certiﬁcate of analysis€¦ · cannabinoid proﬁle test result-analysis method :sop.t.40.020,...

Certificate of AnalysisARNICA CBD MUSCLE RUB JARHarvest/Lot ID: # 91343 19210Batch#: 91343 19210

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Sky Organics CBD16591 Germaine Dr Delray BeachFL, USA 33446(786) [email protected]

SAMPLE:DA90809010-001Sample is BELOW 0.3% THC

Ordered: 08/08/19 Sampled:08/08/19Completed: 08/15/19 Expires: 08/15/20

Image Safety

Pesticides - TestedMicrobials - PassedMycotoxins - PassedHeavy Metals - PassedTerpenes - NOT TestedResidual-Solvents - PassedFilth - PassedWater Activity - NOT TestedMoisture - NOT Tested

Cannabinoids

0.00%Total THC

0.534%Total CBD

0.00 mgTHC/Container

304.38 mgCBD/Container

CannabinoidsAnalyte Weight(%) mg/gD9-THC ND ND

THCA ND ND

CBD 0.534 5.340

CBDA ND ND

CBN ND ND

CBDV ND ND

D8-THC ND ND

THCV ND ND

CBG ND ND

CBGA ND ND

CBC ND ND

TOTAL THC ND ND

TOTAL CBD 0.534 5.340

ND ND 0.534 ND ND ND ND ND ND ND ND ND 0.534D9-THC THCa CBD CBDa CBN CBDV D8-THC THCV CBG CBGa CBC Total THC Total CBD

4131 SW 47th AVENUE SUITE1408DAVIE, FL [email protected] ___________________

Jorge SegredoLab Director

State License # n/aISO Accreditation #97164

This report shall not be reproduced, unless in its entirety, without written approval from EVIO Labs. This report is an EVIO Labs certification. The results relate only to the material or product analyzed.Test results are confidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batch material may vary depending on sampling error. IC=In-control QCparameter, NC=Non-controlled QC parameter, ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) and Limit Of Quantitation (LoQ) are termsused to describe the smallest concentration that can be reliably measured by an analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholds forhuman safety for consumption and/or inhalation.


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Pesticides LOQ Action Level Units ResultDIMETHOATE 0.01 0.05 ppm NDABAMECTIN B1A 0.02 0.1 ppm NDPENTACHLORONITROBENZENE 0.01 0.2 ppm NDMETHYL PARATHION 0.05 0.2 ppm NDCYFLUTHRIN 0.05 1 ppm NDCIS-PERMETHRIN 0.05 0.1 ppm NDACEPHATE 0.01 0.1 ppm NDDIMETHOMORPH 0.005 0.05 ppm NDETHOPROPHOS 0.01 0.05 ppm NDACEQUINOCYL 0.05 0.1 ppm NDACETAMIPRID 0.01 0.05 ppm NDETOFENPROX 0.01 0.05 ppm NDALDICARB 0.02 0.05 ppm NDETOXAZOLE 0.01 0.05 ppm NDAZOXYSTROBIN 0.01 0.05 ppm NDFENHEXAMID 0.01 0.1 ppm NDBIFENAZATE 0.01 0.1 ppm NDFENOXYCARB 0.01 0.05 ppm NDFENPYROXIMATE 0.01 0.5 ppm 0.091BIFENTHRIN 0.01 0.1 ppm NDCARBARYL 0.01 ppm NDFIPRONIL 0.02 0.05 ppm NDFLONICAMID 0.01 0.4 ppm NDCARBOFURAN 0.01 ppm NDCHLORANTRANILIPROLE 0.01 ppm NDFLUDIOXONIL 0.01 0.1 ppm NDHEXYTHIAZOX 0.01 0.25 ppm 0.022CHLORFENAPYR 0.01 0.05 ppm NDIMAZALIL 0.01 0.05 ppm NDCHLORPYRIFOS 0.01 0.1 ppm 0.072IMIDACLOPRID 0.01 0.1 ppm NDCLOFENTEZINE 0.01 0.2 ppm NDKRESOXIM-METHYL 0.01 0.1 ppm ND

