.35 NG471.84 NG572.27 NG479.47 NG543.70 NG844.21 NG250.00 NG544.94 NG.476.47 NG~_508.08 NG90.55 NG~^2B.19 NG290.86 NG
96939893979799929993999395961009997969897959697999899959694951009790941009885969496979297
50
QUANT REPORT
Operator ID: EK1710Output File: ~D1135::AQData File: >D1135::SSName: USTD150disc: QC70337US,QU70337,S:I14,5, ,
ID File: ID0259::U1Title: XUOA13, IFB, PP/UOALast Calibration: 900830 08:26
Compound
Quant Rev: 7 Quant Time:In jected at:
Dilut ion Factor:
Page 2
900831 19:11900831 18:28
1.00000
15UL CAL I+II+XUOA
R.T. Scan* Area Cone Units
43)44)45)46)47)46)
Ch lorobenzeneEthyl benzenep-Bromof luorobenzene (SURR)Styrenem-Xy leneo+p-Xy lenes
272932343436
.38
.66
.73
.51
.94
.11
672731810856867897
39403121B107113077484450266464548513
519.154.206.435.194.209.
641230596294
NGNGNGNGNGNG
958089939790
Compound is ISTD
51
TOTRL ION CHROMPT08RPMFile >D1134 35.0-260.0 sum. VSTP200
800 400
aC7fl337VS , QV70337 , S i
e0e ,
48
IS 16 80 84 88 38 36 40
Data File: >D1134::SS Quant Output File: ~D1134::AQName: USTD200Misc: QC70337«JS,QU70337,S:M4,5, , 20UL CAL 1 + II+XUOA
Id F i Je : I D 0 2 5 9 : : U 1Title: XUOA13, IFB, PP/UOALast Calibration: 900B30 08:26
Operator ID: EK1710Quant Time: 900831 18:20Injected at: 900831 17:38
52
QUANT REPORT Page
Operator ID: EK1710Output File: "D1134::AQData File: >D1134::SSName: USTD200Misc: QC70337US,QU70337,S:M4,5,,
ID File: ID0259::U1Title: XUOA13, IFB, PP/VOALast Calibration: 900830 08:26
Compound
Quant Re<*>: 7 Quan t Time:In jec ted at
Di1ut ion Factor:
900831 18:20900831 17:38
1.00000
20UL CAL I+II+XUOA
R.T. Scan* Area Cone Un i ts
1)2)3 )4)5)6)7)8)9)10)11)12)13)14)15)15)16)17)18)19)20)>1 )-2)23)23)24)25)26)27)28)29)30)31)32)33)34)35)36)37)38)39)40)41)
"BromochloromethaneMethyl chlorideMe t hy 1 brom i deDi-chlorodifl uorome thaneUi ny 1 ch 1 o r ideCh loroe t haneMethylene chlorideAero le i nAcetoneAery 1 on i t r i leCarbon disulfideTr ich lorof luoromethane1,1-Dichloroethylene1,1-DichloroethaneTet rahydrof uranTet rahydrofuran1 ,2-Trans-dichloroethyleneCh lorof orml,2-Dichloroethane-D4 (SLJRR)1,2-Dichloroethane
*l,4-DifluorobenzeneMethyl ethyl ketone1,1,1-TrichloroetheneCarbon t et rach lor i deCarbon t e t rach 1 or ideUi ny 1 acetateDichlorobromomethane1,2-Dichloropropanec is- 1,3-Dich loropropyleneTrichloroethyleneChlorodibromome thanebisCChloromethyl )etherBenzene1,1,2-Trichloroethanet rans-1 , 3-D ich loropropylene2-Ch 1 oroe t hy 1 vi ny 1 etherBromof orm
*Ch Iorobenzene-d5Me t hy 1- i so-bu t y 1 ketone2-Hexanone1,1,2,2-TetrachloroethaneTet rach loroethyleneToluene-D8 CSURR)
11.2.3.4.4.5.8.6.8.9.9.10.11.12.12.13.13.13.14.14.22,14.15.15.16.16.16.18.18.19.19.19.19.19.19.20.22.27.22.24.24.24.26.
64305028396712899763744014505823278955672759999942539235591779796791919955259752838701
26726577780113176196198215218235254289291308309325342345541343379379390393403440446461477477474480480508548669559599607608637
4098560820421466174
119839816271803452900764318150446600734416550174809349501248943702
1974144021459148430660317911212463489865581284632722992854022861892532725072458822823939155754154216642224880197032201236129084141331105153211235276545187418
25044023635458493553
27024174820
10391285468749
22989341860167521857125092877117934728845662667747796
2165609672582627990250641-52804
-*42228
.00
.94
.01
.78
.28
.77
.03
.99
.35
.22
.96
.47
.55
.46
.73
.82
.89
.92
.69
.64
.00
.25
.11
.29
.78
.74
.42
.78
.71
.72
.17
.22
.96
.72
.61
.86
.77
.00
.44
.28
.49
.84
.34
NGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNG
959698969794969294979895969710010097989898969096999896999795939910097899310098839693979994
53
QUANT REPORT
Operator ID: EK1710Output File: ~D1134:: AQData File: >D1134::SSName: USTD200Misc: QC70337US,QU70337,S:M4,5,,
ID File: ID0259::U1Title: XUOA13, IFB, PP/UQALast Calibration: 900830 08:26
Compound
Quant Rev: 7 Quant Time'Injected at:
Dilution Factor:
Page 2
900831 18:20900831 17:38
1.00000
20UL CAL I+II+XUOA
R.T. Scan# Area Cone Uni ts
42)43)44)45)46)47)48)
To 1 ueneCh 1 orobenzeneEthylbenzenep-Bromo f 1 uorobenzene (SURR)St yrenem-Xy 1 eneo+p-Xy 1 enes
26.27.29.32.34.34.36.
16366576589721
641672731811858868900
373158484885265874105635585U15325561669319
377.665.195.200.547.247.266.
59053943073043
NGNGNGNGNGNGNG
97958090959791
* Compound is ISTD
54
7AUOLATILE CONTINUING CALIBRATION CHECK
Lab Name:ETCNJ I Laboratory Contract:
Lab Code: Case No.: SAS No.:
Instrument ID:GC/MS D Calibration Date: 09/01/90
SDG. No,
Time: 2107
Lab File ID: >D1147 I n i t Ca1ib. Dates(s): OB/31/90 OB/31/90
Hatrix: (soiI/water) SOIL Leve1: ( 1 ow/med) LOW Co 1umn: (pack/cap) PACK
Mm RRF50 for SPCC(#) - 0.300 (0.250 for Bromoform) Max SRSD for CCCC*) = 25.OS
11 COMPOUND
1 1KRF 1
1 Ch 1 orome thane # .37411 Bromome thane 1 .3031lUmul Chloride * .74811 Ch 1 oroe t haneIMetnulene Chloride1 Ace t one1 Carbon Disu 1 f ide
1 .50811. 181 1
1 .31413.613 1
1 1 . 1-Dichloroethene * 1.09011 1 ,1-Dichloroethane # 2.22411 1 ,2-Dichlorethene (total) __ 1 1.2201IChloroform * 2.56311 1 ,2-DichloroethaneI 2-Bu t anone1 1 ,1 ,1-TrichloroethaneICarbon Te t rach lor idelUmvl Acetate1 Bromod i chl orome t hane1 1 . 2-Di ch 1 oropropane *lcis-1,, 3-Dichl oropropene ___1 Tr ich loroetheneIDibromochloromethane11 rl .2-Trichloroethane1 Benzene1 trans-l,3-Dich 1 oropropene __IBromoform . =!4-Methvl-2-Pentanone1 2-Hexanone1 Tet rach loroethene
2. 0101. 019 1.731 1.658 1.416 1.590 1.286 1.3941.363 1.421 1.268 !.8121.370 1
I .2931.3221.2531.5551
1 1, 1,2,2- Tetrachlo roe thane _ # . 459 1IToluene * .75611 Ch lorobenzene * .9951lEthvlbenzene * .544'!1 St vrene1 Xvlene (total )
1 To 1 uene-dBIBromofluorobenzene1 1 ,2-Di chl oroe thane-d41
1.203 1.685 1
1.443 i.840 1
2. 169 11
1RRF50 1
.362 1
.3341
.722 1
.50711. 085 1.3271
3.413 11. 061 12. 190 11. 15712.48011.9851.0^01.6921.599 1.448 !.5551.281 1.3801.351 1.3H5 1.269 1.795 1.357!.2541.3321.266 1.5371. 464 1. 744 1.982 1.539 1
1. 182 1.660 1
1.459 1.849 1
2. 109 11
XD= = « = =3. H10.43.4*. 1
8. 14.45.52.6*1.5}5.23.2*1.24.25.49. 07.66. 11.6*3.63.38.4.5
2.03.4
13.5}2.94.83.3.9
1.7*1.2fl.9*
1.73.7
1.21:. 12
-i
FORM UII UOA 1/87
Lab Naa«:.Lab Cod«:
7AVOLATILE CONTINUING CALIBRATION CHECK
_ Contract:_____ SAS NO.:Case No.:
Instrun«nt ID:
Lab Fil« ID:
CalibrationSDG No.:
Tia«: =
it. Calib. Dat«(«);
Matrix: (»oil/wat«r) S ? L«v«l: (low/««d) c u.- Coluan: (pack/ cap)Min RRT50 for SPCC(I) • 0.300 (0.250 for Broaofon) Max ID for CCC(*j 2 5 . C \
CORPOUND
; Tetrahydrofuran.
I 55?•I 1
I
._
f:
J.I"*
l,2-Dichloro^thana^dT
rom vii VGA
ID
.1*
1/87 Re-.
56
TOTAL ION CHROMOT06RPM
48808-
30888-
20080-
ieee&-
File >D1147 35.0-260.0 *mu. VSTD5B
80000-
70000
60000
QC78337VS,QV703377sI
T I 1 ) I * I I ' I • I I • i • I " ) " I r I I8 IS 16 26 24 ZB 32 36 40
Quant Output File: "D1147::AQData File: >D1147::U1Name: USTD50flisc: QC70337US,QU70337,S:M4,5, , 5UL CAL I + II+XUOA
Id File: ID0259::UlTitle: XUOA13, IFB, PP/UOALast Calibration: 900901 17:25
Operator ID: MGRMSQuant Time: 900901 21:50Injected at: 900901 21:07
57
Operator ID: MGRMSOutput File: ~D1147::AQData File: >D1147::U1Name: USTD50Misc: QC70337US,QU70337,S:M4,5,,
ID File: ID0259::U1T i t l e : XVOA13, IFB, PP/UOALast Calibration: 900901 17:25
QUANT REPORT
Quant Rev: 7 Quant TimeInjected at
D i l u t i o n Factor:
Page 1
900901 21:50900901 21:07
1. 000005UL CAL I+II+XUOA
12;3;5)6)7)6)9)10)11)12)13)14)15)16)17)18)19)0)
21)22)23)23)24)25)26)27)26)29)30)31)32)33)34)35)36 ) «37)38)39)40)*,\\42)43)
Compound
) *Bromoch loromethane1 Methyl chloride1 Methyl bromide
Uinyl chlorideCh loroethaneMethylene chlorideAero le inAcetoneAcrylon i t r i leCarbon disulfideTnchlorof luoromethane1,1-Dichloroethylene1,1-Dich loroethaneTet rahydrof uran1,2-Trans-dichloroethyleneChloroforml,2-Dichloroethane-D4 (SURRi1 O r» • L * ^ OLJfTK J1,2-Dichloroethane
*l,4-Dif luorobenzeneMethyl ethyl ketone1,1,1-Trich loroethaneCarbon t e t rach 1 o r i deCarbon t e t rach 1 o r i deYinyl acetateDichlorobromome thane1,2-Dichloropropanecis-1 3-Dichloropropylene1 nchloroethyleneChlorodibromome thanebisCChloromethyl )etherBenzene1 ,1,2-Tr ichloroethanetrans-l,3-D,chloropropylene2-Chloroethylwnyl etherBromo formChlorobenzene-d5Methyl- l s o_ b u t y l ketone^-nexanone1, 1, 2, 2-Tet rach loroethanelet rachloroethylene""J-fYuene-TJB (SURR)To 1 ueneCh 1 orobenzene
R.T.
11.622 O s. 243.364.295.578 nc. Up8.798.839.609.76
10.3811.1512.5112.5513.2913.8714.5314.6422.2514.5716.0016.0016.4316.5416.9318.3318.6019.1419.8019.7619.6919.8819.8820.9722.5227.2222.9824.5324.812A.<3A25.9726.1327.37
Scan*
266245377110174193194214218234254289290309324341344540342379379390393403439446460477476474479479507547668559599606-bTT?636640672
Area
451981638215110326402293249062859751479615021
154259110960479589900379015227211210495316897381944093807
134581162331164458704310780854718739486826274873240751546505234569428306134928614357347629381506659477UB:?209496106780141019
Cone Uni
250.00 NG-242.27 NG276.04 NG241.45 NG249.63 NG999 "?o kir-*-£-T . sy (sik4173.13 NG260.91 NG395.11 NG236.19 NG237.75 NG243.38 NG246.20 NG261.33 NG237.01 NGOX1 QQ i.|f^ *+ 1. . oy Nla243.02 NG246.98 NG250.00 NG260.45 NG236.61 NG31.71 NG227.47 NG268.96 NG234.78 NG245.89 NG241.08 NG241.86 NG228.96 NG228.71 NG244.97 NG251.13 NG241.53 NG408. 17 NG216.21 NG250. 00 NG7.37 NG
2fc2.08 NG252.36 NG241.63 NGOCO QQ klf^£7^ . OO Nb
245.85 NG58246.91 NG
ts q
Q r-77
9299gof DO<is O
9895959099989598100999996969887979699979693959494
100959295
100978496919<tT 96979795
QUANT REPORT
Operator ID: MGRMSOutput File: 01147:. 'AQData Fi le: >D1147: :U1Name: USTD50Misc: QC70337US,QU70337,S:ri4,5,
ID Fi le: ID0259: : UlTit l e : XUOA13, IFB, PP/UOALast Calibration: 900901 17:25
Quant Rev: 7 Quant TimeInjected a t i
Di lut i on Factor
Page 2
900901 21:50900901, 21:07
1.00000
5UL CAL I+II+XUOA
Compound R.T. Scan* Area Cone Units
44;45)46;47;48;
Ethylbenzene 29.66 731 77353 247.82 NGp-Bromofluorobenzene (SURR) 32.73 810 121844 252.72 NGStyrene 34.55 857 169775 245.79 NGm-Xylene 34.94 867 94391 245.17 NGo+p-Xylenes 36.22 900 189412 481.47 NG
Compound is ISTD
8090959691
59
8AUOLATILE INTERNAL STANDARD AREA SUMMARY
Lab Name: ETCNJ Contract:
Lab Code: Case No.: SAS No.: SDG No.:
Lab File ID (Standard): >D1133 Data Analyzed: Q8/31/9U
Instrument ID: GC/MS D Time Analyzed: 160U
Hatr ix : (soiI/water) SOIL Leve1:(1ow/med) LOW Co 1umn: (pack/cap ) ____
01020304050607OB0910111213141516171819202122
12 HOUR STD
UPPER LIMIT
LOWER LIMIT
EPA SAMPLENO.
..*»»...»UBLK01A4376A4377A4377MSA4377MSD
IS1CBCMJAREA #
40389
80778...«.es.»
20194
4022338756386523872239137
RT
11.60
11.5711.6211.6111.6711.66
IS2(DFB)AREA #
171790
343580
85895
166162159608163S01160645163573
RT
22.23
22.2322.2022.2422.2622.20
I S3 ( CBZ )AREA #
128746
257492
64373
126268117999121448119629120366
RT
27.21
27.2127.2127.2127.2327. 17
Bromoch lorome thane1,4-Dif luorobenzeneChlorobenzene-d5
151 CBCM)152 (DFB)153 (CB2)
# Column used to fla_q, i-oAt,1; •?.
page __ of __—— ——
UPPER LIMIT - + 1UOMof internal standard area.LOWER LIMIT - - 50%of internal standard area.
area va'lues with an asterisk
FORM Oil I UOA 1/87
60
8AUOLATILE INTERNAL STANDARD AREA SUMMARY
Lab Name: ETCNJ Contract:
Lab Code: Case No.: SAS No.: SDG No.:
Lab F i l e ID (Standard): >D1147 Data Analyzed: 09/01/91)
Instrument ID: GC/MS D Time Analyzed: 2107
Mat r i x : (so i 1 /wa t er ) SOIL Leve1:(1ow/med) LGU) Co 1 umn :( pack/cap ) ____
01020304050607080910111213141516171819202122
12 HOUR STD
UPPER LIMIT
LOUER LIMIT
EPA SAMPLENO.
UBLK02A4377
ISKBCM)ARE.A #
45198
90396
22599
4103941796
RT
11.62
11.6211.62
IS2CDFB)AREA #
194409
388818
97205
173451170952
RT
22.25
22.2422.24
IS3(CBZ)AREA #
143573
287146
71786
==========130884127870
RT
27.22
27.2127.21
151 (8CM) = Bromochloromethane152 (DFB) = 1,4-Difluorobenzene153 (CBZ) = ChIorobenzene-d5
UPPER LIMIT - + 100%of internal standard area.LOWER LIMIT = - bO*of internal standard area.
# Column used to flag internal standard area values with an asterisk,
page __ of __
FORM U I I 1 UOA 1/87 Rev.
61
ETC
RAW QC DATA
62
MS Data File: >D1132::UO
Name: .................... Operator: EK1710Misc: p-BFB
Date/Time: 8/31/90 15:31
File >D1Bpk Ob 4
4800--
4400^
4000^
360EK
3200:
880fr-
-_
-1600^
-1200^
J800-«i
132363
50
\ ,,
1 68 -
N|ii 1.1
I * " 1 * '
40
c
'5
1
1.1 ll 180
p-BFB
>5t
174
133 147
I ' ' ' 1 ' ' ' 1 ' ' ' 1 " '
1S0 160
Sc»n10.51
X ,! V8,300
189nin .
rl!0
-100
•90
80
-76
-60
•50
40
30
20
f-10
63
MS Data File: >D1132::UO
Date/Time: 8/31/90 15:31Mi sc : p-BFB
>D1132189 NRM
Fi le: >D1132 Scan #:
m/z
37.1038. 0539. 0541. 0543. 0544. 0545. 0549.0550.0551. 0555. 0556. 0557. 05
I
54224855195237
nt .
.868
.492
.590
.957
.882
.870
.134
.088
.551
.776
.452
.461
. 105
m/z
58.0559. 0559.9561.0562.0563.0567.0568. 0569.0570. 0571. 0573.0574. 05
189
Int .
3.3231.6271.2385.7305.7533.5981. 031
11.82712.7891.9711.74214.37119.299
p-BFB
Re t n . t ime :
m/z
75.0576.0578.9579.9580.9581.9587.0588.0592.0593.0594.0595.0596. 05
Int .
57.2084.6764. 1711.3524.6761. 1923.2785.6153.0484.60711. 116
100. 0007.816
10.51
m/z
97.05102.95105.05105.95117. 00119. 00133.00141.00143. 00147.00149. 00155.00
Int .
.8021. 1461.008.871
1.3291.9251.8341.2611. 0542.292.711.825
m/z
173.175.176.177.179.190.192.194.207.208.209.222.
900000000095950505050595
Int .
90.6266.41888. 1966.395.802
1.8573.896.665
8.5722.1091.4443.392
64
MS Data File: >D1132::UO
Name: .................... Operator: EK1710flisc: p-BFB
Date /T ime: B/31/90 15:31
File >D113£TIC
p-BFB
40 80 120 160 200 240 880i i , i • i . , , i , . . i . i , i . • i i i . . i • . . i. i • i . . . i . . . i . . i i i i • i i . . i .-100
:90
-80
-70
-68
-30
-40
-30
-20
4.0 5.0 6.6 7.0 8.8 9.6 16.611.612.613.014.015.6
65
:ARINI
MS Data File: >D1145::Ul
Name: .................... Operator: MGRMSMisc: p-BFB
Date/Time: 9/01/90 19:52
File >D1145 p-BFBBpk Ob 5004
5200-
4800-
4400-
4000-
3600-
3200-
£800-
2400-
2000-
1600-
1800-
800-
400-
75
50
)5f 174
\
1 68
• I f I I 133 147
IlilJI JJl IJlLMlJ ./ . ,/„ S .
177X
40 ' 80 ' 180 ' 160
Sc*n 19316.56 min.
-110
807\ 80 6
K 1' ' ! • ' ' • • I1"
-i0e
-96
'-ez
-70
-60
-50
r40
38
-80
-10
800
66
MS Data File: >D1145::Ul
Date/Time: 9/01x90 19:52h i sc : p
>D1145193
File: >
m/z
37. 1038. 0538.9539.9541. 0543. 0544. 0545. 0546.9549. 0550. 0551. 05
-BFB
NRH
D1145 Scan #:
Irvt .
5.6554.9962.6981.7192.8384.4769. 0735.456.779
4.45620. 1045.975
m/z
55.0556. 0557. 0558.0559.0559.9561. 0562.0563.0568.0569.0570. 05
—r~
193
Int .
2.2.6.2.1.1.5.4.3.11.12.1.
398658675678319159556996857651450239
p-BFB
Re tr» . t ime :
m/z
73. 0574. 0575. 0576.0576.9578.9579.9580.9585. 0587. 0588. 0591.05
Int .
12.95017.36656.0154.796.979
3.5971. 1593.9771. 0393.3575.256.879
10.56
m/z
92. 0593. 0594. 0595. 0596. 05114.90117. 00119. 00127.90133. 00135.00140.90
Int.
3.4.
15 .100.7.,
1.1..
1.,
1.
217217671000294620119399819559779399
m/z
142.90147.00162.90173.90175.00175.90176.90192.95194.85206.95208. 05222.95
Int .
1. 0191.799.560
94. 1056.89491.6676.7353.857.600
5.4161.2993.477
67
MS Data F i l e : >D1145: :U1
M i s c : p-BFB
Film >D1145 35.6-866.6 *nu. p-BFB
46000^-
36066-
38000^
£8000^
84000-
20660-
16030^
12000-
6-
40 80 180 160 800 £40 880
11 i/
]/ 1
/ \
J V^vJ l^ __ Y4'.e c'.e 6 '.9 ?'.e e'.e $le le.e n'.e le'.e is'.e 14.0 is.
-166
-90
-86
-70
*e
-50
-46
-36
-26
0
68
1AUOLATILE ORGANJCS ANALYSIS DATA SHEET
ERA SAMPLE NO.
I IIUBLK01
Lab Name: ETCNJ
Lab Code: Case No. :
Matrix: (soil/water) SOIL
Con tract:
SAS No.:
Sample wt/vol: 5.0
Level: (low/med) LGUJ
% rioisture: not dec. 0
Column: (pack/cap) PACK
(g/mL) G
SDG No. :
Lab Sample ID: QC70337U
Lab File ID: >D1138os-/s>3/?0
Date Received: 09 'OBS**
Date Analyzed: 08/31/90
D i l u t i o n Factor: 1
CAS NO. - COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
74-87-3---- — —— Chl orome thane______________I 1074-83-9---------Bromomethane_______________I 1075-01-4- ——————— Uinyl Chloride______________I 1075-00-3--- ———— -Chloroe thane_______________I 1075-09-2---------Methylene Chloride_________1467-64-l---------Acetone____________________I 1075-15-0---------Carbon Disulf ide___________I 575-35-4- — -- ——— 1,1-Dichloroethene_________1575-34-3- ——— --—1,1-Di chloroe thane_________15540-59-0--------l,2-Dichlorethene (total)__1567-66-3---------Ch lorof orm_________________I 5107-06-2--------l,2-Dich loroe thane_________I 578-93-3 — --- —— -2-Butanone_________________I 1071-55-6- ———— -—1,1,1-Tri ch loroe thane______1556-23-5- — - ———— Carbon Te t rach 1 o r i de_______15108-05-4——— — — Uinyl Acetate______________I 1075-27-4---------Bromodichloromet hane_______ I 578-87-5-- ——— ---1,2-Dichloropropane________1510061-01-5 ———— -cis-l,3-Dichloropropene____1579-01-6--- —— ---Trichloroethene____________15124-48-l--------Dibromoch 1 orome t hane_______ I 579-00-5 ——— -———1,1,2-Tr i ch 1 oroe t hane_______1571-43-2- ——— - —— Benzene____________________1210061-02-6------trans-l,3-Dichloropropene__1575-25-2---------Bromof orm__________________I 5108-10-1--------4-Me thy 1-2-Pent a none_______ I 10591-78-6 — - ———— 2-Hexanone_________________I 10127-18-4--------Tetrachloroethene___________1579-34-5------- —1,1,2,2-Tetrachloroethane__15108-88-3 ——— — — Toluene____________________12108-90-7--------Ch lorobenzene______________I 5100-41-4- —— ----Ethyl benzene_______________15100-42-5--------Styrene_____________________ I 51330-20-7——————Xylene (total )_____________15___________________________________________I
U
IUIUI LIIUI JIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIJIUIUIUIUIUIUIJIUIUIUIUI
FORri I UGA 1/87 Rev.
69
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAXFLE NO.
Lab Nana;
Lab Coda: Casa No.:
Contract:,
SAS No.: SDG No. :
Matrix: (»oil/vatcr) .got u
Sainpla vt/vol : 5,0 (q/aL)
Laval: (low/B«d)
\ Moistur*: not d«c. O
Column: (pack/cap)
Lab Sanpl* ID:
Lab Fil« ID: >J> 1
Data R«ctiv«d: *9/
Data Anaiyzad:
CAS NO. COMPOUND
Dilution Factor:
CONCENTRATION UNITS:(ug/L or ug/Kg)
Tetrahydrofuran_
FORM I VOA
i
1/87 Rev.
70
IEVOLATILE ORGAN ICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
IOBLK01Lab Name:ETCNJ I Laboratory
Lab Code: Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: Uow/med) LOW
?i Moisture: not dec. 0
Column: (pack/cap) PACK
Number TICs found: 0
Con tract:
SAb No.: SDG No.:
Lab Sample ID: QC70337U
Lab File ID: >D1138
Date Received: f&*4l-& HJ "/
Date Analyzed: 08/31/90
D i l u t i o n Factor : 1. U
CONCENTRATION UNITS:(ug/L or ug/K'j ) UG/KG
CAS NUMBER
111
COMPOUND NAME
FORM I UOA-TIC
RT EST. CONC
.
—— > —————————-i1/87
7
Q
ke^.
1
TOTfiL ION CHROMflTOGRfiMPile >D1138 35.0-S60.8 amu. VBLK01 QC70337V ,QV70337,Sl
88000-
70000-
60000
50000-
30000--
20000-
10000-
0-
S00 f 400 i 600 ( 800 ( 1000
i ! *P* c S .j-. p1 I il !1 ic
7
5 I5 Qcr
4 8 IS
N
, 22 281J1
5 h
•r_^
40
1 11 1s
3
S.
4648
1 6 ' 2 0 24 ' 28 ' 32 ' 36 ' 40
Data File: >D1138::SSName: UBLK01Misc: QC70337U ;QU70337,S:M4,5,,
Id Fi le: ID0259: :U1T i t l e : XUOA13, IFB, PP/UOALast Calibration: 900901 17:25
Operator ID: EK1710Quant Time: 900901 17:30Injected at: 900831 21:00
Quant Output File: ~D1138::AQ
BLANK
72
, QUANT REPORT
Opera tor ID:Output File:Data File:Name: UBLK01nisc: QC70337U
EK1710"-D1138:>D1138:
Quant Rev: 7:AQ:SS
Quant Time'In jec ted at
Dilution Factor.'
Page 1
900901 17:30900831 21:00
1.00000
,QV70337,S:ri4,5, , BLANK
ID File: ID0259::UlTitle: XUOA13, IFB, PP/UOALast Calibration: 900901 17:25
Compound R.T. Scan* Area Cone Uni ts
1 )7)18)20)22)28)31)36)40)41)42)43)45)46)48)
*Bromoch loro me thaneMethylene chloride L/l,2-Dichloroethane-D4 (SURR)
*l,4-Difluorobenzene1-, 1 , 1- Ti nil lui ue Uitine
Benzene i/*Ch Iorobenzene-d5Tm t . - nh i TnrtJiy lege—Toluene-08 (SURR)To 1 uene \X
p-Bromo f 1 uorobenzene (SURR)
11814221519192724252627323436
.57
. 01
.48
.23
.91
. 09
.68
.21
.83
.96
.12
.32
.71
.57
.13
265173340540377459474668607636640671810858898
40223363581881166162240522255098
1262682075
18109234423398
10833432764181
250.. 19.234.250.4.9.9.
250.7.
248.9.6.
255.5.12.
0013590095224500405601764939
NGNGNGNGNGNGNGNGNGNGNGNGNGNGNG
989593989590948596929882898791
* Compound is ISTD
73
REFERENCE STfiNDQRD SPCCTRUtlFile >C4697Bpk fib 9999
49. s
•
0-
47t
51
f48 5c
Tarset Reference Spectra Scan 143HRH NOn 6.59 fnin.
84 [-100-^ t
t56 60 64 6e 7£ 76 66 84
SfiMPLE SPECTRUM <BflCKGROUND SUBTRACTED)File >D1138 VBLK01 QC70337V ,QV70337 ,S :M4 ,5 , Scan 173Bpk Pb 367 SUB 8.01 min.
49400-
-
gK
47
i l
' 34 h10051S
JL48 ' 5S ' 56 ' 60 ' 64 ' 68 ' 7£ ' 76 ' 80 ' 84
SBMPLE SPECTRUM <UNBLTERED>FileBpk
>D1138fib 367
400n
01
44
VBLK01 QC70337V .UV70337 ,S :M4 ,5 , Scan 1738.01 min.
49
47
1 ,
' 54f51 in
Ve' ' 1B
I2
1 | 1 5 I 6 1 1 '6'0' "6V 'e'e' ' V8' ' '?6 ' 'e'e' "84 ' '
-100
•e
Data File: >D1138::SS Quant Output File:Name: YBLK01Misc: QC70337U ,QU70337,S:M4,5,, BLANKQuant Time: 900901 17:30 Quant ID File: ID0259::LJ1Injected at: 900631 21:00 Last Calibration: 900901 17:25
Compound No: 7Compound Name: M e t h y l e n e c h l o r i d eScan Number: 173Retention Time: 8.01 min.Quant Ion: 84.0Area: 3635Concentration: 19.13 NGq-value: 95
74
REFERENCE STflNOflRD SPECTRUMTile >C4697 Taraet Reference SpectraBpk fib 9999 SUB
7810000-
.
0-| . ! . | . | . I i I . I .
52
II 146 60 60 180
NRrt MOM
128 140 168
Scan 43617.95 min.
-100
-n188 288
SfiMPLE SPECTRUM (BRCK6POUND SUBTRRCTED)Tile >D1138 VBLK01Bpk Hb 259
78
200-• 5S (.1
rv |H ' " '40 69 80
QC70337V ,aV70337,S:M4,5,SUB
S3*•"
160 120 140 160 180
Scan 47419.68 min.
[-100
267 L|L0
200
SRMPLE SPECTRUM <UN«LTERED>File >D1138Bpk fib 859
289-•
Ck_
52
40
VBLK01 QC70337V .QV70337 ,S :H4 .5 , Scan19.68
78^
61* / 1fi 1 1
83 207^ ~*-.\
60 ' 80 ' 100 ' 120 ' 140 ' 160 ' 180 ' 200
474mm .
f-100
LB
Data File: >D1138::SS Quant Output File:Name: UBLK01Misc: QC70337U , QU70337 , S: (14,5 , , BLANKQuant Time: 900901 17:30 Quant ID File: ID0259::U1Injected at: 900831 21:00 Last Calibration: 900901 17:25
Compound No: 31Compound Name: BenzeneScan Number: 474Retention Time: 19.68 min.Quant Ion: 78.0Area: 5098Concentration: 9.45 NGq-value: 94
75
REFERENCE STBNDRRP SPECTRUMFile >C4697Bpk fib 9999
10000-
! 39
a-C i40
Target Reference SpectraNRH NOft
91\ 92
- I1 II's'e' ' 'e'e' ' '100' ' '120 ' '140' ' 'lie '
Scan 66224.39 A. in.
-iee
_o
180 200SOUPLE SPECTRUM (BRCKGROUND SUBTRACTED)File >D1138 VBLK01 QC78337V .QV70337 ,S :M4 ,5 ,Bpk Pb 502 SUB
91
400-
0-
1
39 65 1
40 60 80 100 120 140 168 180
Scan 64026.18 min.
207
200
-180
"SfiMPLE SPECTRUM CUNOLTERED)File >D1138Bpk fib 1957
2000-
_-
0J , .
42/
n 1 1 if40
VBLK01
•54 78
.1 1 .. «l i .68 80
aC70337V ,aV70337,S:M4,5, Scan 64026.12 min.
98
91
I,• II . .1
'
\ 807\
i i..
-100
-e180 ' 120 ' 140 ' 168 ' 180 ' 888
Data File: >D1138::SS Quant Output File: ^01138::AQName: UBLK01Misc: QC70337U ,QU70337,S:M4,5,, BLANKOuant Time: 900901 17:30 Quant ID File: ID0259::U1Injected at: 900831 21:00 Last Calibration: 900901 17:25
Compound No: 42Compound Name: TolueneScan Number: 640Retention Time: 26.12 min.Quant Ion: 92.0Area: 3442Concentration: 9.01 NG
98
76
1AUOLATILE ORGAN 1CS ANALYSIS DATA SHEET
ERA SAMPLE NO.
IIUBLK02
Lab Name: ETCNJ
Lab Code:
Cont ract:
Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 Ig/mL) G
Level: (low/med) LOU)
% Moisture: not dec. 0
Column: (pack/cap) PACK
CAS NO. COMPOUND
SAS No.: SDG No.:
Lab Sample ID: QC70337U2
Lab F i l e ID: >D1149
Date Received: Q9-1'00-'"?U
Date Analyzed: 09/01/90
D i l u t i o n Factor: 1
CONCENTRATION UNITS:lug/L or ug/Kg) UG/KG U
I74-87-3-- — - ——— Chl or ome thane_______________I 1074-83-9----- — --Bromo me thane________________I 1075-01-4- — —— ---Uinyl Chloride______________I 1075-00-3---------Ch loroe thane________________I 1075-09-2- — - — —— Methylene Chloride__________1567-64-l---------Acetone_____________________I 1075-15-0---------Carbon Disulf ide___________I 575-35-4———-———1,1-Dichloroethene__________1575-34-3---- ——— -1,1-Dich loroe thane__________15540-59-0————---1,2-Dichlorethene (total)___1567-66-3- — ------Ch lorof orm__________________I 5107-06-2------—1/2-Dich loroe thane__________1578-93-3- — — ——— 2-Butanone__________________I 1071-55-6- —— ---—1,1,1-Trich loroe thane_______1556-23-5---------Carbon Tetrachlor ide________15108-05-4--- — - — Uinyl Acetate_______________I 1075-27-4---------Bromodichl or ome thane_______ I 578-87-5---------l,2-Dich loropropane________I 510061-01-5------cis-l,3-Dichloropropene_____1579-01-6--- — ----Trich loroethene_____________I 5124-48- l--------Dibromoch 1 orome thane________ I 579-00-5 —— — ——— 1,1,2-Tr ich loroe thane______1571-43-2- ———— ---Benzene_________________1510061-02-6---—-trans-l,3-Dichloropropene___1575-25-2---------Bromo form__________________15108-10-1- ————— -4-Methyl-2-Pentanone________I 10591-78-6- — — ---2-Hexanone__________________I 1012 7- 18-4- ------- Tetrach loroethene__________I 579-34-5---—----i,1,2,2-Tetrachloroethane__15108-88-3 ——————— Toluene____________________15108-90-7--------Ch lorobenzene_______________I 5100-41-4--------Ethyl benzene______________15100-42-5- —— —— -Styrene_____________________151330-20-7— ——— -Xylene (.total )_____________15
_____ _______ ___________I __
IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI
FORM I UOA 1/8
1AUOLATILE ORGAN1CS ANALYSIS DATA SHEET
ERA SAMPLE NO.
IIUBLK02
Lab Name: ETCNJ
Lab Code: Case No. :
M a t r i x : Isoil/water) SOIL
Sample wt/vol: 5.0 Ig/mL) G
Le^e1: (low/med) LOW
H Moisture: not dec. 0
Column: Cpack/cap) PACK
Con tract:
SAS No.:
I
LAS NO. COMPOUND
SDG 'No. :
Lab Sample ID: QC7U337<J^
Lab F i l e ID: >D1149
Date Received: 09;fDO;"?U
Date Analyzed: 09/01/90
Dilution Factor: 1
CONCENTRATION UNITS:Cug/L or ug/Kg) UG/kG LJ
I74-8 7-3---------Ch lorome thane______________I 1074-83-9---- — ---Bromome thane_______________I 1075-01-4——————--Uinyl Chloride____________I 1075-00-3 — —— - —— Ch lor oe thane_____________I 1075-09-2- ———— ---Methylene Chloride_________1567-64-l---------Acetone__________________I 1075-15-0-- —— - — -Carbon Disulf ide___________1575-35-4———————1 ,1-Dich loroethene_________1575-34-3————————1,1-Dichlo roe thane_________15540-59-0 —— ————1,2-Dichlorethene C tota l )__1567-66-3- —— - ——— Chloroform_________________15107-06-2--------l,2-Dich loroe thane_________1578-93-3---------2-Butanone_________________I 1071-55-6- —————— -1,1,1-Tr ich loroe thane______1556-23-5---------Carbon Tetrachlor ide_______I 5108-05-4—- ——— -Umyl Acetate_____________\ 10•75-27-4---------Bromod ich lorome thane_______ I 578-87-5---------l,2-Dich loropropane________I 510061-01-5------C1S-1,3-Dichloropropene_____I 579-01-6---------Trich loroethene____________I 5124-48-l--------Dibromoch 1 oromethane_______ I 579-00-5————————1,1,2-Tr ich loroe thane______1571-43-2- ——— ——— Benzene____________________1510061-02-6-- — --trans-l,3-Dichloropropene___I 575-25-2- — - ——— -Bromoform__________________15108-10-l--------4-Methy 1-2-Pen t anone_______ I 10591-78-6 ——————— 2-Hexanone_________________I 10127-18-4- ——— — -Tetrach loroethene__________1579-34-5---------l,l,2,2-Tetrachloroethane__15108-88-3 ——————— Toluene____________________15108-90-7--------Ch lorobenzene______________I 5100-41-4————- — Ethyl benzene_______________15100-42-5---- —— -Styrene__________________151330-20-7—— — --Xylene t total )____________15
IIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI
FORM I UOA 1/8
Lab Nana:
Lab Cod*:
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
_ Contract:____
___ SAS No.:
EPA SAXrLE NO.
Ca»a No.: SDC No. :
Matrix: (soil/water) _S£Sainpl* wt/vol: S~O ___
L«v«l: (low/m«d)
\ Moistur*: not d«c.
Column: (pack/cap)
(g/nL) %"Lab Sampla ID:
Lab Fil« ID:
Data Rccaivad:
Data Analyzad: ^f/olDilution Factor: /
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg)
Tetrahydrofuran_ UL
FORM I VOA 1/8? Rev.
78
IEVOLATILE ORGAN 1CS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
Lab Name:ETC Corp. I Laboratory
Lab Code: Case No.:
Matrix: I soi1/water) WATER
Sample wt/vol: 5.0 Cg/mL) ML
Level: Clow/med) LOLJ
% Moisture: not dec.
Column: (pack/cap) PACK
Con t rac t :
SAS No.:
EPA SAMPLE NO.
IIUBLK02I______
SDG No.:
Lab Sample ID: QC7033702
Lab Fi l e ID: >D11490?/2 >/?°
Date Received: 9-9.•'01••fl'C
Date Analyzed: 09/01/90
D i l u t i o n Factor: 1.0
Number TICs found: 0CONCENTRATION UNITS:Cug/L or ug/Kg) UG/L
CAS NUMBER COMPOUND NAME
FORM I UOA-T1C
RT EST. CONC
1/87
7
Q
Kev.
9
TOTflL ION CHROMRT06RPMFi le >D1149 35.0-860.6 amu. VBLK0S OC70337VS .QV70337 ,S i
800 , 4T60 A 600 i 600 , 1606
70000-
65006-
60006-
55800-
56000-
45006-
40006-"
35008-
30908-
85006--
86006--
15666-
10600-
tt.
J*»
I B - 5 -g S _f 1 if I
. § | II I
I ? ?c ?5 S-- ^V ®
I 1a o
\
C«l^|
I4 8 18 16 £0
f §g
I" 1i
JTj|[j
3 J
IL84 88 38 36 40
Data File: >D1149::U1Name: UBLK02rHsc: QC70?37U2,QU70337,S:M4,5,, BLANK
Id File: ID0259::U1Title: XUOA13, IFB, PP/UOALast Calibration: 900902 15:34
Operator ID: (1GRMSQuant Time: 900902 15:36Injected at: 900901 22:49
Quant Output File: ~D1149::AQ
80
QUANT REPORT Page 1
Operator ID: MGRMS Quant Rev: 7 Quant Time: 900902 15:36Output File: ~D1149::AQ Injected at: 900901 22:49Data File: >D1149::(J1 Dilution Factor: 1.00000Name: UBLK02Misc: QC70337U2,QU70337,S:M4,5,, BLANK
ID File: ID0259::UlTitle: XUOA13, IFB, PP/UOALast Calibration: 900902 15:34
Compound R.T. Scan# Area Cone Units
1 )18)20)36)41)43)45)
*Bromochloro me thane1 ,2-Dichloroethane-D4 (SURR)
*1 ,4-Di f luorobenzene*Ch Iorobenrene-d5Toluene-08 (SURR)CMaPeb«na»no -p-Bromofluorobenzene (SURR)
11142227252732
.62
.53
.24
.21
.96
.33
.68
266341540668636"71O / 1809
41039860231734511308841900762721
111869
2502482502502485
251
. 00
.49
. 00
. 00
.82
.29
.79
NGNGNGNGNGNGNG
94959883957789
* Compound is ISTD
81
Lab Name: ETCNJ
1AUOLATILE ORGAN 1CS ANALYSIS DATA SHEET
Cont rac t:
ERA SAMPLE NO.
IIA4377MSI_______
Lab Code: Case No.: SAS No.: SDb No.:
Matrix: (soil/water) SOIL Lab Sample ID: CA4377Ub
Sample wt/vol: .0 (g/mL) 6 Lab File ID:
Level: (low/med) LOU) Date Recei*
% Moisture: not dec. 0
Column: (pack/cap) PACK
Date Analyzed: 09/01/90
D i l u t i o n Factor: 10U
CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) US/KG
I74-87-3-- — -----Chlorome thane______________I 100074-83- 9- --------Bromome thane_____________I 100075-01-4---- — ---Uinyl Chloride___________I 100075-00-3--- —— — -Chloroe thane_______________I 10UO75-09-2 — -- ———— Methylene Chloride_________150067-64-1 — - —— — -Acetone_____________________1610075-15-0 —— - — — -Carbon Disulf ide___________150075-35-4——— — ——1,1-Dichloroethene_________1540075-34-3————————1,1-Di chloroe thane_________1500540-59-0—————1,2-Dichlorethene (total)___150067-66-3- ———— —— Chloroform_________________1500107-06-2 — —————1,2-Di chloroe thane_________150078-93-3 ———————— 2-Butanone_________________13200071-55-6 —— —————1,1,1-Tr i chloroe thane______150056-23-5---------Carbon Tetrachlor ide_______I 500108-05-4———————Uinyl Acetate______________I 1000•75-27-4------ —— Bromodich loromethane_______150078-87-5---- — ---1,2-Dich loropropane________150010061-01-5------cis-l,3-Dichloropropene____150079-01-6--- — —— -Tr ichloroethene__________15500124-48-1---- — --Dibromoch lorome thane_______I 50079-00-5--- ——— —1,1,2-Tn chloroe thane_____150071-43-2- —— — - — Benzene________________1540010061-02-6----—trans-1,3-Dichloropropene__150075-25-2---------Bromof orm__________________I 500108-10-1 —— - — — 4-Methyl-2-Pentanone_______I 10UO591-78-6---- ——— 2-Hexanone_______________I 1000127-18-4---- — --Tetrech loroethene__________I 50079-34-5- — -————1,1,2,2-Tetrachloroe thane__1500108-88-3-- —— —— Toluene____________________I54UO108-90-7- — — — -Chlorobenzene______________15600100-41-4——- —— -Ethyl benzene________________1500100-42-5- — - — --Styrene_____________________15001330-20-7——- —— Xylene (total )_____________1500
U
IUIUIUIUIUIIUIIUIUIUIUIIUIUIUIUIUIUIIUIUIIUIUIUIUIUIUIIIUIUIUI
FORM I UOA 1/8:8 6e
Lab Name:.
