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INSTALLATION RESTORATION PROGRAM

INFORMAL TECHNICAL INFORMATION REPORT FOR UNDERGROUND STORAGE TANK SITES

EGLIN AIR FORCE BASE FLORIDA

ENGINEERING-SCIENCE ATLANTA, GEORGIA

flpäiä^---;

APRIL 1992

PREPARED FOR

HEADQUARTERS AIR FORCE SYSTEMS COMMAND COMMAND CIVIL ENGINEER (HQS AFSC/DEV) ANDREWS AIR FORCE BASE, MARYLAND 20334-5000

UNITED STATES AIR FORCE AIR FORCE CENTER FOR ENVIRONMENTAL EXCELLENCE (AFCEE) ENVIRONMENTAL RESTORATION DIVISION (ESR) 3ROOKS AIR FORCE BASE, TEXAS 78235-5000

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INSTALLATION RESTORATION PROGRAM

INFORMAL TECHNICAL INFORMATION REPORT FOR UNDERGROUND STORAGE TANK SITES

AIR FORCE SYSTEMS COMMAND EGLIN AIR FORCE BASE, FLORIDA

APRIL 10,1992

PREPAREDBY

ENGINEERING-SCIENCE, INC. 57 EXECUTIVE PARK SOUTH, N.E.

SUITE 590 ATLANTA, GEORGIA 30329

USAF CONTRACT NO. F33615-90-D-4014, DELIVERY ORDER NO.4 AIR FORCE CENTER FOR ENVIRONMENTAL EXCELLENCE (AFCEE)

ENVIRONMENTAL RESTORATION DIVISION (ESR) 2nd Lt. RODNEY HAMMEL

AIR FORCE CENTER FOR ENVIRONMENTAL EXCELLENCE (AFCEE) ENVIRONMENTAL RESTORATION DIVISION (ESR)

BROOKS AIR FORCE BASE, TEXAS 78235-5000

G/AT51MTIR-COV.PM4/BB/392

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n. TITLE (Include Security Clarification)

Informal Technical Information Report for Underground Storage Tanks at Eglin AFB

ERSONAl AUTHOR(S) Engineering-Science, Inc.

13*. TYPE OF REPORT Draft

Ub. TIME rnvpREo FROM 12/91 TO 4/92

U. OATE OF REPORT (Year. Month. OjyJ 15. PAGE COUNT 1992 April 10

16. SUPPLEMENTARY NOTATION

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FIELD GROUP SUB-GROUP

18 SUBJECT TERMS (Continue on went if neceuary and identify ov brfodt numoer) Informal Technical Information Report for UST Sites Eglin AFB, Florida

19. ABSTRACT {Continue on revert* if necessary and identify by block number)

As part of an on-going Installation Restoration Program (IRP) at Eglin AFB, Florida ten Underground Storage Tank Sites are being investigated to determine if contamination is present in the groundwater at these sites. Previous remediation efforts at these sites have included removal of the tanks and off-site bioremediation of contaminated soils. This is an Informal Technical Information Report (ITIR) presenting the analytical results and

pertin-.nt field data gathered during the investigation effort.

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2! ABSTRACT SECURITY CLASSlP'CAnON Unclassified

22». .NAME OF RESPONSIBLE INQIVIOUAL USAF HSD 2nd Lt. Rodney Hamel

22b. TELEPHONE (Indue* Area Code) (512) 536-9001

22c. OFP1C3 SYMBOL ' AFCEE/ESR

DO FORM 1473. ft* MAR 33 APR edition may 0« viMd antii exnaustad. All otfter edition* arm obsolet«.

SECRlTV CAS5l*CxnCN OF "^'S ^AGc

NOTICE

This Informal Techncial Information Report (ITIR) has been prepared for the United States Air Force by Engineering-Science, Inc. for the purpose of aiding in the implementation of a final remedial action plan under the Air Force Installation Restoration Program (IRP). As the plan relates to actual or possible releases of potentially hazardous substances, its release prior to an Air Force final decision on remedial action may be in the public's interest. The limited objectives of this plan and the ongoing nature of the IRP, along with the evolving knowledge of site conditions and chemical effects on the environment and health, must be considered when evaluating this plan, since subsequent facts may become known which may make this plan premature or inaccurate. Acceptance of this plan in performance of the contract under which it is prepared does not mean that the United States Air Force adopts the conclusions, recommendations or other views expressed herein, which are those of the contractor only and do not necessarily reflect the official position of the United States Air Force.

Copies of this niR may be purchased from:

Government agencies and their contractors registered with the Defense Technical Information Center should direct requests for copies of this plan to: Defense Technical Information Center (DTIC), Cameron Station, Alexandria, VA 22304-6145.

Non-Government agencies may purchase copies of this document from: National Technical Information Services (NTIS), 5285 Port Royal Road, Springfield, VA 22161.

AT510/923J189

PREFACE

This Informal Technical Information Report presents the analytical results and pertinent data associated with the Underground Storage Tank Sites at Eglin AFB, Florida.

Engineering-Science, Inc., Atlanta, Georgia is contractor for this work. Mr. Ola A Awosika, P.G., will be the primary responsible scientist performing the work.

The ITIR commences on December 1, 1991 and continues through April 10, 1992.

2nd Lt. Rodney Hamel, United States Air Force AFCEE/ESR, Brooks AFB, Texas is the Technical Program Manager.

Approved:

Contract Program Manager

ÄT510/923J189

TABLE OF CONTENTS

SECTION Pa8e

1.0 INTRODUCTION 1

2.0 BACKGROUND 1

3.0 GROUNDWATER INVESTIGATION AND RESULTS 2

3.1 Field Effort 2 3.2 Analytical Results 3 3.3 Validated Data 3 3.4 Recommendation 3

APPENDIX A DRILLING RECORDS

APPENDIX B ANALYTICAL DATA

AT510/923J189

LIST OF FIGURES

Number Title

1 Building 91129 -Hurlburt Field 2 Building 6001 - Auxiliary Field No. 6 3 Building 6024 - Auxiliary Field No. 6 4 Building 3021 - Auxiliary Field No. 3 (Duke) 5 Building 4024 - Auxiliary Field No. 4 6 Building 792 - Eglin Main Field 7 Building 981 - Eglin Main Field 8 Building 9990 - D3 Coast Guard Facility

Page

4 5 6 7 8 9 10 11

LIST OF TABLES

Number Title

1 Underground Storage Tank Removal Data 2 Physical Parameters as Measured Prior to Sampling 3 Analytical Results 4 Sample Identification Cross-Reference 5 Summary of Extraction and Analyses Dates 6 Summary of QC Acceptance Criteria and Detection Limits 7 Summary of Analytical Results

Page

12 13 14 20 21 25 26

AT510/923J189 11

EGLINAFB USTITIR

1.0 INTRODUCTION

Engineering-Science (ES) has prepared this letter report to present the results of the environmental sampling work conducted at eight (8) Underground Storage Tank (UST) sites at Eglin AFB, Florida. The locations of these UST sites are depicted in Figures 1 through 8. The results of this investigation are contained in

this report and are organized as foUows:

• Background

• Sampling Effort

• Analytical Results

• Validated Data

• Recommendation

2.0 BACKGROUND

In 1989, CH2MHÜ1 was contracted to compile a comprehensive list of old and inactive USTs at Eglin AFB. In 1990/1991, EA Engineering, Science, and Technology, Inc. were chosen to perform a removal and disposal effort in conjunction with remediation of contaminated soils as necessary. During the course of EA's removal actions, ten UST sites required some degree of soil remediation in accordance with the Federal Department of Environmental Regulation (FDER) criteria. Soil pile bioremediation methods were implemented at an offsite location in six of these cases where OVA readings exceeded 500 ppm or more (Figure 1). Local soils from a borrow pit were used to backfill the holes. The four other sites displayed OVA readings between 80 and 140 ppm during excavation. Soils for these sites were allowed to aerate naturally onsite and were reused as backfill when the

OVA readings had diminished. Information pertinent to the tank removal and soil

remediation efforts are summarized in Table 1.

AT510\923J189

The objective of the current investigation at the UST sites is to comply with FDER assessment requirements by determining if contamination is present in the groundwater and to quantify the extent of the contamination if identified. This objective was accomplished through drilling of soil borings, installation of

monitoring wells, collection of groundwater samples for chemical analyses,

validation of analytical results, and the interpretation and analysis of the validated

data.

3.0 GROUNDWATER INVESTIGATION AND RESULTS

3.1 Field Effort

This investigation effort was originally intended for the ten sites requiring remediation as discussed above. However, at the request of the Base, two sites (near Building 501 at Eglin Main and 90219 at Hurlburt Field) were deleted from this investigation due to the presence of monitoring wells onsite from previous groundwater investigations. The field effort at each individual UST site consisted of drilling, installation, development, and sampling of one monitoring well for physical and chemical analyses. The specific location of each well was selected in the field. An attempt was made to locate each well either within the previously excavated area or a nearby downgradient location, depending on site conditions (for example, presence of overhead power lines, communication lines, and trees). An estimate of the flow direction at each site was made based on surrounding topography, proximity of nearby streams, and professional judgment. Boreholes were made to accommodate each well. Soil samples were then collected for evaluation of lithological attributes and any physical evidence of contamination. Organic vapors readings were taken with an HNu during the clrilling effort. Drilling records and other information pertinent to the drilling effort are presented in Appendix A. None of the wells installed were surveyed since a potentiometric map for each site could not be developed using data from only one well.

The field work was conducted on February 3 through February 13,1992 and on February 19 through February 21, 1992. Eight groundwater samples were collected for chemical analysis. All samples were sent to Southwest Laboratory for analyses. The analyses requested included total petroleum hydrocarbons, polynuclear

aromatic hydrocarbons, 1,2-dichloroethane, ethylene dibromide, lead, BTEX, and

MTBE as required by FDER.

AT510\923J189

32 Analytical Results

A summary of the analytical results are presented in Tables 2 through 7. Tables 3 through 6 are in accordance with reporting requirements in the IRP Handbook.

Ethylene dibromide and 1,2-dichloroethane were not detected in groundwater

samples collected from any of the UST sites. Total petroleum hydrocarbons were

reported in samples from MW981-1 and MW9990-1 at levels 600 /ig/L and 1600 /ig/L, respectively. No polynuclear aromatic hydrocarbons, with the exception of fluoranthene in MW3021-1 at 2.0 /ig/L, were identified in groundwater samples. Lead in a sample from MW792-1 at a concentration of 142 /ig/L exceeded the Florida MCL of 50 /ig/L. A low concentration of toluene was reported in the

MW3021-1 sample from the BTEX analyses but the second column run did not provide confirmation. All eight samples were free of detectable MTBE contamination. A copy of the original raw data forms provided by the laboratory

are included in Appendix B.

3.3 Validated Data

The analytical data, preceded by a comprehensive review of quality assurance and quality control (QA/QC) qualifiers, is presented in Appendix B.

The lead results from the MW4204 sample and the matrix spike are considered estimated due to a low percent recovery. Xylenes at a concentration of 0.7 /ig/L were detected in the equipment rinsate UST-ER2 but were not confirmed due to the absence of a second column analyses. With the exception of the sample from MW9990-1, all polynuclear aromatic hydrocarbon analyses exceeded the established holding time criteria for sample extraction. Therefore, these results are estimated

at the laboratory method detection limits.

3.4 Recommendation

Based on the sampling results, a second groundwater sample should be collected from MW792-1 to verify the presence of lead contamination. The remaining seven sites did not show sufficient evidence of groundwater contamination attributable to the USTs to warrant further characterization. Therefore, no further investigations are recommended for these sites.

ATS10\923J189

Figure 1

UST SITE BUILDING 91129 - HURLBURT FIELD

EGLIN AFB, FLORIDA

M- 85'- -15'-*+«- -46'-

GRADED AREA

»UTILITY POLE

SB91129-1

SB91129-2 MW91129-1 ''h

FUEL BLADDER STORAGE

L=2_. L=2_.

BUILDING 91129 - REMOVED

NEW CONCRETE

SLAB

43'

O

i tu 8 8

8

• EXPLANATION

•" "^j Approximate location of tanks before removal

# Chain-link fence

® Monitoring well

• Soil boring location

NOT TO SCALE

Q/AT510MP1/CD/DSS/040792 ENGINEERING-SCIENCE

Figure 2

UST SITE BUILDING 6001 - AUXILIARY FIELD #6

EGLIN AFB, FLORIDA

w w IT

o < Ü

BUILDING 6001

PAVED DRIVEWAY

44'

lA)

GRASSY AREA

MW6001-1 SB6001-1

WHITE AVE

V \

EXPLANATION

ZZJ Approximate location of tanks before removal

l\\N Soil cuttings

® Monitoring well

NOT TO SCALE

(VAT510MP2/CD/DSS/040792 ENGINEERING-SCIENCE

Figure 3


EGLIN AFB, FLORIDA

*

<.

24'

lb

GRASSY AREA

M 431-

-29'-

SB6024-2 MW6024-1

"g

LH SB6024-1

::

K.

ROCK COVER

ABOVE GROUND

TANKS

MOTORPOOL COVERED STORAGE

BUILDING 6024

w**-

CARO STREET

s y NOT TO SCALE

G/AT510MP3/CD/DSS/040792

EXPLANATION

LZi Approximate location of tank before removal

• Soil boring location

® Monitoring well

-*«- Chain-link fence

■ ■ > Overhead power line

ENGINEERING-SCIENCE

r UST SITE

BUILDING 3021 - AUXILIARY FIELD #3 (Duke) EGLIN AFB, FLORIDA

A

NOT TO SCALE

HEMBY AVENUE

GRASSY AREA

PAVED PARKING AREA

GRASSY AREA

M 17*- SB3021-1

„ MW3021-1

(g) T I UST

^

BUILDING 3021

Figure

TO SHORT - STREET

4 Q-OC

a

TO FLIGHTUNE

I

EXPLANATION

^Zi Approximate location of tank before removal

® Monitoring well

GWT510MP4/CD/DSS/040792 ENGINEERING-SCIENCE

Figure 5


EGLIN AFB, FLORIDA

. FIELD 4 ENTRANCE

a < O EC

Q 111

1

/

/

EXPLANATION

^_"jj Approximate location of tank before removal

// Chain-link fence

0 Monitoring well

NOT TO SCALE

GWVT510MP5/CD/DSS/040792 ENGINEERING-SCIENCE

Figure 6

UST SITE BUILDING 792 - EGLIN MAIN FIELD

EGLIN AFB, FLORIDA

WEEKLY BAYOU

I Lil > a. a a w 1

BUILDING 792

GRASSY AREA

EXPLANATION

" "^j Approximate location of tank before removal

0 Monitoring well

• • Overhead telephone line

NOT TO SCALE

G/AT510MP6/CO/OSS/040892 ENGINEERING-SCIENCE

Figure 7

UST SITE BUILDING 981 - EGLIN MAIN FIELD

EGLIN AFB, FLORIDA

BUILDING 978

Q

i

i

8 < m < o CO UJ

81 ■

EXPLANATION

Uli Approximate location of tank before removal

® Monitoring well

NOT TO SCALE

O/AT510MP7/CD/DSS/040892

10 ENGINEERING-SCIENCE

Figure t

UST SITE BUILDING 9990 - D3 COAST GUARD FACILITY

EGLIN AFB, FLORIDA

BUILDING 9991

MW9990-1 SB9990-1

LOCKED GATE

BUILDING 9990

PAVED PARKING

LOT

GARAGE

\ NOT TO SCALE

GULF OF MEXICO

EXPLANATION

LZi Approximate location of tank before removal

® Monitoring well

GWT510MP8/CD/DSS/040892

11 ENGINEERING-SCIENCE

TABLE 1 UNDERGROUND STORAGE TANK REMOVAL DATA

EGLIN AFB

UST Number

Size (gallons)

Storage Use

Maximum OVA Reading during

Excavation (ppm)

Maximum OVA Reading during Well Installation

(ppm)

91129-2 10,000 Diesel 104 200

6001 1,000 Diesel 1000+ 220

6024 500 Diesel 1000+ 600

3021 500 Diesel 80 500

4204 55 Gasoline 1000+ 280

792 1,000 Diesel 1000+ 34

981-2 5,000 Diesel 1000+ 600

9990 1,000 Diesel 82 0

AT510/923J189/T-1.XLS 12

TABLE 2 PHYSICAL PARAMETERS

AS MEASURED PRIOR TO SAMPLING UST SITES EGLIN AFB

Site Number

Well Number OH

Conductivity umhos/cm

Temperature °C

Sampling Date

91129 MW91129-1 8.63 850 16.2 92/2/19

6001 MW6001-1 8.95 200 21.9 92/2/19

6024 MW6024-1 7.73 30 21.8 92/2/19

3021 MW3021-1 7.83 30 18.2 92/2/20

4204 MW4204-1 8.16 60 20.7 92/2/19

792 MW792-1 9.30 230 17.0 92/2/20

981 MW981-1 9.10 170 20.4 92/2/20

9990 MW9990-1 8.8S 460 15.8 92/2/21

AT510/923J189/T-2.XLS 13

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24

TABLE 6 SUMMARY OF QC ACCEPTANCE CRITERIA AND DETECTION LIMITS

FOR MATRIX SPIKES, MATRIX SPIKE DUPLICATES AND SURROGATE SPIKES

UST SITES EGLIN AFB

Spike Relative Recovery, Percent

Detection Percent Difference Analyte Method Limit Units (Ranee) (Range)

1,2-Dichloroethane EPA 601 1.0 ug/L 80-120 % <20 %

Ethylene Dibromide EPA 504.1 0.01 ug/L 80-120 % <20 %

Petroleum Hydrocarbons EPA 418.1 500 * ug/L 75-125 % <20 %

Lead EPA 239.2 3.0 ug/L 75-125 % <20 %

BTEX EPA 602 1.0 ug/L 80-120 % <20 %

MTBE EPA 602 1.0 ug/L 80-120 % <20 %

Polynuclear Aromatic Hydrocarbons EPA 610 1.0 ug/L 80-120 % <20 %

* - Varies. See Table 7 for complete list of detection limits

AT510/923J189/USTQCAC.XLS 25

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27

APPENDIX A DRILLING RECORDS

ENGINEERING - SOIL BORING LOG AND WELL

SCIENCE CONSTRUCTION RECORD

riisnt Ealin AFB Site Blda. 3021 - Duke Field Boring T n. SB3021-1 r,aningi=;WFnninsgr R. Surrencv Drilling Method HSA 4.25 ID Sampling Method Split Spoon Date St-arted 2/5/92 Date Completed 2/5/92 . Dni Her Griner Drilling Co. Borehole Diameter (in) 6 Depth Drilled (ft) _SS .— Ground Elevation fft^ Not measured Depth to Water (ft) 55.25 Date Measured 2/6/92

Page 1 of 2

Pro Wei Dat Dat Cas Scr Cas Scr Sum Wei TOC Wat Dat

AT510.04

Sch. 40

ject I.I 1 T n. MW3Q21-1 e Installed 2/6/92 e Grouted 2/6/92 ing Material 2" PVC een Material same. 0.010 slot ing Interval (ft) 0-49 eened Interval (ft) 49-59 p Installed?_Ng_

1 Depth (ft)_59 Elevation (ft) Not measured

er Level (ft) 55 e Measured 2/6/92

-25.

