anama package & container testing services, inc. 2019.6.19.pdf · anama packaging &...

ANAMA Package & Container Testing Services, Inc.

607 Fayette Avenue, Mamaroneck, NY 10543

Tel: (914) 899-3300 | Fax: (914) 899-3325

[email protected] | www.anamapackagetesting.com

Project #2477

Certification #+CM0428

Date of Report: 6/19/2019

Periodic Retest Date: 6/19/2021

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DEPARTMENT OF TRANSPORTATION

PERFORMANCE ORIENTED PACKAGE TESTING

CERTIFICATION

Testing Performed by:

ANAMA Package & Container Testing Services, Inc. (+CM)

Approval CA2013040016

607 Fayette Avenue

Mamaroneck, NY 10543

(914) 899-3300

Testing Performed for:

Owen Oil Tools, Inc.

12001 County Road 1000

Godley, TX 76044

Mr. Matt Holzer

(817) 551-0540

[email protected]

4G Design Re-Qualification Testing

Iteration 1: Fibreboard Box with 2-11.4 Kg Average Gross Weight Barrier Bags (4 SLOT)

Iteration 2: Fibreboard Box with 2-11.2 Kg Average Gross Weight Barrier Bags (MEDIUM HOLE)

Iteration 3: Fibreboard Box with 2-11.4 Kg Average Gross Weight Barrier Bags (2 ½ HEX)

Iteration 4: Fibreboard Box with 10-2.24 Kg Average Gross Weight Steel Cylinder Assemblies (001-UNI DET)

Box ID: 1313-700

4G / Y 23.7 / S / **

USA / +CM0428

** insert year the packaging is manufactured

________________________________________________________________________

Anton Cotaj, Certification Officer

u n

tel:(914)

mailto:[email protected]

http://www.anamapackagetesting.com/


____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________

CA2013040016 Project #2477

ANAMA Package & Container Testing Services, Inc.

607 Fayette Avenue, Mamaroneck, NY 10543

Tel:(914) 899-3300 | Fax: (914) 899-3325

[email protected] | www.anamapackagetesting.com




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SECTION 1 - CERTIFICATION

4G Design Re-Qualification Testing of the Owen Oil Tools, Inc., Godley, TX Packages

Iteration 1: Fibreboard Box with 2-11.4 Kg Average Gross Weight Barrier Bags (4 SLOT)

Iteration 2: Fibreboard Box with 2-11.2 Kg Average Gross Weight Barrier Bags (MEDIUM HOLE)

Iteration 3: Fibreboard Box with 2-11.4 Kg Average Gross Weight Barrier Bags (2 ½ HEX)

Iteration 4: Fibreboard Box with 10-2.24 Kg Average Gross Weight Steel Cylinder Assemblies (001-UNI DET)

Box ID: 1313-700

Requesting Party:

Owen Oil Tools, Inc. Tel: (817) 551-0540

12001 County Road 1000, PO Box 765 Email: [email protected]

Godley, TX 76044

Attn: Mr. Matt Holzer

ANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under

§107.403 and certifies that the Owen Oil Tools, Inc., Godley, TX packaging prepared as for transport, referenced above and

tested in May & June 2019 has passed the Standards of the US Department of Transportation, Title 49CFR, Performance

Oriented Packaging Standards; Section 178. This package is also certified under IMDG and UN Recommendations of the

Committee of Experts on the Transportation of Dangerous Goods. It is the responsibility of the shipper / end user to ensure

appropriate use.

The use of other packaging methods or components other than those documented in this report may render this report

invalid.

SUMMARY OF PERFORMANCE TESTS

Test Specification Test Level Time Results

Drop 49 CFR 178.603 1.2 m N/A Pass

Stacking 49 CFR 178.606 347.3 kg 24 Hours Pass

Cobb 49 CFR 178.516 122.2 gr/m² 30 Minutes Pass

Vibration 49 CFR 178.608 235 CPM 60 Minutes Pass

Test Report #0428

UN Marking (49 CFR 178.503)

4G / Y 23.7 / S / **

USA / +CM0428

Package Identification Code 4G - Fibreboard Box (49 CFR 178.516)

Performance Standard Y - Packaging meets Packing Group II and III Tests

Authorized Gross Mass 23.7 kg (52.14 lbs)

"S" Designation Denotes Inner Packaging

Year of Manufacture ** Insert year the packaging is manufactured

Country Authorizing The Mark USA

DOT UN Third-Party Certification Agency (+CM) ANAMA Package & Container Testing Services, Inc.

Approval CA2013040016

Third Party Packaging Identification Number +CM0428

________________________________________________________________________

Anton Cotaj, Certification Officer

tel:(914)


http://www.anamapackagetesting.com/






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CA2013040016 Project #2477

SECTION 2 – DESCRIPTION OF THE TESTED PACKAGE

Iteration 1 (4 SLOT):

Two (2) up to 11.4 kg average gross weight solid product simulant filled barrier bags, inner packagings, stacked on top of

each other within a regular slotted fibreboard carton (International Box Code 0201) outer packaging with double-wall

corrugated sheets on top and bottom.

Iteration 2 (MEDIUM HOLE):



corrugated sheets on top and bottom.

Iteration 3 (2 ½ HEX):



corrugated sheet on top.

