certificate of analysis · accreditation # 97338 11711 hermitage road, suite #5, little rock, ar...

Accreditation # 97338

11711 HERMITAGE ROAD, SUITE #5,LITTLE ROCK, AR 72211

LICENSE #: BL157155

CERTIFICATE OF ANALYSIS

Brandon ThorntonPharm D. Co-Owner & CEODate: 10/11/2019

The following results relate only to the samples tested and forthe specific tests conducted. Steep Hill grants permission to

reproduce this document in full only.

© 2019 STEEP HILL, INC. ALL RIGHTS RESERVED

CERTIFICATE #: AR74177REVISION #: AR74177.1

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Sample Name: 1000 mg Full Spectrum Drops

Steep Hill ID: AR74177

Batch ID: 07.10.19.D1M7.10F

State ID:

Sample Type: Tincture

Date Received: 10/1/2019

Date Reported: 10/11/2019

Pkg. Volume: 30 mL

# of Servings: 30

Density: 1.023 g/mL

Customer: New Age Hemp LLC

4931 Central Ave

Hot Springs, AR 71913

Total THC Total CBD

0.167 % 3.3 %

1.67 mg/g 33 mg/g

1.71 mg/mL 34 mg/mL

51 mg/pkg 1006 mg/pkg

1.71 mg/serv 34 mg/serv

Cannabinoid Results – Standard Potency 10/11/2019Standard potency analysis utilizing Ultra High Performance Liquid Chromatography(UHPLC; SOP-068-AR)Analyte % mg/g mg/mL mg/pkg mg/serv LOD mg/g LOQ mg/g

CBD 3.3 33 34 1006 34 0.0111 0.037

CBDA ND ND ND ND ND 0.0110 0.037

THC 0.154 1.54 1.57 47 1.57 0.0124 0.041

THCA 0.0150 0.150 0.153 4.6 0.153 0.0053 0.0175

Total 3.4 34 35 1058 35

Cannabinoid Results – Extended Cannabinoids NTExtended cannabinoid analysis utilizing Ultra High Performance Liquid Chromatography(UHPLC; SOP-068-AR)

Analyte % mg/g mg/mL mg/pkg mg/serv LOD mg/g LOQ mg/g

CBC NT NT NT NT NT NT NT

CBD NT NT NT NT NT NT NT

CBDA NT NT NT NT NT NT NT

CBDV NT NT NT NT NT NT NT

CBG NT NT NT NT NT NT NT

CBGA NT NT NT NT NT NT NT

CBN NT NT NT NT NT NT NT

THC NT NT NT NT NT NT NT

∆8-THC NT NT NT NT NT NT NT

THCA NT NT NT NT NT NT NT

THCV NT NT NT NT NT NT NT

Total NT NT NT NT NT NT NT

Moisture Results NTMoisture content analysis utilizing Moisture Balance (MB; SOP-055-AR)

Analyte %

Moisture NT

Water Activity Results NTWater activity analysis utilizing Water Activity Meter (WAM; SOP-059-AR) - Limit units: Aw

Analyte Pass/Fail Aw Limit

Water Activity NT NT

ND: Not DetectedNT: Not TestedLOQ: Limit of QuantitationLOD: Limit of Detection



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Residual Pesticides Results Pass 10/2/2019Residual pesticide analysis utilizing Liquid and Gas Chromatography – Mass Spectrometry (LC-MSMS + GC-MSMS;SOP-070-AR + SOP-073-AR) - Limit units: ug/g = ppmAnalyte Pass/Fail µg/g Limit LOD µg/g LOQ µg/g Analyte Pass/Fail µg/g Limit LOD µg/g LOQ µg/g

