analytical report 6 - 3348 south street report testamerica laboratories, inc. ... method: 200.7 rev...

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Savannah5102 LaRoche AvenueSavannah, GA 31404Tel: (912)354-7858

TestAmerica Job ID: 680-146495-2Client Project/Site: South Street Site

For:GFA International Inc5851 Country Lakes DriveFort Myers, Florida 33905-5504

Attn: Scott McManus

Authorized for release by:12/21/2017 4:32:05 PM

Noel Savoie, Project Manager I(850)[email protected]

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Definitions/GlossaryTestAmerica Job ID: 680-146495-2Client: GFA International Inc

Project/Site: South Street Site

Qualifiers

Metals

Qualifier Description

U Indicates that the compound was analyzed for but not detected.

Qualifier

I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.

General Chemistry

Qualifier Description

U Indicates that the compound was analyzed for but not detected.

Qualifier

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains No Free Liquid

DER Duplicate Error Ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL Detection Limit (DoD/DOE)

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision Level Concentration (Radiochemistry)

EDL Estimated Detection Limit (Dioxin)

LOD Limit of Detection (DoD/DOE)

LOQ Limit of Quantitation (DoD/DOE)

MDA Minimum Detectable Activity (Radiochemistry)

MDC Minimum Detectable Concentration (Radiochemistry)

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not Detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative Error Ratio (Radiochemistry)

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TestAmerica Savannah

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Sample SummaryTestAmerica Job ID: 680-146495-2Client: GFA International Inc


Lab Sample ID Client Sample ID ReceivedCollectedMatrix

680-146495-5 MW-2 Water 12/05/17 08:20 12/07/17 09:15

680-146495-6 MW-3 Water 12/05/17 09:28 12/07/17 09:15

680-146495-7 MW-4 Water 12/05/17 10:35 12/07/17 09:15

680-146495-8 MW-6 Water 12/05/17 11:48 12/07/17 09:15

680-146495-9 MW-5 Water 12/05/17 13:38 12/07/17 09:15

680-146495-10 Field Blank Water 12/05/17 10:50 12/07/17 09:15


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Case NarrativeClient: GFA International Inc TestAmerica Job ID: 680-146495-2Project/Site: South Street Site

Job ID: 680-146495-2

Laboratory: TestAmerica Savannah

Narrative

Job Narrative680-146495-2

Comments

Samples collected on 12/4/17 is reported on job 680-146495-1.

Receipt

The samples were received on 12/7/2017 9:15 AM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperature of the cooler at receipt was 2.6º C.

Metals No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

General Chemistry No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

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Client Sample ResultsTestAmerica Job ID: 680-146495-2Client: GFA International Inc


Lab Sample ID: 680-146495-5Client Sample ID: MW-2Matrix: WaterDate Collected: 12/05/17 08:20

Date Received: 12/07/17 09:15

Method: 200.7 Rev 4.4 - Metals (ICP)PQL MDL

Aluminum 0.0240 U 0.200 0.0240 mg/L 12/11/17 15:07 12/12/17 21:45 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

0.0500 0.0170 mg/L 12/11/17 15:07 12/12/17 21:45 1Iron 4.13

0.0100 0.00100 mg/L 12/11/17 15:07 12/12/17 21:45 1Manganese 0.0516

Method: 200.8 - ICPMS Dissolved Metals by 200.8 - DissolvedPQL MDL

Dissolved Arsenic 0.0268 0.00100 0.000370 mg/L 12/12/17 11:42 12/12/17 20:18 1


Method: 200.8 - Metals (ICP/MS)PQL MDL

Arsenic 0.0258 0.00100 0.000370 mg/L 12/11/17 15:07 12/12/17 16:22 1


General ChemistryPQL MDL

Total Dissolved Solids 828 10.0 10.0 mg/L 12/11/17 16:17 1



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Aluminum 0.0240 U 0.200 0.0240 mg/L 12/11/17 15:07 12/12/17 21:56 1


0.0500 0.0170 mg/L 12/11/17 15:07 12/12/17 21:56 1Iron 2.21

0.0100 0.00100 mg/L 12/11/17 15:07 12/12/17 21:56 1Manganese 0.0376





Arsenic 0.0138 0.00100 0.000370 mg/L 12/11/17 15:07 12/12/17 16:32 1






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Aluminum 0.0482 I 0.200 0.0240 mg/L 12/11/17 15:07 12/12/17 20:48 1