Iteration 4 (001-UNI DET):

Ten (10) up to 2.25 kg average gross weight solid product filled steel pipes with screw on end caps, inner packagings each

filled with up to 730 grams average gross weight of solid product. The steel pipe assemblies are placed sideways 2-layers

high, 5 assemblies per layer within the center special slotted fibreboard carton (International Box Code 0204) outer

packaging with double-wall corrugated sheets on top, bottom, sides and between layers and side honeycomb pads.

The use of other packaging methods or components may render this report invalid.





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CA2013040016 Project #2477

INNER PACKAGING #1 – Reference Section 7 for drawings

BARRIER BAG [ITERATIONS: 1 (4 Slot), 2 (MH-7) & 3 (2 ½ HEX)]

Quantity 2

Style/Description

Laminated watervaporproof, greaseproof,

flexible barrier bag with heat-sealed bottom

and sides

Type MIL-PRF-131K, Type 1, Class 1, Style 1

Manufacturer Cadillac Products Packaging Company

Supplier East Texas Seals, LLC, Dallas, TX

Part # MB20.5X18

Material of Construction Plastic/foil/plastic laminate, 5 Mil nominal

gauge

Minimum Thickness 0.120 mm (0.0045")

Nominal Thickness 0.127 mm (0.005")

Dimension (mm, OD), W X L, flat 475 x 530

Dimension (mm, ID), W X L, flat 445 x 470

Dimension (mm, OD) filled

Iteration 1: 340 x 340 x 65



Bottom Seam Width 11.5 mm

Side Seam Width 12.8 mm

Top Seam Width 8.0 mm, 37 mm away from top edge

Average Tare Weight 61.1 grams

Average Gross Weight (as tested)

Iteration 1: 9.95 kg

Iteration 2: 523.5 grams

Iteration: 5.80 kg

Print EMI/STATIC SHIELD

Method of Closure

Test material was inserted into bag. Air was expelled from bag, then bag was

heat-sealed. Corners and top of the bag were folded against the sides (Refer to

Section 6.2)

Bag Width Bag Depth





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CA2013040016 Project #2477

INNER PACKAGING #2 – Reference Section 7 for drawings

STEEL PIPE ASSEMBLY [ITERATION 4 (001-UNI DET)]

Quantity 10

Style/Description Steel cylinder with screw on end caps

Supplier Romar

Part # DET-PIPE-001

Material of Construction SCH40 Black Steel

Minimum Thickness 3.68 mm

Nominal Thickness 3.80 mm

Dimension (mm, OD) 76.7 x 200 (closed)

Dimension (mm, OD) 60.5 x 152 pipe only

Dimension (mm, ID) 52.4 x 152 pipe only

Thread Height 27.8 mm on each end


Average Gross Weight 2722.5 grams

Average Net Weight 1205 grams

END CAPS

Quantity 20 (2 per pipe)

Part # DET-PIPE-002

Material of Construction SCH40 Black Steel

Dimension (mm, OD) 76.7 x 37.0

Dimension (mm, ID) 56.4 x 30.4


Test Material Steel pieces

Method of Closure Screwed on





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CA2013040016 Project #2477

INNER PACKAGING DETAIL #1-1 - Reference Section 7 for drawings

CORRUGATED TRAY [FOR ITERATION 1 (4 SLOT)]

Quantity 2

Style Tray with Locking Ends

Material 200# (42/26/42) Kraft/Kraft B-Flute Corrugate

Manufacturer/Supplier Danhil Container, Brownwood, TX

Part # 1313-PARTITION TRAY

File # 43736

Part # 1313-TRAY

Size (mm, OD) – set-up 335 x 335 x 50

Size (mm, ID) – set-up 320 x 320 x 45

Size (mm) flat 543 x 537

Caliper 3.07 mm


Average Gross Weight 9.85 kg

Method of Joining Panels Roll & Lock

Joint Locations Both Ends, bottom edges

Print None

Notes These corrugated trays were placed inside the

barrier bags, 1 tray per bag


PARTITION SYSTEM [FOR ITERATION 1 (4 SLOT)]

Quantity 2

Material 275# (42/26/26/26/42) Kraft/Kraft BC-Flute

Corrugate

Manufacturer/Supplier Danhil Container, Brownwood, TX

Part # 1313-225 D/C 4 SLOT PRTN

File # 5797

Size (mm, OD) set-up 320 x 320 x 45

Caliper 6.81 mm


Notes

8 die-cut corrugated sheets (4 along and 4 across) interlock with each other to

form a 5 x 5 open-cell partition system. These partitions were placed inside the

corrugated trays





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CA2013040016 Project #2477


DIE-CUT FOLDED CORRUGATED PAD

Quantity Iteration 1: 2

Iteration 2: 4


Manufacturer/Supplier All Star Corrugated, Fort Worth TX

Part # 1313-225B

Spec. # 1343

Size (mm, OD) folded 340 x 340 x 12

Caliper 6.58 mm


Location

Iteration 1: These die-cut folded in-half corrugated sheets were placed over the

steel cylinders/disks inside the corrugated trays into each barrier bag. Each side

contains 25 13.4 mm diameter die-cut openings

Iteration 2: These stacked folded die-cut pads were placed over the die-cut pads to

form the tray


PLAIN CORRUGATED PAD

Quantity

Iteration 1: 0

Iteration 2: 2

Iteration 3: 2



Part # 1313-104 WHS

Spec. # 113615

Size (mm, OD) flat 340 x 340

Caliper 6.38 mm


Location Iteration 2: 1 pad was placed under die-cut pads to form the tray

Iteration 3: Placed over the honeycomb pad


DIE-CUT CORRUGATED INSERT [FOR ITERATION 2 (MEDIUM HOLE)]

