bracewell new york jason b. &giuliani washington, … · &giuliani may 26,2011 texas new...

BRACEWELL &GIULIANI

May 26,2011

Texas New York Washington, DC Connecticut Seattle Oubal London

Jason B. Hull Partner

202.828.5850 Office 202.857.2114 Fax

[email protected]

Bracewell & Giuliani LLP 2000 K Street NW Suite 500 Washington, DC 20006-1872

ByFedEx

Jacqueline Morrison Land and Chemicals Division (3LCOO) U.S. Environmental Protection Agency Region Ill 1650 Arch Street Philadelphia, Pennsylvania 19103

Re: Request for Information on Marcellus Shale Flowback Water

Dear Ms. Morrison:

As discussed with Humane Zia and in our meeting today with EPA Region Ill, enclosed please find Chesapeake Energy Corporation's response to RFI Nos. 1 and 4 of United States Environmental Protection Agency Region III's ("EPA Region III") Request for Information dated May 12, 2011 (the "RFI"), CHK00000001 -CHK00000024. Subject to our discussion on Friday, May 27, 2011 with Bill Early regarding how best to prioritize the EPA Region III's pending requests for information, Chesapeake intends to continue working diligently and in good faith to respond to this RFI on a rolling basis. Chesapeake expects to complete its response within the next two weeks. In the meantime, please do not hesitate to contact the undersigned with any questions regarding this matter.

Very truly yours,

Enclosure

cc: Humane Zia, USEP A Region 1II Steven Feisal, Chesapeake Energy Corporation Mike Brownell, Chesapeake Energy Corporation Stephanie Timmermeyer, Chesapeake Energy Corporation

BRACEWELL &GIULIANI

June 9, 2011

Texas New York Washington, DC Connecticut Seattle Dubai London

Jacqueline Morrison Land and Chemicals Division (3LCOO) U.S. Environmental Protection Agency Region III 1650 Arch Street Philadelphia, Pennsylvania 19103


Dear Ms. Morrison:

Enclosed please find Chesapeake Energy Corporation's updated response to RFI No. 1 and response to RFI Nos. 2, 3, 5, and 6 of United States Environmental Protection Agency Region III's ("EPA Region III") Request for Information dated May 12, 2011 (the "RFI"), CHK00000025-CHK00000028.

Very truly yours,

Jason B. Hutt Partner

202.828.5850 Office 202.857.2114 Fax

[email protected]


By FedEx

Bracew~ll & Giuliani 1 I

/t/1 1 7,

.,. Jaso~ B. Hutt

Enclosure

cc: Humane Zia, USEP A Region III Steven Feisal, Chesapeake Energy Corporation Mike Brownell, Chesapeake Energy Corporation Stephanie Timmermeyer, Chesapeake Energy Corporation

BRACEWELL GIULIANI

Jacqueline Monison

June 17, 2011

Texas New York Washington, DC Connecticut Seattle Dubai London

Land and Chemicals Division (3LCOO) U.S. Environmental Protection Agency Region III 1650 Arch Street Philadelphia, Pennsy 1 vania 191 03


Dear Ms. Morrison:

In our June 91h submittal on behalf of Chesapeake Energy Corporation related to the United

States Environmental Protection Agency Region III's Request for Information dated May 12, 201 1, we inadvertently excluded the attachments referenced in the nanative enclosure, CHK00000025-CHK00000028. Enclosed please find those excluded attachments, CHK00000029 to CHK00000174.

Very truly yours,

Jason B. Hutt Partner

202.828.5850 Office 202.857.2114 Fax

[email protected]


By FedEx

Bracewell & Giuliani LLP

Enclosure

cc: Humane Zia, USEPA Region III Steven Feisal, Chesapeake Energy Corporation Mike Brownell, Chesapeake Energy Corporation Stephanie Timmermeyer, Chesapeake Energy Corporation

CHESAPEAKE ENERGY CORPORATION Response to USEPA Region III May 12, 2011 RFI on Marcellus Shale Flowback Water

May 25, 2011 Question 1. Provide a list identifying each state permitted Well that you own or operate in EPA Region III and include the latitude and longitude for each Well and identify whether each Well is actively being drilled, is completed, or is producing natural gas. Please see attachment CHK00000002-000000024. Question 4. Identify your intentions for disposal, reuse, treatment, recycling, and reclamation of Gas Extraction Wastewater after May 19, 2011, including your expected methods and locations for disposal, treatment, or recycling during calendar year 2011. Provide the expected percentage of your Gas Extraction Wastewater by disposal, treatment, or recycling method. For produced water from Marcellus shale gas wells in EPA Region III, Chesapeake Energy Corporation ("Chesapeake") intends to either recycle or dispose of such produced water at state permitted UIC wells during the remainder of calendar year 2011. For such recycling, Chesapeake intends to use filtration in Pennsylvania and West Virginia. For such disposal, Chesapeake intends to utilize UIC wells in West Virginia and Ohio. In Pennsylvania, Chesapeake expects its recycling to disposal percentage to be approximately 90:10 for such produced water. In West Virginia, Chesapeake expects its recycling to disposal percentage to be approximately 50:50 for such produced water. Chesapeake does not expect to generate produced water at any Marcellus shale gas well in any other parts of EPA Region III during the remainder of calendar year 2011.

CHK00000001


June 9, 2011 In providing this second, and final submission of information requested by U.S. Environmental Protection Agency Region III’s (“EPA Region III”) Request for Information on Marcellus Shale Flowback Water (“RFI”), Chesapeake has made a good faith effort to compile and produce responsive information through the date of the RFI, but reserves the right to supplement its response consistent with the terms of the RFI to the extent that additional information becomes available or EPA Region III clarifies the scope of the RFI. Chesapeake is providing the enclosed information on a voluntary basis to assist EPA Region III in understanding the important role that recycling and reuse of produced water plays in the Chesapeake's Marcellus Shale exploration and production activities. In providing this information, Chesapeake does not waive any objections as to the scope of EPA Region Ill's information request authority under the statutes cited in the RFI. Among other things, Chesapeake does not agree that EPA Region III has the authority to require the submission quarterly reports on waste disposal and recycling practices under any of the statutes cited in the RFI, or to submit information regarding all discharges or releases of any substance or waste without regard to the quantity or identity of such substances or wastes. To the extent these or similar objections are made by other companies responding to the RFI, Chesapeake incorporates and adopts those objections into this response by reference as if fully stated herein. While reserving any and all legal rights associated with these objections, Chesapeake responds to the RFI as follows: Question 1. Provide a list identifying each state permitted Well that you own or operate in EPA Region III and include the latitude and longitude for each Well and identify whether each Well is actively being drilled, is completed, or is producing natural gas. Please see Folder 1 on the enclosed compact disc for a revised list of Chesapeake’s Marcellus Shale gas wells. Note, this information is current as of June 2, 2011. Question 2. Provide all Pennsylvania "26R" forms completed and submitted to the Commonwealth of Pennsylvania for all Gas Extraction Wastewaters associated with your Wells for the calendar year 2010, including complete Chemical Analysis Attachments associated with each. Responsive information is contained in Folder 2 on the enclosed compact disc. Question 3. For the period of April 19, 2011 to present, identify your Gas Extraction Wastewater management activities, including disposal, reuse, treatment, recycling, and reclamation for your Wells. In doing so, provide the following: a. For each Well, the actual or estimated amount of Gas Extraction Wastewater generated; “Flowback” is a process whereby “produced water”, which consists of formation water and injected waters, is returned to the surface from the wellbore. For the purpose of responding to

CHK00000025


June 9, 2011

-2-

this question, Chesapeake has provided information on “produced water”; information responsive to this part is contained in Folder 1 on the enclosed compact disc. b. For each facility that has received your Gas Extraction Wastewater, including but not limited to, underground injection wells, wastewater treatment plants, and recycling facilities, provide the name and address for each such facility, the name and address of any entity that transported your Gas Extraction Wastewater to each facility, and the volume (in gallons) of such Gas Extraction Wastewater sent to each such facility; During the relevant time period all of Chesapeake's produced water was either recycled or injected into governmet-permitted underground disposal wells. Further information responsive to this part is contained in Folder 3b on the enclosed compact disc. Note; latitude and longitude coordinates have been provided in lieu of a specific address. c. The total volume (in gallons) of Gas Extraction Wastewater that you treated and recycled or caused to be treated or recycled for all your Well sites; Responsive information is contained in the attachment referenced in Question 3b. d. A description of the method or methods by which you or any third party recyclers recycled such Gas Extraction Wastewater; and Chesapeake utilizes filtration, primarily employing 20 micron filter bags, and dewatering in order to reuse/recycle our produced water. Chesapeake continually explores for ways to enhance and increase our reuse/recycling efforts. e. All modified disposal plans that you submitted after April 19, 2011 to the Commonwealth pursuant to the Pennsylvania Code Title 52 Section 78.55. Chesapeake has not been required to submit a modified disposal plan to the Commonwealth of Pennsylvania. f. Describe your use of pits, lagoons, impoundments or other land-based units for the storage or disposal of such Gas Extraction Wastewater associated with your gas extraction activities. None. g. Provide the latitude and longitude for all pits, lagoons, impoundments or other land-based units used for the storage of Gas Extraction Wastewater associated with your gas extraction activities. Not applicable.

CHK00000026


June 9, 2011

-3-

Question 4. Identify your intentions for disposal, reuse, treatment, recycling, and reclamation of Gas Extraction Wastewater after May 19, 2011, including your expected methods and locations for disposal, treatment, or recycling during calendar year 2011. Provide the expected percentage of your Gas Extraction Wastewater by disposal, treatment, or recycling method. Please see Chesapeake’s previous response submitted on May 26, 2011. Question 5. Submit quarterly reports to EPA on your waste disposal and recycling practices commencing on July 1, 2011 and continuing on a quarterly basis thereafter until June 30, 2012, for a total of four (4) reports. Such quarterly reports shall include the following information for the prior quarter: Chesapeake wishes to register its objection to Question 5 and its various subparts. Question 5 appears to exceed EPA Region Ill's authority under the statutes cited in the RFI because it requires quarterly reporting not currently mandated by any of the statutory or regulatory authorities relied upon by EPA Region III in issuing the RFI. Nonetheless, while reserving any and all rights associated with these objections, Chesapeake is willing to work on a voluntary basis with EPA Region III and the other recipients of this RFI so that an orderly, consistent and transparent process for responding to Question 5 is achieved; currently, no further information is required under this question until July 1, 2011. a. For each Well, the actual or estimated volume (in gallons) of Gas Extraction Wastewater generated; b. For each facility that has received your Gas Extraction Wastewater, including but not limited to, underground injection wells, wastewater treatment plants, and recycling facilities, provide the name and address for each such facility, the name and address of any entity that transported your Gas Extraction Wastewater to each facility, and the volume (in gallons) of Gas Extraction Wastewater sent to each such facility; c. The total volume (in gallons) of Gas Extraction Wastewater that you or any third parties treated and recycled or caused to be treated or recycled for all your Well sites; d. A description of the method or methods by which you or any third party recyclers recycled such Gas Extraction Wastewater; and e. Describe your use of pits, lagoons, impoundments or other land-based units for the storage or disposal of such Gas Extraction Wastewater for your gas extraction activities. f. Provide the latitude and longitude for all pits, lagoons, impoundments or other land-based units used for the storage of Gas Extraction Wastewater associated with your gas extraction activities. Question 6. Identify any and all discharges or releases of any substances, wastes, and/or Gas Extraction Wastewater from facilities that contain Wells that you own or operate and all

CHK00000027


June 9, 2011

-4-

media (air, water, or land) that were affected by such discharges or releases and the estimated quantities of all substances discharged or released for the past five (5) years. Chesapeake objects to Question 6 because the request is vague, overbroad in scope, and, accordingly, exceeds EPA Region III’s statutory authority to request such information. Without any limiting principle on Question 6, Chesapeake cannot provide any meaningful response. As a result, Chesapeake requests EPA Region III provide clarification as to the definition and scope of terms used in Question 6 so that Chesapeake can better assess whether it has responsive information.

CHK00000028

~ ChesaP,~~e

June 8, 2011

Jim Mi ller Pennsylvania Department of Environmental Protection Northcentral f~egional Office 208 West Third Street, Suite 101 Williamsport. PA 17701

Dear Mr. M11ler

Attached is the Forrn 26R Chemical Analysis of Residual Waste Annual F~epon by the generator for fluids, along with the Statement of Qualifications and the analytical report from Test America.

If you should have any questions or require additional information. please do not hesitate to contact me.

Best Regards.

Chesapeake Appalachia. L.l.C

\\ .. l.1! Ud~:n

Tal Oden Regulatory tv1anager North, Eastern Div1sion

Enclosures

Ch~..;.1p .. :1 "- c r !h.' I\~\ t,. fll P•,f1tif>lt

1.1.' '-'·! ~ "':pi'•t • \ 1 .1.1''-'":\ J I, ;(~ 1 I~~ - ~ " ;_,I ·'J~ '" • j I ~' '· "'\\ •r~··~ \":!,.'l':.oA, • 1 ld 11 1 II

~ r r" ') ~ \ -FI- <i • 1.1 \ ..:.~ r ·: ...:~p·~ .- ~; ~- · ., • .:, ... l -V• ,< ;.; r ~ lj J . i • r.t! •. t. · :· • 1 :

CHK00000036

fJ' .P~~nsylvan1a COMMONWEALTH OF PENNSYLVANIA DEPARTMENT OF ENVIRONMENTAL PROTECTION

BUREAU OF WASTE MANAGEMENT

FORM 26R CHEMICAL ANALYSIS OF RESIDUAL WASTE

ANNUAL REPORT BY THE GENERATOR ; This forri1 must be fully and acc~rate'iy-compieted. All requiredinformatioi\nlust'"i)e "l____ DEP.US-EONtv·-- ... ! : typed or legibly printed in the spaces provided. If additional space is necessary, identify Date Rec<;o ;~;~a&'Gene_r.iii'Ncles. 1

l)ach attached sheet as Form 26R, reference the item number and identify the date i prepared. The date on attached sheets needs to match the elate noted below. ·

General Reference 287 .54 -------------'-·----·--·-""'j Date Prepared/Revised 05/3012011 !

---··-- ~ -· ·----········-···----··-j·-···- ·- ···~----··-- · ·-. ----~ ·-. :~=~=-~·~:~=----- ~ .. f::CI!Q:~ _A: ... ~!:!~_ti]_l_~~~~-~~-!9_~ _ _Qf_T_HE_WASTE) INFORMATION !

Cornpany Narne C!•esapeake Energ, Corp:Jr;:,!ion -· . .. --------------·-·-·-·--------------EPA-Generatorlo# ···--~--·~ If a Sl1hsid1ary, Name or Parent Company : .. >·es.ap et.-1..::f' ~ ·nit~r~;H!Cn £ J;·n: Cornp;my Mailrng Address Li:·"" 1 · rr 1 i'J f·f;:; '1 Stree·

-Zi~:;:;:-r-------Phoi,e Cornpanyt\ddrcss L·1st lirrt• -- City State Ext. ~.:'lens PA 18810 5i'0888656·~ Company Contact Last Name F:-ir-tlt:-N:-:-am-e'-'---'-·----'c..:..::: Ml -------Sutifx- · ...... .. ---·--·--·- · '

.. ~1A0'_ott ____ Ma • ~~---·······-··· ---·-·-·· _ Municipality County .:\:11ens Boro Bradford contact Phone E~i ·-·--··-e:·;:;;:liact.Emaif"i> .. ddress--·-----··· ·· -------·-·- ---· ;s7t~-~~~!~6g~erated at ti,1-6~~~airy'-'M3ii1i~~§z~t~~~~~1~;bove)? ------· -··------···--·· ·········.i T ~,;-e;;····---(Z!· r~;; ·· _.J If 'No', describe ocation of waste generation and storage. see a\tacl~ed

················ ·----- ·-----···---c;;;:inty State ..

SECTION B. WASTE DESCRIPTION ·---·· .. ----··---···---·--.. --; ·-· ·--·"··-... ··----····-·-... ----·-·.- ------·---·---..,--·--·~ ----... ~ .. ···-· .. -·- --·---· ·-----~·-·" - l

qesidual Residuai Waste . : Unit of I Time Waste Code Code_Descripti~!' ... _______ , ____ i __ _2mo_l!_':~.. _ .!. Measure l Frame

1 1 t.20 Process vva st:::waters 1 12 422 544 ~--a--~~~yd- .... ~.9.9 ·- 1 --~--- :::· · -, ·· · . ' ' ; lb C ton , C vnE" l.rne

- - --- -- -------:-1-. -::G:--E-N-ER_A_L-:P;'-R-0-P-ER-T-IE-S---~-- ~--- - --;

a. pH Range 5.·:1 0 to 8 ,1 (based on analyses or kncwleclge) ·········rs:·· LiQuid·vv-a-ste .. iE.PATieih"od9o95i ____ ·····-·····------------·----·- ···----m-- ······· ···· ..... ----b. ·Physical'si·ate

L Solid c.::::~l·\ i~1e:hod 9095) L Gas {arnbient ~ernperature e pressUH!)

c. --Physical Appeuance Color ... 9.!:?.1. ... \? ... ~!.2':'::.~.--··· ·-· --·- ______ Odor no~e . -..,j

Number of Solid or Liquid Phases of Separation

Describe each phase of separation .•

2. Ci-iEMICAL ANALYSIS ATTACHMENTS - ------ -·------a. Tne r~· sults of a det.ll eel chemical characterization of the waste, as described in the

il'structions is attached .. A detailed descnrnion of the waste-sam.pjing method.is .. attac-hed. -~·Yes··········· LJ N<:

.. The quality assurance:c;u<llity co11trol.proceCiures.empioy.ed 'b'ytl1etab'orator;i(iesf is · ~.az; ·yes .. _o NQ attact1ed

d . Thc, results of tre hazardousw3'5't(!Cieterri1"i~1atTOii'Ts"attache<i':- ·-·· ·· - . .,--ye-;:-~ No _____ h;! - ----4=---

e. 11 applicable, a detailed e-x!)Tar;·ation-supportingL1sc-otgencrator .. knowledge.fn c Yes [2j No :_ N/A );cu of actual chem1cal '!!'l.~.§~S_!!_ttached.

. 1 -

CHK00000037

25~0-PM-BWM0347 Rev. 1/:?01 I

3 . PROCESS DESCRIPTION & SCHEMATIC ATTACHMENTS I .;~ . Adetalled descriptron of the lilan-ufa~turing aqd/or pollutJon control processes produc ing '"" _j Nr,

the waste, as specified ln the mstructlons , Is attached.

., ,~ ,_ b. A schematic of the manufacturing andfor pollution control processes producing the wasle t~s ' as speci fied In the instructions, is attached.

1 c . If portions ofihc tiiformation submitted are confidentia l, the sub-stantiation for (SJ Yc•\; N J/, :=! "; ~ _j

a confidentiality clarm, as described In t ile mstructlons , is attached.

SECTION C. MANAGEMENT OF RESIDUAL WASTE ~ --=--=----=-=-=-·----1. PROCESSING OR DISPOSAL 'F.Acn.ln IES)_ -

The. area below (a.-d.) wi ll accornmodi'te the lclentifrcation of two f.<cilitles . Attach additional st,e<•l~' t>f!r.essary

a Solid w;~ste permit nu,llber(s) fo r processing or d tS!,osal facil ity being tJlll izE'!d

b Fac il ity Na~ne T_i~C.Oc; 'l t' Address Line 1 i487 Tor1's Run Ro._,a,_,o,_· __ Address Line 1

Address City State ZlP Hol lbrook Municipality

c . Fadilty ContaCt Na;n;;--Title ---Roi -Koiller ..c.:.:::.:.'.:.::::.. __________ _

Phone Email Address

: d Vo l-ume of was to sllrpped lo precessing o r disposal facilitYlOtho p~vJ ous year I 0 cu yd [J gal ::J lb 0 tnn 1c••cr· "

I· a.- s oiid-wasteperrrut .. n•lmberls) for processing or disposal facility belng-u tiifzed .

----------tl. Facility Name

Address L.i11e 1

Address line 1 Address City State ZIP

Municlpal•ty Count/

c. Factlfty.Contact Name

Title PI; one Erpa ll Address

-d , Volume of waste sh1pped to processmg or disposal fac•llly 111 the prev1ous ye<or 0 0 cu yd C gar C Jr, l r•.Jr\ lr- (• l

2. BENEFfClAL USE

a. Has the waste been approved for benefic ial use-?

If ''Yes··, list the genera! perrnr t number or approva l number.

b. Volurrie of waste benefrcla lly used in the prevtous year 0 0 cu ya 0 gal 0 lb 0 tor 1check • ,,- 1

- 2 -

CHK00000038

2540-P.Y1-8WMC3~7 Hev 1:201'

SECTION D. CERTIFICATION I cert1fy. under penalty of law. that I have personally examined and am familiar with the information submitted in this Annual Report and all attact1ed (iocumcnts and that based upon my inquiry of those individuals immediately respons1ble for obtaining the ir,forrna:ion, I verify that tl1e submitted information is true, accurate and complete to the best of my knowledge. I understand that tho submission of false information herein is made subject to the penalties of 18 Pa. C.S. §4904. relat1ng to unsworn falsification to authorities, which include fine and imprisonment.

Cneck t11e follow1ng. 1f applicable:

2J I cc1t1fy ttw in formation r~quired in Section B-1, General Properties was suppliecl to the Department for the year 2009 j ;wd has net changed. 1

Form Submitted: ~ Form 251~ I .___. Other (Specify) ........ m ········m····- ···m···-----··--·--·--------· ·-··-·----·-- . _ 1

Date S\Jbrnitted: _9.~/.9J!?..~~1Q~ ---------------------I r;ertiiy the in formation required in Section B-2, Chemical A11alysis was SLJpplied to the Department for tt1e year 2009 and nas not chan >Jed.

'"onn Submitted. Q Form 26f'l

0 CUler (specify}

Da:e Subrnitlcu.

I c.ertify t ·w 111fonn<.~tw" -equirccl in Section B-3, Process Description and SchematiC, was supplied to the Department forth\' yoar _2010 and h;Js not changed.

F:::nn 26R

Date Submitted: Q~tQ 1/?010 __ --

Name of ;espons1blc Offic1al Title

""?A7. DDeu Signature ~-;{:?::_==-·- .-=:·~~--~:~-~=- Date 06108/2011

- 3-

CHK00000039

2540-PM BWM03-i7 Rev •,2011

~~ ppnnsylvania .ra COMMONWEALTH OF PEN NSYLVANIA

DEPARTMENT OF ENVIRONMENTAL PRO ' ~CTION BUREAU OF WASTE MANAGEMENT

FORM 26R CHEMICAL ANALYSIS OF RESIDUAL WASTE

ANNUAL REPORT BY THE GENERATOR

r This fOrm must be hi lly-arid accurately completed. - Ail required infonnation n1ust be f DEP USE ONLY ' typed or legibly printed in t~ e spaces pr0111ded. lf additional space is necessary, Identify ~D~·e Rece·v;,d i •:ier ;,•~l rl::-:es J each attaclwct sheet as Form 26R. refe1·ence the item number ahd idcnt1fy the date

prepared . The date on attac:hed sheets needs to match lhe c.Ja le noted below

General Refere11ce 287.54 -~·~ ..... Date Prepared/Revised 05'30120 11

I SECTION A. CUEf::!J (GENERATOR OF THE WASTE) INFORMATION Company Name Chesap_~ake Energ_y Co~pora l _on If a Subsidiary . Name of Parent Company EPA Genera o r ID;,I C;~esapeake Opemt10r1~ l!1c Company Mailing Address L111e 1 Company Mailing Address line 2 101 N :vla 1n S t~ee: Comp-any Addre ss -Last l1 ne - City State Zip+4 Phon e .A.thens PA 'I SS 1C -- -Company Contact Las~ Narnl.' First Name Ml

s-,,,; -"'C-: ... -1

S ot ff ' _!Jl ary_o.:.:_ MarY.. A Munlc.pa11ty C o~mty .A.thens 3oro Bradicro Contact Phone Ext Contact Email Add ress 570-888-6564 8406' mary mar :ott a;ch.k.C01] Is tl1e wasle gE:nerated at tile Com pany Mailing Address (noted above;? 11 No ' , describe location o f waste genera 1on and storage . .o:S;:.ce~"-"'-.;J>-"II a"'-:.'-·'l""e""d _____ _

Mun lciparity -------------o::C:-o-u-n.,-ty-------------... -.. --Statc

SECTION B. WASTE DESCRIPTION - -~

Residual Un 11 o f Amount Measure '!Yaste_ C~qe __ ,_ _

Res idual Wasle C~~ Descnption

420 P 1/o' I t 12.422.544 C C~l yo 0 J<l l

j - -=~--P=-H Ran_g.cr~:= -v-a_s_e_"-~_'a-~_rs1_0 ____ _,.1-. -:G~E-N-E-~-A-L-:P::"R-o-P-ER_T_I_Es------'=C lb tJ ~~ ~ :: to 8 1 [based on a naly ~es or ~ n::.wled~l" I b. Physical State C) L•quid Waste (E PA Method 9095) -

)c.