Lab Code:
VOLATILE ORGANIC ANALYSIS DATA SHEET
_ Contract:____
___ SAS No.:
EPA SAXPLE NO.
Case No.: SDC No. :
Matrix: (soil/water)
Sample wt/vol: .o
Level: (lov/ned)
% Moisture: not dec.
Column: (pack/cap)
CAS NO.
.(g/mL)
Sample ID: C- AV37 7^
Lab File ID: ?& / /4-S
Date Received: _
Date Analyzed: _
Dilution Factor:
COMPOUNDCONCENTRATION UKITS:(ug/L or ug/Kg)
iTetrahydrofuran^ 5co
FORM I VGA 1/87 Rev.
TOTflL ION CHROMflTOSRPMTile >D1142 35.0-260.0 amu. 0437705,, C04377VS ,QV70337 ,S »r
80000^
70008^
HID30888;
20080-
10000-
J
. . . . . . . .&...:...*•...,. .. W. ... 8P» ...,...W.
2"
8"1 | s
1 I. 1| s —
If illIf 1 1v_%_ii i8 L I *(
i
\
3 J
m
"
\ 46
4 ' 8 ' 12 ' 16 20 ' 24 ' 28 ' 32 ' 36 ' 40
Data File: >D1142::SS Quant Output File: ~D1142::.AQName: A4377MS,,Misc: CA4377US,QU70337,S:M4,0.05,, 1:100 DL 10UL IFB SPIKE
Id File: ID0259::U1Title: XUOA13, IFB, PP/UOALast Calibration: 900901 17:25
Operator ID: EK1710Quant Time: 900901 17:37Injected at: 900901 00:20
84
Operator ID: EK1710Output File: ~D1142Data File: >D1142Name: A4377MS,,Misc :
: AQ:SS
QUANT REPORT
Quant Rev: 7 Quant Time:In jected at:
fry Dilution Factor:
1:100 DL 10UL IFB SPIKE
Page 1
900901 17:37900901 00:20
1.00000
ID File: ID0259: : UlTitle: XUOA13, IFB, PP/UOALast Calibration: 900901 17:25
Compound R.T. Scan# Area Cone Un i ts
1791315182021283031364142434546
)))))))))•))))))))
*Bromoch loromethaneH«thyl«ne eh+o-r d«-Acet one V1,1-DichloroethyleneTe t rahydrof uranl,2-Dichloroethane-D4 (SURR)
*1, 4- Dif luorobenzeneMethyl ethyl ketoneTrichloroethyleneh i f Th 1 rrnmnthy 1 1« thnrBenzene
*Chlorobenzene-d5Toluene-08 (SURR)To lueneCh lorobenzenep-Bromof luorobenzene (SURR)
11.•
9.11.12.14.22.14.19.19.19.27.25.26.27.32.-•,6..
6714421372542662157070239814347354
266175208252293340539342459473473667635639670809R54
38722•T D O O
14828454919985785831606451950864250C7OXo /DO
13956811962917505498141133985985889995
250.20.
305.269.385.233.250.
1615.275.101.267.250.253.271.281.245.
•?
00932148498700114901550060195441P7
NGki^*NGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNIC
95O PTO
939310095979492100958495969689•74.
Compound is ISTD
85
Lab Name: ETCNJ
1AVOLATILE ORGAN1CS ANALYSIS DATA SHEET
Cont ract:
ERA SAMPLE NO.
IA4377MSD II____________ I
Lab Code: Case No.: SAS No.: SDb No.:
M a t r i x : (soiI/water) SOIL Lab Sample ID: CA4377UK
Sample wt/vol: .0 Cg/mL) G Lab F i l e ID: >Dl'i43
Level: (low/med) LOU) Date Received: 09/06/90
% Moisture: not dec. 0
Column: (pack/cap) PRCK
CAS NO. COMPOUND
Date Analyzed: 09/01/90
Di lut ion Factor : 1UU
CONCENTRATION UNITS:(ug/L or ug/Kg^ UG/KG
I74-8 7-3---------Ch lo rome thane______________I 100074-83-9---------Bromome thane_______________I 100075-01-4---------Uinyl Chloride______________I 100075-00-3---------Ch lo roe thane_______________I 100075-09-2--- — ----Methylene Chloride__________I50067-64-l---------ttcetone____________________I 590075-15-0- — ——— --Carbon Disulf ide__________150075-35-4—— — ----I , 1-Dichloroethene_________1540075-34-3------——1,1-Dichlo roe thane_________1500540-59-0--------l,2-Dichlorethene (total)__I 50067-66-3- ———— — -Chloroform__________________1500107-06-2 — ———— -1,2-Dichlo roe thane_________150078-93-3-- — - — --2-Butanone_________________13100071-55-6-- — ——— -1,1,1-Tr i ch 1 oroe t hane______150056-23-5--- —— ---Carbon Te t rach 1 or i de_______1500108-05-4— — ——— Uinyl Acetate_______________I 10UO75-27-4- — -- —— -Bromodichlorome thane_______150078-87-5---------l,2-Dich loropropane________I 50010061-01-5--——cis-1, 3-Dichloropropene____1500"7^-'tTi-b---------~l r ich'loroethene____________15500124-48-l--------Dibromoch loromethane_______150079-00-5- ———— - — 1,1,2-Tr ich lo roe t hane______150071-43-2-- —— - — -Benzene____________________153001006l-02-6------trans-l,3-Dichloropropene___150075-25-2---------Bromo form__________________I 500108-10-1-- — - —— 4-Methyl-2-Pentanone_______I 1000591-78-6 — -- — --2-Hexanone_________________I 1000127-18-4--------Tetrach loroethene__________I 50079-34-5-———----1,1,2,2-Tetrach1oroethane__1500108-88-3------ — Toluene____________________15400108-90-7- — --- — Chlorobenzene______________15700100-41-4----- — -Ethyl benzene________________I 500100-42-5--------St yrene_____________________15001330-20-7- —— — -Xylene (total )_____________1500
LI
IUIUIUIUIUIIUIIUIUIUIUIIUIUIUIUIUIUIIUIUIIUIUIUIUIUIUIIIUIUIUI
FORM I UOA 1/8$ ge
Lab Name:
Lab Cod*:
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
-&TCCase No.:
Contract:
SAS No . :
EPA SAKPLE NO.
A
SDG No. :
Matrix: (soil/water)
Sample wt/vol: .0
Level: (lov/ned)
% Moisture: not dec.
Column: (pack/cap)
CAS NO.
Lab Sample ID:-
Lab Fil« ID:
Data R«c«ivad:
Data Analyzed:
COMPOUND
Dilution Factor:
CONCENTRATION UNITS:(ug/L or ug/Kg)
Tetrahydrofuran_
FORM X VGA 1/87 Rev.
87
TOTfiL ION CHROMOT06RPMFile >D1143 35.8-860.8 «mu.
200
76666-
60000-
seeee-
40086-
30000-
28800-
18000-
TIC400
CR4377VR,OV70337,S«t
600 800 . 10.00
Data File: >D1143::SS Quant Output File: ~D1143::AQName: A4377MSD,,Misc: CA4377UR,QU70337,S:M4,0.05,, 1:100 DL 10UL IFB SPIKE
Id File: ID0259::U1T i t l e : XUOA13, IFB, PP/UOALast Calibration: 900901 17:25
Operator ID: EK1710Quant Time: 900901 17:39Injected at: 900901 01:11
88
QUANT REPORT
Quant Re<*>: 7I Quant Time:In jected at:
Di lut ion Fac tor:
Operator ID: EK1710Output File: ~D1143::AQData File: >D1143::SSName: A4377MSD,,Misc: CA4377UR,QU70337,S:M4,er«*-?, 1:100 DL 10UL IFB SPIKE
ID File: ID0259::U1T i t l e : XUOA13, IFB, PP/UOALast Calibration: 900901 17:25
Page 1
900901 17:39900901 01:11
1.00000
Compound R.T. Scan* Area Cone Units
1 )7)9)13)15)18)20)21)28)30)31)36)41 )42)43)45)
*Bromoch loro me thaneM fc h 1
Acetone v*hl e i - ide
1,1-DichloroethyleneTetrahydrofuran1 ,2-Dichloroethane-D4 (SURR)
*1 ,4-Di f luorobenzeneMethyl ethyl ketoneTrichloroethylene
Benzene*Ch Iorobenzene-d5To luene-D8To luene
(SURR)
Ch lorobenzenep-Bromof luorobenzene (SURR)
119
11121422141919192725262732
.66
.13
.37
.08
.70
.49
.20
.60
. 10
.64
.64
.17
.92
.13
.33
.68
267176208252294340539343459473473667635640671809
39137355414363457109511779741635731883365142
1419711203661785209904913547499004
250.19.
292.267.363.229 .250.
1531.274.101.267.250.257.272.282.244.
00225090305900313206280004029393
NGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNG
9595939410091979592100958599999586
Compound is ISTD
89
ETC
SEMIVOLATILE DATA
90
ETC
QC SUMMARY
91
2DSOIL SEMIUOLATILE SURROGATE RECOVERY
Lab Name: ETCNJ Contract: __
Lab Code: Case No.: ____ SAS No.:
Level : (LOU/MED ) LOU)
SDG No,
ERASAMPLE NO.
SBLK01A4376A4377A4377ttSA4377MSD
51( NBZ ) #
6972687071
52(FBP)*
6366656562
S3(TPH)*
6065656872
54(PHL)#
7464646468
55C2FP)#
6558536343
56(TBP)#
9356476364
OTHER TOTOUT
00000
01020304050607080910111213141516171819.2021222324252627282930
51 (NBZ) - Nitrobenzene-d552 (FBP) - 2-Fluorobiphenyl53 (TPH) - Terphenyl-dl454 (PHD - Phenol-d555 (2FP) - 2-Fluorophenol56 (TBP) - 2,4,6-Tribromopheno1
QC LIMITS(23-120)(30-115)(18-137)(24-113)(25-121)(19-122)
Column to be used to flagUalues outside QC limitsSurrogates di l u t e d out
recovery values-?
oaae 1 of
3DSOIL SENIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOUERY
Lab Name: ETCNJ Contract: __________
Lab Code: Case No.: ____ SAS No.: SDG No.:
Matrix Spike - EPA Sample No.: A4377 Leve 1 : (LOUJ/MED) LOW
11
COMPOUND 1
Phenol 12-Ch loropheno 1 11 .4-Dich lorobenzene ,.,,, 1N-Nitroso-di-n-prop. (l)_l1 ,2 , 4-Tr ich lorobenzene __ 14-Chloro-3-methylphenol_lAcenaphthene 14-Ni t ropheno 1 12 ,4-Din i t rot o luene 1Pen tach loropheno 1 1Purene 1
1
SPIKEADDED(ug/Kg)
7927.0707927.0703963.5353963.5353963.5357927.0703963.5357927.0703963.5357927.0703963.535
SAMPLECONCENTRATION
(ug/Kg)
0.0000.0000.0000.0000.0000. 0000. 0000.0000.0000. 0000.000
MSCONCENTRATION
(ug/Kg)
5377.9234612.1942710.5132552.5543106.7596135.9032754.79616571.4023129.4807019.5883300.994
MS\REC
68586864787770209798983
1 QC1 LIMITS
#1 REC.
126- 90125-102128-104141-126138-107126-103131-137
* 1 11-114128- 89117-109135-1421
1 SPIKE1 ADDED
COMPOUND 1 (ug/Kg)
Phenol 17927.0702-Chlorophenol 17927.0701 ,4- D ich lorobenzene ____ 13963.535N-Nitroso-di-n-prop. ( 1 )_l 3963 . 5351,2 , 4-Tr ich lorobenzene __ 13963 .5354-Chloro-3-methylphenol_l 7927. 070Acenaphthene 13963.5354-Nitroohenol 17927.0702 .4-Dinitrotoluene 13963.535Pentach loropheno 1 17927.070Purene 13963.535
1
MSDCONCENTRATION
(ug/Kg)
5229.3084795.7992817.6562778.6643035.4666127.4842672.5607985.8643650.3677036.2193226.100
MSD\REC *
6660717077776710192 «8961
\RPD ft
3448203
70 «1502
QC LIMITSRPD 1 REC.
35 126- 9050 125-10227 128-10438 141-12623 138-10733 126-10319 131-13750 111-11447 128- 8947 117-10936 135-142
1
(1) N-Ni t roso-d i -n-propy lamine
# Column to be used to flag recovery and RPD values with an asterisk
* Ualues outside of l i m i t s
RPD: 1 out of 11 outside l i m i t sSpike Recovery: 2 out of 22 outside limi t s
Comments: - 7U
FORM III SU -2 1/87 Rev.
93
4BSEMIUOLATILE METHOD BLANK SUMMARY
Lab Name: ETCNJ
Lab Code: Case No.
Lab File ID: >P9853
Date Extracted: 08/30/90
Date Analyzed 09/04/90
Matrix: (soil/water) SOIL
Instrument ID: GC/MS P
Contract: __________
SAS No.: SDG No.:
Lab Sample ID: SBLK01
Extraction:CSepF/Cont/Sonc) SONC
Time Analyzed: 1718
Leve1:(low/med) LOU
THIS METHOD BLANK APPLIES TO THE FOLLOUING SAMPLES, MS AND MSD:
010203040506070809101112131415161718192021222324252627282930
EPA -SAMPLE NO.
A4376A4377A4377MSA4377MSD •
LABSAMPLE ID
CA4376CCA4377CCA4377CSCA4377CR
LABFILE ID
>P9854>P9855>P9856>P9B75
'
DATEANALYZED
09/04/9009/04/9009/04/9009/05/90
Comments:
page 1 of (FORM IU SU 1/87 Rev.
94
9BSEMI VOLATILE ORGANIC GCxMS TUNING AND MASS
CALIBRATION - DECAFLUOROTRIPHENYLPHOSPHINE (DFTPP)
Lab NameJETCNJ
Lab Code: Case No.:
Lab Fi la ID: >P9711
Instrument ID: EC/MS P
Contract:
SAS No . : SDG No. :
DFTPP Injaction Data:08^25x90
DFTPP Injaction Time:1418
11 mxe
1 511 681 691 701 127197
. 1981 1991 2751 3651 4411 4421 4431 ____
ION ABUNDANCE CRITERIA
30.0 - 60. OS of mass 198Less than 2.0 S of mass 69Mass 69 relative abundanceLess than 2 . OS of mass 6940.0 - 60. OS of mass 198Less than 1 . OS of mass 198Base peak, 100S relative abundance5.0 to 9. OS of mass 19810.0 - 30. OS of mass 198Greater than l.OOS of mass 198Present, but less than mass 443Greater than 40. OS of mass 19817.0 - 23. OS of mass 442
S RELATIUEABUNDANCE
45.10.0 C 0. )1
51.8.3 C . )1
44.80.0
100.06.9
19.21.5
10.266.312.6 C 19. )2
1-Ualue is S mass 69 2-Ualua is S mass 442
THIS TUNE APPLIES TO THE FOLLOWING SAMPLES, MS, MSO, BLANKS, AND STANDARDS:
1 EPA1 SAMPLE NO.
Oil SSTD160021 SSTD120031 SSTD80041 SSTD50051 SSTD2006 107 1oai091101111121131141151141171iai191201211221
LABSAMPLE ID
IFBXBNA160PPIFBXBNA120PPIFBXBNA80PPMIFBXBNA50PPMIFBXBNA20PPM
I
LABFILE ID
>P9712>P9713>P9714>P9715>P9716
DATEANALYZED
08X25X9008X25X9008X25X9008X25X9008X25X90
;
TIMEANALYZED
14351534163317321830
iI
paga of FORM U SU 1X87 Rev.
95
5BSEMIVOLATILE ORGANIC GC/MS TUNING AND MASS
CALIBRATION - DECAFLUOROTRIPHENYLPHOSPHINE (DFTPP)
Lab Name: ETC CORP Cont ract:
Lab Code: Case No.: SAS No.: SDG No. :.
Lab File ID:>P98513>
Instrument ID.: '
DFTPP Injection Date: 09x04/90
DFTPP Injection time: 16:04
m/e
51iCQXQ
701271971 OQ
199\ 275\ 365\ 441\ 4421 4431
ION ABUNDANCE CRITERIA
30-60* of mass 198 —————— ————————— —— ————————Less than 2* of mass 69 — ———— - ——— ————— —————— — —Mass 69 relative abundance- —— --- —————— ————— ———Less than 2* of mass 69 ——————— - ——————— ___________40-60* of mass 198 — —— ——— —— —— —— —— —————— ———Less than 1* of mass 198 —————— —— —————— -T- —— -----Base peak, 100* relative abundance- — —————————— - —5-9* of mass 198 — ————— —— ——— ———— ————— — —— ————10-30* of mass 198 ————— ————— ——— ————— ———————Greater than 1* of mass 198- — ———— —— ______________Present, but less than mass 443 —————— ——————— - ———— -Greater than 40* of mass 198- ————— — - — —————— _____17-23* of mass 442 —————————————————————————
* RELATIVEABUNDANCE
47 9O.OC 0.0)154.6
,3( .6)141.40.0
100.06.4
19.71.38 JL
&r> 4.11. 6( 18.5)2
1-Ualue is * mass 69 2-Ualue is * mass 442
THIS TUNE APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS:
1 EPA1 SAMPLE NO.
Oil SS7KSO02 1 Sit-f/r/03 1 /3?G041 y^S.??
05 | x4v3?^A<J061071081091101111121131141151161171181
LABSAMPLE ID
$>(. 1l3^\f £-C/4t/H<e£,C/9V.1?3-^O?t/3?^t^
191 1201 1211 1221 1
LAB 1 DATE 1 TIMEFILE ID (ANALYZED I ANALYZED
?P*.Pi»"2f">^3.3" c -Si V" O rfSii
~?fjS*5Tc
o4/0i//6o/11
J/'
-u_-J
fotf/ 3- ji-s
f f fv^
ff/^t>I^O(f
<2oo /
page ( of ( _FORM U SU 1/87 V
5BSEMIUOLATILE ORGANIC EC/MS TUNING AND MASS
CALIBRATION - DECAFLUOROTRIPHENYLPHOSPHINE (DFTPP
Lab Name: ETC CORP Con t r ac t :
Lab Code: Case No.: SAS No.: SDG No.:
Lab F i l e ID:>P9871
. rI nst rument ID.:
DFTPP Injection Date: 09/05x90
DFTPP Injection time: 18:14
1m/e
511 A Q
A Q
1 701271971 Q D
199<-\ -~}tr
365441442443
ION ABUNDANCE CRITERIA
30-60* of mass 198------------------ ----------------Less than 2* of mass 69-----------------------------
Less than 2* of mass 69-----------------------------40-60* of mass 198----------------------------------Less than 1* of mass 198----------------------------
5-9* of mass 198------ — —— -- — --- —— - — —— ---- — — -10-30* of mass 198----------------------------------Greater than 1* of mass 198-------------------------Present,but less than mass 443----------------------Greater than 40* of mass 198---- — ------ — _ _ _ _ _ _ _ _ _ _17-23* of mass 442--- — - — — -- — ---- —— — — _ _ _ _ _ _ _ _ _
* RELATIUEABUNDANCE
47.60 . 0 ( 0.0)1
55.3.3C .6)1
41.80.0
100. 06 . 6
22.7i o
11 .3"70 i
IX. ~7 t 1O ClD
1-Ualue is, * mass 69 2-Ualue is * mass 442
THIS TUNE APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS:
01• 02
030405060708091011121314151617181921)2122
page /
EPASAMPLE NO.
-SO
LAB ISAMPLE ID t
LABFILE ID
S0|
- so
CA <
DATEANALYZED
TIMEANALYZED
/ ofFORM U SU
—— 971/87 REU
ETC
DATA
98
IBSEMI VOLATILE ORGAN ICS ANALYSIS DATA SHEET
ERA SAMPLE NO.
IA4376Lab Name: ETCNJ Contract:
Lab Code: Case No.: ____ SAS No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) G
Level: (low/med) LOW
54 Moisture: not dec. 18 dec.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) Y- pH: 7.0
SDG No.:
Lab Sample ID: CA4376C
Lab File ID: >P9854
Date Received: 08/23/90
Date Extracted: 08/30/90
Date Analyzed: 09/D4/90
Dilution Factor: 1
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
108-95-2 ——————— Phenol _____________________ 1111-44-4 ——————— bis(2-Chloroethyl )ether ____ 195-57-8 ———————— 2-Chlorophenol _____________ 1541-73-1 ——————— 1,3-Dichlorobenzene ________ 1106-46-7 ——————— 1,4-Dichlorobenzene ________ 1100-51-6 ——————— Benzyl alcohol _____________ 195-50-1 ———————— 1,2-Dichlorobenzene ________ 195-48-7 ———————— 2-Methyl phenol _____________ 1108-60-1 — ------bis(2-Chloroisopropyl)ether_!106-44-5 ——————— 4-Methyl phenol _____________ 1621-64-7--------N-Ni t roso-d i-n-propy lamine __ I67-72-1 —————— — Hexachloroe thane ___________ 198-95-3----- — --Nitrobenzene _______________ 178-59-1- ——— -- — Isophorone _________________ 188-75-5 ———————— 2-Nitrophenol ______________ 1105-67-9 ——————— 2, 4-Di methyl phenol _________ 165-85-0 — -------Benzo ic acid _______________ 1111-91-1 — ——— — b is (2-Chloroethoxy)me thane __ 1120-83-2 ——————— 2,4-Dichlorophenol _________ 1120-82-1- —— - — -1,2,4-Tr ich lorobenzene _____ I9 1-2 0-3- - — — —— Naphthalene ________________ 1106-47-8 ——————— 4-Chloroani 1 ine ____________ 187-68-3------ — -Hexachlorobutad icne ________ I59-50-7 ———————— 4-Chloro-3-methyl phenol ____ 191-57-6 ———— —— -2-Methyl naphthalene ________ 177-47-4------- — Hexach lorocyc 1 open tad iene __ I88-06-2 ———————— 2,4,6-Tr ich loropheno 1 ______ 195-95-4 ——— ——— -2,4,5-Tr ich loropheno 1 _______ 191-58-7 — -------2-Ch loronaphtha Iene ________ I88-74-4 ———————— 2-Nitroani 1 ine _____________ 113 1-11- 3-- ——— --Dimethylph thai ate __________ 12 08-96 -B--- —— — Acenaph thy Iene _____________ 1606-20-2--------2,6-Dinitroto luene _________ I
4104104104104104104104104104104104104104104104109541041041041041041041041041041020004102000410410'
Q
IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIJIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU
FORM I SU -1 7 Rev.
1CSEMIUOLATILE ORSANICS ANALYSIS DATA SHEET
Lab Name: ETCNJ
Lab Code: Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) G
Level: (low/med) LOW
Cont rac t:
SAS No.:
ERA SAMPLE NO.
IA4376I_____
Moisture: not dec. 18 dec .
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) Y pH: 7.0
CAS NO. COMPOUND
SDG No.:
Lab Sample ID: CA4376C
Lab File ID: >P9854
Date Received: 08/23/90
Date Extracted: 08/30/90
Date Analyzed: 09/04/90
Dilution Factor: 1
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
99-09-2 ———— -83-32-9 ———— -51-28-5 ———— -100-02-7 ——— -132-64-9 ——— -121-14-2 ——— -84-66-2 ———— -7005-72-3 —— -86-73-7 ———— -100-01-6 ——— -534-52-1 ——— -86-30-6 ———— -101-55-3 ——— -118-74-1 ——— -87-86-5 ———— -85-01-8 ———— •120-12-7 ——— -84-74-2 ———— -206-44-0 ——— -129-00-0 ——— -85-68-7 ———— -91-94-1 ———— -56-55-3 ———— -218-01-9 ——— -117-81-7 ——— -117-84-0 ——— -205-99-2 ——— -207-08-9 ——— -50-32-8 ———— -193-39-5 ——— -53-70-3 ———— -191-24-2 ——— -
----3-Nitroani 1 ine----Acenaphthene----2,4-Dinitrophenol----4-Ni trophenol----Dibenzofuran----2r4-Dinitrotoluene----Diet hvlphtha late----4-Ch lorophenyl-phenylethe r __----F luorene----4-Nitroani 1 ine----4,6-Dinitro-2-methylpheno 1 __----N-Ni t rosod ipheny lami ne (1) __._ — 4-Bromopheny 1-pheny let her __----Hexachlorobenzene----Pent ach lorophenol-- — Phe nan throne- - - - An thracene----Di-n-butylphtha late----Fluoranthene----Pyrene- - - - Bu t y 1 b e n z y 1 p h t h a 1 a t e----3.3'-Dichlorobenzidine---- Be nzo (a )an thracene----Chrysene-- — bis(2-Ethylhexyl )phthalate _— --Di-n-octylphthalate----Benzo(b)f luoranthene----Benzo(k)fluoranthene----Benzo(a)pyrene----Indeno(1.2.3-cd)p<jrene----DibenzC a, h) an thracene----Benzo(g,hr i )pervlene
112000141012000120001410141014101410141012000120001410141014101200014101410165141014101410181014101410134014101410141014101410141014101
1IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1 JIUIUIUIUIUIU1 JIUIUIUIUIUIUIU1
(1) - Cannot be separated from Diphenylamine
FORM I SU -2 1/87 Rev,
100
IFSEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
IA4376Lab Name:ETCNJ
Lab Code: Case No.: ____
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) G
Level: (low/med) LOUI
\ Moisture: not dec. 18 dec. 0
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) Y PH: 7.0
Number TICs found: 12
Con t rac t:
SAS No.: SDG No.:
Lab Sample ID: CA4376C
Lab File ID: >P9854
Date Received: 08/23/90
Date Extracted:08/30/90
Date Analyzed: 09/04/90
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER
01. 123-79-502.03.04.05.06.07. 116-02-908. 873-94-909.10.11.12. 52195-40-1
COMPOUND NAME
Hexanedioic acid, dioctyl esUnknownUnknownUnknownUnknownUnknownCyc lohexano 1 , 3 ,3 ,5- t r i methyCyc 1 ohexanone , 3 ,3 ,5- t r ime t hUnknownUnknownUnknown1-Propene, 1- (me thy 1 1 h io >- ,
RT
33.337.779.0314.916. 0411.9213.0012.677.0210.5210.7214.63
H
EST. CONC
1600064003200450440340300260240230220170
Q
JBJBJJJJJJJJJJ
FORM I SU-TIC 7 Rev.
TOTAL ION CHROHATOCRRHFile >P9854 35.8-588.8 mmu. 04376, 7, 18
TIC...... 4ee. ..... .88e. ....
2888888-
1888888-
1688888-
Meeeee-
1288888-
1888888-
888888
eeeeee-
488888-
288888-
*•* dpi
** w
2
i1
u
1 1 t!! f! '! 8 :4"f75 ,
J
i •i »
2 S
i t
1 I * ^• T ?E •L * *! i ;
ii-i!
E ( ^
. »w .
1sl} ••
CR4376C ,OC78246,Sl
. ... .«e ..... ?e.e?
I
;
\ \r
B.
8 12 16 28 24
62
28 '
[
1P 6D Fid f5 Nr,2 !
32 ' 36 ' 48 ' 44 '
Data File: >P9854::U2Name: A4376,7,18Misc: CA4376C ,QC70246,S:M4,24.63,1
Id File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900904 17:29
Operator ID: KU0786Quant Time: 900904 18:99Injected at: 900904 18:12
Quant Output File: "P9854::UL
BTL* 4
102
QUANT REPORT Page 1
Operator ID: KU07B6Output File: •*P9854::YLData File: >P9854::U2Name: A4376,7,18Misc: CA4376C ,QC70246,S:M4,24.63,1
ID File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900904 17:29
Quant Rev: 7 Quant Time: 900904 16:59Injected at: 900904 18:12
Dilution Factor: 1.00000
BTL* 4
Compound R.T. Scan* Area Cone Units
1)2)3)5)12)14)15)17)18)26)32)36)50)52)54)62)65)66)67)72)73)
•d4-l,4-Dichlorobenzene 11.98 383 167718N-Nitrosodimethylamine 4.96 38 722012-Fluorophenol (SURR) 8.89 231 625356Phenol-05 (SURR) 11.37 353 900841N-Nitro&odi-n-propylamine 13.73 469 653002-Methylphenol 13.49 457 30224-Methylphenol 13.49 457 3022
•d8-Naphthalene 15.81 571 596875Nitrobenzene-05 (SURR) 13.73 469 426607Benzoic acid 15.40 551 6467
•dlO-Acenaphthalene 21.36 844 2680532-Fluorobiphenyl (SURR) 19.35 745 677857Fluorene 23.89 968 77912,4,6-Tribromophenol (SURR) 23.89 968 141081
•dlO-Phenanthrene 25.96 1070 350361Di-n-butyl phthalate 28.22 1181 18655•d!2-Chrysene 34.36 1483 182673Benzidine 25.96 1070 42703Terphenyl-014 (SURR) 31.17 1326 442331bis(2-Ethylhexyl)phthalate 34.87 1508 33620
«dl2-Perylene 38.68 1695 125295
40.00• 19.01-116.21128.5414.06
UG/MLUB/T1LUG/ML—UG/ML--OG ML
.6?0 US-^ML ~
.-530 UC.'ML40.0072.252.3340.0065.68,999
UG/MLUG/ML-UG/ML-UG/MLUG/ML-UC-'rH-
112.8040.001.6140.00
UG/ML-UG/MLUG/ML-UG/ML4JCXML
65.088.4940.00
UGXML-UG/hL-UG/ML
89100849038879494918692989293989895100929186
* Compound is ISTD
103
REFERENCE STANDARD SPECTRUMFil» >J1646Bpk Ab 9999.
10000-
*.,....,..
60 ,-"
1140 58
TARGET REFERENCE SPECTRP Scan 389SUB NRM NOM 9.99 min.
77 l?E 19*
' ~\,KX •188
«40 78 88 98 108 118 128
SAMPLE SPECTRUM (BACKGROUND SUBTRACTED)nit >P9854 A4376.7.18 CA4376C .QC70246 .SiH4.24 Scan 551Bpk Rb 1436.
ieee-0J
El39 ^
il .
SUB 15.40 *in.
77"***•
T 52 /6Ir". ,/40 50 60 70
105
78r .
/ 122"-».
i
hi 80
•a88 98 108 118 128
SAMPLE SPECTRUM (UNALTERED)File >P9854 A4376,7,18 CA4376C ,QC70246 ,S iM4 ,24 Scan 551Bpk Ab 1436.
1088-
^
43 51
,1 1 III
77"^^
1B^ 581, i Ir-" , ii ,
48 58 60 70
15.48 «in.iee
78f .
/ 122•
i
hi 00
ft68 98 100 lie lie
Data File: >P9854::U2 Quant Output File: AP9854::ULName: A4376,7,1Bhisc: CA4376C ,QC70246,S:M4,24.63,1 BTL* 4Quant Time: 900904 18:59 Quant ID File: IP0085::PFInjected at: 900904 18:12 Last Calibration: 900904 17:29
Compound No: 26Compound Name: Benzoic acidScan Number: 951Retention Time: 15.40 min.Quant Ion: 105.0Area: 6467Concentration: 2.33 UG/MLq-value: 86
104
REFERENCE STANDARD SPECTRUMFil« >EBpk Rb
18888-
8-i
4169 TARGET REFERENCE SPE9999. SUB NRH NOM
149
»e ee 128
CTRA Scan 128. 8B •
' 166 268
614in.
•188
9
SAMPLE SPECTRUM (BACKGROUND SUBTRACTED)File >P96S4Bpk Rb 7327
5888-'• 41. f**
48
A4376,7,16
/' « '\f * >
86 "
CA4376C ,OC78246,S:M4,24 Scan 1161SUB 26.22 Bin.
149
1§4"\/ \285f
hi 66
126 ' 166 ' 2^8
SAMPLE SPECTRUM (UNALTERED)Fil» >P9854Bpk Rb 7327
seee-41
46
A4376,7,16 CA4376C .QC76246 ,S |H4 ,24 Scan 116128.22 «in.
149V.
67 76 " 16412xl/ , T i , \ . / Y 265
hi 86
A
88 ' 128 ' lie ' 280 '
Data File: >P9854::U2 Quant Output File: /"P9854::ULName: A4376,7,1BMisc: CA4376C ,QC70246,S:M4,24.63,1 BTL* 4Quant Time: 900904 18:59 Quant ID File: IP0085::PFInjected at: 900904 18:12 Last Calibration: 900904 17:29
Compound No: 62Compound Name: Di-n-butyl phthaleteScan Number: 1181Retention Time: 28.22 min.Quant Ion: 149.0Area: 18655Concentration: 1.61 UG/MLq-value: 98
105
REFERENCE STAHPARP SPECTRUMFile >J7992Bpk Ab 9999.
18888-• 67
" .
B- '48
71/
T+rr^86
TARGET REFERENCE SPECTRASUB NRM MOM149**"*
167**
1128 168 288
Scan 284833.28 Bin.
-188
.Q246 288
SAMPLE SPECTRUM (BACKCROUND SUBTRACTED)File >P9854Bpk flb 1487
leeee- B7•*•>
6~ j jL.y48
A4376.7.18
. 7/ 83 113 »«
i ,-rrX T •88 ' 128
CA4376CSUB
149^•j
167
- , "I' 168
,QC78246>S:M4,24 Sc«n 158834.87 Bin.
W 88
279L -A
268 ' 248 ' 286
SAMPLE SPECTRUM (UNALTERED)FilBpk
» >P9864 A4376Ab 14999.
16686-
tU
57•*
46
71
,7,18
83 113^
88
132
i ,N128
CA4376C149">
i "i' ' ' 168
,QC78246,SiM4,24 Sc«n34.87
287 279
288 ' 248 ' 2
1668Bin.
hi 68
-aT -B8
Data File: >P9854::U2 Quant Output File: AP9B54::dLName: A4376,7,18Misc: CA4376C ,QC70246,S:M4,24.63,1 BTL* 4Quant Time: 900904 16:59 Quant ID File: IP006?::PFInjected at: 900904 18:12 Last Cal i b r a t i o n : 900904 17:29
Compound No: 72Compound Name: bis(2-EthyIhexyl)phthalateScan Number: 1908Retention Time: 34.87 min.Quant Ion: 149.0Area: 33620Concentration: 8.49 UG/MLq-value: 91
106
File >P9864 04376,7,18Bpk fib 9999.
1 67 78 „«J 3^i i r^ n
CA4376C ,OC78246,SiH4,24 Scan 1432SUB NRM 33.33 mir, .
l/ 172 199 223 241 372 313 f--J y .. j r f :*~ s . -^ .L
1 'lie' ' iie' ' '24e' ' '28V 'File >BICDB H«xan»dioic acid, BODO <2-» thy lh»xy 1 ) •* t»r (9CBpk Bb 9999.
J 66 78 112 f 14,29 If -^ \ l/ 172 199 ^241 268
' 48 88 1^8 ' 168 ' 2de ' s4e ' 2^8File >B!CDB Nonan*, 3-Btthyl- (8CI9CI)Bpk fib 9999.
| 2/'j I I ll^ 127 142 143
48 ' 88 128 ' 168 ' 28*8 ' 24*8 ' 2^8 '
File >BICDB Cycloh«xan», (••thyl-ac i-ni tro) - (9CI)Bpk Rb 9999.
A { 83Pt^ | J ^ 138^144^49
' 48 88 126 168 ' 28*8 ' a4e ' 2^8
'328'Scan 138BBe.ee Bin.
328
Scan 11159e.ee *in.
328
Scan 11852e.ee Bin.
I328' '
Data File: >P9854::U2Name: A4376,7,18Misc Data: CA4376C ,QC70246,S:M4,24.63,1RT (min): 33.33Scan: 1432Area: 4692173 Rank: 2Semi-quantitative Cone (unconnected): 403.09 KG/MLSemi-quantitative Cone ( corrected ): 16365.60 ug/kgCalculated using Istd: d!2-Chrysene § 34.36 minutes
BTL* 4
*ru,PRE ,,PBR181,,,1,31. Hexanedioic acid, mono(2-ethylhexyl)ester (9CI)2. Nonane, 3-methyl- (8CI9CI)3. Cyclohexane, (methyl-aci-nitro)- (9CI)
296 C14H2604142 C10H22143 C7H13N02
Sample file: >P9854 Spectrum f:Search speed: 1 Tilting option: S
1432No. of ion ranges searched: 46
Prob. CAS * CON * ROOT
1. 65 4337659 13850 "BIGDB2. 30» 5911046 11159 "BIGDB3. 25« 55937976 11052 "BIGDB
K
754740
DK *FLG TILT \ CON C_I R_I
703752
022
0it,
513031
314442
24126
552113
107
File >P9854 R4376.7.16 CR4376C .QC70246 ,S iM4 ,24 Scan 176Bpk
FileBpk
FileBpk
FileBpk
Ab 9999. SUB NRH 7.77 Bin.
J 39
................. . n~f20 40
E9 L.56 ' 69 72 03 !?l,*.| ,.v .,. /r-*' ;. , ft.E«
60 80 ' 100
>BICDB 2-Propanone (9CI) Scan 1231Ab 9999.
1 « f| 2 / 25 27 39n*f~' ,,|| " ifp'. **"),. ll,.
20' " 40
>BI6DB CuanidineAb 9999.
43J ie /17 f 28 40> .f. . »!,......... l^. ....... .^. ...
0.00 Bin.
H53 ™ 59 f/ . . 1 - •-' _ t«
60 ' 80 ' 100
(8CI9CI) Scan 15810.00 Bin.
/
Jr e ^60 ' ' " ' ' " ' '00 ' 100
>BICIB Hydroperoxide, 1 , l-diB»thylethyl (9CI) Scan 1591Ob 9999. 0.00 nin.
13 15 25 31 39J — ,,./;. ,... ,< , ,:r.,t. t20 40
59/ ,
56 73 89 [
60 ' 80 ' 100
Data File: >P9854::U2Name: A4376,7,18Misc Data: CA4376C ,QC70246,S:M4,24.63,1RT (min): 7.77Scan: 176Area: 3636347 Rank: 3Semi-quantitative Cone (uncorrected): 157.17 UG/MLSemi-quantitative Cone ( corrected ): 6381.36 ug/kgCalculated using Istd: d4-l,4-Dichlorobenzene § 11.98 minutes
BTL* 4
*ru,PRE ,,PBR181,,,1,31. 2-Propanone C9CI)2. Guanidine (8CI9CI)3. Hydroperoxide, 1,1-dimethylethyl (9CI
58 C3H6059 CH5N390 C4H1002
Sample file: >P9854 Spectrum *:Search speed: 1 Tilting option: S
176No. of ion ranges searched: 45
1.2.3.
Prob.
30«25«20
CAS * CON *
6764111300875912
123115811591
ROOT
"BIGDB"BIGDB"BIGDB
K
252036
DK #FLG TILT X CON C_I R_I<J
46 047 244 1
g6 73
6150
444955
8 187 135 13
108
Fil« >P9864 84376,7,18 CA4376C ,QC78246,S |H4 ,24Bpk
FileBpk
FileBpk
Ob 9999. SUB
1 ^ ? t* 1 I'l'l' T - l - l - l 1
28 ' 46
HI9.- 62
' ? f *i,i .,.,.,, ,l|i,[|.s ..i^iji,., ,7,68 86
>BJCDB Cyclop»ntan«, ••thyl*n»- (8CI9CI)Ab 9999.
1^18 26 29 4' 49 ^
28 48
67
8263 77 / 84
66 ' 88
>BICDB l-Penttn-3-ol . 4-a«thyl- (8CI9CI)Rb 9999.
1 27 29 4^ 43 66
28 46
Fil* >BI6DB 2-H«x»n-l-ol.Bpk ftb 9999.
j V 'tr •"26 ' 46
67
6/ 71 82 85
68 ' 86
(Z)- (8CI9CI)67
" 71 8/2
68 86
Scan 2389.83 min.
98 tee f.-. ..L168
Scan 31468.66 Bin.
I' 186 ' '
Scan 53846.88 *in.
96 188 [* _t«
Scan 53218.88 ain.
98 188 t.r^..^ L''"I'j • • »^188
Data File: >P9854::U2Name: A4376,7,18Misc Data: CA4376C ,QC70246,S:M4,24.63,1RT (min): 9.03Scan: 238Area: 182818? Rank: 6Semi-quantitative Cone (uncorrected): 79.02 UG/MLSemi-quantitative Cone C corrected ): 3208.29 ug/kgCalculated using Istd: d4-l,4-Dichlorobenzene § 11.98 minutes
BTL* 4
*ru,PRE ,,PBR181,,,1,31. Cyclopentane, methylene- (8CI9CI)2. l-Penten-3-ol, 4-methyl- (8CI9CI)3. 2-Hexen-l-ol, (2)- (8CI9C1)
82 C6H10100 C6H120100 C6H120
Sample file: >P9854 Spectrum *: 238Search speed: 1 Tilting option: S No. of ion ranges searched:
1.2.3.
Prob.
29»28«25*
CAS * CON f
15283094798452928949
314653045321
ROOT
"BIGDB"BIGDB"BIGDB
422428
DK *FLG TILT \ CON C_I R_IU
316070
120
2t)
2710060
423B48
8 1710 147 19
109
Pil* >P9864 A4376,7,18Bpk fib 9999.
11680-3
18868-
9688-
8860-
7888-
6080-
5888:
4868-
3880-
2886-
1668-
63j
57
36
,]
/83
UkJ.J48 68 86
CR4376C ,QC78246,SiH4,24 Scan 627SUB NRH 14.91 min.
142\
\ie6 ?l
III Jill \ III J,, , JLI. .
rue196""
172146 163 if
/ I/ 11188 128 146 168 188
•188
•98
«e
•78
«.68
48
•38
•26
•16
e
Data File: >P9854::U2Name: A4376,7,18Miac Data: CA4376C ,QC70246,S:M4,24.63,1RT (min): 14.91Scan: 527Area: 330480 Rank: 10Semi-quantitative Cone (uncorrected): 10.99 US/MLSemi-quantitative Cone ( corrected ): 446.28 ug/kgCalculated using Istd: dB-Naphthalene § 15.81 minutes
BTL* 4
No PBM hits for this scan.
110
Fil* >P9864 R4376,7,Bpk fib 9999.
18888-
8888-
6888-
4090-
2888-
8-
18 C04376C ,0078246, SiM4, 24 Scan 91SUB NRM 6.84 «ln.
4
36 39
\%\\
13/ 47
7349 56 57 7j// 88
•188
«8
<e•48
•28
-a"''"j'e" *' ""38 48 ^ 58 ' 68* ' 78 T 88
Fil* >BICDBBpk fib 9999 .
10888-
8880-
6880-
4080-
2888-
8-
6
ie 24 28
Propanoic acid, 2-oxo- (9CI) Scan 118.88 Bin.
*•*
y? 36 48
45
/ 62 66 68 68 69 77 88
" 2'e""'""3e •'•"4le"T ""ee""1" ee" ' ""?e '""e'e""1"
•188
-88
-68
-48
-28
-8
Data File: >P9854::U2Name: A4376,7,1BMisc Data: CA4376C ,QC70246,S:M4,24.63,1RT (min): 6.04Scan: 91Area: 291420 Rank: 11Semi-quantitative Cone (uncorrected)! 10.87 DC/MLSemi-quantitative Cone ( corrected ): 441.21 ug/kgCalculated using Istd: d4-l,4-Dichlorobenzene @ 11.98 minutes
BTL* 4
*ru,PRE ,,PBR181, ,,1,31. Propanoic acid, 2-oxo- (9CI) 88 C3H403
Sample file: >P9854 Spectrum *:Search speed: 1 Tilting option: S
91No. of ion ranges searched: 45
1.
Prob. CAS * CON * ROOT K DK *FLG TILT S CON C_I R_IU
20« 127173 11 "BIGDB 26 51 1 0 80 51 5 14
111
F1U >PBpk fib
11880-
18888-
9888-
8888-
7888-
6888-
5888-
4888-
3880-
2060-
1080-j
98649995
A
4-48
\ 04376,7,18 (>. SU
3
C
65 73I / ?8/
k. 4..... ....68 88
:04376C ,QC78246,SlH4,24 ScanB HRH 11.92 •
»7
97 JIB 158, V ' \ v' 188 ' 1^8 ' 148 '
388in.•118
•188
•98
•88
•79
«•
50
48
•38
28
•18
e
Data File: >P9854::U2Name: A4376,7,18Misc Data: CA4376C ,QC70246,S:M4,24.63,1RT (min): 11.92Scan: 380Area: 190983 Rank: 12Semi-quantitative Cone (uncorrected): 8.2? UG/MLSemi-quantitative Cone ( corrected ): 335.15 ug/kgCalculated using Istd: d4-l,4-Dichlorobenzene § 11.98 minutes
BTL* 4
No PBM hits for this scan.