Quantity 6 (3 per barrier bag)

Material 200# Kraft/Kraft BC-Flute Corrugate


Part # 1313-425

Spec. # 71285


Caliper 6.38 mm

Weight 54.4 grams

Location These stacked die-cut pads were placed under the die-cut folded pads to form the

tray. Each pad contains 25 47.5 mm die-cut openings arranged 5 X 5





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CA2013040016 Project #2477


HEXACOMB PAD [FOR ITERATION 3 (2 ½ HEX)]

Quantity 2

Material Hexacomb Core Type 3 light facing

Manufacturer/Supplier Pregis Hexacomb Corporation

Supplier All Star Corrugated, Fort Worth TX

Reference # J2V218A

Spec # J2V274


Caliper 76 mm


Location Inside each barrier bag. Each pad contains 25 40 mm diameter, 38 mm depth

opening arranged 5 X 5


POLY-STRAPS

Quantity

Iteration 1: 6

Iteration 2: 4

Iteration 3: 4

Iteration 4: 0

Material Polypropylene

Manufacturer/Supplier Uline, Inc. Waukegan, IL

Item # S-1761

Length 775

Width 12.5 mm

Caliper 0.48 mm

Break Strength 300 lbs


Notes Each corrugated tray was strapped with 2 poly-

straps, 2 x 1 long way

Overall Inner Package Tare

Weight (IPTW)

Iteration 1:

IPTW1 = 2 X [61.1 + (2 x 146.0) + (2 x 96.5) + (3 x 2.8) + (2 x 203.5)]

IPTW1 = 2 X (61.6 + 292+ 193 + 8.4+ 407) = 2 X 962 = 1924.0 grams

Iteration 2:

IPTW 2 = 2 X [61.1 + (2 x 2.8) + (4 x 203.5) + (2 x 104.5) + (3 x 54.4)]

IPTW2 = 2 X (61.6 + 11.2 + 814 + 209 + 163.2) = 2 X 1259 = 2518.0 grams

Iteration 3:

IPTW3 = 2 X [61.1 + (2 x 2.8) + 104.5 + 224.2]

IPTW3 = 2 X (61.1 + 5.6 + 104.5 + 224.2) = 2 X 295.9 = 791.8 grams

Iteration 4:

IPTW4 = 10 X [696.3 + (2 x 410.6)] = 10 X (696.3 + 821.2)

IPTW4 = 10 X 1517.5 = 15,175 grams





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CA2013040016 Project #2477

PRODUCT SIMULANT/TEST MATERIAL #1

DUMMY LOAD 1 [ITERATION 1 (4 SLOT)]


Style/Description Solid steel disks

Dimension (mm, OD), D X H 53.5 x 62.9 (max height)

Dimension (mm, ID), D X H 44.1 x 50.8

Thickness 4.76

Average Gross Weight (as tested) 376.6 grams

Location Placed 5 X 5 within each corrugated trays

PRODUCT SIMULANT/TEST MATERIAL #1-1

ADDITIONAL DUMMY LOAD 1 [ITERATION 1 (4 SLOT)]

Quantity 2

Style/Description Zip-locked bags filled with steel powder

Average Gross Weight (as tested) 3.84 kg

Location Placed over the filled barrier bag, under top pad


DUMMY LOAD 2 [ITERATION 2 (MEDIUM HOLE)]

Quantity 30 (30 over each barrier bag)

Style/Description Solid steel pieces with hole in center


Thickness 9.2

Average Gross Weight (as tested) 423 grams

Location Placed over barrier bags


DUMMY LOAD 3 [ITERATION 1 (2 ½ HEX)]


Style/Description Solid steel disks

Dimension (mm, OD), D X H 44.1 x 56.5 (max height)


Thickness 3.96


Location Placed 5 X 5 within each Hexacomb Pad





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CA2013040016 Project #2477

PRODUCT SIMULANT/TEST MATERIAL #3-1

ADDITIONAL DUMMY LOAD 3 [ITERATION 3 (2 ½ HEX)]

Quantity 4

Style/Description Zip-locked bags filled with steel powder

Average Gross Weight (as tested) 4.23 kg

Location Placed over the bottom layer barrier bag


DUMMY LOAD 4 [ITERATION 4 (001-UNI DET)]

Quantity 300 (30 per pipe assembly)

Style/Description Solid steel curved pieces


Thickness 1.6


Location Placed over barrier bags

Overall Dummy Load Gross Weight

(DLGW)

Iteration 1:

IPTW1 = (50 x 0.376) + (2 x 3.84) = 18.8 + 7.68 = 26.48 kg

Iteration 2:

IPTW 2 = 60 x 423 = 25.38 kg

Iteration 3:

IPTW 3 = (50 x 0.0.215) + (4 x 4.23) = 10.76 + 16.95 = 26.48 kg

Iteration 4:

IPTW4 = 10 X (30 x 0.0401) = 10 X 1.2049 = 12.05 kg





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CA2013040016 Project #2477

OUTER PACKAGING - Reference Section 7 for drawings

FIBREBOARD BOX – UN 4G

Style Center Special Slotted Container (CSSC),

FEDCO Style: 0204


Part # 1313-700 CHG BOX

File # 43703

Material of Construction Kraft/Kraft Vertical Corrugated, 40H Michelman outside with MRA

Dimension (mm, OD), L X W X H 353 x 353 x 208

Dimension (mm, ID), L X W X H 341 x 341 x 186 (Panel-To-Panel)

Stacking Height (mm) 208

Number of Walls - Flute Type Double-Wall BC-Flute

Tare Weight 685.1 grams

BMC (Box Marked Certification) 275#

Tested Basis Weight (lbs/1000ft²) 43.19 – 24.89– 28.59 – 24.32 – 43.35

Combined Weight (lbs/1000ft²) 115.13

Tested Burst Strength (lbs/inch²) 300.5

Tested Caliper 6.74 mm

Method of Joining Panels Glued inside

Mfr's Joint Flap Size 70 mm

Mfr's Joint Location 5-2 corner as per the ASTM diagram

Top Flap Gap/Meet Inner: Meet Outer: Meet

Bottom Flap Gap/Meet Inner: Meet Outer: Meet

Print None

BOX SEALING STAPLES (Refer to Section 6 for Closing Instruction and Section 7 for Specs)

Part # 3/4" C34 Stick Staples S-1396 Uline

Description 18 mm (3/4") long, 31 mm (1-1/4") crown

galvanized metal staples

Manufacturer/Supplier Uline, Inc. Waukegan, IL

Uline Item # S-1396

Quantity 8


Top Pattern 4 staples along the flap seam, 51 mm (2") away from boxes outside edges, 76

mm (3") apart on both sides & 100 mm (4") apart on center

Bottom Pattern 4 staples along the flap seam, 51 mm (2") away from boxes outside edges, 76

mm (3") apart on both sides & 100 mm (4") apart on center

Method of Closure See Section 7.2





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CA2013040016 Project #2477

OUTER PACKAGING DETAIL #1 - Reference Section 7 for drawings

PLAIN CORRUGATED PAD

Quantity

Iteration 1: 2

Iteration 2: 6

Iteration 3: 1

Iteration 4: 3



Part # 1313-104 WHS

Spec. # 113615


Caliper 6.50 mm


Location

Iteration 2: 7 plain corrugated sheets were placed over and 1 below the barrier

bags

Iteration 3: 1 pad was placed over the barrier bags

Iteration 4: 1 pad was placed over and 2 below the pipe assemblies


HEXACOMB PAD [ITERATION 4 (001-UNI DET)]

Quantity 2

Material Hexacomb Core Type 4 light facing

Manufacturer/Supplier Pregis Hexacomb Corporation

Supplier All Star Corrugated, Fort Worth TX

Spec # H0687483


Caliper 51 mm


Location These honeycomb pads were placed against box inner walls


DIVIDER PAD [ITERATION 4 (001-UNI DET)]

Quantity 1

Material 275# Kraft/Kraft BC-Flute Corrugate


Part # 1313-104 C SAW CUT

Spec. # 113615

Size (mm, OD) 343 x 239

Caliper 6.48 mm

Tare Weight 68.5 grams

Location Placed between 2 layers of pipe assemblies





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CA2013040016 Project #2477

Overall Outer Package Tare Weight

(OPTW)

Iteration 1:

OPTW1 = [685.1 + (8 x 0.8)] + (2 x 104.5) = 691.5 + 209 = 905.0 grams

Iteration 2:

OPTW2 = [685.1 + (8 x 0.8)] + (6 x 104.5) = 691.5 + 627 = 1318.5 grams

Iteration 3:

OPTW3 = [685.1 + (8 x 0.8)] + 104.5 = 691.5 + 104.5 = 796.0 grams

Iteration 4:

OPTW4 = [685.1 + (8 x 0.8)] + (3 x 104.5) + (2 x 95.5) + 68.5 =

OPTW4 = 691.5 + 313.5 + 191 + 68.5 = 1264.5 grams





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CA2013040016 Project #2477

SECTION 3 – TEST DESCRIPTIONS & TEST RESULTS

Drop Test – 49 CFR 178.603

Test Specimen/Contents Characteristics -

Number of Packages Tested 20 (5 per iteration)

Product Specific Gravity 1.2

Packing Group Number PG II

State Solid

Dummy Load Steel disks or blocks

Drop Height Multiplier 0.67 for PG III; 1 for PG II & 1.5 for PG I

Drop Height Used 1.2 m

Conditioning Temperature & Duration, 49 CFR178.603(c) 24 Hours @ 73 °F & 50 % R.H.

Test Method -

The inner packagings were filled to 95% overflow capacity with solid load.

The packages were assembled as per closing instruction (Reference Section 6).

Assembled packages were dropped onto a solid steel plated concrete floor.

Drops were conducted within 60 seconds of removal of the assembled packages from the

conditioning chamber.

Test Results -

Drop /

Sample #

Test Weight

(kg) Box Orientation Results

1-1 29.52 Top (mfr's) corner

(Corner 1-2-5)

Box outside impact corner was slightly crushed around,

approximately 3" in diameter, however box was still in-tact

and capable and safe for further handling.