Abamectin Pass ND 0.5 0.165 0.55 Imazalil Pass ND 0.2 0.021 0.071

Acephate Pass ND 0.4 0.0129 0.043 Imidacloprid Pass ND 0.4 0.0100 0.033

Acequinocyl Pass ND 2 0.184 0.61 Kresoxim-methyl Pass ND 0.4 0.0089 0.030

Acetamiprid Pass ND 0.2 0.0130 0.043 Malathion Pass ND 0.2 0.0062 0.021

Aldicarb Pass ND 0.4 0.083 0.28 Metalaxyl Pass ND 0.2 0.0091 0.030

Azoxystrobin Pass ND 0.2 0.0117 0.039 Methiocarb Pass ND 0.2 0.0087 0.029

Bifenazate Pass ND 0.2 0.0081 0.027 Methomyl Pass ND 0.4 0.0131 0.044

Bifenthrin Pass ND 0.2 0.066 0.22 Methyl Parathion Pass ND 0.2 0.0146 0.043

Boscalid Pass ND 0.4 0.021 0.069 MGK-264 Pass ND 0.2 0.00194 0.0049

Carbaryl Pass ND 0.2 0.0078 0.026 Myclobutanil Pass ND 0.2 0.0110 0.037

Carbofuran Pass ND 0.2 0.0092 0.030 Naled Pass ND 0.5 0.0196 0.065

Chlorantraniliprole Pass ND 0.2 0.0143 0.048 Oxamyl Pass ND 1 0.0185 0.062

Chlorfenapyr Pass ND 1 0.0146 0.043 Paclobutrazol Pass ND 0.4 0.0155 0.052

Chlorpyrifos Pass ND 0.2 0.0132 0.044 Permethrins Pass ND 0.2 0.0136 0.040

Clofentezine Pass ND 0.2 0.0183 0.061 Phosmet Pass ND 0.2 0.0137 0.046

Cyfluthrin Pass ND 1 0.022 0.065 Piperonyl Butoxide Pass ND 2 0.0090 0.030

Cypermethrin Pass ND 1 0.022 0.067 Prallethrin Pass ND 0.2 0.030 0.099

Daminozide Pass ND 1 0.027 0.089 Propiconazole Pass ND 0.4 0.0064 0.021

Diazinon Pass ND 0.1 0.0095 0.032 Propoxur Pass ND 0.2 0.0070 0.023

DDVP (Dichlorvos) Pass ND 0.2 0.0125 0.042 Pyrethrins Pass ND 1 0.0099 0.033

Dimethoate Pass ND 0.2 0.0131 0.044 Pyridaben Pass ND 0.2 0.0150 0.050

Ethoprophos Pass ND 0.2 0.0127 0.042 Spinosad Pass ND 0.2 0.0170 0.057

Etofenprox Pass ND 0.4 0.0180 0.060 Spiromesifen Pass ND 0.2 0.0147 0.049

Etoxazole Pass ND 0.2 0.0145 0.048 Spirotetramat Pass ND 0.2 0.0072 0.024

Fenoxycarb Pass ND 0.2 0.0115 0.038 Spiroxamine Pass ND 0.4 0.022 0.073

Fenpyroximate Pass ND 0.4 0.0093 0.031 Tebuconazole Pass ND 0.4 0.0065 0.022

Fipronil Pass ND 0.4 0.0180 0.060 Thiacloprid Pass ND 0.2 0.0076 0.025

Flonicamid Pass ND 1 0.023 0.077 Thiamethoxam Pass ND 0.2 0.0076 0.025

Fludioxonil Pass ND 0.4 0.022 0.073 Trifloxystrobin Pass ND 0.2 0.0094 0.031

Hexythiazox Pass ND 1 0.0096 0.032

Microbial Impurities Results Pass 10/2/2019Microbiological screening utilizing 3M Petrifilm (SOP-700-AR) - Limit units:CFU/gAnalyte Pass/Fail Result Limit LOQ

Coliform Pass ND Not Detected in 1 gram

General E. coli NT NT NT NT

Heavy Metals Results Pass 10/3/2019Heavy metals analysis utilizing Inductively Coupled Plasma MassSpectrometry (ICP-MS; SOP-072-AR) - Limit units: µg/kg

Analyte Pass/Fail µg/kg Limit LOD µg/kg LOQ µg/kg

Arsenic Pass ND 200 1.58 5.3

Cadmium Pass 1.85 200 0.52 1.72

Lead Pass < LOQ 500 1.37 4.6

Mercury Pass < LOQ 100 0.85 2.8

Terpenoid Results - Standard Terpenes NTStandard terpene analysis utilizing Gas Chromatography – MassSpectrometry (GC-MS; SOP-069-AR)Analyte % mg/g mg/mL LOD mg/g LOQ mg/g

Caryophyllene Oxide NT NT NT NT NT

β-Caryophyllene NT NT NT NT NT

α-Humulene NT NT NT NT NT

Limonene NT NT NT NT NT

Linalool NT NT NT NT NT

β-Myrcene NT NT NT NT NT

α-Pinene NT NT NT NT NT

β-Pinene NT NT NT NT NT

Terpinolene NT NT NT NT NT

Total NT NT NT NT NT



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Terpenoid Results - Extended Terpenes NTExtended terpene analysis utilizing Gas Chromatography – Mass Spectrometry (GC-MS; SOP-069-AR)Analyte % mg/g mg/mL LOD mg/g LOQ mg/g Analyte % mg/g mg/mL LOD mg/g LOQ mg/g