112
File >P9854 R4376.7.18 CR4376CBpk Bb 9999.
14,,,,,,i,l,i48
SUB HRh,QC7e246,SiM4,24
109
44 ** *?™ "3 9S 97 f|7 .(1|l|l(, vlji.l, - .ii|,l, . ..r" .1, f." ' " "ee" " ' " "e'e" " 'iee ""iie'
File >BICDB Cyc lohexanol , 3 ,3 ,5-t r i»» thy 1- (8CI9CI)Bpk Rb 9999.
1 « Vj f I Iej. .'i'ni.i.il|lill40
File >BICDBBpk fib 9999.
. 41
JiT7 if.^^i ^ ° * * i *48
File >B1CDBBpk Rb 9999.
1 r«Lj . .'
189
t7 83^4 SS 67^ , 9
' ' ' 60" ' ' 80 '
BicycloCB.l .03 octane67
64 I 82"^ 79 ' 9
. . 1 . l.^.\ | . . . Ma . . . ,
3,4-Pyridinediaaine
V|l|l|f|rii|i|i|l|iee
(8CI9CI)
5••i'l iee•C9CI)
' 'Vl|n.|.|.mfr|t126
'"ill
'"'lie'
Scan 43313.ee Bin.
12« 127 F
148
Scan 183876.86 min.
-4i4^L"""""IVScan E369e.ee *in.
, i1 " lieScan 103450 .ee Bin .
109
52 B4 6B 82
' V0 ' 80 iee__ne' 128
, i1 lie
Data File: >P9854::U2Name: A4376,7,18Misc Data: CA4376C ,QC70246 ,S: 114,24. 63 ,1RT (min): 13.00Scan: 433Area: 168621 Rank: 13Semi-quantitative Cone (unconnected): 7.29 UG/MLSemi-quantitative Cone ( corrected >: 299.91 ug/kgCalculated using Istd: d4-l,4-Dichlorobenzene § 11.98 minutes
BTL* 4
*ru,PRE ,,PBR181,,,1,31. Cyclohexanol, 3,3,5-trimethy1- (8CI9CI)2. BicycloC5.1.03octane (8CI9CI)3. 3,4-Pyridinediamine (9CI)
142 C9H180110 C8H14109 C5H7N3
Sample file: >P9854 Spectrum *:Search speed: 1 Tilting option: S
433No. of ion ranges searched: 47
1.2.3.
Prob.
8931*
CAS * CON *
11602928643154966
10387536910345
ROOT
'BIGDB•BIGDB'BIGDB
K
974827
DK *FLG TILT \ CON C_I R_I«J
153655
122
0"2
781889
54461
66 6312 222 14
113
Film >P9864 04376,7,18Bpk Ab 9999.
J 41 66^s. 43 /.l.lii.. — ..Hi..
C04376C ,0078246, S i M 4 ,24 Scan 417SUB NRH 12.67 Bin .
8369 r^ t-( 74 97 167 126 14^ E
28 46 68 86 166 128 148
F i l e >BICDB Cyc lohcxanon* ,Bpk Ob 9999.
1 16 « ^ 43 B/B4,-:-,- A, .Mvrrnil-,
3,3,6-tr i«»thyl- (8C19CI) Scan 663583 e'8e •*"•
6/9 f \82 97 112 122 125 146 \
....... I. 7TB ... . . ...<. ^. ^> f.. ^..L28 48 68 86 188 128 148
Fi l e >BICD£ Cyclohexane, bu ty l - ( 8 C I 9 C I ) Scan 16789Bpk Ob 9999. 6.86 K i n .
83H B6 62 f L.
28 4 , L « 3 { 67 ^| 97 ln »«M
28 ' 48 ' 68 ' e'e ' iee ' i2e ' lieFile >BI6DB Cycloh»x*nt,Bpk Ob 9999.
66-j 41 /3 27 *^ 43
pj /.I. JiCi-j'lta
(2-«»thylpropyl ) - (9CI) Scan 56366 .88 «in .
83.. 8i r 97 t^/ ^ f n2 n3 12S '\ [28 46 66 88 166 126 146
Data File: >P9854::U2Name: A4376,7,18Misc Data: CA4376C ,QC70246,S:M4,24.63,1RT (min): 12.67Scan: 417Area: 149323 Rank: 14Semi-quantitative Cone (uncorrected): 6.45 UG/MLSemi-quantitative Cone ( corrected ): 262.04 ug/kgCalculated using Istd: d4-l,4-Dichlorobenzene @ 11.98 minutes
BTL* 4
*ru,PRE ,,PBR181,,,1,31. Cyclohexanone, 3,3,5-trimethy1- (8CI9CI)2. Cyclohexane, butyl- (8CI9CI)3. Cyclohexane, (2-methyIpropy1)- (9CI)
140 C9H160140 C10H20140 C10H20
Sample file: >P9854 Spectrum *:Search speed: 1 Tilting optionion: S
417No . of ion ranges searched: 47
1.2.3.
Prob.
79«67»60»
CAS * CON *
87394916789391678984
5635157895636
ROOT
"BIGDB"BIGDB"BIGDB
K
664639
DK #FLG TILT S CON C_I R_IU
365264
123
00
8175100
111511
433430
662113
114
File >P98S4 P4376,7,10Bpk Ab 9999.iieee-.
18000-
9088-
8800-
7008-
6000-
5800-
4000-
3000-
2000-
1000-
CB4376C ,QC70246,StH4,24 Scan 139SUB HUH 7.82 «in.
riie43
42NS
^
60
I40
E49
s'e
866
\\( 1.
'1f 84
i \ 87 7 ie\1 1 i ( ^
•100
•90
«0
•70
•60
€0
•40
•30
•20
•10
«60 1 ' 70 80 ' 90 ' 188 '
Data File: >P9854::U2Name: A4376,7,18Misc Data: CA4376C ,QC70246,S:M4,24.63,1RT (min): 7.02Scan: 139Area: 136410 Rank: 16Semi-quantitative Cone (uncorrected): 5.96 UG/MLSemi-quantitative Cone ( corrected ): 242.89 ug/kgCalculated using Istd: d4-l,4-Dichlorobenzene g 11.96 minutes
BTL* 4
No PBM hits for this scan.
115
Fil* >P98C4 R4376,7,18Bpk fib 9999.
41 4S
J ^ v . /
,, i..Mi.n-1'iMiU ivi'l20 40
CR4376C ,0078246, SiH4 ,24 Scan 311SUB NRM 18.62 Bin.
>7
60 73 84 98 183 112 117 131 fjlr-''. i .jlj / . / . .71 "^ / " tfl60 ' 89 ' 180 ' 120
Fil* >B!CDB 1 ,3-Butan*diol (8CI9CI) Scan 333Bpk Rb 9999. 0.00 Bin.
4S
] 27 41 1 67 72 90 f*J,,l,,lM1.,,,>l|l,l,,.|<r >f» < t*
20 40 68 "80 ' lie ' l 2 0
Fil* >BICDB 4-P*nt*n-2-ol (8CI9C1) Scan 328Bpk Ab 9999. 8.00 Bin.
j 27 «j| 53 67 71 72 |
20 40 60 ' 88 ' 180 ' 120
Fil* >BI6DB 2-But*non*, 3-hydroxy- (8CI9CI) Scan'353Bpk flb 9999. 0.80 Bin.
j i5 ZJ 41 |j 55 60 72 86 88 99 114 115 f
20 ' ' 40 ' ' ' "60 ' 80 ' 188 ' 120
Data File: >P9854::U2Name: A4376,7,18Misc Data: CA4376C ,QC70246,S:M4,24.63,1RT (min): 10.52Scan: 311Area: 131121 Rank: 17Semi-quantitative Cone (unconnected): 5.67 LJG/fILSemi-quantitative Cone ( corrected ): 230.10 ug/kgCalculated using Istd: d4-l,4-Dichlorobenzene § 11.98 minutes
BTL* 4
tru,PRE ,,PBR181,,,1,31. 1,3-Butanediol (8CI9CI)2. 4-Penten-2-ol (8CI9CI)7. 2-Butanone, 3-hydroxy- (8CI9CI)
90 C4H100286 C5H10088 C4H802
Sample file: >P9854 Spectrum #:Search speed: 1 Tilting option: S
311No. of ion ranges searched: 45
Prob. CAS * CON * ROOT K
1. 20« 107880 333 "BIGDB 322. 15 625310 328 "BIGDB 353. 15 513860 353 "BIGDB 35
DK #FLG TILT
433850
111
688382
CON C_I R_IU
556058
5 173 133 13
116
Ft l* >P9664 R4376.7.18Bpk
F i l eBpk
Fi l eBpk
Fi leBpk
CA4376C ,QC78246,SiH4,24 Scan 321SUB NRM 16.72 B in ."" ""' « s,
J,,,,,,,,,iL26 46
~->
£9 " 77 98 ^«3¥^ ^ i i i - i ' i I't iC^ i- i ' l i \\ i i ii i 'Vi i |
66 66 166
> B I C D B 1 ,3-Butanediol ( 8 C I 9 C I )fib 9999.
J '? ^ 'e j.. , , , i i | i , i , , .Tpiiin^-26 46
7 72 96> •(•• (
68 88 186
> B I C D B 2-Butanone, 3-hydroxy- ( 8 C I 9 C I )fib 9999. ^
if ?: %lf26 46
55 59 72 83 88 99• I ' l ' i - i - . i • i ' | ' l ' i ' . • i ••• i - l - i . . . .'| • . . . |68 86 tee
>BICDB Diaz«n«, b i s C l , l -diB»thyl«thyl > - (9CI )Rb 9999.
V7 L126
Scan 3338.66 B in .
IScan 353
6.86 Bin.
114 115 [
Scan 11766. 66 Bin .
57
J 29 41
,,,Q£,26 46
59 71 83 85 97 185
66 86 166 '
Ill 127 fr-~ ^.L»
Data F i l e : >P9854::U2Name: A4376,7,18Misc Data: CA4376C ,QC70246,S:M4,24.63,1RT (min): 10.72Scan: 321Area: 122916 Rank: IBSemi-quantitative Cone (uncorrected): 5.31 UG/MLSemi-quantitative Cone ( corrected ): 215.70 ug/kgCalculated using Istd: d4-l,4-Dichlorobenzene @ 11.98 minutes
BTL* 4
*ru,PRE ,,PBR181,,,1,31. 1 ,3 -Butaned io l ( 8 C I 9 C I )2. 2-Butanone, 3-hydroxy- (8CI9CI)3. Diazene, bis(1,1-dimethylethyl)- (9CI)
90 C4H100288 C4H802142 C8H18N2
Sample file: >P9854 Spectrum *:Search speed: 1 Tilting option: S
321No. of ion ranges searched: 47
1.2.3.
Prob.
20»1511
CAS 4
107880513860927833
CON 4
3333531176
ROOT
'BIGDB'BIGDB'BIGDB
243535
DK *FLG TILT \ CON C_I R_W
515036
212
00
9884100
525864
5 143 132 12
1 1 7
FileBpk
FileBpk
FileBpk
FileBpk
>P9664Rb 9999
1_j
28
>BICDBFib 9999
JU628
>BISDBRb 9999
1 1B• (Jr""28
>BICDBRb 9999
£J ~X
28
R4376,7,18 CR4376CSUB NRH
/
- 43 67 67
1 Lff . . I I *>:>......
' 48 68 88
1-Propene, l-(*ethyl thio)46 73
39 f (28 / 63 61 a
48 ' 68 88
,aC78246,SlH4,24 Scan14.63
88^f
83 181 118116 12'
' lee lie-, CZ>- (9CI) Scane.ee
88
5 98
{e'e ' i2eBut«noic acid, 2-ftethyl-, nethyl ester, (.+-. Scan
6729 41 (' I 43 61 74 '
.III.., i.l .iTT . ill.l..- ' i (48 68 88
e.ee88
^ iei n61, . { f
iee tieButane, 2-»ethoxy-2,3,3-tri«ethyl- (9CI) Scan
73
29 41 43 66 65
48 68 e'e
83 91 99 11B 117
"'''"i^e"'1 "'iie'"
613• in.
rfte
6997• in*
I7885• in.
f
tfl
4481
I
Data File: >P9854::U2Name: A4376,7,18Misc Data: CA4376C ,QC70246,S:M4,24.63,1RT (min): 14.63Scan: 513Area: 122753 Rank: 19Semi-quantitative Cone (uncorrected): 4.08 UG/MLSemi-quantitative Cone ( corrected ): 165.77 ug/kgCalculated using Istd: d8-Naphthalene § 15.81 minutes
BTL* 4
*ru,PRE ,,PBR181,,,1,31. 1-Propene, 1-(methylthio)-, (Z>- (9C1) 88 C4H8S2. Butanoic acid, 2-methyl-, methyl ester, (.+-.)- (9CI 116 C6H12023. Butane, 2-methoxy-2,3,3-trimethyl- (9C1) 130 C8H180
Sample file: >P9854 Spectrum *: 513Search speed: 1 Tilting option: S No. of ion ranges searched: 47
Prob. CAS * CON
1. 41» 52195401 69972. 20« 53955810 70053. 15 27705211 4401
ROOT
'BIGDB'BIGDB'BIGDB
232533
DK #FLG TILT \ CON C_I R_I
927841
331
0TO
828395
215160
1753
121312
118
IBSEMIUOLATILE ORGAN ICS ANALYSIS DATA SHEET
Lab Name: ETCNJ Contract:
Lab Code: Case No.: ____ SAS No.:
M a t r i x : (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) G
Level: (lou/med) LOU
>S Moisture: not dec. 16 dec.
Extraction: CSepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) Y. pH: 7.0
EPA SAMPLE NO.
IA4377I_____
SDG No.:
Lab Sample ID: CA4377C
Lab Fi l e ID: >P9855
Date Received: 08/23/90
Date Extracted: 08/30/90
Date Analyzed: 09/04/90
Dilution Factor: 1
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q
108-95-2 ———111-44-4- ——95-57-8-- ——541-73-1 ———106-46-7 ———100-51-6 ———95-50-1- ———95-48-7 ————108-60-1 ———106-44-5 ———621-64-7 ———67-72-1 ————98-95-3 ————78-59-1 ————DO ~7C K
105-67-9 ———65-85-0- ———111-91-1 ———120-83-2 ———120-82-1 ———91-20-3 ——— -106-47-8 ———87-68 3 —— -59-50-7 ————91-57-6 ————77-47-4- — _88-06 295-95-4 ————91-58-7----88-74-4 ————
1 131-11-3 ———1 208-96-8 ———1 606-20-2----1
1----Phenol 1----b is (2-Ch loroethvl )ether 1----2-Ch 1 oropheno 1 1---- 1 ,3-Dich lorobenzene 1---- 1 .4-Di ch 1 orobenzene 1----Benzol alcohol 1---- 1 j,2-Dich 1 orobenzene 1- — -2-Methvlphenol 1----bis(2-Chloroisopropyl)ether_l----4-Me t hvlpheno 1 1----N-Nitroso-di -n-propy lamine __ 1----Hexach 1 oroe thane 1----Nitrobenzene 1---- I sophorone 1----2-Ni t ropheno 1 1----2 .4-Dimethvlpheno 1 1----Benzoic acid 1----b is (2-Ch loroethoxy) me thane _ 1----2 ,4-D i ch loropheno 1 1----1 .2 .4-Tr ich lorobenzene 1----Naphthalene 1----4-Ch loroan i 1 ine 1
----4-Ch loro-3-methylpheno 1 ____ 1
----Hexach lorocvc lopent ad i ene 1----2 .4 .6-Tr i ch loropheno 1 1----2 ,4 .5-Tr ich loropheno 1 1
----2-Ni t roan i 1 me 1----D ime thvlph t ha la te 1----Acenaph t hv lene 1----2 ,6-D in i t ro t o 1 uene 1
1
4004004004004004004004004004004004004004004004009640040040040040040040040040040020004002000400400-'400
1IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1 JIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1
FORM I SU -1 7 Rev.
1CSEMIUOLATILE ORGAN ICS ANALYSIS DATA SHEET
Lab Name: ETCNJ
Lab Code: Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) G
Level: (low/med) LOW
Con t rac t :
SAS No.:
EPA SAMPLE NO.
IA4377I_____
Moisture: not dec. 16 dec.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) Y pH: 7.0
CAS NO. COMPOUND
SDG No.:
Lab Sample ID: CA4377C
Lab Fi l e ID: >P9855
Date Received: 08/23/90
Date Extracted: 08/30/90
Date Analyzed: 09/04/90
Dilution Factor: 1
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
I99-09-2- — ------3-Nitroanil me_____________12000B3-32-9---------Acenaphthene_______________ I 40051-26-5- —— -----2,4-Dini t rophenol__________12000100-02-7——--——4-N it rophenol______________12000132-64-9 ——————— Dibenzofuran_______________1400121-14-2 ——— - — -2,4-Dini trotoluene_________140084-66-2 — - —— — -Diethylphthalate___________14007005-72-3-------4-Ch1oropheny1-phenylether__I 40086-73-7—- — - —— Fluorene___________________1400100-01-6 ———— -- -4-N it roan i 1 me_____________12000534-52-l--------4,6-Dinitro-2-methylphenol_1200086-30-6-- — -----N-Nitrosodiphenylamme (1)_1400101-55-3--------4-Bromopheny1-phenylether__I 400118-74-1-- — ----Hexach lorobenzene___________140087-86-5---------Pentachloropheno 1__________I 200085-01-8-- — -----Phenanthrene_______________140012 0-12-7-- —— — -Anthracene_________________140084-74-2---------Di-n-butylphtha late________167206-44-0--------Fluoranthene_______________I 400129-00-0- — - — --Pyrene_____________________140085-68-7---------Butylbenzylphthalate_______I 40091-94-1 ———————— 3,3 '-Dichlorobenzidme_____179056-55-3--------- Be nzo ( a )anthracene_________I 400218-01-9 —— —— --Chrysene___________________1400117-81-7—--- — -bis(2-Ethylhexyl)phthe late__I 120117-84-0- —— - — -Di-n-octylphthalate________1400205-99-2--------Benzo(b)fluoranthene______1400207-08-9- —— ----Benzo(k ) f luoranthene_______140050-32-8---------Benzo (a )pyrene_____________I 400193-39-5———————Indeno(l,2,3-cd)pyrene______140053-70-3----- — --Dibenz(a,h)anthracene_______I 400191-24-2-- — ----Benzo(g,h, i )perylene_______I 400
___________________________________________I(1) - Cannot be separated from Dipheny1 am me
FORM I SU -2
IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIJIUIUIUIUIUIUIJIUIUIUIUIUIUIUI
1/87 Rev.
120
IFSEMI VOLATILE ORGAN ICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
ERA SAMPLE NO.
IA4377Lab Name:ETCNJ
Lab Code: Case No.: ____
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) G
Level: (low/med) LOW
\ Moisture: not dec. 16 dec. 0
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) Y pH: 7.0
Number TICs found: 11
Cont rac t :
SAS No.:
I
SDG No.:
Lab Sample ID: CA4377C
Lab File ID: >P9855
Date Received: 08/23/90
Date Extracted:08/30/90
Date Analyzed: 09/04/90
Di lut ion Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
CAS NUMBER
01. 123-79-502.03. 928-94-904.05.06.07.08.09. 503-74-210. 149-57-511. 116-02-9
COMPOUND NAME
Hexaned 10 i c acid, dioctyl esUnknown2-Hexen-l-ol , (2)- (8CI9CI)UnknownUnknownUnknownUnknownUnknownButanoic acid, 3-methyl- (9CHexanoic acid, 2-ethyl- (8CICyc lohexano 1 , 3 ,3 ,5- t r imet hy
'
RT
33.347.769.00
14.916.03
11.9114.5617.738.58
14.6412.99
m
EST. CONC
2500054005300540360300230170210170200
Q
JEJBJJJJJJJJJ
FORM I SU-T1C 1/87 Rev.
121
TOTRL ION CHROMRTOCRRHFll* >P9856 35.0-508.8 MHJ . R4377,7,16 CR4377C ,OC7B24fc,Si
40e , l\l , 1200 , itee , 2000
2088088-
1680088-
1608880-
1400000^
1200080-;
1888888-
680888--
688000^
480080-
28B080-
* Ig &
|(A
t
I]
^
»^4
i® I \\ is s 1 :ii•j .; i
A
' 12
• i i '1 *. ri
i * " '
b' ' 1
i*E ' •16 ' 20
1' [i *
*• 'N Ii ' °; s Ti l: J&U 1
62
24 ' 26 ' 32
A
! ?•o £!
h T36 40 44
Data File: >P9855::U2Namo: A4377,7,16Misc: CA4377C ,QC70246,S:M4,25.22,1
Id File: IP0085::PFTitle: IFB/BNA, PPxBNA, TCLBN1Last Calibration: 900904 17:29
Operator ID: KU0786Quant Time: 900904 19:53Injected at: 900904 19:06
Quant Output File: ~P9855
BTL* 5
122
QUANT REPORT Page
Operator ID:Output File:Data Fi le:
KU07B6~P9855::UL>P9855::U2
Name: A4377,7,16hisc: CA4377C ,QC70246,S:M4,25.22,1
Quant Rev: 7 Quant Time:In jected at
Di lut ion Factor:
900904 19:53900904 19:06
1.00000
BTL* 5
ID File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900904 17:29
Compound R.T. Scan* Area Cone Units
1)3)5)12)14)15)17)18)26)32)36)50)52)54)62)65)66)67)72)73)
*d4-l,4-Dichlorobenzene2-Fluorophenol (SURR)Phenol-D5 (SURR)N-Nitrosod i-n-propylamine2-Methylphenol4-MethyIpheno1
*d8-NaphthaleneNitrobenzene-05 (SURR)Benzoic acid
*dlO-Acenaphthaione2-Fluorobiphenyl (SURR)Fluorene2 ,4,6-Tribromopheno1 (SURR)
*dlO-PhenanthreneDi-n-butyl phthalate*d!2-ChryseneBenz idineTerphenyl-D14 (SURR)bis(2-Ethylhexyl)phthalate*d!2-Perylene
12.00 383 175259 40.00 UG/ML 908.72 222 117415 20.88 UG/ML- 8511.36 352 943691 128.86 UG/ML- 9013.73 468 64208 '1J.23 UG/ML 3813.48 456 2160 .431 UG/ML 8913.48 456 2160 - .J6J UO/ML 9615.82 571 628868 40.00 UG/ML 9413.73 468 421478 67.75 UG/Mtr 9215.42 551 7076 2.42 UG/ML- 9421.36 843 281694 40.00 UG/ML 9619.34 744 706683 65.15 UG/MIr 9723.88 967 6893 .041 UG^ML 9123.88 967 124183 94.48 UG/ML~ 9725.98 1070 369837 40.00 UG/ML 9928.24 1181 20748 1.69 UG/ML- 9634.36 1482 182568 40.00 UG/ML 9825.98 1070 45671 K2.B9 UC 'ML 10031.17 1325 444760 65.47 UG/ML- 9134.87 1507 11747 2.97 UG/ML~ 8838.68 1694 131870 40.00 UG/ML 83
* Compound is ISTD
123
REFERENCE STANDARD SPECTRUMFil« >J1646Bpk Ab 9999.
18000-j
0^ . , . . , . , . .
60 J-1
1148 68
TARGET REFERENCE SPECTRA Scan 389SUB
68 70
NRH NOM 9.99 Bin.185
77 / 122r [-100
•Ae'e 90 tee 110 120
SAMPLE SPECTRUM (BACK6ROUND SUBTRACTED)File >P9855 A4377.7.16 CA4377C .QC78246 ,S sM4 ,25 Scan 551Bpk Ab 1595. SUB 16.42 Bin.
1888- 60 B1
39 £ r" 67 6' 741 1 1 1 i ill , . i i i 1 1 148 60 60 70
10677
85i i f
/ 122
, 1.•100
«80 90 ' 100 ' 110 120
SAMPLE SPECTRUM (UNALTERED)Fi l» >PBpk Ab
0-
9065 04377,7,16 CA4377C ,QC70246,SlM1696.
177
~~^i ^ r' ^ 69 7A es. i l | i | l | i /ll i|l 1 i i f . i l i i !
4,25 Scan15.42 •
?5 I»
I
40 60 66 70 66 90 1^6 110 120
.561in.
•100
•0
Data File: >P9855::U2 Quant Output File: ~P9855::ULName: A4377,7,16Misc: CA4377C ,QC70246,5:M4,25.22,1 BTL* 5Quant Time: 900904 19:53 Quant ID File: IP0085::PFInjected at: 900904 19:06 Last Calibration: 900904 17:29
Compound No: 26Compound Name: Benzoic acidScan Number: 551Retention Time: 15.42 min.Quant Ion: 105.0Area: 7076Concentration: 2.42 UG/MLq-value: 94
124
REFERENCE STRHPRRP SPECTRUMFil* >E4169Bpk Rb 9999.
leeee-
B- ii i i%'e' • • ' •
TRRCET REFERENCE SPECTRR Sc«n 1SUB NRM NOM 26.65 •
149•«v
e'e ' 126 160 266
ei4in.
•166
•6
SRMPLE SPECTRUM (BRCK6ROUND SUBTRRCTED)File >PBpk Rb
seee-6
t
98SS R4377.7.167926.
41 B6 93
fr . r r i i . .h ., .,'.,(.16 66
CR4377C ,SUB
149•v.
121V
\'126 ' ' '
QC76246,SiH4,25 Scan 126.24 •
265h f166 ' 266
181in.
hi 06
^
SAMPLE SPECTRUM (UNRLTERED)Fil» >P98SB 04377,7,16Bpk Rb 7926.
5606-;*» 67 76 "jT.-' ... . .\46 88
CR4377C ,QC76246,SiM4,25 Scan 118128.24 Din.
149^
164 h • —
265L f i
-166
-a126 ' 166 ' 266
Data File: >P9B55::U2 Quant Output File: AP9B55::ULName: A4377,7,16Misc: CA4377C ,QC70246 ,S: (14,25 . 22 ,1 BTL* 5Quant Time: 900904 19:53 Quant ID File: IP0085::PFInjected at: 900904 19:06 Last Calibration: 900904 17:29
Compound No: 62Compound Name: Di-n-butyl phthaleteScan Number: 1181Retention Time: 28.24 min.Quant Ion: 149.0Area: 20748Concentration: 1.69 UG/MLq-value: 96
125
REFERENCE STANDARD SPECTRUMFil» >J7992Bpk Ab 9999.
10000-1
0-1
57 7j
»e 80
TARCET REFERENCE SPECTRASUB NRM NOM
149^v-
167
"1' 120 ' 160 ' 200
Scan 204833.28 Bin.
240 ' 28
-100
•0e
SAMPLE SPECTRUM (BPCKCROUND SUBTRACTED)File >P9855Bpk Ab 4623
4080-' 57
•
48
A4377.7.16
.. y 83 113^ 13*
80 ' 120
CA4377CSUB
149
167
' 160
,flC70246,S!M4,2S Scan 150734.87 »in.
-100
*** 279
200 ' 240 ' 280
SAMPLE SPECTRUM (UNALTERED)Fil* >P9855Bpk Ab 4623
4080-
A-
67SK
P4377,?,.
71 „_1 ' ?J jL. /
1 e'0 '
16 CA4377C
149-h** .
..'?, N .167,n
' ' ' ' 120 " ' " 160 '
,OC70246,S|H4,25 Scan 150734.87 Bin.
«? 279k j»
-100
fi200 ' 240 ' 280
Data File: >P9855::U2 Quant Output File: ~P9855::ULName: A4377,7,16Misc: CA4377C ,QC70246,S:M4,25.22,1 BTL* 5Quant Time: 900904 19:53 Quant ID File: IP0085::PFInjected at: 900904 19:06 Last Calibration: 900904 17:29
Compound No: 72Compound Name: bis(2-Ethylhexyl)phthalateScan Number: 1507Retention Time: 34.87 min.Quant Ion: 149.0Area: 11747Concentration: 2.97 UG/MLq-value: 88
126
File >P98E6 «4377,7,16Bpk Ob 9999.
~40 ' 60 ' ' 'l20
C04377C ,8078246, SiH4, 26 Scan 1432SUB NRH 33.34 Bin.
129
1B7 199212 241 284 313 341 378 fJ --*" J ff L ~ ~^ ~^. ~~-^ ~^~k*'l6e' ' 268 ' 246' 286 326 ' see'
File >BICDB Hexanedioic acid, dioctyl ester (9CI) Scan 13849Bpk Ob 9999. 0.88 Bin.
j ^-| j f"^ / 166 199212 24! 279313 341 376 [
40 80 120 160 ' 246 ' 246 ' 266
File >BICDB Hexanedioic acid, »ono (2-ethylhexyl)esterBpk Rb 9999.K 129
j 4-L. { r"~ ' \ 157 199212 241 268
*40 88 1 28 lie ' 280 ' 24*e ' 268
File >BI6DB Octane, l,l'-oxybi«- (9CI)Bpk Rb 9999.
57 71
j ^ j J 1 1/2 127.153 182 218242
48 ' 86 128 ' 166 ' 28*8 ' 24e ' 286 '
326 ' 368
(9C Scan 13856e.ee Bin.
, . ,t328 ' 368'
Scan 166228.88 Bin.
I326 ' 366
Data File: >P9855::U2Name: A4377,7,16Misc Data: CA4377C ,QC70246,S:M4,25.22,1RT (min): 33.34Scan: 1432Area: 7808578 Rank: 1Semi-quantitative Cone (uncorrected): 631.33 UG/MLSemi-quantitative Cone ( corrected ): 25033.02 ug/kgCalculated using Istd: d!2-Chrysene § 34.38 minutes
BTL* 5
*ru,PRE ,,PBR181,,,1,31. Hexanedioic acid, dioctyl ester (9CI)2. Hexanedioic acid, mono(2-ethyIhexyl)ester (9CI)3. Octane, l,l'-oxybis- C9CI)
370 C22H4204258 C14H2604242 C16H340
Sample file: >P9855 Spectrum f:Search speed: 1 Tilting option: S
1432No. of ion ranges searched: 46
1.2.3.
Prob.
87"6829*
CAS * CON #
1237954337659629823
138491385010822
ROOT K
"BIGDB 123"BIGDB 97"BIGDB 40
DK *FLG TILT * CON C_I R_IU
414879
001
1-1L
697626
132338
553010
865915
127
File >P9866 P.4377,7,16 COBpk Pb 9999. SUB
1 ^ ''20 40
Fil» >BICDB 2-PropancBpk Pb 9999.
| 2 / 26 27 39
Fil.Bpk
FileBpk
........ .^ ....... __ .
>BICBB 6u»nldin<Pb 9999.
43H 18 /] ^r" /e 4e
26 40
>BI6DB Hydropcroxid*. 1,1Pb 9999.
1] 15 25 31 39*^ \ v \ ** i'i / ri'i'l i-i i i f j . ....... . l . . . . l . . .
20 40
4377C ,QC70246.StH4,26 Sc«n 176NRM 7.76 Bin.
B9 L.66 ' 69 72 83 lft
'''' V0' ''''''' V0' ' '''''' 100
n» (9CI) Sc*n 12310.00 Bin.
63 ™ 69 t
60 ' 80 ' 100
t (8C19CI) Scan 168169 e'ee 'in-
( " f
60 ' 80 ' 100
-diMthylethyl (9CI) Scan 15910.00 Bin.
69
56 73 89 f->]t\ ^ ,- If
' 60 ' 80 ' 106
Data File: >P9855::U2Name: A4377,7,16Misc Data: CA4377C ,QC70246,S:M4,25.22,1RT Cmin): 7.76Scan: 175Area: 3391432 Rank: 3Semi-quantitative Cone (uncorrected): 135.13 UG/MLSemi-quantitative Cone ( corrected ): 5357.96 ug/kgCalculated using Istd: d4-l,4-Dichlorobenzene § 12.00 minutes
BTL* 5
*ru,PRE ,,PBR1B1,,,1,31. 2-Propanone (9CI)2. Guanidine (8CI9CI)3. Hydroperoxide, 1,1-dimethylethy1 C9CI)
58 C3H6059 CH5N390 C4H1002
Sample file: >P9855 Spectrum #:Search speed: 1 T i l t i n g option: S
175No. of ion ranges searched: 45
1.2.3.
Prob.
30«25»20
CAS * CON * ROOT
67641 1231 "BIGDB113008 1581 "BIGDB75912 1591 "BIGDB
K
252036
DK #FLG TILT CON C_I R_IU
464744
021
0fli)
736254
444955
8 187 135 13
128
File >P985E H4377.7.16Bpk Rb 9999.
1 41 44
-' "'/•, vrnr
CR4377C ,eC78246,SiM4,2E ScanSUB HRH 9.88
67 82
B8 ^ 79 --" 108 181
48 68 ee iee izeFile >BICDB 2-Hexen-l-ol, (Z>- (8CI9CI) ScanBpk Rb 9999.
j 41 ""•*>8.88
67 8258 S" 79 -- 96 98 188
48 68 ' 88 ' iee ' 128
File >PIGDB Hexane, 2Bpk Rb 9999.
Or
1 29 4-L i3 ilJ...f,...:j.ir: ,.JIfr40 6
,2,3-tri«*thyl- (8CI9CI) Scan8.88
B8 71 77 8E 91 97 1J2 113 128
8 88 ' 188 ' 128
File >BI6BB Cyc 1 open tanol , 2-«ethyl-, ci«- (8CI9CI) ScanBpk Ob 9999. 8.88
67
j \" r.."r" ,." r r
236• in.
I6321• in.
I978• in.
i§361• in.
I4*e ' 68 ' e'e ' tee ' 128
Data File: >P9855::U2Name: A4377,7,16Misc Data: CA4377C ,QC70246,S:M4,25.22,1RT (min): 9.00Scan: 236Area: 3384249 Rank: 4Semi-quantitative Cone (unconnected): 134.84 UG/MLSemi-quantitative Cone ( corrected ): 9346.61 ug/kgCalculated using Istd: d4-l,4-Dichlorobenzene § 12.00 minutes
BTL* 5
*ru,PRE ,,PBR181,,,1,31. 2-Hexen-l-ol, (Z)- (8CI9CI)2. Hexane, 2,2,3-trimethy1- (8CI9CI)3. Cyclopentano1, 2-methyl-, cis- C8CI9CI)
100 C6H120128 C9H20100 C6H120
Sample file: >P9855 Spectrum #:Search speed: 1 Tilting option: S
236No. of ion ranges searched: 47
Prob. CAS * CON *
1. 60* 928949 53212. 20 16747254 9703. 11 25144052 5361
ROOT
'BIGDB•BIGDB'BIGDB
453535
DK *FLG TILT * CON C_I R_IU
534551
221
00
687932
155363
3052
191213
129
File >P9855 R4377.7.16Bpk fib 9999.
10080-
8880-
6880-
4888-
2888-
A.
63
|
38 68 I I
e-1— , — . t , , . , . , .48 68
File >BICDB Benzene,Bpk fib 9999.
18888-
8888-
6888-
4888-
2888-
8-
CB4377C ,0078246, SiH4, 26 Sc*n 526SUB NRH 14.91 Bin.
83
4i JB .!$V r 188' l
198/
142 144
11 119 \/ 163 /'
[._/ ,. IJ, L^ [L L
•188
•ee•68
-48
•28
•A
128 ' 148 ' 168 ' 180
l-bro»o-4-chloro- (8CI9CI) Sc«f> 23168
1
7568
36 \ 55
48 68
f
96
.r*/-|1t, „„,88 ' 188 F
8.88 Bin.192.
11
1 138 131 165 157
1 \x \x
t
I'lie' ' 'i4e ' lie' ' 'lie' 1
•188
•ee•69
•48
-28
Data File: >P9855::U2Name: A4377,7,16Misc Data: CA4377C ,QC70246,S:h4,25.22,1RT (min): 14.91Scan: 526Area: 427907 Rank: 10Semi-quantitative Cone (uncorrected):Semi-quantitative Cone ( corrected )
13.54 UG/ML537.04 ug/kg
Calculated using Istd: dB-Naphthalene § 15.82 minutes
BTL* 5
*ru,PRE ,,PBR181,,,1,31. Benzene, l-bromo-4-chloro- (8CI9CI) 190 C6H4BrCl
Sample file: >P9855 Spectrum *: 526Search speed: 1 Tilting option: S No. of ion ranges searched: 45
1.
Prob. CAS * CON * ROOT K
30* 106398 23150 "BIGDB 32
DK *FLG TILT X CON C_I R_IU
94 3 0 96 32 12 13
130
Fil* >P9866 04377,7,16 C04377C .OC78246.SiM4.25 Scan 98Bpk flb 9999. SUB NRM ' 6.83 Bin.
18888-
8888-
6888-
4888-
2888-
8-
t
39/||i ' ii' 1 1
28 "' 38 ' 48
47y
_7 7349 56 B7 72 / 88y \ / \ \
•tee«e•68
•48
28
AT- ..,,...,....,,...,....,.. .,,....,.. ,.,... -
58 68 78 88
Fll* >BICPB Propanoic acid, 2-oxo- (9CI) Scan 11Bpk Rb 9999.
18888-
8088-
6888-•
4888-
2888-
8-
43
16
.I
(
18 24 28 /' 36 48
.,(.. \',..l\... \.\,\
e.ee Bin.
46/ 62 66 68 68 69 77 88
•28 38 48
\ \ \ \/ / \ll..,llll lll..l....l..lfll...l.f..l....,..l
•188
«e68
48
28
-8
Data File: >P9855::U2Name: A4377,7,16Misc Data: CA4377C ,QC70246,S:M4,25.22,1RT (min): 6.03Scan: 90Area: 225330 Rank: 12Semi-quantitative Cone (uncorrected):Semi-quantitative Cone ( corrected ):
8.9B UG/ML355.99 ug/kg
BTLf 5
Calculated using Istd: d4-l,4-Dichlorobenzene g 12.00 minutes
*ru,PRE ,,PBR181,,,1,31. Propanoic acid, 2-oxo- (9CI) 86 C3H403
Sample file: >P9855 Spectrum *:Search speed: 1 Tilting option: S
90No. of ion ranges searched: 46
1.
Prob. CAS * CON * ROOT K DK #FLG TILT \ CON C_I R_IU
20« 127173 11 "BIGDB 26 51 1 0 81 51 5 14
131
File >P98SE R4377,7,16 CA4377C ,QC70246 ,S iH4 ,2E Se*n 379Bpk Rb 9999. SUB NRM 11.91 »in.
11000-
10000-
9080-
8000-
7880-
6080-
6800-
4000-
3000-
2000-
1000-
e-
43
42\
"**
~
87
63 *? 61 70 7? 831, .\L,l/ .,(,{ V.
40 ' 60 ' 60 ' 78 ' 88
97 183J,,,,,,,/,,,,,.',,,,,,,,.90 100 110
•lie
•188
•90
•08
•78
•68
€8
«"
•30
•20
•18
Data File: >P9B55::U2Name: A4377,7,16Mi»c Data: CA4377C ,QC70246,S:H4,25.22,1RT (min): 11.91Scan: 379Area: 190450 Rank: 13Semi-quantitative Cone (uncorrected): 7.59 UG/MLSemi-quantitative Cone ( corrected ): 300.88 ug/kgCalculated using Istd: d4-l,4-Dichlorobenzene § 12.00 minutes
BTL* 5
No PBM hits for this scan.
132
Fil» >P9865 04377,7,16 C04377CBpk Ob 9999.
10080-
8008-
6888-
4888-
2080-
0-
39
\
t 1
SUB HRH73
65k.~^^
41/
|.^ . . . . . .^.
Fil* >BICDB
J I'')
67
/ 68
III III,
s^
,QC78246,SiH4l25 Scan 68914.66 Bin.
88/
83
Mill' ' ' • ' - Ve • " • • • e'e'
Propane, 1-ethoxy-Bpk flb 9999.
*d
99 ' '"
, li Y,tf6lNiee ' 128
•188
•ee•68
•48
e
(9CI) Scan 69538. t8 Bin.
31 r
10088-
8888-
6000-
4000-
2000-
8-
•>x,
1.39\
69
43/
' ' " • V e 1
55
,', \-,
88
73 87 S 91
( .. . . . ^ ... . . _ ..f^^
•100
•88
«e•48
•ee-a
188 ' 128
Data File: >P9855::U2Name: A4377,7,16Miac Data: CA4377C ,QC70246,S:M4,25.22,1RT (min): 14.56Scan: 509Area: 180891 Rank: 14Semi-quantitative Cone (uncorrected ):Semi-quantitative Cone ( corrected
5.73 UG/ML227.03 ug/kg
Calculated using Istd: dB-Naphthalene § 15.62 minutes
BTL* 5
*ru,PRE ,,PBR181,,,1,31. Propane, 1-ethoxy- (9CI) 88 C5H120
Sample file: >P9855 Spectrum #: 509Search speed: 1 Tilting option: S No. of ion ranges searched: 47
1.
Prob. CAS * CON # ROOT K DK *FLG TILT * CON C_I R_IU
11" 628320 6953 "BIGDB 28 60 2 0 172 64 2 14
133
File >P98S6 «4377,7,16 CB4377CBpk fib 9999.
18800-
8880-
6808-
4060-
2800-
39\
t 1
SUB HRM
65•w_~ k
41/
I48
File >B!C£BBpk flb 9999.
3118000-
8000-
6800-
4000-
2000-
e-
^
1. \
,1 nil
67
73
/ 66
III ll66
*^
,QC78246,SlH4,
88/
83
M i l lr- ^86
Propane, 1-ethoxy-
/'.
43/
.48
65
,i, N,.
(|
r
7 "\100
(9CI)
88/
73 67
, *,V. N66 86
91
188
25 Sc*n 68914.66 Bin.
11612J.
HI! M
•188
«0
•60
•46
•26
«126
SCAD 69636.80 »ln.
•188
-88
•60
-40
•20
-a126
Data File: >P9855::U2Name: A4377,7,16hiac Data: CA4377C ,QC70246,S:M4,25.22,1RT Cmin): 14.56Scan: 509Area: 180891 Rank: 14Semi-quantitative Cone (unconnected) : 5.73 UG/tILSemi-quantitative Cone ( corrected ): 227.03 ug/kgCalculated using Istd: d8-Naphthalene § 15.82 minutes
BTL* 5
*ru,PRE ,,PBR181,,,1,31. Propane, 1-ethoxy- (9CI) 88 C5H120
Sample file: >P9855 Spectrum #:Search speed: 1 Tilting option: S
509No. of ion ranges searched: 47
1.
Prob. CAS * CON # ROOT K DK *FLG TILT * CON C_I R_HJ
11» 628320 6953 "BIGDB 28 60 2 0 172 64 2 14
133
F i l * >P985E P4377.7.16Bpk Pb 9999.
eeee-4fl 41
4eee- \X /P. Jl i ^ .^ ^Li
26 46 66
CA4377C ,QC78246,SiH4,2E Scan 665SUB NRH 17.73 B i n .
178
.9
9786 / 165 119... \ .1 / / !/
•66
•46
•e' 86 ' 166 ' 126 ' 146 166
Fi l* > B I C D B 1 ,3-Cyclop»ntan»dion», 2-broBO- ( B C I 9 C I ) Scan 21166Bpk flb 9999. 6. 66 Bin .
176, 69 ^
eeee-41 "
4AAA— S \4BB8- X
„: \\ fJ 1 ,i26 46 66
1/ 166 . oB .40 L1 / / 1J3 f |,, L ' v ** iJr r
•ee•46
A
86 166 126 146 166
F i l « > B I C D B I» id*zoC5, l - fKl ,2 ,43 tr i*zin»-2 ,7-di*«in» , 4, Scan 21391Bpk Rb 9999.
8898-<Mr \ VrV26 ' 46 66
6.66 Bin.178
X 81 9E 197 J2l 137
1 ' f" 1"^ 1 - ' ' I 1 • /• 1 '"'I • 1 • 1 • 1 •'86 166 126 146 166
•86
•46
•e
Data File: >P9855::U2Name: A4377,7,16Misc Data: CA4377C ,QC70246,S:M4,25.22,1RT (min): 17.73Scan: 66?Area: 137219 Rank: 15Semi-quantitative Cone (uncorrected): 4.34 UG/MLSemi-quantitative Cone ( corrected ): 172.22 ug/kgCalculated using Istd: dB-Naphthalene § 15.62 minutes
BTL* 5
*ru,PRE ,,PBR181,,,1,31. 1,3-Cyclopentanedione, 2-bromo- (8CI9CI) 176 C5H5Br022. Imidazo[5,l-f]tl,2,4]triazine-2,7-diamine, 4,5-dimet 178 C7H10N6
hyl- (9CI)
Sample file: >P9855 Spectrum #: 665Search speed: 1 Tilting option: S No. of ion ranges searched: 47
1.2.