There was no leakage of the filling substance

1-2 29.39 Top surface (Face 1) There was no visible damage to the outer packaging, there

was no leakage of the filling substance

1-3 29.39 Short side (Face 5) There was no visible damage to the outer packaging, there


1-4 29.48 Long side (Face 2) There was no visible damage to the outer packaging, there


1-5 29.39 Bottom surface (Face 3) There was no visible damage to the outer packaging, there


Drop 1 –

Top Corner

Drop 2 –

Top Surface

Drop 3 –

Short Side

Drop 4 –

Long Side

Drop 5 –

Bottom Surface





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CA2013040016 Project #2477

Drop Test Results (Continued) -

Drop /

Sample #

Test Weight



(Corner 1-2-5)













Drop 1 –

Top Corner

Drop 2 –

Top Surface

Drop 3 –

Short Side

Drop 4 –

Long Side

Drop 5 –

Bottom Surface


(Corner 1-2-5)













Drop 1 –

Top Corner

Drop 2 –

Top Surface

Drop 3 –

Short Side

Drop 4 –

Long Side

Drop 5 –

Bottom Surface





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CA2013040016 Project #2477

Drop Test Results (Continued) -

Drop /

Sample #

Test Weight



(Corner 1-2-5)













Drop 1 –

Top Corner

Drop 2 –

Top Surface

Drop 3 –

Short Side

Drop 4 –

Long Side

Drop 5 –

Bottom Surface

Drop Test Pass/Fail Criteria -

A package is considered to successfully pass the drop tests if for each sample tested:

For packaging containing liquid, there is no leakage of the filling substance from the inner packaging.

There is no damage to the outer packaging likely to adversely affect safety during transport.

Inner receptacles, inner packagings or articles must remain completely within the outer packaging.

Any discharge from a closure is slight and ceases immediately after impact or pressure equalization with no further

leakage.

No rupture is permitted in packagings for materials in Class 1 which would permit spillage of loose explosive

substances or articles from the outer packaging.

1 – Iteration 1 (4 Slot); 2 – Iteration 2 (MH-7); 3 - Iteration 3 (2 ½ HEX) & 4 – Iteration 4 (001-UNI DET)





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CA2013040016 Project #2477

Stacking Test - 49 CFR 178.606 (See Section 5.2 for Calculation)

Test Specimen/Contents Characteristics

Number of Packages Tested 12 (3 per iteration)

State Solid

Dummy Load Steel disks or blocks

Conditioning of Outer Packaging - 49 CFR 178.602(d) 24 Hours @ 73 °F & 50 % R.H.

Test Temperature 73 °F & 50 % R.H.

Test Method Free standing, static (dead weight) test

Test Duration 24 hours

Minimum calculated stacking test weight 331.8 kg (729.9 lbs) per package

Actual stacking test weight 347.3 kg (765 lbs) per package

Test Method -


The packages were assembled as per closing instruction (Reference Section 6).

Stacking test load (dead weight) of 247.3 kg was applied individually to the top of the three (3) assembled packages per

each iteration using wood load spreaders and the weight was maintained for 24 hours.

Test Results -

Test Sample

#

Test Sample

Weight (kg)

Test Load

(Kg) Duration Stacking Test Results

1-6 29.39 347.3 24 Hours

Boxes did not show

any signs of

deterioration or

distortion, there was

no leakage of the

filling substance

1-7 29.48 347.3 24 Hours

1-8 29.30 347.3 24 Hours

2-6 29.27 347.3 24 Hours

Boxes did not show

any signs of

deterioration or


no leakage of the

filling substance

2-7 29.30 347.3 24 Hours

2-8 29.60 347.3 24 Hours





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CA2013040016 Project #2477

Stacking Test Results (Continued) -

Test Sample

#

Test Sample

Weight (kg)

Test Load

(Kg) Duration Stacking Test Results

3-6 29.75 347.3 24 Hours

Boxes did not show

any signs of

deterioration or


no leakage of the

filling substance

3-7 29.57 347.3 24 Hours

3-8 30.20 347.3 24 Hours

4-6 29.30 347.3 24 Hours

Boxes did not show

any signs of

deterioration or


no leakage of the

filling substance

4-7 30.48 347.3 24 Hours

4-8 30.60 347.3 24 Hours

Pass/Fail Criteria -

A package is considered to successfully pass the stack tests if for each sample tested:

No test sample shows any deterioration or distortion that could adversely affect safety during transport causing

instability in stacks of packages, or cause damage to inner packagings that is likely to reduce safety in transport.

There no leakage of the filling substance from the inner receptacle, or inner packaging.






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CA2013040016 Project #2477

Vibration Test - 49 CFR 178.608


Number of Packages Tested 12 (3 simultaneously, 3 per iteration) same samples used for

stacking test

State Solid

Dummy Load Steel cylinders wrapped around with plastic film

Conditioning of Outer Packaging - 49 CFR 178.602(d) 24 Hours @ 73 °F & 50 % R.H.

Test Temperature Ambient

Test Method ASTM D999-08 Rotary Motion Vibration

Test Duration 60 minutes

Test Frequency 235 CPM

Test Method -


The packages were re-assembled as per closing instruction (Reference Section 6).