:x 10-

15-

-X

25-

U3 ^»» C/5

CD _1 CO

1.2. 1 . 1

1.1. 1 . 1

2.3. 4.6

4.5. 6.7

4.4, 4.4

M

3.9. 13, 16

o LU a:

50

70

100

85

o e

75

75

60

85

100

100

LITHOLOGIC DESCRIPTION

SAND, fine to medium, trace silt, light brown, very loose, slightly moist.

SAND, fine to medium, moderately sorted, yellowish brown, very loose, slightly moist.

SAND, fine to medium, light brown, very loose to loose, slightly moist.

SANO. fine to medium, moderately sorted, orangish brown, loose, slightly moist.

250

320

GRAPHIC LOG

SW

As above except very loose.

SAND and CLAY, fine to medium, trace silt, white to reddish brown, mottled, loose to firm, slightly moist.

SC

SW

WELL DIAGRAM

F^ z

3 O C 10

8 9 9 9 9 9 9 9 9 9 9

% 9 i 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 4 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9

9 9 9 9 9 9 9 9 9 9 9 9

M BMLTINU6

ENGINEERING - SCIENCE SOIL BORING LOG AND WELL CONSTRUCTION RECORD

Client Eolin AFB Site Blda. 3021 - Duke Field Boring T.n. SB3021-1 Rpnlnnist R. Sumencv

30- :E

35-

40-

45-

50-

55-

60-

65-

CO

Ul z o _l CO

9. 12 . 13 . 14

9, 12 . 13. 15

6,9. 12. 13

5,9. 13 ,21

7,11, 13, 16

cc

90

100

100

100

100

Page 2 of 2 Project I.D. AT510.04 Well T.n. MW3021-1 Date Installed 2/6/92

o e 3 CL

500

300

160

125

400


SAND, some silt, fine to medium, white to orangish brown, firm, slightly moist.

SAND, fine to medium, trace silt, white to light gray, loose to firm, slightly moist.

SAND, fine to medium, well sorted, white, loose to firm, slightly moist.

SW

As above except loose to very firm.

SAND, fine to medium, trace silt, white, firm, moist.

9.13. 14. 14

11.10, 11 . 13

95

95

340

130

As above, moist to 55.8', wet at 55.8'.

GRAPHIC LOG

SAND, fine to medium, some silt, white, loose to firm.

Total Depth = 59'

4'2*

WELL DIAGRAM

o c o

9 9 9 9 1/ 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9

i

u. u (0 Q.

■v c ID tn

i T

0) i-t

*+ o> c V) o c

TO) m

c 0)

01 c «I 01 c

1

BHLTINU6


Clie Site Bor i Geol Dril Samp Date Date Dril Bore Dept Grou Dept Date

nt Eolin AFB Bldo. 4204 - Field No

ng T.n. F5B4204-1 Surrencv ogist/Engineer.

ling MPthnri HSA 4.25 ID ling Mpt-hnd Split Sooon

Started_2ZZZS2 Completed ler Griner

2/7/92 Drilling Co

(in) 50

hole Diameter h Drilled (ft) nd Elevation (ft) h to Water (ft) 48. 12 Measured 2/7/92

Not measured

D. LU CD

5-

10-

15-

20-

25-

Page 1 of 2

Project T.D. AT510.04 Well T.D. MW4204-1 Date Installed 2/7/92 Date Grouted 2/7/92 Casing Material 2M PVC Sch. 40 Screen Material same. O.OIO slot Casing Interval (ft) 0-40 Screened Interval (ft) 40-50 Sump Installed?_No_ Well Depth (ft) 50 TOC Elevation (ft) Not measured Water Level (ft) 48.12 Date Measured 2/7/92

CO

CO

o _l CO

4,3. 3.2

1.3. 2.2

3.3, A , A

4,5, 8. 13

5,8, 8.7

9.11. 21 .26

o LU CC

X

70

40

75

95

75

85

10

12

60

13

200

B


SAND, fine to medium, trace silt, shell fragments, reddish brown, very loose, well sorted, slightly moist.

SAND, fine to medium, trace silt, yellowish brown, very loose, moderately sorted, slightly moist.

SAND, fine to medium, light yellowish brown, very loose, moderately sorted, slightly moist.

SAND, fine to medium, trace silt, orangish brown to 15', white from 15- 15.4*. orangish brown from 15.4-15.8", white, fine sand from 15.8-16', loose to firm, slightly moist.

SAND, fine to medium, white to 20.2", brown from 20.2 to 21', loose, slightly moist.

SAND, fine to medium, white to light brown, banded, firm to very firm, slightly moist.

GRAPHIC LOG

SW

o c CD

*-3

WELL DIAGRAM

7A 1 ^ 9 9 9 9 9 9 9 9 9 9 9 9 t/ 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 ^ ^ BHLTINU6


Client Ealin AFB Site Blda. 4204 - Field No Boring I.D.. Geoloaist R

SB42Q4-1 Surrencv

a. LU a

30- :s

35-

40-

45-

50-

55-

60-

65-

Page 2 of 2

Project I.D. AT510.04 Well I.D. MW4204-1 Date Installed 2/7/92

to CO

O _l CO

4,8, 9,8

8, 14 , 19,23

5.11, 14 , 19

9.11. 16. 16

4,6, 9,23

cc

80

75

90

100

70

50

240

180

280


SAND, fine to medium, white to 30.5' dark brown from 30.5-31', loose, moderately sorted.

SAND, medium to coarse, white to light brown, poorly sorted, firm to very firm, slightly moist.

SAND, medium to coarse to 40.6', fine to medium from 40.6-41', white to light brown, firm, slightly moist.

SAND and SILT, fine to medium to 45.5" medium to coarse from 45.5-46', dark brown, wet at 45.5".

SAND, medium to coarse, some silt, light brown, poorly sorted, loose to very firm, wet.

Total Depth - 50'

SW

SM v'y V *i *+ v

SW

GRAPHIC LOG

!»V \°VVJ

WELL DIAGRAM

0 v 3 a

1 ii

c

Ii

T > c 01

1

BHLTINU6

A-4-


Client Ealin AFB Site Bldg BOOl - Field No Boring T.n. SB60Q1-1 Rpnlnnist/Fnaineer R. Surrencv Drilling Method HSA 4.25 ID Sampling Method Split Sooon Date Started 2/4/92 Date Completed 2/4/92 Dri1ler Griner Orillina Co. Borehole Diameter (in) _6 Depth Drilled (ft) 64 Ground Elevation (ft) Not measured Depth to Water (ft) 59.13 Date Measured 2/5/92

Page 1 of 3 Project I.D. AT510.04 Well TO. MWBOOl-l Date Installed 2/4/92 Date Grouted 2/4/92 Casing MatPrial ?" PVC Sch. 40 Screen Material same. 0.010 slot Casing Interval (ft) 0-49 Screened Interval (ft) 49-54 Sump Installed?_No Well Depth (ft) 64 TOC Elevation (ft) Not measured Water Level (ft) 59.13 Date Measured 2/5/92

1=1 —

5-

10-

15-

20-

25-

H

U3

CO

o _l CO

3,2. 2.3

1.2. 1 . 1

1.1. 1 . 1

3.5. 5,7

5,6, 6,6

5.9, 13, 16

o LU CC

60

60

90

90

95

90

o e

15

20

140

130


SAND, medium to coarse, trace silt, pebbly, reddish brown, very loose, slightly moist.

As above, well sorted, moist, very loose.

SAND, medium to coarse, trace silt, reddish brown, very loose, moist.

SAND, fine to medium, some silt, trace clay, reddish brown, loose, moist.

SAND and SILT, trace clay, fine to medium, reddish brown to light brown, loose, trace of black color (possibly fuel staining), slight fuel odor, moist.

SAND, medium to coarse, trace silt, light brown to 25', reddish brown from 25-26", slight fuel odor, loose to firm, slightly moist.

GRAPHIC LOG

SW

SM

SW

US-

UELL DIAGRAM

]

BMLTINU6


Hlipnt Fa 1 in AFB Page 2 of 3

Site Blda. 6001 - Field No. 6 Project I Well I.D..

D. AT510.04 MW6001-1 Rnrinq TO. SB6001-1

Geol oaist R. Surnencv nai-p Tnstalled 2/4/92

DEPT

H (f

eet)

LU

z H-t

CO > .— CO CO -t _l GRAPHIC

WELL DIAGRAM

Q.

CO

CO IE O _l m

LU a: •>»» a. 3 C3. z —

LITHOLOGIC DESCRIPTION _J t—( o CO

LOG

30- *

4. 10 . 100 175 SAND, fine to medium, light gray, well SW

1 I 11.11 sorted, slight fuel odor, loose to

35- Y 9.11. 90 220

firm, slightly moist.

SAND, medium to coarse, trace silt,

•v ;•■'•': ;■■'•■'

A 13. 13 reddish brown to 35.5'. light gray from ■'■'•''. '•'•'.: +>

40- Y 5,9, 80 180

35.5-36*. slight odor, slightly moist.

SAND, medium to coarse, well sorted.

: :'••'.: :'■•'.:

A 11 . 14 white, slight odor, loose to firm, *•".* * • v * slightly moist.

'.'•':'.'•'."'. 1'

•:•>•:•'•:• II T 45- Y 6,11. 80 175 SAND, medium, well sorted, white to

.■'•''• •"/•""■ •'.

"3 r W- * *1 A 16, 17 light pink, loose to firm, slightly *. t* . '. / . * '.'.' '.;.' 01 f

- moist, slight odor.

.■'•'•■'•'•;•' '•' :•'. '.;•'

■n o> C (0 o c

w :■'■•'.'•:•'.•'.'■: '.;•' -

01 CD

r

50- X 5,9, 13,20

60 170 As above. V-V '':•'':•'. :':'.

•/,

:•'•:'■:•'•:•'. '.;•' •'/•"•'.'•".• i£ *.* — •,*

U <-4

- ,_ '/ • * I* •"••*. Q. '.v '.*•' <0

55^ X 10.15. 60 60 SAND, medium, well sorted, white, no ':/:•':/:•'. C ';', = ,",\ c

01

A 17,20 odor, firm, moist. : •:'[■:;:':.\ (0 10 ;." == ;.• c

»-4

':•': ■'.'•':•'. •;•; ■•;

13 01 c 0»

r—1

'.■•'•':'.■'. V '.;•' ot

b o OT * w ' •* • * •*.*. '. • • ■

60- A 3.8. 10. 13

90 17 As above, loose to firm, wet. {•'•:•'.•'•:•'. v ■ *.'

-

y As above. r

/* ./

_ 1

Total DeDth = 64' M"" ' " ~ —

BMLTINU6

>K


Client Ealin AFB Site Blda. 6001 - Field No. 6 Boring T.D. SB6001-1 Geologist R. Surrencv

UJ " a —

65- :E

70-

75-

80-

85-

90-

95-

100-

U3

to o _l CO

0,0, 0,7

GC

90

Page 3 of 3 Project I.D. AT510.04 Well T.D. MW6001-1 Date Installed 2/4/92


SW

GRAPHIC LOG

WELL DIAGRAM

BMLTINU6

A-n


Clie Site Bor i Geol Dril Samp Date Date Dril Bore Dept Grou Dept Date

nt Ealin AFB Bldo. 6024 - Field No

ng I.D. SB6024-2 og ist/Enaineer R. Surrencv ling Method HSA 4.25 ID ling Method Split Sooon Started 2/5/92 Completed 2/5/92 ler Griner Drilling Co. hole Diameter (in) _§ h Drilled (ft) _EQ nd Elevation (ft) Not measured h to Water (ft) 57.85 Measured 2/5/92

UJ «

1 5:X

-X

-X

-X

25-

X

CO

CO X o _l CO

3.4. 6.8

2,2. 2.4

3.2, 3.3

5,4, 5.3

7.9. 9. 11

4,7, 9. 11

o UJ cr

80

50

85

90

90

80

O

10

10

11

11

12

13

Page 1 of 2 Project I.D. AT51Q.Q4 Well T.n. MWK024-1 Date Installed 2/5/92 Date Grouted 2/5/92 Casing Material 2" PVC Sch. 40 Screen Material same. 0.010 slot Casing Interval (ft) 0-50 Screened Interval (ft) 50-50 Sump Installed? No Well Depth (ft) 60 TOC Elevation (ft) Not measured Water Level (ft) 57.85 Date Measured 2/5/92


SAND, fine to coarse, yellowish brown, very loose to loose, slightly moist.

SAND, fine to medium, trace silt, yellowish brown, very loose, slightly moist.

SAND, fine to medium, some silt, reddish brown, very loose, slightly moist.

As above except very loose to loose.

SAND, fine to medium, some silt, reddish brown, loose to firm, slightly moist.

SAND, fine to medium, trace silt, white to light pink, loose to firm, moderately sorted, slightly moist.

4-t

sw

GRAPHIC LOG

WELL DIAGRAM

JZ

BMLTINU6


Client EQlin AFB Site Blda. 6024 - Field No. 6 Boring T.n. SB6024-2 RsnloQist R. Surrencv

SJ »J

30- :x

-X

40-

45-

50-

55-

Page 2 of 2

Project T.n. AT510.04 Well T.n. MWS024-1 Date Installed 2/5/92

-X

65-

(£>

CO X o _J CO

5, 12, 12. 14

5.9, 16, 14

5.9. 13.15

6. 14 . 14 . 16

9.11. 19.21

11.14, 18. 16

0.0, 4,5

cc

80

80

75

80

90

90

50

5» o e —. a. 3 Q.

12

12

450

600

200

240

35


SAND, fine to medium, orangish brown to white, firm, banded, moderately sorted, slightly moist.

As above except loose to firm.

SAND, fine to medium, white, loose to firm, well sorted, no odor, slightly moist.

SAND, fine to medium, trace silt, white, firm, well sorted, no odor, very moist.

As above except firm to very firm, no odor, moist.

SAND, fine to medium, well sorted, light brown to white, firm, no odor, moist to 55.7', wet at 55.7".

SAND, fine to medium, trace silt, orangish brown, very loose to loose, no odor, wet.

Total Depth = 60'

GRAPHIC LOG

SW

WELL DIAGRAM

3 a c (3

V i i i

* ? ? ? i ? ? % %

\

10 a.