Prob.
60»20»
CAS * CON *
1420324850473864
2116021391
ROOT
"BIGDB"BIGDB
3538
DK *FLG TILT J« CON C_I R_IU
8764
33
06
77100
1353
305
1313
134
Fil« >PBpk Ob
8888-
4888-
8-
Fil* >BBpk Ob
8888-
4888-
8-
Fil. >BBpk Ob
eeee-4880-
8-
9BBE 04377,7,16 C04379999. SUB HRM
(
41 43^1 /
S3
7C ,0078246, SiM4,2S Scan8.68 •
>0
69 67
, N ? J28' 48 68' ' 68 ' 188 '
ICDB Butanoic acid, 3-«9999.
t
41 43
2^ 2.9 [ 65
vE. ,1,1.. .1.1 1. ....>,,!.
•thyl- (9CI) Scan 18. 88 •
>8
'X ?8\ ??,. >!..,!. N ..1. /28 48 68 88 188
[CDB Pvntanoic ac i9999.
6
27 ^ \43 g6
!• !• ni . .'I1!')'! . i.|l| J» i...|ni|i|'ii . , , . , . . . , , , . . , , . . . . . . ,
d (9CI) Scan 18. 88 •
8
69 74 63 8/ 92 lel
20 48 68 88 188
215in.
ee•48
668in .
«e
-48
-8
866in.
ee-48
-8
Data File: >P9855::U2Name: A4377,7,16Misc Date: CA4377C ,QC70246,S:M4,25.22,1RT (mm): 6.58Scan: 215Area: 133095 Rank: 16Semi-quantitative Cone (uncorrected ) :Semi-quantitative Cone ( corrected ):
5.30 UG/ML210.27 ug/kg
BTL* 5
Calculated using Istd: d4-l,4-Dichlorobenzene § 12.00 minutes
#ru,PRE ,,PBR181,,,1,31. Butanoic acid, 3-methyl- (9CI)2. Pentanoic acid (9CI)
102 C5H1002102 C5H1002
Sample file: >P9855 Spectrum #:Search speed: 1 Tilting option: S
215No. of ion ranges searched: 46
1.2.
Prob.
7060
CAS * CON
503742109524
18681866
ROOT
'BIGDB'BIGDB
K
5443
DK *FLG TILT \ CON C_I R_IU
4345
22
8792
613
4230
1514
135
FiU >P9855 04377,7,16Bpk Pb 9999.
1 V .5
26 46
File >BICDB HexanoiBpk Rb 9999.
J 41
Lr•if j .I26 46
File >BICBB UrBpk Rb 9999.
38 44, / -^^
j 18 45
26 46 '
File >BICDB HydrazinBpk flb 9999.
H 29 44 *5
e ,..,...i|i|., ...ynjlTr,..'26 46
CP4377C ,QC78246,SiH4,26SUB HRh7i. 86
J* 83^ f 181 118^16 i
66 88 168 126
c acid, 2-»thyl- (BCI9CI)73 88
57 ^ (f 63 181 116
66 ' 88 ' 188 ' 128
»a, ethyl- C8CI9CI)
73 go
^56 1 77 f 89
68 ' 86 ' 188 ' 126
e, 1-butyl-l-ethyl- (9CI)73>
66 181 llfe
66 86 188 126
Scan14.64
28 129
'''"•i4eScan8.86
129 145
146
Scan6.66
146
Scan 1e.ee
•P— •
146
513• in.
I7626• in.
I6952• in.,
t
1721• in.
I
Data File: >P9855::U2Name: A4377,7,16Misc Data: CA4377C ,QC70246,S:M4,25.22,1RT Cmin): 14.64Scan: 513Area: 131563 Rank: 17Semi-quan t i ta t i we Cone (uncorrected): 4.16 UG/tILSemi-quantitative Cone C corrected ): 165.12 ug/kgCalculated using Istd: dB-Naphthalene § 15.82 minutes
BTL* 5
*ru,PRE ,,PBR1B1,,,1,31. Hexanoic acid, 2-ethyl- C8CI9CI)2. Urea, ethyl- (8CI9CI)3. Hydrarine, 1-buty1-1-ethy1- C9CI)
144 C8H160288 C3H8N20116 C6H16N2
Sample file: >P9855 Spectrum *:Search speed: 1 Tilting option: S
513No. of ion ranges searched: 48
Prob. CAS *
1. 83 1495752. 42« 6255253. 20» 52728560
CON *
70266952
11721
ROOT
"BIGDB"BIGDB"BIGDB
K
662238
DK
337944
*FLG
222
TILT
0J]0
*
7112889
CON
32555
c_i57175
R_IU
231319
136
Fil.Bpk
Fil*Bpk
Fil*Bpk
FileBpk
>P985S 04377,7,16 CP4377C .QC78246 ,S |H4 ,25 Scan 432Pb 9999. SUB HRM
-j 41 63
40 60 80
12.99 Bin.109
t97 123 I24 127 t
100 ' 120 ' 140
>BICDB Cyclohvxanol , 3 ,3 ,5-tri«»thyl- (8CI9CI) Scan 18387fib 9999.
1 29 4^ 43 55 67 7l *?
40 60 80
109 <»•<"> »in.
IM r97 123 I?4 146 Ist(rjr') ,, j.,. irr, r i-Mf100 120 140
>BICDB BicycloCE.l .83oct*ne (8CI9CI) Scan 5369fib 9999.
j 41 54 / 82
40 60 80
0.80 Bin..
l£m [180 ' 120 ' 140
>BICIB Cyclop»ntan», (2-»ethylpropyl )- (9CI) Scan 5415Rb 9999. 8.80 «in.
, \ 56 6' 831 27 1 43 ( | ,„ /\f K 1 i |U^ 1 91
Jj^ —— l,llL.,....lll.,M....ll ——— rW40 60 88
98 HI 126 128 [
180 120 ' 140
Data File: >P9855::U2Name: A4377,7,16tlisc Data: CA4377C ,QC70246,S:M4,25.22,1RT (min): 12.99Scan: 432Area: 127466 Rank: 18Semi-quantitative Cone (uncorrected): 5.08 DC/MLSemi-quantitative Cone ( corrected ): 201.38 ug/kgCalculated using Istd: d4-l,4-Dichlorobenzene @ 12.00 minutes
BTL* 5
*ru,PRE ,,PBR181,,,1,31. Cyclohexanol, 3,3,5-trimethyl- (8CI9CI)2. Bicyclo[5.1.0]octene (8CI9CI)3. Cyclopentane, (2-methyIpropy1)- (9CI)
142 C9H180110 C8H14126 C9H18
Sample file: >P9855 Spectrum *:Search speed: 1 Tilting option: S
432No. of ion ranges searched: 47
1.2.3.
Prob.
8931«27»
CAS *
1160292864313788327
CON *
1038753695415
ROOT
"BIGDB"BIGDB"BIGDB
K
1034843
DK
93645
*FLG
122
TILT
0:2^
*
741816
CON
54443
C_I R_IU
66128
762215
137
#~lia
61:02 S06006 : ** pa*oatu i<iS:60 906006 :
:QI
906006 :
PI
0003
a.i3
29
Q T ^ T Q
?
!
ii
0091 003T 888Oil
08*
•n«w 8'88S-9'Se
:9
-eee00a
000009
-0000081
-08080ZI
-8888891
-0800881
HOI
QUANT REPORT
Operator ID: KU0786Output File: /"P9874::ULData File: >P9874::U3Name; A4377,7,16Misc: CA4377C ,QC70246,S:M4,25.22,1
Quant Rev: 7 Quan t Time:Injected at
Di1ution Fac tor:
Page 1
900906 09:57900905 20:19
1. 00000
BTL# 4
ID Fjle:T i t l e : IFB/BNA,Last Calibration:
IPOOB5::PFPP/BNA, TCLBN1900906 09:54
Compound R.T. Scan* Area Cone Un i ts
1 )2)3)5)6)12)14)15)17)18)26)32)36)49)50)52)54)62)65)66)67)72)73)
*d4- 1 ,4-Dich lorobenzeneN-Ni t rosod imethylamine2-Fluorophenol (SURR)Phenol-05 (SURR)Pheno 1N-Nitrosodi-n-propylamine2-Me t hy Ipheno 14-flethylpheno 1
»d8-Naphtha leneNitrobenzene-05 (SURR)Benzo i c acid
*dlO-Acenaphthalene2-Fluorobiphenyl (SURR)Diethyl phthalateF 1 uo rene2 ,4, 6-Tr ibromopheno 1 (SURR)*dlO-PhenanthreneDi-n-butyl phthalate
»dl2-Chrys>eneBenz id ineTerphenyl-D14 (SURR)bis(2-Ethylhexyl)phthalate*d!2-Perylene
11.4.8.
11.11.13.13.13.15.13.15.21.19.22.23.23.25.28.34.25.31.34.38.
9282853335674343776740302999838191172991128059
379302283503514654534535684655508407419239649631066117714781066132215031689
21481640843691638M1088170
140518274121522152
77174153507112077
375518866257
24819526
181350584262320163151717345470913416368230034
40-7
96119
*
••J. -4
.-
.-
40673
4063
9240240
1 O f.
62240
.00CO
• -f *.
.75
.79
. 61-• L> 4.
* 8-OTJ-7•"• ' '
. 00
.71
.34
.00
.662-H-U X U.51. 00. 17.00D ni B U
.65
.61
. 00
UG/MLi ir* ^MILJI_ i IL_
UG/ML—UG/ML—-BG^ML-WS/ML-yG/ML1 If"1 '"MlLJLJ 1 IL_
UG/MLUG/ML-UG^hL—UG/fILUGXMI^
-W6-/MLUG/MC'UG^MLUG/ML-UG^MLI If^ r^M!
UG/Mt-UG/ML —UG/T1L
871008692713689999492929997978696989797100899184
* Compound is ISTD
139
ETC
STANDARDS DATA
140
6BSEMIUOLATILE ORGAN ICS INITIAL CALIBRATION DATA
Lab Name:ETCNJ Contract:__________
Lab Code: Case No.:____ SAS No.: SDG No.:
Instrument ID:GC/MS P Ca l i b r a t i o n Date(s) 08/25/90' 08/25/90
Mm RRF for SPCC(#) - 0.050 Max XRSD for CCC(«) « 30.0
LAB FILE ID:RRF80 ->P9714
RRF20 'RRF120'
= >P9716= >P9713
RRF50 ->P9715RRF160=>P9712
I1 11 COMPOUND IRRF20
IPhenol * 1.375Ibis(2-Chloroethyl )ether 1 1.31112-Chlorophenol 1 1.4331 1 .3-Dichlorobenzene 1 1.4851 1 .4-Dich lorobenzene * 1.516IBenzvl alcohol 1 1.0241 1 ,2-Dich lorobenzene 1 1.55812-Methvlohenol 1 1.065Ibis(2-Chloroisopropyl ) e t her 1 .33114-Methvlphenol 1 1.275IN-Nitroso-di-n-propylami ne_# .9211 Hexach 1 oroe thane 1 .6591 Ni t robenzene 1 .3511 Isoohorone 1 . 7281 2-Ni t ropheno 1 * .19112 ,4-Dimeth<jlpheno 1 1 .3491 Benzo ic ac id 1 . 130Ib is (2-Ch loroe thoxy ) me t hane_l .3591 2 .4-Dich loropheno 1 « .2991 1 ,2 ,4-Tr ich lorobenzene 1 .363(Naphthalene 1 1.02014-Ch loroan i 1 me 1 .360IHexach lorobutad iene « .2331 4-Ch loro-3-methylpheno 1 ____ * .27912-Methvlnaphthalene 1 .5501 Hexach lorocyc lopentad iene _ # .31812 .4.6-Tr ichlorophenol » .37112 .4.5-Tr ichlorophenol 1 .3881 2-Ch loronaphtha lene 1 1.20412-Nitroani 1 me 1 .2851 Dimethvlphtha late 1 1.4841 Acenaphthvlene 1 1.8321 2 .6-Din i t roto luene 1 .28413-Nitroani 1 me 1 .2421 Acenaph thene * 1.2041 2 .4-Dm 1 1 ropheno 1 * .08314-Nitrophenol * .0881 1
RRF50
1.3531.2621.3751.3821.4341.0241.3901.201.413
1.201.884.554.334.690. 193.329.153.341.280.324.907.352.194.259.511.376.381.392
1.170.285
1.3261.746.286.226
1.125. 092. 080
RRFBO
1.3581.2401.3801.3401.3921. 0401.2951. 098.394
1. 098.866.507.330.637.197.316.165.320.288.324.772.345. 190.260.495.410.399.408
1.208.315
1.3531.633.308.248
1. 131.137.086
1RRF120 IRRF160= = = ««=«= )..====1.2571 1.2091.2021 1.0101.3061 1.3351.311 1 1.3101.3621 1.2281.0341 .9461.3071 1.2761.1721 1.142
.3161 .3751.1721 1.142.8791 .852.5291 .538.3211 .328.5541 .480.1981 .209.3101 .317.1521 .153.3251 .322.2601 .264.3141 .321.6741 .587.3341 .345.1821 .175.2551 .270.4641 .452.4231 .404.4091 .406.4161 .407
1.2001 1.147.333! .351
1.3511 1.2541.4291 1.269.3341 .333.2691 .281
1.1161 1.049.1561 .167.0891 .090
1
RRF
1.3111.2051.3661.3661.3861.0141.3651.136.366
1. 178.880.557.333.618.197.324.150.333.278.329.792.347.195.265.494.386.393.40?
1. 186.314
1.3541.582.309.253
1.125. 127.087
\ 1RSD !
= = = = = |5.6*9.613.5 15.417.6*3.818.514.8 1
11.315.613.0*
10.613.41
16.3 13.5*4.718.514.9 16. 0*5.9 1
22. 0 12.8 111.6*3.6*7.91
10.9*4.2*2.912.219.3 16. 1114.6 17.9 18.614.9*29.8*4.6*
1FORM UI SU -1 1/87 Rev.
141
6CSEMIUOLATILE ORGAN ICS INITIAL CALIBRATION DATA
Lab Name:ETCNJ Contract:__________
Lab Code: Case No.:____ SAS No.: SDG No.:
Instrument ID:GC/MS P Cali b r a t i o n DateCs) OB/25/90 08/25/90
Min RRF for SPCC(#) - 0.050 Max HRSD for CCC(«) 30. (
I LAB FILE ID:IRRF60 ->P9714
RRF20 =>P9716RRF120=>P9713
RRF50 ->P9715RRF160=>P9712
I
!I COMPOUND
I D i benzo f uran1 2 .4-Din i t roto luene1 Diet hvlphtha latel4-Chlorophenyl-phenylether_1 F 1 uorene14-Nitroani 1 mel4,6-Dinitro-2-methylphenol_1 N-N i t rosod ipheny 1 am i ne ( 1 )_*1 4-Bro mo pheny 1 -pheny let her __1 Hexach lorobenzene1 Pen t ach loropheno 1 *1 Phenan t h rene1 An t hraceneIDi-n-butvlphthalate1 F 1 uo r an t hene *1 PvreneIButvlbenzvlphthalate13 ,3 '-DichlorobenzidineIBenzo(a)anthracene1 Ch r vseneIbis(2-Ethylhexyl )phthalate_1 Di-n-ocfolphtha late *1 Benzo (b ) f luoranthene1 Benzo (k ) f luorantheneIBenzo(a)pvrene *1 Indeno ( 1 ,2 ,3-cd )pyrene _____IDibenzCa th)anthracene1 Benzo (q ,h f i Jperylene
1 Ni t robenzene-d51 2-F luorob iphenul! Te rphenv 1 -d!4IPhenol-d512-Fluorophenol12 ? 4 F 6-Tr i br o mop he no 11
RRF20
1.529.369
1.352.556
1.139. 171. 116
* .544.231.288
* . 115.993
1.0051.345
* .876.884.751. 180
1. Ill.972.920
1.6891.3251. 129
• .969.807.568.700
.3411.3381.2371.4791.300. 171
RRF50
1.427.362
1.231.511
1. 026. 191. 130.540.225.277. 116.971.961
1.280.791.779.773.273
1. 074.971.896
1.7411.2231.3081. 036.828.590.703
.3331.2721.3011.4341.164. 156
1RRF80 IRRF120
1.5101 1.390.4161 .441
1.2391 1.211.5301 .531
1.0591 1.054.2361 .263.1441 .153.5161 .504.2201 .207.2631 .256.1201 .117.9471 .907.9711 .886
1.1091 .942.7951 .768.7691 .736.7901 .799.3171 .330
1.1241 1.100.9731 .940.9581 .950
1.7671 1.6931.2761 1.3491.1661 1.0571.0711 1.058.9631 1.013.6891 .731.8241 .862
.3381 .3381.2671 1.1981.3231 1.3331.4481 1.4451.1341 1.140.1711 .182
1
RRF160
1.268.461.991.495
1. 046.284. 154.449.213.253. 121.849.783.791.728.720.896.338
1. 1971. 0021.0391.7501.4421. 1531.111.980.707.846
.3441. 1131.5061.3191. 174.185
RRF
1.425.410
1.205.524
1. 065.229.139.511.219.267. 118.933.921
1. 093.792.777.802.288
1. 121.972.953
1.7261.3231. 1621. 049.918.657.787
.3391.2381.3401.4251. 182.173
\ 1RSD 1
»«» 17.4110.7!10.914.414. 1 1
20.7111.7!7.5*4.315.5 !2. 1*6.119.6 1
21.1 16.8»8.3 17.01
22.714. 1 12.2 15.712.0-6.217.9 15. 0*10.2 111. 1 110.1 1
1.2 16.917.5 14.3 15.716.61
1
(1) Cannot be separated from Dipheny1 amineFORM UI SU -2 1/87 Rev.
142
TOTflL ION CHKOnflTOeRBH
58888-
File >P?716 35.0-900.8 aau.
688888- -"
688888-
088888-
588888-
408888-
488888-
308888-
388888-
858888-
888888-
158888-
1888IFB-'BNH 28 PPtl
1688 8888
6? i -
" itlil r.24 88 38 36 48 44 48
Data File: >P9716::U5Name: SSTD20Miac: IFB/BNA 20 PPM
Id File: IP0085::PFT i t l e : IFB/BNA. PP/BNA, TCLBN1Last C a l i b r a t i o n : 900823 17:10
Operator ID: KU0796Quant Time: 900825 19:21I n jec ted at: 90082? 18:30
Quant Output File: AP9716::UL
BTL* 6
143
QUANT REPORT Page 1
Operator 10: KU0786Output File: ~P9716:»ULOata File: >P9716::U5Name: SSTD20rtisc: IFB/BNA 20 PPM
ID File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900823 17:10
Compound
Quant Rev/: 7 Quant Time:In jected at:
Di lut ion Factor:
900825 19:2190082? 18:30
1.00000
BTL* 6
R.T. Scan* Area Cone Units
1)2)2)3)4)5)6)7)8)8)8)9)9)9)10)10)10)11)12)13)14)15)16)16)17)18)19)19)20)21)21)22)23)24)25)26)27)27)28)29)30)31 )31 )
•d 4-1, 4-Dich lorobenzeneN-Nitrosodi methyl am meN-Ni trosodimethylamine2-Fluorophenol (SURR)b is (2-Ch loroe t hyl ) etherPhenol -05 (SURR)Pheno 12-Chlorophenol1.3-Dich lorobenzene1,3-Dich lorobenzene1 . 3-Dieh lorobenzene1 , 4-Dich lorobenzene1 .4-Dich lorobenzene1 , 4-Dich lorobenzene1.2-Dich lorobenzene1 ,2-Dich lorobenzene1 ,2-Dich lorobenzeneBenzyl alcoholN-Nitrosodi-n-propylamineHexach 1 o roe thane2-Me t hylpheno 14-Me thy Ipheno 1b is (2-Ch lore isopropyl )etherbis(2-Chloro isopropyl )ether
*d8-NaphthaleneNitrobenzene-05 (SURR)Nit robenzen*Ni t robenzena- i .Isophorone SSte"-2-Ni t rophenaJHHT2-Ni t ropheno^R^^2 ,4-Di methyl phenolb is (2-Ch lo roe thoxy)aie thane1 ,2 ,4-Tr ich lorobenzene2 . 4-Dich loropheno 1Benzoic acidNaphtha laneNaphtha lene4-Ch loroan i 1 ineHexach lorobutadiene2 -Methyl naphtha lenep-Ch loro-m-creso 1p-Ch loro-m-creso 1
12.345.185.228.9211.7711.6111.6511.8312.2212.3812.9112.2212.3812.9112.2212.3812.9112.8913.8013.8413.3613.8013.4013.8416.2014.0713.4414.1114.8614.8615.1115.3915.6716.1015.8615.8215.8616.2516.5316.9218.4219.4419.54
3732123205345337339348367375401367375401367375401400445447423445425447563458427460497497509523537558546544546565579598672722727
14000153895391290998M9177510351896260100292103970106100109084103970106100109084103970106100109084716966 4476 M46106745 74M8928 OM2315314634476352812189969836041735073417454628304085431864997130330859113205
24285885839M5557013107327192894
40.00 UG/ML42.45 UG/ML3.08 UG/ML20.25 UG/ML20.12 UG/ML19.08 UG/ML17.30 UG/ML19.51 UG/ML20.45 UG/flL20.87 UG/ML21.46 UG/ML19.69 UG/ML20.09 UG/ML20.66 UG/ML18.90 UG/ML19.29 UG/ML19.83 UG/ML33.56 UG/ML15.84 UG/ML19.11 UG/ML19.67 UG/ML27.18 UG/ML15.64 UG/ML9.89 UG/ML40.00 UG/ML16.71 UG/ML1.96 UG/ML16.42 UG/ML19.15 UG/ML1.25 UG/ML16.67 UG/ML18.43 UG/ML16.37 UG/ML19.61 UG/ML18.67 UG/ML17.31 UG/ML.273 UG/ML
20.66 UG/ML- 18.86 UG/ML18.86 UG/ML
>20.05 UG/ML.921 UG/ML.980 UGJKML
90100100
8494869891868799969798969785
92
1001009594737593618794879495
8790
9885100100
144
QUANT REPORT Page
Operator ID: KU0786Output File:Data File:Name: SSTD20Misc: IFB/BNA 20 PPM
Quant Rev: 7
>P9716::U5
Quant Time:In jected at:
Di lut ion Factor:
900825 19:2190082? 18:30
1.00000
5TL* 6
ID Fila: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900823 17:10
Comoound R.T. Scan# Area Cone Un»ts
31)32)33)34)34)35)35)36)37)37)38)39)40)41)41 )42)43)44)45 )46)'<7 )"' ix t47)48)49 )50)51)51)52)53)54)55)56)56)57)58)59)60)£,0)61)61)62)63)
p-Chloro-m-cresol*dlO-Acenaphtha leneHexach lorocyclopentadiene2,4,6-Trichlorophenol2,4,6-Trichlorophenol2,4,5-Trichlorophenol2.4,5-Trichlorophenol2-Fluorobiphenyl (SURR)2-Chloronaphthalene2-Chloronaphthalene2-Ni t roan i 1 ineDimethyl phthalateAcenaphthy lene2.6-Oinitrotoluene2,6-Dinitroto luene3-Ni t roan i 1 ineAcenaph t hene2,4-DinitrophenolDibenzof uran2,4-Dinitrotoluene4-Ni t ropheno 14-Ni t ropheno 14-Ni t ropheno 14-Ni t roan i 1 ineDiethyl phthalateF 1 uorene4-Ch lorophenyl phenyl ether4-Ch lorophenj*^ phenyl ether2,4,6-Tribroipfkhanol (SURR)1 . 2-DiphenymBgiraz ine
•d!0-Phenanth«*SRe4,6-Dini t ro-o-creso 1N-Ni trosodiphenylanvineN-Nitrosod ipheny lamina4-Bromopheny 1 phenyl etherHexach lorobenzenePentachlorophenolPhenanthrenePhenanthreneAnthraceneAnthraceneDi-n-butyl phthalateFluorant hene
18. 1621.7619. 1919.4419.5419.4419.5419.7019.4419.9320.4021. 1721.2521.3322.5321.7021.8622.0222.3522.5323.4523.5323.9423.6323.4523.4523.2423.5324.2624.0226.3823.8123.5323.9425.0325.4426.0326.4626.5326.4626.5828.6330.22
659836710722727722727735722746769807811815874833841849865874919923943928919919909923959947106393792394399710171046106710731067107311741252
66355M24318638647450974721245097472121626895090
146347346301804332227913451444868294171463661005418595444868107154329318720823M1643841384885289675652075412937333632619452723291459389154840719262167010168964167010168964226149147332
22.47 UG/ML40.00 UG/ML10.90 UG/ML16.61 UG/ML17.39 UG/ML18.66 UG/ML19.54 UG/ML17.43 UG/ML.604 UG/ML
17.38 UG/ML16.61 UG/ML23.03 UG/ML19.24 UG/ML19.38 UG/ML25.20 UG/ML22.31 UG/ML19.18 UG/ML21.25 UG/ML19.06 UG/ML24.40 UG/ML20. 19 UG/ML8.16 UG/ML6.01 UG/ML29.88 UG/ML25.33 UG/ML20.05 UG/ML1.58 UG/ML20.24 UG/ML19.42 UG/ML17.41 UG/ML40.00 UG/ML17.81 UG/ML1.53 UG/ML
19.36 UG/ML15.21 UG/ML15.08 UG/ML27.23 UG/ML18.71 UG/ML18.93 UG/ML19.07 UG/MLJ.9.29 UG/ML27.04 UG/ML26.04 UGf'ML
1009697959893999956968895987979100971008992100100100
939697889782988178969299929.y^'97969696
145
QUANT REPORT
Operator ID: KU0786Output File: ~P9716::ULData File: >P9716»:U5Name: SSTD20Misc: IFB/BNA 20 PPM
Quant Rev: 7 Quant Time:In jected at:
Di lut ion Factori
Page 3
900825 19:21900825 18:30
1.00000
BTL* 6
ID Fi le: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900823 17:10
Compound R.T. Scan* Area Cone Un i ts
63)64),5)66)67)66)69)69)70)70)71)72)73)74)75)75)75)76)76)76)"•7)/7)78)79)80)
FluoranthenePyrene•d!2-ChryseneBenz id ineTerphenyl-D14 CSURR)Butyl benzyl phthalateBe nzo (a) anthraceneBenzo(a)anthraceneChryseneChrysene3 .3 '-Dlchlorobenzidinebis (2-Ethylhexyl ) phthalate
•d!2-PeryleneDi-n-octyl phthalateBenzo (b ) f luorantheneBenzo (b)f luorantheneBenzo (b)f luorantheneBenzo(k)fluorantheneBenzo (k ) f luorantheneBe nzo (k ) f luorantheneBenzo (a)pyreneBenzo (a)pyreneIndeno (1,2 ,3-c ,d )pyrenebibenzo(a,h)anthraceneBenzoCghi )perylene
30.30.34.26.31.33.34.34.34.34.34.35.39.37.37.38.38.37.38.38.38.38.43.43.44.
91918003563174887488762719109907999907990799284046
1286128614771046131814041474148114741481147515001693159016341638168316341638168316381683189419001952
1486711486711719533626
106337645879555383575955538357515475790771013848563BM6714857209491226714857209491225720949122409102878735501
26.27.40.2.14.20.20.17.20.18.25.23.40.19.22.19.16.23.19.17.20.17.17.17.16.
27980004487342869835014400668244693791107683041831
UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/ML
9797981009397100100100100869082998889899192929191100100100
* Compound is ISTD
146
TOTAL ION>PO?15 35.B-900.0 «*u. |fJD8i
«M
Data File: >P9715::U5Name: SSTD50Misc: IFB/BNA 50 PPM
Id File: IP0085::PFT t t l e : IFB/BNA, PP^BNA, TCLBN1Last Calibration: 900623 17:10
Operator ID: KU0786Quant Time: 900827 09:31Iniected at: 900829 17:32
Quant Output File: AP9715::UL
BTL* 5
147
QUANT REPORT Page
Operator ID:Output File:Data File:Name: SSTD50Misc: IFB/BNA 50
KU0786
>P9715::U5
PPM
Quant Rev: 7 Quant Time:In iected at:
Dilut ion Factor:
900827 09:31900825 17:32
1.00000
BTL* 5
ID File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900823 17:10
Compound R.T. Scan* Area Cone Un i ts
1)2)2)3)4)5)6)7)8)8)8)
. 9)9)9)10)10)11)12)12)13)14)15)15)16)16)17)18)19)19)19)19)20)21)21)22)22)23)24)25)26)27)27)28)
*d 4-1 ,4- Dich lorobenzeneN-Ni t rosod i me thy lamineN-Ni t rosod i me thy lamine2-Fluorophenol (SURR)b is(2-Ch loroethvl ) etherPhenol -05 ' (SURR)Pheno 12-Ch loropheno 11 ,3-Dich lorobenzene1 ,3-Dich lorobenzene1.3-Dich lorobenrene1 ,4- Dich lorobenzene1 ,4- Dich lorobenzene1 ,4-Dich lorobenzene1 .2 -Dich lorobenzene1 ,2-D ich lorobenzeneBenzyl alcoholN-Nitrosod i-n-propy lamineN-Ni t rosod i-n-propy lamineHexach 1 or oe thane2-Methy Ipheno 14-Methy Ipheno 14-Me thy Ipheno 1bis(2-Chloro i sop ropy 1 )etherbis(2-Chloro i sop ropy 1 )ether•dB-NaphthaleneNitrobenzene-05 (SURR)Ni t robenzenaNi t robenzenaNi t robenzenaNi t robenzenaIsophorone2-Ni t ropheno 1 f2-Ni t ropheno 12 ,4-Dime thy Ipheno 12 ,4-Dime thy Ipheno 1b is (2-Ch loroethoxy) me thane1 ,2 ,4-Tr ich lorubenzene2 .4-0 ich loropheno 1Benzoic acidNaphtha laneNaphtha lane4-Ch loroani 1 ina
12558111111111212121212121212121314131313131313161413131314141415151615161516151615
.35
.19
.25
.93
.80
.63
.68
.84
.23
.41
.94
.23
.41
.94
.41
.94
.92
.85
.10
.85
.83
.39
.83
.41
.85
.21
.10
.39
.47
.83
.16
.91
.91
.11
.42
.11
.70
.11
.89
.01
.89
.28
.89
3742225206347339341349368377403368377403377403402448460448447425447426448564460425429447463500500510525559539559548554548567548
1440991319013861
2095982272432583392437702476162489062583712503122489062583712503122583712503121843661593123465599787216268172221216268743143060353208322141010427625033651532222314587228936
1282162191282714
2268262153571864331014898908
6030502961
401002
4548464246474947454746454483388405550634820404018411394524243.
384343
. 50.
3* 45.
.00
.94
.95
.31
.40
.26
.57
.81
.57
.37
.83
.80
.54
.05
.63
.21
.83
.02
.27
.19
.43
.94
.97
.77
.08
.00
.79
.34
.40
.46
.08
.34
.93
.10
.54539.90.71.71.96678.92583
UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUGVML
911001007385918496878888979897999788823889876097100100949361695184975881946884939991888961
148
QUANT REPORT Pag*
Operator ID: KU0786Jut put File: "-P9715JData File: >P9715:Name: SSTD50Misc: IFB/BNA 50 PPM
ID Fi le: IP0085::PFT i t l e : IFB/BNA, PP/BNA. TCLBN1Last Calibration: 900823 17:10
Compound
Quant Rev: 7 Quant Time:In jected at'
Di lut ion Factor
900827 09:31900825 17:32
1.00000
BTL* 5
R.T. Scan* Area Cone Uni ts
2B)28)?9)30)31)32)33)34)34)35)35)36)37)37)37)38)39)39)40)41)U)42)42)43)44)45)46)47)47)47)47)47)48)49)50)50)51)51)52)53)54)55)56)
4-Ch loroan i 1 ine4-Ch loroan i 1 ineHexachlorobutadiene2-Methylnaphthalenep-Ch loro-m-creso 1
•dlO-AcenaphthaleneHexachlorocyc 1 open tad iene2,4,6-Trichlorophenol2,4,6-Trich loropheno 12,4,5-Tnchlorophenol2,4,5-Trichlorophenol2-Fluorobiphenyl (SURR)2-Chloronaphthalene2-Chloronaphthalene2-Chloronaphthalene2-Ni t roan i 1 ineDimethyl phthalateDimethyl phthalateAcenaph thy lene2,6-Dinitrotoluene.2 ,6-Din i t roto luene3-Ni t roan i 1 ine3-Ni t roan i 1 ineAcenaph thane2 ,4-Dini t ropheno 1Dibenzof uran2 ,4-Dini t rotoluvne4-N 1 1 rophano bt*.4-N i t rophenalfe :4-Nitrophenatjr^p4-Ni t ropheno IT •"4-Ni t ropheno 14-Ni t roan i 1 ine (Diethyl phthalateFluoreneFluorene4-Ch lorophenyl phenyl ether4-Ch lorophany 1 ph-jnyl ether2 ,4,6-Tr ibromophenol (SURR)1 ,2-Dipheny Ihydraz ine
•dlO-Phenanthrene4,6 -Din i t ro-o-cresolN-Ni t rosod ipheny lamina
16.2816.5616.9318.4318.1721.7719.2119.4519.5519.4519.5519.7419.4519.5519.9620.4121.2022.4021.2621.3622.5621.7322.3821.8722.0422.3822.5623.2623.4623.5423.6823.9523.6823.4823.4624.2823.2623.5424.2824.0326.3923.8523.54
5675815996736608377117237287237287377237287487708098688128178768358678428508678769109209249319449319219209609109249609481064939924
78152234294129323339735172399252476118609120243123815120243123815401510131324228
3692578998641841511322
55112990140114122712853718
35513929160450422114122209925258105384587667360261M388570323786285913965161321493563614753216545216417820
15.38 UG/ML46.10 UG/ML39.30 UG/ML46.53 UG/ML52.27 UG/ML40.00 UG/ML32.23 UG/ML42.67 UG/ML43.93 UG/ML47.93 UG/ML49.36 UG/ML41.44 UG/ML1.50 UG/ML.484 UG/ML
42.23 UG/ML41.58 UG/ML51.45 UG/ML1.39 UG/ML45.85 UG/ML48.76 KG/ML61.73 UG/ML52.08 UG/ML2.72 UG/ML44.83 UG/ML59.35 UG/ML44.46 UG/ML59.78 UG/ML3,81 UG/ML45.85 UG/ML19.13 UG/ML8.33 UG/ML12.11 UG/ML83.28 UG/ML57.68 UG/ML45 . 16 UG/ML.399 UG/ML4.03 UG/ML46.54 UG/ML44.48 UG/ML
. 46.86 UG/ML40.00 UG/ML
> 49.94 UG/ML3.94 UG^ML
7262958210096989796969599576097809897977979100100961009291100100100100100
92987599909584987277
49
QUANT REPORT Paga 3
Operator ID: KU0786Output File:Data File:Name: SSTD50Misc: IFB/BNA 50 PPM
Quant
>P9715»:U5
7 Quant Time:In iactad at:
Dilution Factor:
900827 09:31900825 17:32
1.00000
BTL* 5
ID File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900823 17:10
Compound R.T. Scan* Area Cone Units
56)57)58)59)60)60)61)61)62)63)63)64)65)66)67)66)69)69)70)70)71)72)73)74)75)75)75)76)76)76)77)77)77)78)79)80)
N-Ni trosodiphenylamine4-Bromopheny 1 phenyl etherHexach lorobenzenePentach loropheno 1PhenanthrenePhenan t hreneAnthraceneAnthraceneDi-n-butyl phthalateFluorantheneF 1 uorant henePyrene•d!2-ChryseneBenz id ineTerphenyl-D14 (SURR)Butyl benzyl phthalateBenzo (a ) anthraceneBenzo (a ) anthraceneChryseneChrysene3 ,3 ' -Dich lorobenz id inebis(2-Ethylhexyl ) phthalate•d!2-PeryleneDi-n-octyl phthalateBenzo (b )f luoran thaneBenzo (b ) f luoran thaneBenzo (b ) f luoran thaneBenzo (k ) f luorawthaneBenzo (k ) f luoi |i|heneBenzo (k ) f luo«*£itheneBenzo (a )pyraiwFrBenzo (a)pyrenaBenzo (a )pyrene fIndeno(l,2,3-c,d )pyrenaDibenzoCa.h ) anthraceneBenzoCghi )perylene
23.25.25.26.26.26.26.26.28.30.30.30.34.26.31.33.34.34.34.34.34.35.39.37.38.38.39.38.38.39.38.38.39.43.43.44.
950546054760476063249393790558337587758777281911010700010700010700293947
944998
1018104710681074106810741174125312871287147710471319140514751481147514811476150116931591163516381684163516381684163516381684189519001953
2172979046511137746808390452386361390452386361514481318031313065313065135054
84912196541304981812491639771812491639774614815120169242150675M105861113174896601058611131748966010586111317489660716665105860808
48363669454546466458576140638534944504594574050525644535745566047434440
.10
.98
.27
.19
.74
.26
.61
.12
.31
.77
.85
.62
.00
.08
.09
.32
.33
.63
.68
.85
.94
.07
.00
.64
.67
.31
.61
.95
.68
.69
.26
.15
.65
.72
.60
.90
UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/ML
96909897979896999596969898100929010010010010085958198909190949493929392100100100
* Compound is ISTD
150
TOTflL ION CH*OHBT00*fln>P9714 33.0-300.0 MU
400 . 000 1200
iFB'BNn1600 3000
32 36 40 44 40
Data File: >P9714::U5Name: SSTD80disc: IFB/BNA 80 PPM
Id File: IP0085::PFTitle: IFB/"BNA, PP/BNA, TCLBN1Last Calibration: 90082? 17:10
Operator ID: KU0786Quant Time: 900827 09:28Injected at: 90082? 16:33
Quant Output File: AP9714::UL
BTL* 4
151
QUANT REPORT Page
Operator ID: KU0786Output File: "P9714::ULData Fila: >P9714::U5Name: SSTD80Misc: IFB/BNA 80 PPM
ID Fila: IP0085::PFTitle: IFB/BNA. PP/BNA, TCLBN1Last Calibration: 900823 17:10
Compound
Quant Rev: 7 Quant TimeiIn iected ati
Dilut ion Factor:
900827 09:28900825 16:33
1.00000
BTL* 4
R.T. Scan* Area Cone Un i ts
1223456788a999
10101112121213141515151616171819191920212122222 >2324252626
)))))))))))))))))))))))))))))))))))))))))))
*d4-l ,4-Dich lorobenzeneN-NitrosodimethylamineN-Ni trosodi me thy lamina2-Fluoroohenol (SURR)bis(2-Chloroethvl ) etherPhenol-05 ' (SURR)Pheno 12-Ch loropheno 11, 3-D ich lorobenzene1,3-0 ich lorobenzene1,3-Dich lorobenzene1 .4-0 ich lorobenzene1 , 4- D ich lorobenzene1 ,4-Dich lorobenzene1 ,2-Dich lorobenzene1 ,2-Dich lorobenzeneBenzyl alcoholN-Nitrosod i-n-p ropy laminaN-Ni trosodi-n-propylamineN-Ni trosodi-n-propy laminaHexachloroethane2-Me thy Ipheno 14-Me t hy Ipheno 14-Me thy Ipheno 14-Me thylpheno 1b is (2-Ch loro i sop ropy 1 )etherb is (2-Ch loro i»opropyl Jet her*d8 -Naphtha !•!»*.£.Ni t robenzene-B|Sf (SURR)Ni t robenzen«.-j s,5gi*Ni t robenzeneNi t robenzeneIsophorone f
2-Ni t ropheno 12-Ni t ropheno 12 , 4-Dimethy Ipheno 12 , 4-Dimethy Ipheno 1o is (2-Ch 1 o roe thoxy)me thanebis (2-Ch loroe t hoxy) me thane1 ,2 , 4- Tr ich lorobenzene2 ,4-Dich loropheno 1Benzoic acidBenzoic acid
12558111111111212121212121212121313141313131313131316141313141414151515151516151516
.36
.25
.31
.95
.81
.67
.71
.88
.24
.40
.93
.24
.40
.93
.40
.93
.97
.79
.91
.11
.85
.87
.40
.79
.87
.42
.85
.23
.11
.40
.87
.18
.95
.95
.13
.36
.46
.64
.72
.13
.91
.66
.17
3752528207348341343351369377403369377403377403405445451461448449426445449427448565461426449464502502511522527536540560549537562
1545762139361213635070638338244767341992042653941436343043540027241436343043540027243043540027232148111864267631594581565983395502843894335
33955012182447663570248385421173834103772376702726782129512241841623036079921717364501369535 -328245 _" 4350 >187819M"
40.152.8.70.76.74.68.75.73.76.71.71.73.68.70.65.136.2.59.13.58.81.78.1.
93.74.29.40.66.28.17.61.67.3.68.3.66.3.58.69.71.2.87.
00636667127436178268310783658690276455237913422063531600265203810297680190483398810499
UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/ML
891001007379918297888689989597969882777738938662909610010095956151799659828994838095948696
152
QUANT REPORT Page 2
Operator ID: KU0786Output File: ~P9714J:ULData File: >P9714::U5Name: SSTD80Misc: IFB/BNA 80 PPM
Quant Raw: 7 Quant Time:In jected at:
Dilution Factor:
900827 09:28900825 16:33
1.00000
BTL* 4
ID Fi
Last
26)27)27)28)28)28)29)29)30)30)31)32)33)34)34)35)35)36)37)37)37)38)39)39)40)41)41)42)42)43)44)45)45)46)47)47)47)47),47)48)49)50)50)
la: IP0085::PF: IFB/BNA, PP/BNA , TCLBN1Calibration: 900823 17:10
Compound
Benzoic acidNaphtha leneNaph t ha lene4-Ch loroan i 1 ine4-Ch loroani 1 ine4-Ch loroan i 1 ineHexach lorobutadieneHexachlorobutad lene2-Methylnaphthalene2-Methylnaphthalenep-Chloro-m-cresol
•dlO-AcenaphthaleneHexach lorocyclopentadiene2,4,6-Trichlorophenol2,4,6-Trich loropheno 12,4,5-Trichlorophenol2 ,4,5-Trichlorophenol2-Fluorobiphenyl (SURR)2-Chloronaphthalene2-Chloronaphthalene2-Chloronaphthalene2-Ni t roani 1 ineDimethyl phthalateDimethyl phthalateAce naph thy lene2,6-Dinitroto luene2,6-Dinit roto luene3-Ni t roani 1 in*3-Ni t roani 1 in*'Acenaphthene> -S2 ,4-0 in i t rophinolDibenzofuranDibenzofuran *2 ,4-Din i t roto luene4-Ni t ropheno 14-Ni t ropheno 14-Ni t ropheno 1^-Ni t ropheno 14-Ni t ropheno 14-Ni t roan i 1 ineDiethyl phthalataFluoreneFluorene
R
16151615161616161818182119191919191919191920212221212221222122222222232323232323232324
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
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.
.•
B
•
,
.
•
•
.
,
.
.
•
.•
•
.•
,
k
*
T.
17932993295842924576197720475747577547579645224028405977368908084059284856759975504830
Scan*
562550568550568582574599674689661837711724729724729738724729748772810868813819877837866843852852868877911921925
1-934-946934922921961
Area
2717215435
8803075032
1288803937013020
2171095649352880
296659264729217269211164216247211164216247670578232546970
639487166634716093321358645681629622204271311062130
599009727132540
799498220427395545363171079650128041250966561425605125339
Cone
121
62.
2372,
6172,
83405671738082662.