Three (3) assembled packages for each iteration were simultaneously placed on a rotary vibration table platform having

25.4 mm peak-to-peak displacement and vibrated in normal shipping orientation for one (1) hour at 235 CPM such that

a 1.6 mm thickness could be passed between the bottom of the samples and the platform. Immediately thereafter, the

packages were removed from the platform and turned on its side for examination.

Test Results -

Test Sample

#

Test Sample

Weight (kg)

Frequency

(CPM)

Duration

(Minutes) Vibration Test Results

1-6 29.39 235 60

There was no

rupture or

deterioration of

boxes, there was no

leakage of the filling

substance

1-7 29.48 235 60

1-8 29.30 235 60

2-6 29.27 235 60

There was no

rupture or

deterioration of

boxes, there was no


substance

2-7 29.30 235 60

2-8 29.60 235 60





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CA2013040016 Project #2477

Vibration Test Results (Continued) -

Test Sample

#

Test Sample

Weight (kg)

Frequency

(CPM)

Duration

(Minutes) Vibration Test Results

3-6 29.75 235 60

There was no

rupture or

deterioration of

boxes, there was no


substance

3-7 29.57 235 60

3-8 30.20 235 60

4-6 29.30 235 60

There was no

rupture or

deterioration of

boxes, there was no


substance

4-7 30.48 235 60

4-8 30.60 235 60


A package is considered to successfully pass the vibration test, if for each sample tested after it was immediately

removed from table platform and turned on its side:

There is no leakage or rupture from any of the packaging.

No test sample shows any deterioration which could adversely affect safety or container strength, during transport

liable to reduce packaging strength.






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CA2013040016 Project #2477

Cobb (Water Absorption) Test - 49 CFR 178.516


Number of Samples Tested 5

Test Duration 30 Minutes

Test Intensity 100 mL Distilled Water

Conditioning of Test Samples 24 Hours @ 73 °F & 50 % R.H.

Test Method - ISO International Standard 535-1976 (E), Cobb Method

Test Results -

Sample # #1 #2 #3 #4 #5 Average Results

grams/m² 126.5 122.2 123.9 116.4 122.4 122.2 Pass


An increase in mass of greater than 155 grams/m² over the 30 minute duration of the tests represents an

unacceptable level of water absorption

SECTION 4 – SHIPPERS RESPONSIBILITY

It is the responsibility of the end shipper to determine authorization for use under these regulations.

It is the shippers responsibility to determine if the packaging is compatible for products to be shipped.

Use of the marking of this certification for any variations without further testing as allowed under US DOT 49

CFR Section 178.601 will be at complete responsibility of the shipper. By continuing to place the UN Markings

on Packagings, the packaging manufacturer or shipper is certifying that each packaging is constructed in the

same manner as the originally tested and certified packaging, and that each packaging is capable of withstanding

the prescribed performance tests.

According to 49 CFR Section 178.601 (1) Variation 1 - variations are permitted in inner packaging of a tested

combination packaging without further testing of the package, provided an equivalent level of performance is

maintained as described in 178.601 (1) Variation 4 (i),(A),(B),(C),(D),(E) and (F) and (ii).

According to US DOT 49 CFR Section 178.601 (e), the packaging manufacturer shall achieve successful test

results for the periodic retesting at intervals established by the manufacturer of sufficient frequency to ensure

that each packaging produced by manufacturer is capable of passing the design qualification test. Changes in

retest frequency are subject to the approval of the Associate Administrator for Hazardous Materials Safety. For

combination packaging, the periodic retest must be conducted at least once every 24 months.





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SECTION 5 - CALCULATIONS

5.1 Certified Package Gross Mass Calculations Based on Test Level

Overall Inner Package Tare Weight (IPTW)


Iteration 2: 2518 grams


Iteration 4: 15,175.0 grams

Overall Outer Package Tare Weight (OPTW)



Iteration 3: 796 grams


Overall Dummy Load Gross Weight (DLGW)





Number of Inner Packaging (NIP)

Iteration 1: 2

Iteration 2: 2

Iteration 3: 2

Iteration 4: 10

Packing Group Number II

Minimum Package Weight as Tested (PGW)

Iteration 1: PGW1 = 29.30 kg




Packing Group Multiplication Factor (PMF) 1.0

Formula for Calculating Certified Gross Mass

(CGW)

CGW = Minimum PGW

CGW = Minimum PGW4 = 28.48 kg

CGW = 23.7 kg

CGW = 23.7 kg (52.14 lbs)

(scaled down to match current marking)

Certified Package Marking Y = 23.7 (52.14 lbs)

5.2 Stacking Strength Test Calculations

Test Load (TL) TL = [(SH - PH) - 1] x CGW (static)

TL = [(SH - PH) - 1] x CGW x 1.5 (dynamic)

Overall Stacking Height of Packages (SH) 3000 mm (10 feet)

Overall Stacking Height of Package (PH) 208 mm

TL (Static)

TL = [(3000/208) - 1] x 23.7 = 14 (rounded up) x 23.7

TL = 331.8 kg (729.9 lbs)

Rounded up to at 347.3 kg (765 lbs) per package for test purposes





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Appendix A – Regulatory & Industry Standard References

Regulatory Standard References:

Test 1. 2. 3. 4. 5.