0.0500 0.0170 mg/L 12/11/17 15:07 12/12/17 20:48 1Iron 5.97

0.0100 0.00100 mg/L 12/11/17 15:07 12/12/17 20:48 1Manganese 0.0275





Arsenic 0.00506 0.00100 0.000370 mg/L 12/11/17 15:07 12/12/17 15:40 1






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Aluminum 0.0240 U 0.200 0.0240 mg/L 12/11/17 15:07 12/12/17 21:30 1


0.0500 0.0170 mg/L 12/11/17 15:07 12/12/17 21:30 1Iron 1.21

0.0100 0.00100 mg/L 12/11/17 15:07 12/12/17 21:30 1Manganese 0.0849





Arsenic 0.00426 0.00100 0.000370 mg/L 12/11/17 15:07 12/12/17 16:18 1






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Aluminum 0.0240 U 0.200 0.0240 mg/L 12/11/17 15:07 12/12/17 21:04 1


0.0500 0.0170 mg/L 12/11/17 15:07 12/12/17 21:04 1Iron 2.32

0.0100 0.00100 mg/L 12/11/17 15:07 12/12/17 21:04 1Manganese 0.0461





Arsenic 0.0312 0.00100 0.000370 mg/L 12/11/17 15:07 12/12/17 16:00 1






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Lab Sample ID: 680-146495-10Client Sample ID: Field BlankMatrix: WaterDate Collected: 12/05/17 10:50



Antimony 0.000400 U 0.00100 0.000400 mg/L 12/20/17 11:50 12/20/17 18:04 1


0.00100 0.000370 mg/L 12/20/17 11:50 12/20/17 18:04 1Arsenic 0.000370 U

0.000400 0.000150 mg/L 12/20/17 11:50 12/20/17 18:04 1Beryllium 0.000150 U

0.000500 0.0000430 mg/L 12/20/17 11:50 12/20/17 18:04 1Cadmium 0.0000430 U

0.00200 0.00100 mg/L 12/20/17 11:50 12/20/17 18:04 1Chromium 0.00100 U

0.00500 0.000500 mg/L 12/20/17 11:50 12/20/17 18:04 1Copper 0.000500 U

0.000300 0.0000600 mg/L 12/20/17 11:50 12/20/17 18:04 1Lead 0.0000600 U

0.00100 0.000450 mg/L 12/20/17 11:50 12/20/17 18:04 1Molybdenum 0.000450 U

0.00500 0.000400 mg/L 12/20/17 11:50 12/20/17 18:04 1Nickel 0.000400 U

0.00200 0.000580 mg/L 12/20/17 11:50 12/20/17 18:04 1Selenium 0.000580 U

0.00100 0.000100 mg/L 12/20/17 11:50 12/20/17 18:04 1Silver 0.000100 U

0.000200 0.000100 mg/L 12/20/17 11:50 12/20/17 18:04 1Thallium 0.000100 U

0.0200 0.00280 mg/L 12/20/17 11:50 12/20/17 18:04 1Zinc 0.00280 U

Method: 245.1 - Mercury (CVAA)PQL MDL

Mercury 0.0000800 U 0.000200 0.0000800 mg/L 12/08/17 09:29 12/08/17 15:53 1



Total Dissolved Solids 36.0 5.00 5.00 mg/L 12/11/17 16:17 1



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QC Sample ResultsTestAmerica Job ID: 680-146495-2Client: GFA International Inc


Method: 200.7 Rev 4.4 - Metals (ICP)

Client Sample ID: Method BlankLab Sample ID: MB 680-505946/1-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 506233 Prep Batch: 505946

PQL MDL

Aluminum 0.0240 U 0.200 0.0240 mg/L 12/11/17 15:07 12/12/17 20:22 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

0.0170 U 0.01700.0500 mg/L 12/11/17 15:07 12/12/17 20:22 1Iron

0.00100 U 0.001000.0100 mg/L 12/11/17 15:07 12/12/17 20:22 1Manganese

Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-505946/2-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 506233 Prep Batch: 505946

Aluminum 2.00 2.015 mg/L 101 85 - 115

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Iron 2.00 2.049 mg/L 102 85 - 115

Manganese 0.200 0.2139 mg/L 107 85 - 115

Client Sample ID: MW-4Lab Sample ID: 680-146495-7 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 506233 Prep Batch: 505946

Aluminum 0.0482 I 2.00 2.195 mg/L 107 75 - 125

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Iron 5.97 2.00 7.920 mg/L 97 75 - 125