69738336884113911
72141
.73
.10
.54924.66.28856.57.20368.92.00.31.46.18.28.21.00.54760.76.44.97.77.59.07.72.35.48.12.15.239
7511067829162216492
.74
.27
.12
.85
.54
.62
.71
.17
.88
.89
.55^ .710
Units
UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUGXML
q88869858756297988373100979697969697975658938398979482781001009810053808510010010010010091929683
153
QUANT REPORT Page
Operator ID: KU0786Dutput File: "P9714HULData File: >P9714itU5Name: SSTD80Misc: IFB/BNA 60 PPM
ID File: IP0085::PFT i t l e : IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900823 17:10
Compound
Quant Rev: 7 Quant TimeIn iected at:
Dilut ion Factor
900827 09:28900825 16:33
1.00000
BTL* 4
R.T. Scant Area Cone Units*
51)51)~2)53)54)55)56)56)57)56)59)60)60)61)61 )62)63)63)64)65)S6 )67)68)69)69)70)70)71)72)73)74)75)75)75)76)76)76)77)77)78)79)80)
4-Ch lorophenyl phenyl ether4-Ch loropheny 1 phenyl ether2 ,4, 6-Tr ibromopheno 1 (SURR)1 ,2-Diphenylhydrazine
•dlO-Phenanthrene4,6-Dinitro-o-creaolN-Nitrosod ipheny lam ineN-Nitrosodiphenylamine4-Bromopheny 1 phenyl etherHexach lorobenzenePentachlorophenolPhenanthrenePhenan t hreneAnthraceneAnthraceneOi-n-butyl phthalateFluorantheneF luoran thenePyrene«dl2-ChryseneBenz id meTerphenyl-D14 (SURR)Butyl benzyl phthalateBenzo (a ) anthraceneBenzo(a)anthraceneChryseneChrysene3,3'-Dichlore**nzidinebis (2-Ethylhejaj&^)phtha late•d!2-P«ryl •nipper.Di-n-octyl phfh*l«taBenzo (b ) f luoran theneBenzo (b) f luoran then*Benzo (b ) f luoran thaneBenzo (k ) f luoran theneBenzo (k ) f luoran theneBenzo (k) f luoran theneBenz-.j x« )pyraneBenzo (a )pyreneIndenod ,2 , 3-c,d )pyrenaDibenzo (a ,h) anthraceneBenzoCghi )perylene
232324242623232325252626262626283030303426313334343434343539373838393838393839434344
.28
.56
.30
.05
.39
.91
.56
.99
.07
.48
.07
.50
.64
.50
.64
.65
.26
.95
.95
.81
.05
.58
.33
.75
.90
.75
.90
.77
.28
.21
.11
.01
.09
.03
.01
.09
.03
.09
.03
.34
.42
.52
9119259619491064942925946999101910481069107610691076117512541288128814781047131914051475148214751482147615011694159116351639168516351639168516391685189719011955
25646280379907096704223772291085863072338901416605619847390193714232732608714232732608836328600123580195580195154291163244083592436543468783001423468783001429784629573394187332860M240451219586201759240451219586201759
+1 219586-201759181347129832155135 ^
~?
7,77.77.82.40.88.5.73.57.55.
113.71.73.72.74.89.94.91.97.40.10.61.87.82.71.84.73.176.97.40.82.87.80.73.90.82.75.85.78.81.83.
. 76.
061596890063804388116835186956145642370023991563509046207100249532800927597983333872
* Compound is ISTD
UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/ML
t
154
96919385978078989197959796969597969799971009297100100100100849382988890899293929191100100100
TOTHL ION CHROnflTOBRflnMl* >P9713 33.0-300.8 M
4«* . ••• 12M
wrnaaae
Data File: >P9713::U5Name: SSTD120M i s c : IFB/BN6 120 PPM
Id File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900823 17:10
Operator ID: KU07B6Quant Time: 900827 09:27In,ectad at: 900825 15:34
Quant Output File: ~P9713::UL
BTL* 3
155
QUANT REPORT Paga
Operator ID: KU0786Output File: AP9713::WLData Fila: >P9713::U5Mama: SSTD120Misc: IFB/BNA 120 PPM
ID Fi la: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900823 17:10
Compound
Quant Rev: 7 Quant Time:In jacted at:
Dilution Factor:
900827 09:27900829 19:34
1.00000
BTL* 3
R.T. Scan* Area Cone Units
1 )2)2)3)4)5)6 )7)8)8)8)9)9)9)10)10)10)11)12)12)2)
j.3)14)15)15 )15)16)16)17)18)19)19)20)20)20)21)21)22)22)23)23)24)2S)
•d4-l ,4-Dich lorobenzeneN-Ni trosodimethylamineN-Ni t rosod i me thy lamine2-Fluorophenol (SURR)b is (2-Ch loroethvl ) etherPheno 1-D5 ' (SURR)Pheno 12-Ch loropheno 11 ,3-Dich lorobenzene1 ,3-Dich lorobenzene1 ,3- Dich lorobenzene1,4- Dich lorobenzene1 ,4-Dich lorobenzene1,4-Dich lorobenzene1 ,2-Dich lorobenzene1 ,2-Dich lorobenzene1 ,2-Dich lorobenzeneBenzyl alcoholN-Ni t rosod i-n-propy lamineN-Ni t rosod i-n-propy laminaN-Ni t rosod i-n-propy lamineHexach loroe thane2-Methylpheno 14-Methy Ipheno 14-Methy Ipheno 14-Methy Ipheno 1b is (2-Ch loro isopropy 1 )etherb is (2-Ch loro iftppropyl )ather
•d8-Naohthalana),.Nitrobanzan»»C4t (SURR)Ni t robenzanaNit robanzenaIsophorone fIsophoroneIsophorona2-Ni t rophano 12-Nitrophanol2 ,4-Dime thy Ipheno 12 , 4-D i me t hy 1 pheno 1bis (2-Ch loroethoxy ) me thanebis (2-Ch loroethoxy )me thane1 ,2 ,4-Tr ichlorobanzana2 ,4-Dich loropheno 1
12.5.5.8.11.11.11.11.12.12.12.12.12.12.12.12.12.13.13.13.14.13.13.13.13.13.13.13.16.14.13.14.14.14.15.14.15.15.15.15.15.16.15.
36283296857175892642952642952642950180991587914280914487231544219098199817374964741384
3752729208350343345352370378404370378404370378404407446455463449451427446451428449565463428466500504514504513523529536541560546
1534913547731555752472155331266517857898060155660353862715060184360353862715060184360353862715060184347625614210404725863482435225396674191261497553966714550774128553959562283251597533049457899204251304949249
328792360485159352587853948852202425719
4025411
10611011194106108112107104108103100103992033
9019921291164
149894540994290487122
103698488
1101" 5
.00
.89
.18
.49
.64
.83
.92
.76
.28
.52
.98
.25
.33
.96
.06
.98
.78
.31
.18
.68
.35
.07
.86
.39
.16
.86
.65
.67
.00
.51
.50
.04
.35
.37
.39
.92
.69
.ta
.47
.26
.88
.77
.79
UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUGJ'ML
891001007392908198868587969496979597857876389687589299100100949364799296976187939379809595
156
QUANT REPORT Paga 2
Operator ID: KU0786Output File: ~P9713::ULData Fila: >P9713::U5Name: SSTD120Misc: IFB/BNfl 120 PPM
ID File: IPOOB5::PFT i t l e : IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900823 17:10
Compound
Quant Rev: 7 Quant TimeIn lac ted at
Dilut ion Factor
900827 09:2790082? 19:34
1.00000
BTL* 3
R.T. Scan* Area Cone Dm ts
25)26)26)26)27)27)28)28)28)29)29)30)30)31)32)33)34)34)35)35)36)57)37)37)38)39)39)40)41)41)42)42)42)43)44)45)45)45)45)46)47)47)47)
2,4-DichlorophenolBenzoic acidBenzoic acidBenzo i c acidNaphtha leneNaphtha 1 ene4-Ch loroani 1 ine4-Ch loroan i 1 ine4-Ch loroani 1 ineHexachlorobutadieneHexachlorobutadiene2- Methyl naphtha lene2-Methylnaohthalenep-Ch loro-m-creao 1
•dlO-AcenaphthaleneHexach lorocyc lopentadiena2,4,6-Trichlorophenol2 ,4,6-Tr ich loropheno 12 ,4,5-Tr ich loropheno 12, 4, 5-Tr ich loropheno 12-Fluorobiphenyl (SURR)2-Ch loronaohthalene2-Ch loronaphtha lene2-Ch loronaphtha lene2-Ni t roam 1 ineDimethyl phthalataDimethyl phthalataAcenaph thy len*2 .6-0 in i t rotoluane2 ,6-Dini t ro toluene3-Ni t roan i 1 in*3-Ni t roani 1 ine3-Ni t roan i 1 ine /Acenaphthene2,4-DinitrophenolDibenzof uranDibenzof uranD ibenzof uranDibenzof uran2,4-Dinitroto luana4-Ni t rophano 14-Ni t ropheno 14-Ni t ropheno 1
15.9415.6816.2316.2715.9416.3115.9416.3116.6016.4316.9418.4718.7518.2021.7919.2219.4919.6119.4919.6119.7719.4919.6119.9820.4621.2422.4221.3021.4222.6221.8122.1122.4021.9122.1122.1122.4222.9523.2722.6223.3023.5023.58
551538565567551569551569583575600675689662838712725731725731739725731749773811869814820879839854868844854854869895911879912922926
4316083609
252723M10157820441
11200066668
1832355558744598
3023947714074451
424459247924314875304073309567304073309567891316331179790
892204247730100509549708
1062506248332328017199862291310047
8302751159343912
103354420977265
32801758126613820848
97.20 UG/ML1.74 UG/ML
121.88 UG/ML48.99 UG/ML1.49 UG/ML
81.91 UG/ML1.26 UG/ML
34.63 UG/ML105.05 UG/ML1.34 UG/ML88.27 UG/ML101.48 UG/ML.586 UG/ML
123.61 UG/ML40.00 UG/ML87.14 UG/ML109.88 UG/ML111.86 UG/ML123.43 UG/ML125.66 UG/ML93.67 UG/ML3.86 UG/ML1. 14 UG/ML
103.92 UG/ML116.58 UG/ML125.85 UG/ML6.22 UG/ML90.01 UG/ML136.80 UG/ML180.70 UG/ML148.70 UG/ML2.17 UG/ML7.47 UG/ML
106.74 UG/ML240.30 UG/ML
.393 UG/ML103.90 UG/ML
.211 L":/ML
.730 Ub/ML174.98 UG/ML10.74 UG/ML
:3»122.27 UG/ML^ 38.54 UGH1L
95389583S9926474629696798310095989495959693566191809796857777100100100981005270513387100100100
157
QUANT REPORT Page
Operator ID: KU0786Output File: ~P9713i:ULData File: >P9713::U5Name: SSTD120Misc: IFB/BNA 120 PPM
ID File: IP0085::PFT i t l e : IFB/BNA, PP/BNA, TCLBN1_a»t Calibration: 900823 17:10
Compound
Quant Rev: 7 Quant TimeIn iactad at
Di lut ion Factor
900827 09:27900825 15:34
1.00000
BTL* 3
R.T. Scan* Area Cone Un i ts
47)47)48)49 )50)50)51)51)52)53)53)54)5'?)5'5)56)56)57)58)59)60)60)M)ol)62)63)63)64)65)66)67)68)69)69)69)70)70)70)71)72)72)73)74)75)
4-Ni t ropheno 14-Ni t ropheno 14-Ni t roan i 1 ineDiethyl phthalate .FluoreneFluorene4-Ch loropheny 1 phenyl ether4-Ch lorooheny 1 phenyl ether2 ,4 ,6-Tr ibromophenol (SURR)1 .2-0 ipheny Ihydraz me .1 ,2-Di phenyl hydraz ine
•dlO-Phenanthrene4.6-Dinitro-o-cresol4,6-Dinitro-o-cresolN-Ni t rosod ipheny lam ineN-Ni t rosod ipheny lamina4-Bromooheny 1 phenyl etherHexach lorobenzenePentach lorophenolPhenan thronePhenanthreneAnthraceneAnthraceneDi-n-butyl phthalateFluoranthaneF luoranthenePyrene•dl2-ChrysenaBenz id ineTerphenyl-D14>« " (SURR)Butyl benzyl plithalateBenzo (a ) anthraceneBenzo (a )anthracene ,Benzo (a ) anthraceneChryseneChrysanaChrysene3,3 '-Dichlorobenzidinabis (2-Ethy Ihexyl ) phthalateb is (2-Ethy Ihexyl )phthalata•dl2-PeryleneDi-n-octyl phthalateBenzo (b)fluoranthana
23.24.23.23.23.24.23.23.24.24.25.26.23.23.23.24.25.25.26.26.26.26.26.28.30.30.30.34.26.31.33.34.34.34.34.34.34.34.35.36.39.37.38.
81038152503427583207094178955803095009496649666526959582056033759298759298792820211103
937'94893792392296391192696295010001065936944926948100010201049106910771069107711751254128812881478104713201405147514831486147514831486147715011546169415911636
1549920023195456900571783681
8143374993952461352999931751288383692652476
16929542182558191229704283536129463100464898159610046489815961043509850761815127815127146546245615859053511114834204132716360
4834204132716360
144968417728
359195397484513(1385973
28.37.
275.136.111.
1.11.
116.124.131.17.40.2.
141.8.
107.81.80.166.102.100.104.102.113.136.131.139.40.16.93.132.121.103.
1.124.106.
1.274.145.1.
. 40.118.139 .
65020813301602131613010006171364784369521746066294207500206422256560575064863125001838
UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/M"UG/hi_UG/MLUG/MLUG/MLUG/ML
10010097949786929297853997807378968293999897999892969798961009196100100100100100100919459839690
158
QUANT REPORT
Operator ID: KU0786Output File: ~P9713»:ULData File: >P9713::U5Name: S5T0120Misc: IFB/BNA 120 PPM
ID File: IP0085::PFT i t l e : IFB/BNA. PP/BNA, TCLBN1Last Calibration: 900823 17:10
Compound
Quant Rev: 7 Quant Time:In iected at:
Di lution Factor:
Page 4
900827 09:2790082? 15:34
1.00000
BTL* 3
R.T. Scant Area Cone Un i ts
75)75)76)'6)76)77)77)77)78)79)80)
Benzo (b)f luorantheneBenzo (b)f luorantheneBenzo (k)f luorantheneBenzo (k)f luorantheneBenzo (k)f luorantheneBenzo Ca )pyreneBenzo (a )pyreneBenzo (a )pyreneIndeno(l,2,3-c,d )pyreneDibenzoCa ,h)anthraceneBenzo (gh i )perylene
38.39.38.38.39.38.38.39.43.43.44.
1103031103031103364654
16401685163616401685163616401685189819031956
302623302832385973302623302832385973302623302832290044209148246607
109109142111112148116116128132120
.29
.36
.77
.94
.02
.89
.73
.82
.43
.61
.41
UG/MLUG/MLDC/MLUG/MLUG/MLUG/MLUG/MLKG/MLUG/MLUG/MLUG/ML
9089939392919191100100100
• Compound is ISTD
159
TOTflL ION CHEOHftTOaHflH
Data Fila: >P9712::U5Name: SSTD160Misc: IFB/BNA 160 PPM
Id File: IP0085::PFTitle: IFB/BNft, PP/BNA. TCLBN1Last Calibration: 900831 12:04
Ooerator ID: KU0786Quant Time: 900831 14:16Injected at: 900829 14:39
Quant Output File: ~P9712::i
BTL* 2
160
QUANT REPORT Page
Operator ID: KU0786Output File: ~P9712::U1-Data Fila: >P9712::U5Name: SSTD160Misc: IFB/BNA 160 PPM
ID Fila: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900831 12:04
Compound
Quant Rev: 7 Quant Time:In jected at:
Oilut ion Factor:
900831 14:16900825 14:35
1.00000
BTL* 2
R.T. Scant Area Cone Un i ts
1)212)3)4)5)6 )7)8)9)9)9)9)9)10)10)10)11)11)12)12)12)13)14)14)14)15)15)15)16)16)17)18)19)19)19)19)19)20)20)20)21)21)
*d4-l , 4- Dich lorobenzeneN-NitrosodimethylamineN-Nitrosodimethylamine2-Fluorophenol ' (SURR)b is(2-Ch loroethvl ) etherPhenol-05 " (SURR)Pheno 12-Ch loropheno 11, 3-D ich lorobenzene1,3-Dich lorobenzene1, 3-D ich lorobenzene1 ,4- Dich lorobenzene1,4-Dich lorobenzene1 ,4-0 ich lorobenzene1 ,2-Dich lorobenzene1,2-D ich lorobenzene1 ,2-Dich lorobenzeneBenzyl alcoholBenzyl alcoholN-Ni trosodi-n-propy laminaN-Ni trosodi-n-propylamineN-Ni t rosod i-n-propy laminaHexach loroethane.2-Methy Ipheno 12-Methy Ipheno 12-Methy Iphenol4- Me thy I phenol4-Methylpheno44-Methylpha r>» V -.;b is (2-Ch loroiujpropy 1 )etherb is (2-Ch loroi*ojaropyl )ether
•d8-NaphthaleneNitrobenzene-05 (BURR)Ni t robenzeneNi t robenzeneNi t robenzeneNi t robenzeneV t robenzeneIsophoroneIsophoroneIsophorone2-Ni t ropheno 12-Ni t ropheno 1
12558111111111212121212121212121213131414131313131313131313161413131314141415151515
.38
.30
.34
.98
.87
.75
.79
.91
.28
.44
.97
.28
.44
.97
.28
.44
.97
.89
.05
.82
.03
.17
.87
.46
.85
.95
.46
.85
.95
.46
.87
.25
.17
.46
.50
.85
.23
.92
.92
.05
.25
.17
.25
3762830
209351345347353371379405371379405371379405401409447457464449429448453429448453429449566464429431448467Wl5Di507517513517
154400455348191297250786236278145877469128242088087797583947879668087797583947879668087797583947879668002358444118488
52601110587333244455424565064705151554245650647051512317821031085518857583303420156458819837724264286580545
10601443542604603704473
40.144.6.
152.116.132.128.144.140.131.136.136.128.133.138.129.134.19.141.4.
134.27.155.128.15.162.107.12.136.138.61.40.144.64.12.3.
135..57.
101.- 34.154.
3* i.
00900981706907523258716816160141463207748815730103862459442148001007107269377482023350
UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUGVML
901001007594918996889290979798989699918882863894698486629396100100949264758775689597958073
161
QUANT REPORT Page
Operator ID:Output File:Data File:Name: SSTD160M i sc
KU0786~P9712::UL>P9712::U5
Quant Rev: 7 Quant Time:In jected at:
Dilution Factor:S3 I UJ.O U
IFB/BNA 160 PPM
900831 14:16900825 14:35
1.00000
BTL* 2
ID File: IP0085::PFT i t l e : IFB/BNA, PP/BNA, TCLBN1i_ast Calibration: 900831 12:04
Compound R.T. Scan* Area Cone Un i ts
22)22)22)22)23)23)24)24)25)25)26)26)26)27)27)27)28)28)28)29)29)JO)30)31)31 )31)31)32)33)34)34)35)35)36)37)37)37)38)39)40)41)42)42)
2,4-Dimethylphenol2 ,4-Dimethylphenol2 ,4-Dime thy Ipheno 12 ,4-Dimethylphenolbis(2-Chloroethoxy)methanebis(2-Chloroethoxy)methane1,2,4-Trichlorobenzene1 ,2 ,4-Trichlorobenzene2.4-Dichlorophenol2,4-DichlorophenolBenzo ic ac idBenzoic acidBenzoic acidNaphtha leneNaphtha leneNaphtha lene4-Ch loroan i 1 ine4-Ch loroani 1 ine4-Ch loroani 1 ineHexachlorobutadleneHexachlorobutadlene2- Methyl naphtha lene2-Methylnaphthalenep-Chloro-m-cresolp-Ch loro-m-creso 1p-Ch loro-m-creso 1p-Ch 1 oro-m-creso 1
*dlO-Acenaphth«leneHexach lorocy«lopentad lene2 ,4 ,6-Tr ichioropheno 12 ,4 ,6-Tr ich loropheno 12,4,5-Trich loropheno 12 ,4,5-Trich lorophen* 12-Fluorobiphenyl (SURR)2-Ch loronaphtha lene2-Ch loronaphtha lene2-Ch loronaphtha lene2-Ni t n in i 1 ineDimethyl phthalateAcenaph thy lene2,6-Dinitrotoluene3— Nitroani 1 ine3-Ni t roan i 1 ine
14.5615.3915.5416.0715.6615.7616. 1516.8415.8415.9815.7216.0516.3915.9816.3116.3915.9816.3316.6216.4316.9418.4918.7518.2218.2918.8619.2221.7919.2219.5119.6319.5119.6319.7919.5119.6320.0020.5121.2621.3021.4721.6921.85
483524531557537542561595546553540556573553569573553570584575600676689663666694712838712726732726732740726732750775812814822833841
319950592699177302952278711895708308268048171582028422784037338636M26931
129551856889179
2386077606676451
3873579967745450
595129242424482476
25976642009342179442329342179442329311564204505913436
1191604Jo503913031251318512345911 '3914 ^
291798 J
.652 UG/ML10.31 UG/ML142.44 UG/ML
.617 UG/ML9.73 UG/ML
132.53 UG/ML140.56 UG/ML
.532 UG/ML11.55 UG/ML
139.50 UG/ML2.19 UG/ML43.63 UG/ML175.82 UG/ML
1.87 UG/ML89.87 UG/ML.395 UG/ML1.63 UG/ML42.45 UG/ML135.34 UG/ML2.12 UG/ML
127.25 UG/ML134.25 UG/ML
.734 UG/ML169.15 UG/ML
.689 UG/ML
.696 UG/ML
.704 UG/ML40.00 UG/ML232.85 UG/ML150.61 UG/ML151.14 UG/ML145.51 UG/ML146.03 UG/ML112.38 UG/ML4.84 UG/ML1.44 UG/ML
127.91 UG/ML145.03 UG/ML133.82 UG/ML103.30 UG/ML163.90 UG/ML, 2.06 UG/ML153.28 UGKML
82949469817995969796809392909488637361969766831001001001009497969797978854619786948278100100
162
QUANT REPORT Page
Operator ID: KU0786Output File: ~P9712:Data File: >P9712::U5Name: SSTD160Misc: IFB/BNA 160 PPM
ID File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1_aat Calibration: 900831 12:04
Compound
Quant Rev: 7 Quant Time:In lected at:
Dilution Factor:
900831 14:16900825 14:35
1.00000
BTL* 2
R.T. Scan* Area Cone Un i ts
42 )42)43)*4)44)45)45)46)47)47)47 )47)47)48)49)49)50)50)51)51)52)3)
54)55)55)56)57)58)59)60)60)61)61)62)62)62)63)63)64)64)64)65)66)
3-Ni t roan i 1 ine3-Ni t roan i 1 ineAcenaoht hene2 ,4-D in i t ropheno 12 ,4-DinitrophenolDibenzof uranD i benzof uran2 ,4-Din itrotoluene4-Ni t ropheno 14-Ni t ropheno 14-Ni t ropheno 14-Ni t ropheno 14-Ni t ropheno 14-Ni t roan i 1 ineDiethyl phthalateDiethyl phthalateF 1 uoreneF 1 uorene4-Ch lorophenyl phenyl ether4-Ch loropheny 1 phenyl ether2 ,4,6-Tr ibromophenol CSURR)1 , 2 -Di phenyl hydraz ine
•dlO-Phenanthrene4,6-Dinitro-o-cresol4,6-Dinitro-o-cresolN-Nitrosod i phenyl am me4-Bromophenyl phenyl etherHexach loroben««nePentachloroph«nolPhenanthren* ^PhenanthreneAnthraceneAnthracene fDi-n-butyl phthalateDi-n-butyl phthalateDi-n-butyl phthalateFluorant heneFluoranth* aPyrenePyrenePyrene•dl2-ChryseneBenz i d ine
22.22.21.22.22.22.22.22.23.23.23.23.24.23.22.23.23.24.23.23.24.24.26.23.23.24.25.25.26.26.26.26.26.28.28.28.30.30.30.30.31.34.26.
16449304144497673052598905896756523630593410428199050952095268526801688628982898618205
856870845850855870896881912923926941949941881925923964912926963951106593794694910001021104910701078107010781143117611851255128912551289132014781047
469224574
10894662368
1738541317390
30004789428725935472373724914302472949816341
10300981086449112715333351392119270812756263904503941
2397747017973325903947451885481326626122364213266261223642
53011235878
33551137133112417:113713.*1124120
239213129335222
2.4612.91133.707.24
531.44120.31.274
187.8916.34175.1944.4546.6656.64193.67.760
123.43144.291.5014.24137.26182.90170.7240.003.55
216.23114.94121.00126.56172.23125.27115.55124.99115.29.434
101.26.275
139.53137.93139.97138.37.294
_ 40.00V* 49.85
UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG'/ML
100100951001005952841001001001001009573969790998497929888739688979888879088978280979693934797100
163
QUANT REPORT
Ocerator ID: KU0786Output File: AP9712::ULOata File: >P9712::U5Name: SSTD160ttisc: IFB/BNA 160 PPM
ID Fi le: IP0085::PFT i t l e : IFB/BNA, PP/BNA, TCLBN1-ast Calibration: 900831 12:04
Compound
Quant Rev: 7 Quant Time:In iacted at:
Di lut ion Factor:
Page 4
900831 14:16900825 14:35
1.00000
BTL* 2
R.T. Scan* Area Cone Uni ts
66)67)68)69)69)69)70)70)70)71)72)72)72)73)74)74)75)75)75)76)76)76)77)77)77)78)79)BO)80)
Benz id meTerphenyl-D14 ( SURR )Butyl benzyl phthalateBe nzo (a) anthraceneBenzo(a)enthraceneBenzo (a ) anthraceneChryseneChryseneChrysene3 ,3 '-Dichlorobenzidinebis(2-Ethylhexyl) phthalatebis(2-Ethylhexyl ) phthalatebis(2-Ethylhexyl ) phthalate»d!2-PeryleneDi-n-octyl phthalateDi-n-octyl phthalateBenzo (b)f luorantheneBenzo (b ) f luorantheneBenzo (b ) f luorantheneBenzo (k ) f luorantheneBenzo (k)fluoranthenaBenzo (k ) f luoranthenaBenzo (a)pyreneBenzo (a )pyreneBenzo (a )pyreneIndeno(l,2,3-c,d )pyreneDibenzo(a,h ) anthraceneBenzo (gh i )peryl«neBenzo (gh i )peryl«n«
26.31.33.34.34.34.34.34.34.34.34.35.36.39.36.37.38.38.39.38.38.39.38.38.39.43.43.43.44.
4261347892997892998080292122211204120404120404120437473757
10651320140514761483148614761483I48614771477150115461694154615911636164016851636164016851636164016851898190318981957
502387907174705626288575259945061
6288575259945061
1776993974
5457195545797745545
676590460161367899354622460161367899354622460161367899354622312828225643312828270082
71.190.183.165.138.
1.179.150.
1.127.
1.170.
1.40.1.
182.192.153.148.191.153.147.214.171.165.138.136.158.136.
1052001312336123459724317300492348893456156353513248311352
UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/ML
100929510010010010010010084999357839998888790929193908992100100100100
Compound is ISTO
164
7BSEM1UOLATILE CONTINUING CALIBRATION CHECK
Lab Name:ETCNJ Contract:_________
Lab Code: Case No.:____ SAS No.:
Instrument ID:GC/MS P Calibration Date: 09/04X90
SDG No.:
Time: 1619
Lab F i l e ID: >P9B52
Min RRF50 for SPCC(#)
I n i t Calib. Dates(s): 08/25/90 OB/25/90
0. 050 Max SRSD for CCC(») 25. C
11 COMPOUND!„., = .,„ = = «« = __ = « = = _„ = = = = =1 PhenolIbis(2-Chloroethyl )e ther ____1 2-Ch loropheno 11 1 ,3-Dichlorobenzene1 1,4-Dichlorobenzene1 Benzu 1 a Icoho 11 1,2-Dichlorobenzene1 2-Methvlpheno 1Ibis(2-Chloroisopropyl ) e t her14-Methvlohenol
11
*
111*11111
IN-Nitroso-d i-n-propy lamine_#1 Hexach 1 oroe thane 11 Ni t robenzene1 I sophorone1 2-Ni t ropheno 112 r 4- Dime thy Ip he no 11 Benzo ic acidI b i s (2-Ch loroethoxy)methane_12 ,4-Dichlorophenol1 1 ,2 ,4-Tr ich 1 orobenzene1 Naph t ha lene14-Chloroani 1 me1 Hexachlorobutadiene1 4-Ch loro-3-methvlpheno 11 2- Me t hy 1 naphtha lene1 Hexach lorocyc lopentad lene _12 ,4,6-Trichlorophenol12,4,5-Trichlorophenol12-Chloronaphthalene1 2-Ni t roan i 1 meIDimethulphthalatelAcenaphthulene12.6-Dinitrotoluene1 3-Ni t roan i 1 ine1 Acenaph t hene12 r4-Dinitrophenol1 4-Ni t ropheno 11
11*111*111
1**
*
*
1
RRF IRRF50
1.3111.2051.3661.3661.3861. 0141.3651. 136.366
1. 178.880.557.333.618.197.324. 150.333.278.329.792.347.195.265.494.386.393.403
1. 186.314
1.3541.582.309.253
1. 125. 127. 087
1.6051 .4891.5421.5281.547.867
1.5281. 144.449
1.3591. 107.589.390.855.225.374. 186.410.293.358.982.390.204,262
.'431
.417
.4421.394.391
1.5171.992.339.262
1.294.112.081
1XD 1
22.5*23.6 112.9 111.9 111.6*14.5 112.0 1
.8 122.9 115.4125.8*5.8 117.2 138.4114. 1*15.4123.6123. 1 15.4*8.71
24. 1112.2 14.4*1.0*
11.6*6. 0*9.9117.5 124.7112. 1 126.0 19.713.5115. 0*11.9*6.6*
1
FORM UII SU -1 1/87 Rev.
165
7CSEMIVOLATILE CONTINUING CALIBRATION CHECK
Lab Name:ETCNJ Contract:__________
Lab Code: Case No.:_____ SAS No.:
Instrument ID:GC/MS P Calibration Date: 09/04X90
SDG No.:
Time: 1619
Lab File ID: >P9852
Min RRF50 for SPCC(#)
Init Calib. Dates(s): 08/25/90 08/25/90
0.050 Max %RSD for CCC(») -25.0
11 COMPOUND!«...«.«...«.....«........«.1 Dibenzof uran12 ,4-Dinitrotoluene1 Diethvlphtha late14-Ch lorophenyl-phenylether_1 F 1 uo rene14-Nitroani 1 me!4,6-Dinitro-2-methylphenol_IN-Nitrosodiphenylamine (1)_*1 4-Bromophenyl -pheny let her __IHexachlorobenzene1 Pen t ach 1 oropheno 1 *1 Phenanthrene1 An t hraceneIDi-n-butulphthalate1 Fluoran t hene «1 PvreneIButvlbenz«jlphthalate13 ,3 '-Dichlorobenzidine1 Benzo (a )anthracene1 ChrvseneIbis(2-Ethylhexyl)phthalate_1 Di-n-octulphtha late «IBenzoCbJfluorantheneIBenzo(k)fluoranthene1 Benzo (a )p<jrene *1 Indeno(l,2,3-cd)pyrene1 Di benz ( a .h)anthraceneIBenzo(g,h , i )perylene
INitrobenzene-d512-Fluorobiphenyl1 Terphenul-dl4IPhenol-d512-Fluoropheno 11 2 ,4 ,6-Tr ibromophenol1
RRF
1.425.410
1.205.524
1. 065.229.139.511.219.267
* .118.933.921
1.093.792.777.802.288
1. 121.972.953
1.7281.3231. 162
* 1.049.918.657.787
.3391.2381.3401.4251. 182.173
RRF50
1.713.392
1.295.586
1.164.218.156.624.268.328. 145
1.0991.1401.325.861.850.773.252
1. 1691.040.867
1.7581.2601.3821.104.914.667.791
.3961.5401.4881.6711.283.187
XD
20.24.37.5
11.89.44.712.422.1«22.222.823. 1*17.723.721.28.8*9.33.612.44.37.09. 01.7*4.818.95.3*.5
1.5.5
16.824.411.117.38.67.8
(1) Cannot be separated from Dipheny1amine
FORM UII SU -2 1/87 Rev.
166
TOTRL ION CHROMflTOCRPMFile >P9B52 35.8-588.8 MU . SST558 50 PPH
1288 1688 2888
16 26 24 26 32 36 40 44e1 '' '12
Data File: >P9852::U2Name: SSTD50Misc: IFB/BNA 50 PPM
Id File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900831 14:26
Operator ID: KU0786Quant Time: 900904 17:06Injected at: 900904 16:19
Quant Output File: ~P9852::UL
BTL* 2
167
QUANT REPORT Page
Operator ID: KU0786Output File: "P9B52 : : Ul_Data File: >P9852::U2Name: SSTD50Misc: IFB/BNA 50 PPM
ID File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900831 14:26
Compound
Quant Rev: 7 Quant TimeIn jected at
Di lut ion Factor;
900904 17:06900904 16:19
1 .00000
BTL* 2
R.T. Scan* Area Cone Un i ts
1)2)2)3)4)5)6)7)8)8)8)9)9)9)10)10)10)11)12)12)13)14)14)15)15)16)16)17)18)19)19)19)20)20)21)21)22)23)24)25)26)27)27)
*d4- 1 , 4- Dich lorobenzeneN-Nitrosod i me thy lamineN-Nitrosodimethylamine2-Fluorophenol • (SURR)bis(2-Ch loroethyl ) etherPhenol -D5 (SURR)Pheno 12-Ch lorophenol1, 3-D ich lorobenzene1,3-Dich lorobenzene1,3-Dich lorobenzene1 ,4- Dich lorobenzene1 ,4- Dich lorobenzene1,4- Dich lorobenzene1 ,2-Dich lorobenzene1 ,2-Dich lorobenzene1,2-Dich lorobenzeneBenzyl alcoholN-Ni trosodi-n-propylamineN-Nitrosodi-n-propylamineHexach loroe thane2-Methylpheno 12-Methylpheno 14-Methy Ipheno 14-Methylpheno 1bis (2-Ch loroisopropyl )etherbis(2-Chloro i sop ropy 1 )ether
•de-NaphthaleneNitrobenzene-D5 (SURR)Ni t robenzeneNit robenzeneNit robenzeneI sophoroneIsophorone2-Ni t ropheno 12-Ni t ropheno 12 ,4- Dime thy Ipheno 1bis (2-Ch loroethoxy) me thane1,2, 4- Tr ich lorobenzene2,4-DichlorophenolBenzo ic ac idNaphtha leneNaphtha lene
11.4.4.6.11.11.11.11.11.12.12.11.12.12.11.12.12.12.13.13.13.13.13.13.13.13.13.15.13.13.13.14.14.15.14.14.15.15.15.15.15.15.15.
99899563463638508905588905588905586052744707520752054784740780555555557610357555715590
3813235216355350351357376384410376384410376384410411456467454434456434456433454570467434470507507556507517534546566556564556573
159147180161
51032553182962243325113193263068193040673078303040403040673078303040403040673078303040401725062202904601611723722764027041222764027041269399367266012062973561619362930921784464260252421144416916528123530842426902722039013974C10604 .73616F
40541
50565556545454545354535657564467145759715161562340522852367.3545858525048.
54
.00
.71
.55
.42
.97
.33
.28
.94
.28
.95
.27
.79
.46
.79
.43
.13
.42
.43
.85
.17
.96
.92
.17
.74
.46
.58
.24
.00
.28
.77
. 08
.17
.18548.66. 15.28.36.02. 09.09785.64
UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/ML
901001006687928195908790989796989796797738956787579810010093896382569582598093869695668691
168
QUANT REPORT Page 2
Operator ID: KV0786Output File:Data File:Name: SSTD50Misc: IFB/BNA 50 PPM
Quant Rev: 7
>P9852::U2
Quant TimeIn jected at:
Dilut ion Factor:
900904 17:06900904 16:19
1.00000
BTL# 2
ID File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900831 14:26
Compound R.T. Scan* Area Cone Units
28)28)28)29)29)30)30)31)32)33)34)34)35)35)36)37)37)37)38)39)40)41)42)42)43)44)45)45)46)47)47)47)47)47)48)49)50)50)51)51)52)53)54)
4-Ch loroan i 1 ine4-Ch loroani 1 ine4-Chloroani 1 ineHexach lorobutadieneHexachlorobutadiene2-Methylnaphtha lene2-Methylnaphtha lenep-Chloro-m-creso 1
*dlO-AcenaphthaleneHexachlorocyclopentadiene2 ,4,6-Tr ich loropheno 12,4,6-Trichlorophenol2, 4, 5-Tr ich loropheno 12, 4, 5-Tr ich loropheno 12-Fluorobiphenyl (SURR)2-Ch loronaphtha lene2- Ch lor on aphtha lene2- Ch loronaphtha lene2-Ni t roan i 1 ineDimethyl phthalateAce naph thy lene2,6-Dinitrotoluene3-Ni t roan i 1 ine3-Ni t roan i 1 meAcenaphthene2 ,4-Din i t ropheno 1D ibenzof uranDibenzof uran2 ,4-Dinitrotoluene4-Ni t ropheno 14-Ni t ropheno 14-Ni t ropheno 14-Ni t ropheno 14-Ni t ropheno 14-Ni t roan i 1 ineDiethyl phthalateF luoreneF 1 uorene4-Ch lorophenyl phenyl ether4-Ch loropheny 1 phenyl ether2 ,4,6-Tr ibromopheno 1 (SURR)1,2-Diphenylhydrazine
•dlO-Phenanthrene
15151616161818172118191919191919191920202020212121212122222223232323232323232223232325
.55
.90
.20
.04
.55
.07
.36
.85
.37
.81
. 09
.19
.09
.19
.36
.09
.19
.56
.05
.82
.86
.99
.35
.98
.47
.68
.98
.86
.19
.86
.06
.14
.31
.57
.31
.10
.06
.88
.86
. 14
.88
.63
.97
5565735885806056806946698427167307357307357437307357537778158178238418728478578729158829159259299379509379279259659159299659531068
342998428292854
20711530904011482077
196858250822135127130614138656130614138656482876141274682
436913122684475524624644106249820977907
405706350975370622840
122997226225349113045098706168457405968365053339215733.18379056517J1441429"*303873
.66619.1256.88.652
48.1658.40.302
53.3740.0049. 1949.0052.0246.9949.8855.601.75.581
54.2053.9258.4254.4954.8949.324.7556.7447.5754.98.291
51.594.4549.8422.2210.0213.8848.2458.8252.49.4884.5953.6249.6956.7740. 00
1
UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/ML69
61696095988490100939598969796995658928698987710010098100923285100100100100100959495908983948698
Operator ID: KU0786Output File: "SP9852::U|_Data File: >P9852:: U2Name: SSTD50Miac: IFB/BNA 50 PPM
ID File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900831 14:26
QUANT REPORT
Quant Rev: 7 Quant Time:In jected at :
Dilut ion Factor:
Page 3
900904 17:06900904 16:19
1.00000
BTL* 2
Compound55)56)56)57)58)59)60)60)61)61)62)63)63)64)64)65)66)66)67)68)69)69)70)70)71)72)73)74)75)75)75)76)76)76)77)77)77)78)79)80)
4,6-Dinitro-o-cresolN-NitrosodiphenylamineN-Ni trosod iphenylamine4-Bromopheny1 pnenyl etherHexachlorobenzenePentachloropheno1PhenanthrenePhenanthreneAn thraceneAnthraceneDi-n-butyl phthalateFluorantheneFluoranthenePyrenePyrene•d!2-ChryseneBenzidineBenz id ineTerphenyl-D14 (SURR)Butyl benzyl phthalateBenzo(a)anthraceneBenzo(a)anthraceneChryseneChrysene3,3'-Dichlorobenz idinebis(2-EthyIhexyl)phthalate
*d!2-PeryleneDi-n-octyl phthalateBenzoCb)fluorantheneBenzo(b)fluorantheneBenzo(b)fluorantheneBenzo(k)fluorantheneBenzo(k)fluorantheneBenzo(k)fluorantheneBenzo(a )pyreneBenzo(a)pyreneBenzo(a)pyreneIndeno(l,2,3-c,d)pyreneDibenzo(a,h)anthraceneBenzoCghi)perylene
R.T. Scan* Area Cone Units q
* Compound is ISTD
23.47 94523.14 92923.57 95024.65 100325.06 102325.65 105226.06 107226.20 107926.06 107226.20 107928.25 118029.82 125730.51 129129.82 125730.51 129134.37 1481
•X25.63 105125.97 1068
1 31.16 132332.91 140934.31 147834.46 148534.31 147834.46 148534.35 148034.88 150638.67 169236.69 159537.55 163737.61 164038.48 168337.55 163737.61 164038.48 168337.55 163737.61 164038.48 1683-42.55 188342.66 1888«3.65 1937
5940819775
236918•1018261246836103641734643285041734643285050345932717332285932717332285912211793773905222718111793117842815872017842815872038455132351651071430951025121125048987510251211250489875102512112504898757439354260"64370 .
54.54 UG/ML4.47 UG/ML53.52 UG/ML54.84 UG/ML55.78 UG/ML58.49 UG/ML57.57 UG/ML59.71 UG/ML55.53 UG/ML57.59 UG/ML63.20 UG/ML56.37 UG/ML55.62 UG/ML58.49 UG/ML57.71 UG/ML40.00 UG/ML52.06 UG/ML216.80 UG/ML57.20 UG/ML53.91 UG/ML53.66 UG/ML47.74 UG/ML58.56 UG/ML52 . 09 UG/ML38.12 UG/ML52.26 UG/ML40.00 UG/ML44.03 UG/ML49.71 UG/ML54.55 UG/ML43.58 UG/ML46.08 UG/ML50.57 UG/ML40.40 UG/ML57.44 UG/ML63.04 UG/ML50.36 UG/ML52.67 UG/ML51.84 UG/ML54.34 UG/ML
68819988979697969695959797989997100100959810010010010092918498918889949192929090100100100
170
7BSEMI VOLATILE CONTINUING CALIBRATION CHECK
Lab NameiETCNJ Contract:__________
Lab Code: Case No.:____ SAS No.: SDG No.:
Instrument ID:GC/MS P Calibration Date: 09/05/90 , Time: 1630
Lab F i l e ID: >P9872 I n i t Calib. Dates(s): 08/25/90 08/25/90
Mm RRF50 for SPCC(#) 0. 050 Max HRSD for CCCC*) 25. 0
COMPOUND
Pheno 1bis(2-Chloroethyl )ether ___2-Ch 1 oropheno 11 T 3-D i ch lorobenzene1 ,4-Dich lorobenzeneBenzvl alcohollT2-Dichlorobenzene2-Methvlpheno 1bis(2-Chloroisopropyl )et her4-Me t hvl pheno 1N-Nitroso-di-n-propylamine_Hexach loroe thaneNit robenzeneIsophor one2-Ni t ropheno 12 . 4-Dimethulpheno 1Benzoic acidb is (2-Ch loroe t hoxy ) me t hane_2 r 4-Dichlo ropheno 11,2,4-Trich lorobenzene ____Naph t ha 1 ene4-Chloroani 1 meHexach lorobutad iene4-Chloro-3- me thy 1 phenol2- he thyl naphtha leneHexach lorocyc lopentad iene _2 ,4,6-Trichlorophenol2 ,4,5-Trichlorophenol2-Ch loronaphtha lene2-N itroani 1 i neDimethvjlphtha lateAcenaph thy 1 ene2 .6-Din 1 1 roto luene3-Ni t roan i 1 i neAcenaph thene2 .4-Dinitrophenol4-Ni t ropheno 1
11
«111*
11111*111*111*
111**1**1I11111*##1
RRF
1.3111.2051.3661.3661.3861. 0141.3651. 136.366
1. 178.880.557.333.618. 197.324. 150.333.278.329.792.347.195.265.494.386.393.403
1.186.314
1.3541.582.309.253
1. 125. 127. 087
RRF50
1.6281.4651.5521.5161.5311. 1081.5031. 146.339
1.4471. 054.594.403.889.233.387. 187.414.323.365
1.030.454.208.321.574.426.471.471
1.346.452
1.5102.026.351.293
1.301. 132. 088
1\D 1
= ««=,,= |24.2*21.6 113.6 111.0110.4*9.31
10.11.9 1
7.4122.9 119.7*6.5 1
21.2143.9 118.3*19.5 124.4124.3 116.3*10.7130.1130.816.5*21.4*16.1110.4*19.9*17.1 113.5 144. 1 111.5128.1 113.7116. 0 115.6*3.6#1.6*
1
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TOTflL ION CHROHRTOSRPMF i l e >P987235.6-580.8 a»u. SSTIBe
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Data File: >P9872::U3Name: SSTD50Misc: IFB/BNA 50 PPM
Id File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900904 17:29
Operator ID: KU0786Quant Time: 900905 19:17Injected at: 900905 18:30
Quant Output F i l e : "-P9872: : UL
BTL# 2
173
QUANT REPORT Page
Operator ID:Output File:Data File:Name: SSTD50disc: IFB/BNA 50 PPM
KU0786"•P9872: :UL>P9B72::U3
Quant 7 Quant Ti me:In jec ted at:
Dilution Factor:
900905 19:17900905 18:30
1.00000
BTL* 2
ID File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900904 17:29
Compound R.T. Scan* Area Cone Un i ts
1)2)2)3)4)5)6)7)8)8)8)9)9 )9)10)10)10)11)12)12)13)14)14)15)15)16)16)17)18)19)19)19)20)21)21)22)23)24)25)26)26)27)27)
*d4-l, 4- Dich lorobenzeneN-Ni t rosod imethylamineN-Nitrosodimethylamine2-Fluorophenol (SURR)b is (2-Ch loroe thy 1 ) etherPhenol-05 (SURR)Pheno 12-Ch 1 o ropheno 11 ,3-Dich lorobenzene1,3-Dichlorobenzene1 ,3-Dich lo robenzene1,4-Dichlorobenzene1,4-Dichlorobenzene1,4-Dichlorobenzene1 ,2-Dich lo robenzene1,2-Dichlorobenzene1 ,2-Dich lorobenzeneBenzy 1 a 1 coho 1N-Ni t rosod i-n-propylamineN-Nitrosodi-n-propylamineHexach loroe thane2-Methylphenol2-Me thy Ipheno 14-Methylphenol4-Methylpheno 1bis(2-Chloroisopropyl )etherbis(2-Chloroisopropyl )ether
*d8-Naphtha leneNitrobenzene-05 (SURR)Ni t robenzeneNi t robenzeneN i t robenzeneI sopho rone2-Ni t ropheno 12-Ni t ropheno 12 ,4-Dimethylpheno 1b is (2-Ch loroethoxy)methane1,2, 4- Trich lorobenzene2 ,4-Dich lo ropheno 1Benzo i c acidBenzo i c acidNaph t ha 1 eneNaphtha lene
11448111111111112121112121112121213131313131313131315131313141414141515151515151515
.96
.86
.90
.58
.41
.30
.34
.47
.83
.00
.53
.83
. 00
.53
.83
. 00
.53
.55
.46
.69
.42
. 01
.48
.01
.48
. 01
.42
.78
.69
. 01
.75
.52
.52
.52
.70
. 05
.29
.70
.50
.46
.72
.50
..a4
3813234
215354349351357375383409375383409375383409410455466453433456433456433453569466433469507507507516533545565555554566555?1
1584852003423687
263718290198335063322487M30739430038530320829767430038530320829767430038530320829767421940620874746968117586227062286693227062286693670753701959481930453516453829996918414
6610091199517355228806930790427102124050850491139189;11789^
7-bSttVo j'
40551
51495050504950494649484950496347105050634253372040512851351351515050551850.