49 CFR UN Regulation IMDG ICAO IATA

Drop Test 178.603 6.1.5.3 6.1.5.3 6.4.3 6.3.3

Stacking Test 178.606 6.1.5.6 6.1.5.6 6.4.6 6.3.6

Hydrostatic

Pressure 173.27(c) 4.1.1.4 4.1.1.4 4.1.1.6 5.0.2.9

Cobb Test 178.516 6.1.4.12.1 6.3.11.1 6.2.12.2

Vibration Test 178.608 - - 4.1.1.1 5.0.2.7

1. United States Code of Federal Regulations (CFR), Title 49, Transportation, Parts 100-199

2. The United Nations Recommendations on The Transport of Dangerous Goods – Model Regulations (Orange

Book)

3. International Maritime Dangerous Goods Code (IMDG)

4. Technical Instructions for the Safe Transport of Dangerous Goods by Air (ICAO)

5. International Air Transport Association (IATA), Dangerous Goods Regulations

Industry Standard References:

Drop Test ASTM D5276 Standard Test Method for Drop Test of Loaded Containers by Free Fall

Stacking Test ASTM D4577 Standard Test Method for Compression Resistance of a Container Under Constant

Load

Hydrostatic

Pressure ASTM D7660

Standard Guide for Conducting Internal Pressure Tests on United Nations (UN) Packagings

Cobb Test ISO 535 Paper and Board – Determination of Water Absorption – Cobb Method

Vibration Test ASTM D999 Standard Test Method for Vibration Testing of Shipping Containers

American Society for Testing and Materials (ASTM) International Organization for Standardization (ISO)





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Appendix B – Test Equipment & Instrumentation

No. Test Machine, Model # and Serial # Capacity Calibration

Date

Re-Calibration

Date

1. Drop Table, Lansmont Corporation:

Model #PDT-56-ED; Serial #M-1245 11" ÷ 72" 2/22/2019 2/22/2020

2. Drop Table, Gaynes Eng. Inc., Serial #G-13673-2 12" ÷ 120" 2/22/2019 2/22/2020

3. Vibration Table, Gaynes Eng. Inc.: Model #6000V 3000 lbs 2/22/2019 2/22/2020

4. Compression Machine, TechLab Systems:

Model #Validator; S/N #1005971T078 5000 lbs 2/22/2019 2/22/2020

5. VWR Traceable Digital Thermometer:

Serial #51234531 (for Conditioning, Freezer), -58° ÷ 302° F 2/13/2019 2/13/2020

6. AMETEK Digital Thermometer: Model #DT-8350 -50° ÷ 450° F 2/22/2019 2/22/2020

7. Paperless Temperature & Humidity Recorder, Dickson:

Model #TH660 (for Cold Chamber) -148° ÷ 350° F 2/22/2019 2/22/2020

8. Paperless Temperature & Humidity Recorder, Dickson:

Model #TH635 (for Conditioning Room)

-140° ÷ 185° F,

0% ÷ 95% RH 2/22/2019 2/22/2020

9. Thermometer & Hygrometer,

Omega Engineering: Model #RH520 (for Hot Chamber)