-----Physical Apuearance

CJ Sol id (EPA ·~eiMd 90951 .:J Ga~ (ambient temperatura & t•ressure,

Color _.9I..<I.Y J.o ~.c9wn ----- _ Odor Number of Solid or Liquid Phases of Separation

Describe each phase of separat ion.--------

"2. CHEMiCAL ANALYSIS A TACHMENTS 'a:- The results of a deta.""ile_d_ c_lle_n_J.,...Ic--a.,-1-c=.:h:.....ar...:::a_;_c:.::te;:;.r:.:.;iz::.:..alion ofthc waste. as described In the

instruc tlo~l:! ,] s att~g"J:led . . ..... --,-----b A detailed descript ion of lhe waste sam pliny method is attacl1ed. c The qu;;Ti(y assurar1celquallty "~ontrol pro~edures empi O'J';c:Jby the l aboratory (les) Is

attached d. '1'hc results of the hnarcJous wa ste dete;;:;;mation is attached. e. 1f applicable, a dCtlllled E! )(p lanation supportlllg use of {jenera tor knowledge Ill ~

lleU o f 3ctual chemical analys1s 1S atta ch~~

•i

r"·: --~ j

Ext

·-t::~ 'I · '

-, "'~ t<J r. ~.

I ~! ~I':

~ ~ ·~ ,,,

'i (I ...

CHK00000040

2S40·PM·BWM0347 RQv. 112011

a.

b.

c.

·· 3. PRociss oescRiP"no.N&·s-cH'e.MAnc AnACHMENrs

A detaiied descript;o•l of the manufacturing and/or pollution contrOlpro cesses producing the waste. as specified in the instructions. is attached.

A schernatrc of t11e manufacturing-andiorpo~u'\ion co.ntrofproces.ses -producing thev 1aste. ~z: YE:s as specified m the nstructions. is attached .

. . ifportrons of thf: information ~;I!rnitted are confu:i'entia'i, the substanti<ttior1 for ::J Ye~ a confrdentiality claim. as described in the instructions, is attached.

-:---:---....,--::·-·-·-·· .. -· ........... .. SECTION C. MANAGEMENT OF RESIDUAL WASTE

0 ~Jo

I I

··········-··· ........ .. __ 1_ . .f!3_9_C:§§J?.I.~_ORQtSPOSAL FA . .:::C.:.::IL::..:ITY~(l:::E.:::.S)L., __ .,.......,. --------,

The area below (a.-:.l.i will accommodate the identification of two facilities. Attach additional sheets if necessary.

a.

b.

c.

cl.

Solid waste -pern1it number(si for processing or disposal facilit)' beirig utilized. WMGf~123

Facility Name Address line 1 Address line 1 Address City State ZIP Munrclpa tity

Facility Contact Na;ne Title Phone

Eureka ........ ·····"'······-·---· ·--------

... 41 ~-Second .. $.!!.~~~ ...........

vViifiaf!iiiJ.9iL·:~=~:::·::: .. · -·r;;;· - - 17Yc 1 Williamsport Boro County Lyco'T1ing

·-··••oH000H00 ___ _

......Q.§o~ .. rt~l . . ........ . owner 570-971-9978 Email Address d.ertei@Jertal com

Volume of waste shipped to processfngordlsp .. osai·f·ac"iifty.in t,...h_e_p-re_v..,.io_u_s-ye_a_r-. --

2 COC' 000 0 cu yd 0 gal 0 lb LJ ton (check one,

a. -SOiicl waste permit i1Umber(s) for processing or disposal fa·c·iiity .. belng util ized :· PAC0::26913

b. Facility Narne Address lrne 1

Address line 1 Address Crty State ZIP Munrcipalrty

Fa<::iity Contact Narne Tit!u Phone

·············--···-·········-···-·-··········----·--·· - - -fv1.<::.t.S~~~P.?.r..tYY9..?.t~ .. hY.t.l~g~\X ____ _

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Joe Rost E;ecu .. ti;;-eoirector .. 4'12-673-9701 Email Address rnacm Jrost@,•enzon.net

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2540-PM-BWM0347 Rev 112011

- --:-::-::::-:::-:-c::c-:-·- ··-- -- """·----···········--··- --· SECTION D. CERTIFICATION ---- ···-·---····-·--····-············---·-- ·-· ! I certify. under penalty of law, that I h;we personally examined and am familiar with the inforrnatron ;;uhrnitted in this Annua!

i Report and all attached documents and that based upon my inquiry of those individuals immediately responsible for

I' obtaining the information, I verify that the submitted information is true , accurate and complete to the best of my

knowledge. I under:;tand that the submission of false information herein Is made subject to ihe p;~nalties of 18 Pa . C.S. §4904, relating to unsworn falsification to au~horities, which include fine and imprisonment.

I Check the following , if applicable:

I BJ I certify the information required in Section B-1, General Properties was supplied to ttre Depart111ent for the year 2009 and has not changed.

Form Submitted:

Date Submitted;

IS FQffl1 26R

C C ii1er (specify)

04i0"112010

' 0 I certify the information required in Sectiol"l B-2 , Chemical Analysis was suppliecl to the Dcp<Jrtrnent for the yea r 2009 and has not char·ged.

Form Submitted · iZJ Form 26R

0 O:he; (specify)

Date Submitted: 04i01/20i0 ...................... .............. -...

!S) I certify the information required in Section 8-3 , Process Description and Schematic , was supplied to the Depa ,trnent for the year 2010 and has not changed.

Form Submitted : tSJ Form 26R

0 Other (specify)

Date Submitted:

Narne of ResrJonsible Offrcial Title

s1gnatur: ~_ca~~:.:.::~········ ···················--- Date 06/08/2011 .

. 3-

CHK00000042

THE LEADER IN ENVIRONMENTAL TESTING

Statement of Qualifications Vol.l

www.testamericainc.com

866-785-LABS

CHK00000043

Missi.on Statement & Values

Vision Statement TestArnerica will be the industry leader for environmental testing and data deliverables.

Mission Statement TestArnerica is committed to providing exceptional client service, highest quality legally defensible data, and the most comprehensive range of capabilities in the environmental testing industry.

Core Values

Integrity: We adhere to 1.he higl"est n oral and ethical standards in all that we do.

Client Service: We strive to ensure our clients' satisfaction and success.

Performance: We set challenging goals, hold one another accountable, and reward rp~ult<,.

Technical Excellence: We continually invest in new technologies to provide exceptional data quality and to develop new and emerging methods.

Teamwork: We help each other succeed through a cooperative team effort, in an atmosphere of civility and respect.

People: We invest in training, professional development and career progression for our employee>.

Growth: We manage our business for profitable and sustainable growth.

CHK00000044

Sustainability Statement ~- .

T~::-stAmenca takes pnde 111 bt;,ing the industry leader for environmental testing and data deliverables. Our se;vices enable clit.>nts to make business decisions that positively impact the environment, the importance of which is not overshadowE:d by TestArnerica's commitment to ope1 ating in an environmentally conscious manner. In response, TestAmeica obligates Itself to achieving sustainable financial returns and respecting the environment and community within which •.ve work and live.

Su~,tainabilty hy deflnit on i~> inherently broad. TestArnerica follows a sustainability framework that ensUies the .. ompany oper<~tes 1n a manner that achieves financial success through the practice of environmental stewardship, etrlicalleadership and by embracing our role as corporate citizen in the communities where we work. The follndation blocks of the ·;·cstArnerica Sustainability Framework include:

Governance, Ethics and Compliance: Operating in a responsible and ethical manner in accordance with our e•hics policy and the !avv, promoting ethical sales and purchasing practices;

Employees: Providinq 2 rewarding, diverse, and inciLJSive wc,rkpiace for employees;

Environment, Health and Safety: Capitalizing on the !nherenr financial and social benefits stemming from '.uund (•Jw!:<JmncrJtdl pr<•diu·'· <mel a >afe <Jnd healthy workplace;

Supply Chain: Wor!.. ing <:vi:h suppliers to Improve their social and environmental perforn c.nce and cooperatively ;eekin9 oppo· ·L, ... HtiE'' tG reduce the carbon footprint relative to the delivery of services to TestAmerica laboratories and ri!E'IIl ,.

Charitable & Community Support: Encouraging the support of local and national charitable organizations and or her Initiatives that support local communities connected t_o our business and employees;

Economic Impacts: Using financial resources wisely t•.:> benefit co1npany stakeholders and to address key su5talr:ab.lity issues;

Public Policy: Work;ng with governments. regulators and policymakers to improve the quality of analytical methods ensuring the consistent delivery of legally defensible data.

Ou1 employees v.•ork to integrate sustainable solut1ons witt · in every business division, every service category <~r,d e'.•ery dt,pcl\rw?nt of our operations. Susrainability is integral to and embeddt:'d within all our actions and :!~if:' serv~<.e "::'!fi pro\;i:..~ :·.

CHK00000045

3

Introduction

Through strategic inve~trnent in people, technology. capital equipment and infrastrunure, Tesl:flmc:rka ha:; dP'!''klpHi

the world's le11dmg env!lonmental testing company. Our unique combination of expcnence ;,nd c><pert1se I> backr:d by recognized industry experts and an unprecedented scale of andlytlca : services that addres5 .~m ext0nsive range of environmental applications. TestAmerica is a leading provider of critical analytiCal support scrvicb to bo:h p~1biic and private sector clients. Whet:~er it is the Department of Defense, Department of Energy, Fortune 500 industria is. or the consulting and engineering firms that support them, TestAmerica leads the industry in developing i1 novative solutions to address their testing needs.

TestAmerlca focuses on the refinement of method~ that add res~ cun ent environ1nenta! issues and invests in the development of new solutions for challenges that the market and our clients anticipate facing in the future. To facilitate this process, TestAmerica routinely assumes leadership positions with a variety of environmenta! trade associ?.tiom, regulatory review boards anci lab industry steering committees. TestAmerica's leadership helps to $h!lpe how analytical solutions are brought to market, sets the standard for quality and ethics, and challenges conventional wisdorn to driv<~

an industry culture of continuous improvement. TesiAmerica holds active leadership positions in each of rhe foilowinq organizations:

• NELAC- National Environmental Laboratory Accreditation Conference

• ITRC -Interstate Technology & Regulatory Council

• ACIL ·American Council of Independent Laboratories

• SAME- Society of American Military Engineers

• AWMA -Air & Waste Management Association

Through a network of 36 fixed base lab operations, 33 service centers and a fleet of mobile laboiAto;!es, TestAmerka brings a unique blend of expertise and convenience to its c~1stomers. Our ability to deliver thE' ;•,o idr:-st v.:.ri.ety of environmental testing services is a function of our unmatched scale. Among the large variE>ty d !E:·:;ting <lpp!lu ltiGns TestA1ncrica provides are:

• Metals by iCP & ICP/MS • Chemical Warfare Agents • Low Level Mercury • Petroleum Hydrocarbons B;oav<1ilabillty • Bioavailable Arsenic & Lead • Radiological & Mixed w,~ste • Alkyl Tins • Radiobioassay & Radio Dating • Metals Speciation • Sediments & EllJtriates • Trace Level Volatile Organics • Plant & Animal Tissues • Trace Level Semivolatile Organics • Aquatic Toxicology • Pesticides by HR/MS • Drinking Water • Agricultural Pesticides • Mold, Fungi & Legioneila • Herbtcides • Ambient & Source Air Emissions • PCB Congeners & Homologs • Geotechnical • High Resolution Dioxin & Furans • Multi-Increment Sampling • Explosive & Energetic Compounds • Oil Fingerprinting/Biomarkers

4

CHK00000046

"llie expertise provided i)y Test America, and the services we offer, are de5igned to address the specific requirements of;:; broad spectrun of regulatory programs. The ability to understand regulatory platforms. the decision criteria they drive and their prescr-iption for quality analytical testing is critical for the development and delivery of test results that meet the neecL of tiiP.il intended me. TestArnerica has long led the industry in the development and refinerr ent uf analytical tcest rnE-thodoJc,qi(•S for a host of regulatory programs and has often served as.~ rnemb!~r of steerin9 conHnittee< who t•ave ~h 1ped the standard of quality and practice for the environmental testing industry. Among the regulatllrY progr.J!TJ> Te~tA:ll'~rica routinely supports are:

'

• Resource Conservation & Recovery Act (RCRA) • Clean Water Act ~ CWA)

• Clean Air Act tCAA) • Safe Dnnking WatE·r Act (SDWA) • Conwrehemive Environmental Response,

Compensation & Liability Act (CERCLAJ • Superfund Ame'1dments & Heauthorization Act

(SAHAi ~ Toxic Subst<mces Control Act (TSCA) • Federal 1nsectic1de. Fungicide & Rodenticide Act

iFIFRA) • Nationa l Environme11tal Policy Act (NEPAl • Inland, Upland & Ocean Testing Manuals • Total M.:;>:imum Daily Load (TMDL)

• National Pollution Discharge Elimination System (NPDES)

• Marine Protection, Research & Sanctuaries Act (MPRSA)

• Maximum Achievable Control Technology (MACT) • Boiler & Industrial Furnace (BIF) • Radioactive Environmental Monitoring Program

(REMP) • Cluster Rule • DoD QSM, Version 4.1 • Leaking Underground Storage Tank (LUST/UST) • Comprehensive State Brownfields Programs • National Em1ssion Standards for Hdzardous Air

Pollutants (NESHAP)

5

CHK00000047

TotaiAccess -----------·-------------·-----------·-----------

Total An overriding benefi~ that TestAmerica clients receive as a function of our scale and coverage is t11E' inherE>nt convenience in the way we deliver our services. Convenience takes on many definitions and each client':; clernand~ are unique. TestAmerica adds the element of convenience to its analytical service offering in the foiiO\.-'.'ing W<lj!S.

Totalr'\ccess allows you to track all aspects of your environmental data program, with instant access through your own familiar web browser. TotaiAccess is a web-based project information tool that provides you with: '

~r- ~=;~~ •· '¥"'"• • _ .• --~-~"'- .!1 ... ~ .::;:-.z.

• Rapid Data Access • Complete Document M;magement Library • Point & Click Downloads of Project Files • User Customized Data Reporting Functionality • Automated Comparison Against Hundreds of Regulatory Lists • Data Relationship & Trending Wizard • Analytical Budget Mar,agement • Fu!ly Customizable User Pwference Settings

Total Access provides TestAmerica clientele with online, secure access to services that enable faster communications, rapid access to data, and a centralized repository for all your projecl information. Users of the Total Access system benefit from having ...

6

• Quick reference to their contacts for each site or program they manage with TestAmerica support. • Instant notification on project status, including results, electronic deliverables and other ducuments

generated by TestAmerica. • Online access and download of project documentation including invoices, reports, EDDs and COCs • Interactive search utility for analytical capabilities and methodologies available within the TestAmerica

organization. • Interactive search utility for lab certification programs detailing which TestArnerica labs hold accreditation

and for what program elements. • Customizable displays capturing data in a single grid and single click downloads to Excel, PDF. or XPS. • Budget management tools to keep track of analytical expenditures and purchase order crcilings

'\,. ,, ............. , ...

The TotaiAccess system is available free of charge to all TestAmerica customers.

CHK00000048

Ask the Expert

Ask ........ The Expert

Tf.stAtrericil is reco JniLNJ <JS the industry's technical leader, focming on global concerns related to environrnental testing. Featuring over 30 mdustry professionals, TcstAmerica's "Ask the Expert" program allows any individual with r.1 question reiJtive to environmental testing to access the thoughts and opinions of recognized experts in their field through a free, easy to use online platform.

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"Of all the serv1ces requested by our customers, none is more sought aftt'r than <JtJr knowledge. Ali environmental decisions are in part b<Jsed upon the data collectl?d. Our customers prefer ;:md m some Cdses demand the app11cation specific expertise we provide as 1t adds assurance that data provided appropriiltely rnatches their decision objectives," offered Jim Miller, Vice President of Marketing and National Accounts .

CHK00000049

7

Mobile Laboratories

Environmental projf;'cts of higi, sen:;itivity and compressed time lines car- require on··site labor;.•ory supporL Testf,m c. ncd has a fleet of mobile laboratories equipped to address virtually any testing application that C<•r• bf> do~,,, in,, fixed base lab. Typrcal on-site projects comph:ted by lestArnerica include srte assrssments, investrgation.;, r<'trlPdiatiGn p!urne deline<Jtion, groundwatE•r monitoring. natural attenuation. soil gas surveys and pt>rimerer arr rnonrto1 •ng.

Mobile lab analytical results are available for revrew rn the field immecl iC;tely upon completion. Hh!ilt·, a•<" r=•O'-:!d(·d ~fu.-r

each analysis with final hard ropy report provrded upon completron ofrhe sampk delivery group. D:.Ha b oi") rnilde available via the ·lotaiAccess system for r.en· nte project suppor·t personnel.

TestArnerica also has an extensive history assisting clients with out~ourc ed manag<~rnent of their OP·Sitt: laborat(;r)facilities. Utilizing a customer service based business model that employs commercrallaborc;tory b;~st pract:cc·s. TestAmerica assists clients with:

• Analytical instrument procurement and maintenance • Lab supply procurement and inventory management • Vendor selection and management • Establishing and managing performance metrics • Managing operation and staffing schedules • Work load planning and surge capacity management • Developing internal and external client feedback systems • Records management and storage.

TestAmerica's on-site lab management programs help (lients achieve their goals of cost reduction, process improvement and system optimrzation. Our strategy, which is employed throughout our industry's leading network of labs. drives focus on cost control. productrvity improvement and increased customer satisfaction.

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CHK00000050

National Program Coordination

Ciients mterested in devel ~>ping a uniform approach to contracting lab services on a national level benefit from

resr /\wericc~'s unique c:ppro,Kh w national accou,,t support. TestArnerica is the only environmental lab st:!rvices provider to

offer truly natrona! coverage through a network of over 65 business locations in the cor.tir1ental United States, Alaska and

>-iawaii as wei I"'" internationa lly in Bangkok, Manila, a1 d SeouL Our coverage <1llows Test.b,merica to provide its national

cu:;t<nnt:• '• with rl i.>t<'Mith :rnd depth of S<'l vin: offe1 ings that is unmatched in the industry and couple that coverage with

al l the <.orweniETces olfe· (:d by a local suppltet. Each of ou1 national servicE> programs is customized to meet the Lmique

rw•::<i:~ of !:•ii( r1 < U'>l<•nwr '". d i~, :r~itnilged through a s1ngle point of contact a National Program tv1anager, capdble of m cht.·stratir•q th~-> d"l1ver .' of -,,:rv ices from the entire ·JestAmerica network.

Among the many benefits clients enjoy when contracting with TestAmerica on a national basis are:

F-inancial Driven by individual buyer phik.>>'JfJ hy and goals. TestP,merica dt:ve!op; c< l'i<Jtn ser w:<· p l•·kaq!'' that cr.~ate financi~l incentiVi! ~nd ·'C2k: Hon0my bePefns fer ou1 ci:•,'nts. 'iuprwt ting a variety of indL>try pr;:-ferrEd E: pr<xur<:rnent $}'Stern~, TestAmerica facil:tates further dient ~<JVings and sus!.ain,;bility oby2crtves through the us!' of f:lf:'r:.tr,;i,K d;ll1111(~rc·~ te<.hnvk1cv.

Consistency & Centralized Program Management ThE> Te~.tt,merie<J approach to n?tionai progrc~m support drives cc·nsist.::ncy in th.:: 'ncnner in wh,ch andytical data are developed, prep:Jred <11\d deliver~d to our cii<:nts. Our approach provides clit,nts a>st.nance that dat:• th<;y obtain to support a variety of p;ograms under a ''<Hiery of 10gulatory requirements is prepared \v:th a standa1d of care and ctrtalyticai practice that is consistent ;·,cr~~;ss l<1bCH<1V::ry facil1tie:

Consolidation W;\h over 65 bv ines; location> 1n the United States. Alaska and Hawaii TestAir<erica couners prov;de rnore geographic coverage thar: any otner lab in \he country. Our combination of locatic,ns rt1ciir<t<Wt> n:rtificot:on~ in a!l 50 states and under several government pro~;ra:m. AL :ocations prov1de logistical support for s<'lmpl>? transport to and frc::•rn the lab and many locations offer samplin9 support to assist ciiPrtts with their c:ornpliance rnonitorin() ne<>ds. TestAmeric~·, broad based coverage is unique in the 1ndustry and p·ovides clients the opportunity to centralize their program, leveraging their purchasing dollar without compromise to the serv:ce dernands of their monitoring programs.

Custom Planning Complex project> oftc·n requift' project specific quality assurance pl~ns cus.trJmized to suit t•w m~ed~ of the regulating body. T.;,stJ\rneric,J routinely assists it> clir:nts with Evaluating project opecific data quality o!.ljective> and employs appropriate analyt10l tec:hniques to ensure that th::ne objectives i.lre consistently met.

Testi\merica SOPs are widely utiiiz.::d in project plans governed by federal and state regulators ar,d are wid12!y recognized for their h1gh quality standards

\"ihen commonly pre~<.ribed test rneti1ods don't meet project specifK needs. TestArnericil works CO<Jperatively with its clients !'t, develop sound scientifi( applications that deliver confidence ,3nd data suitable for 1ts Intended use. As the industry leader. TestAmerir.a routinely serves on industry ;teeriP9 cornmittees that ~valuate, tc,>fine and promote n"!w ~nalytical practic•~s to ad:Jr«ss the evol;•ing testing needs presented by en;erging analy<ical chc llenges

Database Management National and rnlllti-national clients who centrally manage environmental data benefit from Test America's information technology expertis<~. Our staff of over 100 dedicated IT professionals focuses exciusive!y on tlw delivery of dor.a via electro·1ic means to accommodate hundreds of cii<mt custom data rnanaaernent systems.

The procurement of enviror·rnental services is being r(';vo!utionizE'd by the introdLKtion of new <)n·line business software ~olutions that help clients efficientiy nunage their expend1tures for environmental services. TestArnerica leads the ind,mry by providing a dedicated team of fmance professionc.ls to assist clients with the implementation ;:lrld management of their e-solutions for procuring labor;ltory services, saving each client significant time and money. TesrArnerica supports dozens of commercial and client proprietary e-procuternent systems that includ€':

• Ariba • Bottom line Bl;siness • Enfos • Exostar • OB10

• Oracle • Oii-Dex • Web-Commerce • WebEDI • Xign

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Services a ned C·apabili'ties

Laboratories :

TestAmerica is the leading environmental testing firm in the United States, including 36laboratories and 33 service centers providing innovative technical expertise and comprehensive <malytical testing serv1ces. Specialty. analyses includf:: source and a1nbicnt <Hr, aquatic toxicity. explosives, specialty organics, dioxins, drinking water, sediments and tissues, emerging cont~minants, radiochemistry and mixed wa>te testing.