Manganese 0.0275 0.200 0.2411 mg/L 107 75 - 125

Client Sample ID: MW-4Lab Sample ID: 680-146495-7 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 506233 Prep Batch: 505946

Aluminum 0.0482 I 2.00 2.165 mg/L 106 75 - 125 1 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Iron 5.97 2.00 8.045 mg/L 104 75 - 125 2 20

Manganese 0.0275 0.200 0.2389 mg/L 106 75 - 125 1 20


Aluminum 0.0240 U 2.00 2.124 mg/L 106 75 - 125

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Iron 2.32 2.00 4.366 mg/L 102 75 - 125

Manganese 0.0461 0.200 0.2601 mg/L 107 75 - 125


Aluminum 0.0240 U 2.00 2.119 mg/L 106 75 - 125 0 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Iron 2.32 2.00 4.345 mg/L 101 75 - 125 0 20

Manganese 0.0461 0.200 0.2597 mg/L 107 75 - 125 0 20


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Method: 200.8 - Metals (ICP/MS)


PQL MDL

Arsenic 0.000370 U 0.00100 0.000370 mg/L 12/11/17 15:07 12/12/17 15:30 1

MB MB



Arsenic 0.0400 0.04191 mg/L 105 85 - 115

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Arsenic 0.00506 0.0400 0.04615 mg/L 103 70 - 130

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Arsenic 0.00506 0.0400 0.04515 mg/L 100 70 - 130 2 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


Arsenic 0.0312 0.0400 0.07116 mg/L 100 70 - 130

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Arsenic 0.0312 0.0400 0.07438 mg/L 108 70 - 130 4 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


PQL MDL

Antimony 0.000400 U 0.00100 0.000400 mg/L 12/20/17 11:50 12/20/17 16:49 1

MB MB


0.000370 U 0.0003700.00100 mg/L 12/20/17 11:50 12/20/17 16:49 1Arsenic

0.000150 U 0.0001500.000400 mg/L 12/20/17 11:50 12/20/17 16:49 1Beryllium

0.0000430 U 0.00004300.000500 mg/L 12/20/17 11:50 12/20/17 16:49 1Cadmium

0.00100 U 0.001000.00200 mg/L 12/20/17 11:50 12/20/17 16:49 1Chromium

0.000500 U 0.0005000.00500 mg/L 12/20/17 11:50 12/20/17 16:49 1Copper

0.0000600 U 0.00006000.000300 mg/L 12/20/17 11:50 12/20/17 16:49 1Lead


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Method: 200.8 - Metals (ICP/MS) (Continued)


PQL MDL

Molybdenum 0.000450 U 0.00100 0.000450 mg/L 12/20/17 11:50 12/20/17 16:49 1

MB MB


0.000400 U 0.0004000.00500 mg/L 12/20/17 11:50 12/20/17 16:49 1Nickel

0.000580 U 0.0005800.00200 mg/L 12/20/17 11:50 12/20/17 16:49 1Selenium

0.000100 U 0.0001000.00100 mg/L 12/20/17 11:50 12/20/17 16:49 1Silver

0.000100 U 0.0001000.000200 mg/L 12/20/17 11:50 12/20/17 16:49 1Thallium

0.00280 U 0.002800.0200 mg/L 12/20/17 11:50 12/20/17 16:49 1Zinc


Antimony 0.0200 0.02213 mg/L 111 85 - 115

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Arsenic 0.0400 0.04412 mg/L 110 85 - 115

Beryllium 0.0200 0.02229 mg/L 111 85 - 115

Cadmium 0.0200 0.02200 mg/L 110 85 - 115

Chromium 0.0400 0.04149 mg/L 104 85 - 115

Copper 0.0400 0.04430 mg/L 111 85 - 115

Lead 0.200 0.2121 mg/L 106 85 - 115

Molybdenum 0.0400 0.04274 mg/L 107 85 - 115

Nickel 0.0400 0.04453 mg/L 111 85 - 115

Selenium 0.0400 0.04225 mg/L 106 85 - 115

Silver 0.0200 0.02090 mg/L 105 85 - 115

Thallium 0.0160 0.01771 mg/L 111 85 - 115

Zinc 0.0400 0.04509 mg/L 113 85 - 115

Method: 200.8 - ICPMS Dissolved Metals by 200.8


PQL MDL

Dissolved Arsenic 0.000370 U 0.00100 0.000370 mg/L 12/12/17 11:42 12/12/17 19:02 1