-20° ÷ 140° F,

10% ÷ 95% RH 2/22/2019 2/22/2020

10. Bench Scale, SeiKo Scale Division:

Model #WA200001XP; S/N #160808009 10mg ÷ 20 kg 5/16/2019 5/16/2020

10. Mettler Toledo D-72458 Albstadt:

Model #BBK-462-35ST; S/N #2986871-7CK 0 ÷ 35 kg 4/19/2019 4/19/2020

11. Mettler Toledo D-72458 Albstadt:

Model #XS16001L; S/N #B112123112 0 ÷ 16.1 kg 4/19/2019 4/19/2020

12. Analytical Balance, PCA, Germany:

Model #AB200; S/N #2626 10mg ÷ 200 g 5/16/2019 5/16/2020

13. Bench Scale, Ohaus: Serial #5040335-5XZ 0 ÷ 200 lbm 5/16/2019 5/16/2020

14. Caliper, Fowler: Model #54-100-112-1 ;

S/N: 1205A58182 0 ÷ 12" 5/16/2019 5/16/2020

15. Mitutoyo Cor. Micrometer:

Model #Absolute Digimatic CD-8C; S/N: 4934 0 ÷ 6" 5/16/2019 5/16/2020

16. Electronic Torque-Meter, Kaps-All:

Model #EB-650; S/N #11051 3 ÷ 100 inch-lbs 4/19/2019 4/19/2020

17. Toque Wrench, CDI, Model No. 301LDIN 0 ÷ 30 inch-lbs 5/16/2019 5/16/2020

18. Omega Digital Pressure Gauge:

Model #DPG7010-200; S/N #1305276 0 ÷ 200 psi 5/15/2018 5/15/2019

19. Omega Digital Pressure Gauge:

Model #DPG8001-30V30; S/N #16121406000 -30" ÷ 30 psi 2/13/2019 2/13/2020

20. Winters Pressure Gauge, WG2-6 0 - 60 psi 5/16/2019 5/16/2020

21. Ashcroft Pressure Gauge, V/300 Psi

Model #DG 25: S/N #16080906005 -30 - 300 psi 10/21/2018 10/21/2019

22. The Mullen Tester, B.F Perkins and Son: Serial #14047 0 ÷ 800 psi

0 ÷ 300 psi 5/16/2019 5/16/2020

23 The Mullen Tester, B.F Perkins and Son: Serial #2180 0 ÷ 800 psi

0 ÷ 1500 psi 5/16/2019 5/16/2020

24. ECT Tester, Testing Machines, Inc.: S/N #13748 0 ÷ 120 lbs 5/16/2019 5/16/2020

25. Measuring Tape, Ultra-Touch: ANAMA TM1 & TM2 0 ÷ 25 Feet 5/16/2019 5/16/2020

26. Measuring Tape, Stanley Power Lock, 33-425;

ANAMA TM3 0 ÷ 25 Feet 5/16/2019 5/16/2020

27. Measuring Tape, Made In China; ANAMA TM4 0 ÷ 25 Feet 5/16/2019 5/16/2020

28. Presto Dart Impact Tester, Model No. PDI-350;

S/N: 2010167076 21" ÷ 1.7 feet 2/22/2019 2/22/2020





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SECTION 6 – PACKAGING ASSEMBLY (CLOSING) INSTRUCTIONS

Section 6.1 - Testing Laboratory Closing Instructions:

Note: Packages were received assembled.

ITERATION 1 (4 SLOT) - Step-By-Step Packaging Assembly Demonstration

Articles Corrugated Tray Installation of Partition

System into Tray

Installation of Articles into

Tray

Installation of Top Pad over

Articles

Poly-Strapping Method of

Filled Tray


Filled Tray

Installation of Poly-Strapped

Tray into Barrier Bag

Barrier Bag Closing/Sealing

Method Sealed Barrier Bags Outer Box Closure Pattern Erected Outer Box

Installation of Bottom Pad

into Outer Box

Installation of Bottom Layer

Barrier Bag into Outer Box

Installation of Bottom Layer

Barrier Bag into Outer Box

Installation of Additional

Weight into Outer Box

Installation of Top Pad into

Outer Box Closed Outer Box Top View

Closed Outer Box Top/Side

View

Closed Outer Box

Bottom/Side View





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ITERATION 2 (MEDIUM HOLE) - Step-By-Step Packaging Assembly Demonstration


(Filled) Tray


(Filled) Tray

Installation of Poly-

Strapped Tray into

Barrier Bag

Barrier Bag

Closing/Sealing Method

Sealed Barrier Bags Outer Box Closure

Pattern Erected Outer Box

Installation of Bottom

Pads into Outer Box


Layer Barrier Bag into

Outer Box

Installation of Layer Pad

over Barrier Bag into

Outer Box

Installation of Dummy

Load over Bottom Layer

Pad


over Bottom Layer

Dummy Load into Outer

Box

Installation of Top Layer

Barrier Bag into Outer

Box


over Barrier Bag into

Outer Box

Installation of Dummy

Load over Top Layer Pad

Installation of Top Pad

into Outer Box

Closed Outer Box Top View Closed Outer Box Bottom/Side

View Closed Outer Box Bottom View





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ITERATION 3 (2 ½ HEX) - Step-By-Step Packaging Assembly Demonstration

Articles Installation of Articles

into Hexacomb Pad


over filled Hexacomb Pad


Filled Hexacomb Pad


Filled Hexacomb Pad

Installation of Poly-

Strapped Hexacomb Pad

into Barrier Bag

Barrier Bag

Closing/Sealing Method Sealed Barrier Bags

Outer Box Closure



Layer Barrier Bag into

Outer Box

Installation of Assittional

Weight over Bottom

Layer Bag into Outer Box


Barrier Bag into Outer

Box


into Outer Box

Closed Outer Box Top

View

Closed Outer Box Bottom

View





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ITERATION 4 (001-UNI DET) - Step-By-Step Packaging Assembly Demonstration

Articles Outer Box Closure



Pad into Outer Box

Installation of Side

Hexacomb Pads


Layer Articles into Outer

Box

Installation of Divider

Pad over Articles


Articles into Outer Box


into Outer Box

Closed Outer Box Top

View

Closed Outer Box Bottom

View

Closed Outer Box

Bottom/Side View





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Section 6.2 - Manufacturer’s Closing Instructions:

ITERATION 1 (4 SLOT) – CLOSING INSTRUCTION





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ITERATION 1 (4 SLOT) – CLOSING INSTRUCTION (CONTINUED)





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ITERATION 2 (MEDIUM HOLE) – CLOSING INSTRUCTION (CONTINUED)






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ITERATION 3 (2 ½ HEX) – CLOSING INSTRUCTION





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ITERATION 3 (2 ½ HEX) – CLOSING INSTRUCTION (CONTINUED)





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ITERATION 4 – CLOSING INSTRUCTION





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ITERATION 4 (001-UNI DET) – CLOSING INSTRUCTION (CONTINUED)





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SECTION 7 – PACKAGING COMPONENTS SPECIFICATION & DRAWING

Manufacturer’s List of Suppliers





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Barrier Drawing & Specification





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Barrier Specification





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Corrugated Tray Drawing & Specification





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Corrugated 4 Slot Partition Drawing & Specification





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Corrugated Die-Cut Folded Pad Drawing & Specification





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Hexacomb Pad Drawing & Specification





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Corrugated Perforated Pad Drawing & Specification





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Poly-Strap Specification





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Hexacomb Pad Drawing & Specification





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Outer Box Drawing & Specification





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Plain Pad Drawing & Specification





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Carton Sealing Staples Specification

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