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laboratories:

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Personnel & Management ·------------------------------- ....

TestAmerica attributes its success to the professionalism and technical expertise of its people. Ench person contributes directly to the company's growth and success. TestAmerica has made a commitment to its employees to help them achieve both personal and professional success.

TestAmerica employs exceptional people who welcome challenges. We value and reward high performance, hard work, honesty and temnwork. Test America emrJioyees hold themselves accountable to the hi9h<~sr standards oi ~>thirs. trust, and quality. These high professioria sta"ndards, coupled with unparalleled technicall,::>adershi~, dHided!y set TestAmerica apart from the competition.

,, See Organizational Chart on Page 13

12

CHK00000054

i

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Organizati~nal Chart

James E. Hyman President & CEO

I I I I I

Dr. Keith Mike Bogar Wheatstone Jim Miller

coo VP of Mar~ting & Dave Spurlock coo

Products& National Accounts VP of Field Sales TestAmer ica Laboratories

Services

General Presl~ntof Director of Exe<:utlve 1- 1- 1-

Managers QED 1- National Directors of Environmental Accounts Sales

O~tions President of National FC'deral - i- METCO - Accounts ..... Programs

Director Environmental Managers Director

.__ Director of President of Dire<:tor of TestAmerica '-

Client Advocacy Drilling

Marketin']

'- President of EMl.abP&K

T I I I

Dr. Charlie Carter Nancy Ploof Benjamin E. Erwin VP of Quality Human Resources Dan Santaniello

CFO &Technical Director CIO

Services

Corporate Director of HR Infrastructure ..... 1- 1-Controller

Technical Managers Managers Services

Financial Legal& HRIS UMS - - Contracts System r- Conver~lons Director Director Administrator Manager

Financial Director of HR Applications

- Reporting ~ Quality & Client Project Manager 1- Ot!velapment Director Advocacy Director

Applications "- Support

Managers

13

Executive Team

James E. Hyman, President & CEO Mr. Hyman is President and Chief Exewtive Officer ofTestAmerica Laboratories Inc., reporting to

the company's Board of Directo1 s. Prior to joining TestArneric:a in 201 1, he served as CEO of Cornel\

Companies, inc., a provider to govemment agencies of corrections, education, rehabilitation and

treatment services. With over 25 years of experience in international business leadership, Mr. Hyrnan

also has held ext.>cutive positio11s with.Starwo;;~i'l·lotels & Resorts Worldwide, GE Capital Servic;:s.

McKinsey & Company, and JP Morgan. Mr. Hyman curre11tiy serves on the Americas Board of the

Grosvenor Group, a global real estato? company and chairs the not-for-profit Mega-Cities Projef'. Mr.

Hyman has an MBA with Distinction from Harvard Business Schoo\ and an AB wit.h Honors fron1 the

Universi i y of Chicago.

Dr. Keith Wheatstone, Chief Operating Officer With a Ph.D. in Analytica l Chemistry and over 40 year~ of enviror;mentallal,or." tory e~per icnce. Dr. Wheatstone is responsible for the daily management of all TestAn <:rica I. aborawries faci!ities. The coo·-, responsibilities include allocation of personnel and resources, long-term planning, and developnwnt of technical policies and m_:magement plans. Dr Wheatstone is a Chartered Sc ienti5t, Chartc:red Chemisr and a Fellow of the Hoyal Society of Chemistry (UK).

Michael J. Bogar, Chief Operating Officer, Products and Services With over 25 years of executive management in marketing, sales, operations Z>~Kl business leader~hip, Mr Bogar is responsible for the d2ily management of all of rhe Products and Se; vices businesses. The COO's responsibilities include the development and execution of business plans for all the P10ducts and Services businesses.

Benjamin E. Erwin, Chief Financial Officer Mr. Erwin has 15 years experience in developing, executing and li::<lding globa1 <:oroor<lti:' strate9ies aeo~s a variety of industries. As CFO, he is directly responsible for rnarHge•1wnt of fm;wce. iKCOuntin<J trea~u ry and purchasing functions at -restAmPrica He has deep tinanciill ~'-Pi:'! tis·: with ~ t rent,;th 111

corporate finance, plann1ng & ilnalysis, merger & acquisition transactions ;; :1d I~?S1 runuring. M i'. Erwin graduated w1th honors degrees in Economic and in Politics from Wahe Forest LJpivc;rsity.

James Miller, Vice President Marketing & National Accounts Mr. Miller is responsible for the company 's National Client Program5 and rnarl<et:ing related efforts, reporting to the President and CEO. Mr. Miller holds dual degrees in Chemica! Engineering and Journalism. Mr. Miller previously worked with Occidental Petroleum Corporation as well as various media outlets. Mr. Miller has 23 years of experience in the environmental industry, 20 of \.v: 11(h he served in various officer posts.

CHK00000056

Dr. Charles Carter, Vit.e President Quality & Technical Services Dr. Charles Carter is Vice President of Quality and Technical Services, reporting to the President and CEO. In thi.s role he has overall responsibility for corporate quality assurance and laboratory technical development, and he is also involved with legal issues, contracts, health and safety, and information technology efforts . Dr. Carter has a Ph.D. in environmental chemistry, has over 30 years experience in the environmental laboratory industry. and is a recognized industry expert in numerous areas of environmental and analytical chemistry. He has been active in various industry organizations and is a frequent speaker at environmental forums and conferences .

David B. Spurlock/ Vice President Field Sales Mr. Spurk,·.:." is VICe President of FiE'Iti Sale~ for TestAmerica Laboratories, Inc. and has overallleaders1 ip re~por's'hill!y for thr field <1nd f,,deral sales teams. He v,;or"s 111 close association with Jim Miller, Vice Presicen t of Marketing and National Accounts. Mr. Spurlock holds a B.S. degree in Business Admintstr;.;tion from Robert Morris Unive. sity and has 25 years of leadership experience in the clinical labort:tory ir,dustry with such companies as Sm1thKiine Beecham, Quest Diagnostics, <jnd LabCorp Inc.

Dan Santaniello; Chief Information Officer Mr. S<Jntanie!lo is CIO, reporting ;o the President and CEO. In this role he has overall responsibility for information technology and Laboratory Information Management Systems (l.IMS). Mr. Santanielio has ~'B.S. in Electrical Engineerir•g ;, nJ has over 17 years of experience gained through various information tr:chnology and operation:; nlilnagernent roles In the environmental lab industry. Mr. Santan iello is an industry leader in hts iield ha•:ing designed severalliMS and on-line environmental data systen1s in .:ornmercial ust~ today.

Nancy Ploof, Human Resources Director Ms. Ploof serves as the Hurnan Resources Director responsible for leadership, functional expertise, and strat,:gic direction for the management of human resources throughout the organization. She worh ck,seiy with all levels within TestAmet ica to identify and implement necessary HR strategies. She ho,cf s an/\./\. in '-iuman Resources Managernent from Baker College located in Flint, MI. She holds the Professionc!lln Human Resources Management accreditation (PHR) from SHRM since 2000. Ms. Ploof has 1 r; yciJ;~' of r:nvironrnental teqin9 industry expe-rience, 11 of which have been in the HR field.

15

CHK00000057

Senior Management Team

Chip Meador, General Manager Mr. Meador earned his B.S. and M.S. degrees in Botany/Ecology at the University of Florida. He hJs I.H"en a General Manager since 2007 and has worked in a variety of n.anagement roles in the environmental industry since 1980. He is experienced in all aspects of laboratory operation and management and is v0ry familiar with RCRA and rrany aspects of hazardous waste management.

~ l

:.=-:~.J Scott Morris, General Manager Mr. Morris, as General Manager, has overall leadership responsibility for 10 Te~tAmerica labordtory locations based in Alaska, California, Hawaii, Oreqon and Washington as wr·11 d) Soutl1<:~<1>t Asia. In 13 years with the TestAmerica organization. he l1as served in a variety of lrader>hlp roi<>S rnclud1ng General Manager, Laboratory Director, Procurement, Marketing and Business Development. Mr. Morris experience also includes mergers and acquisitions as well as post mer9er integral ion. Mr. Morris earned an MBA at the University of Warwick in Coventry, England and his undergradu<'lte cleqree from UCE Birmingham, Engl;md.

Chris Oprandi, General Manager Mr. Oprandi has been I ll the analytical industry since 1983. He began his care•.:r as a laboratory technician and then advanced into laboratory management wht~re he is CllfiNltly Genet al Man;;q:·r. 1'/;r. Oprandi is sktlled 1n designing improvements to increase capacity and in tdentifying and elirnir,du·,,,; production bottlenecks. He is experienced in all aspects of laboratory ma•.agement: •.. roductio.-. control, project management. database management, quality assurance, environmental health & s:dety, business d€'velopment and customer relations. Mr. Oprandi has extensive management anclleade;;hip experience. He has developed and in1plernented numerous training programs addressing both thr~ technical and leadersh tp functions of the business.

Dr. Jack Tuschall, General Manager Dr. Tuschall earned his Ph.D. and M.S. degrees in Environmental Engineering Science at the University of Florida. He has been a General Manager forTestAmeric;:; and preclt~cessor com;Mnies for !he past 9 years. Dr. Tmchall has extensive experience in managing full-service analytical laboratories; analytical methods development; design, implementation. and management of environmentalrnon'rtorin~J programs; trace organic, inorganic, and mixed-waste analy5es; design and implementation of qua!ity assurance ptograms: and production and use of analytical reference standards. His diverse experience in the environmental analytical chemistry field provides the foundation for successfully leading the Mobile. ~~ashville. Orlando, Pensacola, Tallahassee and Tampa laboratories. In addition to his Generall>~ana9ement responsibilities, D•. Tuschall is the Director of Best Practices, Environmental Health and Safety Director and IS responsible for fostering Continuous improvement through tlie development and implementation of best practices across the company's laboratories.

Rusty Vicinie, General Manager Mr. Vicinie b responsible for the operations ofTestArnerica laboratories in Kr_1oxville, Dayton, Czntc,n, Pittsburgh, King of Prussia, Edison and Burlington. Mr. Vicinie's professional e:<pertise include<o environmental chemistry focused on air toxics, sediment and tiSSlle analysis as v1ell as having il background in industrial hygiene and clinical laboratory services. He holds degrees in both Cht:'1•!~\ry and Biology with gr<lduate work conducted in the areas of Analytical Olf?.rnis!ry and Pharrnacoiotr;' !\k Vicinie has 29 years of analyticallabo•atory experience with 20 of thc,se years being in the envir(Jt ,m,;ntal practice.

CHK00000058

Dr. Richard Burrows- Director of Technical Services Dr. Burrows is the Technical Director for TestAmerica's network of laboratories in the United States. His duti('>$ include implernc-ntinq new technology, impro•Jing E>X~St1ng methods and leading technic.al groups within Test!irnerica. Dr. Burrc:·.v~ has over 25 years of expenence in analytical chemistry working in both <!cacl.=mic and cornrnerciallatloratories of which 18 years have l.Jeen 1n the environmental laboratory fl<'kl. He h.':S b~~en ;:,ctiv,Jy involved with environmental methods and techniques through the U.S. Env ronrnent;,l Pmtection A9ency iUSEPAl and American Council of Independent I. aboratories (ACIL). His rnethod development ·...vorl-. h«s irr;olwd bringing new perspPctives tcJ method detection li1111ts, calibr<;tion,~ (Jl·<JI:ty <:is;,urance <md quality control and method developrne11t. Dr. Burrows is currently a member of the .j bw,r,:,nmental Laborat<)I.Y Advisory Board and is tWICe a recipient of the 1\C!L Preston Millar J\v.;a.rd. Dr. • Bcl;ro·,vs received :;is f<.S 1n U••:'mistry and Ph D. 1n An-:~lytictJI Chemistry from the University of Bristol in fn,:!lann.

Sharon Gordon - Legal and Contracts Director Ms. Gordon is responsible for contract review, negotiation, general legal matters and oversight of cont1act compliance for the entire TestAmerica group of companies. Ms. Gordon regularly conducts training for ccrnpany employees on contracts, as well as ethics and compliance issues. Ms. Gordon is an attorney, with degrees fron: Hastings College of Law (JD) and U.C.L.A (B.A. and Masters in Environmental Planning), and a member of the State of California and Kansas Bar Association. She has 3-1 years of legal experience including 29 years experience in the environmental consulting field, 16 of

.·.:' . whkh have been with environmental testing laboratories . . ·-·~ ... ._ ...... .:. .. ,

Bosco Ramirez- Operations Director Mr. Hamirez has ope1 ational responsibilities that include defining standard operational policies, development and provision of training, as well as operational tools and process development. He also i:; responsible for the temporary takeover and management of individual laboratory operations during periods of transition. Reporting directly to the Chief Operating Officer, Mr. Ramirez works closely with the Genera! Manager team to address operational needs throughout the TestArnerica network of laboratorie~. Mr. R.Hnirez holds a Masters Degree in Analytical Chemistry and brings over 20 years of experience in the env1ronrnentallaboratory field where he has held positions as Lab Director, Technical Director, Quality Assurance Director and Client Services Manager.

P.ay Frederici- Director of Quality and Client Advocacy Mr. Frederici i:; highly experienced with 28 years in the environmental testing industry and extensive ledcie• \hi;:: & management expertise. He possesses excellent abilities for finanCial management, strateg1c planning, performance monitoring, policy development and enforcement. A5 a strong and dec1sivc decision-maker, he takes personal responsibility to spread customer service awareness and leacl organization~:~! improvements and solve problems. Through concise communication, presentation, t-echnical writing and techr,ology/cornputer expertise, he is an organizati<Jnal change agent

Tim O'Shields- Director of Client Advocacy Mr. O'Shields is a passionate, self· motivated professional with 29 year of experience in the environmental laboratory business. Mr. O'Shields' roles have ranged from positions in laboratory and corporate management to roles in technical leadership. He has spent a number of years in developing and delivering comprehensive leadership development programs. Most recently, his role includes development of programs and training to enhance client service company-wide to Best in Class. This roie i•Kiudes hands· on work a::ro~s the company for process improvement. Major strengths are technical depth, laboratory operations, business management, leadership team development, quality assurance, process improvement, action pl,,nning to resolve issues and for business growth, and business development

CHK00000059

Resources

As the world's leading environmental testing company, TestAmerica offers an unparalleled collectron of phys1cal resources designed and managed to support the wide and varied needs of our clientele. Strategically pos1t1oned expertise and a cawfully orchestrated system of planned redundancy provides a platform for ;ne clt>livery of analytical services that meets the exacting needs of hundreds of regulatory and client programs wh1le providing the capacity to address peak demand without compromise to client schedules and budget

Facility & lnstrument·Summcrry -------------

l,c,_ ,Facllities Size, Employees and &~ ~M:JQr Instrumentation w, :0:•' ~ ~ :.·- -

Major Instrument Summary

~

I

' ., VI ... <( ,. u

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A•>ehorage Laborarory 36oo I s ..... _______ .. _ --.. - .. ;---i- ---t---t------1 A1.rst:in ... aboratory 27000 40 3 1 _ .. _ B~ngi.;c ~~ . Thaii~11d Labor~tory 3300 10 ----, Buffalo Laboratory 30000 100 1 I 1

I ~

Conn<!<tiwt (She! ron, CTi t.•oo·•t•)"l 16000 4() I. 1 1 1 1 , i

Corpus Chr l;t t abor-'-a·t'-'-o-'rr:...' -------+-'1-'--S'-~ov:..;_+--'3:..:0_t---ii--l-+---t--l -ii---t--1-f Da11on Labo•ator)' 20:JOO 60 1 1 1 2

I I }

1 ·--·-,- r-: --7~----~

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Houston Laboratory 30000 60 I 2 1 2

~lrv_i_n~_L_a_b_~r_ar_o~ry'-·-------------4~0~0~~o~.~1~:n~--+----~-4~4-~t5~+---~~2~4-~2-+-~'-r--·-· -i---~--~ King Of Prussia Laboratory i 0000 46 1 2 I 1 I

) ] --···- --1--'-'N.:;as:...h;.:.vl:...lle:....::La:.::b~o-=ra..:.:to:...'Y'--' - - - -----r-4..::8.::.000;.::...-;•- i..:l.::.5 --+·--;_3 _ ·-·····~·-··

Norrh Canton Laborator)' 51000 ifJO 1 1 ' : Pensacola Lal>oralory 20000 43 I ---;-, i I ~

3 2 I

R•chla•1d La bora tory 40000 35 1 1 1-;..._;_--'--..<---------t---t----t---+--t-- -t---t---t--------~ --- .. -S•n Francisco (Pieasa~ton) Laboratory 210C.O 35 ; 1 1 l I I Savannah Labo'"tory 55000 iOO 2 -:1---1-·-4- +--j--t-- -1- 1 2 I I

~ea:tle Labotatofy ~ ' ioooo n 1 .1 " 1

1 2

Tallah-a \ see Laboratory 26000 40 1 i 3 "1 I ~-".::..:.....:..:.:.::..:...::.::..:....:.~-------+-.::..:..::.::..:...+__;,;:.......t---i--'-+-__;,;+---=---11---+-;:..._ ·· - - .. " ..... - ....... ! ....... _·--+---! r-~:...-·t~1p:..:a:..:l.::.ab.;..o:..:r.;..at'-o~ry ______________ 1 __ 14.::.~.;..00-i--'-"7'--+-----t--";__+'--2'--il __ .::.3 __ t--~i-'-2;__~1------r-~3-~--i----

Va 'pa raiso Laboratory 15000 35 I I 2 3 2 I

-- .... -----Tot.> I 976100 2111 26 45 75 60 .?. 69 :~-:- 5)

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,, td l :'tr::+"i!'~ll 'IH~111F-! • ,, r. • Major Instrument Summary

iii ~

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Facilities Size, Employees and ~ ::: ~ ·j E ~ "' .2 ~ ~ E ·~ e i3 0 ·!! ~ t i "' " 9 "' ~ e 8.<= .g· ~ II ~ •

rvi'aior ~~-~trumentatlon "' ::; ~ l5 e & .s 2 ~ :X < ~ t: ~ 2j. a g v .. "'

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Cvrp-J~ (hris:llaborot,.,., l ) \0 6

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.~ll'.!'er l~r ... ~c:;.$1·1 ~'t',:..O.ri!rnrJ· J ~ 2~ .,., }a!Mol'l'~~~f.!:a;y. ?I if, ;io,~:t..!:ftlib"·~~tit ... ,. "

., '6 -

HoustL'n t.abor~·ltol y IIi 9 - ·-------· ·--~-:..:::.:.:.~~-::.~~!:::~_:L ... --~----- 2 ~ 32

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~1o~Jg)~"'!Q~.r..C~t~w: •· lll .. ,., Nashville Lilbt:nii~<:ry 4 6C 35 -----r~s·r~:-. (;;qten LabV'!!lC:I j 12 IS

Pf!n>ac.ola L~tr:·,,Ho::.: 21 9-

flQ.~~~nt~l-:a~er~.:~~r~. J._ ,"'(.', ''" 4 1 ~ i" 'P;i~lsbu•1l1l'Ll!.fl'Ot\!t(;;;t ' 1 "i2 1<2- !:i • nlifr;_(~1;.:aJit:;;'d':~r.;,.n_;JI!:!b;;.~~tCI~ .! :c 1.6 8 ,

'''~~-~~~~:.~:~-?..~.~~:~~•••••w• ~86 li 1H 8 2

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Scr·.:.lfli•tth Lt~l.H.Jrato!y 1: IS

$~~~Ji~2j~~_hor<~_~_(.;(Y •. ~ 1 \.1 h

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St !.9,~;·~ (:~rt': (.;t')!) L~:)o:a!r•ty l II) 9 ,;. .

'7~ ·e ftJ ·~ Tallahassee !..2borato1y 1J 6

-~:ampa L~bora:~--- & g

W1 para ~q LabCirtHor i 6

V'/~t~-~!•Wl1lt.t!~oratory ~ ~s

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W~>11i~ldtlat:tJiatorv !,jr Ia. ~ Toni 51 10 J'" ., 409 10 362 20 142 11 4 19

CHK00000061

Accreditations and Certification

Quality Assurance TestAmerica is committed to providing the highest quality data and the best overall service available in the envir onmcnta' testing industry. To ensure that data produced and reported by TestAmerica meet the requirements of our clients and comply with the letter and spirit of municipal, state and federal regulations, we maintain a quality system that is clear, effective, well communicated and supported at all levels of the organization.

Under the supervision of the Corporate Qualrty Director, TestAmerica has instituted a cu lture of quJirty that i<> a product of its organizational design, compre-hensive training programs and industry leading systems of ( h!·cks and balances TestAmerica quality programs are governed by a corporate quality manual that defines our bus t'0S S poil ci !'s and management practices, and articulates our systems for quality control, quality assessment and q 11ality irnprovf:rnrnt It is our policy to: • Provide high quality, consistent and objective environmental testing services that meet all f .. dPrnL \I ,H t> ,1nd r r\rnrcipal

regLrlatory requirements • Generate data that are scientifically sound, legally defensible. meet project objective, dnd •• r.-· •• pprupr rJt<' io r r:wu

intended use • Build continuous improvement mechanisms into all laboratory, admrnistratrve and managN t,!l c.c tr vnr r:~

• Maintain a working environment that fosters open communication with both clr ents and st,,ff

TestAr.nerica analyzes Proficiency Test (PT) samples as required for accreditation and as outlinea I!' the ~<ational Environmental Laboratory Accreditation Conference (NELAC). Eacl) facility participates in the PT program semiannually for each area of testing and matrix (e.g. organics, inorganics, microscopy, radiological. microbiological, aqueous and drinking water) for which It is certified.

Proficiency Testing scores are a key performance rnea5ure of company petformance capability l..::;borC~tory scon2s ~:e rnonirored to ensure continuous improvement and sustained high achievement. Tt"stAmeriCiJ consi5[t:ni:ly ranks abo-,•eindustry-wide proficiency testing norms.

State & NELAP Accreditations The TestAmerica network of laboratories collectively maintains laboratory certifications. accreditations andi~)r approvals in all SO U.S. states. All TestArnerica laboratory facilities hold NELAP <Jccreditation as well. TestAnwrica is an actiV'~ n'~'rnl:>E: r

of the NELAC community, chairing a number of committees and participating in the dewiopnH·nt and irnplementatJon of the national c;tandards, now set as requirements under the program. Test/\rnerica rn;;!ntams accr editiltrons 1Ni1h sufflcient redundancy between laboratories tu enable work sharing on national, regional and local levels. Trw. inc!uc!e ~ maintdinlnq redundant method capabilities and technologies to manage large program samplt' volumes

20

CHK00000062

Federal Accreditations !esti\merica had the fir~t lilboracory to be audited and approved under the new DoD Envtronmental Laboratoiy Approval P1ograrn (EL/\Pj and now llib 11 facilities accredited under the program. TestAmf'rica has been closely involved with the DoD's devf:loprnE:nt of the new accreditation program, and has made many contnbutions that are tncluded in the new DoD Quality Systems Manual (QSM) Version 4.1. TestAmerica is also active in Department of Energy (DOE) programs \Vith multiple facilities having successfully pas~ed DOECAP audits. Additionally, TestAmenca is a participant in the USEPA Conti art Laboratory Program and has 15 facilities with membership ln the USEPA Environmental Response Laboratory Network iERLN) and Wate1 Laboratory Alliance (WLA).

See Certification Table on Page 22

Accredited to Work in Canada restArn<'Jtca s t-Ja.;hvtlle, TN C~ r1 d TestAme1 ica·s Savannah, GA laboratories are accredited in accordance with international ,tandard ISO., /0/ '' 7005 for il defined scope and meet the principles of ISO 9001:2008. These TestArnerica laboratories rn,;intain <in ISO 1 ;o~s cornp l:.;. n: scope of accreditation through tl1e internationally recognized .~ccreditation body "rm·ri<.an A•,snctdt irJ' fc: t db .>rilt'ory Ar creditat1on (A2LAJ. Based on a mutual recog1ition agreement generated by rne i"!tenattoro .~l ! abo : at :~r} rv·creditat,on Coopetation (!LAC). these Te~tArnerica laboratories have been recognized as -nC:eling t ~le tnten~< .. :~C.Jn :jl requi rEmen ts of ISO 17025:2005 and as qualified to provide environmental testing support for , ,mcJdti111 envt·onmL-'ltol n t•· r· ·sts in many Canarlt >.111 Te r ntorie~ and Provinces.