MB MB



Dissolved Arsenic 0.0400 0.04157 mg/L 104 85 - 115

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


PQL MDL

Dissolved Arsenic 0.000370 U 0.00100 0.000370 mg/L 12/18/17 13:48 12/19/17 14:51 1

MB MB



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Method: 200.8 - ICPMS Dissolved Metals by 200.8 (Continued)


Dissolved Arsenic 0.0400 0.04302 mg/L 108 85 - 115

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Method: 245.1 - Mercury (CVAA)


PQL MDL

Mercury 0.0000800 U 0.000200 0.0000800 mg/L 12/08/17 09:29 12/08/17 15:06 1

MB MB



Mercury 0.00250 0.002443 mg/L 98 85 - 115

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Method: SM 2540C - Solids, Total Dissolved (TDS)

Client Sample ID: Method BlankLab Sample ID: MB 680-505965/1Matrix: Water Prep Type: Total/NAAnalysis Batch: 505965

PQL MDL

Total Dissolved Solids 5.00 U 5.00 5.00 mg/L 12/11/17 16:17 1

MB MB


Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-505965/2Matrix: Water Prep Type: Total/NAAnalysis Batch: 505965

Total Dissolved Solids 55.0 58.00 mg/L 105 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-505965/3Matrix: Water Prep Type: Total/NAAnalysis Batch: 505965

Total Dissolved Solids 55.0 59.00 mg/L 107 80 - 120 2 25

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD


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QC Association SummaryTestAmerica Job ID: 680-146495-2Client: GFA International Inc


Metals

Prep Batch: 505603

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 245.1680-146495-10 Field Blank Total/NA

Water 245.1MB 680-505603/13-A Method Blank Total/NA

Water 245.1LCS 680-505603/14-A Lab Control Sample Total/NA

Analysis Batch: 505859


Water 245.1 505603680-146495-10 Field Blank Total/NA

Water 245.1 505603MB 680-505603/13-A Method Blank Total/NA

Water 245.1 505603LCS 680-505603/14-A Lab Control Sample Total/NA

Prep Batch: 505943


Water 200680-146495-5 MW-2 Total/NA





Water 200MB 680-505943/1-A Method Blank Total/NA

Water 200LCS 680-505943/2-A Lab Control Sample Total/NA

Water 200680-146495-7 MS MW-4 Total/NA

Water 200680-146495-7 MSD MW-4 Total/NA



Prep Batch: 505946













Prep Batch: 506063


Water 200680-146495-5 MW-2 Dissolved





Water 200.8 506063680-146495-5 MW-2 Dissolved

Water 200.8 505943680-146495-5 MW-2 Total/NA

Water 200.8 505943680-146495-6 MW-3 Total/NA

Water 200.8 505943680-146495-7 MW-4 Total/NA

Water 200.8 505943680-146495-8 MW-6 Total/NA


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Metals (Continued)

Analysis Batch: 506216 (Continued)


Water 200.8 505943680-146495-9 MW-5 Total/NA





Water 200.8 505943680-146495-7 MS MW-4 Total/NA

Water 200.8 505943680-146495-7 MSD MW-4 Total/NA

Water 200.8 505943680-146495-9 MS MW-5 Total/NA

Water 200.8 505943680-146495-9 MSD MW-5 Total/NA



Water 200.7 Rev 4.4 505946680-146495-5 MW-2 Total/NA





Water 200.7 Rev 4.4 505946MB 680-505946/1-A Method Blank Total/NA

Water 200.7 Rev 4.4 505946LCS 680-505946/2-A Lab Control Sample Total/NA

Water 200.7 Rev 4.4 505946680-146495-7 MS MW-4 Total/NA

Water 200.7 Rev 4.4 505946680-146495-7 MSD MW-4 Total/NA

Water 200.7 Rev 4.4 505946680-146495-9 MS MW-5 Total/NA

Water 200.7 Rev 4.4 505946680-146495-9 MSD MW-5 Total/NA

Prep Batch: 506835
















Prep Batch: 507179


Water 200680-146495-10 Field Blank Total/NA





Water 200.8 507179680-146495-10 Field Blank Total/NA


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Metals (Continued)

Analysis Batch: 507334 (Continued)