α-Bisabolol NT NT NT NT NT Linalool NT NT NT NT NT

endo-Borneol NT NT NT NT NT Menthol NT NT NT NT NT

Camphene NT NT NT NT NT β-Myrcene NT NT NT NT NT

Camphor NT NT NT NT NT Nerol NT NT NT NT NT

3-Carene NT NT NT NT NT cis-Nerolidol NT NT NT NT NT

Caryophyllene Oxide NT NT NT NT NT trans-Nerolidol NT NT NT NT NT

β-Caryophyllene NT NT NT NT NT cis-β-Ocimene NT NT NT NT NT

α-Cedrene NT NT NT NT NT trans-β-Ocimene NT NT NT NT NT

Cedrol NT NT NT NT NT α-Phellandrene NT NT NT NT NT

Eucalyptol NT NT NT NT NT α-Pinene NT NT NT NT NT

β-Farnesene NT NT NT NT NT β-Pinene NT NT NT NT NT

Fenchol NT NT NT NT NT Pulegone NT NT NT NT NT

Fenchone NT NT NT NT NT Sabinene NT NT NT NT NT

Geraniol NT NT NT NT NT Sabinene Hydrate NT NT NT NT NT

Geranyl Acetate NT NT NT NT NT α-Terpinene NT NT NT NT NT

Guaiol NT NT NT NT NT γ-Terpinene NT NT NT NT NT

α-Humulene NT NT NT NT NT Terpineol NT NT NT NT NT

Isoborneol NT NT NT NT NT Terpinolene NT NT NT NT NT

Isopulegol NT NT NT NT NT Valencene NT NT NT NT NT

Limonene NT NT NT NT NT Total NT NT NT NT NT

Residual Solvents Results Pass 10/3/2019Residual solvents and processing chemicals analysis utilizing Headspace Gas Chromatography – Mass Spectrometry (HS-GC-MS; SOP-010-AR) - Limitunits: µg/g

Analyte Pass/Fail µg/g Limit LOD µg/g LOQ µg/g Analyte Pass/Fail µg/g Limit LOD µg/g LOQ µg/g

1-Butanol Pass ND 5000 14.4 48 Dimethyl Sulfoxide Pass ND 5000 12.5 42

1-Pentanol Pass ND 5000 24 80 Ethanol Pass ND 5000 17.5 58

1-Propanol Pass ND 5000 36 120 Ethyl Acetate Pass ND 5000 6.3 21

1,2-Dimethoxyethane Pass ND 100 19.3 64 Ethyl Ether Pass ND 5000 2.2 7.4

1,4-Dioxane Pass ND 380 18.7 62 Ethylene Glycol Pass ND 620 2.1 6.9

2-Butanol Pass ND 5000 18.3 61 Ethylene Oxide Pass ND 50 1.45 4.8

2-Butanone Pass ND 5000 10.1 34 Heptane Pass ND 5000 8.0 27

2-Ethoxyethanol Pass ND 160 13.5 45 n-Hexane Pass ND 290 2.3 7.7

2-Methylbutane Pass ND 5000 1.73 5.8 Isopropyl Acetate Pass ND 5000 10.9 36

2-Methylpentane Pass ND 290 2.1 6.9 Methanol Pass ND 3000 7.8 26

2-Propanol (IPA) Pass < LOQ 5000 26 83 Methylpropane Pass ND 5000 2.1 7.0

2,2-Dimethylbutane Pass ND 290 3.9 12.9 N,N-Dimethylacetamide Pass ND 1090 14.6 49

2,3-Dimethylbutane Pass ND 290 1.68 5.6 N,N-Dimethylfromamide Pass ND 880 19.8 66

3-Methylpentane Pass ND 290 2.1 7.1 Pentane Pass ND 5000 1.83 6.1

Acetone Pass ND 5000 40 135 Propane Pass < LOQ 5000 2.1 6.9

Acetonitrile Pass ND 410 16.4 49 Pyridine Pass ND 200 12.1 40

Benzene Pass ND 2 0.37 1.23 Sulfolane Pass ND 160 7.3 24

Butane Pass ND 5000 1.65 5.5 Tetrahydrofuran Pass ND 720 8.5 28

Cumene Pass ND 70 7.2 24 Toluene Pass ND 890 19.0 63

Cyclohexane Pass ND 3880 4.4 14.6 Xylenes Pass ND 2170 26 87

Dichloromethane Pass ND 600 1.85 6.2

certificate of analysis · accreditation # 97338 11711 hermitage road, suite #5, little rock, ar...

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