Electronic Data Te~tArneriu provides electronic data deltvcrables (EDDs) to numerous government and commercial clients. EDDs can be prc,vi(ied in rnany Test/1merica standard formats, or can be customized to meet client requirements. We currently provide EDDs in various ASO. Access. DBF and Excel spreadsheet file formats.

While offering many stand<11d formats, most EDDs are customized to meet our clients' individual requirements. some c1f which are very complex. Tesu\merica employs a technical staff that is dedicated to EDD development and client (\msultation, ensuring that electronic data provided to our clients are accurate a11d formatted to meet the clients' exacting

req u i rem en ts.

Healtn and Safety TestArnerica is committed to providing a work environment that is free of recognized environmental safety and health rnzards. it is TestAmerica policy that all work will be conducted in a manner that is safe to r.he employee, the community -"''d the environment. We believe that every employee can work without injury or unreasonable exposure to hazardous work condition~. '1'./e further believe that all work can be done in a manner that protects the environment.

Tht'' TesU\merica Environmen tal Health & Safety Director (EHSD) ensures our comm1tment to operating a safe and .:-nvi'onrr'er·tally sou no bu>tne:;, is not compromised. Under the supervision of the EHSD, each busines5 unit has il dt'Si9niited Envh·, ;rnenral H~;;,1:th & Safety Coordtnato; tEHSC), wh() is responsible for ensuring that health and safety •.>;~eJatiiH) pr>licip· Mtd p'd( l'iu's <lrP ddhHed ro dt ,.;1: levels of the operating untt they oversee.

21

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Project Experience

As the industry leading provider of environmental analytical services, comprised of 36 operating labor·atory units combining hundreds of years of experience, Test America has developed broad based exp~~ri ence in support of a multitude of environrnentai projects for public and private sector clients alike.

I , /

------·----~

Automotive • TestAmerica provides c:omprehensive analytrcal support to one of the nations largest arrtomctiv.:: manufacturers

supporting a variety of compliance programs, waste management needs and large scale remediation efforts. Projects often involve analysis of a full range of organic and inorganic parameters covering a variety o f environnwntal n·Edia to include; wastewater, groundwater, sediment, soil, concrete & waste mi.ltrices. TestAmerk:;; IOUtinely (OOrdinates specialty analytical services through a network team to address large scale and complex investigation programs.

• TestAmerica developed and deployed a mobile lab unit to a remote Midwestern destination tc assist with a 3·year PCB investigation and remediation program at a large auto manuf;;ctunng facility. Services required included the analysi~ of dozens of samples daily with confirmed data dlre the same day san.ples were delivered. Confirrnatinn ;;nrl quillity control support was provided byTestAmerica fixed base laboratories. Results produced frorn the mob1!e lab were reported following Level IV data package requirements.

Brownfields TestAmerica has provid;:d ongoing support for rhe State of Hawaii Bwwnfields program. fu·>deci L>y r eder<JI ~lriir-.t~. Supporting brownfield redevelopment efforts at a forml?r MSW lncin;:rator facility, TE:st/,mr-r~(.,1 p£,rformed analys~:~s for heavy m~?tals for a variety of invesrrgation and cleanup actions over the past five years. and rnost recently h.:Js implemented multi-incremental sample processing procedures for large (2 Kgl sampie composit(·S coupled with up· scaled (i 0 gl met<1ls digestion procedures. TestArnerica ha; provided Level IV data pack<>ges for third party validation for a! I sites Slrpported under this program. TestAmerica provides analytical support to an Eastern U.S. environmental consulting firm i1t six discreet projeCIIocation~; in support of Brownflelds site assessments and redevelopment activities. Project analytical requirements include Volatile Organic Compounds (VOC), Semi-Volatile Organic Compounds (SVOC), Pesticides, Polychlorinated Biphenyls (PCBs), Polyarornatic Hydrocarbons (PAHs), Herbicides, Total & Dissolved Metals, and ii";organic parameters. Four ofthe six sites were funded by EPA Brownsfields Pilot Project money therefore requiring hill CLP analytical protocols and data packages prepared for third part)t validation. TestAmerica provides services at a former chrome plating shop located in. California, working cooperatively with a global environmental engineering finn under a USEPA Brownfields grant. Hundreds of soil <1nd groundwater samples have been analyzed to date for VOCs, metals, and hex<lValent chromium, often requiring fmal results within 24 li<Jws o f sample receipt at the lab.

Building and Construction • TestAmerica worked cooperatively with a national environmental services company to complete a long-term project

involving a bridge expansion in the greater Philadelphia area. Critical to project S\JCcess wils our ability to me•::t demanding turnaround time requirements on a large volume of samples for a wide range of ,.r;alyses. Analyti\"ill requirements included DRO·OAM, volatile and semi-volatile organic compounds. RCRA charcKto::ristic rMrameters. sulfur. metals, herbicides, and total organic halides. Project specific communication standards v;ere dt::veloped to ensure d iem and project expectations were met and the project completed on time and on budget.

• TestAmerica has provrded extended support services for a large RCRA investigation conduc:E-d rr; <Onjunction v-nth ,; major airport expansion in Ohio. Testing demands include the analysis of subsurface samplr:~. used tr) delineate the nature and extent of site contamination. Services ;:~re also being provided to support the f..;c illty NPDES program for process and storrn water discharg~~s as well as qeneral waste characterization services.

CHK00000066

Chemical Manufacturing • TestAmcrica prov1des comprehensive analytical and logistical support for a major petrochemical corporation. Services

are p1ovided for multiple! foc:ility compliance programs to Include industrial discharge, RCRA waste chM<Jcterization, groundwater and amb .;;nr air monitori11g. Additionally, metrod development studies were also conducted to facilitate the t1ar1Sfer of responsibilities from a client operated e"'vironmentallab to TestAmeri<:a.

• TestAirErio provides analytical support for a major chem1cal company, including analyses of all environmental n ed1a for Appendix VII!. Appendix IX, TCL and TAL compounds and elemer.ts, providing OC oversight involving replicate confirmation sampling ancl analysis. Continued support is prov1ded for a CERCLA driven remediation program at acld1tiona! operating units (OUs) including analytical support for remedial investigation, feasibility study <lnd remedial ac tion steps.

• TestAm<:riGl It as worked in wnjuncrion with state and federal agenc1es to provide ongoing method development and analytical SLipport ~,,,rvices for the evaluation of PCBs 1n water, sediment and biota matrices on behalf of a major chemic'li wmpany. Several hLindred samples of varied rrauices h<lve been characterized for PCB Aroclor <lnd Homolog mixtures Hnploy!ng GC-ECU and GCiMS-SIM met! .oclology. Test America staff wo1 ked in close association with regulators ,';nd cornpJ!ly rc;)resenratives to develop techniques to provide method con;parison studies contrasting EP/\ SWS46 Merhocl 8082 a' 1d a rilOdified GC/MS Method 680 SIM technique for PCB quantification. Several hundred fi r,;·l fillet co:npos!tE~> of ,•;j i WU> fresh water species were evaluated employing both techniques during a two-yea1 lake

1;;-stl\n~E!I ;u: hi:> bePI pt:·rlor ming di.lily, lnonthly and quarterly NPDES sa;npling and analysis tor a major chemical rncinuf.:ctunng cornpa:' :r · 1n12r:ting the1r regulatory reqUirement~ for disch;1rge monitoring. Analyses include various inorg..,nic '-!I:Jiys;:·s t>n il da ily basis, 7 Jays a week, 365 days a year. Sample collection is performed by Test America staff using cornpo,ite sampl•' r;, Addition,~! monthly and quarterly testing includes Volatile Organic Compounds (VOCs), :.en,i-Volc,r!le 01gMJic Compounds (SVOCs), t'olychlorinated biphenyls (PCBs), Metals, and general chen ,is try.

Consumer Goods • TestAmerica provides sampling and analytical services to a major fragrance manufacturer supporting the company's

compliance monitoring program. D<lily, monthly and quarterly NPDES discharge samples are collected and analyzed for 0ach of three fJcilitie:;, one of wh1ch also requires semi-annual ground water sampling and analy$is. All field sampling and analyses are performed in accordance wiih applicable state guidelines. A wide range of organic and inorganic constituents are routinely monitored, including several program specific compounds performed by the lab ~;pecificoliy to meet the rt:quir~n 1~nts of this client.

• Testf,r:lerica perforrns sarnpiing aPd analysis services for a major food, home care, and personal products manufacturer. TestAJC1erica field technicians complete numerous client requirements on-site, which include preparation of maintenanu:: field lo~JS <!lld ~;arnpling field logs for multiple locations. On-site field support is required daily, 365 days a year. SummMy data and activity reports are compiled and submitted monthly and submitted electronically. Additionally. Test!\merica prepares industrial Self-Monitoring Reports (SMR) for submittal to the iocai sanitary district .:~nd prepares NPOES required Monthly Monitoring Reports (MMR) for submittal to the state agency.

• TestArr:erica, i1 support oi ~,nonprofit applied science and technology development company. performs analysis ot air particulates. wate1, soilisedirnent, milk, wine, vegetation, lichen, wildlife, vegetables and silica gel for the following i:;otopE·5: Americium, C <\I bon. Curium, Gamma Isotopes, Gross Alpha, Gross Beta, iodine, Plutonium, Radium, Strontium, T"•dnetiurn, Thcmum. Tritium and Uranium (Isotopic and Total).

25

CHK00000067

Project Experience

Department of Defense (DoD) • TestAmerica has provided continued support to an international environmental and engirH" (•ri;~g fi11n in support

of their efforts at th~! Massachusetts Military Reserve, a very high profile Department of Dt:f;>nse p!Oject !oration. Currently in the third phase of project execution, TestAmerica provides rapid turnarouncl an ·,lym for ar. ongoing groundwater project. Select drilling process samples are analyzed and reported on a 2·1-hour TAT bam allowing fc1 continuous, uninterrupted field drilling activities. TestAmerica developed a modification to EPA rnethod B330 to address a need for lower soil reporting limits, allowing for the quantification of trace levels of explosive residue ten times lower than standard method protocols.

• Test America continues to support an international consulting!engineering firm at a numbe1 of Federal Depa! trnent of Defense sites throLrghout the country. Support is provided for soil, sediment, water, and wa,t-:: samp!.:s. Analy~es me perforn ed following the DOD QSM or the AFCEE QAPP, dependin~1 on the site. Leve! IV d.:~ta packages, ready- for third party validation, are provided along with the appropriate electronic data de!iverabl.:~s (ERPIMS or ERiS).

• Test America provides support t:o a global consulting engineering fnm i·or RFI ard risk asses~rT;ent efforts c;nducted at Altus AFB. AFCEE 3.0 protocols are followed and modified for Appendix IX analytes. Pri;mry :,c~rnplr.s ore i.;nalyzed for volatiles. semi-volatiles, and metals. Periodically S\1rnples are analyzed for pesticides, ~'xp! o r. r ·,.,.,,, aninns, di<;5<'!vecl gases, radiochemistry parameters and dioxins. /\11 cleliverables are provido::d as fullr<tv; dilt.:; p.':,rk.'lg>?s in both !v"d copy and CD-ROM formats. EDDs are submitted in AFCEE's ERPIMS 4.0 format.

• TestAmerica provides full .. service lz•boriltory SLrpport to a Departrnent of Defense installi1t i·;n c(;ndunrnq ;,,.,,,dyw:; ;-, ,l Volatile Organic Compounds (VOCsl, PAHs, PCBs, pesticide~. hydrazine, NOMA, and a vari "tY ,)f metals ancl i no:~Janic

parameters in soil and water samples employing SW-846 methods and following AFCEE 3. i pr•) tocol. Data de!IVEJ<ibies include long-form raw data and a customized electronic deliverable. Under this project. TestAmuica has providd research and development support tor rhe analysis of hydrazine to ensure compliance wi th :;tate requi1ernents.

• TestAmerica has provided analytical support to multiple environmental engineering f1rms managing projects at a Midwest located Department of Defense Army Ammunition Arsenal for the past 12 years. Work w<lS performed following the Arrny Shell document. and subsequently graduated to Corp District specific guidelines. Test.A.rneric~ worked closely with USACE to support the development of this unique program, including providing R,<',D work to develop soil grinding techniques used in multi-incremental .sample processing_ Analytical support to date has irwolved full TCL!fAL Organic and Inorganic parameters, various general chemistry analyses and TCI..P analyst~s as well as explosive and energetic compounds. Report deliverables include level IV data package and c!il?nt specific electronic data files.

• TestAmerica works as a subcontractor to a USACEtHTRW prime contractor, providing 5Lrpport for semi-annual groundwater sampling events conducted at various operational units within Fort Wainwri9ht. 1\l\ and other military sites. Groundwater and soil samples are analyzed for GRO, DRO, RRO, VOCs, SVOCs, PAH SIM. Pesticides, PCBs and Metals and wet chemistry methods. All work is performed in accordance with the DOD QSM with full COE prescribed data packages including EDF and SEDD electronic deliverables.

• TesiAmerica provides routine support to a USACE district office conducting chemical and ra.(jiochernical analyse-s on a variety of sample types tor a noted FUSRAP site. Often, samples resLrlt from emergency r~: !; pr.' J l>'e r.:dateci acuvitie:; <md require rapid turnaround time support for the Hazardous. Toxic, and Radioactive Waste tHTRv\' l progr<mL

26

CHK00000068

Department of Energy (DoE) • TestArnenca participate:< in rnany stlldies conducted in and around Department of Energy plants located in Oak Ridge,

TN and 1\-tn< .. J> ( ity. /1.' 0. r .. oncern:> over PCB levels contained in native fish tissues have resulted in the estilblishment ()f ·;t>wrdl :w:"w:l •l0r ll ) ~ ; \l•.ldies. TestArnerica began supporting the projE-cts curing the 2006 monitorrng event ;wa!y2 i'• ·J 1nn: ,. 1 i il l'• iOf.l fiSh and clams over the I<Jst th1ee years for PCB a roc lor~ by SW 8082 and for PCB congeners by 166<lA. D·-,gonf! ~s ;;;•: r" al;o analyzed for PCB congeners by 1668;\.

• T·,·~tf,rn ···r ir J lid ~ •, u ppo1I P~ l ongoing efforts at the Savannah River Site i.SRS). providing analytical services for chemical, p!Jy,ic.;i ond 1 adi,xh - ); ic;JI analyses on a variety of different m<Jtrices including soil, sediment, sludge. groundwater, ~urf,Ke ,,,,1ter. v • .;~te rl tiltr:Cb and building materials such as wood, concrete, metals. and painted materials as t equ1red. All <Jilalyst·s <:rc perfonYh?d under strict adherence to the DOE Quality Systems for Analytical Services (QSAS! Version 2.4.

• T~stAnwri .::a per forms anJiysis of urine and fecal tissue for routine and rapid turnaround times to support a large scale pPrsonnel e,;posure rnonitori ng program. Analysis is conducted for the following isotopes: Amenciun,, Plutonium, Strontii.m1. Thorrum, Tritium <md Uranium (Isotopic). In support of this program, T<~stAmerica Slrpp!ies a contract speci'iz UJS\(lmized clat,1 report and EDD format.

Emergency Response • TestArn?rica. re;Hning with a major environmental engineering firm, successfully responded to an off-hours spill at a

l0ad:n9 tele;ornn)Jn•cations provider. The coordinated effort rnvolved the receip: and processing of a large number of sarrples on a Friday afternoon of a holiday weekend. Results were fLrrnished immediately upon completion allowing the resoonse tE·am to initial~~ a remedy the very next morning.

• The TestAmenca network of laboratories collaborated to support emergency level support effort for an impacted river and aqUtfe1 caused by tl e iKCidental release of lly ash slud9e. TestAmerica led the effort to supply high-quality data to id-:mify and define tht: physical and chemical characteristics of fly ash, soils, groundwater, surface water, sediment, drinking watel, biota. and rnacro invertebrates in support of the recovery effort. Data was used for characterization and for assessing the degree of remediation achieved, as well as potential litigation.

• k~tArne.-ic.<J provided <!11il:ytiCill support for an emergency respon~e effort resulting from a fire at a Midwest chemical rnan. fa' tut inc fC~cil t ty. Work includf:d accelerated turnaround of a high volume of soil and water samples analyzed for rnetals. ::rqinoiC <Hod w r:t chemistry pararnett'rs. Po~t emergency response work continued with waste classification <n.:ily ~.,·~· r!' qu•red fo; ~·;,) :, ;,~ disposal and soil, groundwater and drinking w.'lter ;malyses condl•cted to assess residua: envrronmenr~l imp;;cts <ls soci~~ted with the chemical f1re . Test America continues to provide long-term monitoring suppc·rt to the site.

27

CHK00000069

Project Experience

International • Through facilities in Southeast Asia, TestAmenca provides support for multipie multination<J! oil compdnie~, with

monitorinq projects asso<:iated with rhe operation of offshor~ oil platforms. Sampl·;;> matnces incluci<e seawater. sed1rnents, and biota for the determination of PAHs, particle size, metals and TPH at chalh:nninq low reporting lirnit '· Testf>.merica also p1ovides technicians for onboard sample extraction a1.d analysis.

• TestAmenca prov1des analytical services and field support for interna•.ional consulting firms r t);Hiuct;ng Piii•~:c II site 1nvest1gat1ons and underground stor,1ge tank projects in several Asian countries. Dat.r ,JI E;· ~'rucluccri to !1'2-('r USEPA, international and country-specific technical and defensibility criteria. Te>tAn.erici' ;~,~;,~,;~.by providinq pr,1je:r management, coordtnating international sample shipments and fur: lishing technical suppc>rt UJV!::'rii11J muitip!t; cottrltr l e~, includ1ng very remote project locations.

• TestArnenca has prov1ded lab support to the investigation and remediation of a large clo~c::d c•xp!oration and prodLICtion tract in South America for an international oil and gas corporation. An in-country lab was e';tablished to facilitate quick turnaround timE' requirements and assist with sample logistics for samples bf:ing returned to the United States. Lab support includE'd full range organics with metals analyses along with Le::veiiV deliverable>.

• TestAmenca provide5 support to an international environmental consulting company, <ma!yzing sampies from vadous site assessments, investigations and monitoring programs conducted at retail gas stations. terminals and refmeries located th1oughout Latin Anterica, South America and the Caribbean. Analyses of sedirm:n!, ',oil and ('_FOund~vatH typically include Petroleum Hydrocarbons, Pi\Hs, BTEX/t~rHBE/Ethanol, metals and variou:; inon~anic ana!yses. TestAmenca coordinates international shipments of samples and sampling supplies to and from the field addr,'::-SIIl9" variety of country specific requirements and restrictions.

Mining • TestAmerica has been providing analytical services in support of a !arge remediation project ,:;t a mining site in

Southern Nevada. /',full range of analytical tests are provided to include: Appendix IX 8260 and 8270, met3!s, hexavalent chromiLitn, pesticides and PCBs, cyanide, full wet chemistry ana!ysis, '1625( for NDi'AA, low level 1 A-dioxane, PCBSA, j.Jerchlorate and radiocht:'mistry analyses. TestAmerica·s service center in Las Vegas hilS been used to St<l9•"

sampling equipment and provide courier service to facilitate moving large sample volume <melt ime sensitive Silmples.

28

CHK00000070

Oil & Gas Refining & Marketing • T"stAmeri<:<l prepared anc1 deployed a mobile lab facility to support the excavation and removal of a retired pipeline

in Dutch Harbor. The mobile !aboratory oblained full certification by Alaska DEC. This project called for the analysis of hundreds of environmental samples under 24 hour turnaround conditions. Results were provided on time routinely following project specific 1equirernents for electronic data transfer.

• TestAnwrica has conducted an ;;;rnbient air monitoring program to a consortium of petrochemical refineries in the Gulf Co.':>t re9ion for mon' th<;n 20 yE!cHS. Thi~ ongoing project involves analysis by T0-15 (GC/MS) of more than 160 organic compounds in a single <>nalytical run with part per trillion (PPT) reporting limits.

• TestAmerica provides research and development services in support of proprietary prodliCt identification projects for co1npani,:?s in the petroleum industry. The laboratory works with clients to help establish effective test methodology for the identification of unique organic compounds. Addressing these analytical challenges often requires modification to routine preparatory and analytical methods resulting in a CLIStomized approach to p1ocluct identification.

• TestArnericil has been ;)ssisting a major petrochemical retir:ery for several years with their compliance monitoring and f azardous waste clilSSifc,)\'ion programs. Analytical testing involves a wide range of wet chemistry analysis and TCLP fc both OI<}JnJc ard i:-,,:;rgM1ic col ~tituent:s on a variety of chollengi'lg n1atrices coverin9 over 100 sarnples per month.

• res1An•·-~ri<.,l ·, !Jh.: sole cc:11: acted lab supporting systen, monitoring samples at a large former oil terminal pipeline ce::.ciuctlll<:J facility •\:nkd!;ltiun. The analytical support for this p:oject requires tl:e <tnalysis of over 300 sampl<:s : :w·1thly for V:JC + I' H .:c·~npounr.i>. To rneet customer specific n'!eds for this project, TestArnericd invested in ;,pec•alizc:d ~<H11pllng rncd,.;, Jl1d \.jel!v,~rs a customized data <ieliver,'lbie.

Power Utilities • TestArncrica provides cna:ysE:s of soil, groundwater and bl:ilding debris, working cooperatively with a national

c::>r:sulting enqineer in91inn to support the decommissioning of a major nuclear power facility. TestArnerica maintains ~~RC materials handling licenses and provides for the safe handling of ali samples taken during the decommissioning Dr<Ke!;s. Sarnplf:~ are analyzed for Volatile Organic Compounds (VOCs), Semi-Volatile Organic Compotmds (SVOCs), Pesticides Jnd Polychlorinated Biphenyis (PCBs). Metals and Wet Chemistry parameters.

• T''>tAmerica contmues to offer support to a global environmental consulting firm conducting investigation artd ;ernedi<Jtion of land contr:minated with by-proclliCts from manufactllred gas plant operations. Testi\merica prov1clc'S clnalytical <;ervices that include the analysis of Volatile Organic CompoLmds (VOCs), Polycyclic Aromatic '-lydrocar bon~ (PAHsi il5 well a;; total particulates and metals in air samples using NIOSH methods: NIOSH 150 I, NIOSH SS06. hiCSH 0500 anc: NIOSH 7300. Data provided is used to support risk assessments for a nearby residential area.

• Te>tArnerica provides support to a major Te)(as based power company for their transformer mainren<Jnce and spill remedidtion firograms. Daily support requires routine analysis of a large number of transformer oil samples for PCBs to ensure compliance witL EP,~ requ!ations and to address clean-up of contaminated sites.

• Tesli\rnerica provides analytical services for groundwater compliance monitoring at multiple locations for a large c:;nergy co·Ppany with opcr,,tions th1oughout New Jersey. Sites range from active, operating substations to closed manufactured ~Ja'' plant (M(jP) facililies. Site-specific analytical pro9rarns encompass testin9 for organic. inor~j(mic, general chemist1y, biolcgic<JI. and monitored natural attenuation parameters. TestAmerica field service teams provide low-fiow 9ro:.r)d'1'JiltN •,.'Hnpie collection services in accordance with NJDEP Fie!d Sampling protocols following client spe-cific ~~ire saft~ty p1 oturoh.