! ii

T a > c 0)

c « 0)

1

<0

C (0 o

^

BMLTINU6


Cl ien Site_ Borin Geolo Drill Samp 1 Date Date Drill Boreh Depth Groun Depth Date

t Eolin AFB Blda. 792 - Ealin Main g I .D. gist/E ing Me ing Me Starte Comple er Gri

SB792-1 Surrencv

4.25 ID ngineerj thod HSA thod Split Spoon d 2/10/92 ted ner

2/10/92 Drilling Co

ole Di Drill

d Elev to Wa

Measur

(in) 13

ameter ed (ft) ation (ft) ter (ft) Not ed 2/11/92

Not measured measured

Q" <"

5-

10-

15-

20-

25-

10 en o _l CD

Hand Auger

2, l. 1 .3

1.3, 3.6

o LU CE

100

80

50

24

17

34

Page 1 of 1

Pro j Well Date Date Cas i Sere Casi Sere Sump Well TOC Wate Date

ect I.D. AT510.04 I.D. MW792-1 Installed 2/10/92 Grouted 2/11/92

ng Material 2" PVC Sch. 40 en Material same. O.OIO slot ng Interval (ft) 0-3 ened Interval (ft) 3-13 Installed? No Depth (ft) 13

Elevation (ft) Not measured r Level (ft) Not measured

Measured 2/11/92


SAND, fine to medium, moderately sorted, tan to light brown, slightly moist.

SAND, fine to medium, moderately sorted, tan to white, very loose, wet.

SAND, medium to coarse, trace silt, poorly sorted, tan to white, very loose to loose, wet.

Total Depth = 13'

SW

GRAPHIC LOG

WELL DIAGRAM

BHLTINU6

A-iO


Clien Site_ Bor in Geolo Drill Sampl Date Date Drill Boreh Depth Groun Depth Date

t Ealin AFB Blda. 91129 - Hurlburt Field g T n. qRQ1129-2

R. Surrencv gist/Engineer, ing Met-hnrl HSA 4.25 ID ing Mpt-hnd Split Spoon Parted 2/3/92 Completed, en Griner

2/3/92 Drilling Co

ole Diameter (in) Drilled (ft) 14

d Elevation (ft) to Water (ft) _9

Measured 2/4/92

Not measured 73

Q. LU o

-I

10-

20-

25-

-^ in ■x. o _i m

3.5. 5.5

3.5. 5.2

2.3. 3.5

3,4. 9. 12

o LU CC

90

75

75

30

>■ — O E •— a. 3 a.

0.3

200

0.3

Page 1 of 1 Project T.n. AT510.04 Well T.n. MW91129-1 Date Installed 2/3/92 Date Grouted_2/3/92 Casing Material 2" PVC Sch. 40 Screen Material same. 0.010 slot Casing Interval (ft) 0-4 Screened Interval (ft) 4-14 Sump Installed?_No Well Depth (ft) _1A T0C Elevation ff+1 Not measured Water Level (ft) 9.73 Date Measured 2/4/92


SAND, medium to coarse, trace silt, reddish brown, shell fragments, asphalt fragments, loose, slightly moist.

SAND and SILT, reddish brown, wood fragments, very loose to loose, gray sand at 5.5', slightly moist, wet at 5.8'.

SAND, fine to medium, some silt, black, wood fragments at 10', slight organic odor, very loose to loose, wet.

SAND, medium to coarse, white, wood fragments at 15", very loose to firm, well sorted, wet.

Total Depth - 14'

GRAPHIC LOG

SW

SM

SW >.Vv\'*.'»

WELL OIAGRAM

BMLTINU6

A~*


Cl ien Site_ Bor in Geo lo Drill Samp 1 Date Date Drill Boreh Depth Groun Depth Date

t Ealin AFB Blda. 981 - Ealin Main 9 I.D. SB981-1

R gist/Engineer ing Method HSA ing Method Split Started 2/10/92 Completed, er Griner

Surrencv 4.25 ID

Spoon

2/10/92 Drilling Co

ole Diameter (in) 6 Drilled (f t) _44____

d Elevation (ft) Not to Water (ft) 41 .32

Measured

measured

2/11/92

10-

20-

25-

n

CO

en x o _J GO

Hand Auger

l.i. 1. 1

1.1. l .2

1.3. 3.5

6.9, 12.15

3.9. 13.17

LLl CC

100

70

B0

90

80

80

o 3

600

320

360

80

12

Page 1 of 2

Pro j ect I.D Well T.n. MW9B1-1

AT510.04

Date Installed 2/10/92 Date Grouted 2/11/92 Casing Material 2" PVC Sch. 40 Screen Material same. 0.010 slot Casing Interval (ft) 0-34 Screened Interval (ft) 34-44 Sump Installed?_No Well Depth (ft) A4 TOC Elevation (ft) Not measured Water Level (ft) 41.32 Date Measured 2/11/92


SAND, fine to medium, moderately sorted, tan to light brown, slightly moist.

As above except brown and very loose.

SAND, fine to medium, moderately sorted, brown, very loose, slightly moist.

SAND, fine to medium, trace silt, moderately sorted, yellowish brown to tan, very loose to loose, slightly moist.

SAND, fine to medium, well sorted, orangish brown, loose to firm, slightly moist.

SAND, fine to medium, well sorted, orangish brown to white, loose to firm, slightly moist.

SW

GRAPHIC LOG

WELL DIAGRAM

3 O C (9

9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9

9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9

A-i'L*

S3-

o <o *> 01 C (0 <u

• m

j BMLTINU6


Client Ealin AFB Site Blda. 981 - Ealin Main

Boring T.n. spgai-i Rpnlnnist R. Sumencv

S£

30- X

35-

40-

45-

50-

to 00 X o _l CO

9. 18. 25,31

9, 13. 18.27

6. 10 , 19.25

6, 15. 19.52

80

80

50

70

55-

60-

Page 2 of 2 Project T.n. AT510.04 Well T.n. MW981-1 Date Installed 2/10/92

o e --» a.

13

12

11

11


SAND, medium to coarse, poorly sorted, orangish brown to white, firm to dense, slightly moist.

SAND, fine, well sorted, white, firm to very firm, slightly moist.

SAND, medium to coarse, poorly sorted, light gray to white, loose to very firm, wet.

SAND, medium to coarse, poorly sorted, brown, firm to very dense, wet.

Total Depth = 44'

GRAPHIC LOG

SW

WELL DIAGRAM

c 01

T

1

65-

A-&>

BMLTINU6


Client Ealin AFB Rii-p Rlf-fa. 9990 - C3D6 San Bias Rnrinn T . D . SB9990-1 Rpnlngist/Enaineer R. nnillinq Method HSA 4.

Surrencv 25 ID

Samolina Method SDI it Sooon nstP Starter! 2/13/92 Date Completed 2/13/92 nniilpn Rriner Drillina Co. Borehole Diameter (in) Depth Drilled (ft) 12 Ground Elevation (ft) Depth to Water (ft) 2. nate Measured 2/13/92

6

Not measured 82

10-

15-

20-

25-

to CO ae o _i CO

Post Hole

2,3. 6,11

2.3. 3.6

LU

100

70

50

Page 1 of1 AT510.04 Pro j ect I.D,

Well T.n. MW9990-1 Date Installed 2/13/92 Date Grouted 2/13/92 Casing Material 2" PVC Sch. 40 Screen Material same. 0.010 slot Casing Interval (ft) 0-2 Screened Interval (ft) Sump Installed? No Well Depth (ft) _12__

3-18

TOC Elevation (ft) Not measured Water Level (ft) 2.82 Date Measured 2/13/92

o e --» o. LITHOLOGIC DESCRIPTION

SAND, fine, light brown, slightly moist.

SAND, fine, white, very loose to firm, wet.

SAND, fine, gray, very loose to loose, wet.

Total Depth =» 12*

GRAPHIC LOG

SW

WELL DIAGRAM

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APPENDIX B ANALYTICAL DATA

ANALYTICAL DATA BATCH 8794

ENGINEERING-SCIENCE

MEMORANDUM

March 30,1992

To: File

From: J. A. Banton

Subject: Eglin AFB, Job No. AT510.04 Data Review, UST Sites Batch 8794

TPH (E418.1) analyses met QA/QC criteria for holding times, blanks, and matrix spike/matrix spike duplicates.

BETX and MTBE (E602) analyses met QA/QC criteria for holding times, blanks, matrix spike/matrix spike duplicate, and surrogate recoveries. Benzene results that were analyzed by E602 failed to meet USAF maximum allowable detection limits; however, the detection limits did meet Florida petroleum contamination site clean-up criteria maximum allowable detection limits.

EDB (E504) analyses met QA/QC criteria for holding times, LCS matrix spike/matrix spike duplicate, and surrogate recoveries.

Lead (E239.2) analyses met QA/QC criteria for holding times. The matrix spike/matrix spike duplicate had a low percent recovery. The lead result in sample MW4204 was flagged "J" due to this problem.

1,2-DCE (E601) analyses met QA/QC criteria for holding times, blanks, matrix spike/matrix spike duplicate, and surrogate recoveries.

PAH (E610) analyses met criteria for blanks and surrogate recoveries. The samples MW91129-1, MW9160-1, MW6024-1, MW6001, MW4204, and UST-ER1 exceeded holding times criteria. All the compounds were flagged in the associated samples "UJ" along with the detection limit due to this problem. The compounds naphthalene, acenaphthylene, acenaphthene, benzo-(a)-anthracene, chrysene, and dibenzo(a,h)anthracene/ indeno(l,2,3-cd)pyrene had low percent recovery in the matrix spike/matrix spike duplicate. These compounds were flagged "J" due to this problem in sample MW4204 (the spiked sample). In addition, the RPDs for all the

AT510\923J189

e>-\

ENGINEERING-SCIENCE

Memorandum to File Page 2 March 30, 1992

compounds in the matrix spike/matrix spike duplicate did not meet criteria. This problem require no flagging activity.

ENGINEERING-SCIENCE, INC.

J. A. Banton Chemist, ES Atlanta

AT510\923J189

4-a,

HI "TT H 1 J.I 1 ■CBY 717.it «FBI 1 «.' ̂ >;-^:'.;-:JGI ^^

Tf SfißKÄTl^ I i i

Is^jggggs ' / 1 1 1 w JJJJ-i-^ T/T L -7 7 / 1 1 1 \ I X. >

SOUTHWEST LABORATORY OF OKLAHOMA, INC.

March 20, 1992

Ola Awosika ENGINEERING SCIENCE, INC. 57 Executive Park South, Suite 5 90 Atlanta, GA 30329

Project: AT 510 '"-■■ SWLO Episode #: 879J:;*;8%- 8f|4.10

Dear Mr. Awosika:;

Enclosed we are. ilbmittincf the analytical results for your samples received in our^laboratory on February 20, 1992 for the abovejfeaptioned project.

If, in ymr review, you should have any questions or require additional informa^ion, please call.

Sincerely,

Daryl Alstatt Project Officer

DA/rb

Enclosures * N>

•v'

1700 WEST ALBANY • BROKEN ARROW, OK 74012 (918)251-2858 • FAX (918) 251-2599

6-3

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mrmrn SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Albanv • Broken Arrow. Oklahoma ""-+012

CLIENT: ENGINEERING SCIENCE, INC. 57 EXECUTIVE PARK SOUTH, SUITE 590 ATLANTA, GA 30329 ATTN: OLA AWOSIKA

Office (918) 251-2858 • Fax l91«) 251-2H5«

REPORT: 8794.01 - .10HV

DATE: 03-19-92

SAMPLE MATRIX: WATER SWLO #: 8794.01 - .10 DATE SUBMITTED: 02-20-92 DATE ANALYZED: 02-24-92 PROJECT: AT 510

METHOD REFERENCE FOR 1,2-D ICHLOROETHÄ»8i EPA 601

SWLO "*i :* D«i- CT.TENT ID T.D * #3TMIT TIKTT RESULT

MW91129-1 8794.01 :;;, i-P; ug/L ND

MW91601-1 8794.02 ::S 1.0- ug/L ND

UST-TB1 8794.03 1 1-0 ug/L ND

MW6024-1 8794.04 M 1.0 ug/L ND

MW6001-.i:,A-.:*-x ,8794.05 1.0 ug/L ND

MW4204fl '■i:lm®M6 1.0 ug/L ND

UST-BR1 8794.10 1.0 ug/L ND

Co

ND = NOT DETECTED ABOVE QUANTITATION LIMIT EPA = #EPA600/4-79-020, MARCH 1985 SM = STANDARD METHOD, 16TH EDITION

■•-^i

6-G-

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1"00 West Alhanv • Broken Arrow. Oklahoma ~-t012 Office (918) 251-2858 Fax (918) 251-285*

CLIENT: ENGINEERING SCIENCE, INC. 57 EXECUTIVE PARK SOUTH, SUITE 590

ATLANTA, GA 30329

ATTN: OLA AWOSIKA

REPORT: 8794.01 - .10HVS

DATE: 03-19-92

SWLO # 8794 METHOD REFERENCE:

PROJECT: AT 510

EPA 601

SAMPLE I.D.

8794.01

8794.02 8794.03 8794.04

8794.05 8794.06

8794.10

HALOGENATED VOLATILE QA/QC SURROGATE RECOVERIES

COMPOUND

CIS-1,2-DIQ^OROETHlNE CIS-1, 2-DICHli(|ROE,]ggENE CIS -1, 2 - DI CHLÖfKHEPHENE CIS-1,2-DICHLORÖE5HENE CIS-1, 2-DICHL%OETSBBNE C I#-1, 2 -DI CHLOSOETHINE

Cli-1, 2-DICHLof£>ETHENE

PBPOKNT RECOVERY

96% 97%

103% 106% 105%

96% 108%

CM

D J B

= SURROGATE DILUTED OUT = ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATION = ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE = SURROGATE RECOVERY OUTSIDE OF QC LIMITS

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■'■■-->'■

^Wffe^g /-/ / M v*xv/

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Albany Broken Arrow. Oklahoma ""-+012 • Office (918) 251-2858 • Fax (918) 251-2858


REPORT: 8794.01

DATE: 03-20-92

10EDB

SAMPLE MATRIX: WATER SWLO #: 8794.01 - .10 METHOD REFERENCE: EPA 504.1 DATE SUBMITTED: 02-20-92 DATE EXTRACTED: 02-24-92 PROJECT: AT 510

RESULTS REPORTED IN ug/:#br PARfS PER BIElTON

CLIENT ID

MW911£$-1 MW91SÖ1-1 UST-2B1 MW6024-1 MW600t-l MW4204-iM:"!; UST-ER1

SWLO :: DET.

I - D § LIMIT RESULTS DATE ANALYZED

mzxloi 0.01 ND 02-24-92

8794.02 0.01 ND 02-24-92

8794.03 0.01 ND 02-24-92

8794.04 0.01 ND 02-25-92

8794.05 0.01 ND 02-25-92

8794.06 0.01 ND 02-25-92

8794.10 0.01 ND 02-25-92


•"*«

ß-tf

SOUTHWEST LABORATORY OF OKLAHOMA, INC. POO West Alhanv Broken Arrow. Oklahoma 4012 Office (918) 251-2858 Fax (91«! 251-2858


REPORT: 8794.01 - , 10EDBSR

DATE: 03-20-92

SWLO # 8794 METHOD REFERENCE: PROJECT: AT 510

EPA 504.1

ffftMPT.E I.D.