V2
. 00
.83
. 03
.86
. 19
.60
.71
.30
.60
.07
. 15
.99
.45
.55
.61
. 07
. 16
.86
.58
.71
.36
.08
.23
. 16
.23
.67
.79
. 00
.76
.37
.72
. 18
.98
.58
.85
.77
.45
.91
. 15
.26
.34807!.42
UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/ML
911001008286918288886589979595969596857838957086609510010094916381639755799486959892898991
174
QUANT REPORT Page
Operator ID: KU0786Output File: "P9672::ULData File: >P9872::U3Name: SSTD50Misc: IFB/BNA 50 PPM
ID File: IP0085::PFTi t l e : IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900904 17:29
Compound
Quant Rev: 7 Quant T i meIn jected at:
Dilut ion Factor
900905 19:17900905 16:30
1.00000
BTL* 2
R.T. Scan* Area Cone Uni ts
28)28)28)29)29)30)30)31)31)32)33)34)34)35)35)36)37)37)37)38)39)40)41)42)42)43)44)45)46)47)47)47)47)47)48)49)50)50)51)51)52)53)54)
4-Chloroani 1 ine4-Ch loroanilme4-Chloroani 1 meHexach lorobutad leneHexachlorobutadiene2-Methylnaphthalene2-Methylnaphtha lenep-Chloro-m-cresolp-Chloro-m-creso 1
*dlO-AcenaphthaleneHexachlorocyclopentadiene2 ,4 ,6-Tr ich loropheno 12,4,6-Trichlorophenol2,4,5-Trichlorophenol2,4,5-Trichlorophenol2-Fluorob ipheny 1 (SURR)2-Chloronaphthalene2-Chloronaphthalene2-Ch loronaphtha lene2-N 1 1 roan i 1 i neDimethyl phthalateAcenaphthylene2,6-Dmitrotoluene3-Ni t roan i 1 me3-Ni t roan i 1 meAcenaph t hene2,4-DinitrophenolDibenzof uran2,4-Dmitrotoluene4-N i t ropheno 14-N 1 1 ropheno 14-Ni t ropheno 14-Ni t ropheno 14-N i t ropheno 14-Nitroani 1 ineDie thy 1 phtha lateF 1 uo r eneF 1 uorene4-Ch 1 oropheny 1 phenyl ether4-Ch loropheny 1 phenyl ether2 ,4,6-Tr ibromopheno 1 (SURR)1 ,2-Diphenylhydraz me
*dlO-Phenanthrene
15151615161818171721181919191919191919202020202121212121222223232323232323232223232325
.50
.84
. 15
.99
.50
.02
.33
.80
.86
.32
.77
. 04
. 16
. 04
.16
.30
. 04
. 16
.51
. 00
.79
.83
.95
.32
.93
.44
.65
.93
. 14
.83
.01
. 11
.28
.52
.28
.05
.01
.85
.83
.09
.83
.60
.92
5555725875796046796946686718417167297357297357427297357527768158178238418718478578718819159249299379499379269249659159289649531067
3670974673377612039
154463426655
2203238754
2056294005156687173165173271173165173271532678183346054
4947261662265547687446881289931078459948
47807348406665199151093264832318136996098834579897460277460648424719044
22565876744
553160 ,,355075-'
1658.
5053.
61.
404956565353471.
4857495051565
50585252454231014494853.
452555340
633.82.29673.99.75278.29528.00.46.55.59.27.31. 06.79591.30.80.76.85.79.03.17.26.83.83.40.46.38.05.26. 04.78.36.83496.42.37.94.45. 00
UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/ML
68656389988177
10010096939896989697555992849998801001009610091831001001001001009293968595819875•99
175
QUANT REPORTOperator ID:Output File:Data File:Name: SSTD50Misc: IFB/BNA 50 PPM
KU0786~P9872::UL>P9872::U3
Quant Rev: 7 Quant TimeInjected at:
D i l u t i o n Factor;
Page 3
900905 19:17900905 18:30
1. 00000
ID File: IP0085::PFT i t l e : IFB/BNA, PP/BNA, TCLBN1
Calibration: 900904 17:29
Compound
Last
R.T. Scan*55) 4 ,6-D in i t ro-o-creso 156) N-N i t rosod ipheny 1 am me56) N-N i t rosod i pheny lam i ne57) 4-Bromopheny 1 phenyl ether58) Hexach lo robenzene59) Pen t ach 1 oropheno 160) Phenanthrene60) Phenanthrene61 ) Anthracene61) Anthracene62) Di-n-butyl phthalate63) Fluoranthene63) Fluoranthene64 ) Pyrene64) Pyrene65) *d!2-Chrysene66 ) Benz id ine66 ) Benz id ine67) Terphenyl-D14 (SURR)68) Butyl benzyl phthalate69) Benzo (a )an t hracene69) Benzo (a )an t h racene70) Chrysene70) Chrysene71) 3 ,3 ' -D ich 1 orobenz id ine72) b is (2-Ethy Ihexyl )phtha late73) «d!2-Perylene74) Di-n-octyl phthalate75) Benzo (b ) f luo ran thene75) Benzo (b ) f 1 uoran t hene75) Benzo (b ) f 1 uo ran t hene76) Benzo (k ) f 1 uo ran thene76) Benzo (k ) f 1 uoran thene76) Benzo C k ) f 1 uoran thene77) Benzo (a )pyrene77) Benzo C a )pyrene77) Benzo ( a )py r ene78) 1 ndeno ( 1 ,2 , 3-c , d )pyrene79) Dibenzo ( a , h )an t hracene79) D ibenzo ( a ,h )an t h racene80) Benzo ( gh i ) pe ry 1 ene
, , , , , _j>_. a i t v-
23.44 94523.11 92923.52 94924.60 100225.01 102225.60 105126.00 107126.15 107826.00 107126.15 107828.18 117829.75 125530.44 128929.75 125530.44 128934.30 147925.58 105025.92 106731.09 132132.84 140734.24 147634.38 148334.24 147634.38 148334.28 147834.81 150438.58 168936.64 159437.46 163437.54 163838.39 168037.46 163437.54 163838.39 168037.46 163437.54 163838.39 168042.40 187742.50 188243.48 193043.50 1931
Hrea
663902321028179812535514813464178M485303505851485303505B514478673255963263203255963263201177231081945552211403107498173019155125173019155125476441312187323116431713260297797998691326029779799869132602977979986983944606352057:71115;,
Cone Lln i t ;
47.82 UG/ML4.19 UG/ML50.90 UG/ML52.68 UG/ML50.84 UG/ML49.93 UG/ML49.76 UG/ML51.86 UG/ML47.98 UG/ML50.01 UG/ML38. 07 UG/ML42.58 UG/ML42.68 UG/ML43. 15 UG/ML43.25 UG/ML40.00 UG/ML59.84 UG/ML251.96 UG/ML48.26 UG/ML47.28 UG/ML50.29 UG/ML45. 09 UG/ML56.54 UG/ML50.69 UG/ML64.26 UG/ML51.42 UG/ML40.00 UG/ML51.05 UG/ML57.50 UG/ML42.41 UG/ML43.31 UG/ML52.39 UG/ML38.64 UG/ML39.46 UG/ML65.59 UG/ML48.37 UG/ML49.40 UG/ML50.16 UG/ML49.68 UG/ML1.69 UG/ML
49.11 UG/ML
s q
7576989097Q j£7 O
9797O -ty O
96o /7t>Q 7 6o .7*6O P7 t?
99O £.7 O
100100959210010010010085878497918989949292939091100100100100
176
BBSEMIUOLATILE INTERNAL STANDARD AREA SUMMARY
Lab Name: ETCNJ Contract: __________
Lab Code: Case No.: ____ SAS No.: SDG No.:
Lab File ID (Standard): >P9852 Data Analyzed: 09/04/90
Instrument ID: GC/MS P Time Analyzed: 1619
0102030405060708091011121314151617IB1920211221
12 HOUR STD
UPPER LIMIT
LOWER LIMIT
EPA SAMPLENO.
SBLK01A4376A4377A4377MSf\ s, -T -p-purarN
ISKDCB)AREA *
159147
316294
7957?
1846631677181752591696461 JO "p.<O
RT
11.99
11.9711.9812. 0012. 00•f^^i y j
IS2CNPT)AREA #
601208
1202416
300604
706682596875628868609666d1" 1 Q QfT ~^
RT
15.84
15.8215.8115.8215.631 c riii
I S3 CANT)AREA *
250822
501644
125411
354881268053281694275078AC f /, r" i
RT
21.37
21.3821.3621.3621.37
151 (DCB) • l,4-Dichlorobenzene-d4152 (NPT) - Naphthalene-d8153 (ANT) - Acenaphthene-dlO
UPPER LIMIT - + 10OXof internal standard area.LOUER LIMIT - - 50*of internal standard area.
page
Column used to flag internal standard area values with an asterisk.
' of /
FORM UII I SU -1 1/87 Rev.
177
8CSEMIUOLATILE INTERNAL STANDARD AREA SUMMARY
Lab Name: ETCNJ Contract: ___________
Lab Code: Case No.: ____ SAS No.: SDE No.:
Lab File ID (Standard): >P9852 Data Analyzed: 09/04/90
Instrument ID: GC/MS P Time Analyzed: 1619
01020304050607080910111213141516171819202122
12 HOUR STD
UPPER LIMIT
LOWER LIMIT
EPA SAMPLENO.
SBLK01A4376A4377A4377MS043771 ISO
IS4CPHN)AREA #
303873
607746
151936
5.93908350361369837343488TT O 1-1 ~r n •>
RT
25.97
25.9825.9625.9825.99O C AO
IS5CCRY)AREA #
122117
244234
61059
346705*182673182568172147O *"! A i A 3 1
RT
34.37
34.3934.3634.3634.371/i T 4
1 56 (PRY)AREA #
65107
130214
32554
268737*125295131870*119193i r"iX~ ** ••— ™* —
RT
38.67
38.6938.6838.6838.6738.68'
154 (PHN) - Phenanthrene-dlO155 (CRY) - Naphthalene-d8156 (PRY) - Perylene-dl2
UPPER LIMIT - + 100*of internal standard area.LOWER LIMIT - - 50*of internal standard area.
# Column used to flag internal standard area values with an asterisk,
page ' of _j__
FORM UII I SU -2 1/87 Rev.
178
BBSEMIUOLATILE INTERNAL STANDARD AREA SUMMARY
Lab Name: ETCNJ Contract: __________
Lab Code: Case No.: ____ SAS No.: SDG No.:
Lab File ID (Standard): >P9872 Data Analyzed: 09/05/90
Instrument ID: GC/MS P Time Analyzed: 1830
01020304050607080910111213141516171819202122
12 HOUR STD
UPPER LIMIT
LOWER LIMIT
EPA SAMPLENO.
SBLK01A4377A4377MSD
ISKDCB)AREA #
158485
316970
79243
182387214816194160
RT
11.96
..»..
11.9311.9211.94
IS2(NPT)AREA #
594819
1189638
297409
692666771741745793
RT
15.78
15.7615.7715.77
I S3 (ANT)AREA #
294005
588010
147002
363277375518390503
RT
21.32
21.3221.3021.31
151 (DCB) - l,4-Dichlorobenzene-d4152 (NPT) - Naphthalene-d8153 (ANT) - Acenaphthene-dlO
UPPER LIMIT - + 100\of internal standard area.LOWER LIMIT - - 5OXof internal standard area.
# Column used to flag internal standard area values with an asterisk.
Pa9e / of /
FORM U I I I SU -1 ^ 1/87 Rev.
179
8CSEMIUOLATILE INTERNAL STANDARD AREA SUMMARY
Lab Name: ETCNJ Contract: __________
Lab Code: Case No.: ____ SAS No.: SDG No.:
Lab File ID (Standard): >P9872 Data Analyzed: 09/05/90
Instrument ID: GC/MS P Time Analyzed: 1830
01020304050607080910111213141516171819202122
12 HOUR STD
UPPER LIMIT
LOWER LIMIT
EPA SAMPLENO.
SBLK01A4377A4377MSD
I 54 (PHN)AREA #
355075
710150
177538
S'tea fO584262562635
RT
25.92
O&-VLJ25.9125.92
IS5(CRY)AREA #
117723
235446
58861
3?)SJf *315171*218938
RT
34.30
3</.3/
34.2934.28
1 56 (PRY)AREA #
73231
146462
36615
^^/fc*230034*138885
RT
38.58
3S.&P38.593 8 . 5 8
154 (PHN) - Phenanthrene-dlO155 (CRY) - Naphthalene-d8156 (PRY) - Perylene-dl2
UPPER LIMIT - + 100*of internal standard area.LOWER LIMIT - - 50*of internal standard area
page
Column used to flag internal standard area values with an asterisk
' of /
FORM UII I SU -2 1/87
180
ETC
RAW QC DATA.
S Data Fil«: >P9711::U5
ii»c: OFTPPOperator: KU0786 D«t«/Tim«: 8x25/90 14:18
BTL* 1
Fil« >P9711Bpk Ob 1M.
110-
ie»
' 99-
99.
78-
6fr
5»-
46-
3»
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51/
1 ,
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69
NRtl
187\
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141 ^.(^ j^Lise a
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44S\
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T T r TI3*t 361 4«*
•ii«
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9«
•••
•79
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182
IS Data Film: >P9711::U5
•lama: . . . . . . . . . . . . . . . . . . . . Operator: KU0786 DataxTim*: 8x25x90 14:18i i»cs DFTPP BTL* 1
•P9711544 NRM
DFTPP
- i l a : >P9711 Scan #:
Int. mxz
544 Ratn. t ima: 6.65
Int . mXz Int . Int . mXz Int.
37. .00?8.003 9 . 0 0•*4. 005 0 . 0 051.005 2 . 0 05 5 . 0 055 .905 7 . 0 057.9061 .006 2 . 0 06 3 . 0 06 4 . 0 064.9067.0068.90-o. oo73. 1074.0075 .0076. 1077 . 0 078.007 9 . 0 09 0 . 0 080.9082. 00P ' . O O85. 0086. 0036.9087.9039. 0093.9091.909 3 . 0 093.8595 e«>97.0597.9598.8599.95
.00.95102.95
.231
.7463.595
.92412.52045. 052
2.144.323
1.4933.509
.140.504.679
1.647.244.777.108
51.855.295.541
4.2046.9892.287
42.3033.1003.2662.4923.283
.786
.798
.598
.873
.349
.155
.140
.850
.8374.761
.347
.161
.1633.6652.737
.2941.647
.671
103.85104.95106.95107.95109.95110.95111.95115.15116.95117.95121.95122.95123.85124.95126.95127.95128.95129.95130.95131.95132.75133.85134.95135.95137.05137.85138.85140.05140.95141.9*142. tf143. Mr-145. 9mA14*.f*v147. 99148.95149.85151.05151.95152.95153.85154.90155.90156.90157.80158.90
.9991.080
12.4691.794
28.8853.895
.542
.0728.785
.733
.8271.345
.634
.62844.811
3.44620.327
1.690.274.119.099.597
1.510.568.622.179.125.234
2.259.824.529.138
. .4431.2122.S42
.506
.157
.299
.205
.739
.6191.2571.479
.378
.359
.285
159.90160.90161.90163.90164.80166.00166.90168.00168.90169.90170.90171.90172.90173.90175.00175.90176.90178.00178.90179.90180.90182.00183.00184.00185.00185.90186.90188.10188.90189.90190.90192.00193.00194.00195.90197.90198.90199.90201.40203.00204.00204.90206.00207.00207.90
1
31
1
22
1102
1
2100
6
24
192
.722
.067
.307
.146
.862
.606
.800
.669
.273
.166
.192
.345
.449
.873
.507
.508
.909
.303
.986
.014
.994
.193
.161
.295
.475
.849
.960
.311
.652
."99
.304
.894
.002
.192
.880
.000
.914
.444
.627
.630
.760
.543
.848
.590
.605
208.90211.60214.90215.90216.85217.85220.85222.85223.95224.95226.95227. 85228.85230.95233.05233.95234.95235.85236.95238.85240.85241.95242.95243.95244.95245.95246.85248 . 85251.95252.95254.95255.95256.95257.95258.95264.95265.95271.95272.95•i ) 952x4.95275 . 95276.95277.75282.90
5
61
1023
811
415
2
13
1921
.172
.862
.208
.419
.033
.605
.023
.045
.364
.370
.886
.640
.900
.389
.073
.227
.297
.201
.316
.145
.244
.525
.762
.129
.198
.339
.299
.325
.128
.205
.478
.898
.413
.263
.315
.671
.114
.097
.169
.450
.145
.619
.263
.169
.137
284.00254.90293.00295.80296.90298.00302.90314.00314.90315.90320 .90321.80322.90324 .00326.90327.90331.80333.00333.90335.00340.95345.95351.95352.95353.95364.85365.85370.95371.95372.75382.95389.95390.95401.95402.90403.80420.90422.00422.90423.90438.70440.90441.90442.90443.90
.102
.253
.3163.975
.609
.089
.568
.159
.486
.324
. 144
.1291.723
.317
.252
.167
. 101
. 169
.860
.280
.163
.302
.409
.338
.5451.551
.230
.138
.869
.193
.240
.125
.107
.372
.418
.129
.372
.5473.756
.651
.06510.22366.24512.650
1.219
183
1S Data Pilau >P9711::U5
>lam«: .................... Operator: KU0786ls»c: DFTPP
D«t»XTin»: 8x25x90 14:18BTL* 1
686666-
866886-saaeea-488666-
448888-
368688-
32B686-386868-
348888-
286888-168888-
120888-
86888-
48888-
a-
9711 30.6-468.8 MU. TJCifa eaa afa 4fa saa
4.4 4.8 9.8 S.t 6.6 6.4 '
«66 766 6f6
•
6.8 7.Z 7.6 8.1
•iaa
•99
•99
•79
•69
•56
•48
38
-ee
la
•91
184
MS Data File: >P9851::U2
Name: .................... Operator: KU0786disc: DFTPP
Date/Time: 9/04/90 16:04BTL* 1
T i l * >P9851Bpk fib 60088.
65000-
60080-
65008-
50000-
45000-
40080-
35000-
30000-
25000-
28000-
15000-
10000-
6000-
cu.
X51
1 L
69S
198
127
160
\ lJ100
\
186\
141 1h i t i 1 Aj l
255\
ii 1
DFTPP Sc»n 5016.45 B in .
442X
27S
i j160 200 260
f
*? /3 3« 403L I / » x / J
•110
•100
•90
*0
•70
<0
•60
•48
-30
•20
•10
A300 360 400
185
MS Data File: >P9851::U2
Name: .................... Operator: KY0786Misc: DFTPP
Date/Time: 9/04/90 16:04BTL* 1
>P9851501 NRM
DFTPP
"ilc: >
m/z
37.0037.9039.0040.0040.9043.0043.8048.9050.0051.0052. 0055.1055.9057. 0057.9060.9061.9063. 0065. 0067. 0068.9070. 0073. 0074.0074.9076.0077.0078.0079. 0080.0080.9081.9083. 0085.0085.9086.9091. 0092.0092.9093.9596.0597.8598.9599.95
P985
In
,
4.,
.
•
,
.
12.47.2.•
1.3..
a
•
1..
.
54.,
B
4.6.2.40.2.3.2.3.,
B
.
,
B
,
,
4.f
.
3.2.
B
1 £
t .
251762690201379185328473385916215428456678143654729531887186587318356146672170873894368303202800902584799341757789194371238502580270
Scan *:
m/z
100.95101.95102.85103.95104.95106.95107.95109.95110.95111.85115.95116.95117.85119.95121.95122.95123.95124.95126.95127.95128.95129.95131.05133.95134.95135.95136.95137.65138.85139.95140.95141.95142.95143.95144.25145.75146.95147.95148.85150.95151.55152.95153.95
503
Int.
1.508.120.528
1. 123.977
11.3352.02730. 0363.774.416.767
6.892.601.148.637
1.296.508.538
41.3793.36817.1171.516.320.526
1.291.499.651.216.150.218
1.751.885.506.136.128.348
1.0501.623.401.310.200.536.434
L Re t n .
m/z
154.90156.00157.10157.90159.00159.90161. 00161.80164.90166.00166.90167.90168.90169.90170.20170.80171.90172.90173.90174.90175.70176.90178.00178.90179.90180.90183.80184.90185.90186.90187.90188.90190.90191.90192.90193.90195.00195.90197.90198.90199.90201.30202.90
, t ime :
Int .
.9591.736.378.388.288.574.799.270.707.729
3.3901.408.310.125.098.210.300.451.744
1.090.486.742.306
2.2251.586.914.243
1.3089.5682.596.256.572.343.809.962.186.230
2.724100.0006.386.428.657.506
6.
m
203204206207208209210214215216217220222223224225226227228230233234236238240241242243244245246248252254255256257258264265272273274
45
/z
.90
.90
.00
.00
.00
.00
.90
.90
.90
.85
.85
.85
.95
.95
.95
.95
.85
.85
.95
.95
.85
.95
.85
.95
.85
.85
.95
.95
.95
.85
.85
.75
.95
.95
.95
.85
.95
.95
.95
.95
.95
.95
.95
Int .
2.2254. 12617.5442.388.506.245.797.173.411
4.460.592
6.3691.1359.7162.433.255
3.210.506.884.341.176.190.346.196.185.453.596
8.2431.0071.163.285.359.136
34.9494.969.388
1.658.258.586.1161.1273.27919.679
m/z
275.95276.95277.95281.00283. 00284.90292.90295.90296.90302.90314.00314.80316.00320.80322.90324.10326.90327.90331.90334.00334.90340.95345.95351.95352.85353.95354.85355.05364.85365.85371.95372.75382.95401.95402.90403.80420.90422.90423.90440.90441.90442.90443.90
Int .
2.6841.082.158.120.160.198.341
3.398.563.446.228.354.266.151
1.649.251.281.150.131.774.258. 168.311.424.293.523.121.115
1.325.161.719.163.261.271.396. 123.373
3.227.639
8.60962.64111.5661. 045
186
MS Data File: >P9851::U2
Name: .................... Operator: KU0786Misc: DFTPP
Date/Time: 9/04/90 16:04BTLt 1
Fil* >P
520000-460800-
440000-
406000-
360600-
320000-
2B0000-
240000-
260000-1
160000-
126000-
80000-
40006-
0-
96E1 36.0-450.0 »»u .100 206 306 400 S
DFTPP
0 600 700 80,6
Ji4.'4 ' 4.'6 ' S'.2 ' E.'6 ' 6.'e ' fcU ' 6ls ' ?'.£ ' 7\f> ' el
•tee
•30
•60
•70
•68
•66
r40
•36
•2e
•IB
-ee
187
MS Data File: >P9871::U3
N=ime: .................... Operator: KU0786M i s c : DFTPP
Date/Time: 9/05/9G 18:14BTLlt 1
File >P9671Epk Ob 77888.
•e00ee-
70060;
bWKK*-
50000-
40000-
:3o0eo:
20*0*-
leooo-
*:
C
L
i
ii.
x
ise
69'
1
L.1Jlee
.
2?
L
186\
148
156U
198
255N^
j lit»i .1 .ftlb> 4 ..
DFTPP Scan 5046.40 m i n .
[-110
442
\
275
' • -260 250
. , , . , . . , . . . . , . . . .306 356 460
-ie0
0
-S0
•e,*
-40
-30
-20
-10
188
MS Data F i l e : >P9871: :
n i sc :
>P9B71504
DFTPP
NRM
^ i la: >P9871 Scan #:
m/z
35.9037.0038.0059. 0060. 0040.9043. 004.} .9044 . 9050. 0051.0052. 0055. 0056. 0057.0057.9060.9062. 0063.0063.9065. 0067. 0068.9069 . 9070.90?3. 0074. 0075 . 0 076. 1077. 0078 . 0 079 . 0 0HO. 00H 1 . 0 1181.9083. 0084. 0085. 00H5.90H6 . 90SB. 0090.9092. 00^2.9093. 85V4.95
Int. m/z
.104 95.85
.229 97.95
.824 98.954.316 99.85.248 100.95.291 102.95.148 103.95.657 104.95.141 105.95
12.030 106.9547.566 107.952.483 109.95.371 110.95
1.583 111.853.256 115.95.172 116.95.496 117.95.616 118.95
1.638 121.85.302 122.95.704 123.95.139 124.95
55.310 126.95.342 127.95.103 128.95.478 129.95
4.170 130.956.626 131.852.077 133.8541. 054 134.952.763 135.953.156 137.052.297 139.953.093 140.95.750 141.95.749 142.85.214 143.85.628 145.95
1.005 146.95.437 147.95.135 148.85.799 151.15.736 151.35
4.433 151.95.300 152.95.09U 153.95
:U3
KV0786 Date/Tim«i 9/05/90BTL* 1
18: 14
DFTPP
504 Retn
In t . m/z
.245 154.903.160 156.002.484 156.80.271 157.80
1.562 158.90.524 159.90.936 160.90.967 161.80.381 164.00
11.504 164.901.627 166. 00
29.622 166.903.839 167.90.425 168.90.723 170.10
7.096 171.00.539 171.90.125 172.90.671 174.00
1.285 175.00.624 175.80.534 177.00
41.793 178.003.324 178.9016.522 179.901.579 180.90.309 183.90.167 184.90.460 185.90
1.312 186.90.497 187.80.588 188.90.230 190.90
1 .837 191 .90.687 192.90.406 193.90.143 195.90.315 197.90.887 198.90
1.860 199.90.398 201.40.298 202.90.297 203.90. 164 204.90.588 206.00.517 207. 00
. t ime : 6.40
Int. m/z
1. 114 207.901.584 208.90.389 210.90.351 215. 10.281 216.85.544 217.85.835 219. 05.268 220.85. 130 222.95.636 223.95.624 224.95
3.364 225.951.588 226.85.334 227.85.132 228.95. 175 230.95.285 233.95.392 234.95.715 235.851.394 236.85.467 240.85.718 241.95.325 242.95
2.464 243.951.764 244.95.903 245.95.262 246.85
1.500 248.8510.256 252.852.949 254.95.295 255.95.643 256.95. 368 257.95.815 259.05.926 259.95.211 264.85
3.021 265.95100. 000 270.756.586 272.05.546 272.95.517 273.95. 399 274.95
2.540 275.954. 184 276.9518.627 277.952.418 282.90
In t . m/z
.611 284.90
.182 292.90
.801 295.90
.175 296.904.198 302.10.612 302.90.083 303.90
6.906 314.00.967 314.90
9.855 315.902.511 321. 00
x .351 321.903.219 323.00.494 323.90.864 326.90.411 327.90.243 333.00.236 334.00.190 334.90.284 340.85.232 345.85.404 351.95.702 352.95
9.461 353.951.087 354.951.156 364.85.316 365.85.321 371.05.137 371.95
40.160 372.955.643 382.95.380 389.95
2.063 390.85.307 391 .95.089 401.85.660 402.90.125 403.80.108 420.90.136 421.90
1.417 422.903.770 423.9022.679 440.902.682 441.901.372 443.00.231 443.90. 154 444.80
Int.
.253
.2933.972.598.126.460.146.217.452.267.158. 089
1.700.300.273.135.185.971.279.200.276.394.344.573.108
1.840.239.145.901.196.217. 121.109. 100.312.494.195.484.440
4.075.751
11.31679.61214.7021.403.069
89
M-3 Data F i l e : >P9871::U?
Name: .................... Operator: KU0786 Date/Time: 9/05/90 18:14M i s c : DFTPP BTLtt 1
File --P9871 35.0-4E0.0 amu . DFTPP
£68808-
520000-
480808-1
400880-
360800-
320806-
248000-
200060-
i20eee-80000-
40000--
e-
180 zee 380 400 see 6ee ree see
111 .
.0 4.4 4.6 5.2 5.6 6.B 6.4 6.6 7.2 7.6 6.
-100
-90
•ee
-7 if
-te
€0
+•
-30
20
-10
-fle
190
IBSEMI VOLATILE ORGAN ICS ANALYSIS DATA SHEET
Lab Name: ETCNJ Contract: _______
ERA SAMPLE NO.
ISBLK01I
Lab Code: Case No.: ____ SAS No.: 'SDG No.:
Matrix: (soil/water) SOIL Lab Sample ID: QC70246C
Sample wt/vol: 30.0 (g/mL) G Lab File ID: >P9853
Level: (low/med) LOUI Date Received: 08/23/90
Moisture: not dec. 0 dec.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) Y
CAS NO.
pH: 7.0
COMPOUND
Date Extracted: 08/30/90
Date Analyzed: 09/04/90
Dilution Fac tor
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q
l*DB-9^-2 ——111-44-4 ——95-57-8 ———541-73-1 ——106-46-7 — -100-51-6 ——Q f- cr n 1
95-48-7 ———i n o ^ n 1
106-44-5 ——621-64-7- —i —} "70 i98-95-3- --78-59-1 ——B8-75-5 ———105-67-9 ——65-85-0 ———111-91-1 ——120-63-2 ——120-82-1 ——91-20-3 ———106-47-8 ——87-68-3 ———59-50-7 ———91-57-6 ———77_47_4_ ——88-06-295-95-4----91 58-7 ——88-74-4 ———131-11-3 ——208-96-8 — -606-20-2 ——
-----Pheno 1_____bis(2-Chloroethul )ether-----2-Chlorophenol-----1,3-Dichlorobenzene-----1,4-Dichlorobenzene_____Benzyl alcohol-----1 .2-Dichlorobenzene-----2-Methylphenol
-----4-Methylphenol_ _ _ _ _ N _ N it roso-d i-n-p ropy 1 a mine _
-----Nitrobenzene----- Isophorone— ---2-Nitrophenol-----2, 4- Dime thy 1 phono 1-----Benzoic acid__ — -bis(2-Ch loroethoxy) me thane _-----2,4-Dichlorophenol-----1 .2 .4-Trichlorobenzene-----Naphthalene_____4_Cnloroani i jne
-----Hexach lorobutadiene-----4-Chloro-3-methylpheno 1 ______-----2-Methylnaphtha lene-----Hexachlorocyclopentad iene __-----2 .4.6-Trichlorophenol-----2 .4.5-Trichloroohenol
-----2-Ni t roani 1 ine-----Dimethylphthalate
-----2,6-Dinitrotoluene
113301330133013301330133013301330133013301330133013301330133013301 170013301330133013301330133013301330133013301 17001330117001330 -13301330 3*1
i.IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1
FORM I SU -1 87 Rev.
1CSEMI VOLATILE ORGAN ICS ANALYSIS DATA SHEET
Lab Name: ETCNJ
Lab Code: Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 0 dec.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) Y pH: 7.0
Con t rac t:
SAS No.:
EPA SAMPLE NO.
I1SBLK01I______________
SDG No.:
Lab Sample ID: QC70246C
Lab File ID: >P9B53
Date Received: 08/23/90
Date Extracted: 08/30/90
Date Analyzed: 09/04/90
D i l u t i o n Factor: 1
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
99-09-2---- — — -3-Nitroanil me______________t 170083-32-9---------Acenaphthene_______________I 33051-2B-5---------2,4-Dmitropheno 1___________I 1700100-02-7----- —— 4-Nitrophenol_______________I 1700132-64-9 — - — - — Dibenzofuran________________1330121-14-2--------2,4-Dinitroto luene__________I 33084-66-2 —— - — - — Die thylph thai ate____________13307005-72-3-------4-Chlorophenyl-phenylether_I 33086-73-7————————Fluorene____________________1330100-01-6 ——————— 4-Nitroani 1 me_____________I 1700534-52-l--------4,6-Dinitro-2-methylphenol__I 170086-30-6---------N-Nitrosodiphenylamine (1)_I 330101-55-3--------4-Bromopheny1-phenylether___I 330118-74-1---- — --Hexach lorobenzene___________I 330S7-86-5---------Pentachloropheno 1___________| 170085-01-8---------Phenanthrene________________ I 330120-12-7———————Anthracene__________________133084-74-2---------Di-n-butylphtha late_________I 702 06-44-0--------Fluor an thene________________I 330129-00-0--- —— --Pyrene______________________133085-68-7----- —— -Butylbenzylphthalate________133091-94-1- —— -----3,3 '-Dichlorobenzidme_____167056-55-3---------Benzo (a ) anthracene__________I 330
I 218-01-9 ——————— Chrysene____________________1330I 117-81-7———————bis(2-Ethylhexyl )phthalate__150I 117-84-0--------Di-n-octylpht ha late_________1330205-99-2--------BenzoCb ) fluoranthene________I 330207-08-9--------Benzo(k)fluoranthene_______133050-32-8---------Benzo (a )pyrene______________I 330193-39-5——————— IndenoCl,2,3-cd)pyrene______133053-70-3---------Dibenz(a,h)anthracene_______I 330191-24-2 —— — ---Benzo(g,h,i )perylene________1330
(1) - Cannot be separated from Dipheny1 amine
FORM I SU -2
Q
IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIJIUIUIUIUIUIUIJIUIUIUIUIUIUIU
1/37
192Rev.
IFSEMIUOLATILE ORGAN ICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
ERA SAMPLE NO.
ISBLK01Lab Name:ETCNJ
'Lab "Lode : tase No . : ____
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) G
Level: (low/med) LOUI
\ Moisture: not dec. 0 dec.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: CY/N) Y PH: 7.0
Number TICs found: 2
Cont ract:
SAS No.: SDG No.:
Lab Sample ID: QC70246C
Lab File ID: >P9853
Date Received: 08/23x90
Date Extracted:08/30/90
Date Analyzed: 09/04/90
D i l u t i o n Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
ICAS NUMBER
01. 123-79-502.
COMPOUND NAME
Hexanedioic acid, dioctyl esUnknown
RT
33.337.72
EST. CONC
92004200
Q
3J
FORM I Sv-TIC Rev.
TOTAL ION CHROMPTOCRPMFile >P9653 35.0-506.0 *»u.
4
2880000-
2600000-
2400000-
2200000-
2080000-
1800000-
1600000-
1480080-
1280000-
1000000-
880000-
600080-
480000-
280000-A-
I~ I•51 11 Jw 3It"
,1
Be
f *Mijr* •i.
a 12
j
8§^
1 i*
! ;i> s^ i
t i
ji C: '!
J
SBLK01TICeae ( 1200
I I !i
E-| •[• !
i iI \
•
j[
1 B.gJ :
A 2
5 :\ c
I 1! 14 . 9V • i<> ** I JI7
1 " 1
<j
62
16 28 24 26
OC70246C ,0078246, Si
( 1600 ( 2000
t-••«is.
6
im 3
CM £
V N
^5
2 1
32 ' 36" ' "40" ' "44 '
Data File: >P9B53::U2Name: SBLK01Misc: QC70246C ,QC70246,S:M4,30.00,1
Id File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900904 17:29
Operator ID: KU0786Quant Time: 900904 18:05Injected at: 900904 17:18
Quant Output File: ~P9853::UL
BTL* 3
194
QUANT REPORT Page
Operator ID: KU0786Output File: -P9853::ULData File: >P9853:: U2Name: SBLK01Misc: QC70246C ,QC70246,S:M4,30.00,1
ID File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900904 17:29
Quant Rev:" 7 Quant Time:Injected at
Di lut ion Factor:
900904 18:135900904 17:18
1.00000
BTL* 3
Compound R.T. Scan* Area Cone Units
1)3)5)12)17)18)32)36)49)50)52)54)62)65)66)67)68)68)72)73)
•d4-l,4-Dichlorobenzene 11.97 382 1846632-Fluorophenol (SURR) 8.72 222 765027Phenol-05 (SURR) 11.36 352 1136970N-Nitrosodi-n-propylamine 13.72 468 .75322
•d8-Naphthalene 15.82 571 706682Nitrobenzene-D5 (SURR) 13.72 468 484303
•dlO-Acenaphthalene 21.38 844 3548812-Fluorobiphenyl (SURR) 19.34 744 860460Diethyl phthalate 23.07 927 3241Fluorene 23.90 968 161402,4,6-Tribromophenol (SURR) 23.90 968 306500
•dlO-Phenanthrene 25.98 1070 593908Di-n-butyl phthalate 28.22 1180 41554»d!2-Chrysene 34.39 1483 346705Benzidine 25.98 1070 72155Terphenyl-D14 (SURR) 31.19 1326 779357Butyl benzyl phthalate 32.90 1410 3353Butyl benzyl phthalate 33.33 1431 2890bis(2-Ethylhexyl)phthalate 34.88 1507 11277•d!2-Perylene 38.69 1694 268737
40.00129.12147.34
UG/MLUG/MLTUG/Mlr--UG-41L
40. 0069.2840.0062.97
.282
UG/MLUG/Mlr-UG/MLUG/Mb
Sii UG>t1L185.10
40 .002.11
40 .00
UG/MlrUG/MLUG/ML—UG/ML
60.42 UG/ML.501 UC/ML.432 UG^ML1.50 UG/ML"
40.00 UG/ML
8883903893919499928394999697
1009490489182
* Compound is ISTD
195
REFERENCE STRNPPRP SPECTRUMFil* >EBpk Pb
teeee-
e-4
41699999.
ie ee
TflRCET REFERSUB MR
149
ENCE SPECTRfl Sc«n 1tM NOM 26.85 •
' 128 T 1^8 ' 288 ' 24*8 '
814In.
•188
<
SAHPLE SPECTRUM (BACKGROUND SUBTRACTED)File >P9653 SBLK81Bpk Pb 14271.
18e9e" « « «*V OO -X
46 ' ' e'0
QC78246CSUB
149
~]' 184 121 MSB
128 ' 168 i '
,QC78246,SlM4,3e
286 223^ /
' 288 ' ' ' ' ' 24e
Sc«n 118828.22 Bin.
[-166
278
, . , . .T' -8
SAMPLE SPECTRUM (UNPLTERED)File >P9863 SBLK81 QC78246CBpk Ab 14271.
149.
18886-^
*> 71.6 184 121 156r: ,46 86 128 168
,0076246,5 IM4.36
286X
' 288 '
223X
240
Sc»n 118028.22 Bin.
278
hi 88
A
Data File: >P9853::U2 Quant Output File: ~P9853::ULName: SBLK01Misc: QC70246C ,QC70246,S:M4,30.00,1 BTL* 3Quant Time: 900904 18:05 Quant ID File: IP0085::PFInjected at: 900904 17:18 Last Calibration: 900904 17:29
Compound No: 62Compound Name: Di-n-butyl phthalateScan Number: 1180Retention Time: 28.22 mm.Quant Ion: 149.0Area: 41554Concentration: 2.11 DC/MLq-value: 96
196
REFERENCE STANDARD SPECTRUMFil» >JBpk Ab
teeee-
4
7992 TARGET REFER9999. SUB N
149•.
57^ 7j
ENCE SPECTRA Scan 2?M NOM 33.26 •
167
i
848in.
•186
«16 ' 86 ' 126 166 ' 288 ' 246 ' 288
SAMPLE SPECTRUM (BACKGROUND SUBTRACTED)File >P9853 SBLK81Bpk Ab 4327.
4666-
- 5^ 7/ 83 IK.fL } ,-/./. 74e' ' ' e'e
QC78246CSUB
149""*"
167' 122 ^•^ .' . \ 1' 126 ' 166
,QC7e246,S:M4,3e
248\
286 ' 248
Scan 156734.66 Bin.
-188
279b J*
288
SAMPLE SPECTRUM (UNALTERED)Fil» >P98E3Bpk Ab 4327
A Oft ft-4866- B?•*-,
46
SBLK61n
"^ i 83 11:il i,^ ^r\ ( i i . , i . r^ i88
QC78246C149">
' 122~? X
167
128 ' 166
,QC78246tSiM4,38
267 246/ \
286 246
Scan 156734.88 «in.
-188
279
' 268
Data File: >P9853::U2 Quant Output File: "SP9B53::ULName: SBLK01Misc: QC70246C ,QC70246,S:M4,30.00,1 BTL* 7Quant Time: 900904 16:05 Quant ID File: IPOOB5::PFInjected at: 900904 17:18 Last Calibration: 900904 17:29
Compound No: 72Compound Name: bis(2-Ethylhexy1)phthalateScan Number: 1507Retention Time: 34.86 min.Quant Ion: 149.0Area: 11277Concentrat ion: 1.50 LJG/flL.q-value: 91
197
QUANT REPORT Page
Operator ID: KY0786 Quant Re-j:Output File: ~P9873::ULData File: >P9873: : U3Name: SBLK01Misc: QC70246C,QC70246,S:M4,3Q. 00,1
ID Fi le: IP0085: : PFTitle: IFB/BNA, PP/BNA, TCLBN1Last
1)3)5)6)12)17)18)32)36)49)50)52)54)62)65)66)67)68)72)73)
Calibration: 900906 09:54
Compound
*d4-l ,4-Dichlorobenzene2-Fluorophenol (SURR)Phenol -D5 (SURR)PhenolN-Ni t rosodi-n-propylamine
«d8-Naphtha leneNitrobenzene-05 (SURR)
*dlO-Acenaphthalene2-Fluorobiphenyl (SURR)Diethyl phthalateF 1 uorene2 ,4,6-Tr ibromophenol (SURR)•dlO-PhenanthreneDi-n- butyl phthalate*d!2-ChryseneBenzidineTerphenyl-D14 (SURR)Butyl benzyl phthalatebis£2-£thylhexyl )phthalate
*d!2-Perylene
R.
11.8.11.11.13.15.13.21.19.23.23.23.25.28.34.*? G
31.32.34.38.
T.
93663234667666323001RAD*»849216319211848058
7 Quant T ime :Injected at
Di 1 ut ion Fac tor:
Scan*
3802193503514655684658417429249f 596510671177147910671322140715031689
Area
1823877545921097796
5654767496926664910353632778503673436
1 O C C16777
3253775952103704433383174205772292295310013
269916
: 900906 09:55: 900905 19:2?: 1.00000
BTL4 3
Cone
40.124.142.' '
•L J ,
40.69.40.64.
•»• 'i171.40.2.40.
^ 11 n
64.s.
1.40.
003234
nn' '00230060n °— ~XQ
57004700C "T
41O X
3500
Units
UG/MLUG/ML-"UG/ML—-tte/MLt_H_l' ' 'I—
UG/MLUG/MLTUG/MLUG/Mbr-UG/ML-UG/MLUG/MCUG/MLUG/ML-^UG/MLUGj'MLUG/ML-1 IO xMI
UG/ML—UG/ML
q89829390389391979892B £\9497969610093879480
* Compound is ISTD
201
Til*Bpk
Bpk*
>P98S3 SBLK81flb 9999.