• -~est.i\! :H~rica Dl cwide~ ''' •alytical support on a large remediation effort for a large energy wmpany located in the sr;uthe<,,tern United St;;t(;'c. This project 1equires d~.;ily sample delivery to the lab, encompassing a 2-3 year project life cyde. ,<\!! ~.;mp!e~; <Jk an:.;lyz(~·:l for a variety of rnetals and inorganic parameters on an accelerated turnaround basis so that or::pin9 di~posal ;,ncJt;eatrn•::nt dec:isions can be rnade. minirn1zing costly project interruptions. Client specific Qf!.. j)roto<:oi~ have b~~en esu;t:listK'd to meet data usability requirements and ail data is provided in a Level IV data package. Customized rnuhi-flie EQUIS deliverables are included with the delivery of each data set. Total number of samples exct?eds SOD per month on average.

29

CHK00000071

Project Experience

Steel & Primary Meta~s • TestAmerica provides support to a multi-national steel making organization on an environ1nentai dredging proji'ct

involving PCB contamination. During the height of the project. dredging operations were cvnducted 24 hours per day, 6 days per week. An ambient air monitoring program was conducted during dredging act1vit1Ps to d'-SUrE' that the nearby residents and workers were not exposed to fugitive air contaminants that could adw:rsely ilffe<.t humiln health. Test America analyzed more than 700 samples for PCB Aroclors using method TO 41\, i AH> by 10·13!\ <md volatiles byT0-14/T0-15. All samples were done on a fast turnaround time basis. Monltorinq for volatdf.s by r0-15 remains ongoing.

• TestAmerica has performed compliance analytical services for the world's leading beverage ::;,~n mJker c1t ·11 location~ nationwide since 1990. Through centralized project coordination, TestAmerica employs its m::twor~ of l;;borata; 1es to

meet rhis client's national testing demands. The laboratories analyze compliance samples (1f"l ''monthly bas1s as well as perform waste characterization services. Slim mary data packages for submittal to the faciliti<'s' local agpncir-s.

Sediment Management • Test America, in support of private industry, provides analytical support for a river S('dim(,;nt 1nvPS':19athn in easte1 n

New York. The river has been the subject of a major investi~~ation and remediation effort ;:l!Jr:lre•;sinq Pr;lychiorin;l!r,-d Biphenyl (PCB) contamination. TestAmerica continues to provide support to a Fortune 500 cnn'nany Pr!\J<!g>?d 1n remedial action for contaminated sediments playing a significant role by performing apprc·xim<:tely 20.000 analyses to date for PCBs in sediment. Samples are analyled using a modification to traditionzll rnr::u·o<ioloqy to ilddrcss site-specific and matrix concerns resulting in high quality data used to make critical decis ;on~ thrCllghout tiH' remediation process.

30

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State Government • Tr:stAmerica, 1n ~upport of the State of New York, Department of Environmental Conservatio11 !DEC), receives samples

from dll \ YSDEC region:; t() dddress the analytical requirements of remedial investigations, discharge evaluations, spill respon:,P> and :;• ate Supe1 fund activ1ties. TestAmerica performs a!l analyses adhering to the NYS Analytical Services Protocol (ASP!. which n)imics EPA ClP Methods. Sample matrices include wastes, soils, drinking waters, groundwaters, sediments. discharge s-)rnples and air. This contract requires strict adherence to the required methodologies resulting in high qu;,lity. legally ddensible data for the State of New York.

• T<:stAmerica maintain:; ,,n<ilytical support contracts with each of three major engineering firms holding primary c;Jntrc:cts with the Illinois St<Jte Department ofTransportaticn. in this capacityTestAmerie<:1 performs a broad range of ar:a!yses for statewide ''ssessments and investigations. In over 10 years of Sllpport provided under this program, To:?s,Ameri~" hi:!s uniquely positioned it~elf to addre5s the program·s custom requir('rr ent·~.

• Test.h.mr.:r:~a ·,the prim.::rr laboratory supporting development of the Hawaii Department of ~ealth Technical Cu!d<HKC ;\:L;r:u;d (TCMi 1<: >~ ~.Fnpl1ng and risk assessmer1t. Support indudes application of drc1ft TGM procedures to d.:t,~rrn:n:e "ff1c.:1<"Y ;,t SE'kn<:cl sites o·.ter the past two years. One site in this effort consisted of a former agricultur<•l .:.Jtc)pc:rty d :.1rT:I1l<.H!? island lo( . .:lli<.m that requ!1ed testing fell Or9an0chlorine Pesticides. Organochlorine Herbicide~. ·; ;·i;!zint':'. c,rb.-HlirHh. t·h·:~;,ls. WCJC'. end Dioxin~ as a prerr~quisitc~ for a housing development. TestAmerica provid('d ~cl:;tion<; to hr·lp rt!solvc; probh•n,atiC sample tran:;port logistics from the site. In addition, TestAmerica developed and applied the~ first· ever ~upE:r-scaled (5 Kg) multi-inc: em ental sam pi·: processing application fer a number of the tested pararreters, conduclirl9 l(.·i.Khabihty stud1es on a!l positive samples, and pioneering commercial lab implementation of :he Huby-:Jre•ler s<~mp!e preparation technique to determine the 'bioaccessible' component of detected arsenic roncentrations.

• TestAm~rio is the primary laboratory supporting an ambient air monitoring project within residential dwellings. This ambient air program is under the cohtrol of a state government agency and is highly visible within the public domain. Test.America has d<!dic,1ted approximately 180 summa canisters and 130 flow controllers exclusively for use by this clirmt. C.:mistNs are suppiir~d to the client on a weekly basis. batch screened for both SIM and SCAN modes of EPA Method TO- i 5, rn~1in:aining a seamless cycle of appropriate sampling media to the field for systematic project cxecuuon.

• Te>tA.rnerica worked V·.'ith trle Florida Department of Environmental Protection (FDEP) to v,1liclate analytical techniques us~'d fo1 the identifie<nion of., ,4-diox<Jne following 8260SIM methodology. TestAmerica was the first laboratory in Horid<1 certified for ;Jrnlysis of 1 ,4-dioxane by 8260SIM.

• Testl\rnerica hJs proiif~rat:~d irs analy!"ical capabilities to expand its-test offerings specific to the evaluation of He~<W<llent Chromium in <~nvironmental samples. TestAmerica currently serves as the lead lab for an extensiw: NJLJEP project .:;ddres,in~J the ev<JiU<•tion of background chromium corKentrations in urban soils. Processing thousands of samples for state driver· prograrns, the laboratory not only complies with the diffrcult Ne·.v Jersey data validation £1uidelines but also pr~rforms other non-routin~' procedures. SliCh as the Japanese Slab Cakt.> method.

31

CHK00000073

Project Experience

Transportation • TestAmerica has provided ongoing environmental testing services for a major transportation company sine<'., e.g; wi1h

sites located throughout the eastern US. A variety of mat rice~ have beeh evc11uated for environmc~ntal rompl ·ar-.ce which rnclude water, soil, waste. complex organic n at rices, and air. Routine analytical suvices in<.iuc\e the restrng of various matrices for volatile organics, semrvolatile organ res, metals and •.vet chemistry paemelH~ for gwundw-1~ <:' :

and surface water monitoring, and waste evaluation programs. Special methodology hds bE:cn deve!op•:cl w mePt unique regulatory compliance cor cerns, ensuring that minimum reporting levels are achic'vcc: ck·sp:u:· complex rnatri;.. interferences. Data deliverables are customized to m~et regLrlatory and dar a management '''~'-'ciS.

• TestAmerica currently supports a comprehensive remediation effort for a 240-acre rail yarci working in wr r,iunctior with a major consulting engineering firm. High sample volumes and quick turnaround are required to n;onitor ti1<:' ext~;nt of impacted groundwater, groundwater treatment: effectiveness, soil remediation effectivenes:, and to keep stockpiic'; moving. Over 700,000 cubic yards of soil has been excavated to elate. Samples are analyzed for 8260, 8270. BO 15. Metals, STLC and TCLP parameters. Customized qu<;lity assurance pl<ms were developed to address chalienging matrix and site conditions. Data reports and electronic deliverables were also w~tornized to adclress client specific nf:?eds.

Waste Management • TestAmeri(a holds a national contract with a national waste management firm to provide .sampling and anuiytical

~ervices throughout the United States. TestAmerica conducts a wide range of environmental a:;alvscs for S•.:V~'r d!

hundred sol id waste landfills under this agreement. assisting the client with meeting <heir rpgulatory complrz,nce requirements. In addition, at selected locations OSHA trained field personnel are provided to collt::ct groundwater, surface water and leachate samples. TestAmerica provides au~omated sample scl:eduling services, site spedic sample kits, long term data management and client specific data handling supporting a wide variety of reporting formats.

• TestAmerica maintains a unique support arrangement with a Midwest area industrial wa~;te 1ecycling facility providing ;,vast(! screening and characterization services as well as process related testing. TestAmerrca services .ore uniquely designed to ensure the efficient daily operation of the facility and uninterrupted service to fadrty clients.

Water Treatment • TestAmerica supports an international environmental and natmal resource management firm with water quality

monitoring for a large scale TMDL program. 1\nalytical services designed to meE>t specific f'Mf';_ requ~rernenb are provided at varioL,s water bodies thwughout the Southeastern United States. Analysrs con clunf~d in:.ludc: ;(,.-, .. levl' i or tho and total phosphorus, TKN, nitrates, coliform. alkalinity, TDS, TSS, color, turbrdity, chlorophyll A. •ln;on; .;nd metals.

• TestArnerica is the primary laboratory supporting a large .. scale drinking water progra m for a n"1jor Cali for nra utility company. Required analyses fall under EPA Title 22 regulations, many of which are (Ond•.r <:ted under 24·-hour turnaround conditions. TestAmerica orchestrates a statewide sample transport system picking up sarrples at varrous locations in the state and delivering them to the lab within time to address sl·ort hold-time parameters. Project sp<:cinc communication standards have been developed to immediately notify the client for any positive results, including weekends and holidays. Five different report types are needed as dictated by project specific requrr£:rnen·~.

• TestAmerica provided analytical support for a wastewater treatment plant pilot study in south Florida. This study was designed to evaluate treatment of reuse water as a potential source used to recharge local aquifers currently used to provide community drinking water. Samples were collected daily, weekly and monthly with over 1500 samples bein~J studied. Analytical requirements included full list organic and inorganic analyses utilizing wastewatr-r. potable water and pharmaceutical and personal.care products (PPCP) methodologies.

CHK00000074

···"""

TestAmerica Products & Services Businesses

i

TcstArnerica afflliates includ€ EML.ab P&K, the leader in analytical microscopy and indoor <ur quality testing; QED Erwironrnenlill Systems, lm. t!w leading supplier of groundwater san1plrng r~quipment and remediation pumping

syswrm: Test/\merica [)rillin() Corp., provider of innovative environmental and geotechnical drilling, anctTestArnerica Air Ernisc:ir:-ns Corp. (rviETCO tnvi·onmental), specializi11g in <~ir emissions testing.

\

'"···----· -~-------···-·-

EMLab P&K is the le,1ding indoor air qucolity (!AQ) testing laboratory in North

!•.me rica, specializing in lab analysis oi' air and surface samples for mold. fungr, bacteria, asbestos <111d a!!ergens with more accredited locations and Jndlysts than any other l~1b in tiw nation. Em lab P&K is committed to providrng out~tanding "er vic(~. quality' and support to industrial hvy1enrsts, idbcratorres, st<Jte .::nd local pLrblic health departments. t'osprtills and il\0 professron:;;t:;.

QED Environmental Systems, Inc. h t'l'lt'~ kadrnsJ rntern<~trona! ::upplier of air-powered purnping systems for gr C>undwater sampling, groundvvater remediation and landfill liquids. OED cle:veloped products include:

· :V.icroPurge low-flow groundwater sampling equipment

· AllloPump· re"nediation o>nd landfi!l air-powered pumps for use in severe conditions of sol'ds solv;::nts, corrosives and high temperatures

·Genre· systems selectively pump floating layers of hydrocarbon • E-Z Tr:~y' air strippers remove VOC's frorn groundwater and wa~te water

-·--·----·-- ----------_..,

J

33

CHK00000075

TestAmerica Products & Services Businesses

TestAmerica Drilling Corp. is a leading drilling contractor in the western United States. specializing in environmental, geotechnical. and infrastru<:ture subsurface investigations. Their innovations mclude the indusrry·s first der.or"ltarnination trailer, Umired <~ccess drill rigs and vvell surface completion toolings. TestAmerica Drilling is widely recognized for its ability. to deliver your project on·time and on·budget.

METCO Environmental is a leader 111 source emis:,ions testing, serving a full spectrum of industries mcluding, refining, petrochemical, combustion and utiliti~s. both in the U.S. and inte1nationally. i'v1ETCO has built a reputation for exacting sampling methods and rigorous quality control, based on having sampled over 25,000 sources. METCO is staffed by highly qualified and train~d full-t ime professional employees who maintain the highest ~arety standards in the industry.

CHK00000076

I

~ l '

Notes: - - .. -- -------------.....

35

CHK00000077

CHK00000078

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lo t~)is icp,lrt. lf: ... •\JI.iiV<.: ;11~~ '-fu::;liHJL rdrtting ''' tl.is ~n:il} rical rcpiJ!1, plccsc c<•nlllct ~om Labor.H,·lr~ Pnl!c;.·· '.:.:,!,;t- t : ,;:

1·800·765·04.}80. AI~) -.) pi nu..)n$. ife~.preS>I!d . <Jrt: L\tJtside !he SC't.ip!.! ofth(· L nburalur; ·s ~t<..:cr<:d!~;l(i~m.

This materi:tl is inccndcJ only tt;r !he ust cf the ln<ll\'idual{$) or tntit~ to whom lt is :\.:h.tn.~~x:d. w; .i ill.t: ~.·.•nt:tin mli.oHn~!i·~r: !lu; ! . .; privileged aud ~onri ... l'.!nual. If you ar~ no1 th~ intended recJp ;c,.t, or the empkl)\!t: or :tgent respl'il~ib:t; l~;r \!\:\;\ cn :1g !hi~ m:nc·inl h l tl:::

int~-.nfo.ied r~ci;Jil!nt. .'Ou ~re hcrCh) n•.;rilied 1l1.1t an~ d!~s~minatitm. distributi~.>n. or (;Opyin~ iJI' this m:lt.:m·.! l~ :"o\n~ll) rrl)!llh!r~J If :"u ha,·e re(ct~.ted this mncarial ir· en\1r, pie::.~.: 11otit~ us irnmed ta tcJy ur 615· 726 .. {\ 17?,

CHK00000079

Test America THE LEADER IN E.NVfRONMENT.6,L TESTING

Work Order : f'l1cm: Chcsap.ea~e l:.;1-erg: Co;po:-ntk)JJ

6 !OG l'\ \\'<:t;tern t\ -.-cmt~ Ot::lahoma C1ty. (.lK 7311R

Pr~JC:C:t i'iamf. th:S:.tpc\:kt Shok l'r'ujec< · l'A ~nti flro_i<'Ct :-Juml'<!t. 4100SIOiO I

12102!08 08:30

At.lditionnl Laboraror:, Ct>tnm~ttt;.; This is a 'omplc-tc fuwl report. Th~ sub.:onrra~t~d pnmmel~rs are li;;ted h~low i.lnd c.tr5! attache,i to 1he ~nJ of this r\!pon.

~il <;ubCt11tlr,u.: r\!'d \in:a t!' artr1d ;<.:~i ;JI thL"I.!nd nt" th\: ·l\!l~h\·illt R,cpot1. P.:: r cih..'tlt rcq~1cs r. the Ra2"26 anli Ra2?S 'TotJi Rmiiun .j ti t." I~ ,i> w;r < ' "'''"''·d I<> Gamma Sp~c Analysis b~ lvl.etllod 90 I IM due .to-sample ma,ri:x .:tH!l}~k\il it.·~ tlm.t pre\ "~meJ thl" nr.st ;J~aly~ is trom proper <.:Umplctiun Thcrefbr\!. the Gammel Spe.: \\.HI he icpr)rt<:l! in \h !-- n:pvrt in li .... tt v ft! u..: ll.1tal R\u.Jiutn. ~() funht:( c..haJlge; ... ~.ere mad~

All samples t.rTh ed in good ccndil iqri and "ithin tcmp.:r.itui~ nllownnce. The pH tested at sampk r~ceipt for the Cyanide c\llltain<-rs was pll - I 0. Thi$ was likely contributed to the comple)( ity of-the saniple matrix und its eft\;cls on the a~id prescr; :nion in lite f:rot!le. Client rcquesr~d we proceed with analysis as recci"-ed.

The rnutrix .~r t l;~ ~amr.k a•··ol) ; cd required the usc (If both prep and analytical diltrtions in ,·arious tcs:; to £h.'Cl)ll1modute ihe krHI\\ 11 ~.:~mpk mn{nx ertCcts that hn\·e bce.n seeu with this project Th::~e matrix efl'ecls ha\'e ctlu;-;~d soiue te -; t~ h) :-cpon \\ 11h dcvat~ci detet1ion limits due to th~sc interference~ in I he anoiylicalmclhnds hy the ~;m.plc.' Ct' il! Pk'il~ TIF,; ~,_~ ~~su:t~ <H;t' n,,ted m the rc:porl with ''RJ..l'' quatificr~ indiculing lO\\CC diltllt.'d ;md undiluted nm~ Oil th i~ aml 1 ~-~ ~ :- ".·.ere nN fe;.tjiblc due! to method OC Clln:-otraint~ .

Specific Cnnduct:m~~ is I~p\)cttd "· ith an "E" , -~lue slighrl:· o,·er the up;xr lin,•nr range . lite highest second scrur~~ staaJwd that can 1'1<! purchtiscd and m;ed in this data set was m I 01),(100 umho.'cm thcrelly esr:ibiishing the :rpper lit' ear r~n:;:c of the instro:ment l>y our normal SOP t\.1r the Itlethod. At th~ rtquest of the cli~nl. an in.-housc standard ,.,.d, prcjlared rHtd a:l.11yzed r;n the inslrumer]t probe sho1•ing lin¢ariJy ot'lhc instnnnent wi1hin nonnnl acc.:ph1l>lc QC ranges 10 250.000 umhoicm. Thcrefore.the linearity of the insrrument was considered \'alid to this higher rang": lt,1\\CI cr. any \'Oit.e abO\'C tl;c 100.000 umhoicm WflS noted wiih Rh "E" qualifier Jli the report a; per the method SOP rc~ommendations . .

l'•uc ;o the s:unplc «'tnplc~ily ;,sues. the empirical relationship b~twcen ihe Specirk conducti,·ity nnd TDS ,·a\u;: ttta~ II<)( agree. This \\Ould lih:ly t~~ due lu ih;• amount of soluble organics andfO< anr separate\! out oils r~pr~SC'llte<.l in the I'D$ ,·abc that ltla)' ttlll be renected .in 'tho! Specific Condu•·tnnc~ analys}s. Tlrt:'· us~ of smaller romplc aliq~r,us wa~ use,l in ;l ;:l'ordanc~ to the me tho~ when possible to· help minimize th" ~mple ~:ornplexity

--i~~ucs and imprt.l\'e the empir;cal 1 ar·iance~ in thc$C.-IC$[!..

·n ,e T[)~ 1·alu~ i;. 1\o!d "ith an • •\;0 I" qua litter. llri: ddinitioil <tfth.is sp~cial notation is locut~d in .th~ sumple qualifier definition p:tg;e at the end 0f the rep<>rt.

In comparist>n of T otal and Drss<JI\ccd metal ekm(nts some of the metals resuits Jrll'cr. Tl:is is likely attributed ltJ

the s~mple nwtrix complex it~ that i;; causing the total rec(weries to be less thn:r the diss,,h•ed rcco,·cries. The lxtttlts were dtc.:ked t<i m:rkc sure the) \\'tn: labeled corr~ctl~·. Tl,cr<: wer~ no \'isible signs not~d by the an•lysts during. the tem t!.:l! i:ldr~a!~d ~ pt<'Jll!l' digest ion and analysis didn't occur. so t!te dam was acce11icri as 1\:fXlrr~d .

fhc- It ; ... alcnl Cnmmmm r<:!>uh ~ :Ht! reporting lWi~ due-lOa c~nnputcr ~~- ~t1:m erfl..\ r. The do!tcctit)n lint it of I 000 111g..-l i-..th \ ;due ihat _o:.!h: uJhl !·.: u s ~d fi,r;:,n:uati \C purp<;:;.~s. The 1(10 m~1. Jett><':iou limit should :tol be u~;;·O fpr ;\.p\Jr:ing jHI~~~c> l., ~.:' '

CHK00000080

L 1,,·111 Cht·~~r,·nk~ rn-.:-rg:• C.Hf .... lrJ!I\i/ 1

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li•)(J)<I0701

f'lrnpLw . and Kcpon~ \\CIC hia-> ... "d IO\\ in th~ t\prertdi\ 1'\ Sen· ivi)I:HIIe ;un!~ ~~~ . 'J h~)e comp"'llnd:' arc considcr.::-d n po\u p~ni-.rrr.c; b:. the mc-lhnd due \o rcncllrity c,l' the comr«.'und. Sunt«! ,,fthl! s~· \\l!'r~ IHtl dct ... ·~.: l:.:d 111

the Hhmk Spik~ a( un~ rcco, c r:. hut due tv th\! nuturc ~.t these t:ompc,un~ls ond its r{'acti\ity to the C\traction

prot:\!':-:-. th.: ~ample ''u ~ HCJt re·cxlnKt":l tOr rcanal:·;iis. The Jaw ''a.~ aCl'eJ>l<d a:. qu l liiicd foi til:s \.:tJI\1pn1u:U. I\ is nvt~d " 'rth :u "L2'" quu!i ficr in the rep<>n.

Some o:omp,•unds 11crc biased hogh i1\ tl:~ Blad: Spike recovcliC'>. lhe snrnplc res,tlt:; t\1r these nms \\er, :dl non~dctect ctnd not~J in th~ t~pcrt \dth :m •·t.·· qu:\t.ficL The d~un \\::1!; tlO\ ailCctcd ~o n(l fltrtht!r r.ctit) ll wils t:.1ken

Til~ Rro:nide rccoW>) in the asst>ciarcd Q( was r~panec :~s n~ccpt~hl~ \\"I thin the rcco' cry rJrg:c ,,1.80-120 "• ir . ~lea<l <l fth~ m~t!iod d:I!Jnh of90·1 JO"n due to tl".e comrlexil) of the sample uwri~. The artcct''.d srunplc :-cc.:ncrit!~ are tMled ,,jtJ, o ''l ~·~ an:.l''l..l'. qtmiificr in the r~rc>~t. "fhe ~..·licnt wa!- 111.tJI! m\ure \lrthis OCl\!rn.•.!ce

due wthc ChhJt id~ intaiCn.:n~~~ during dh:: lt:· r.n~tl~ l;)h '\(' t'utthl.!r ocli<,n wa~ t~kcn .

There i; •t det,lil~d lis: in;! of the dat:t q:,clitias us(d in this r<port l•Jcm~u at the• end ,,fth<' ~ ~·IXJl1 be!brc' the COC sectii:m.

Subcomracted ,\nalys~s :

The fGIIO\\ing te:o:ts \\er<: !-!ubcomractcd to nlher Tt~~tAmerkn lt~~t) nltol ·ie-~ 1h~ir rc:.nlt-. ''ill h! loca!ed '' i1!lin tl ~ bud~ ol ' thc r(:pot1 unlcs;, nl'tcd ;._li hcr\\IS' ~lt the l't.•ginmng olth~ I' Ctnati-.~

('(JIOr an ~ll~ Si!'> \\~:: ()CI r,,nll(:d by tk: Tt:.:'tAnv..:rk'lt ~<.!\ anmdl !~fhl(:!.(.)r_ .. .