8794.01 8794.02 8794.03 8794.04 8794.05 8794.06 8794.10

ETHYLENE DIBROMIDE QA/QC StÄROGATE RECOVERIES

r-riMPonND PWttCBNT RECOVERY

1,1,2, 2-TETfBSCHLOROifHANE 1,1,2, 2-TETRÄföBLORSäETHANE 1,1,2, 2-TETRAClR|ÖROETHANE 1,1,2,2-TETRACHLOSOETHANE 1,1,2, 2-TETRA%LORtS|THANE 1,1,2 , 2-TETRAC||üOROETHANE 1 Mi 2 i 2-TETRAc||JLOROETHANE

108% 109% 106% 107% 111% 106% 108%

D = SURROGATE DILUTED OUT J = ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATION B = ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE * = SURROGATE RECOVERY OUTSIDE OF QC LIMITS

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(14 •' U 9 ■' 9 2 14 : 1)6 ©918 2512599 SOUTHWEST LAB @ 002

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1700 West Albany • Broken Arrow, Oklahoma 74012 • Office (918) 251-2858 • Fax (918) 251-2858

CLIENT: ENGINEERING SCIENCE, INC. 57 EXECUTIVE PARK SOUTH, SUITE S90 ATLANTA, GA 30329 ATTN: OLA AWOSIKA

REPORT: 8794.01 - . 10TPH

DATE: 03-20-92


METHOD REFERENCE FOR TOTAL PETROLEUM;1 HYDROCARBON :

switf%-,. DEZ. CLIENT ID I.D LIMIT. UKIT RES

MW91129-1 8794.01 0,5 mg/L ND MW91601-1 3794.02 0.5 mg/L ND UST-TB1 8794.03 o.s mg/L ND MW6024-1 S794.04 o.s mg/L ND MW6001-1 :. S794.OS* 0.5 mg/L ND MW4204-1 8794.06 0.5 mg/L ND MW4204-1 DUP 8794.07 0.5 mg/L 28 MW4204-1 MS 8794.03 0.5 mg/L 25 USTT-ERI 8794.10 0.5 mg/L ND

ND = NOT DETECTED ABOVE QUANTITATION LIMIT EPA = #EPA600/4-79-02O, MARCH 19B5 SM = STANDARD METHOD, 16TH EDITION

-++ 'iijimmi

Hf / ' ' t^hKS&h ■//-/■rj-} •$&?&. t i ; I ! iWV.4

SOUTHWEST LABORATORY OF OKLAHOMA, INC. "00 West Alhany Broken Arrow. Oklahoma ~-+012


Office (918) 251-2858 • Fax (918) 251-285H

REPORT: 8794.01 - .10LD

DATE: 03-20-92


METHOD REFERENCE FOR LEAD:

SWLO

E«Ä::2:3,9

DEÜ

2

rT.TRNT TD T . D 'S?:;:;., ^^ftlT UNIT RESULT

MW91129-1 :;:#79*-iM, 3.0 ug/L 26.6

MW91601-1 8794.02% 3V.Q. ug/L 21.4

MW6024-1 8794.04 : 3.0 ug/L 10.2

MW6001-1 8794.05 h 3.0 ug/L ND

MW4204-1 8794.06 1 • 3.0 ug/L 6.9T MW4204-1 B8F' :, 8794.07 3.0 ug/L 8.0 J MW4204F1 MS fc?S4.08 3.0 ug/L 16.5 J" UST-ER1 : 8794.10 3.0 ug/L ND


'-■1

&rW

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 VC'esr Aihanv Broken Arrow. Oklahoma ~-t012 • Office (918) 251-2858 • Fax (918) 251-2858


REPORT: 8794.01BX

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO #: 8794.01 METHOD REFERENCE: EPA 602 DATE SAMPLED : 02-19-92 DATE SUBMITTED: 02-20-92 DATE ANALYZED: 02-21-92 PROJECT: AT 510 SAMPLE ID: MW91129-1

PARAMETER

ftAS CHBOMATOGRAPHY

BENZENE TOLUENE ETHYLBENZENE XYLENES MTBE

DET.

1.0

:Si;;.o 1.0 1.0

UNIT

ug/L ug/L ug/L ug/L ug/L

RESTTT.TS

ND

ND

ND

ND

ND

CD

pA/or SURROGATE RECOVERIES

4-BROMOFLUOROBENZENE (65-135%) 94%

ND = NOT DETECTED ABOVE QUANTITATION LIMIT B = ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE J = ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATION * = SURROGATE RECOVERY OUTSIDE OF QC LIMITS ON ORIGINAL RUN AND RERUN. SW = TEST METHODS FOR EVALUATING SOLID WASTE, EPA PUBLICATION #SW846, THIRD

EDITION, NOVEMBER 1986

S-i"Z-

"fl"T ' ui^r

4^W^ SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 «est Albanv Broken Arrow Oklahoma "4012 • Office (918) 251-2858 • Fax (91«) 251-2858

CLIENT: ENGINEERING SCIENCE, INC. 5 7 EXECUTIVE PARK SOUTH, SUITE 590

ATLANTA, GA 30329

ATTN: OLA AWOSIKA

REPORT: 8794.01P

DATE: 03-20-92

SAMPLE MATRIX: WATER

SWLO #: 8794.01 DATE SUBMITTED: 02-20-92

DATE EXTRACTED: 02-28-92

DATE ANALYZED : 03-06-92

METHOD REFERENCE: EPA 610

PROJECT: AT 510 SAMPLE ID: MW91129-1

RESULTS REPORTED IN ug/t|,OR Par|s Per Billion (PPB)

pr.TYVTTrT.KAW AROMATIC HYDROCRRBOMS

NAPHTHALENE ACENAPHTHYLENE

ACENAPHTHENE

FLUORENE PHENANTHRENE

ANTHRACENE FLUORANTHENE \

PYRENE BENZO(A)ANTHRACENE

CHRYSENE BENZO ( B) FLUORANTHlfi;i:

BENZO(K)FLUORANTHENE

BENZO(A)PYRENE

DIBENZO(A,H)ANTHRACENE/ INDENOU, 2, 3-CD)PYRENE **

BENZO(G,H,I)PERYLENE

nttTPICTTOM LIMIT

1.0 1.0 1.0 1.0 1.0

RESULTS

ND 7~ ND _"" ND"'" ND 7 ND ""' ND " ND"' ND ND" ND 7" ND 7" ND '"" ND r NDT NDC ND ^

fVlf STTWPnftATP! RBmVHBTES

2-FLUOROBIPHENYL

p-TERPHENYL

102.3%

88%

en m

ND = NONE DETECTED ABOVE QUANTISATION LIMIT J = ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATION

B = ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE

* = SURROGATE RECOVERY OUTSIDE OF QC LIMITS

** = THESE COMPOUNDS COELUTE (AS INDICATED IN METHOD 610).

0,-13

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Alhanv Broken Arrow. Oklahoma ~~t0\2 • Office (918) 251-2858 • Fax (918) 251-2858

CLIENT: ENGINEERING SCIENCE, INC. 5 7 EXECUTIVE PARK SOUTH, SUITE 590 ATLANTA, GA 30329 ATTN: OLA AWOSIKA


REPORT: 8794.02BX

DATE: 03-20-92

PARAMETER

GAS CHROMATOGRAPHY

BENZENE TOLUENE ETHYLBENZENE XYLENES MT BE

DET.

1.0

1,,,Q1P" i:fo 1.0 1.0

™TT


RESULTS

ND ND ND ND ND

"M

QA/OC SURROGATE RECOVERIES




6-14-

SOUTHWEST LABORATORY OF OKLAHOMA, INC. POO West Albany • Broken Arrow. Oklahoma 74012 • Office (918) 251-2858 • Fax (918) 251-2S58


SAMPLE MATRIX: WATER SWLO #: 8794.02 DATE SUBMITTED: 02-20-92 DATE EXTRACTED: 02-28-92 DATE ANALYZED : 03-06-92 METHOD REFERENCE: EPA 610 PROJECT: AT 510 SAMPLE ID: MW91601-1

REPORT: 8794.02P

DATE: 03-20-92

RESULTS REPORTED IN ug/t OR Part|& Per Billion (PPB)

pr>T.VTmci,E»B AROMATIC HYDROCARBONS

NAPHTHALENE ACENAPHTHYLENE ACENAPHTHENE FLUORENE PHENANTHRENE ANTHRACENE FLUORANTHENE PYRENE BENZO(A)ANTHRACENE CHRYSENE BENZO ( B) FLUORANTHffliP* BENZO(K)FLUORANTHENE BENZO(A)PYRENE DIBENZO(A,H)ANTHRACENE/

INDENO(1,2,3-CD)PYRENE BENZO(G,H,I)PERYLENE

nr.ARBONS hFTECTTOH

♦ :- 1.0

LIMIT RESULTS

ND7' 1.0 ND7*

1.0 ND "•"

1.0 ND '

1.0 ND 7

1.0 ND X

1.0 NDT

1.0 NDT 1.0 ND"' 1.0 ND'' 1.0 ND • 1.0 NDT

1.0 NDT

1.0 ND 7

** 1.0 1.0

ND? ND^"

QAVQC SURROGATE RRnOVBRIES

2-FLUOROBIPHENYL 95.8%

p-TERPHENYL 84.8%

ND J B

NONE DETECTED ABOVE QUANTITATION LIMIT ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATION ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE SURROGATE RECOVERY OUTSIDE OF QC LIMITS THESE COMPOUNDS COELUTE (AS INDICATED IN METHOD 610).

6-IS

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 Wesr Albany Broken Arrow. Oklahoma --+012 • Office (918) 251-2858 • Fax (918) 251-2858

CLIENT: ENGINEERING SCIENCE, INC. 5 7 EXECUTIVE PARK SOUTH, .SUITE 590 ATLANTA, GA 30329 ATTN: OLA AWOSIKA

REPORT: 8794.03BX

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO #: 8794.03 METHOD REFERENCE: EPA 602 DATE SAMPLED : 02-19-92 DATE SUBMITTED: 02-20-92 DATE ANALYZED: 02-21-92 PROJECT: AT 510 SAMPLE ID: UST-TB1

PARAMETER ^ET.

- ttüftr ITOTT 1

RAS CHROMATOORAPHY

BENZENE TOLUENE ETHYLBENZENE /:>" XYLENES MTBE

1.0 ... ..!*#"

"■-:::"::-f:o 1.0 1.0


0A/0C SURROGATE RECOVERIES


RESULTS

ND ND ND ND ND



6-It

SOUTHWEST LABORATORY OF OKLAHOMA, INC. l-00 Wesr Albany Broken Arrow. Oklahoma "4012 • Office (918) 251-2858 • Fax (918) 251-2858

CLIENT: ENGINEERING SCIENCE, INC. 57 EXECUTIVE PARK SOUTH, .SUITE 590 ATLANTA, GA 30329 ATTN: OLA AWOSIKA

REPORT: 8794.04BX

DATE: 03-20-92


PARAMETER

OET. TIKTT RESULTS

CAS CHROMATOGRAPHY

BENZENE TOLUENE ETHYLBENZENE :fW XYLENES MTBE

1.0

1.0 1.0


ND

ND

ND

ND

ND

or» -73

0A/0C SURROGATE RECOVERIES ' "^


ND = B = J = * =

SW =

NOT DETECTED ABOVE QUANTITATION LIMIT **" ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATION SURROGATE RECOVERY OUTSIDE OF QC LIMITS ON ORIGINAL RUN AND RERUN. TEST METHODS FOR EVALUATING SOLID WASTE, EPA PUBLICATION #SW846, THIRD


ß-17

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SOUTHWEST LABORATORY OF OKLAHOMA, INC. l-00 West Alhanv • Broken Arrow. Oklahoma "4012 • Office (918) 251-2858 « Fax (918) 251-2858


REPORT: 8794.04P

DATE: 03-20-92


RESULTS REPORTED IN ug/sffOR Par# Per Billion (PPB)

p^r.vMTTPT.WAB AROMATIC Hvrmnr.ARBONS ttETECTIQH LIMIT BESHLXS

NAPHTHALENE ACENAPHTHYLENE ACENAPHTHENE FLUORENE PHENANTHRENE ANTHRACENE FLUORANTHENE PYRENE BENZO(A)ANTHRACENE CHRYSENE BENZO ( B) FLUORANTHSi*£ ;ft

BEN ZO(K)FLUORANTHENE BENZO(A)PYRENE DIBENZO(A,H)ANTHRACENE/

INDENO(l,2,3-CD)PYRENE ** BENZO(G,H,I)PERYLENE

1.0 1.0 1.0

,0 .0 .0 .0 .0 .0 .0 .0 .0 .0 .0

1.0 1.0

ND," ND -r NDT ND*" ND"f ND T ND7 NDT ND-r NDT* NDT" ND* NDT NDT ND"T

ND T

OA/OC SOTWOOATF RgmVgttlES

2-FLUOROBIPHENYL p-TERPHENYL

76.5% 82.2%

c-

ND = NONE DETECTED ABOVE QUANTITATION LIMIT J = ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATION B = ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE * = SURROGATE RECOVERY OUTSIDE OF QC LIMITS ** = THESE COMPOUNDS COELUTE (AS INDICATED IN METHOD 610).

6-17

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~"00 West Alhanv • Broken Arrow. Oklahoma "4012 • Office (918) 251-2858 • Fax (918) 251-2858


REPORT: 8794.05BX

DATE: 03-20-92


PARAMETER BET. "<:i

_UM1I_ RESULTS

GAS CHROMATOGRAPHY


l.C

::r::o 1.0 1.0


ND ND ND ND ND

OA/QC SURROGATE RECOVERIES




T-,f

ö-l^

SOUTHWEST LABORATORY OF OKLAHOMA, INC. POO West Albany • Broken Arrow. Oklahoma "4012 • Office (918) 251-2858 • Fax (9\H) 251-2H58



REPORT: 8794.05P

DATE: 03-20-92

RESULTS REPORTED IN ug/i|ÖR Par# Per Billion (PPB)

PflTiYM™^™* awoMATTr ffvnWQCARBONS

NAPHTHALENE ACENAPHTHYLENE ACENAPHTHENE FLUORENE PHENANTHRENE ANTHRACENE FLUORANTHENE PYRENE BENZO(A)ANTHRACENE CHRYSENE BENZO (B) FLUORANTHliaPS?::

BENZO(K)FLUORANTHENE BENZO(A)PYRENE DIBENZO(A,H)ANTHRACENE/


tlWTWCTTOM LIMIT

:b:- 1.0 1.0 1.0 1.0

WKSUT/TS

ND(f NDT NDT ND,r NDT NDf ND:

NDJ NDT ND7" ND"; ND;

ND T NDT ND T

NDv'

n*(pr sTTPwnnaTW BBrnranTHg


59.1% 57.2%

CD

ND J B

NONE DETECTED ABOVE QUANTITATION LIMIT ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATION ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE SURROGATE RECOVERY OUTSIDE OF QC LIMITS THESE COMPOUNDS COELUTE (AS INDICATED IN METHOD 610).

&-20

SOUTHWEST LABORATORY OF OKLAHOMA, INC. rOO West Albany • Broken Arrow. Oklahoma --+012 • Office (918) 251-2858 • Fax (918) 251-2858



REPORT: 8794.06BX

DATE: 03-20-92

PARAMETER

P.ftfi r-HTiOMATOGRAPHY

BENZENE TOLUENE ETHYLBENZENE XYLENES

MTBE

DET. ;!

LIMIT

1.0 1 • Qd i.tf 1.0 1.0

JffilX-


RESULTS

ftA/ftf! SITRROftATtt RECOVERIES


ND ND ND ND ND

cry en

ND B J *

sw

NOT DETECTED ABOVE QUANTITATION LIMIT ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATION SURROGATE RECOVERY OUTSIDE OF QC LIMITS ON ORIGINAL RUN AND RERUN. TEST METHODS FOR EVALUATING SOLID WASTE, EPA PUBLICATION #SW846, THIRD


ß-a/

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 Wesr Albany • Broken Arrow. Oklahoma "-+012 • Office (918) 251-2858 • Fax (918) 251-2858



REPORT: 8794.06P

DATE: 03-20-92

RESULTS REPORTED IN ug/:||ÖR Partf Per Billion (PPB)

pftT,YUiTrT.WAB AWOMATTC HYDROCARBONS ftBTgCTIOM LIMIT

NAPHTHALENE ACENAPHTHYLENE ACENAPHTHENE FLUORENE PHENANTHRENE ANTHRACENE FLUORANTHENE ';■ PYRENE BENZO(A)ANTHRACENE CHRYSENE BENZO (B) FLU0RANTHB8I: BENZO(K)FLUORANTHENE BENZO(A)PYRENE DIBENZO(A,H)ANTHRACENE/


1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0

RESULTS

ND 7" ND T ND 7 ND J NDT ND V ND"f ND T NDJ- NDJ" ND~ NDT NDT NDT ND7 NDT

naftir strewnflATH BgrnvwuiBS


74.6% 80.0%


6-aa

I E SOUTHWEST LABORATORY OF OKLAHOMA, INC.