J 41 / 78 112
"liH...L.-' 48
>BICDBPb 9999.
' se ' ' 'i 2*e
QC70246C ,eC70246.SiN4,30 Scan 1431SUB NRM 33.33 Bin.
157 199212 241 284 313 341 |
T i1er ' 288 ' 248H*x*n*dioic *c id. dice tyl **t*r
* OO
r^irirFileBpk
FileBpk
' '48 88 128r !68
A /
168
199212 2*1
288 248
288' ' 328
(9CJ)
' 368
Scan 138498.08 Bin.
279313 341 378 [
288 ' 328
>BIGHB Hexanedioic acid, »ono(2-ethylhexyl )ester (9CAb 9999.
j 'S' 48
>BICDBHb 9999.
-K40
55
A-78 112
^•^ . /
80 120
129
157,T1 fT 'lie '
199212 241
200 ' 248
268^288 ' 328
Hexanedioic acid, dicyclohexvl ester (9CI)
55 83 »U
88 128
129s*
169
T lie1 '
184 211 229
288 ' 248 '288 ' 328
' 368 '
Scan 138588.88 Bin.
-L368Scan 138838.08 Bin.
I.368
Data File: >P9853::U2Name: 5BLK01Misc Data: QC70246C ,QC70246,S:M4,30 . 00 ,1RT (min): 33.33Scan: 1431Area: 6312340 Rank: 1Semi-quantitative Cone (uncorrected): 275.48 UG/MLSemi-quantitative Cone ( corrected ): 9182.63 ug/kgCalculated using Istd: d!2-Chrysene § 34.39 minutes
BTL* 3
*ru,PRE ,,PBR181,,,1,31. Hexanedioic acid, dioctyl ester (9CI)2. Hexanedioic acid, mono(2-ethyIhexy1)ester C9CI)3. Hexanedioic acid, dicyclohexyl ester (9C1 )
370 C22H4204258 C14H2604310 C18H3004
Sample file: >P9853 Spectrum #:Search speed: 1 Tilting option: S
1431No. of ion ranges searched: 46
1.2.~> .
Prob.
82«7627
CAS *
1237954337659849990
CON *
13849138.50.13803
ROOT
"BIGDB" (3,T.rcC'E)"BIGDB
K
125*yy63
DK #FLG
394"ti75
002
TILT \
1-10
62•70" 89
CON
381537
C_I R_IU
374010
L5913
198
Film >P9863 SBLK81 OC78246C ,BC78246 ,S iH4 ,38 Scan 173Bpk Ab 9999. SUB NRM 7.72 Bin.
43
8888-
4888-
8-
69
44 66 69 71 83 10:
'20 38 48 68 68 78 88 98 188
-ee-48
-8
Film >BICDB Cuanidin* (8CI9CI) Scan 1681Bpk Ob 9999. 8.88 Bin.
69J 43 / (.
8888-
4888-
8-
v.18r «/j, t\. / ,,-28 38 48
44 68
VB' ' 68 ' '7'*' ' ' 'e'e' ' ' Ve' ' ' lee
•88
•48
Fil* >BICDB Ac»taBid» (8CI9CI) Scan 1677Bpk Ob 9999. 8.88 Bin.
59
8888-
4888-
8-
43*«s.
28 31
f / ,i rl'f'i ii|'28 38 48
r
61 61
68 68 78 88 98 188
«8
•48
•8
Data File: >P9853::U2Name: SBLK01Misc Data: QC70246C ,QC70246,S:M4,30.00,1RT (min): 7.72Scan: 173Area: 3238740 Rank: 2Semi-quantitative Cone (uncorrected): 124.84 UG/MLSemi-quantitative Cone ( corrected ): 4161.43 ug/kgCalculated using Istd: d4-l,4-Dichlorobenzene § 11.97 minutes
BTL* 3
*ru,PRE ,,PBR181,,,1,31. Guanidine (6CI9CI)2. Acetamide (8CI9CI)
59 CH5N359 C2H5NO
Sample file: >P9853 Spectrum #:Search speed: 1 Tilting option: S
173No. of ion ranges searched: 46
1.2.
Prob. CAS *
25* 11300815« 60355
CON *
15811577
ROOT
"BIGDB"BIGDB
K
2020
DK
4755
*FLG
12
TILT
00
K
5454
CON
4660
C_I R_IU
73
1413
199
IBSEMI VOLATILE ORGAN ICS ANALYSIS DATA SHEET
Lab Name: ETCNJ Cont ract: _______
ERA SAMPLE NO.
A4377MS
Lab Code: Case No.: ____ SAS No.: SDG No.:
Matrix: (soil/water) SOIL Lab Sample ID: CA4377CS
Sample wt/vol: J5^Z 3O Cg/mL) G Lab File ID: >P9856
Level: (low/med) LOU ,, . Date Received: 08/23/90
* Moisture: not dec. *-«*/<* dec. Date Extracted: 08/30/90
Date Analyzed: 09/04/90
Dilution Factor: 1
Extract ion: CSepF/Cont/Sonc) SONC
GPC-Cleanup: (Y/N) Y pH: 7.0
CAS NO. COMPOUNDCONCENTRATION UN-ITS:(ug/L or ug/Kg) UG/KG
108-95-2 ——————— Phenol_____________________15400111-44-4———————b is C2-Chloroethy l)ether____140095-57-8 ———————— 2-Chlorophenol_____________14600541-73-1 ——————— 1,3-Dichlorobenzene________1400106-46-7———————1,4-Dichlorobenzene________12700100-51-6 ——————— Benzyl alcohol_____________140095-50-1 — ——————1,2-Dichlorobenzene________140095-48-7————————2-Methyl phenol_____________1400108-60-1 ———— —-bisC2-Chloroisopropy 1)ether_|400106-44-5 ——————— 4-Methylphenol_____________1400621-64-7- —————— N-Ni troso-di-n-p ropy lam ine__1260067-72-1 ———————— Hexachloroe thane___________140098-95-3-- —————— Nitrobenzene_______________140078-59-1———— — —Isophorone_________________140088-75-5- — — — — 2-Nitrophenol______________1400105-67-9———————2,4-Dimethylphenol_________140065-85-0———————Benzoic acid_______________1120111-91-1 — —————b is (2-Chloroethoxyimethane__1400120-83-2———————2,4-Dichlorophenol_________1400120-82-1 ——— ——— 1,2,4-Trichlorobenzene_____1310091-20-3 ———————— Naphthalene________________1400106-47-8 ——————— 4-Chloroani 1 ine____________140087-68-3 —————— --Hexachlorobutad iene________140059-50-7———— ——— 4-Chloro-3-methyl phenol____1610091-57-6 ———————— 2-Methyl naphtha Iene________140077-47-4-- — -----Hexachlorocyc1 open tadiene__140088-06-2 —— —— —— 2,4,6-Tr ich loropheno 1______140095-95-4————————2,4,5-Trichlorophenol______1200091-58-7——- ———— 2-Chloronaphthe Iene________140088-74-4———————2-Ni t roan i line____________12000131-11-3 ——————— Dimethylphtha late__________1400 -*2 08-96-8-- ———— Acenaph thy Iene____________1400606-20-2 —— ——— -2,6-Dinitrotoluene_________1400 -__________________________________________I
Q
IUtIUIIUtuIUIUIUIIUIUIUIUIUuIUIUIIUIUIUIIUIUIUIUIUIUIUIUIUI
FORM I S"J -1 Rev.
TOTOL ION CHROMOTOCRRMFile >P
2688888-
2400000-
2288800-
2008880-
1888080-
1688880-
1400000-
1280000-
1808080-
888888-
688000-
400000-
280880-
Ck-
9973 ss.e-see.e *«u. SBLKBI488 888
- 1 I f| i f i j
J til l|i1 | f Y » «;
lil:' s
' 49
8 ' 12 16 ' 28 ' 2
1288
?•
i ^
! ! ,; f ?i •>
62 6
4 ' 28 ' 32
9C78246C ,QC78246 ,S if
1680 2888
i1 I1 "°f2 i36 48 44
Data File: >P9873::U3Name: SBLK01Misc: QC70246C,QC70246,S:M4,30.00,1
Id File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900906 09:54
Operator ID: KU0786Quant Time: 900906 09:55Injected at: 900905 19:25
Quant Output File: ~P9873::IJL
BTL* 3
200
1CSEMI VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
IA4377MSLab Name: ETCNJ
Lab Code: Case No.:
Metrix: (soil /water) SOIL
Sample wt/vol: ^5^2 ?O (g/mL) G
Level: Clow/med) LOUJ &T *}/&}&
\ Moisture: not dec. --0" /fa dec .
Extraction: (SepF/Cont /Sonc ) SONC
GPC Cleanup: <Y/N) Y pH: 7.0
Contract:
SAS No.:
CAS NO. COMPOUND
SDG No.:
Lab Sample ID: CA4377CS
Lab File ID: >P9B56
Date Received: 08/23/90
Date Extracted: 08/30/90
Date Analyzed: 09/04/90
Di lut ion Factor: 1
CONCENTRATION UNITS:Cug/L or ug/Kg) UG/KG
99-09-2 ———— -83-32-9 ————51-2B-5 ———— -100-02-7 ———132-64-9 ——— -121-14-2 ——— -84-66-2 ———— -7005-72-3 —— -86-73-7 ———— -100-01-6 ——— -534 52- 1- _ --B6-30-6 ———— -101-55-3 ——— -118-74-1 ——— -87-B6-5 ———— -85-01-8 ———— -120-12-7 ——— -84-74-2 ———— -206-44-0 ——— -129-00-0 ——— -85-68-7 ———— -91.94-1 ———— .56-55-3 ———— -218-01-9 ——— -117-81-7 ——— -117-B4-0 ——— -205-99-2 ——— -207-08-9 ——— -50-32-8 ———— -193-39-5 ——— -53-70-3 ———— -191-24-2 ——— -
-___3-Ni t roan i 1 ine, . —----Acenaphthene----2 ,4-Dinitrophenol----4-Ni t ropheno 1----Dibenzofuran----2,4-Dinitrotoluene----Diet h-jloht ha late'---4-Chlorophenyl-pheny 1 ether _----Fluorene----4-Ni t roan i 1 ine_ _ ,•---4,6-Dinitro-2~methylpheno 1 _----N-Nitrosodiphenylamine (1 )___•---4-Bromopheny 1-pheny let her __----Hexach lorobenzene•---Pentachlorophanol•---Phenanthrane• ---Anthracene^,----Di-n-but-jlphthelate•---Fluoranthene----Pgrene ,• ---But ulbenzsjlphtha late----3 .3 '-Dichlorobenzidine•---Benzo (a) anthracene----Chrysene.- —— bi»(2-Ethylhexyl )phthalate _----Di-n-octvlphthalate•---Benzo(b)fluoranthene----Benzo Ck ) f luoranthene• ---Benzo(a)pyreneg,---- Indeno C 1 .2 .3-cd )purene---Dibenz Ca .hlanthracene----Benzo Cg .h r i )oer«jlene
11200012800120001170001400131001400140014001200012000140014001400170001400140018114001330014001790140014001811400140014001400140014001400 -1
1IU1IU1IU1IUIUIUIUIUIUIUIU1IUIUIJIU1IUIUIUIUIJIUIUIUIUIUIUIU1
(1) - Cannot be separated from Diphenylamine
FORM I SU -2 1/87 Rev
203
TOTAL ION CHKOHflTOCROMFiU >P9656
2200000-
2000000-
1000000-
1600000-
1400000-
1200000-
1 000000-
000000-
600000-
400000-
200000-.
A.2
35.0-690.0 «*U. B4377H5 CR*t^77CS .iC70246i5lTIC
t 400 t 0f 0 f 1 2,00 , 1 600 ( 2000
:;
g
i £&
* 1j-. 5 aI
i
( i
II ]s j
9
1
; ;1
i!2
«
i **L
[ !
31T •t
*L.
r
l
••<
1
^
J
f
i
\\ iE
11 ';' t« I•IT 1
p
!L; 1 j
v < F2
& 12 ' 16 ' 20 24 ' 26 ' 32 ' 36 ' 40 ' 4*4 '
Data File: >P9856::U2Nam«: A4377MSMi»c: CA4377CS ,QC70246,S:M4,25.23,1
Id File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibrationi 900904 17:29
Operator ID: KU0786Quant Time: 900904 20:48Injected at: 900904 20:01
Quant Output File: /SP9656::UL
BTL* 6
204
QUANT REPORT Page
Operator ID: KV0786Output File: ~P9856::OLData File: >P9856::U2Name: A4377MS
CA4377CS ,QC70246 ,S:M4,25. 23 ,1
Quant Rev: 7 QuantInjected at
Di lut ion Factor
900904 20:48900904 20:01
1.00000
BTLt 6
ID File: IP0085: :PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900904 17:29
Compound R.T. Scant Area Cone Unite
1)2)3)5)6)7)8)9)10)12)12)14)15)17)18)24)26)31)31)32)36)43)46)47)90)52)54)59)59)62)63)64)65)66)67)72)73)
*d4-l,4-DichlorobenzeneN-Ni trocodimethylamine2-Fluoropheno1 C5URR)Phenol-D5 CSURR)Phenol2-Chloropheno11.3-Dichlorobanzana1.4-Dichlorobenzene1,2-DichlorobenzeneN-Nit rosodi-n-propylamineN-Nitrosodi-n-propylamine2-Methylphenol4-Methylphenol
*de-NaphthalaneNitrobenzene-05 (SURR)1,2,4-TrichlorobenzeneBanzoic acidp-Chloro-m-crasolp-Chloro-m-cresol
*dlO-Acenaphthalene2-Fluorobiphenyl (SURR)Acanaphthane2,4-Dinitrotoluene4-Nitrophenoli/Fluorana2,4,6-Tribromophenol (SURR)
*dlO-PhenanthrenePentachloropheno 1Pentachloropheno1Di-n-butyl phthaiateFluoranthenaPyrane»d!2-ChryseneBanzidinaTerphenyl-D14 (SURR)bi*(2-Ethylhexyl)phthalate*d!2-Perylene
12.00 383 169646 40.00 UG/ML 894.84 31 40377 -10.PI UB>'ML 1008.70 221 127897 23.50 UG/MLr 83
11.41 354 904007 127.52 US/Mb- 9311.45 356 -923722 135.68 UG/ML— 8811.53 360 761171 116.37 UG/ML- 9412.04 385 448802 <P,B? UG/ML 8612.04 385 448802 68.39 UG/ML~ 9512.04 385 448802 69.84 UG/ML 9613.51 457 302456 64.40 UG/ML 7413.73 468 64713 13.79 UC/ML 3813.49 456 4775 r e4-WG/nU 8513.49 456 4775 .828 USxtlL 9615.83 571 609666 40.00 UG/ML 9313.73 468 423903 70.29 UGxMlT 9415.75 567 427679 78.38 UG/ML~ 9615.44 552 8832 3.12 UGXML- 9517.86 671 618082 154.81 UG/ML- 10017.93 674 3797 .9P1 UB;'ML 10021.37 843 275078 40.00 UG/ML 9519.35 744 692227 65.36 UG/(1lr- 9821.49 849 618498 69.50 UG/ML— 9922.20 884 213012 78.96 UG/ML- 9022.08 878 232465 418.10 UG/MLr- 10023.89 967 8767 1.09 UBvML 9123.87 966 161440 125.78 UG/ML— 9225.99 1070 343488 40.00 UG/ML 9925.66 1054 220216 177.10 UG/ML- 9926.44 1092 2687 ~2_1&-U£/ML 9328.23 1180 23201 2.04 UG/Mt—— 9530.50 1292 607889 -02.19 UQ;11L 9830.50 1292 607889 83.28 UG/ML- 9734.37 1482 172147 40.00 UG/ML 9625.99 1070 43113 ItJ.OB UC/ML 10031.18 1325 436719 68.18 UG/ML- 9334.88 1507 7605 2.04 UG/ML"~ 9038.67 1693 119193 40.00 UG/ML 80
* Compound is 1STD
205
IBSEMI VOLATILE ORGAN ICS ANALYSIS DATA SHEET
ERA SAMPLE NO.
IA4377MSDLab Name: ETCNJ
Lab Code: Case No.: ____
Matrix: (soil/water) SOIL
Sample wt/vol: 2%~2 -*° Cg/mL) G
Level: Clow/mod) LOU
% Moisture: not dec. Jfr* /fa dec.*T 7/Wf o
Extract ion: (SepF/Cont/Sonc> SONC
Cont ract:
SAS No.:
GPC Cleanup: CY/N) Y
CAS NO.
pH: 7.0
COMPOUND
SDG No.:
Lab Sample ID: CA4377CR
Lab File ID: >P9875
Date Received: 08/23/90
Date Extracted: 08/30/90
Date Analyzed: 09/05/90
Dilution Factor: 1
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG
I108-95-2 ——————— Phenol._____________________15200111-44-4———————bia(2-Chloroethyl)ether____140095-57-8 ———————— 2-Chlorophenol_____________14800541-73-1 ——————— 1,3-Dichlorobenzene________1400106-46-7——————1,4-Dichlorobenzene________12800100-51-6 ——————— Benzyl alcohol_____________140095-50-1 —— ————— 1,2-Dichlorobenzene________140095-48-7————————2-Methylphenol_____________1400108-60-1 ——————— bi5(2-Chloroisopropyl >ether_l400106-44-5———————4-Methylphenol_____________1400621-64-7———————N-Ni t roeo-d i-n-p ropy lam me_1280067-72-1 ——————— Hexachlo roe thane__________140098-95-3 ———————— Nitrobenzene_______________140078-59-1———————— Isophorone_________________140088-75-5———————2-Nitrophenol_____________1400105-67-9 ——————— 2,4-Diro»thyl phenol_________140065-85-0——-————Benzole acid_______________1150111-91-1——————-bia(2-Chloroethoxy)methane__1400120-83-2 ——————— 2,4-Dichlorophenol_________1400120-82-1 ———— —— 1,2,4-Tr ichlorobenzene_____1300091-20-3————————Naphthalene________________1400106-47-8 ——————— 4-Chloroani 1 ine____________140087-68-3 — —————— Hexachlorobutad iene________140059-50-7————————4-Chloro-3-methyl phenol____1610091-57-6 ———————— 2-Methylnaphthe Iene________140077-47-4----- — --Hexachlorocyc1 opentad iene__140088-06-2 ———————— 2,4,6-Trichlorophenol______140095-95-4————————2,4,5-Trichlorophenol______1200091-58-7——— ———— 2-Chloronaphthalene________140088-74-4———————2-N i t roan i line____________12000131-11-3———————Dimethylphthalete__________1400208-96-8———————Acenaphthy Iene_____________I400-*606-20-2 ——————— 2,6-Dinitrotoluene_________I 40OX,
IUIIUIIUIUIUIUIUItuIUIUIUIU13tuIUIIUIUIUIIUIUIUIUIUIUIUIUIU
FORM I SO -1 Rev.
1CSEMI VOLATILE ORGAN ICS ANALYSIS DATA SHEET
ERA SAMPLE NO,
A4377MSDLab Name: ETCNJ
Lab Code:
Cont rac t:
Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: _2Ji*-2 $o Cg/mL) G
Level: (lou/med) LOU
S Moisture: not dec. *& k> dec.<*T 4/tf/fe
Extract ion: (SepF/Cont/Sonc) SONC
GPC Cleanup: CY/N) Y pH: 7.0
SAS No.: SDG No.:
Lab Sample ID: CA4377CR
Lab File ID: >P9875
Date Received: 08/23/90
Date Extracted: 08/30/90
Date Analyzed: 09/05/90
Di lut ion Factor: 1
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg). UG/KG
99-09-2— ——— —— 3-Nitroani 1 ine___83-32-9 — -- ———— Acenaphthene____51-28-5- ———— —— 2,4-Dinitropheno 1,100-02-7———————4-Nitrophenol___132-64-9 —————— -Dibenzofuran____121-14-2 —————— -2,4-Dinitrotoluene.84-66-2- ——————— Diethylphthalate.
I__12000__12700__12000__18000__1400___13700__1400
7005-72-3——————4-Chlorophenyl-phenylether_140086-73-7———————Fluorene_________________1400100-01-6——————4-Ni t roan i line____________12000534-52-1——————4,6-Dinitro-2-methylphenol_1200086-30-6————————N-Nitrosodiphenylamine (1)_1400101-55-3———————4-Bromophenyl-phenylether__1400118-74-1 — — ——— Hexachlorobenzene_________140087-86-5 ———————— Pentachlorophenol__________1700085-01-8—— ————— Phenanthrene_______________1400120-12-7—— ———— Anthracene______________ 1400
__184__1400__13200__1400__1790__1400__1400
84-74-2————————Di-n-butylphthalate.206-44-0———————Fluoranthene_______129-00-0————85-68-7—————
•Pyrene.------Butylbenzylphtha late
91-94-1 ——— ———— 3,3'-Dichlorobenzidine.56-55-3---------Benzo<a) anthracene____218-01-9————-----Chrysene_________________117-81-7———————bisC2-Ethylhexyl )phthalate__I 100117-84-0———————Di-n-octylph thai ate________1400205-99-2 ————— — Benzo(b)f luo rant none_______1400207-08-9 ——————— BenzoCk)f luoranthene_______140050-32-8 —— ———— -BenzoCa)pyrene_____________1400193-39-5———————Indenod,2,3-cd)pyrene_____140053-70-3 —— — -- — D i benz C a, h) anthracene______1400191-24-2 —— —— — BenzoCg,h,i )perylene_______1400 ;
(1) - Cannot be separated from Diphenylamine
FORM I SU -2
Q
IUItu1IUIIUtuIUIUIUIUIUIUIIUIUIJIUIIUIUIUIUIJIUIUIUIUIUIUIUI
1/87 Rev,
207
TOTPL ION CHROHflTOCRflMFile >P9075
2608000-
2480090-
99Aaaaa^C£OWW
2999000-
1808888-
1688880-
1488088-
1 288880-
1000000-
800009-
600088-
400880-
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Date File: >P9875::U3Name: A4377MSDMi»c: CA4377CR,QC70246,S:M4,25.23,1
Id File: IP0085:iPFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900906 09:94
Operator 10: KU07B6Quant Time: 900906 10:02Injected at: 90090? 21:14
Quant Output File: ^P9B75::«JL
BTL# 5
208
QUANT REPORT Page
Operator ID: KU07B6Output File: ^P9875::ULData File: >P9875::U3Name: A4377MSDM i sc: CA4377CR,QC70246,S:M4,25.23,
ID File: IP0085::PFTitle: IFB/BNA, PP/BNA, TCLBN1Last Calibration: 900906 09:54
Quant Rev: 7 Quant TimeInjected at
Oilut ion Factor
900906 10:02900905 21:14
1.00000
BTL* 5
Compound R.T. Scant Area Cone Units
1)2)3)5)6)7)6)9)10)12)12)12)14)15)17)18)24)25)26)27)3D31)32)36)41)43)46)47)49)50)52)54)59)59)62)63)64)65)66)67)72)73)
»d4-l,4-Dichlorobenzene 11.94 380 194160N-Nitrosodime thylamine 5.37 57 198552-Fluorophenol (SURR) 8.85 228 555297Phenol-05 (SURR) 11.37 352 1119238Pheno1 11.41 354 10424982-Chlorophenol 11.50 35B 9113291.3-Dichlorobenzene 11.99 382 5281381.4-Dichlorobenzene 11.99 362 5281381,2-Dichlorobenzene 11.99 382 52B13BN-Nitrosodi-n-propylamine 13.37 450 62336N-Nitrosodi-n-propylamine 13.47 455 358571N-Ni trosodi-n-propylamine 13.70 466 834032-Methylphenol 13.45 454 52544-Methylphenol 13.45 454 5254*d8-Naphthalene 15.77 568 745793Nitrobenzene-05 CSURR) 13.70 466 5424151,2,4-Trichlorobenzene 15.69 564 5204862,4-Dichlorophenol 15.45 552 3330Benzoic acid 15.43 551 13379Naphthalene 16.00 579 2548p-Chloro-m-cresol 17.85 670 925579p-Chloro-m-cresol 17.89 672 6504
*dlO-Acenaphthalene 21.31 840 3905032-Fluorobiphenyl (SURR) 19.30 741 BB05072,6-Dinitrotoluene 20.90 820 3132Acenephthene 21.43 846 8563252,4-Dinitrotoluene 22.15 881 3696564-Nitrophenol 22.07 877 172975Diethyl phthalate 23.02 924 2524Fluorene 23.84 964 135702,4,6-Tribromophenol (SURR) 23.84 964 260755
*dlO-Phenanthrene 25.92 1066 562635Pentachlorophenol 25.61 1051 361060Pentach loropheno1 26.36 1088 3882Di-n-butyl phthalate 28.15 1176 30182Fluoranthene 30.45 1289 841735Pyrene 30.45 1289 841735
*d!2-Chrysene 34.28 1477 218938Benzidine 25.94 1067 70328Terphenyl-D14 (SURR) 31.11 1321 562601bis(2-Ethylhexyl)phthalate 34.79 1502 12913
*d!2-Perylene 38.58 1688 138889*'
40.00 UG/ML 86•wi.Q'i UC.rEIL 10085.94 UG/ML 87136.32 UG/ML 93131.94 UG/ML 90121.00 UG/ML 92?1. 7*6 UG/ML 8671.09 UG/ML 957?2,4l UC/ML 961IB.19 UG/ML 7870.11 UG/ML 7416.31 tJG/ML ' 38'.944 OG/ML 86..7 0 U&^ML 9440.00 UG/ML 9471.03 UG/ML 9276.58 UG/ML 94.SSS> UC TIL 923.83 UG/ML 87i1JJ UG/ML 83
154.60 UG/ML 1001.09 US/ML 10040.00 UG/ML 9562.23 UG/ML 94•.Plrt UCfML 7567.43 UG/ML 9992.10 UG/ML 82201.48 UG/ML 100T206 U6*'ML 951.11 UC/ML 82
127.91 UG/ML 9540.00 UG/ML 99
177.52 UG/ML 97•4~&L-LLG/ML 962.13 UG/ML 98
01.56 UB/'ML 9781.39 UG/ML 9740.00 UG/ML 96
i74.?6 UB^IIL 10071.55 UG/ML 92
2.65 UG/ML 8840 .00 UG/ML 84
* Compound is ISTD
ETC
r>ESTXOXDE/E»GB DATA
210
ETC
QC
211
2FSOIL PESTICIDE SURROGATE RECOVERY
Lab Name: ETCNJ Contract:
Lab Code: Case No.: SAS No.:
Level : (LOIO/MED)LQW
SDG No
EPASAMPLE NO.
PBLK01A4376A4377A4377SA4377R
SIf DBC ) #
9290619286
OTHER TOTOUT
00000
1I
010203040506070809101112131415161718192021222324252627282930
SI lDBC) " Dibutylchlorendate
ADUISORYOC LIMITS(20-150)
page 1 of
# Column to be used to flag recovery values* Ualues outside OC l i m i t sD S u r r o g a t e s d i l u t e d o u t
FORM II PEST-2 Rev
3FSOIL PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOUERY
Lab Name: ETCNJ Contract:
Lab Code: Case No.: SAS No.: SDG No.:
Ma t r i x Spike - EPA Sample No.: A4377 Leva1:(LOW/MED) LOU
COMPOUND
qamma -BHCCLindane 3Hep t ach lorAldr inDie Idr inEndr in4.4--DDT
SPIKEADDED(ug/Kg)
63.41763.41763.417158.541158.541158.541
SAMPLECONCENTRATION
tug/Kg)
.142
.4500. 0001.542
"*1C
1.076
MSCONCENTRATION
(ug/Kg )
59.68849.97648.955139. 172ICO 4. Q 1
MS t OCS ILIMITS
REC *l REC.
94 146-12778 135-13077 134-13287 131-13496 142-139101 123-134
1
111 COMPOUND
i aamma-BHCCLi ndane )1 Hept ach lor1 A l d r i n1 Die Idr int Endrin1 4.4--DDT1
SPIKEADDED(ug/Kg)
63.36663.36663.366158.416158.416158.416
MSD 1CONCENTRATION!
(ug/Kg) 1
57.679 148.201 147.645 1144.921 1150.354 1147.751 1
1
MSDsREC *
91757591
\RPD *
3434
95 1 193 1 8
QCRPD
503143384550
1LIMITS 1
1 REC. 1
146-1271135-1301134-132 1131-1341142-139 1123-13411 1
# Column to be used to flag recovery and RPD values with an asterisk
* Ualues outside of l i m i t s
RPD: 0 out of 6 outside limitsSpike Recovery: 0 out of 12 outside limits
Commen t s : ____________________________________________________ _..
FORM III PEST-2 1/87 Rev.
213
4CPESTICIDE METHOD BLANK SUMMARY
Lab Name: ETCNJ
Lab Code: Case No.
Lab Sample ID: PBLK01
Matrix: (soil/water) SOIL
Date Extracted: 08/30/90
Date Analyzed CU: 09/05/90
Time Analyzed CD: 1239
Inst rument ID CD: QA
GC Column ID (1): DB608
Cont rac t :
SAS No.: SDG No.:
Lab Fil e ID: >QA191
Leve1:(low/med) LOW
Extract ion: CSepF/Cont/Sonc) SONC
Date Analyzed C2):
Time Analyzed (2):
Instrument ID (2):
GC Column ID (2):
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:
0102030405D60708091011121314151617181920212223242526
EPASAMPLE NO.
A4376A4377A4377SA4377R
LABSAMPLE ID
CA4376GCA4377GCA4377GSCA4377GR
DATEANALYZED 1
09/05/9009/05/9009/05/9009/05/90
DATEANALYZED 2
Commen t
page 1 ofFORM IU PEST 1/87 Re<
214
ETC
DATA
215
IDPESTICIDE ORGAN ICS ANALYSIS DATA SHEET
Lab Name: ETCNJ Cont ract:
ERA SAMPLE NO
IA4376
Lab Code: Case No.: SAS No.: SDG No.:
Matrix: (soil/water) SOIL Lab Sample ID: CA4376G
Sample wt/vol: 30.0 Ig/mL) G Lab File ID: >QA193
Leve1: (low/med) LOU Date Received:
Moisture: not dec. 18 dec
Extract ion: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) N pH: 7.0
Date Extracted: 06/30/90
Date Analyzed: 09/05/90
D i l u t i o n Factor: 0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/kg) UG/KG
319-64-6--- ———— alpha-BHC________319-65-7- —————— beta-BHC_________319-86-8 —— - ——— delta-BHC________58-89-9----——--gamma-BHCCLxndane).76-44-8---------Heptach1 or________309-00-2 ——————— Aldnn___________1024-57-3---—--Heptachlor epoxide959-98-8——————Endosulfan I______60-57-l---~-----Dieldrin_________72-55-9 ———————— 4,4'-DDE_________72-2G-8---------Endrin___________33213-65-9 ————— Endosulfan II_____72-54-8 ———————— 4,4'-DDD_________1031-07-8——--—Endosulfan sulfate50-29-3 ———————— 4,4'-DDT__________72-43-5——--——Methoxychlor______53494-70-5--—--Endrin ketone_____5103-71-9 —————— alpha-Chlordane___5103-74-2-------gamma-Ch1o rdane___8Q01-35-2-------Toxaphene________12674-11-2*-———Aroclor-1016______11104-28-2*- ——— Ar o c I or-1221______11141-16-5 ————— Aroclor-1232______53469-21-9 ————— Aroc lor-1242______12672-29-6--——-Aroclor-1248______11097-69-1 ————— Aroc lor-1254______11096-82-5 ————— Aroc lor-1260______
9.8009.8009.800
800800800800soo
19.4019.4019.4019.4019.4019.4019.409819.4019,4019.401909896989898194194
Q
IIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI UIUIUIUIUI UIUIUIUIUIU
FORM I PEST 1/87 Re-
216
rile >QR193 l.B uu.48B
H4376 ,7 ,18
neeee*
leeBBBfr
eeeeee
seeeee
aeeee*
iseeCR43766 ,0678246 ,S 16
eeee
84 86 38
Data File: >QA193::U6 Quant Output FileName: A4376,7,19 Instrument IDdisc: CA43 76G , QG70 2 46 , S : G3 , 24 . 6 3 , 2 0
QA
Id File: I223QA::USTit le: IFBXPSTXPCB QA DB6 08Leet Cal ibrat ion: 900906 15:13
Operator ID: RLJ8206Quant Time: 900906 16:90Injected at: 900905 14:00
2ul INJ.
217
QUANT REPORT
Operator ID: RUJB206Output File: *QA193::AQData File: >QA193::U6Name: A4376,7,18flisc: CA4376G,QG70246, S:G3,24.63,20
Quant Rev: 7
ID File: I223QA::USTitle: IFB/PST/PCB QALast Calibration: 900906
Compound
DB608
Quant Time!In jected at:
Dilution Factor:Inst rument ID
2ul INJ.
Page 1
900906 16:90900909 14:00
1.00000
R.T. Scant Height Cone Units
19) #Dibutylchlorendate
t Compound uaes ESTD
30.55 1833 322434 .180 UG/ML 100
218
IDPESTICIDE ORGANICS ANALYSIS DATA SHEET
ERA SAMPLE NO.
Lab Name: ETCNJ
Lab Code: Case No.:
Matrix: (soil/water) SOIL
Samplewt/vol: 30.0 C g/mL) G
Level: (low/med) LOUJ
^Moisture: not dec. 16 dec.
Extraction: CSepF/Cont/SoncJ SONC
GPC Cleanup: (Y/N) N pH: 7.0
Con t rac t:
SAS No.:
. IA4377I
SDG No.:
Lab Sample ID: CA4377G
Lab File ID: >QA194
Date Received:
Date Extracted: 08/30/90
Date Analyzed: 09/05/90
Di lut ion Factor: 0
CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UG/KG
FORM I PEST
Q
319-64-6 -----319-65-7 ————319-86-8 ————58-89-9 ----- -76-44-8 -----309-00-2 -----1024-57-3 ———959-98-8 ————60-57-1 —————72-55-9 ------72-20-8-- ----33213-65-9 ——72-54-8 —————1031-07-8 ———50-29-3 —————72-43-5 ------53494-70-5 - —5103-71-9 -- —5103-74-2 ———8001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 - —53469-21-9 ——12672-29-6 ——11097-69-1---11096-82-5 ——
—— alpha-BHC—— beta-BHC—— delta-BHC---qamma-BHC CL indane )---Hept ach lor— -Aldr in---Heptachlor epoxide---Endosulfan I---Die Idr in—— 4.4'-DDE---Endr in---Endosulfan II—— 4.4'-DDD---Endosulfan sulfate—— 4.4--DDT---Methoxvchlor---Endr in ketone---alpha-Chlordane---oamma-Ch lordane---Toxaphene— -Aroclor-1016— -Aroclor-1221—— Aroclor-1232— -Aroclor-1242---Aroc lor-1248---Aroc lor-1254- — Aroc lor-1260
I19.60019.600(9.60019.60019.60019.60019.60019.6001 19. 00119.001 19. 001 19. 001 19. 00119. 001 19. 001961 19. 0019.60019.6001 1901961961961 Orf.
1961 1901 1901
1IU1LJIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIU1
1/87 Rev
219
CHROMfiTOeRflMFile >Qfll94 1.0 «mu. B4377,7,16 CR43776,067^46,
400 800 ieee ieee 2000
1300000-
1100000-
1000004
900090!
700004
600004
D00004
380000:
**4*ee
Data File: >QA194::U6 Quant Output File: "QA194::AQName: £4377,7,16 Instrument ID: QAMisc: CA4377G,QG70246,S:G3,25.22,20
Id File: I223QA::USTi t le : IFB/PST/PCB QA DB606Last Calibration: 900906 19:13
Operator ID: RUI8206Quant Time: 900906 16:92Injected at: 900906 14:40
2ul INJ.
220
QUANT REPORT
Operator ID: RUJ8206Output File: ~QA194::AQData File: >QA194: :U6Name: A4377,7,16Misc: CA4377G,QG70246,S:G3,25.22,20
Quant Rev: 7
ID F i l e : I223QA::USTitle: IFB/PST/PCB QA DB608Last C a l i b r a t i o n : 900906 15:13
Compound
Quant TimeInjected at
Di l u t i o n FactorInstrument ID
2ul INJ.
Page 1
900906 16:52900905 14:40
1.00000QA
R.T. Scan* Height Cone Units
19) *DibutyIchlorendate
# Compound uses ESTD
30.55 1633 289921 .162 UG/ML 100
221
ETC
S TAN D ARD S D AT A.
222
8DPESTICIDE EUALUATION STANDARDS SUMMARY
Lab Name:ETCNJ Contract:
Lab Code: Case No.: SAS No.: SDG No.:
Instrument ID: QA GC Column ID: DB608
Dates of Analyses: 09/04/90 to 09/05/90
Evaluation Check for Linearity
PESTICIDE
ALDRINENDRIN4.4'-DDTDEC
1 CALIBRATION1 FACTORt EUAL MIX A
1 3500800.51 2115200.5
_l 1782400.21 1506150.21
CALIBRATIONFACTOR
EUAL MIX B
3409940.52093450.01754250.01417600.0
CALIBRATIONFACTOR
EvAL MIX C*
3299860.01951690.01616010.01238405.0
% RSD( </-10. OS)
3.04.35.29.B
(1) If > 10.OS RSD, plot a standard curve and determine the ngfor each sample in that set from the curve.
Evaluation Check for 4,4'-DDT/Endrin Breakdown(percent breakdown expressed as total degradation)
0102030405060708091011121314
INITIALEvAL MIX B•EUAL MIX BEUAL MIX B'EUAL MIX BEvAL MIX BEUAL MIX BEUAL MIX BEv-AL MIX BEvAL MIX BEUAL MIX BEvAL MIX BEUAL MIX BEUAL MIX BEUAL MIX B
DATEANALYZED
09/04/9009/05/9009/05/90
TIMEANALYZED
174605151320
ENDRIN
6.08.76.8
4,4'-DDT'
8.411.99.7
COMBINED(2)
(2) See form instructions.
FORM v I I I PEST-1
I ll)
1/67 Rev,
223
BEPESTICIDE EVALUATION FOR STANDARDS SUMMARY
Evaluation of Retention Time Shift for Dibutylchlorendate
Lab NameiETCNJ
Lab Code : Case No.:
Inst rument ID: QA
Cant ract:
SAS No.: SDG No
GC Column ID:DB6Q8
Dates of Analyses: 09/04/90 to 09/05/90
1 EPA 1 LAB SAMPLE1 SAMPLE NO. 1 ID1. ......... | ............
OllEVALA IEUALAQ2IE'JALB IEVALB03IE'JALC IEVALC041 INDA 1 INDA051 INDB 1 INDB06ITOXAPHENE 1 TOXAPHENE07IAR1016 IAR101608IAR1221 IAR122109IAR1232 IAR123210IAR1242 IAR124211IAR1248 IAR124B12 IAR1254 1AR125413IAR1260 IAR126014IPBLK01 IQC7Q223G151 A4639 ICA4639G16IA4459 ICA4459G17IA4460 ICA4460G181A4460S ICA4460GS19IEUALB IEUALB201A4460R ICA4460GR21IA4477 1CA4477G22IA4528 ICA4528G23IPBLK01 IQC7023424IA4714 ICA4714G251 INDA 1 INDA26IA4717 1CA4717G27IA4674 ICA4674G28 1 A4674S 1 CA4674GS29 1 A4674R 1 CA4674GR3QIPBLKQ1 IQC70246G31 IEUALB IEUALB32IA4376 ICA4376G33IA4377 1 CA4/77G34 1 A4377S 1 CA4377GS351A4377R ICA4377GR361 INDA 1 INDA371 INDB 1 INDB38 1 1
DATEANALYZED
09/04/9009/04/9009/04/9009/04/9009/04/9009/04/9009/04/9009/04/9009/04/9009/04/9009/04/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/9009/05/90
TIMEANALYZED*
1706174618261907194720272108214822292309235000300111015102320312035304340515055506360716075608370917095710381118115912391320140014401520160116411722
*D
0. 00.00.00. 00.0.1
0.00.00. 00.00.0.1
1.00.00.00.00.00.00.00. 00.00.00.00.00.00.00.00.00.00.00.0.1.1.1.1.1.1
*
Ua lues outside of QC l i m i t s0.3S for capillary columns)
(2.OK fcr packed columns,
page 1 ofFORM <JI!I PEST-2 1/87 Re224
PESTICIDE/PCS STANDARDS SUMMARY
Lab Name: ETCNJ
Lab Code:
Inst rument ID: QA
Case No.:
Cont ract:
SAS No.: SDG No.:
GC Column ID: DB608
11 COMPOUNDII----""------*lalpha-BHCIbeta-BHC1 de Ita-BHC1 g a mma - BHC ___1 Hept ach 1 or __lAldnn1 Hep t . epox ide1 Endosu 1 fan I_1 Die Id r in _____14. 4 '-DDE1 Endr in1 Endosu 1 fan I II4T4'-DDD1 Endo . su 1 f ate_I4,4'-DDT ____Itlethoxych 1 or__lEndrin ketonela. Ch lordaneIg. Chlordane_1 Toxaphene1 Aroclor-10161 Aroclor-1221_1 Aroclor-1232_1 Aroclor-1242_1 Aroclor-12481 Aroclor-1254I Aroclor-126Q_1
DATECS) OF FROM: 09/04/90ANALYSIS TO: 09/05/90TIMECS) OF FROM: 19 07ANALYSIS TO: 01 11
RT
6.478.5210.408.179.7211.4815.0217.3219.5519.4022.2323.7323.7327.4726.0333.6733.5517.2316.0823.959.856.328.079.8515.6820.4334.00
RTUIINDOU
FROM 1 TO
6.461 6.488.501 8.5310.381 10.428.151 8.189.701 9.73
11.451 11.5114.991 15.0517.291 17.3519.521 19.5819.361 19.4422.201 22.2723.701 23.7623.701 23.7727.431 27.5025.981 26. OB33.641 33.7033.501 33.6017.211 17.2616.061 16.1123.911 23.999.841 9.866.311 6.338.051 8.089.841 9.8615.661 15.7120.401 20.4633.951 34.05
1
*
CALIBRATIONFACTOR
404610121457602539340353974030221002411520203136017318401726090160577013498201687050117184011878401095680704132134016023334402319360313922374401372169248420697610828815449768994
DATE OF ANALYSIS 09/05/90TIME OF ANALYSIS 0917EPA SAMPLE NO.(STANDARD) INDA
RT CALIBRATIONFACTOR
8.179.7211.4815.0217.3219.55
23.73
26.0533.67
397314133408202650041221440019392011877130
1826570
1166080744762
1QNTY/N
YYYYYY
Y
YY
\D
12.210.59.99.012.08.8
3.3
6.45.8
Under QNT Y/N:HD must be lessor equal to 20.
enter Y i.f quantitation was performed, N if not performed.than c/r equal to 15. OS for quantitation, and less than
OX for confirmation.