Total,.._ Di~so:,·ed ZirCt\niuml>~ !\ktlwd oO?Oll and l"vlai Sull\:r b~ ~~~tltr>d 602!1 11 \\W~ :tl>a!~l.;:.lt:o:. d • .: ·1 estAnlcn,'n Conn~etict.:t l:thornhV)'. Ci~nH~ll.l ~p~l'ln.lil\lP." illld ( 'fll'i' ·\lp1Hl and (u ~)~!> Bctu '.\ ..:-r'-· :m::!l.' 1-:J h~ the ~r. Louis iabotator:-.

The Chain(>) 0f Cu;t<>d~. 41 png~s. arc included and m·~ un im~grul part of this rcJA1rt.

All solid; results nrc r.:por,~d in '<"et W<'ight tml~s·s >JJ<.-ci!·,c~:Jy >laW~.

Estimated uncertainty i' n> ai!ablc upon request .

Thb repon h:h ht!en ck~tronk·2Hy signed.

Rcp\trt -\ppr.l<·cJ By:

-.

CHK00000081

Test America THE \.EADER IN ENVIRONI.IENTAL TESTING

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CHK00000082

Test America THE LEADER IN ENVIRONMENTAL TESTiNG

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CHK00000083

T estAmerica THE LEADER IN ENVIRONMENT;\L TESTING

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CERliFIC.-\"110' 'ii' .\1\I -\RY

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.t !~I(IS;I) i(ll

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Page 50 ,,r51

CHK00000128

Test America 1"HE LE,\D~fliN ENVII~ONMENlAL TESTING

( lJ:..· : .t Ch.;-.;lf'l'u\.,: F.nug~ C-..rp<IT~l=i .• ,.~

t,Jfl:) ,. \\\:~t..:::) ::'.,\'CII\IC

\\'vrh 01d<r. Proj".:\ '101·o~·

SRI 0012

,\•Ill

A·(!la

E 11!3

I]TJ I.

1.1

L2 \12

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\18 M:-;R

\1\"RI '\J IU R~

'W

Oi-.!!!lJomtt Cn.~· ( H·~ 73 t , ~

I Tt:C (ilp:\~)1~

Pr\IJ('t.:l Numht>l' ~ 10\iS i{l7 il

Rect1vt·C 12.0:!.~S !)X 3'J

ll.\T.\ Ql .\IIFif:ll~ A '\I) J)EFJ\ITIO'~

Condu.:ti'. · it~ proh,;/m~\~r li1tc;u to 250.000 un:ltos!cm. Sample \\eight on filter i$ grcJtcr tho P 0.2 gnuns. Conc~ntr'-ltion t.:\.<.:ccJ:, the "-'alibr,tlion rang~ and thL·rcli.,rc.: rc.:mlt is ~~mi~qui.mtnutiv(.',

Sample r~cci,ed \\itlt in~ufiicicm hoiJing tin,e r~mainmg ti.•r auulysis ll> be p~rf(onned within the method's lt,.J,!in~ tim rcquircrn1.!'nt!'. The ho lding iiO .I.' tOr thi~ h!.;~ i:l htiiJi~diah!. I ht! labOn.ll<)f~ l(lCusurelltcltt. thL'I~I'or~. ltlU) IIOl fie ~lllltlblc r l lr c ..• :~. pli:HI~'c.. plHjh~:·~~ -

1 :lhorato:: Cnntrol Sampk i.lnd/or Lnh(JfiJh"H) Cont1PI ~an;p:t• Duplic:tt'! r~CP\er~ \\i.l'i ~h'''~ tlu: Jt:l..:pt..t!h. ~o i1~l ib \uui~ h.: m~~

dct~clcd. d:~t -:"1 110! imp;J<:h:d

l . ab<.tn.\Wf'~ Contml s~1Jl pll' !"lmf·nr I :thllfi:lhlr~ ('(llltn)l "'antpk Duplicate rCCt)\tr;- \\ :IS uhu,c Jl'( 'L~ pt~:r: .. : ... ' 111'' : ! ...

l. :tbl.lrat«..ll '~ c~)ntrol ~~tntpl~ :m ... l :,}1 L~thnrntor~ («..llltrr•l ~.ample! Duplic~!h.! rc;,;o\~r~ \\:1:0: ~ChJ\\ ,\._·,cr•·H 1(c.; =it'll l b .

1 ht ~1:-- ;.:td ,,,. M~I> ".:rc hhl" the acc.:rtar.tc Iii 1it> d:•c hJ ;~mpk motr:, intcrfcr.:ucc ~c~ B IJI k ~P~~~ il.t.. '-;

Th" :\1~ · i\\ SD rcquir.:-~.i a dilution du~ to n.atr i:\ mtcrff.."rl'llL'<.•. Because n!'th!s d!IUiinn. tl ~ rn:ltr!\ ;-)plk~ c..l\IH ~ IItr .oim1:.; m :b: !'Uiltplc! :.,~,r~ rcduc..:-J to a lc,cf "here the rcc~wcr.l' c~k~uJ,ttiou dot!~ 1·01 pro' ide us~li1l intnnll.lt!Oit. ~l't nl t.Htk :--.ri~t· (I ( ~i

!"heM~ ami _. ,. \1',() \\l'IC ubo\C th~ :M·cptali('C hrn it$ ~.:c fll<1:1k Spi~c ILC'>i. Th~ ~IS anJ 'umple used 1i1r tl:c ~·IS/~lSD r.:qnirc,l (lilutivn " '" H• !''' ' ""'Pic 1 l:Hr"

Bc~au,:" ,,)this. the spik~ C•lmpounds were diluted b"lo" tl.e Jctection limit. I here \\as no MS/fl..f$[) analyze~ ''ith this h.ttch d11.: to iosunicicnt »:nnplc ,.,,lumc. Sec Bbnh '> pi k:: !'.cc tase narratile. "I he RPD "'''et:d.:c! t!t.: llcccptancc limit. Due w the h>\\ le\ds ofm.al;•te in the ,,ampk.thc duplicrrte RPD cakulati•1n doe< nP: rrol"idc u'clul inli>rmatit>n.

'\oi dctcct.:cl attb.: reponing limit lor method detection limit it" sho"n)

\J J:TIIO£> 'IC)DlFI(',\ TIO'\ \OT E:-o

350.1 M • M = Ammon a-Nitrogen methoel modifieel for mieli·distillation with La chat Procedure 1 0·1 07 -06-1-A

COD 410.4 M • M = COD method modified for use of Hach method BOOO

p .1~. '· • ~ • • ( i

CHK00000129

Test1\merica

ANALYTICAL REPORT

Job Number: 680-42739-1

Job Description: NRL0012 Chesepeake Shale Project

For: TestAmerica Laboratories, Inc 2960 Foster Creighton Drive

Nashville , TN 37204

Attention: Mr. Mark Hollingsworth

Abbie Page Project Manager I

[email protected] 12/09/2008

P·~t~ :l ~· .. t,tc;t:• I

1)_.'j ~·~~ 15:~·~ N!

The test n:su:ts •:\ tt·1is r8por1 meet NELAP requirements for parameters for whict1 accreditation is required or available. P ... ny except1or~s tc tt1r:; NEL!\P requirements are noted. ResL1Its pertain only to samples listed in th1s report. Thts report rnay not be repr:Jduced. t':xcepl in lull. without the writren approva; of the laboratory. OL1estions should be directed to the person who signed th1s rerio't.

Savannar1 Certifications and ID #s: A2LA: 0399.01; AL: 41450: ARDEQ: 88-0692: ARDOH; CA: 03217CA; CO; CT: PH0161 : DE; FL: E87052: G.A.: 803; Guam; HI; JL: 200022; IN : fA: 353; KS: E-i0322; KY EPPC: 90084; KY UST; LA DEQ: 30690: LA DHH: LA080008; ME: 2008022: MD: 250; MA: M-GA006; Ml: 9925; MS; NFESC: 249; NV: GA00006; NJ: GA769; NM; NY: 108,>2: NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; Rl: LA000244; SC 98001001; TN: TN0296: TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA WV DEP: 094; WV DHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q

TestAmerica Labora;ories, Inc.

-::si..A.:noenca S\;-.'arntt'1 ~- Q~ l.t1F-!:.'CI1e Avenue. Savannah. GA 314C>4 ... ~! {912) 3~-:v7H58 Fax (912i 352~0165 wyNi h~S1&0113C!Caint; CO:T

Page 1 of B 12/09/2009

CHK00000130

Comments :-~o addlt!onal comments

Receipt

Job Narrative 680·J42739· j

Ali sa11 plt3~; wt3re recf"=v0d rn g<;Od condition wi!h;n fem:;erat:.Jre requirement~.

G&neral Chemistry t·..1e!hod(S! St.A 21208 T11e foEiowmg ::;~1rnL\:eu:,j wa~ received ouiside c·t ho:din~1 t:rrh:: r~RL001 2~0 1 '680-42739v ~)

No ol~er analytl<::al or quality 1ssues w&n; no!eel.

!?age 2 of 8 12/09/2008

CHK00000131

METHOD SUMMARY

Job Nurnber: 680-42738-1

Description Lab Location Method Preparation Method

Matrix Wat~r

TALSAV SM SM 21208

Lab References:

Method References:

Tcsttr..meri:::a Savannah

Page 3 of 8 12/09/2008

CHK00000132

SAMPLE SUMMARY

Ciient TestAmerica Laboratories, Inc

Lab Sample 10 Client Sample 10 Client Matrix

680-4~739-1 N~L0012-01 Water

TestAmerica Savannah

Page 4 of 8

Dateifime

Sampled

12i01i2008 1100

.Job Number 680-42739-1

Date/Time

Received

i:.?!C13f200B ossa

U/09/2008

CHK00000133

Cllenr TestAmerica Lai)O;<ltones Inc

Gone•al Chemistry

Cl ient Sample ID: NRL0012·il1

Analytical Data

Job Number; 680-42739-1

Dale Sampl;·d

Date Receivecl:

12i0 112ll0il 1100

•t2;Q3120013 0858

Gual Units RL Dii Method ·····-··--···--- ·· --·---:-:------'---'---'---'--------_..:::. ___ _..:..:...___~_..:::. __ H>O H PCU 20 4 0 SM 21208

1210312008 1340

TcstArneriea Savannah !'age 5 of 8 12/09/2006

CHK00000134

C!ient· TestAmenca Laboratones Inc

Lab Section Qualifier

General Chemistry

u

H

TestArnenca Savannah

DATA REPORTING QUALIFIERS

Description

Indicates the ana!ytil was analyzed for bLit not de:ecte(j

Sample was prepped or analyzed beyond the spec.f,ed holding time

Page 6 of 8 12/09/2008

CHK00000135

Clten: Test~.rnenca LsbGrmones. inc

Method Blank. Batch : Ge0 -124416

Lii~ .. · S~1rnr;it: iS: t~~s 680~12:~t..1G!1

Chen: f/i.lln~ V\1ater

uiluhn I C• Date .Anaiyzed. 12i03!20Gf.; i:\.W

Dc1:o; Prepa''ed: N!f\

Analysis Balch 6B0-1 24416

Pret; Batch: NIA

Units: PCU

Resull

50

Qual

u

C;A:~.Iat:O!'~S t1ft~ P<:.'!l formed h~'·Jr·~ rounding io avot·j round~cft errors tn culculated results_

TestAmonca Savannah Page 7 of 8

Quality Control Results

Job Number, t>B0-4272,9- '1

Method: SM 21208 Preparation : NIA

Instrument !D, No Equiprnenl Ass1gned

Lab File ID' N!A

Initial Wt~ightNelume

Final WeightNoll•Ol'i!, 1 0 mL

RL

12/09/2008

CHK00000136

SENDING LABORATO.~X;

TestArnerica Nashville

2960 Foster C;e!ghton Road

Nastwn:e, TN 37204 Pllone· 800-765-0980

Fax. 615-726-3404 Project Manager. fvlari<- Hol ii:-:gswortt1

Cli, .. ·n: ( i:t~=-.~r:...\tk~..· l.a .. ·rg~ C\11p~n:~:i•·H1

SUBCONTRACT ORDER

TestAmerica Nashville

NRL0012

RECEIVING LABORATORY:

TestAmerica Savannah

5102 LaRoche f,venue Savannah, GA 31404 Phone .(912) 354-7858 Fax· (912) 352-0155 Project Location. Pennsvivani"' ~.xcipt T l'mpcrnturc: -·- ··c

C~pylR~bg ftom NRJ237 3 Copy!Relog f:om NR..11819. Copy.iRelog from NRJ, 16~1. Co~ 1/Relcg fr~n: NRJ 1 ~55 Copy/f~~~'--.n i:v<TO N'·~Ja;·os Ci>~:y 1R<f(}q fro'n NRJ0546 CopyiRelcg 1rcrn NRJQ4S8.

Analysis Units Due Expires lntcrlab Price Surch Comments

Sample 10: NRL0012-01 Water Sarnpleli: 12101108 11 ;QO

_s_u_b_c_o-nt-ra_c_t __ ...,c:-o-,o-r ____ "l::-, -----,-2:--1-12:-:-::oa~-o=--a:--12::-~ 7:-/'"-1 "', "',~o"".o~o-'---'-"""'-'-'-"s"',s=-'.uoo~'-=o:-:~-:-,, --=su'hlo-T.t.. -s;~ a~;;~~;:;-~-i~~-,t;;;;-$-, .. -,. --

Cont.~iners $(1pplied:

W 500rnL .Amber Glass Unpreserved (NJ

----·--------Relt>ased By Received 8y

Page 8 of 8

2120B

.. , ) -, .,1'- ,;\

'····'

Poq~ 1 o! 1

1.:/09/2008

CHK00000137

Test America 'll\llt~l~\1" ll~ Nr:~l v1l'e TN COOl,ER REC.U

'·!Ri .. Of\1 ':'

Cooler R~cervedi(Jpened On 12i0212008@ 0830

·rackrng ~ ... L:_ ( '{_~{..._ . ___ Jia5t 4 digits , Fed Ex)

Coune •· ferJE.< IR Gun ID

2 TcrnpcratlHC or rep. S(.lmple or temp blank Wh'?n opened:.O u _Dt'!grees Celsius

3. If Item #:i tcmpcr~ture is o<c or less, was the rPpresentative ~~n.,le or tnmp blar1k frozen? YES No .. 6,)

) ~\~~~i~0~.NA '

4. \"''ere custody seals on outside of cooler?

11 yes, !low many antl where: ___ _

5. WrJre the seals intact, signed, and dated correctly? ~ . .. NO ... NA

6. Were custody papers insid~ cooler? ~ ... NO ... NA

1 cer1ifv !bat 1 o;>ened 1!re cooler and answered <Juestions 1·61intiah . _______ b __ 7. WNc custody seals on containers: YES tJO and Intact YES ... Nc ... v

Wore tll•·J>e si;.n•cd and dated correctly? YES ... No_@'~; P. Packing mat'l U$Cd'l ,.elJbbj;;.,~a'P) Plastic bag Pean~ts Verrni<:~:~~':am Insert Paper OtherS)

9. Cooling proc~ss : \.._.._,_./ G Ice-pack ~e (d:;.ectco~tacl); Dry icc Other None

--- (<""";.. K)'.E$). NO ... NA

~ . . NO . .. NA

~.NO ... NA

( YES)NO ... NA

10. Did all conlainr-rs arrive in good condition (unbroken)?

11. Wore all container labels complete(~. datP, signed, pres .. etc)?

12. Did all cor:tair.er lab~ls and tags agree with custody papers?

13;>. Were VOA v·~ls received?

'--·-1' -~ h 1/'/as th<?re •·"{ oDsarvable 11eadspace prese!]_~ in any VOA vial YES\::~~;.NA

14 vV.>>: t;,.,e a T6p B\.tnk in this cooler? ®.NO .. . NA h multiple coolers, sequence# _____ _

1 c;,rttty ttl~\J..!!.!ll.!llHt!?.Q the cool~_ar,tL!!!l.~~~ue.s.tlor.~.I::J~t:'!!J ------ 1Ck-· 15;1 On prr•s'c l>otlles. ditl pH test strrps suggest preservation rea< lr<'d I he correct pH level? ~-~S-~A

/' b uio:l Urn bottle l,lbeis indicate that the correct preMr,atiii&S wee used { YES:7)r-JO ... NA

. '---If P'es~rvatictr in-house was needed, record standard 10 ct prcservati)le usod here _ _ . _____ _

16. W t!o S residual chlorhe preMHll.? • YES .. €J.NA

)_\~J:!.~:£.lhel 1.~!'-d_f:?r chlorine and pH as p~r SOP and answer~ct questions 15·16 l!ntial) L----· 17 . Ware c11stody pa p<>rs properly filled out (Ink, signed, etc)? eNO .. . NA

~ .. NO ... NA

~.NO •.. NA

'CV.NO ... NA

llir.!l!Y.!l'.~Hl'1l!.!tf"ll U;is project jnto LIMS and ans~.t1.~'· . ..:1..:.7.;.:·2..,0'-'!"'in..,_t:.:;la,.l"-)------~=-

iS. Did yol. sigr; tlle custody papers In tile ~ppropriate place?

19. Were correct containers used for the analysis reqCJosted?

2(). Was suf1iclcnt ~rrrctunt of sample sent in each container?

v----j_ccr;jJtJ.I)~J.2lt~.f.hed ~..J.f!9£.!3.i!.tl tho unique LIMS nyrnll.er to each .~:ontainer llntia!l

21. w,;r;, there Non-C:>,forrnance issues at login?@:o Was:: PIPE generated?8NO .. #7/ J? >-

Illu "' '! ,,. ... ·"' · ( c . · .·r 1<. <' ·c l ; ·~• :1! \~.~. I.F-1

Fd :d F<oro;

CHK00000138

Test America Nashville, TN COOLIW. RECEJ PT FORI\1

Cooler Received/Opened On 12!02/2008@ 0830

1. Tracking.# l C l'-'~=-· _.}~ ____ (last 4 digits, FedEx)

Coi.Jrier: FedEx IR Gun 10

2. Temperature of rep. sample or tomp blank when opened:.~ __ Degrees Ce/:<lus

3. If ltem #2 temperatura Is o•c or less, was the representative sarnple or temp blank frozen? YES NO.G.J

4. Were custody s~fr!s on outside or cooler? '1 \ ···\-~ .. NO ... NA

5. Were the sea;s ~ ;ct, slgnad, and dated correctly? @ .. ,NO ... NA

I! yes, how maJ\"\nd where:._____________ :7 ~-"'--

6. Were ctJ<Siody "ers lnsldf! cooler? 6s> ... NO ... NA

1 certify that 1 opened the cooler and answored guastjon:s 1·6 !lntiali ________________ ___Q_ ____ _ 7. Were custody seals on containers: YES NO and Intact

;-;-: .... _

YES .. . NO.;:NA ;

Were thase signed ~nd_.datetl corr"ctly?

8. Packing mat'l used{€;~~ Plastic bag··· Peanuts VermicuJ!.tD:: . .F.oam_~~-sert Paper

9. Cooling process: "--- 8 Ice-pack C:•· (d{oct cor~;;)

y,-:::,. , YES .. NO.[ NA l

~-:·~::.--·/ Othfrr~NC>nH ' ., ___ ,

Dry ICC __. . .2'~he r Non,...

Did all ~ontainers arrive in good condition !Unbroken)? · --- c~:l0 NO ... NA

( YES) .. NO ... NA \..-;-.:: ( YES'.~ NO ... NA

\------r~ YES .. ~~;.NA

10.

11. Were all container labels complete t·~, date, signed, pres., etc)?

12. Did all container labels and tags agree with custody papers?

13a. Were VOA vials received?

C' b. Was there any Observable headspace present in any VOA vial'i YES ... No .. 1NA ) . 6, - \_./ 14. Was th.,re a Trip Blallk in thi.6 cooler? YES ..• NO •. ~ If multi pia coolers, sequonc!! #-:---:::._ .. I cortifv that I unloaded the cooler and answered questions 7-14 !Inti&} ~ );/ __ _

;--15a. On prns'd bottles, did pH test strips suggest preservation reached the correct pH Jeve!? YESlNOlNA

/c--.. ~_/ b. Did the bottle lab~<ls Indicate that the correct preservatives wHe used

If preservation in-house was ne11ded, record standard 10 .ol preservatiya used. here

16. Was re!,idual chlorine present?

I YES.l.NO ... NI\ \._...~/

YES.j~O) .. NA \.....---

1 certify that. I cl1eckecj for chlorine and pH a!! pe(j?OP and answers< I questions 15-16 linti!!)J ; /---~

1!,~?NO .. NA 17. Werfl custody papers property filled out (ink, signed, etc)?