1~00 West Albany- Broken Arrow. Oklahoma "-+012 • Office (918) 251-2858 • Fax (918) 251-2858


SAMPLE MATRIX: WATER SWLO #: 8794.10 METHOD REFERENCE: EPA 602 DATE SAMPLED : 02-19-92 DATE SUBMITTED: 02-20-92 DATE ANALYZED: 02-21-92 PROJECT: AT 510 SAMPLE ID: UST-ER1

REPORT: 8794.10BX

DATE: 03-20-92

PARAMETER

rTAS PHttOMATOGRAPHY


DET. : LIKIT

1.0

fro 1.0 1.0

_UMIT_


RESITLTS

OA/OC SURROGATE RECOVERIES


ND ND ND ND ND

ND = B = J = * =

SW =



ß-33

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Albany Broken Arrow Oklahoma "4012 • Office (918) 251-2858 • Fax (918) 251-285-


REPORT: 8794.10P

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO #: 8794.10 DATE SUBMITTED: 02-20-92 DATE EXTRACTED: 02-28-92 DATE ANALYZED : 03-06-92 METHOD REFERENCE: EPA 610 PROJECT: AT 510 SAMPLE ID: UST-ER1

RESULTS REPORTED IN ug/:l;OR Part* Per Billion (PPB)

pnT.VMITCLEAW AROMATTP. HYDROCARBONS

NAPHTHALENE ACENAPHTHYLENE ACENAPHTHENE FLUORENE PHENANTHRENE ANTHRACENE FLUORANTHENE ■; :

PYRENE BENZO(A)ANTHRACENE CHRYSENE BENZO(B)FLUORANTHSSBB BENZO(K)FLUORANTHENE BENZO(A)PYRENE DIBENZO(A,H)ANTHRACENE/


IhBTttCTIOM LIMIT

•> 1.0 1.0 1.0

1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0

RESULTS

ND T ND7* ND 7* NDy ND,r ND""

ND7 NDT ND T ND T NDT ND';

ND""" NDvT

NDT NDJ-

na^r. siTBPnftATW RErrwFBTKS


87.9% 99.2%

CM m en


8-34-

SOUTHWEST LABORATORY OF OKLAHOMA, INC. rOO West Aibanv • Broken Arrow. Oklahoma "4012 • Office (918) 251-2858 • Fax (918) 2M-2S58

ANALYTICAL REPORT

ENGINEERING-SCIENCE INC. 57 EXECUTIVE PARK SOUTH ATLANTA, GEORGIA 3 0392

SWLO IDENTIFICATION

SAMPLE NO.: 8794.01-8794.10 DATE RECEIVED: 02/20/92

REPORT: 8794

REPORT DATE: 03/13/92

OA/QC

DESCRIPTION fiAAMEf ER RESULTS

METHOD BLANK 03/04/92 WSAD < 3.0 ug/L

BLANK SPIKE 03/04/9^:;: ''"■■^•^EAMX, 9 6% RECOVERY

MATRIX SPIKE MW20 4 -jf L%D 48% RECOVERY

DUPLICATE MW204-1 LEAD 14.76% RPD

ViV-

*"*■*"

ß-as

SOUTHWEST LABORATORY OF OKLAHOMA, INC. rOO West Albanv • Broken Arrow. Oklahoma "4012 • Office (918) 251-2858 . Fax (91S) 251-285*


ATLANTA, GA 30329

HTTN: OLA AWOSIKA

REPORT: 8794a

DATE: 03-19-92


SWLO #: METHOD BLANK DATE ANALYZED : 02-24-92


PROJECT: AT 510

SAMPLE ID: BLANK

RESULTS REPORTED IN ug/l||OR Paffs Per Billion (PPB)

HALOGENATED VOT.ATTI.ES

: DEE»;;::.. TJUHl RESULTS

1, 2-DICHLOROETtlANE si. 0 ND

oa^pc siTRnnnaTB RECOVERIES

CIS-l,2-DICHLOROETHENE (65%-135%) 94%

ND = NOT DETECTED ABOVE QUANTITATION LIMIT J = ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATION

B = ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE * = SURROGATE RECOVERY OUTSIDE OF QC LIMITS

fc'

1 B>'3C

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Albanv • Broken Arrow. Oklahoma "4012 • Office (918) 251-2858 • Fax (918) 251-2858


REPORT: 8794b

DATE: 03-19-92

SAMPLE MATRIX: WATER SWLO # 8794.08 - .09 (MS/MSD) DATE ANALYZED : 02-24-92 METHOD REFERENCE: EPA 601 PROJECT: AT 510 SAMPLE ID: MW4202-1 (MS/MSD)

TTftT-OttRNATEP vnr.aTTT.ES M»T«T*"%**»*/MATRIX SPTKK DUPLICATE RECOVERY

COMPOUND

1,2-DICHLOROETHAN|ff

SPIKE SAMPLE COMC. CONC. MS CONC.

jjBjbOd (ug/Ljf—Ua/ia

MS AMI FOUND PERCENT PERCENT MSD CONC. RECOVERY PERCENT BwrovwwY /ua/Li MSD BED

20.d';i:: siiP^ 17.2 86.0 18.4

MS MSD

frUHB^"1™ wrcrnvBRlES

CIS-1,2-DICHLOROETHENE CIS-1,2-DICHLOROETHENE

100% 97%

92.0 6.7

Ö-P7

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 VC'esT Albany 3ken Arrow. Oklahoma ~-t012 • Office (918) 251-2858 • Fax (918) 251-2858


SAMPLE MATRIX: WATER SWLO #: METHOD BLANK METHOD REFERENCE: EPA 602 DATE ANALYZED: 02-21-92 PROJECT: AT 510 SAMPLE ID: BLANK

REPORT: 8794c

DATE: 03-20-92

PARAMETER

KAS CHROMATOGRAPHY


1.0 1.0 1.0 ,:

10.0

UNIT


RESULTS

ND ND ND ND ND

QA/pr- SURROGATE RECOVERIES




l'"'

6-5T

SOUTHWEST LABORATORY OF OKLAHOMA, INC. "00 West Albany Broken Arrow. Oklahoma "4012 Office (918) 251-2858 Fax (918) 251-2858


REPORT: 8794d

DATE: 03-20-92

SAMPLE MATRIX: WATER DATE ANALYZED: 02-21-92 SWLO #: 8794 (MS/MSD) PROJECT: AT 510 SAMPLE ID: MW4204-1

PABA nn*m»

MATRIX SPIKE

SPIKE CONC. :'SÄMFfeB CONC- CONC. PERCENT

(ug/L) <ugj||) ; >;;:,. (ug/L) RECOVERY

BENZENE 10.0 o j 9.9 99.3%

TOLUENE . imW'- Q:# 9.3 93.1%

ETHYLBENZENE #10.0 :;:©•'•• 9.4 94.4%

TOTAL XYLENES ? 30.0 0 29.4 98.1%

MTBE 40.0 0 44.6 111.5%

MATRIX SPIKE DUP PERCENT REC. RECOVERY PERCENT

NSD CONC. (ug/L) (ug/L) DIFFERENCE

BENZENE 10.1 100.9% 1.60%

TOLUENE 9.5 95.4% 2.44%

ETHYLBENZENE 9.8 98.0% 3.74%

TOTAL XYLENES 30.4 101.3% 3.21%

MTBE 42.4 106.0% 5.1%

-,r> t V * IV«'

e>-3L°l

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 Wesr Albany Broken Arrow. Oklahoma ~-t012 • Office (918) 251-2858 • Fax (918) 251-2858


REPORT: 8794e

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO #: METHOD BLANK METHOD REFERENCE: EPA 504.1 DATE EXTRACTED: 02-24-92 DATE ANALYZED: 02-24-92 PROJECT: AT 510

RESULTS REPORTED IN ug/Jp'br PAR|£ PER BlÜilON

PARAMETER DE«*

ETHYLENE:: mBRÖMDE 0J$1

RESULT

ND

Oft/ft«* SITBWOCaTB RECOVERY

1,1,2,2-TETRACHLOROETHANE 10 3 %


^ .") O

■^

-'.)-■'

■c •** •v ■CLV

ß-30

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 Wesr Alhanv • Broken Arrow. Oklahoma "4012 • Office (918) 251-2858 • Fax (918) 251-2858

CLIENT: ENGINEERING SCIENCE, INC. 57 EXECUTIVE PARK SOUTH, SUITE .590 ATLANTA, GA 30329 ATTN: OLA AWOSIKA

REPORT: 8794f

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO #: 8794 LCS PROJECT: AT 510

T.AROHJgihORY CONTROL SPlkg

SPIJOS CöNC.

*ug/L)

ETHYLENE DIBROMIDE "^ 1.65

CONTROL SAMPLE CONC.

(«g/L)*

LCS CONC. LCS PERCENT (ug/L)* RECOVERY

1.67 101.5%

= DILUTION FACTOR NOT APPLIED TO THESE CONCENTRATIONS

8-3'

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1700 West Albany • Broken Arrow. Oklahoma 74012 • Office (918) 251-2858 • Fax (918) 251-2858


REPORT: 8794g

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO # 8794.08 - .09 (MS/MSD) DATE EXTRACTED: 02-24-92 DATE ANALYZED : 02-25-92 METHOD REFERENCE: EPA 601 PROJECT: AT 510 SAMPLE ID: MW4202-1 (MS/MSD)

wvrm.Km PT«»niiTa#iI>ret*SPraa/MATRIX SPIKB PUPLICMTi RECOVERY

COMPOUND

ETHYLENE DIBROMIÖE

Sf|KE SAMPLEJf .Ca|p. CONC. MS CONC. (11^::!,..J\>f/il (Vl/li)

MS AMX FOUND PERCENT PERCENT MSD CONC. RECOVERY PERCENT BBCOVBRY fua/H MSJ2 RED.

l.# 1.62 97

MS MSD

pnMnnm'1'» »««wi«

CIS-1,2-DICHLOROETHENE CIS-1,2-DICHLOROETHENE

1.80 108

106% 121%

11

>'

&-3^

-+-+1 i;: j n w> u

rf/'/yL/-)L iiÄ^^ÄSS

WfW SOUTHWEST LABORATORY OF OKLAHOMA, INC. nOO West Albany • Broken Arrow. Oklahoma 74012 Office (918) 251-2858 Fax (918) 251-2858


ATLANTA, GA 30329

ATTN: OLA AWOSIKA

REPORT: 8794h

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO #: METHOD BLANK DATE EXTRACTED: 02-28-92



PROJECT: AT 510 SAMPLE ID: WBLK022892-01

RESULTS REPORTED IN ug/1 0R Part* Per Billion (PPB)

pnT.VMTTrT.WAR AWOMATTC HYDROCARBONS


ACENAPHTHENE


ANTHRACENE FLUORANTHENE JW PYRENE BEN ZO(A)ANTHRACENE CHRYSENE BENZO (B) FLUORAIWSHENE..^

BENZO (K) FLUORANTHETte' :;

BENZO(A)PYRENE DIBENZO(A,H)ANTHRACENE/


«WttCTTOM LIMIT

1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0

RESULTS

ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

flA^pr STIPBOflATE WMTOTOEIBS


90.7% 78.6%


&-31

o-'tilMl.

TT/TT- TO« SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Albany Broken Arrow. Oklahoma 74012 Office (918) 251-2858 • Fax (918) 251-2858


SAMPLE MATRIX: WATER SWLO #: 8794 (MS/MSD) DATE EXTRACTED: 02-28-92 DATE ANALYZED : 03-06-92 PROJECT: AT 510 SAMPLE ID: MW4204-1 (MS/MSD)

REPORT: 8794i

DATE: 03-20-92

waTttP PAH MATBTT SPTCT! /MftgftlX SJETKF miPT.TttATE RBCQVBRY

r-OMPOUMD

SPIKE ADDED

(Ug/D

10.0 10.0 io.9;:: io€o

II il

o

NAPTHALENE ACENAPTHYLENE ACENAPTHENE FLUORENE PHENANTHRENE ANTHRACENE FLUORANTHENE PYRENE BENZO-(A)-ANTHRANCENE CHRYSENE BENZO-(B)-FLUORANTHENE BENZO-(K)-FLUORANTHENE BENZO-(A)-PYRENE DIBENZO(A,H)ANTHRACENE/ 20.0

INDENO(l,2,3-CD)PYRENE ** BENZO(G,H,I)PERYLENE 10.0

10J;ij; 10.0 10.0 10.0 10.0 10.0

AMT FOUND AMT PÖipBf MS AMT POUND PERCENT SAMPLB M« PERCENT MSD RECOVERY PBRCEHT /..g/nT /»g/T? iyr<™T ruo/H MSD BEfi

7. m 7«# 7,3 8.6 8.6 8.7 8.4 8.4 7.5 7.0 8. 8. 8. 8.

,9 ,4 ,4 ,1

8.4

76.2 79.0 78.8 85. 86. 87. 84. 84.2 75.2 70.1 81.1 84.2 84.2 41.3

83.9

10.6 10.8 10.8 11. 12. 11. 11. 11.7 9.9 9.3 10.8 11.3 11.1 11.7

12.0

106.2 108.0 107.9 119.4 121.2 118.5 115.4 117.4 99.1 93.4

107.7 113.2 110.6 .58.5

119.5

33. 30. 31. 32. 33. 30. 31. 32. 27. 28.5 28.2 29.4 27.1 34.5

35.1

fl*/ftr- snuwnoATg RECOVERIES


MS MSD 76.7% 106.7% 91.7% 110.0% *> <£

»VALUES OUTSIDE OF QC LIMITS

&-3+-

'■^'■'UiMk

£= SOUTHWEST LABORATORY OF OKLAHOMA, INC. H00 West Albany • Broken Arrow. Oklahoma 74012 • Office (918) 251-2858 • Fax (918) 251-2858


REPORT: 8794j

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO #: METHOD BLANK DATE ANALYZED : 02-25-92 METHOD REFERENCE: EPA 418.1 PROJECT: AT 510 SAMPLE ID: WBLK02249201

RESULTS REPORTED IN mg/fc^R Parjk Per Billion (PPB)

PARAMETER

™:|:;:DB*iS::, REVOLTS

TPH jl.5 ND

ND = NOT DETECTED ABOVE QUANTITATION LIMIT J = ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATION B = ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE * = SURROGATE RECOVERY OUTSIDE OF QC LIMITS

j*

G-3S

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1700 West Albany • Broken Arrow. Oklahoma ~<+012 • Office (918) 251-2858 • Fax (918) 251-2858


REPORT: 8794k

DATE: 03-20-92

SAMPLE MATRIX: WATER DATE ANALYZED: 02-25-92 SWLO #: 8794 (MS/MSD) PROJECT: AT 510 SAMPLE ID: MW4204-1

TPff Mff'rwTT SPTKg/MfcTRir SPIKE PÜLICMB

' s \ MATRIX SPIKE

SPIKE CONC. SÄMWUR COHC. COMC. PERCENT (ug/L) (ug)% (ug/L) RECOVERY

TPH 31.0 25.1 81.0%

,V -f" ■ X

3-36

03/26/92 15:39 ©918 2512595 SOUTHWEST LAB ifcj U U -i

pjl A~ --!- ■II M LXTT"

+ - 3+

_u_! 1 1 .IK- A

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1700 West Albany • Broken Arrow, Oklahoma 74012 • Office (918) 251-2858 • Fax (918) 251-2S58

CLIENT: ENGINEERING SCIENCE, INC. 57 EXECUTIVE PARK SOOTH, SUITE 590

ATLANTA, GA 30329 ATTN: OLA AWOSIKA

SAMPLE MATRIX: WATER DATE ANALYZED: 02-25-92 SWLO #: B794 (MS/MSD) PROJECT! AT 510 SAMPLE ID: MW4204-1

REPORT: 8794k

DATE: 03-20-92

TPH MATRIX KPTKg/MA^BTT SPIKE THTPLICftXE

TPH

SPIKE CONC. <ug/L)

31.0

SAMPLE CONC. (ug/L)

MAIRIX SPIKE CONC. (ug/L)

PERCENT RECOVERY

25.1 81.0%

TPH

MSD CONC. (ug/D*

27.9

MSD PERCENT RECOVERY

90%

RECOVERY PERCENT DIFFERENCE

10.6%

6-37

03'26/92 15:38 ©918 2512599 SOUTHWEST LAB lä 001

FAX NUMBER 918-251-2599

U §KI

m&mz 3-26-?^

1T@S NAME:

CLIENT;

SUBJECT;

FAX #

[MMffl]* NAME:

,4l4 JjjA ^£ÜQX^

^__f^M^^~ f&f&Ä£~.-

LABORATORY:

£Wy/ Msirdt._.

ffXo»MliU&

ÜMM1IS13G8 <m mi

For your comments Please call me about this Information only

As you requested JL AS we discussed Review and forward

■A (Including this cover page)

©J* QiRQ©T}mD(gP@GM £<o

If you have any problems with this transmission

please call ...— at (918)251-2858.

6-37

03•■26.'92 15:39 ©Öl» 25125Ö» iOLinntJi LAD

-J S 'i!

-j

iVm"

il ■'iPrTao *v

.,_7 _, / X/X7 rz^/i 1 IZ _£U—1


March 26, 1992

Ola Awosika ENGINEERING SCIENCE, INC. 57 Executive Park South, Suite 590 Atlanta, GA 30329

Project: AT 510 SWLO Episode #: 8794.01 - 8794.10

Dear Mr. Awosika:

Enclosed we are submitting the corrected TPH MS/MSD report ror'your Samples received^ our laboratory on February 20 1992 for the above-captioned project. We regret any inconvenience this may have caused.

If, in your review, you should have any questions or require additional information, please call.

Sincerely,


DA/rb

Enclosures


&-3?

Ü3'26'92 15:39 ©91S 2512599 SUÜlh«t.i>i LAti

BSl IS:.;. % .^i

SOUTHWEST LABORATORY OF OKLAHOMA, INC, 1700 Vest Albany • Broken Arrow, Oklahoma 74012 • Office (916) 251-2858 * Fax (918) 251-2S5S

CLIENT: ENGINEERING SCIENCE, INC. 57 EXECUTIVE PARK SOUTH, SUITE 590 ATLANTA, GA 30329 ATTN: OLÄ AWÖSIKA

SAMPLE MATRIX: WATER DATE ANALYZED: 02-25-92 SWLO #s 8794 (MS/MSD) PROJECT: AT 510 SAMPLE ID: MW4204-1

REPORT: 8794k

DATE: 03-20-92

TPH MflTKIX_SEJKEZMftXBT7 ffPTKF mFPLICME

TPH

SPIKE CONC. (ug/L)

31.0

SAMPLE CONC. (ug/L>

MATRIX SPIKE CONC. (ug/L)

PERCENT RECOVERY

25.1 81.0%

TPH

MSD CONC. (ug/L)*

27.9


90%


10.6%

ß-3^

ENGINEERING-SCIENCE

MEMORANDUM

March 30,1992

To: File

From: J. A. Banton


TPH (E418.1) analyses met QA/QC criteria for holding times, blanks, and matrix spike/matrix spike duplicates.