Determining that no compounds were found above the CRQLquantitation, and therefore at least one column must meet theNote: is a form of
15.OS criteria
For mu,Licomponent analytes, the single largest peak that is characteristicof the component should be used to establish <~e^ention time and SD.Identification of such analytes is based prim^-ily on pattern recognition.
page 1 of FORM IX PEST 1/87 Rev
225
PESTICIDE/PCB STANDARDS SUMMARY
Lab Name: ETCNJ
Lab Code:
Instrument ID: QA
Case No.:
Cont ract
SAS No. SDG No
GC Column ID: DB608
11 COMPOUND1
1 alpha-BHC!h«ta-BHCIdel ta-BHC1 gamma-BHC ____1 Heptach lor __1 A l d r i n1 Hep t . epox idelEndosulfan I_I Die Idr in ____14. 4 '-DDE1 Endr i n1 Endosu 1 fan II1 4r4'-DDDlEndo. aul fate1 4, 4 '-DOT ____1 Me t hoxych lor_lEndrin ketonela. Chlordane1 q t Ch lordaneI Toxaphene1 Aroclor-1016Ifcroc lor-12211 Aroclor-1232IAroclor-12421 Aroclor-1248I Aroclor-12541 Aroclor-12601
DATECSJ OF FROM: 09/.Q4/90ANALYSIS TO: 09/05/90TIME(S) OF FROM: 1907ANALYSIS TO: 0111
RT
6.478.5210.408.179.72
11.4815.0217.3219.5519.4022.2323.7323.7327.4726.0333.6733.5517.2316. 0823.959.856.328. 079.8515.6820.4334. 00
RTU1INDOUI
FROM TO
'6. 468.5010.388.159.7011.4514.9917.2919.5219.3622.2023.7023.7027.4325.9833.6433.5017.2116.0623.919.846.318.059.8415.6620.4033.95
6.488.5310.428.189.73
11.5115.0517.35
1 19.5819.4422.2723.7623.7727.5026. 0833.7033.6017.2616.1123.999.866.338.089.8615.7120.4634.05
*
CALIBRATIONFACTOR
40461012145760253934035397403022100241152020313601731840172609016057701349820168705011718401187840109568070413213401602333440231936031392237440137216924842069761082881544976B994
DATE OF ANALYSIS 09/05/90TIME OF ANALYSIS 1641EPA SAMPLE NO.(STANDARD) INDA
RT
8.179.72
11.4715. 0017.3019.53
23.75
26.0233.65
CALIBRATIONFACTOR
391632131667402608640227840015244801870730
QNTY/N
YYYYYY
1672970 1 Y1
1245940800852
YY
1
SD
10.64.88.212.212. 08.4
.6
13.713.7
Under QNT Y/N: enter Y if quantitation uiasSD must be less than rfr equal to 15.OH foror equal to 20.OS for confirmation.
performed, N if not performed,quantitation, and less than
Note: Determining that no compounds were found above the CRQL is a form ofquant itation, and therefore at least one column must meet the 15.OX criteria
For mu 11 i-umponent analytes, the single largest p<iak that is characteristicof the component should be used to establish retention tame and SfiD.I d e n t i f i c a t i o n of such analytes is based primani • on pelt tern recognition.
page 2 of FORM IX PEST 1/87 Rev
226
PESTICIDE/PCS STANDARDS SUMMARY
Lab Name: ETCNJ
Lab Code:
Instrument ID: QA
Case No.:
Cont ract:
SA5 No.: SDG No.:
GC Column ID: DB6G8
11 COMPOUND1!»»....«....»«lalpha-BHC ___Ibeta-BHC ____Idelta-BHC ___1 gamma-BHC ___IMeptachlorlAldrin1 Hept . epox i de1 Endosu 1 fan I1 Die Id pin ____14, 4 '-DDE ____lEndnn1 Endosu 1 fan I I14, 4 '-ODD ____1 Endo , su 1 f at e_I4.4--DDT1 Methoxych lor—lEndrin ketonela. Chlordane_Ig. Chlordane—1 Toxaphene1 Aroclor-1016lAroc lor-12211 Arodor-1232IAroclop-1242IAroclor-1248IAroclor-12541 Aroclor-1260_1
DATECS) OF FROM: 09x04/90ANALYSIS TO: 09x05/90TIME(S) OF FROM:1907ANALYSIS TO: 01 11
RT
6.478.5210.408.179.72
11.4815.0217.3219.5519.4022.2323.7323.7327.4726.0333.6733.5517.2316.0823.959.856.328.079.8515.6820.4334.00
RTLJ I NDOU
FROM 1 TO........ I......
6.46! 6.488.501 8.5310.381 10.428.151 8.189.701 9.7311.451 11.5114.991 15. 0517.291 17.3519.521 19.5819,361 19.4422.201 22.2723.701 23.7623.701 23.7727.431 27.5025.981 26.0833.641 33.7033.501 33.6017.211 17.2616.061 16. 1123.911 23,999.841 9.866.311 6.338.051 8.089.841 9.8615.661 15.7120.401 20.4633.951 34.05
1
CALIBRATIONFACTOR
404610121457602539340353974030221002411520203136017318401726090160577013498201687050117184011878401095680704132134016023334402319360313922374401372169248420697610828315449768994
DATE OF ANALYSIS 09/05/90TIME OF ANALYSIS 1722EPA SAMPLE NO.(STANDARD) INDB
RT
6.478.5210.40
19.3822.22
23.7227.45
33.5517.2316.08
CALIBRATIONFACTOR
392834120787202479201
15705701258880
11705601155840
13521102252800 .2234881
QNTY/N
YYY
YY
YY__
YYY
___
_. _ _
*D
2.93.12.4
2.26.7
.12.7
T?~3.53.6
_
Undep QNT Y/N: enter Y, if quantitation was performed, N if not performed.5fiD must be less than or equal to 15.Of for quantitation, and less thanor equal to 20.OS for confirmation.
Note: Determining that no compounds were found above the CRQL is a form ofquant i taf ' -••" , and therefore at least one co lumjL rr» •.•«*• meet the 15.OX criteria
For mu1ticomponent analytes, the single largest peak that is characteristicof the component should be used to establish retention time and 960.Identification of such analytes is based primarily on pat tern recognition.
page 3 of FORM IX PEST 1/87 Rev
227
CMROriPTOeRflttPile >QA16a l.e uu. EVRLR
.,..*?• ... •?• ,,EVBLR
232886-
228008-
224000-
220000.
aeeeee-
209099-
196000-
108000-
104000-
180006-
•••
LjJAj ——— -i • i • r • i • i0 IE 1«
i i • i • i • i •20 £4 B0 32
Data File: >QA162::U6Name: EUALAnisei EUALA
Id File: I223QA::USTitle: IFB/PST/PCB QA DB6 08Lest Calibration: 900906 19:13
Operator ID: RW8206Quant Time: 900906 16:06Injected at: 900904 17:06
Quant Output File: *QA162::AQInstrument ID: QA
2ul INJ
228
QUANT REPORT
Operator ID:Output Fi!•Data File:Name: EUALAnisc: EUALA
RU8206-QA162>QA162
QuantAQU6
7 Quent Time,Injected at
Di lut ton FactorInstrument ID
Page 1
900906 16:06900904 17:06
1.00000QA
ID File: I223QA::USTitle: IFB'PST/PCB QA DB608Last Calibration: 900906 19:13
Compound
2ul INJ.
R.T. Scan* Height Cone Units
6) #Aldrin13) tEndrin16) #4,4'-DOT19) tDibutylchlorendete
# Compound uses ESTD
11.90 690 3900622.25 1335 4230426.0? 1563 3564830.57 1834 30123
.00726 UG/ML 100.0157 UG/ML 100.0163 UGxnt 100.0168 UG/riL 100
KW)
229
Flit >QR163 1.6 MU. EVRLB EVRLB480 , 868 , 1500 t 1600 , 2000
420008-
400000-
380080-•
360*08-•
340600-
320066-
300000-
288066-
260088-
240000-
220000-•
200088-
188888-_l
&\
9v-
ML*.,M
___^AvJ——
j
ss
p£J
JU
58
.-gnnLJ^-
' 4 ' 8" ' 12 ' l'6 ' 86" ' 84 ' 88 ' 3'2 '
Date File: >Q«163::U6Name: EUAL8Misc: EUALB
Id File: I223QA::USTitle: IFB/PST/PCB QA DB6 08Last Calibration: 900906 19:13
Operator ID: RU8206Quant Time: 900906 16:08Injected at: 900904 17:46
Quant Output FileInstrument ID
2ul INJ
QA
2SO
QUANT REPORT
Operator ID: RUI8206Output File: "QA16?nAQData File: >QA163::U6Name: EUALBtlisc: EUALB
ID File: I223QA::USTitle: IFB/PST/PCB QALast Calibration! 900906
Compound
Quant Rev: 7 Quant TimeInjected et
Di lution FactorInstrument ID
Page 1
900906 16:06900904 17:46
1. 00000QA
DB608 2ul INJ.
R.T. Scant Height Cone Units
6)11)13)14)16)19)20)
•Aldrin*4,4'-DOE#Endr in#4, 4 '-ODD#4, 4 '-DOT#Dibutylch lorendate#Endrin ketone
11192223263033
.48
.42
.23
.77
.09
.57
.57
689116513341426156318342014
1704973008
2093451305617542514176013440
.0354.000937.0775.00557.0801.0792.00501
UG/MLUG/P1LUGxtILUG/MLUG/riLUG/MLUG/ML
10010U100100100100100
Compound uses ESTD
£>^ 111)96
231
CHROnPTOSRPMme >OP
680889-
66080*
SE0000-
400088;
360000-
32000fr
2B0000-
—*
164 1.8 UU. EVRLC EVRLC
400 088 1800 1688 2000.. . i ... T ... i - - T . .. i ... i ... i . . ~ i . . . i . . . i . .
_l
I
rw
<L ,.
•i
?
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ijr
->
5
_7L_' 4 ' 0" ' "l'2" ' l'6 ' 80 ' 84 ' 88 ' 38 '
Data File: >QA164::U6Name: EUALCnisc: EOALC
Id File: I225QA::USTitle: IFB/PSTxPCB QA OB606La»t Celibration: 900906 19:13
Operator ID: RU8206Quant Time: 900906 16:10Injected ati 900904 16:26
Quant Output File: AQA164::AQInstrument ID: QA
2ul INJ
232
QUANT REPORT
Operator ID: RUB206Output File: ~QA164::AQData File: >QA164::U6Name: EUALCMisc: EUALC
ID File: I223QA::USTitle: IFB/PST/PCB QA DB6QBLast Calibration: 900906 19:13
Compound
Quant Rev: 7 Quant Time:Injected at
Di lut ion Factor:Instrument ID
Page 1
900906 16:10900904 16:26
1.00000QA
2ul INJ
R.T. Scan* Height Cone Units
6) *Aldrin13) #Endrin16) #4,4'-DDT19) tDibutylchlorendate
* Compound uses ESTD
11.48 68922.23 133426.09 196230.57 1834
329986 .0684 UG/ML 100390338 .145 UG/fIL 100323202 .147 UG/ML 100247681 .138 UG/ML 100
233
CHROHPT09BPMFii« >oniee i.e uu. EVHLB EVHLB
4«e , eee , i ee , it.ee t eeeeaeeeee-aieeee-3e0ve»£90888-
aeeeee-
8se0ee-
eaeeee-seeeee-•eieeee-seeeee-iveeee-
H3»
L *O)
9S r
"
e
Lu
t
u
6
8^U-
1 i ' e ' i'2 ' i'6 ' e'e ' 84~ ' "g'e" ' "a'a" '
Data File: >QA18Q::U6Name: EUALBnisc: EUALB
Id File: I227QA::USTitle! IFBxPSTxPCB QA DB606Last Calibration: 900906 19:13
Operator ID: RLJ8206Quant Time: 900906 16:22.Injected ati 900909 09:15
Quant Output File: AQA160::AQInstrument ID: QA
2ul INJ
234
T REPORT
Operator ID:Output File:Data File:Name: EUALBriisc: EUALB
RU8206 Quant Rev: 7
>QA180: :U6
QUAN
Quant TimeInjected at
Di lut ion Factor:Instrument ID
Page 1
900906 16:22900905 05:15
1.00000QA
ID File: I223QA: : USTitle: IFB/PST/PCB QALast Calibration: 900906
Compound
DB60B 2ul INJ
R.T. Scan* Height Cone Units
6)11)13)14)16)19)20)
*Aldrin#4, 4 '-DDE#Endr in*4,4'-DDD#4)4 '-DOT*DifeutylchlorendatetEndrin ketone
11192223263033
.48
.45
.23
.75
.03
.57
.58
689116713341425156218342015
1075842496
12006410816986248979211402
.0223.000777.0445.00461.0450.0501.00425
UG/MLUC/HLUG/MLUG/T1LUG/MLUG/MLUG/ML
10010U100100100100100
Compound uses ESTD
235
CHROMPTOSRRnFlla >Qfll9a 1.6 MU.
.. «f ..
EVRLB EVflLB
E80000-
£60000-
246009-
seeeee-
Teeee
UA-
ee 24 ' £8
Data File: >QA192: :U6Nama: EUALB
EUALB
Id Fi la: I223QA: :UST 1 1 1 a : I FB/PST/PCB QALast Calibration: 900906
Operator ID: RU8206Quant Time: 900906 16:48Injected at: 900909 13:20
DB6 08
Quant Output File: ~QA192::AQInstrument ID: QA
2ul INJ.
236
QUANT REPORT
Operator ID:Output File:Da t a File:Name: EUALBtlisc: EUALB
RU8206^nAioo * • A OU|nX7& » * rlW
>QA192::U6
Quant Rev: 7 Quant TimeInjected at
Di lut ion Factor:Inst rument ID
Page 1
900906 16:4b900909 13:20
1.00000QA
ID File: I223QA::USTitle: IFB/PST/PCB QA D86 08Last Calibration: 900906 19:13
Compound
2ul INJ
R.T. Scant Height Cone Units
6)13)14)16)19)20)
•Aldnn#Endr in*4,4'-DDD#4, 4 '-DOTtDibuty Ich lorendate*Endr in ketone
112223263033
.47
.23
.80
.03
.57
.57
68813341426156218342014
114176130752
11712109100896009600
.0237
.0484.00500.0498.0500.00358
UG/MLUG/HLUG/MLUG/MLUG/MLUG/ML
1001QU10010U100iou
Compound uses ESTD
237
>OA165 1.8 a»u.
*C_INDR INDR
uaaaa*
leeeaee
eaaaea
saaea»
4eeea»
388889
aeaeefr' "i'6 ' s'a ea ss
Data File: >QA165::U6Name: INDAMisc: INDA
Id File: I223QA::USTi t le : IFB/PST/PCB QA DB6 06Lest Calibration! 900827 07:36
Operator ID: RU8206Quant Time: 900906 09:01Injected et: 900904 19:07
Quant Output File: ^QA165::AQInstrument ID: QA
2ul INJ
238
QUANT REPORT
Operator ID: RUJ6206Output File: ^QA165::AQData File: >QA165: : U6
Quant Rev: 7
Name: I NO AINDA
Quant Time!Injected at:
Di lution Factor:Instrument ID:
Page 1
900906 09:01900904 19:07
1.00000QA
ID File: I223QA::USTitle: IFB/PST/PCB QA DB60SLast Calibration: 900827 07:36
Compound
2ul INJ.
R.T. Scan* Height Cone Units
2)4)6)7)10)12)15)16)17)19)21)
#Gamma-BHCtHeptach lor*Aldrinfrleptachlor epoxidetEndosulfan I*D i e 1 d r i ntEndosulfan 1 1#4, 4 '-DOTtEndrin aldehydetDibutylchlorendatetflethoxych lor
8.9.11.15.17.
•- 19.23.26.26.30.33.
1772480232557303455767
490583689901
1039117314241562158718342020
1769871511051205761015688659217260916870510956811559089536352066
.0243
.0217
.0207
.0198
.0188
.0398
.0457
.0606
.0498
.0481.404
UG/MLUG/MLUG/rlLUGXMLuG/ni_UG/MLUG/MLUG/HLUG/MLUG/MLUG/ML
100100100100100100100100100100100
Compound uses ESTD
239
File >0fl
400000;
30000*
360000;
34000*
33000*
300000;
80000*
86000*
84000*
88000*
80000*
166 1.0 UU. INDB INDB
....«?• .....«.., ...W. . . . ."-•?. . . . .W.5«
.1. . i .
>
S
$o
id53
~
•5a Si
,
S r^
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•*8
1*
-
' 4 ' 0 ' 18 ' 16 ' a'0 84 ' 80 ' 38
Data Tile: >QA166: : U6Name: INDBMi»c: INDB
Id File: I223QA: :USTitle: IFBXPST/PCB QA DB60BLast Celibration: 900827 07:36
Quant Output FileInstrument ID
2ul INJ
QA
Operator ID:Quant Time:Injected at:
RU6206900906 09:03900904 19:47
240
Operator ID:Output File:Data Fi la:Name: INDBdisc: I NOB
RU8206
QUANT REPORT
Quant Rev: 7
>QA166: : U6
Quant Time!Injected at'
Di lut ion Factor:Instrument ID'
Page 1
900906 09:03900904 19:47
1.00000QA
itle: IFB/PST/PCB QA DB608 2u 1 INJ..aet Calibration: 900827 07:36
1)3)5)8)9)11)13)14)18)19)20)
Compound
tAlpha-BHCtBata-BHCtDelte-BHCtgamma-Ch lordanete. 1 pha-Ch^l o rdane#4,4' -DDE*#Endr in#4,4 '-DDD#Endoaulfan sulfatetDibuty Ich lorendate#Endr in ketone
R.
6.e.10.16.17.19.22.23.27.30.33.
T.
4752400623402373475755
Scant
3385116249651034116413341424164818342013
Height
20230510728812696711596811667216057713498211718411878499584134016
Cone
.0301
.0265
.0255
.0207
.0207
.0395
.0383
.0496
.0486
.0535
.0698
Units
UG/tlLUG/MLUG/MLUG/MLUGxntUG/MLUG/MLUG/MLUG/ni_UG/MLUG/HL
q
100100100100100100100100100100100
Compound uses ESTD
241
FH« > Oft 166 1.0 WU. INDR INDH
400 , 000 , 18,00 , 1*00 , £000
120888*
1100006
1000000
800000
70000*
««e.e»
B0000*
_ _ '40000*
30000*
1 ,
t>h
3
"i? 2 S ii J * 3 * * ~ ~ w $ r * .1 i £ S 3 | 1 v ° I
_ UillAJJI ' l ' i ' i ' i ' i " i • i • i ' i • i - i - i - i •
4 * 0 It 16 " 80 * £4 " 80 " 38
IDate File: >QA186:iU6Name: INOArii»c: INDA
Id Fila: I223QA::USTitle: IFB/PST/PCB QA DB6 08Last Calibration: 900906 19:13
Operator ID: RU8206Quant Timai 900906 16:33Injected at: 900909 09:17
Quant Output File: ~QA186::AQInstrument ID; QA
2ul INJ
242
QUANT REPORT
Operator ID:Output File:Da t e File:Name: INDAMisc: INDA
RU8206 Quant Rev: 7
>QA186: :U6
Quant Time!Injected at
Di lut ion FactoriInstrument ID:
Page 1
900906 16:77900905 09:17
1.00000QA
ID File: I223QA::USit liast
2)4)6)7)10)12)15)16)17)19)21)
9 : I FB/PSTxPCB QA DB6 08Calibration: 900906 15:13
Compound
#Gamma-BHCfHeptach lor*Aldrin•Hep tech lor epox ide#Endoaulfan ItDie Idr intEndosulfan II#4, 4 '-DOTtEndrin aldehyde•Dibuty Ich lorendatetrlethoxych lor
2ul IH
R.
e.9.11.15.17.19.23.26.26.30.33.
IJ.
T.
1772460232557305455767
Scan*
4905836899011039117314241563158718342020
Height
1986571670411325021107209696018771318265711660812158594336372381
Cone
.0281
.0276
.0275
.0273
.0280
.0544
.0541
.0532
.0526
.0527.264
Units
UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/nLUG/MLUG/MLUG/rlL
q10010010010010010010010U100100100
Compound uses ESTD
243
File >0fll97 1.0 aau.
1100»0»
IHDR
999999
999999
78098*
699999
999999
499999
399999
S9999+
£•00
4' ' ' t ' 18
Data File: >QA197::U6Name: INOAhiac: INDA
Id File: I223QA::USTitle: IFB/PST/PCB QA DB606Last Calibration: 900906 19:13
Operator ID: RUI8206Quant Time: 900906 16:59Injected at: 900909 16:41
Quant Output File: "QA197::AQInstrument ID: QA
2ul INJ
244
Operator ID:Output FilaiData File:Name: INDAMisci INDA
RU8206
QUANT REPORT
Quant Rev: 7
>QA197::U6
Quant Tima:Injectad at:
Di lut ion FactoriInstrument ID:
Page 1
900906 16:59900909 16:41
1.00000QA
'itl«.ast
2)4)6)7)10)12)15)16)17)19)21)
»: IFB/PST/PCB QA DB608Calibration: 900906 19:13
Compound
*Gamma-BHC#Heptach lorvAldrinftHeptachlor epoxidetEndosulfan ItDieldrintEndosulfan I I#4, 4 '-DOTtEndrin aldehydefDibuty Ich lorendeteftlethoxychlor
2ul IK
R.
6.9.11.15.17.19.23.26.26.30.33.
10.
T.
1772470030537502455565
Scan*
4905836889001038117214251561158718332019
Height
1958161583371304321139207622418707316729712459412537396448400426
Cone
.0277
.0262
.0270
.0280
.0220
.0542
.0496
.0569
.0542
.0539.284
Units
ue/ntUG/ntUG/MLUG/MLUG/MLUG/flLUG/rlLUG/MLUG/MLUG/MLUG/T1L
q100100100100100100100100100100100
* Compound uses E5TD
01/11/90
245
CHROtlRTOORfltlFill >QP
400906;
366696;
36090*
34990*
320090.
30099*
89099*
£6006*
84996*
88069*
20000*
196 1.0 UU. INDB INDB
i 4f° _i *f* i 13M i 16.*e i Miee
«••
&«
_ ^
$
IItj*
- gng £C
». * ,i
^
.,
?1
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*i 1? 9irt rv
- _A
|i\/ j *«**L1 4 ' B ' I'B ' 16 ' 89 ' 84 ' a'e ' a'e '
Data File: >QA19B::U6Name: INDBdisc: INDB
Id Fila; I223QA::USTitle: IFB/PST/PCB QA DB608Last Calibration: 900906 19:13
Operator ID: RU8206Quant Time: 900906 17:02Injected at: 900905 17:22
Quant Output File: AQA196::AQInstrument ID: QA
2ul INJ
246
Operator ID: RUI8206Output File: AQA198::AQData File: >QA198::U6Name: INDBMisc: INDB
QUANT REPORT
Quant Rev: 7 Quant Time;Injected at:
Oi lut ion Factor:Instrument ID:
Page 1
900906 17:02900905 17:22
1.00000QA
'it 1..ast
1)3)5)8)9)11)13)14)16)19)20)
B : I FB/PST/PCB QA DB6 08Calibration: 900906 15:13
Compound
*Alpha-BHC*Beta-BHC*Delta-BHC#gamma-Ch lordane*a Ipha-Ch lordane»4,4'-DDE#Endr in*4,4'-DDD#Endosu Ifan sulfatetDibuty Ich lorendatetEndrin ketone
2ul IN
R.
6.8.10.16.17.19.22.23.27.30.33.
Iw •
T.
4752400823382272455555
Scant
3B85116249651034116313331423164718332013
Height
19641710393612396011174411264015705712588811705611558495232135211
Cone
.0243
.0242
.0244
.0241
.0241
.0489
.0466
.0499
.0487
.0532
.0504
Units
UG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/MLUG/ML
q
10010010010010010010010010010U100
Compound uses ESTD
247
-DOD C -O*-- ft •
O ^ ft
• HOa «- Tft • «
O o 00
o o ofa ^k
tooo>O
toNJ
ft i- a
ft •-•O » —ft •- *n(T (D >-•-> \ Mft TJ M•» tf) W*•• -HOO S 3>3 -0 «" ODC>0 tf)oo(DOIO ^M
MO» Q)W (^OK o
O)
3 Z O~ a ft• 3 n 9 ft
O O —X X «
TJ-0I I vromozz »m m H»
M
i,-/
oC
• or* C-» •*C -D3 C
O«
DO
(KM
n> nt n» re M wm B» * »• w «• « CB * « a« o a a> a •» o o a> « •T.i.9.i.9.i.T.i.?.i.?,
ro^^oo
QUANT REPORT
Operator ID: RUI8206Output Fila: ^QA167::AQData Fila: >QA167::U6Name: TOXAPHENEtliac: TOXAPHENE
ID Fila: I223QA::USTitle: IFB/PST/PCB QA DB6 08Last Calibration: 900627 07:36
Compound
Quant 7 Quant Time:In jected ati
D i l u t ion Factor:Inst rument ID
Page 1
900906 09:06900904 20:27
1.00000QA
2ul INJ.
R.T. Scant Height Cone Units
19) tDibutylchlorendate22) tToxaphene23) #Toxaphene-224) #Toxaphene-3
# Compound uses ESTD
30.53 1832 13126523.95 1437 6278425.85 1551 3555127.47 1648 32704
.0706 UG/ML 100.796 UG/ML 100.696 UG/ML 100.779 UG/tlL 100
249
Flit >OR16B 1.0 aau.
. . . . 4**
aeeeee-
aeeeee-
S49999-
aeeeee-
RK1B16 RR1016
12 i t ee sa
Date Fi le= >QA166::U6Name: AR1016Misc: AR1016
Id File: I223QA::USTi t le : IFB/PST/PCB QA DB606Lest Calibration: 900827 07:36
Operator ID: RU8206Quant Time: 900906 09:08Injected at: 900904 21:06
Quant Output File: ~QA168::AQInstrument ID: QA
2ul INJ
250
QUANT REPORT
Operator ID:Output File:Da t a File:Name: AR1016nisc: AR1016
RU8206~QA168t:AQ>QA168i:U6
Quant 7 Quant Time;Injected at•
Di lut ion Factor:Instrument ID:
Page 1
900906 09:06900904 21:08
1.00000QA
ID File: I223QA: : USTitle: IFB/PST/PCB QA DB60BLast Calibration: 900827 07:36
2ul INJ.
Compound R.T. Scan* Height Cone Units
19)29)26)27)
ftDibutylchlorandate*Aroclor 1016*AR 1016-2*AR 1016-3
30.57 1834 1418B9 .0763 UG/ML 1009.85 591 118720 .265 UG/ML 1008.08 485 92711 .510 UG/ML 10013.60 816 39424 .204 UG/HL 100
Compound uses E5TD
251
CHROHflTOSRPn
KM*File >QH169 l.B «BU.
Data File: >QA169::U6Name: AR1221tlisc: AR1221
Id File: I223QA:lUSTitle: IFB/PST/PCB QA DB608La»t Calibrationi 900627 07:76
Op*rator ID: RU8206Quant Tima: 900906 09:10Injacted at: 900904 21:48
Quant Output File: ~QA169:iAQInstrument ID: QA
2ul 1NJ
252
QUANT REPORT
Operator ID:Output File:Da t a File:Name: AR1221rtisc: AR1221
RU8206AQA169::AQ>QA169::U6
Quant Raw: 7 Quant Time:In jected ati
Oi lut ion Factor:Instrument ID:
Page 1
900906 09:10900904 21:48
1.00000QA
ID File: I223QA::USTitle: IFB/PST/PCB QA DB608Last Calibration: 900827 07:36
Compound
2ul INJ
R.T. Scan* Height Cone Units
19) tDibutylchlorendate28) #Aroclor 122129) *AR 1221-230) *AR 1221-3
# Compound uses ESTD
50.57 1834 801926.32 379 686083.48 209 490565.52 331 31441
.0431 UG/ML 100.282 UG/HL 100.353 UG/ML 100.299 UG/ML 100
253
CHROnPTOORftttFi l* ><W170
270000
860000;
230000-
220000;
210000;
200000-
190000
MU. RR1232
S 9£
lil
AR1E32
1«00 B000
32
Data File: >QA170::U6Nam«: AR1232rii&c: AR1232
Id File: I223QA::USTitle: IFB/PST/PCB Qft DB6 06Last Calibration: 900627 07:36
Operator ID: RU6206Quant Time: 900906 09:11Injected at: 900904 22:29
Quant Output File: AQA17Q::AQInstrument ID: QA
2ul INJ
254
QUANT REPORT
Operator ID: RUI8206Output File: AQA170uAQData Ftle: >QA170i:U6Name: AR1232Misc: AR1232
ID File: I223QA::USTitle: IFB/PST/PCB QA DB608Last Calibration: 900827 07:36
Compound
Quant Rev: 7 Quant TimeInjactad at
Di lut ion Factor:Instrument ID
Page 1
900906 09:11900904 22:29
1.00000QA
2ul INJ.
R.T. Scant Height Cone Units
19) fDibutylchlorandate31) *Aroclor 123232) #AR 1232-233) *AR 1232-3
* Compound uses ESTD
30.57 1634 766088.07 484 462426.32 379 542239.85 591 53184
.0412 UG/'tlL 100.284 UG/tlL 100.278 UG/ML 100.281 UG/riL 100
255
CHROt1PT00RftHFilm >QA171 1.0 ABU.
£90000-
_ _ _ _ _ _RR1R48
870000;868000-zsaaae
eaaeee-
£08000-
19080^
T
£000
16 ee 84 eT 3E
Data File: >QA171::U6Natn«: AR1242flisc: AR1242
Id Fil.: I223QA::USTitle: IFB/PST/PCB QA DB608Leet Calibration: 900827 07136
Operator ID: RU6206Quant Time: 900906 09:13Injected ati 900904 23:09
Quant Output File: ~QA171::AQInstrument ID: QA
2ul INJ
256
Operator ID: RU8206Output File:Data File:Name: AR1242Miec: AR1242
QUANT REPORT
Quant Rev: 7
>QA171i:U6
Quant Time:Injected at:
Dilut ion Factor:Instrument ID:
Page 1
900906 09:13900904 23:09
1.00000QA
ID File: I223QA::USTitle: IFB/PST/PCB QA DB608Laat Calibration: 900627 07:36
Compound
2ul INJ.
R.T. Scan* Height Cone Units
19) #Dibutylchlorendate34) *Aroclor 124235) *AR 1242-236) «AR 1242-3
# Compound uses ESTD
30.57 1834 772489.85 591 1034888.08 465 619626.32 379 43506
.0415 UG/ML 100.673 UG/ML 100.583 UG/ML 100.153 UG/ML 100
257
CHROMPTOBRPnHR1E4B HR1E4B
live £000
Tilt >Qfll72 1.0 UU.
; • 0 - IE £4 38
Data Fi!•: >Qftl72::U6Name: AR124BMisc: AR1248
Id File: I223QA::USTitle: IFB/PST/PCB QA DB606.Last Calibration: 900827 07:36
;Operator ID: RU8206Quant Time: 900906 09:14Injected et: 900904 23:90
Quant Output File: ~QA172::AQInstrument ID: QA
2ul INJ
258
QUANT REPORT
Operator ID:Output Fi1«:Da t a File!Name: AR1246hi»c: AR1246
RU8206^QA172tlAQ>QA172:JU6
Quant Rev: 7 Quant Time:In jected at:
Dilution Factor:Instrument ID:
Page 1
900906 09:14900904 23:50
1.00000QA
ID File: I223QA::USTitle: IFB/PST/PCB QA DB608Last Calibration: 900627 07:36
2ul INJ.
Compound R.T. Scan* Height Cone Units
19)37)38)39)
*Dibutylchlorendate*Aroclor 1248*AR 1246-2*AR 1246-3
30.57 1834 7718415.68 941 541449.65 591 61024
13.62 817 49024
.0415 UG/ML 100.300 UG/ML 100.368 UG/ML 100.160 UG/ML 100
Compound uses E5TD
tiw
259
CHRQMPTOORftnnit >OAi73 i.o
360600
seoee*
seoeeoj
280000;
£60080;
84000*
aeoooo
38
Data Fila: >QA173::U6Name: AR1254Misc: AR1254
Id File: I223QA::USTi t le : IFB/PST/PCB QA DB608Lest Celibration: 900627 07:36
Operetor ID: RU6206Quant Time: 900906 09:16Injected at: 900909 00:30
Quant Output File: AQA17?::AQInstrument ID: QA
2ul INJ
260
QUANT REPORT
Operetor ID: RU6206Output File:Data File:Name: AR12v4Misc: AR1254
Quant Rev: 7
>QA173;:U6
Quant Time:Injected at
Di lution Factor!Instrument ID:
Page 1
90U?06 09:1690,0905 00:30
1.00000QA
ID File: I223QA::USTitle: IFB/PST/PCB QA DB608Last Calibration: 900827 07:36
Compound
2ul INJ
R.T. Scan* Height Cone Units
19) *Dibutylchlorendate40) tAroclor 129441) *AR 1254-242) *AR 1254-3
* Compound uses ESTO
30.55 1833 7910420.43 1226 15449725.85 1551 9913616.72 1003 135872
.0425 UG/ML 100.434 UG/ni_ 100.479 UG/ML 100.887 UG/ML 100
261
&80000;
£00880-
180000
Fll* >M174 1.0 uu.
366080;
340000-
32098*
30000*
RR1E6B
888 iqee 1«00 8008
r T12 16
Data Fi le:Name: AR1260Miftc: AR1260
: : U6
Id File: I223QA: :USTitle: I FB/PSTxPCB QA DB6 06Last Calibration: 900B27 07:36
Operator ID: RU6206Quant Time: 900906 09:16Injected at: 900909 01:11
Quant Output File: AQA174::AQInstrument ID: QA
2ul INJ
262
QUANT REPORT
Operator ID:Output File:Deta File:Name: AR1260disc: AR1260
RLJ8206~QA174:!AQ>QA174::U6
Quant Rev: 7 Quant Time!In jected at:
Di lut ion Factor iInst rument ID
Page 1
900906 09:18900905 01:11
1.00000QA
ID File: I223QA::USTitle: IFB/PST/PCB QA DB6 08Last Calibration: 900827 07:36
Compound
2ul INJ
R.T. Scan* Height Cone Un its
19) tDibutyIchlorendote43) *Aroclor 126044) #AR 1260-245) #AR 1260-3
$ Compound uses ESTD
30.25 1815 15264134.00 2040 6899422.50 1350 12659221.80 1308 114432
.0821 UG/ML 100. 184 UGXflL 100.541 UG/hL 100.413 UG/ML 10Q
263
ETC
RAW QC DATA
264
IDPESTICIDE ORGAN ICS ANALYSIS DATA SHEET
ERA SAMPLE NO-
PBLK01Lab Name: ETCNJ
Lab Code: Case No.:
flat r i x : (soil /water ) SOIL
Sample wt/vol: 30.0 (g/mL) G
Level: I low/mod) LOUI
Ktloisture: not dec. 0 dec.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) N pH:
Cont ract :
SAS No.:
I
SDG No.:
Lab Sample ID: QC7Q246G,
Lab File ID: >QA191
Date Rece ived:
Date Extracted: 06/30/90
Date Analyzed: 09/05/90
Di lut ion Factor: 0
CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg ) UG/KG
319-64-6 ——————— a Ipha-BHC________319-65-7———————beta-BHC_________319-66-8 —————— delta-BHC________56-89-9 ———— ——— gamma-BHC(Lindane).76-44-6 ——————— -Heptachlor_______309-00-2———————Aldrin___________1024-57-3 —————— Heptachlor epoxide.959-98-6 ——————— Endoaulfan I_____60-57-1 ———————— Dieldrin_________72-55-9 ———————— 4,4'-DDE_________72-20-8————————Endrin___________33213-65-9 ————— Endoaulfan II_____72-54-6 ———————— 4,4'-ODD_________1031-07-8-————EndosuIfan sulfate50-29-3————————4,4'-DOT__________72-43-5 ———————— Methoxychlor_____53494-70-5—————Endrin ketone_____5103-71-9 —————— alpha-Chlordane___5103-74-2-------gamma-Chlordane___B 001-35-2- ————— Toxapnene________12674-11-2—————Aroc lor-1016_____11104-26-2 ————— Aroc lor-1221_____11141-16-5—————Aroc lor-1232______53469-21-9 ————— Aroc lor-1242______12672-29-6 ————— Aroc lor-1246______11097-69-1 ————— Aroc lor-1254______11096-82-5 ————— Aroc lor-1260______
I1816161818161618I 16,116I 16116116I 161161801161816116016018018018018011601160I___
Q
IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI
FORM I PEST 1/87 Rev.
265
CHROrtflTOSPflMTile >Qfll91 l.e *nu. FBLK81 QC79£466 ,Q67ee46,Sif
laeeeee-leeeOOe-
iieeeeo-1800000-
980000-
888008-
700000-
600600-
560000-
400800-
380000-
eoeoee-
4ee , eee t i^ee ( isee , geee
L.1
I ift 1Jl II
i i • i • i i ' r ' r ' i ' p • i • i • P ' i ' r • r • i • 1 '4 e is 16 ae 24 es 32
Data File: >Qftl91::U6Name: PBLKQ1
Quant Output FileInstrument ID QA
hisc: QC70246G,QG70246,S:G3,30,20
Id File: I223QA::USTitle: IFB/PST/PCB QA DB608Last Calibration: 900906 15:13
Operator ID: RUI8206Quant Time: 900906 16:45Injected at: 900905 12:39
2ul INJ.
266
QUANT REPORT
Operator ID: RUB206Output Fi le: ~QA191: : AQData File: >QA191::U6Name: PBLK01Misc: QC70246G,QG70246,S:G3,30,20
ID File: I223QA::USTit le: IFB/PST/PCB QA D66Q6Last Calibration: 900906 15:13
Compound
Quant Rev: 7
2ul INJ
Quant Time:In jected at
Di lut ion Factor:Inst rument ID:
Page 1
900906 16:45900905 12:39
1 .00000
R.T. Scan* Height Cone Uni ts
19) *Dibutylchlorendete
# Compound uses ESTD
30.57 1834 329602 .164 UG/ttL 100
267
IDPESTICIDE ORGAN ICS ANALYSIS DATA SHEET
Lab Name: ETCNJ
LabCode: Case No.:
Mat r i x : (soil/water) SO IL
Samp 1 e wt /vo 1 : 30.0 C g--"mL) G
Le^e 1 : C low/mcd ) LDLJ
^ M o i s t u r e : not dec. 16 dec.
Ext ract ion: (SepF/Cont/Sonc) SQNC
GPC Cleanup: (Y-'H) N pH: 7.0
Lont ract:
SAS No.:
ERA SAMPLE NO
IIA4377SI______________
5DG. No.:
Lab Sample ID: CA4377GS
Lab F i l e ID: >QA195
Date Received:
Date Extracted: Q8--"3Q-'90
Date Analyzed: 09/05/90
Di1 u t ion Fac tor: 0
CAS NO. COMPOUNDCONCENTRATION UNITS:vug-''L or ug/Kg,1 UG/'KG
1 319-64-6--------alpha-BHC_________I 319-65-7-——----beta-BHC__________I 319-86-6-——----deIta-BHC_________I 58-39-9---------gamma-BHCCLindane).I 76-44-6---------Heptachlor________I 3 09-00-2-- ————— Aldr in____________I 1024-97-3-------Heptachlor epoxide.I 959-98-8-—— ——— Endosulfan I______I 60-57~l---------Dieldrin___________I 72-55-9-- ———— --4 ,4'-DDE__________I 72-20-6---------Endrin____________I 33213-65-9--——-Endosulfan II_____i 72-54-&---------4,4'-DDD__________I 1031-07-6-----—Endosulfan sulfate.I 50-29-3---------4,4'-DOT__________I 72-43-5---------tie thoxychlo r______I 53494-70-5----—Endrin ketone_____I 5103-71-9-------alpha-Chlordane___I 5103-74-2-------gamma-Chlo rdane___I 8001-35-2-------foxaphene_________I 12fc74-ll-2------Aroclor-1016______I 11104-2S-2------Aroclor-1221______1 11141-16-5------Aroclor-1232______I 5?469-21-9------«roclor-1242______i 12672-29-6------Aroclor-1246_______I 11097-69-1--——-Aroclor-1254_______I 11096-82-5------Aroclor-1260
9.6009.6009.6006050499.6009.60014019 . 0015319. 0019 . 0019. 01619619 . 009.600* . 6 0 01909696969696190190
Q
IUIUIU
IUIUIIUIIUIUIUIIUIUIUIUIUIUIUIUtut uIUIU
FORM 1 PEST 1/87 Re-
268
File >OR1?5 1.0 aau. fl4377S,7,l* CB43776S,oe7ee46,Sie
7800008;
aeeeeee-
,30000.
40e see i2ee i&ee aeee
*,JI
4
I 3 R -II ^s_IL/U_L A /I A . ^ A A• ( l l l ' I ' l • ! • ( • ! ' 1 ' I ' l ' ! ' I
B 12 16 80 24 26 32
Data File: >QA195::U6 Quant Output File: ~QA195::AQName: A4377S,7,16 Instrument ID: QAMisc: CA4377GS,QG70246,S:G3,25.23,20
Id File: I223QA::USTitle: IFB/PST/PCB QA DB6 OBLaat Calibration: 900906 15:13
Operator ID: RU18206Quant Time: 900906 16:54Injected at: 900905 15:20
2ul INJ.
269
QUflNT REPORT
Operator ID: RUB2Q6Output File: *QA195::AQData File: >QA195::U6Name: A4377S,7,16nisc: CA4377GS,QG70246,S:G3,25.23,2Q
Quant Rev: 7 Quant Time!In jected at:
Di lut ion Fac tor:Inst rument ID:
Page 1
900906 16:54900905 15:20
1.OOOOUQA
ID File: I223QA::USTitle: IFB/PST/PCB QA DB60SLast Calibrat ion: 900906 15:13
Compound
2ul IN3
R.T. Scan* Height Cone Un i ts
2)4)6)12)13)16)19)
#Gamma-BHCfc.Heptach lor*Aldr in#Die Idr in#Endr i n#4, 4 '-DOT$Dibutylchlorendate
8.9.11.19.22.26.30.
17724853230355
490583669
1172133415621833
533059381056297857606083520003444750328514
.0753
.0630
. 0616. 176. 193.203. 183
UG/MLUG/MLUG/ttLUG/MLUG/ttLUG/HLUG/ML
10010G100100100100100
Compound uses ESTD
270
IDPESTICIDE ORGANICS ANALYSIS DATA SHEET
Lab Name: ETCNJ Contract:
EPA SAMPLE NO
Lab Code: Case No.: SDG No.:
M a t r i x : I s o i l /water) SOIL
Samp le wt /vo 1 : 30.1 Ig/mL)
Leve 1 : t low/med J LOW
Lab Sample ID: CA4377GR
Lab Fi le ID: >QA196
Date Received:
^Moisture: not dec. 16 dec.
E x t r a c t i o n : (SepF/Cont /Sonc ) SONC
GPC Cleanup: CY/N) N pH: 7.0
Date Extracted: 08/30/90
Date Analyzed: 09/05/90
D i 1 u t ion Fac tor: 0
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kq) UG/KG
319-64-6--------alpha-BHC_________319-65-7- —————— bcta-BHC__________319-86-8———————delta-BHC_________58-89-9------—-gamma-BHCCLindane).76-44-8—----—-Heptachlor________309-00-2 ——————— A l d r in____________1024-57-3-------Heptachlor epoxide.959-98-8- —————— Endosu 1 fan I______60-57-l---------Dieldnn__________72-55-9———— ——— 4 ,4'-DDE__________72-2G-8—-------Endrin____________33213-65-9------Endosulfan I I_____72-54-e---------4,4'-ODD___________1031-07-8---——EndoauIfan sulfate.50-29-3 ——— ————4, 4'-DOT_________72-43-5---------Met hoxych1 or_______53494-70-5------Endrin ketone_____5103-71-9-------alpha-Chlordane___5103-74-2-------gamma-Ch1o rdene___8ClGl-35-2-------Toxaphene_________12674-ll-2------ttroclor-1016______11104-28-2------Aroclor-12 21______11141-16-5------Aroclor-1232______53469-2 1-9------Aroclor-1242______12672-29-6------Aroclor-1246______11097-69-1 —————— Aroc lor-1254_______11096-82-5------Aroclor-1260 ____
9 . 6009.6009.6005875759.6009.6009119. 009519.19.19.939619.19.19.1909696969696190190
000000
000000
Q
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FORM I PEST 1/87 Rev
271
CHROHRTO&RfltlFi l e >QR156 1.6 MU. ft4377R,7,i6 CR43776R ,0678245,575
400 , see , 15*0 1600 goee
7888008;
6886000-
9000000|
4000000J
3000000-
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1000000-
A16 | - !ae 1 • 1as
Data File: >QA196::U6 Quant Output File: ~QA196::AQName: A4377R,7,16 Instrument ID: QAMisc: CA4377GR,QG70246,S:G3,25.25,20
Id File: I223QA::USTitle: IFB/PST/PCB Qft DB60BLast Calibration: 900906 15:13
Operator ID: RU8206Quant Time: 900906 16:57Injected at: 900905 16:01
2ul INJ.
272
QUANT REPORT
Operator ID: RUS206Output File: ~QA196::AQData File: >QA196::U6Name: A4377R,7,16Misc: CA4377GR,QG70246,S:G3,25.25,2Q
Quant Rev: 7 Quant Time:Injected at
Di lut ion Factor:Inst rumen t ID
Page 1
900906 16:57900905 16:01
1. 00000QA
ID File: I223QA::USTitle: IFB/PST/PCB QA DB6 08Last Calibration: 900906 15:13
Compound
2ul INJ
R.T. Scan* Height Cone Uni ts
2)4)6)12)13)16)19)
£Gamma-BHC#Hept ach lor*Aldrin#D ie Idr in#Endr in#4,4'-DDT$Dibut ylchlorendate
891119222630
.17
.72
.46
.53
.23
.03
.55
490583689
1172133415621833
51552336781029011363.1619512451408766308738
.0728
. 0609
. 0602. 183.190.187.172
UG/tlLUG/MLUG/MLUG/tlLUG/tILUG/flLUG/ML
100100100100100100100
Compound uses ESTD
273
ETC
CHAIN OF CUSTODY
274
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<^ETC FIELD PARAMETER FORM (CC2)* ' 12/89
1 1PURGE DA(VY MM D
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