General Chemistry



Water SM 2540C680-146495-5 MW-2 Total/NA





Water SM 2540C680-146495-10 Field Blank Total/NA

Water SM 2540CMB 680-505965/1 Method Blank Total/NA

Water SM 2540CLCS 680-505965/2 Lab Control Sample Total/NA

Water SM 2540CLCSD 680-505965/3 Lab Control Sample Dup Total/NA


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Lab ChronicleClient: GFA International Inc TestAmerica Job ID: 680-146495-2Project/Site: South Street Site

Client Sample ID: MW-2 Lab Sample ID: 680-146495-5Matrix: WaterDate Collected: 12/05/17 08:20


Prep 200 BJB12/11/17 15:07 TAL SAV505946

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 50 mL 50 mL

Analysis 200.7 Rev 4.4 1 506233 12/12/17 21:45 BWR TAL SAVTotal/NA

ICPEInstrument ID:

Prep 200 506063 12/12/17 11:42 AJR TAL SAVDissolved 50 mL 50 mL

Analysis 200.8 1 506216 12/12/17 20:18 BJB TAL SAVDissolved

ICPMSDInstrument ID:

Prep 200 505943 12/11/17 15:07 BJB TAL SAVTotal/NA 50 mL 50 mL

Analysis 200.8 1 506216 12/12/17 16:22 BJB TAL SAVTotal/NA


Analysis SM 2540C 1 505965 12/11/17 16:17 JEC TAL SAVTotal/NA 50 mL 100 mL

NOEQUIPInstrument ID:



Prep 200 BJB12/11/17 15:07 TAL SAV505946

Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil



ICPEInstrument ID:


Analysis 200.8 1 507075 12/19/17 15:50 BWR TAL SAVDissolved









Prep 200 BJB12/11/17 15:07 TAL SAV505946

Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil



ICPEInstrument ID:








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Analysis SM 2540C JEC12/11/17 16:171 TAL SAV505965

Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil





Prep 200 BJB12/11/17 15:07 TAL SAV505946

Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil



ICPEInstrument ID:











Prep 200 BJB12/11/17 15:07 TAL SAV505946

Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil



ICPEInstrument ID:









Client Sample ID: Field Blank Lab Sample ID: 680-146495-10Matrix: WaterDate Collected: 12/05/17 10:50


Prep 200 AJR12/20/17 11:50 TAL SAV507179

Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil



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Client Sample ID: Field Blank Lab Sample ID: 680-146495-10Matrix: WaterDate Collected: 12/05/17 10:50


Analysis 200.8 BWR12/20/17 18:041 TAL SAV507334

Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA


Prep 245.1 505603 12/08/17 09:29 NVF TAL SAVTotal/NA 50 mL 50 mL

Analysis 245.1 1 505859 12/08/17 15:53 NVF TAL SAVTotal/NA

LEEMAN2Instrument ID:



Laboratory References:

TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858


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Accreditation/Certification SummaryClient: GFA International Inc TestAmerica Job ID: 680-146495-2Project/Site: South Street Site

Laboratory: TestAmerica SavannahThe accreditations/certifications listed below are applicable to this report.

Authority Program EPA Region Identification Number Expiration Date

Florida E870524NELAP 06-30-18

Laboratory: TestAmerica TampaThe accreditations/certifications listed below are applicable to this report.

Authority Program EPA Region Identification Number Expiration Date

Florida E842824NELAP 06-30-18


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Method SummaryTestAmerica Job ID: 680-146495-2Client: GFA International Inc


Method Method Description LaboratoryProtocol

EPA200.7 Rev 4.4 Metals (ICP) TAL SAV

EPA200.8 Metals (ICP/MS) TAL SAV

EPA200.8 ICPMS Dissolved Metals by 200.8 TAL SAV

EPA245.1 Mercury (CVAA) TAL SAV

SMSM 2540C Solids, Total Dissolved (TDS) TAL SAV

Protocol References:

EPA = US Environmental Protection Agency

SM = "Standard Methods For The Examination Of Water And Wastewater",

Laboratory References:

TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858


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Login Sample Receipt Checklist

Client: GFA International Inc Job Number: 680-146495-2

Login Number: 146495

Question Answer Comment

Creator: Edwards, Jessica R

List Source: TestAmerica Savannah

List Number: 1

N/ARadioactivity wasn't checked or is </= background as measured by a survey meter.

TrueThe cooler's custody seal, if present, is intact.

TrueSample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time (excluding tests with immediate HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

N/ASample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.

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analytical report 6 - 3348 south street report testamerica laboratories, inc. ... method: 200.7 rev...

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