18. Did you sigry the cu3tody papers in the appropriate placa?

19. Were cc•rrect containers Ltsed for the analysis request&d?

20. Was·su'ficfent amount of sample sent in o~ch container?

~~~ - NO .. NA

( YES~.NO . .• NA 'F._-..._ \~.s! . ~!o .rlA

t certify lhQI.I entered thl$ project into LtMS and answered guestioQ." 17·20 ("'in,_..t"'·al.!-1),__ __ _

I:!!S 'tit Brak~n b shipmer.: C<>o!•r Re<eip FNm <ioc

'" :;' ::: :::::,::::::~;;D!T LF- !

[r,l cfFc'' "'

CHK00000139

10811 CII[Nl NAME •DV RECORD

I 1 Pf,RAME1F.AS·ME11CO!! NUMt,~ER CI-1AIN-<'r.-"' i--r- ~-~ ~ I ' ; I i '\2

PROJE:CTNO · ~ ~ . I ~~ NRLOO '0

0'1 ()

(;K

A•;.;~IOI'\ !:.\ : I..Ar.~..;~t•. IX P.nil<i•;.,~. O\

.~{f·.~:• I )~"""· y~~ • .'.'.:J:> '¢.f:

3' 7,~: '!0 QA :. I ~.~.', /!• :-' · ; l ·!t.:. ·

!'\l~~}llrl ;~!~ : --·-~- -~--·- ------1 ~ I ' I~ I ~ 12~~hlHAM ~~E · _i_ __ ~--~ IU_ Ciod • - ~-~ ~ i ~~~-~ ~ ~~j!ll !IIJI, HEMARKS

ti'Y:"t~-tt•.<: ; .. ~! ,.,. .-:;.: .otlrr,...., "\'.:0' "'"';.r,•l

DATC TIWl I j SAMo'l ~ IUb'IIIF'CATION ~ cl "c nLrcnm. VNr" rr:nw. >'iESo<~ro.

- --·--,--,--+--- • ~ ~ ··-~-------· !- t u~:~:=~~~~~~-· ·-?--".....,..L-j-1100 ~tJ.~-rt:l,.!;;p .tAj,( . 1.. .'-t.'i.lO~I.J..j)_ ____ j \ X..K.,K .... ~-i ><,_~---- - - - ... 2.l (4)250;;:-~f~zP\!L .... -

--1-L.l/\.~ ~--- - 1 ----r---Xr-"1-- ... _- - (i,i'a~So.i;(1)1LPH2S04 ------.. ~ .. --.. ·-·~ -·- --+-----.. - .... _ ··---- - --- . ·--~-~.~---&.. __ ... _ ._ _ _ I --~- -- ------ --- 1 -~- • 1 --- ........ - r---- ~~---- ·-----.... - ·-.-

=- I_ I t ~-- --n l++=--~--=- -1!!f::t1!~=~:.- == • -----1---- I • ·------- ----··-·--·----r-- ·--,·- 1-- I ; --~,~-_;;;!~i~!l>r:",'!I'!.WC .. ,~ ..

~I 1 _ I ----------- . --m- __ _ t 'e-i- ..... • --i1T25t}n.fP~/ZiiAOiiiiii _________ _ ~ ---~-- ---- -- · ·-·--.. ------··-- -- - j .. . -+---fft)!Cioiiii~H:I:904--------·

---- --- ~----~--- . -- ----~.- -~.:_::=-- -- ·-r-· -- __.~,._ --·---t.-.. •. a LX .. - -- .. ..

--- • ------ -- · · ... - 1 -j---- ·1 voc(3)4o~rvoxHti·-----.. ----l ·-:. l 1 I I I"SVOC. -- -· ·- - ·- ----

.'Gel"~ ~~y ~~"') llAlC .!ZJ..!.[p~ lHFCFIV!·IlllY (Sign,nure)

'""~ .A_~ !~ . r~u / TIME I LfQQ ! -~====:::...:.: .. ..................... _. __ .............. +..... . ...... ... ....... ... t--·--................ .. OAT Eo------! liLCCIVEO BY: l~ign•tvr•) DATE: ........... ..... ... ...... j ~MPLE SHIPPED BY: (C•tcle) AIRBIU. i1 q il~;J..l_Ql 1.C.

I.JAI(,: ------ -

liM!:: .............................. --..

TIME : ::::::~ ]nlnN ;..R00~~-:;iiii~~~;-~. PONY xrs '!EL xrs

i 9t.ndlrd ! t-IANDDHIVf:flEIJ liPS Oltltll

TIME:

.........,,c:AtfC_.. , ::rcc.;-;;: r' t>·,- ~~:;c;;..;r(; ;:-,- . . ~- -.. --·t: .. ;~;-:-,~~::;,~~~·;~~:~3::~,~;;;· --· ····· !L •• u ::,:v, 1

1

_ ...... (. • / ./.. _ { -i_ L.( _____ ...... ! rorr.po•,l!; • ., ----~· · 1 ... Wr.tlco ?tcscnt · • I

I VOA's Free o: Hc.rtd~P.~t~ol! Y N 1 (Srgn.uur•) j

/ • t .. J.::om~~~!! .. . - ··- -~ ..

I oAT[ _(_!.file:( ---- iiME ~· )0. ! ---- --- - ·--------l. -- ·--........................ ,_ ........................ ......... ........ ... .... .

f PHONL ;;. .;o& '$:~ 1· :10~~

i ·1~;,. L ; :.: -~.:,..; ;. ,:\~,;.;,.:\;l.,it (t'. . ·~~~·---·-·-·· I~-~-

AL:;)HE..';S. ___ ......, .... ~Dr ......... .. .. (;!IV __ .............. _______ STAT(:. 1N

N

.. II' .Jnl)4

1~1Nr Ar~·r· ...., tieR 0 ................. .

PIIONE . .......... ~,!064

!~f.'Nt:iAt,-t cO:~~TAf.r .. f"'i:;i1.$0~'i{~·- ·-- ·. -

Scali HI•

POINT OF WIIGIN. ·_J NORM!J'j '.J TIJL.SA ...J 1'\f'<t i \ICTON _j r,R!:>MOHF .J liOI.ISTQ>j )(OTH[R -~J.J_f~ ~_'!~ .

P.qGE N I · F?h."'.:E!V1N(i i AH ~';\GE II;: 9~ 1 uH~ i 0 HI· NHAM i'A\.F 63 · PftOJFCT MANAGEH PACE R•l Q~. ·oc CGOHDINArOfl

0 ..q-..-0 0 0 0

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111 7 2 CUCNT NAME

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PAGf 111 - RECEf>IING I i\R PAGf !12 • RCI URN I 0 llF"lfiAM PAGE 1!3 PROJF.CT MANAGtR PAGF. /J·1· OA!OC COOROINA\01-1

..-'V ..-0 0 0 0 0 ~ I u

Test America

ANALYTICAL REPORT

Job Number: 220-7492-1

SDG Number: 220-7492

Job Description: F8L030326

For: TestAmerica Laboratories, Inc.

13715 Rider Trail North Earth City, MO 63045

Attention: Ms. Sherry! Adam

Designee for Erin A Gaus

Project Manager I [email protected]

12/18/2008

The test results 1n th1s report meet all NELAP requirements unless specified within the case narrative. Pursuant to NELAP, this ·eport may not oe reproduced , except in full, without the written approval of the laboratory. All questions rega('(Jmg this report should be directed to the TestAmerica Project Manager.

TestAmerica Connedc.ut Certifications and Approvals: CTDOH PH-047. MADEP CT023, RIDOH A43. NYDOH 10602, NY NELAP 10602, NHDES 2528, NJDEP CT410, ME DOH CT023, UT DOH 2032614458

TestAmerica Laboratories. Inc.

Tcs!A'T' .saric; Cc.rl'le.GIICut 12B Long Hill Cross Road 51'-elton. CT 0648,:.

Tel !2•)3j 829:-8140 Fax (2.03} !.129-8142 ~. .. ··.v.•.:.tes lameric,~ioc C("m

Page 1 of 16 12/18/2008

CHK00000142

Comments No additional comments

Receipt

Job Narrati •e 220-J7492-1

All sarnpl&s were received in ;JOOd cond1t;on ·.vithin temperature requirements

Metals Melhor.l(s) 6020: The fol!ow1ng samp:es w;;;ra dilu~ed due to the nawre of the sample matrix: NRLoo·,z .. o I i.220 ·7·! ':12 -1i, NRLOOi2·0·I·DISSOLVED {220-7<~92·2). Elevat"d report1ng llrn;ts (Rls) are prov:ded.

No other analyt1cal or quaiity issues •llere ncted

&

Page 2 of 16 ~2/18/2008

CHK00000143

Client: Test/lmenca Laboratories, Inc

Description

Matrix Water

Mt:-::~ls i!CP:t.;1S.l Samp~E FJitrewon. F1eld Preparatron Total Met3:s

Lab References:

TAL CT:.: TestArnenca Corr·&cti::;ut

Method References:

METHOD SUMMARY

Lab Location Method

TAL CT TALCT TALCT

SW846 6020

Job Number: 220-7492-1 Sdg Number: 220-7492

Preparation Method

FIELD_FL TRD SW846 3010A

SW84G ""Test f'l1eA·xis F:.>r Evalua;ir:g Solid Waste, Physicai!Chemicai Methods", Tl1ird Ed,t!on. November 1886 And Its Updates

TestArnerica Connecticut

?age 3 of 16 12/18/2006

CHK00000144

METHOD I ANALYST SUMMARY

Client: TestAmerica Laboratories, Inc.

Method Analyst

SW846 6020 Petronchak Nestor

TestAmerica Connecticut

Page 4 of 16

Job Number· 220-7492-·t Sd9 Nurnber: 220-~?492

Analyst ID

N?

12/lS/2008

CHK00000145

SAMP LE SUMMARY

Client Testf>.mer:ca Laboratories, Inc.

Lab Sarnple ID

2 2~-7492··1

2 ~C - 7492-2

Client Sample ID Client Matrix

NRC.00 ~2 .. 1)1 Water NRL0012-0·t -DISSOLVED Water

TestAmeriea Connecticut

Page 5 o f 16

Date/Tirne Sampled

1210112008 0000 12i0 1/2008 0000

Job Number. 220-7492-1 Sdg Number: 220-7492

Date/Time Received

12111/2008 C955 12i11!2008 0955

12/18/2008

CHK00000146

SAMPLE RESULTS

TostAmEtrica Connecticut

Page 6 of 16 U!lS/:iOGS

CHK00000147

Client ·1 est.A·r1enca laboratories. Inc.

Cl ient Sample ID: NRL00"12-01

l..iJb Sa<";; ·e: ID

Client Ma!r 1Y

::2(.- ' •Hi2-1 \-Vater

Methocl 6020 F>rep~1r at1on 301 OfJ.,

Dilution 1 0

Date .Ara;yzed 12i16!200S 1 i23 D;Jt'" Prepare(i. 12!12i20G8 1524

.4nalyte

Zr Sulfur

TestAmerica Connecticlit

6020 Metals (ICP/MS)

Analy&is Batch: 220-22933

Prep Batch 220-22804

Result (ugfL)

10() 82100

Page 7 of 16

Analytical Data

Job Number: 220-7492-1 Sdg Nurnber 220-7492

Date Sampied. 12/01!2008 0000

Date Received. 1 2i1'i!200B 0955

Instrument ID:

Lab File ID:

ln1tial We;ght/Volume

Final WeightNolume:

Agilent ICPMS NIA 5 mL 500 mL

Qualifier MDL

30 30000

RL

u J

100 100000

12/18/2008

CHK00000148

Client: TestAmerica Laboratories. Inc.

Client Sample ID: NRL0012-01-DJSSOL.VED

Lab Sample 10

Chent Matnx.

Method. Preparation Dllut;on Date i\nalyzed Date Prepared

220-7492-2

Water

6020 3010A

1.0 12/16/2008 1727 12/1212008 1524

6020 Metals (ICPIMS)-Dissolved

Analys1s Batch· 220-22933 Prep Batch 220-22804

Analytical Data

Joo Number: 220-7492-1 Sdg Number· 220-7492

Date Samp!ed. 12101!2008 0000 Date Rec(;ived I ~!11!2003 0955

lr.strwnent ID: Lab Fiie !D: Initial Weigh'lVOILilo<: Final Weigt;:/Volwne.

f'gilen! ICPM.S WA

5 1,..L 5(.0 rnL

Analyte R<;Sli!t (ugil..)

10)

QualifiN MO~ RL

Zr u

TestAmerica Connecticut Pa ge 8 o f 1 6 12/18/2008

CHK00000149

Client: T<:stAmenca Laboratones. Inc

Lab SectiOio

Metals

TcstAmcrica ConnectiCllt

Qualifier

lJ

J

OAT A REPORTING QUALIFIERS

Description

lnd1cates anaiyzec for but not oetected

Job Number: 220-7492- i Sdg Number: 220-7492

Sample result is greater than the MDL but below the CRDL

Page 9 of 16 12/18/2008

CHK00000150

QUALITY CONTROL RESULTS

TestAmerlcl1 Connecticut

!>age 10 of 16 !.2/l8i2008

CHK00000151

Clit:nt· TestAmenca Laboratories. Inc.

QC Association Summary

Lab Sample 10 Client Sample 10

Metals

Prep Batch: 220-22804 LCS 220-22804/2-?. t.,!B 220-228041'1 .. f... 220-7481-A-1-B DU 220-7481 -A-1-C MS 220-7492- i 220-7492-2

Analysis Batch:220-22932 LCS 220-:22E'CW2-." !.16 /20-?2504 '1-A

AnalySIS 8atch:2Z0-22933 :<2U 74.: .. _,\ · :> uU .~: ... : ~). ·:-48~ A ; c r.,.l :~~

21.(! 7492· ~

neport Basis

T: Total

TestAmerica Connecticut

L<:b Control Spike i·/ethod 8!:.3nk Ouplicate MtJ!rix Spike NRL0012-0I NRL00-12-01-D!SSOLVED

tab Control Spike ;A .. ..-.th:Jci Biank

r·..1(1trix Sp~~.e :-~RLOC12~0 1 NRLOO 12-01-DISSOL '/ED

Report Basis

T T T T T 0

!

T

T T T D

Page 11 of 16



Client Matrix Method Prep Batch

Water 301CA Water 3010A Water 3010A Water 3010A Water 3010A Water 3010A

Water 6020 220-22804 VVater 5020 220-22804

\:'Vater 6020 220-22804 Water 6020 220-22804 V"Jater 5020 220-22804 VVater 6020 220-22804

12/18/2008

CHK00000152

Client: TestAmerica Laboratories. Inc.

Method Blank- Batch: 220-22804

Lab Sample ID MB 220-2280411-A

Client Matrix Dilution

Date Analyzed.

Date Prepared

Ana.yte

Zr Suliur

Water

1 0 1211612008 1557 12112/2003 1524

Lab Control Spike· Batch: 220-22804

Lab Sample 10 I .. CS 220-22804/2-A

Ci1ent Matiix Water

Dilution 1 0

Date Analyzed 12i16/2008 1600 Date Prepared 12'12!2008 1524

Analyle

Sulfur

Matrix Spike- Batch: 220-22804

Lab Sample 10 220-7481-i\-1-C MS Client t .. 1atrix Water

Dilution 1 0 Date Analyzed ~2/113/2008 ·1628

Date Prf:'pared· 12i12i2008 152-1

f,na!yie

Sulfur

Analysis Batch 220-22932 Prep Batch· 220-22804

Units. ug/L

Result

10 10000

Analysis Batch· 220-22932 Prep Batch· 220-22804 Umts: ugil.

Spik;: Amount

40000 43020

Analysis Batch 220-22933 Prep Batch: 220-22804

Units: ug!L

Qual

u u


Job Number 220-7492-1 Sdg Number: 220-7492

Method: 6020. Preparation: 301 OA

lnstrum"'m ID Ag!lent ICPMS

Lab File ID N;A 1n1t1al Weighl'V~'Iurn"'· 50 nl.. F1na! We!ghUVclume 50:) :nl

MDL

Method: 6020 Preparation: 3010A

R!.

10 •l(ii()·.J

lnstrurr:ent ID t\gd-2nl iCPMS Lab File 10 N.'!l Initial Weig'1:No:urne: 50 .,-,L

F•nal Weighti\Jolunv:; 500 rnL

%Rae Lirn;t Qual

108 5)- 120

Metl;od: 6020 Preparation: 301 OA

Instrument ID Agi:;;-nt ICPMS

Lab File iD N•f,

Initial We1ght!V:;lurne 5 ml

Final V\l&:ghtN,)Iwne 500 ml

Sarnple ReSt.Jit!Oual Spike Amount Res .Jit

J 400000 502300

Calculations are performed before round:ng to avoid ro~.;nd-off errors 111 calculated results

TestAmerica Connecticut Page 12 of 16 12/18/2008

CHK00000153

Cl ient: TestAmerica Laboratories , Inc.

Duplicate· Batch : 220-22804

LC<t! Sample ID :?.2C-7-10'-.~.-1.:·3 DU

OdL:t!On i C

Date Analyze-d 12i16!2008 1·3:1.1 U8tE' Prer.)Eir'::("l" 12! ·1 ~::·2.008 1524

Zr Solfur

Ar.;;lysis Batch. 220·22933

Prep Batch. 220-22804 Units ugll

Sample Result/Qual

37 71800

J J

Result

100 72750

C<Jiculattons are pE:rform&d before rounding to avoid round-off errors in calculated results

TestArnerica Connecticut Page 13 of 16



Method: 6020 Preparation: 301 OA

Instrument 10. Ag ilen\ ICPMS Lao File ID: Nlf', lniltal Wetgt;tiVoturne: 5 rnL Final We1ghl'Volume: 500 rnL

RPD

NC 20 20

Qua:

u J

12/18/2008

CHK00000154

F8L030326 NRL0012 INTER·COMPANY tOG COMMENTS:

Project Manager: Project: 4",QOS1070i Chesepeake Shale Project Report Type: 8 Standard Report

Cl!ent: 490- TestAmetica Nashville

WO_RK LOCATION: .. 16 TestAmerica Connecticut

200$-12-03

2008-12-11

2\:08-12·22

- ..

------~------------------------~--------------~----------= SMP#: CLIE.t!IJP.~ NRL0012-01

SAMPL{i COMMENTS.

METHOD: ZZ

EXTMi!IlQ.tt 88

!-:ONE NONE Archive

NO 5.-.\MPLE PREPARATIOt.J PERFORMED I OC TYPE: 01

l\3 "iPQ1AE

WATER

STAND,\!'<() T!"ST SET

Mt:;I6L. XX

SMP#: 2 v . CLIENT I.Q; NHL0012-'J1-0ISSOLVED

S,~MPLE COMMENTS·

PATE SAMPL!;Q; 20081201 M;\lR[>,;.: I WATER

METHOD. ZZ

EXTRACTIQ" 88

NONE NONE Archive

NO SAMPLE PREPARATIOt\ PERFORMED I C)C TYPE: 01

K31PR1AC

The sample(s) listed on this form are being sent to your location for t11e specilied analysis. If you have any que~lions please contact tr;e Projc::cl Manager listed above. PLEASE RETURN THE ORIGINAL SiGNED FORM WITH THE f~EPORT ;\T THE COMPLETION OF ANALYSiS.

Thank You

TA- St. Louis Sample Receiving

RELINQUISHED BY:~---------- DATE: tz-!4/t.i __ 1/~Jt)_ ___ ._._. __ _

RECEIVED FOR U18 BY:~ ~ ------ DATE:H..:::.../l:.fLE) __ 5•- s;c_;-\"-J a --::s: f'\s.A.tLS( \~9. CoclQ(' <0\J-

PASSED R:t!.W>

SCR~13N

TestArneii<·a · St. Louis pnnted o·1 Tuesda\'. December 09, :woe 04:22 PM

Page 14 of 16

0 / )

12/18/200~

CHK00000155

() :I: /\ 0 0 0 0 0 ...... 01 CJ)

TEST AMERICA CONNECTiCUT PRESE;:(VATIVE RECORD

Job Nurnbe:: 8-i.:).\'.":) =-+ '-\ S '~\.... Client:--:'R.:"-::.--:\·'0· .. ;\.~-Sl.i\J. k:: .... -1.;-Q-0. \~ S 'S.._c;,,

Client ProjeGt: s?:\- Lou\ s (,_tt2.00s::·.':)~C\.(C:.

• i I A.djl.l!iim1mtT pH after I Preservative I Lab Number I Preservative j pH (mls) i /djustrnenl Lot Number l i • . '

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0 I A 0 0 0 0 0 ....... 01 ....,.

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TcstAmerica- ConBecticut Internal Chain-of-Custody

T~: / ftC: ~ ~--

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i Laboratory I Relinquished bv Accepted by Sample# I \ -

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TcstAmerica Form# SivU'00508.C'T

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Date Received:~.-1~J:l.~

Samplc #s: \ -- ':2...

Locations:~ '3. "{\. ~.. .

I Date Rclinquisllf..-d by Accep~)by I

._']v '--{/j) ~~~a

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ANALY'flCAL REPORT

PROJECT NO. 4100810701

Ches~peake Shale Project

- "Lot #: F8L030325

~drk Hollingsworth

TestAmerica Nashville 2960 Foster Creighton Drive

Nashv:ilJe, TN 37204

TESTAMID.UCA LABORl•TORIRS, INC .

~{//d.tltZ:d~ S~l Adam

P::-oj ec: l'ianager

January 13, 2009

TestAmerica .S::. Louis

::::

TestAmerica Laboratories, Inc.

1 o f 13

CHK00000158

Case Narrative LOT NUMBER: F8L030325

This report contains the analytical results for the sample received under chain of custody by TestAmerica St. Louis on December 3, 2008. This sample is associated with your Chesepeake Shale Project NRL0012.

The snalytical results included in tl1is report meet all applicab:e quality control procedure requiremen!s except as noted on the following page.

The test results in this report meet all NELAP requirements for parameters in which eccceditations are held by TestAmerica St. Louis . Any exceptions to NELAP requirements are noted ir the case narrati•e. The casH narrative is an integral part of this report.

All chemical analysis results are based upon sample as received, wet weight, unless noted other:;isc Ai! radioc'lemistry resu!1s are based u;JOn sample as dried and ground with :he exception of tritiUIT\, uniess reauested wet weight by the client.

Observations!Nonconformances Reference the ct1ain of custody and condition upon receipt report for any venations on receipt conditions and ternpera;ure of sarnp!es on receipt.

Gross Alpha/Beta by GFPC The Gross Alpha Beta reporting limit was not met due to a reduction of sample size attributed to the sample's r,igh residual mass. The analytical results are reported with ihe fv1DC achieved.

Affected Samples: F8L030325 (1 ). NRL0012-01

Gamma Spectroscopy- Radium • 226 & Hits • The Pb-21 0 energy, 46.54 keV, 's be!ow the lower end of the laboratory's calibration rar1ge for the applicable geometry for this sampie. The reported results for Pb-210 are estimated. • Ra-226 ·s reported based upon the Bi-214 daughter; -Due to the potentia! loss of Rn-222, the first cecay daughter of Ra226, :he results may be biased low. This is especially true it the smnpies have not been allowed to ingrow for a minimum of 21 days (to reach potential equilibrium). ·

• Tt-e Cesium 137 and Rad'um 228 by g<!rnma spec r9porting limit was not met due to the activily of the sample. The analytical results are reported with the MDC achieved.

• ~b .. 214 exhibited elevated levels of activity in the samples. The Pb-214 242 keV g<.~rnma ernissioP occurs ver; close to the Ra-224 241 keV garnrna emission. causi~·,g interfer.::nc0. T...,e analysis software assigned the observable peak to both Pb-21-1 and Ra-224 in some of the sa1np'es (did not split the peak). Based upon visual inspection of the specL·a and ott1er knowledge of i'<e samp'es (based upon the Th-228 concentration seen in the sample, f-<a-224 '.'VOUid not be expected to be seen above the calculated MDC), it was determined corre:;tion for the Pb-214 co~<lribc-tion to the peck would be necessary to properly report Ra-224 for these samples.