BETX and MTBE (E602) analyses met QA/QC criteria for holding times, blanks, matrix spike/matrix spike duplicate, and surrogate recoveries. Samples MW3021-1 and UST-ER2 had positive results that were not confirmed by a second column analysis. These positive results were flagged "JN" due to this problem. Benzene results failed to meet USAF maximum allowable detection limits; however, the detection limits did meed Florida petroleum contamination site clean- up criteria maximum allowable detection limits.

EDB (E504) analyses met QA/QC criteria for holding times, LCS, matrix spike/matrix spike duplicate, and surrogate recoveries.

Lead analyses met QA/QC criteria for holding times and matrix spike/matrix spike duplicates.

1,2-DCE (E601) analyses met QA/QC criteria for holding times, blanks, matrix spike/matrix spike duplicate, and surrogate recoveries.

AT510\923J189

ß-*0

ENGINEERING-SCIENCE

Memorandum to File Page 2 March 30, 1992

PAH (E610) analyses met criteria for blanks and surrogate recoveries. Samples MW3021-1, MW981-1, MW981-1, MW792-1, and UST-ER2 exceeded holding time criteria. All compounds in the associated samples were flagged to this problem.


J. A. Banton Chemist, ES Atlanta

AT510\923J189

8-41

ß-42-

pjggf SPI SOUTHWEST LABORATORY OF OKLAHOMA, INC.

1~00 West Alhanv • Broken Arrow. Oklahoma --t01J


ATLANTA, GA 30329

ATTN: OLA AWOSIKA

Office (918) 251-2858 Fax (918) 251-2858

REPORT: 8803.01 - .05HV

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO #: 8803.01 - .05 DATE SUBMITTED: 02-21-92 DATE ANALYZED: 02-24-92

PROJECT: AT 510

METHOD REFERENCE FOR 1,2-DICHLOROETHA«?ti EPA 601

CLIENT ID

SWLO

I.D

DESfi LIMIT

ND = NOT DETECTED ABOVE QUANTITATION LIMIT

EPA = #EPA600/4-79-020, MARCH 1985

SM = STANDARD METHOD, 16TH EDITION

UNIT RESULT

MW3021-1 8803.01 1.0;::, ug/L ND

UST-TB2 8803.02 : 1.0:' ug/L ND

MW981-1 8803.03 1.0 ug/L ND

MW792-1 :f 8803.04 | .:? 1.0 ug/L ND

UST-ER2,,:;Äi<*;:" % ;8803.0Sgl:: 1.0 ug/L ND

Co

&-4-Z

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1"00 West Albany Broken Arrow. Oklahoma ~4012 Office (918) 251-2858 Fax (918) 251-2858


ATLANTA, GA 30329

ATTN: OLA AWOSIKA

SWLO # 8803 METHOD REFERENCE:

PROJECT: AT 510

EPA 601

REPORT: 8803.01 - .05HVS

DATE: 03-20-92

SAMPLE I.D.

8803.01 8803.02 8803.03 8803.04

8803.05

HALOGENATED VOLATILE GAZOO SURROGATE RECOVERIES

mMPOUNn .; ;. " PERCENT RECOVERY

CIS-1, 2-DIcmQROETHEjfE CIS -1, 2 -DI CHÜ^PETjillE

CIS-1, 2rr?QlCHLOÜäl0&ME CIS-1,2-DICHLÖfcOETHENE CIS-1, 2-DICHLO^ETHSf(E

106% 100% 97%

105% 94%

& &

V

4\.

D = SURROGATE DILUTED OUT J = ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATION



Ch-4-4-

SOUTHWEST LABORATORY OF OKLAHOMA, INC. POO West Albany Broken Arrow. Oklahoma "+012 • Office (918) 251-2858 • Fax (918) 251-2858

REPORT: 8803.01 - .05EDB

DATE: 03-20-92


SAMPLE MATRIX: WATER SWLO #: 8803.01 - .05 METHOD REFERENCE: EPA 504.1 DATE SUBMITTED: 02-21-92 DATE EXTRACTED: 02-24-92 DATE ANALYZED: 02-25-92 PROJECT: AT 510

RESULTS REPORTED IN ug/B||G!;r PARpS PER BILLION

(TT.TENT IB

MW3024-1 UST-i'B2 MW981-1 MW792^1 UST-ER2- :■

**rn**£ DTBROMIDE

SWLO DET. T-TMIT

8803 01 0.01 8803 02 0.01 8803 03 0.01 8803 04 0.01 8803 05 0.01

RESULTS

ND ND ND ND ND


EPA = #EPA600/4-79-020, MARCH 1985 SM = STANDARD METHOD, 16TH EDITION

~*r

6-4-5T

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1"00 West Albanv Broken Arrow. Oklahoma "-+012 Office (918) 251-2858 Fax (918) 251-2858


ATLANTA, GA 30329

ATTN: OLA AWOSIKA

REPORT: 8803.01 - .05EDBSR

DATE: 03-20-92

SWLO # 8803 METHOD REFERENCE: EPA 504.1 PROJECT: AT 510

.n.

ETHYLENE DIBROMIDE QA/QC StS||ROGATE RECOVERIES

SAMPLET^ COMPOUND PERCENT Rl

8803.01 1,1,2,2 -TET*§i£HLOROEtHANE 109%

8803.02 1,1,2, 2-TETRÄ©8LORjq«THANE 109%

8803.03 1,1,2, 2 -MIRACHIÄioETHANE 110%

8803.04 1,1,2,2-TETRftCHLÖROETHANE 110%

8803.05 1,1,2,2-TETRACHLOROBHHANE 108%

D = SURROGATE DILUTED OUT J = ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATION



•^ cu

V

6r4£

-j w-

'±hrr m$m SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Albany- Broken Arrow. Oklahoma T4012 Office (918) 251-2858 Fax (918) 251-2858


ATLANTA, GA 30329

ATTN: OLA AWOSIKA

REPORT: 8803.01 - .05LD

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO #: 8803.01 - .05 DATE SUBMITTED: 02-21-92

DATE ANALYZED: 03-04-92

PROJECT: AT 510

METHOD REFERENCE FOR LEAD: EPA 239*2

SWLO '%:, DH3P. fTT.TKNT ID I. D f.miT UNIT RESULT

MW3021-1 ,„8803. Off >. 3,:©, ug/L ND

MW981-1 8803.03 , 3.Ö' ug/L 5.4

MW792-1 8803.04 3.0 ug/L 142

UST-ER2 8803.05 : 3.0 ug/L ND


EPA = #EPA600/4-79-020, MARCH 1985 SM = STANDARD METHOD, 16TH EDITION '^V

xV~x

yd' V

-<»v

ß-^7

SOUTHWEST LABORATORY OF OKLAHOMA, INC. POO West Albany • Broken Arrow. Oklahoma ^-+012 • Office (918) 251-2858 • Fax (918) 251-285H


REPORT: 8803.01 - .05TPH

DATE: 03-20-92


METHOD REFERENCE FOR TOTAL PETROLI^; JtDROCARBON: EPA 418.1

CLIEMT ID

MW3021-1 MW981-1 MW792-1 UST-ER2

SWLO I.P

■ 8803 Oil:: 8803 03 -Is.

8803 04 II 8803 05 m

PI*- £IMIT UNIT RKSl

0^5 mg/L ND 0.5 mg/L 0.6 0.5 mg/L ND 1.0 mg/L ND


s?

&-4S

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Albany Broken Arrow. Oklahoma 4012 Office (918) 251-2858 Fax (918) 251-2858


ATLANTA, GA 30329

ATTN: OLA AWOSIKA


SWLO #: 8803.01 METHOD REFERENCE: EPA 602

DATE SAMPLED : 02-20-92

DATE SUBMITTED: 02-21-92

DATE ANALYZED: 02-21-92


REPORT: 8803.01BX

DATE: 03-20-92

PARAMETER

PAS CHROMATOGRAPHY

PET. LIMIT


1.0 1.0 1.0 1.0 1.0

UNIT

ug/L

ug/L

ug/L

ug/L ug/L

QA/pC SURROGATE RECOVERIES


RESULTS

ND

0.5

ND

ND ND


B = ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE J = ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATION

* = SURROGATE RECOVERY OUTSIDE OF QC LIMITS ON ORIGINAL RUN AND RERUN. SW = TEST METHODS FOR EVALUATING SOLID WASTE, EPA PUBLICATION #SW846, THIRD


&-4^

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Albany Broken Arrow. Oklahoma "4012 Office (918) 251-2858 Fax (918) 251-2858


ATLANTA, GA 30329

ATTN: OLA AWOSIKA

REPORT: 8803.01P

DATE: 03-20-92


SWLO #: 8803.01 DATE SUBMITTED: 02-21-92 DATE EXTRACTED: 02-28-92 DATE ANALYZED : 03-06-92 METHOD REFERENCE: EPA 610


RESULTS REPORTED IN ug/||pR Par|| Per Billion (PPB)

POT-VNIICLEAR AROMATIC HYDROCARBOMS


ACENAPHTHENE


ANTHRACENE FLUORANTHENE :


CHRYSENE BENZO (B) FLUORANTHÄR2ii; ::

BENZO(K)FLUORANTHENE BENZO(A)PYRENE

DIBENZO(A,H)ANTHRACENE/ INDENO(l,2,3-CD)PYRENE **


hRTBCTTOM LIMIT

•■; l.o 1.0 1.0

1.0 1.0 1.0 1.0 1.0

RESULTS

NDT ND *■ ND T ND*" ND "" ND ? 2.0 : ND J NDT NDT

NDT NDT NDT NDT NDT NDC"

oa^or sTiwwnwATW RgrrnrawTKS

2-FLUOROBIPHENYL

p-TERPHENYL

82.6%

72%

ND = NONE DETECTED ABOVE QUANTITATION LIMIT J = ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATION


* = SURROGATE RECOVERY OUTSIDE OF QC LIMITS ** = THESE COMPOUNDS COELUTE (AS INDICATED IN METHOD 610).

8 -so

SOUTHWEST LABORATORY OF OKLAHOMA, INC. rOO West Albany • Broken Arrow. Oklahoma 74012 • Office (918) 251-2858 • Fax (918) 251-2858



REPORT: 8803.01PC

DATE: 03-20-92

Cv.t- /C, - ? ,-■/• -- _

■ /■?-<

RESULTS REPORTED IN ug/;||pR Pai^P5 Per Billion (PPB)

P^T.vMTTrT.BAW aHOMATTr ffVTffiOrikMCMS

NAPHTHALENE ACENAPHTHYLENE ACENAPHTHENE FLUORENE PHENANTHRENE ::;|V ANTHRACENE FLUORANTHENE :-:

PYRENE BENZO(A)ANTHRACENE CHRYSENE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO(A)PYRENE DIBENZO(A,H)ANTHRACENE/


nWTECTION LIMIT

2.8 3.6 4.3 0.3 0.9 1.1 0.3 0.5 0.02 0.2 0.03 0.03 0.03 0.05 0.08 0.12

BESDLXS

NDX NDX NDT ND't" NDT' NDT ND7 NDT ND?

NDJ NDT NO? NDf NDJ*

NDT NDT

pA^OC SIIPPOflATB RBrOVBBIBS


48% 36%

'■Ak


6-51

SOUTHWEST LABORATORY OF OKLAHOMA, INC. l-00 West Albany • Broken Arrow. Oklahoma "4012 • Office (918) 251-2858 • Fax (918) 251-2858


REPORT: 8803.02BX

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO #: 8803.02 METHOD REFERENCE: EPA 602 DATE SAMPLED : 02-20-92 DATE SUBMITTED: 02-21-92 DATE ANALYZED: 02-21-92 PROJECT: AT 510 SAMPLE ID: UST-TB2

PARAMETER

HAS CHROMATOflRAPHY


0BT.

1.0

i:.:o 1.0 1.0

"MIT RESULTS


ND ND ND ND ND

OA/pC SURROGATE RECOVERIES




ß-Sz-

-lit: [44-

s^ 'ffili M r\

SQUTHWEST LABORATORY OF OKLAHOMA, INC. rOO West Albany • Broken Arrow. Oklahoma ~4012 • Office (918) 251-2858 • Fax (918) 251-2858



REPORT: 8803.03BX

DATE: 03-20-92

PARAMETER

CAS CHROMATOGRAPHY


T.TMTfe

1.0

1.0 1.0 1.0

JffllX. RESHI/TS


ND ND ND ND ND

Ql/QC. STIRROftftT« HBPOVERIES




6-5S

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Albanv • Broken Arrow. Oklahoma ~4012 • Office (918) 251-2858 Fax (918) 251-2858


ATLANTA, GA 30329

ATTN: OLA AWOSIKA


SWLO #: 8803.03 DATE SUBMITTED: 02-21-92

DATE EXTRACTED: 02-28-92

DATE ANALYZED : 03-06-92 METHOD REFERENCE: EPA 610

PROJECT: AT 510

SAMPLE ID: MW981-1

REPORT: 8803.03P

DATE: 03-20-92

RESULTS REPORTED IN ug/i|OR Parjfs Per Billion (PPB)

pnT.vwTTrrr.wAtt AROMATTC HYDROC

NAPHTHALENE ACENAPHTHYLENE ACENAPHTHENE


ANTHRACENE FLUORANTHENE


CHRYSENE BENZO(B)FLUORANTHENE

BEN ZO(K)FLUORANTHENE

BENZO(A)PYRENE DIBENZO(A,H)ANTHRACENE/

INDENO(1,2,3-CD)PYRENE **


nBTECTIOM LIMIT RESULTS

*■ 1.0 NDVT

1.0 NDT 1.0 ND-^ 1.0 NDj 1.0 NDj 1.0 ND7"

1.0 NDT 1.0 1.0 1.0

ND" ND.T ND7"

1.0 ND*^

1.0 NDT 1.0 NDT 1.0 1.0

NDT NDT

1.0 NDT

f^ftf- SIIRBftftATB BFCnVmtTBS


106.7%

105.1%




«-£<*-

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Albany Broken Arrow. Oklahoma 4012 Office (918) 251-2858 • Fax (918) 251-2858



REPORT: 8803.04BX

DATE: 03-20-92

ÜBT. PARAMETER ■-TTHttS!

r.ÄS CHROMATOGRAPH*

BENZENE 1.0 TOLUENE i.Mf ETHYLBENZENE .

:':::--i::;lD XYLENES 1.0

MTBE 1.0

UNIT


BBSUI/TS

ND ND ND ND ND

pa/ftr stiRRPfrftTF HW«WEBIES


-Si



6-SS

SOUTHWEST LABORATORY OF OKLAHOMA, INC. "00 West Albany • Broken Arrow. Oklahoma '4012 • Office (918) 251-2858 • Fax (918) 251-2858



RESULTS REPORTED IN ug/i|:CR Paul's Per Billion (PPB)

REPORT: 8803.04P

DATE: 03-20-92

PnTiYNTTrT **» AROMATTr HYPFOPMBCrMS

NAPHTHALENE ACENAPHTHYLENE ACENAPHTHENE FLUORENE PHENANTHRENE ANTHRACENE FLUORANTHENE PYRENE BENZO(A)ANTHRACENE CHRYSENE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO(A)PYRENE DIBENZO(A,H)ANTHRACENE/

INDENO(l,2,3-CD)PYRENE * BENZO(G,H,I)PERYLENE

nBTBCTIOM LIMIT

,0 .0 ,0 ,0 ,0 .0 .0

1.0 1.0

.0 ,0 .0 .0 .0

1.0 1.0

RBSUI/TS

NDT ND T NDX UDT NDT* NDT ND7 ND"*' NDJ NDT NDT NDT NDT NDT ND.r ND ■

rta^r. sirawrmATB RgrrwunTES


103.0% 105.7%


l-5€

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Albany Broken Arrow. Oklahoma "'4012 Office (918) 251-2858 Fax (918) 251-2858


SAMPLE MATRIX: WATER SWLO #: 8803.05 METHOD REFERENCE: EPA 602 DATE SAMPLED : 02-20-92 DATE SUBMITTED: 02-21-92 DATE ANALYZED: 02-21-92 PROJECT: AT 510 SAMPLE ID: UST-ER2

REPORT: 8803.05BX

DATE: 03-20-92

PARAMETER

r,AS r.HROMATOGRAPHY


DET. ;

T.*ttlT

1.0

1 • Qx;

1.0 1.0

JffllT-


BESHI/rS

ND ND ND 0.7 Jft ND

'-M

QA/pC? SURRQftATP! RECOVERIES




ft-37

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Albany Broken Arrow. Oklahoma ^4012 Office (918) 251-2858 Fax (918) 251-2858


ATLANTA, GA 30329

ATTN: OLA AWOSIKA

REPORT: 8803.05P

DATE: 03-20-92


SWLO #: 8803.05 DATE SUBMITTED: 02-21-92 DATE EXTRACTED: 02-28-92 DATE ANALYZED : 03-06-92 METHOD REFERENCE: EPA 610

PROJECT: AT 510

SAMPLE ID: UST-ER2

RESULTS REPORTED IN ug^lypR Patfte Per Billion (PPB)

pnT.YMTTrrr.RAW AROMATTC HVnROCAHaQHfi

NAPHTHALENE

ACENAPHTHYLENE

ACENAPHTHENE


ANTHRACENE FLUORANTHENE


CHRYSENE BENZO(B)FLUORANTHENE BEN ZO(K)FLUORANTHENE BENZO(A)PYRENE DIBENZO(A,H)ANTHRACENE/

INDENO(l,2,3-CD)PYRENE **


nFTHCTTON LIMIT

*"■"■ 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0

RESULTS

NDT NDJ NDT ND'T NDT"

ND:

ND7 ND? NDT NDT ND^

NDT

ND"' ND ' ND~ ND~

rvi

pa/or. snawnnaTg wwcnvwHiBS


105.7%

106.6%




A-S^'

TtttTt • ■ ijii^ii-

WuJJi /Wff^S

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1"00 West Albany • Broken Arrow. Oklahoma "4012 • Office (918) 251-2858 • Fax (91«) 251-2858

ANALYTICAL REPORT

ENGINEERING-SCIENCE INC. 57 EXECUTIVE PARK SOUTH ATLANTA, GA 30329

SWLO IDENTIFICATION

SAMPLE NO.: 8803.01-8803.05 DATE RECEIVED: 02/21/92

OA/OC

REPORT: 8803


DESCRIPTION

METHOD BLANK 03/04/92

BLANK SPIKE 03/04/92;

J&RAMEfER

LEAD

RESULTS

< 3.0 ug/L

96% RECOVERY

ß-S?

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Albany • Broken Arrow. Oklahoma "-+012 • Office (918) 251-2858 • Fax (918) 25i-2858


REPORT: 8803a

DATE: 03-19-92

SAMPLE MATRIX: WATER SWLO #: METHOD BLANK DATE ANALYZED : 02-24-92 METHOD REFERENCE: EPA 601 PROJECT: AT 510 SAMPLE ID: BLANK

RESULTS REPORTED IN ug/L OR Par*s Per Billion (PPB)

HALOGENATED ■vDETVÄ YQLAXILES jJMIX INSULTS

1, 2-DICHLOROET%NE ; It. 0 ND

OA/OC SURROGATE RBCOYERIBS

CM en



&-&?

mm SOUTHWEST LABORATORY OF OKLAHOMA, INC. POO West Albany • Broken Arrow. Oklahoma "4(312 • Office (918) 251-2858 • Fax (918) 251-2858


ATLANTA, GA 30329

ATTN: OLA AWOSIKA

REPORT: 8803b

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO # 8803 (MS/MSD) DATE ANALYZED : 02-24-92 METHOD REFERENCE: EPA 601

PROJECT: AT 510 SAMPLE ID: CONFIDENTIAL ID

^T^FwaTED v«r.»TTT.^^MTiTT"%ffiB/inTRTI SPIKE mTPLTCRTfi RECOVERY

rnMPOUND

1,2-DICHLOROETHANB|

SPIKE SAMPLE COmc. CONC. MS CONC.

MS AMT FOUND PERCENT PERCENT MSD CONC. RECOVERY PERCENT wwrnvwHY fim/i^ MSB BED

20.0 ""-™-:wv-0 17.2 86.0 18.4 92.0 6.7

<-, V

#

<br&\

1 j ii jin i I j |

Wft s m ' vvv /■

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Albany • Broken Arrow. Oklahoma 7-+012 • Office (918) 251-2858 • Fax (918) 251-2858



PARAMETER DE*»*

CAS P.HROMATOGRAPHY


1.0 1.0 1.0 j :1*#S:

10.0

REPORT: 8803c

DATE: 03-20-92

_UHIT_


QA/pC SURROGATE RECOVERIES


RESULTS

ND ND ND ND ND

* ^

. V -



6-6^

SOUTHWEST LABORATORY OF OKLAHOMA, INC. POO West Albany • Broken Arrow. Oklahoma 7-tOi; Office (918) 251-2858 • Fax (918) 251-2858


REPORT: 8803d

DATE: 03-20-92

SAMPLE MATRIX: WATER DATE ANALYZED: 02-21-92 SWLO #: 8803 (MS/MSD) PROJECT: AT 510 SAMPLE ID: CONFIDENTIAL ID

WTWT MATBTT SPTlfpffi**TWTlj SPTKW DÜÜfelCATB

MATRIX SPIKE

SPIKE CONC. SAMPL» CONC. CONC. PERCENT

(ug/L) (ug/i)

0 If

(ug/L)

9.9

RECOVERY

BENZENE 10.0 99.3%

TOLUENE ,10^<PV Mß 9.3 93.1%

ETHYLBENZENE irio.o 0 9.4 94.4%

TOTAL XYLENES : 30.0 0 29.4 98.1%

MTBE 40.0 0 44.6 111.5%

MMÄIX SPIKE DUP PERCENT REC. RECOVERY PERCENT

NSD CONC. (ug/L) (ug/L) DIFFERENCE

BENZENE 10.1 100.9% 1.60%

TOLUENE 9.5 95.4% 2.44%


TOTAL XYLENES 30.4 101.3% 3.21%

MTBE 42.4 106.0% 5.1%

% i?

<3-fc'3

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Albany Broken Arrow. Oklahoma ~-*012


Office (918) 251-2858 • Fax (918) 251-2858

REPORT: 8803e

DATE: 03-20-92


RESULTS REPORTED IN ng/Sfbr PARI? PER BlftiON

DET% PARAMETER I^XHJlfC BESHLX

ETHYLE|ffiIB*BRÖ%PE 0^1 ND

Oft/ftP SURROGATE RECOVERY

1,1,2,2-TETRACHLOROETHANE 103%


1- v

(K-&4-

SOUTHWEST LABORATORY OF OKLAHOMA, INC. rOO West Albany Broken Arrow. Oklahoma /4012 Office (918) 251-2858 Fax (918) 251-2858


ATLANTA, GA 30329

ATTN: OLA AWOSIXA

REPORT: 8803f

DATE: 03-20-92


SWLO #: METHOD BLANK DATE EXTRACTED: 02-28-92



PROJECT: AT 510 SAMPLE ID: METHOD WATER BLANK 022892«|l

RESULTS REPORTED IN ug/^pR Partf* Per Billion (PPB)

pnT.VMTTrrr.RAW AROMATIC HYDROCARBONS


ACENAPHTHENE

FLUORENE

PHENANTHRENE

ANTHRACENE

FLUORANTHENE .|


CHRYSENE

BENZO(B)FLUORANTS8NB BENZO (K) FLUORANTHENE'' BENZO(A)PYRENE DIBENZO(A,H)ANTHRACENE/



gfeTECTIOM LIMIT

9 7

5

3

0

1

3

5

02

2 03 03 03 05 08 13

RBSÜLTS

ND ND

ND

ND

ND

ND

ND

ND ND

ND

ND ND ND

ND ND ND

QA/OC SOTBOQATB WBCOVBRIBS


50% 43%


^6 5"

SOUTHWEST LABORATORY OF OKLAHOMA, INC. ■00 West Albany Broken Arrow. Oklahoma 7^012 Office (918) 251-2858 Fax (918) 251-2858


REPORT: 8803g

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO #: METHOD BLANK DATE EXTRACTED: 02-28-92 DATE ANALYZED : 03-06-92 METHOD REFERENCE: EPA 610 PROJECT: AT 510 SAMPLE ID: WBLK022892-01

RESULTS REPORTED IN ug/yjOR Par|s Per Billion (PPB)

PftT.vwTTrr.KAB AROMATTC HYDROCARBOHS'

NAPHTHALENE ACENAPHTHYLENE ACENAPHTHENE FLUORENE PHENANTHRENE ANTHRACENE FLUORANTHENE PYRENE BEN Z O(A)ANTHRACENE CHRYSENE BENZO(B)FLUORARfHENE BENZO(K)FLUORANTHEW2K v

BENZO(A)PYRENE DIBENZO(A,H)ANTHRACENE/ INDENOU, 2, 3-CD) PYRENE **


pyrRPTTOM LIMIT

0 ,0 ,0 ,0 ,0 .0 ,0 .0 .0 .0 .0 .0 .0 .0 .0

1.0

BESDLXS

ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

~\f

^f^r sTTHPonaTW nnrmnraTEB


90.7% 78.6%


(l-LQ

-L. i'Hürttll

H TVTW^S 7 / / / ! lftv /

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1700 West Albany Broken Arrow. Oklahoma "MO 12 Office (918) 251-2858 Fax (918) 251-285S


REPORT: 8803h

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO #: 8803 (MS/MSD) DATE EXTRACTED: 02-28-92 DATE ANALYZED : 03-06-92 PROJECT: AT 510 SAMPLE ID: CONFIDENTIAL ID

WATWR PAH MATBTX SPTra/fffpRTT <t»T1Cg PHTOJeATB RECOVERY

COMPOUND

SPIKE ADDED

(Ug/D

AMI FOUND AMI V&ti&b MS AMT FOUND PERCENT SAMPLE MS PERCENT MSD RECOVERY PERCENT /Ug/H '"ißt itECOVERY fiiq/11 MSB BED.

NAPTHALENE 10 ACENAPTHYLENE 10 ACENAPTHENE 10 FLUORENE 1$ PHENANTHRENE 10 ANTHRACENE 10 FLUORANTHENE lOi PYRENE 10 BENZO-(A)-ANTHRANCENE 10 CHRYSENE 10 BENZO-(B)-FLUORANTHENE 10 BENZO-(K)-FLUORANTHENE 10 BENZO-(A)-PYRENE 10 DIBENZO(A,H)ANTHRACENE/ 20

INDENO(l,2,3-CD)PYRENE * BENZO(G,H,I)PERYLENE 10

.0

.0

«# lo .0 .0 »0

•4*1 . 0 .0 .0 .0 .0 .0 *

.0

7 •:§'

T.9 8. 8. 8. 8. 8. 7. 7. 8. 8. 8. 8.

76.2> 10.6 79.0; 10.8 78.8 10.8 85.9 11.9 86.4 12.1 87.4 11.9 84.1 11.5 84.2 11.7 75.2N 70.1 ;

9.9 9.3

81.1 10.8 84.2 11.3 84.2 11.1 41." 3' 11.7

106.2 33.0 108.0 30.9 107.9 31.1 119.4 32.6 121.2 33.6 118.5 30.3 115.4 31.4 117.4 32.9 99.1 27.5 93.4 28.5

107.7 28.2 113.2 29.4 110.6 27.1 rss.T 34.5

8.4 83.9 12.0 119.5 35.1

OA/Or SPBBOOATB WECOVERIBS


MS 76.7% 91.7%

MSD 106.7% 110.0%


ß-Ly

SOUTHWEST LABORATORY OF OKLAHOMA, INC. POO West Albanv • Broken Arrow. Oklahoma "4012 • Office (918) 251-2858 • Fax (918) 251-2858

CLIENT: ENGINEERING SCIENCE, INC.. 57 EXECUTIVE PARK SOUTH, SUITE 590 ATLANTA, GA 30329 ATTN: OLA AWOSIKA

REPORT: 8803i

DATE: 03-20-92


RESULTS REPORTED IN mg/L%B ^^08 Per Billion (PPB)

PABAMETBR

TPH

DET.. JUIMil Rggtn/rs

m. 5 ND


,V e

s-^y

SOUTHWEST LABORATORY OF OKLAHOMA, INC. rOO West Albany • Broken Arrow. Oklahoma 74012 • Office (918) 251-2858 • Fax (918) 251-2858



REPORT: 8803k

DATE: 03-20-92

TT>W MATRTT SPTKK/ÜÄTBT* SPIKE DPELICATE

TPH

MATRIX SPIKE SPIKE CONC. SAMPLE C08C. CONC. PERCENT

(ug/L)

20.0

(ug/&) (ug/L) RECOVERY

15.6 78.0%

MSD CONC. (mg/L)*



TPH :fSfÖ::;: 80% 2.5%

■£>■ \

r

v

•> v

e>-^

ENGINEERING-SCIENCE

MEMORANDUM

March 30, 1992

To: File

From: J. A. Banton


TPH (E418.1) analyses met QA/QC criteria for holding times, blanks, and matrix spike/matrix spike duplicate.

BETX and MTBE (E602) analyses met QA/QC criteria for holding times, blanks, matrix spike/matrix spike duplicate, and surrogate recoveries. Benzene results failed to meet USAF maximum allowable detection limits; however, the detection limits did meet Florida petroleum contamination site clean-up criteria maximum allowable detection limits.

EDB (E504) analyses met QA/QC criteria for holding times, LCS, matrix spike/matrix spike duplicate, and surrogate recoveries.

Lead analyses met QA/QC criteria for holding times and matrix spike/matrix spike duplicates.

1,2-DCE (E601) analyses met QA/QC criteria for holding times, blanks, matrix spike/spike matrix duplicate, and surrogate recoveries.

PAH (E610) analyses met criteria for holding times, blanks, and surrogate recoveries.


^J. A. Banton Chemist, ES Atlanta

AT510\923J189

6-7?

Tl ! I I «4 | J.l I

»--*--:>>/fill

L *l T TTTTL ^ ■ ri

[ ; ; 1

y'/Vy / /-r-4?j^-YH{JjWYV

/ / /' 77; c ^/^U_ik5^^5^ fc7pLU-^£X>S -Mr Mil M>05


March 20, 1992

Ola Awosika ENGINEERING SCIENCE, INC. 57 Executive Park South, Sui&e |90 Atlanta, GA 30329

Project: AT 510 SWLO Episode #: 88imfmmK8&M.02

Dear Mr. Awosika: ;|

Enclosed we a*» slbniitting7the analytical results for your samples revived in otir laboratory on February 22, 1992 for the above*»captioned project.

If, in your review, you should have any questions or require additional information, please call.

Sincerely,


DA/rb

Enclosures V*


6-7/

IT! Ulli,

•~r~r^ 'tfflwm SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1"00 West Alhanv • Broken Arrow. Oklahoma 74012 • Office (918) 251-2858 • Fax (918) 251-2858


REPORT: 8819.01 - .02HV

DATE: 03-19-92


METHOD REFERENCE FOR 1, 2-DIGHLOROETHSiiS;

SW143 , M DET. r*r TTOTI m T . n i LIMIT

EPA 601

UMTT RESULT

MW9990-1 8819-..01 UST-TB3 TRIP BLANK. 8819.02

:.:: 1.0 1.0

ug/L ND ug/L ND

'J


ß-73

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 Wesr Alhanv • Broken Arrow. Oklahoma "4012 • Office (918) 251-2858 • Fax (918) 251-2858


REPORT: 8819.01 - .02HVS

DATE: 03-20-92

SWLO # 8819 METHOD REFERENCE: EPA 601 PROJECT: AT 510

SAMPT.E T.D.

8819.01 8819.02

HALOGENATED VOLATILE ^JA/IOC SURROGATE RECOVERIES

COMPOUND ..:■:if::'!;:---';:, "^'^ PERCENT RECOVERY

CIS -1, 2 -DI CH^ROETHÄWE CIS -1, 2 -DI CHL:i|g?E.:giiNE

96% 94%

D = SURROGATE DILUTED OUT J = ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATION B = ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE * = SURROGATE RECOVERY OUTSIDE OF QC LIMITS 2/

■■?*

v . 'A

S-"7 4-

SOUTHWEST LABORATORY OF OKLAHOMA, INC. !~00 Wesr Albany Broken Arrow. Oklahoma "-+01J


Office (918) 251-2858 « Fax (918) 251-2858

REPORT: 8819.01 - .02EDB

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO #: 8819.01 - .02 METHOD REFERENCE: EPA 504.1 DATE SUBMITTED: 02-22-92 DATE EXTRACTED: 02-24-92 DATE ANALYZED: 02-25-92 PROJECT: AT 510

RESULTS REPORTED IN ug/fl|gf PAjgfs PER BILLION

ft*BVT,eWE DIBROMIDE

tTT.TEMT IB

MW9990-1 MW91S01-1

SWLO

|it,,,I.P

8819.01 8819.02

DET. LIMIT

0.01 0.01

RBSTILTS

ND ND

>y

ND = NOT DETECTED ABOVE QUANTITATION LIMIT EPA = #EPA600/4-79-020, MARCH 1985 SM = STANDARD METHOD, 16TH EDITION £'

>■$•

8.-75"

SOUTHWEST LABORATORY OF OKLAHOMA, INC. l-00 West Albanv • Broken Arrow. Oklahoma ^012 • Office (918) 251-2858 • Fax (918) 251-2858


SWLO # 8819 METHOD REFERENCE: EPA 504.1 PROJECT: AT 510

REPORT: 8819.01 - .02EDBSR

DATE: 03-20-92

SAMPT.K T.D.