The activity (Sq) reported for Pb-214 for each sample was utilized to deterrr ine tho: correspo~cing peak size that would be present at the 242 keV region basec upon the Pb-214 abJndance a: that energy (7.43%). This peak size was then converted to act;vi:y (Bq) thc.: wou!d contribute to the Ra-224 peak at 241 keV based upon the Ra-224 abundance at t"'•at enE,rgy (4 .1% ). This value was then subtracted from the initial Ra-224 activity to determine the corrected Ra-224 activity. The activity concentration reported is derived from this corrected activity.

Protactinium 234m was identified at the 766 line by the software. Upon further data rev.e•.v, it~~ determined that an interference is causing the identification. The result was re-calculated using only tne 1001 '.(.eV line. The resulis are reported with this narrative.

LOT # ~8 l030 325 - ~R~0 0 12

CHK00000159

~estAme~ica S:. Louis

Affected Samples: F8l030325 (1 ): NHL0:)12-01

FB1030325-NRLJ012 3 of :::.3

CHK00000160

TestAmer~ca S~. ~ou~s

.METHODS SUMl\lARY

ANA.l.Y.TICJU.: P l'.IU\.i-1ETER :'-1li:THOD --·----.. ······-···--·--- .. -·----.... ------Gamm;1 Spectroscopy cesium-137 & Hits Gross ~ .. lpha/Beta by G~'PC

EPJI. 901.1 HOD SW846 9310 t·~OD

References:

EPP.

SKS.;,6

"EASTER!': ENVIROm.fENT~..L RADIATIO~i FACI:WITY RJ.<DI::>CHE!>liS'!"?.','

PP.OCEDURES f>IAN"JJ..L" US El?h EPA 520/s-s.;-006 AU3~i5T 1984

'!Test t-1ethods !or Evaluat.ing Solid Waste, Physical/Chen,.:..cal l'1etl:ods", Third EC.::.ticn, November 1986 an::l. its ~•?dat.es.

LOT # ?Bl030325-NRL0012

CHK00000161

~.:es-LArnerlca S~ .. Louis

SAMPLE SUMM..A.RY

F8L,03032S

SAKPLSD SAM?

----------·--------·---··----- 2~!~·-·------ :±::J;I·(E

COl

NOTE(S) -·-·····--··-··-··-"· ····-···-·······--····-·---·-----------· • 7(): "n~lyt;cal te::..:Jt.~ r;( t:1e s.a.."'O;-Ie~ l!:;;~;; ::bo\'e !:-t ;He!~n:e\1 on the fc-licw:ni p:..ges.

• r.:; c-;1·:.!-.t:.i ~n ... ~r!: pec'o r ;;;~d bel~1 ~~ L'~:~~\:w; t~ ;a.,oi~l r.)und·off erwa ir, e>.lc:.;lated reluirs.

• R~ll:':~ r.o:e::J .!~ ·N:; · \!..!!': .,.,; c.t.:.f.'•!H.'!! a:!:':- tbove lb.· s.btt:ti H:r~:L

· T~i., :er:m :r..o!:-1 ;: ":"~: t.: Jep:-odJ~ej. e~·:tpi :n ~li. with~rJ~ th: writen t.rrro\'31 of the le~m£1.:-sry •

. Rc~..:l:s f;,r !J1e r~~Howin~ r;Mt.:'r.ttt-n ;,.:r JWitl' r¢p.or . ...:>l. r,;: a dry weigh! :asis: ct-lot'. cor:o$h•iry,dee5ii)l, fil.!}';poi..1~. igd!.ltilicy, i.tyus, t>d:n,

pim fihe: tts:, pH. pcrvsi1y rre:;:-,ur::. ;::.;-::i·.dcy, reJJ~x pclenti~l. spec:i!i:; ~tl"i;:o·. ~t>t lt-.5tS, £C~Iids, solut-llicy. ::Jr.?erat'Jre. \'il«:s;:y. and wel~h~.

:2/01/08 ll:GO

5 of 13

CHK00000162

':.'·:~ s :.7\.rne.L ~- ca


Client Sam~le ID: NRL0012-0l

Lab Samp:e !D: ?3 L030325-00 l Work O~der: KJ:?J Natrix; 'dl'-..TE:H

Paramate: Ro!IU.lt

GROSS A/B BY GFPC Sio/R46 9310 l-IOD

Gros& Ba-=a

26200

5900

l:l".Jlll

Radiochemistry

Tot..ol Vnc:~;t .

Da"-P. Ccl.lacte~:

Date Recos:.ve.d: ."L:: ; .-:;:.../(8 1:::_.;; 1 2 , c;; .: '· s r 9: :.

(2 c+/-1 ~de

Prop iJa.t(l

'-~£1:.-·»:itc Do.te

5200

1900

pCi/L Batch fl 0338145 Yld. ~

2li(!0

21CO

12tUJ/09 :2/J6/0&

12!03/02 l2/Di/DB

------------------------·-----·-----····-··-··-· Gar~a Cs-137 & Hi~s by EPA 90l . l HOD ;..cti:1i·.un 22i {i\SSI.L"ne'! -'!0 ec;.:oilib:icr. w/ !h-2~!?;

Actin.iult 220 %0

c:.t~!l".u th Zll e.~ '!h-·2:-:7 ... ;(: r,.:

a::.s;nuth 222 1~0 0

Bi:!i:muth 214 6780

Ce!;.u..-r. U7 -~9 ·' :Se~d 21<:• -DC ~

Lead 212 C. 7 (.'

L~ad 214 6850

Potassiu:n 40 8<-C

l'.rctacti:.:.cr. 1341-1 -2 Ll

?~·<· to5CCi:Oi'J.~ 231 -70 ll

Rad.i= {226) 6780

P.ad..i.·= 228 960 Rad..·~t:.l"l 22.:: 'ast•\...."T:~s - "$~~ ()

equ i. l.1.b!:i'.lli'. w/ 'l'l1-L2i l R&di.<.;.m 224 310

Thallium :oe -o. ., v

Tho::iurn 22'~ -5(1 u '!'nor: i'l.rr. 234 -iO u

U.ran:.~l..--n 235 6!J t:

or."ln.:.urr. :JB _, .') r.;

NOTE. (S)

MDC i~ det~r.mined by ~nst-~c~ pa=~c~nc~ cnly. cold ras~lts are g~~~to~ than ~~e MDC.

·.50

~20

:.50

:70

no 28

'770

~B

00

~so

~4(1J

590

uo 120

l~ 0

c.o 2~

l50

10CC•

160

10•)i~

U ~esult is less than the sa=pie dete~t~or. li~t.

pCi/L

. •, -·

50

Bater.

ll.':

70

1:<00

J.C)

80

320

'D•)

;·e~

70

o.,c

~5C

1200

~iO

1~00

Cl/~5/09 ~!105/09

C~/05/CS Ol/CS/0~

Cl/05/C9 Cl/C5/09

Cl/05/J9 Ol/CS/09

DL/05/09 D1/D5/DI

~l/C5/DP DI/J5iC!

0J/05/0~ 01./05/~~

-cu:.-

LO~ # ?Sl030325-N~L0012 ~ ~ -: : : ...

CHK00000163

Tes::Ane.ri.ca St. ·Louis


Client Sample ID: NRL0012-0l DUP

Radiochemistry

Gamma Cr.-:37 & Hits b:: EPA 901 . 1 MOD

., .. ~~·.;i:. ~ t.~:::.::. ·.: ... Tt- -/<."7i

A~rlHlUJ:. ~29

Ces.l .ur· t 37

Radl.u.~ <226}

R.r"ldita 22B

':'l\~iilr.'! &:Z3 <a!~:t:.r:"~~$

cq~i:.~==.:.u::-. o..::' 7b-;::7;

NOTE {S}

l OOC

- H · -t; l:' t_!

f750

-;~ ~) 0

- -~ ~~ u -.; B u '' 230

:o-:· u ~s~~ u

'It: tl

osc :.OOC•

·-t (l u

35~

tl

·2~ -;

'• _.,

t~ (· 1J

., - !J

:::at.~ are 1.:-:complcto "W"l. tl1ou: ~he c:afiG r.a:.::a--;..i v~.

:1l.)C is dliite:t."lt..l.neC. by i!1::.t=u.:::cint. pe:=....-o:;;:,ar:.ce only. 3~~.ld r.aau.:. r..s ~:.:~ g:::ea:t.o~- t.r.ar; the MDC.

'total t"n.::o.rt..

(~ ,,.,-/-)

1 ~ =·

130

140

180

~:o

;?8

43:0

55

HO 2go

0.0

;:,E;')

410

130

~4C

0.0

25

140

.:9c 2100

>:;,:;

V Re.s\:.1 t: ·'-·' le!!as t ....... a..-: t:.7\~ sample detection lim.i.~.

LO~ g F81030325-NFLJ0l2

Data ::.~ol l ec ced :

l:.•c:i. t. e Pe.-; e ,;. v f: ci:

RL 10dc

::c;o:.;oa :100 : :: / 03/ :) 8 0915

?rep Dat.o

pCl./L Batch It 9005172

23G 0!./>..~~/0?

140 Ol/OS/01'

230 Ol/;:;5/~9

3\•C Jl/S!S/O:i

70 Ol/05/J:l :2 ~E 01/05/0~

500 Cl /05/(~9

?2 01/05/;)~

80 01/CS/09 ~;c Ol/0!:/~:,

0.0 o:;;o:.io~

:::s~..; o: /C5i09

70 Ol./05/09 sc .1.40 Ol/05/09

no {;l/C·S/09

0.0 Ol/05/0S

~2 01/0~/0S

;!3:.: 1.)1 /:.::t;:;g

62i Cl/~5/C2

20J 0l/C5/0S

820 J1/(:.S/C·£

An.&l:,-31.:.• n.-.t:.6

Yld %

01/0G/~9

Ol/06/09

Oi!O<'i"S

Cl/06/J9

Cl/06/09 ~·1 /OC/03

01!06/09

Cl/Of,/09

01/06/Cl!

C.:/06/0S

o:;OG.'C9

o: IOG/C9

0"-/0~/C~

01/06/09 Ol/06/C9

Ol/06/09

01./06.'09

01/0£1(::

01:'06.'09

Ol/06/C:5!

~i !•.)Si()~

; of 13

CHK00000164

METHOD ELANK REPORT

Radiochemistry

F.'Pt 03 J325

nasult

GR:::>SS A/B BY GFi?C SW846 9310 t-!-;;D

G::oss ~.lpt:a

Cross Eeti! -0.11 -o.:;;

l)

u

G~~~a Cs-l37 & Hits by EPA 901.1 MOD

.l;.Ctinit.:JC'• 22:-:' {C.SS'.ll:'lt:S aq·.::ilib:iu:r. ·~~1 :r~-221) J:.ctir..ium 228

!izmu~h 2:1 eq :t-227 B.i.smu-:.n 2:.2 Eismu-ch 2:4

! .. e~d 212

:,~ad 21.-1

?c-t.assi\.:0 10 ?totact:ir.iu.~ 234M

F:ota..:ti:1iu:r. 2.!1

P.adiUJ:t z :r~ ~as ~H,;l<'iii~S l?.;::uil.i~.::r. .: . .:ll ••• : / Th-227 : Radl.um 224

'!'ta.:..l.:.um .::2a Tl:cr!.:..u:, ~z ·;

Thotl.C..:"':\ 23.;

Urar:i~":t 2J5

NOTE (S)

-:~

O.C' u -le. -0. c 0

-4 \]

-. " u 60 ,.

c. ~ \."

G ? --·;c c ·;: ~1

i,.l

-4 \.!

- ~ Q

-1:3 \J

C: .0 : .2 u -lt

u -19 u

u

~.ata a..::o in::o11.1p:ic"";:.e W-thcu:: tl:-.Q ca.u<! na::::ative.

Toc..t!. Cneo::'"!.,

(2 cr+/-)

0.87

30

S4

17 5.3 140

17

0.0

5.:.

:c 160

E2

iCC

pCi/L

pc:.;L

!-'..OC i~ daten:l.!.n.:sd us1.og ir.s:t.z..'"'\!1!\ori.": .PD.t:-%or.o:mce on.!y 5<>lc:l ::<'.su: ts .. re grea-ter the:. "-'"~e !-!PC.

"U ... .-... "1 •• .: ... ,_,.,. 4·l-- .... - ........... - .. _,_ .. ~~~ ....... .; ...... 1..:r-..;,..

LOT ;; FB1030325-XRLG012

MJ:>C

Batch fl 8338145

3.0r:

-i.OC l.S

Bate!'\ # 9005172

l2.C

50

50

9.4

:s :6o J.C0(;

22

'l

sr 260

5:J 26J

~ld ~.

St . Loui .s

~.Aly:;i$

Dato

F9A05u000-·1723

Oi/05/~~ C:/0?/0~

01 / Q ~,~ ~ C ~ / 0$/0~

01/0~!~9 C:!OS/09 Ol ! 05/0~ c:.· o ~;o~

C: /05/0S C:tO;iQ9 G: ! 0S/!l 9 0 l / ~9 / G~

C!/05/ 0? Cl;::9/09

_ ~ / ~, s: r: :.. r. 1 : 1):·

~··

CHK00000165

Tesr.Ame:r::..ca St. Louis

Laboratory Control Sample Repor~

C'~:..ent l.::t r::::

Pa::ame~a=

GROSS A/B 3): GFPC Si>046 ~310 HOD

70.<;

3at.ch 6: S33S:..45

GROSS A/B BY GFl?C SvlS46 9310 MOD

:.;;:·css Al:;na <i S• •• ; S5.Z ~a-r.c:::"l I;: ~3)~1~5

Gaa_-nma Cs-137 & Hits !:)y J::PA 901. ~ MOt

loiOTEiSi

1' l C"• ..

:; :~ '1 ~ '.

LCT " FB1030325-NRL0012

Radiochemistry

Total. t.Jnce~t..

Lab S...:plo IO

(2 c +/-) MDC \ Yld \ Rec 0C Control

Lilllitfl.

pCi/L

pCi/L

pCi/L

6.0

E.D

1100:)

3000 ~~QC

9310 MOD

104

Anzl.ylii.:i llato: 12/05/08

9310 MOD

o.s A:iu.l~·oio !)at.e.: 12/05/00

~01.1 MOD

F8L030000-l4SC

F8L030000-l45C

F9A050000-172C

( 9\J - ll:);

(9[! 11~:

9 of :.3

CHK00000166

DUPLI~~TE EVALUATION REPORT

Clie:r: :.,ct ID :

t·1at;::: ix:

F8L;)30325. r,J/1-·~ER

Sl'.Hl'L!: Result

~ot.al

Uneart.

(2a +/-)

Gamma Cs-:37 & Hits by EPA 90l.l MOO

i':tct:.ni·J.::-. 227 !as!:~:-'7.eS -!10 5qu:..li:-,r.::.um .... ; 1';;-227; I1.ct::.niL:.n"~ 22 S 960

B11R~~t 211 eq ~h-227 -50

: .. oad 2.1~

I.ead 21:,t

Prvtacti:~:.m:1 LJ 4~

R=:.C:i ·J,Jn C22b!

-39

··430

o.: E!'~C!

84 0

-7~

-2

~adi'..!:t! 222 {assu:r.~s -sc eql.:ili.t::.:t.:~ w/ Th- 227l :::t~~!in:':'\ 22'4 310

P.sd!.u.-n 22 8

7~a:liu..rr. 2~f

Thc.ria:.~. : 34

'V ::-aniUJ."Ti 2:.;.;

Uraai:J.r.l ~3&

>50

-0.7 -50 -70

60

··70

\)

f)

u u

u u l:

lSO

120

:so

:o 770

380

.;10

lSO

0.0

120

lSO lOCO .160

lOOJ

Radiocharni.stry

Ptrf%'.tlCA'.r£ R6.aul.t

pC.i./!. 901.1 MOD

:ooo -20 60 6 "1 50

. 25

lC.! -7C -9,0

6-750

-2C

. 359

1000 -3

-2C

HO

HO

'J

a

u (.'

u

930S1n iS3::>;:lo;

GROSS A/B BY GF?:: SW846 9310 MOP

NOTE (S)

8800

l:l00

Batch !i:

3200 lf,~Q

Da.ta a:e incor.lpletc. w:lthout tho case ~a::ati.ve..

pCi/L 9310 MOD

7900

500

:'a:-.e sacr-~le-:!:

Da""::e. P.~:-:c~i;..·e<~ :

t'otal Otu:::e:t.

(2 c~/ -)

180

290

580

0.0 .;10

H~

0.0

l3~

25

H: 49~

2lC0

,90

2900

1300

Ca!.cula':.!.ens a:• fO~fo::rned !:l~~o:::a rc-.:.r.dinq .o:o A'IOJ.c! round ... of! error in cal::ulu.twd :;os--..:lts

L8T # FB1030325-NRLC012

F8L030325-001

. _.:

.:. .;

~F.!.::

H--:p-.

.;·aL0301H-C>Ol

l 0 . .... . ..

CHK00000167

FCI.:~~:;.:).~:.;

\·Uc'i ::::

Sp::.ke h!:\o· .. w t

GF.OSS A/P.. BY :;;p·pc SWS4 6 P. :':l 0 M:>D

GROSS A/B B¥ GFPC SN846 93 10 MOD

Sp::..ke F.esult

MATRIX SPIKE REPORT

Radiochemistry

Vate Sampled: na.te I~e.cei v~d:

Total Cncart. (2o+/-)

pC:./L

Sp-'.ke 'lld.

Sample Re.~ult

9310 MOD

::oc Anai"si~ Date:

pC:./L 9310 MOD

Total TJnce:rt.

(2 c +/-)

::!OE/02

Test:.F~!nerica

li/20/0S 11/25/0B

St. Louis

QC Sa::ple ZD

QC control Liruts

l:'SL030U4-001

107

F8L030l14-001

3200

-----------------------------~~~~c~··:~r~. ~~~=--~B~3~J~6~1~·~·e~--------~A~~~.a~~~Y~!~o~s~C~·a~~~e~=--~l~2~/~0~o~/~C~e~---------------------------------

113~00 105

NOT!:(£)

LOT p FHJ.0303/.:r~ -:;.:=-: r.JOD:; : .. : ::.1 of 13

CHK00000168

SENDING LABORATORY:

TestAmerica Nasr.vi!le 2960 Foster Creighton Road Nashville, TN 37204 Phone: 800-765-0980 Fax: 615-726-3404 Project Manager: Mark Hollingsworth Client: Cbesapea;.:e Energy Corporation

TestAmerlca Nashville

NRL0012

RECEIV!NG LABORATORY:

TestAmerica Sl Louis 13715 Rider Trail North Earth City, MO 63045 Phone :(314) 298-8566 Fax: (314) 298-8566 Project Location: Pennsylvania Receipt Temperature: oc Ice: Y I N

Copy/Re'cg from NRJ2373. Copy/Relog from NRJ1629. Qopy/Relog f~om NRJ1,67. Ccpy!Relog from NRJ1186. Copy/R&Iog f•o:n NRJ0705. Ccpy!Re!og from NRJ0546. Copy/Relog from NRJ0458,

Analysis Units Due Expires lnterlab Price Surch Comments

Sample 10: NRL0012-01 Water

Subcont.ac:- Gr.:~ss Alpha %

Subcont act - Gross Bota %

Subcontract- Radium (total\ %

Subcontract- Sulfur ASTM 2• %

Subcontract, Zircon·um %

Containers Supplied:

Sampled: 12101108 11;00 12/12108 08127/'. 110:00 $32.50

12/12/08 08/27/1110:00

12/12108 08i27/11 10:00

12/12106 08/27/11 ., 0:00

12112/06 08127/11 ·JO:OO

$32.50

$':60.00

$25.00

$50.00

0% sub to TA St. Louis- Meihod 9310

0% sub tc TA St. Louis- ~.1ethod 9:l10

0% ~ub to ·;·i,. St. Louis ·· MP.thod 9315

0% Method 6:J2Ci - send to St. Louis

0% Method 6020 -To St Louis r:-ota! & Dissolve::) ·

R 1 L Plastic HN03 R_1 l Plastic HN03 (AA) (AB)

R 250 mL Plastic HN03 (I)

R_250 ml Plastic HN03 (M)

R_1 L Plastic HN03 (Y)

R 1 l Plastic HN03 (Z)

~ Received 8

LOT # ?81030325-NRL00:2 12 .,_ 13

CHK00000169

leSTArnenca D§bSMHW£1

COJ\'"DITION UPON .I:<.ECEIPT FORM

c!ie~t: .-r~.irl'-"1~"---QuoteNo: ['164<.3

Test~nerica St. Louis

-- .. ,., -·-------""""'--=-' .... """'"'

~---· ____ 3~

COCiRF.A 1\o: tl-~ h.;{lJ,s.kj-CQrL 282 .

Ii;itiated By: ___ J~_f, ___ .. ___________ .. ______ Da~: pj.3+/o:::.........:'6::....__ Time:

Shipping Information 1

Shipper: :JPS DHL Courier Client . Other:------- Muitiple Packages: y

Sh:pping "1: (s):" Sample Tempe~ature (s):••

! .. 12Q3 &~l.LLc; .. :5·~_1___ 6. 1. (lx-y1,b (lJ-- 6. __ _

2. ____ ........ --- ...... ----- 7. -----·-------2. ___ _ 7. ______ _

3. ______ _ 8. ------------

3. ____ _ 8.--------4. ____ ;:....___ ___ -----

9. _________________ _ 4. ___ _ 9.

5. !0. --------·----- 5. 10. _____ _

' --~ j A:e there custody se~ls present on bo:tles?

ToiT"e.ci'i~·= AciTc;;.; ·--- ···-c Clic:nt C;;ntact ·~c.r::e· lnfonned by: C Sm;:plc.(s) prot:cssc~ ":!?. is" C Sarr:ple(s) 0:1 hold '.:r.:i ': ?roje::t M~nager.~en: Review:

Ifreiea~ed. notify: r.·/ ~ Date: ____ LG?:·b:Wr-------------

THJS FOR-~·1 MUST 6E C0f..:FL:01'E::l:>.T IHE T1MS THE ITEMS A~)3ErNG CHECKED iN. IF ANY i';EM 1~ COMPLETED BY SOti.EONE OTHER THAN THE I'Nr.IATOR, THE'! THAT ?c!l.SC~~ IS RSQUI~ED 70 A0 P:.. Y TREIR ·INITIAL AND THE. DATE NEXT TO THAT ITEM.

LOT ~ F8l030325-NRLOJ12 13 o: 13

CHK00000170

CHESAPEAKE ENERGY CORPORATION Response to USEPA Region Ill May 12, 2011 RFI on Marcellus Shale Flowback Water

············ ·· :::::::::::::::::::::::::::::::::::::§1~:~!i?.~::::::::::::: :: ::::::::::::::::::::::::::::::::~:t::::::::::::::::::::::::::::::::~i.~?.~:~;.~~~~~~~~~~~:~!ii;~~P.2B:~::::::~:::::::::::::::::::::::::t::~Y.s?.~~1~9.::::l::::Ef.;:::l Summit Environmental Services-327741 1 774 Pike Road, Johnstown, PA 15909 1 Cambria 1 PA

........ ::::::::::::~~Y.::§:6:~f.9Y.::§:~:~!~:~~;.§:Q:9.~~?::::::::::::::::::::::::J:::::::::::::::::::::::::::::::::~:9..:~:~:~::?.9.:~:~~~;::!?.:~I(~:~;::]XI~:~~9.:::::::::::::::::::::::::::::::··.··········· ................... , ............. . ......... g.~D!~~.1 .. §.~Y.!E9D.~~~.!~!~~?..~.~-~?. ........... ......... .. .i ............................ !:.9. .. ~.'?.~ .. ~}§~! .. P..~r.~.~E~.~.~E£kY.Y.Y. ... ?.~ .. 1.9.?. ............ ...... ....... ... : ......... : .. :.~.~::-: ........ ; .... :.: .. : .. .. .......... .9..~Y.!?D.\~D .. !.~~Y.~!r.!~~::?.~~~9.~ .......................... L .......... ?.~.?. .. ~.'?.Y. .. ~~~-~!.9.~!!!P. .. B2~~l .. ~.'?.~9.~D!9.~~ .... ~ ... ?.§?.9.~ ........... l.~.'?.!:!2~9.~.\!~.l,..Y.Y.Y. ...

.................... ~!).~E9.Y. .. 9.9.!).~r.~.~~!?E~:~.?..?..?.~.~ ........................... L .. ..................... ~.~9.9 .. AY.!.~!\!?D .. YY.~Y. ..... ~Ei.9.9.~P.9.r.!~ .. ~ ... ?.§~~9 ........................ l... .. t!.~r.r.\~.~n ..... j ... Y.Y.Y. ... ............................. t! .. ~ .. t! .. EltQ!~.P..~.~~J~.~.?..~?.?.~ ........................... L ................................ P..9. .. ~.~~ .. ~1.~~ .. §.e~!:!!?.~.r .... Y.Y.Y. ... ?.P.?.!.~ .................................. l.. ..... B.~~!:!~ ....... L.Y.Y.Y. ...

..... t!~~9 .. !::l.~.~.H~9 .. §.t .. Q!~.P..'?..~~!:~.~-~.~~?. ................... L .............................. P..C?. .. ~2~ ... 1.~.9.9.~ .. ~~~.~ .. h~~~ .. w.Y. ... ?.~.~.?..~ .............................. .l.. ...... ~~.~.i.~ ........ L.Y.Y.Y. ... ............................ !5 .. ~ .. !':! .. 9..~n!r.~.~~.iD.9::~?.~J.~.?. ........................... ,l.. ................................. P..9. .. ~9.~.?.Q!.z .. ~.l.~y.i.~~ .... ~ ... ?..?.9.!.~.............................. · · · · · · · · ·

RE!!!.i.~.~!.~ .. ~!:!Y.!r.~!.!.r:!).~.~.~~.!.I..r~!:!~.P..~.r:HB.sD.~.~.?.1.9.~~ .. .L .............................. P..9. .. ~.'?.~.?.9.9.~ .. ~r.!g9.~.P..'?..~· ... w.Y. ... ?.~.~~.9. ............................... L ... ~.:::~:.:.~~.~:.: ..... ;. Select Tanks-327707 i 7994 S. Pleasants Hwv. St. Mary's, WV 26170 i ·

CHK00000171

CHESAPEAKE ENERGY CORPORATION Response to USEPA Region Ill May 12,2011 RFI on Marcellus Shale Flowback Water

USEPA Note: Chesapeake has waived any claim of confidentiality for this document, per email from M. Annstrong, Esq., dated 7/19/2011.

CONFIDENTIAL

CHK00000172


, .......................... .:=:::::~:::~:·~~··;::·;:::;:·:!::::::··:::·:·;"''""'"''"''''''''""''~.: .. : .... j .................................................................................................................... j ......... :::.:·:·:·· ... ::":':":':""'f"j ............... ~ .................................. ~ ........................................ i .......................................... .J

USEPANote: Chesapeake has waived any claim of

CONFIDENTIAL

CHK00000173

confidentiality for this document, per email from M. Annstrong, Esq., dated 711912011.


USEPANote: Chesapeake has waived any claim of confidentiality for this document, per email from M. Armstrong, Esq., dated 711912011.

CONFIDENTIAL

CHK00000174

bracewell new york jason b. &giuliani washington, … · &giuliani may 26,2011 texas new...

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