8819.01 8819.02

ETHYLENE DIBROMIDE QA/QC StftROGATE RECOVERIES

COMPOUND ,-:"'-r :: :; 'h. PERCENT RECOVERY

1,1,2, 2-TEll|i|>CHLORCfj|THANE 1,1,2, 2-TETR»eääLOfl0lTHANE

109% 112%

D = SURROGATE DILUTED OUT J = ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATION B = ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE * = SURROGATE RECOVERY OUTSIDE OF QC LIMITS

V

'3-74

SOUTHWEST LABORATORY OF OKLAHOMA, INC. POO Wesr Albany Broken Arrow, Oklahoma "4012 • Office (918) 251-2858 • Fax (918) 251-2858


REPORT: 8819.01TPH

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO #: 8819.01 DATE SUBMITTED: 02-22-92 DATE ANALYZED: 03-04-92 PROJECT: AT 510

METHOD REFERENCE FOR TOTAL PETROLEUM.1:if|pROCARBON: EPA 418.1

CLIENT ID

MW9990-1

SWLO J2ÜUI UNIT RESULT

8819.01 im mg/L 1.6


„>.

♦V'

6-77

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Albanv Broken Arrow. Oklahoma "401 i Office (918) 251-2858 Fax (918) 251-2858


ATLANTA, GA 30329

ATTN: OLA AWOSIKA

REPORT: 8819.01LD

DATE: 03-20-92


SWLO #: 8819.01 DATE SUBMITTED: 02-22-92 DATE ANALYZED: 03-04-92

PROJECT: AT 510

METHOD REFERENCE FOR LEAD: SPA 239.2;

rrr.TEMT ID

MW9990-1

SWLO

I.D

DE& #;■; jü«T _UHIX_

8819.01 3.$ ug/L

-BESHLl

ND


EPA = #EPA600/4-79-020, MARCH 1985

SM = STANDARD METHOD, 16TH EDITION

ß-7?

-1 '^ljr«3-

?77mdg£gg ///it 1 y^ty^ M 1 f 1 TiVv >

SOUTHWEST LABORATORY OF OKLAHOMA, INC. !"00 West Albany Broken Arrow. Oklahoma ~4012 • Office (918) 251-2858 • Fax (918) 251-2858



REPORT: 8819.01BX

DATE: 03-20-92

PARAMETER

gas CHROMATOGRAPHY

BENZENE TOLUENE ETHYLBENZENE 0 XYLENES MTBE

JJÄÖL

1.0

:f.o 1.0 1.0

UNIT


ftft/pr SITRROOATB RECOVERIES


RBSUI/TS

ND ND ND ND ND

■£"

ND B J *

SW



Pr?!

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Albany • Broken Arrow. Oklahoma "-+012 • Office (918) 251-2858 • Fax (918) 251-2858


REPORT: 8819.01P

DATE: 03-20-92


RESULTS REPORTED IN ug/l|gR Parfl Per Billion (PPB)

pnT.YWTTftT.BAR AROMATIC HYDRO

NAPHTHALENE ACENAPHTHYLENE ACENAPHTHENE FLUORENE PHENANTHRENE ANTHRACENE FLUORANTHENE PYRENE BENZO(A)ANTHRACENE CHRYSENE BENZO ( B) FLUORANTHENE^ BENZO(K)FLUORANTHENE BENZO(A)PYRENE DIBENZO(A,H)ANTHRACENE/


nETECTIOM LIMIT RESULTS

'%■ 1.0 ND 1.0 ND 1.0 ND 1.0 ND 1.0 ND 1.0 ND 1.0 ND 1.0 ND 1.0 ND 1.0 ND 1.0 ND 1.0 ND 1.0 ND 1.0 ND 1.0 ND 1.0 ND

OA/OC STIRWOQATW RBrOCTRIBS


102.0% 140.6%


&-fo.

H±£ -note

Sr? ttm^tm

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1"00 West Albany Broken Arrow. Oklahoma 74012 • Office (918) 251-2858 Fax (918) 251-2858


ATLANTA, GA 30329

ATTN: OLA AWOSIKA


SWLO #: 8819.02 METHOD REFERENCE: EPA 602

DATE SAMPLED : 02-21-92 DATE SUBMITTED: 02-22-92 DATE ANALYZED: 02-25-92

PROJECT: AT 510 SAMPLE ID: UST-TB3 TRIP BL|0»:.;>::,

REPORT: 8819.02BX

DATE: 03-20-92

PARAMETER

CAS rHBOMATOGRAPHY

BENZENE

TOLUENE ETHYLBENZENE

XYLENES MTBE

LIMIX

1.0

;:f.o 1.0 1.0

JffllT-


RESULTS

ND ND ND ND ND

ft*7pr. stTHROffftTTf BttrawERiES


ND =

B =

J = * =

SW =



8-tl

SOUTHWEST LABORATORY OF OKLAHOMA, INC. POO West Albany • Broken Arrow. Oklahoma ~-t012 • Office (918) 251-2858 • Fax (918) 251-2858

ANALYTICAL REPORT

ENGINEERING-SCIENCE INC. 57 EXECUTIVE PARK SOUTH ATLANTA, GA 30329

8WLO IDENTIFICATION

REPORT: 8819


SAMPLE NO.: 8 819.01-8 819.02 DATE RECEIVED: 02/22/92

OA/OC

DESCRIPTION .flÄRAMElER RESULTS

METHOD BLANK 03/04/92 LEAD < 3.0 ug/L

BLANK SPIKE 03/04/92 I^AD 9 6% RECOVERY

s-?z-

ITTTTTT J—- '*M' ■

^■'V ■' •

Köfl^^ SOUTHWEST LABORATORY OF OKLAHOMA, INC. POO West Albanv • Broken Arrow. Oklahoma 74012 • Office (918) 251-2858 • Fax (918) 251-2858

:LIENT: ENGINEERING SCIENCE, INC.

57 EXECUTIVE PARK SOUTH, SUITE 590

ATLANTA, GA 30329

ATTN: OLA AWOSIKA

REPORT: 8819a

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO #: METHOD BLANK DATE ANALYZED : 02-26-92 METHOD REFERENCE: EPA 601 PROJECT: AT 510 SAMPLE ID: BLANK

RESULTS REPORTED IN ug/L.QR Pa#S Per Billion (PPB)

HALOGENAIED VOTATTLES

1,2-DICHLOROETHSfcNE

:>:.DElr";*;:-:::,

%IHIX BSSHLXS

li. o ND

OA^pC STIBBOOATg RgCOVgRIBS


•'S*


8-53

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1~00 West Albany • Broken Arrow. Oklahoma ~4012 • Office (918) 251-2858 • Fax (918) 251-2858

CLIENT: ENGINEERING SCIENCE, INC.

57 EXECUTIVE PARK SOUTH, SUITE 590 ATLANTA, GA 30329 ATTN: OLA AWOSIKA

REPORT: 8819b

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO # 8819 (MS/MSD) DATE ANALYZED : 02-26-92 METHOD REFERENCE: EPA 601 PROJECT: AT 510

SAMPLE ID: CONFIDENTIAL ID

HALOGENATED VOLATILE^ MJHMTX WJKB/MATRIX SPTKB ntlPLICATF WECOVBRY

COMPOUND

SP|KE SAMPLE f MS AMT POUND PERCENT

Coi|c. CONC. MS CONC. PERCENT MSD CONC. RECOVERY PERCENT

,..::,::W^»#|ij—Üis/Wi Üia/ia RECOVERY (ug/L) MSD BPD

1,2-DICHLOROETHANKr' 20.0 20.1 100.5 20.5 102.5 2.0

£'

6-14-

SOUTHWEST LABORATORY OF OKLAHOMA, INC. POO West Albanv • Broken Arrow. Oklahoma ""4012 • Office (918) 251-2858 • Fax (918) 251-2858

CLIENT: ENGINEERING SCIENCE, INC. 57 EXECUTIVE PARK SOUTH, 3UITE 590 ATLANTA, GA 30329 ATTN: OLA AWOSIKA


REPORT: 8819c

DATE: 03-20-92

PARAMETER

r.AS THBOMATOGRAPHY


DBA»-

1.0 1.0 1.0 :: 1.0 10.0

"WIT


QA/OC SPRBOQATE RECOVERIES


RESULTS

ND ND ND ND ND

'V



s-sr

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1"00 West Albanv • Broken Arrow. Oklahoma "4012 • Office (918) 251-2858 • Fax (918) 251-2858


REPORT: 8819d

DATE: 03-20-92


mc-a. ru»J.nj.A ,-ii-iiMfi

.

MATRIX SPIKE SPIKE CONC* SAMPLE cone. CONC. PERCENT

(ug/L) (U9ÜI>) ': (ug/L) RECOVERY

BENZENE 10.0 o i 9.8 98.4%

TOLUENE 10.0 0 9.0 89.5%

ETHYLBENZENE :#10.0 0 9.3 93.3%

TOTAL XYLENES : f 30.0 0 29.1 97.0%

MTBE 40.0 0 36.0 90.0%

ÜÜK&^PXXE DUP PERCENT REC. RECOVERY PERCENT

NSD COMC. (ug/L) (ug/L) DIFFERENCE

7.72% BENZENE 10.6 106.3%

TOLUENE 9.1 90.8% 1.43%


TOTAL XYLENES 29.4 97.9% 0.92%

MTBE 43.1 107.8% 18.0%

s* ^

6-S6

SOUTHWEST LABORATORY OF OKLAHOMA, INC. l'OO West Albany • Broken Arrow. Oklahoma "4012 • Office (918) 251-2858 • Fax (918) 251-2858


REPORT: 8819e

DATE: 03-20-92


RESULTS REPORTED IN ug/;g|for PAR|| PER BILCTON

PARAMETER DETii!: LIMlt BESI1LX

ETHYLBÄBÄBRoilOE .0#1 ND

pa/pc SURROGATE RECOVERY

1,1,2,2-TETRACHLOROETHANE 103%


„ 7 -v

S-^7

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1-00 West Albany • Broken Arrow. Oklahoma ~4012 • Office (918) 251-2858 • Fax (91«) 251-2858


REPORT: 8819f

DATE: 03-20-92

SAMPLE MATRIX: WATER SWLO #: METHOD BLANK DATE EXTRACTED: 02-28-92 DATE ANALYZED : 03-06-92 METHOD REFERENCE: EPA 610 PROJECT: AT 510 SAMPLE ID: WBLK022892-01

RESULTS REPORTED IN uq/lJSjik Part* Per Billon (PPB)

pflT.VWTTCT.RAR AROMATIC HYDROCARBONS v BED 5CTTOM LIMIT

1.0

RESULTS

NAPHTHALENE ND

ACENAPHTHYLENE 1.0 ND

ACENAPHTHENE 1.0 ND

FLUORENE 1.0 ND

PHENANTHRENE 1.0 ND

ANTHRACENE 1.0 ND

FLUORANTHENE £? 1.0 ND

PYRENE 1.0 ND

BENZO(A)ANTHRACENE 1.0 ND

CHRYSENE 1.0 ND

BENZO (B) FLUORANffiSNE. 1.0 ND

BENZO(K)FLUORANTHENl- 1.0 ND

BENZO(A)PYRENE 1.0 ND

DIBENZO(A,H)ANTHRACENE/ 1.0 ND

INDENO(l,2,3-CD)PYRENE ** 1.0 ND

BENZO(G,H,I)PERYLENE 1.0 ND

9A/flC SURROGATE RFCOVBRIKS

2-FLUOROBIPHENYL 90.7% D-TERPHENYL 78.6%


•>-?

,3-5V

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1_00 West Albany • Broken Arrow. Oklahoma 74012 • Office (918) 251-2858 • Fax (918) 251-2858

CLIENT: ENGINEERING SCIENCE, INC.

57 EXECUTIVE PARK SOUTH, SUITE 590

ATLANTA, GA 30329

ATTN: OLA AWOSIKA

SAMPLE MATRIX: WATER SWLO #: 8819 (MS/MSD) DATE EXTRACTED: 02-28-92


PROJECT: AT 510 SAMPLE ID: CONFIDENTIAL ID

REPORT: 8819g

DATE: 03-20-92

Til

SPIKE AMT FOUMD AMT FOltiiD MS AMT FOUND PERCENT

ADDED SAMPLS M» PERCENT MSD RECOVERY 1 PERCEN1

COMPOUND (ua/l\ fu^/lS (ug/U

7.1

*RC!OVERY (ug/1) MSD HPD

NAPTHALENE 10.0 llo 76.2 10.6 106.2 33.0

ACENAPTHYLENE 10.0 ... m TS 79.0 10.8 108.0 30.9

ACENAPTHENE 10,£P ' fca,,,.. WK 9 78.8 10.8 107.9 31.1

FLUORENE lifb 0 8.6 85.9 11.9 119.4 32.6

PHENANTHRENE 10.0 Ck-S 8.6 86.4 12.1 121.2 33.6

ANTHRACENE mo 0s, 8.7 87.4 11.9 118.5 30.3

FLUORANTHENE mo W 8.4 84.1 11.5 115.4 31.4

PYRENE m&-.:„. .,,,a#0 8.4 84.2 11.7 117.4 32.9

BENZO-(A)-ANTHRANCENE 10.0 ""■"■ mm"-' 0 7.5 75.2 9.9 99.1 27.5

CHRYSENE 10.0 0 7.0 70.1; 9.3 93.4 28.5

BENZO-(B)-FLUORANTHENE 10.0 0 8.1 81.1 10.8 107.7 28.2

BENZO-(K)-FLUORANTHENE 10.0 0 8.4 84.2 11.3 113.2 29.4

BENZO-(A)-PYRENE 10.0 0 8.4 84.2 11.1 110.6 27.1

DIBENZO(A,H)ANTHRACENE/ 20.0 0 8.3 41.3 11.7 58.5 34.5


BENZO(G,H,I)PERYLENE 10.0 0 8.4 83.9 12.0 119.5 35.1


OA/OC SPBWOOATB RECOVERIES

??

&-JI

[Ill TP-T-

'ttf ' • ■'£ TT ft J Fv^Pvc ft1 If I x^>Q§

SOUTHWEST LABORATORY OF OKLAHOMA, INC. rOO West Albany • Broken Arrow. Oklahoma ~4012 • Office (918) 251-2858 • Fax (918) 251-2858


REPORT: 8819h

DATE: 03-20-92


RESULTS REPORTED IN mg/L OP Parjs Per Billion (PPB)

PAWAMETBR

TPH 0.5

RESULTS

ND


& c «>'

&^0

CLIENT:

TPH

SOUTHWEST LABORATORY OF OKLAHOMA, INC. POO West Albany • Broken Arrow. Oklahoma "4012 • Office (918) 251-2858 • Fax (918) 251-2858

ENGINEERING SCIENCE, INC. REPORT: 8819i 57 EXECUTIVE PARK SOUTH, SUITE 590 ATLANTA, GA 30329 DATE: 03-20-92 ATTN: OLA AWOSIKA

SAMPLE MATRIX: WATER DATE ANALYZED: 03-04-92 SWLO #: 8819 (MS/MSD) PROJECT: AT 510 || SAMPLE ID: CONFIDENTIAL ID

TPH MATRIX SPT«q|/*»TRlf SPIKE DttfolGATE

MAXRIZ SPIKE SPIKE CONC. SAN»« C0*C. COMC. PERCENT

(ug/L) (ug%) % (ug/L) RECOVERY

20.0 0 if 15.2 76.0%

■\

A-

* >

V V

&-*l

ij o ■ it)' a -

SOUTHWEST LABORATORY OF OKLAHOMA, INC. 1700 West Albanv - Broken Arrow, Oklahoma 74012 • Office (918) 251-2858 • Fax (918) 251-285«


SAMPLE MATRIX! WATER DATE ANALYZED: 03-04-92 SWLO #i 3819 (MS/MSD) PROJECT: AT 510 SAMPLE ID: CONFIDENTIAL ID

REPORT: 8819i

DATE: 03-20-92

TP)T MATRIX gPTra/MAT»TX SPIKE DUPLICATE

TPH

SPIKE CONC. (ug/L)

20.0

SAMPLE CONC (ug/L)

MATRIX SPIKE CONC. (ug/L)

PERCENT RECOVERY

15.2 76.0%

TPH

MSD CONC. (ug/1)*

16.0


80%


2.5%

ß-°l^