Pesticides LOQ ActionLevel

Units Result

COUMAPHOS 0.005 0.05 ppm 0.171MALATHION 0.01 0.05 ppm NDCYPERMETHRIN 0.02 0.5 ppm NDDAMINOZIDE 0.02 0.5 ppm NDMETALAXYL 0.01 0.05 ppm NDDICHLORVOS 0.05 0.1 ppm NDMETHIOCARB 0.01 0.05 ppm NDMETHOMYL 0.01 0.1 ppm NDDIAZANON 0.01 0.05 ppm NDMEVINPHOS 0.01 0.05 ppm NDMYCLOBUTANIL 0.01 0.1 ppm NDNALED 0.01 0.25 ppm NDOXAMYL 0.01 0.25 ppm NDPACLOBUTRAZOL 0.01 0.05 ppm NDTRANS-PERMETHRIN 0.05 0.1 ppm NDPHOSMET 0.01 0.1 ppm NDPIPERONYL BUTOXIDE 0.01 3 ppm 0.080PRALLETHRIN 0.05 0.1 ppm NDPROPICONAZOLE 0.01 0.1 ppm NDPROPOXUR 0.01 0.1 ppm NDPYRETHRINS (PYRETHRIN I) 0.01 0.5 ppm NDPYRIDABEN 0.01 0.2 ppm NDSPINOSAD (SPINOSYN A) 0.01 0.1 ppm NDSPINOSAD (SPINOSYN D) 0.01 0.1 ppm NDSPIROMESIFEN 0.01 0.1 ppm NDSPIROTETRAMAT 0.02 0.1 ppm NDSPIROXAMINE 0.01 0.05 ppm NDTEBUCONAZOLE 0.01 0.05 ppm NDTHIACLOPRID 0.01 0.05 ppm NDTHIAMETHOXAM 0.01 0.05 ppm NDTRIFLOXYSTROBIN 0.01 0.1 ppm ND






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Residual solvent Action Level(ppm) Pass/Fail Results(ppm)1,2-DICHLOROETHANE 2 Pass ND1,1-DICHLOROETHENE 8 Pass ND1,4-DIOXANE Pass ND2-BUTANOL Pass ND2-ETHOXYETHANOL Pass ND2-PROPANOL 500 Pass NDACETONE 750 Pass NDACETONITRILE 60 Pass NDBENZENE 1 Pass NDBUTANES (ISO-BUTANE) 2000 Pass NDBUTANES (N-BUTANE) 2000 Pass NDCHLOROFORM 2 Pass NDETHANOL 5000 Pass NDETHYL ACETATE 400 Pass NDCYCLOHEXANE Pass NDDICHLOROMETHANE Pass NDETHYL ETHER 500 Pass NDETHYLENE OXIDE 5 Pass NDETHYLBENZENE Pass NDHEPTANE 500 Pass NDHEXANES (2,2-DIMETHYLBUTANE) 60 Pass NDHEXANES (2,3-DIMETHYLBUTANE) 60 Pass NDHEXANES (2-METHYLPENTANE) 60 Pass NDHEXANES (3-METHYLPENTANE) 60 Pass NDISOPROPYL ACETATE Pass NDMETHALENE CHLORIDE 125 Pass NDMETHANOL 250 Pass NDN-HEXANE 60 Pass NDPENTANES (ISO-PENTANE) Pass NDPENTANES (N-PENTANE) 750 Pass NDPENTANES (NEO-PENTANE) Pass NDPROPANE 2100 Pass NDTETRAHYDROFURAN Pass NDTOLUENE 150 Pass NDTOTAL XYLENES 150 Pass NDTRICHLOROETHYLENE 25 Pass ND






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Cannabinoid Profile Test Result-Analysis Method :SOP.T.40.020, SOP.T.30.050 Analytical Batch:DA005507

Reagent LOT ID Dilution Consumables Id080919.R02 76124-662080819.R03 SFN-BX-1025

Reagent LOT ID Dilution Consumables Id080819.R02 849C4-849AK

840C6-840H

Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 for sample prep and Shimadzu High Sensitivity MethodSOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).Filth and foreign Materials-Analysis Method : Analytical Batch:DA005504

This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing waste and by-products. An SH-2B/T Stereo Microscope is use for inspection.

Mycotoxin Analysis-Analysis Method :SOP.T.30.065, SOP.T.40.065 Analytical Batch:DA005487Analyte Results Action LevelAFLATOXIN_G2 ND 0.02AFLATOXIN_G1 ND 0.02AFLATOXIN_B2 ND 0.02AFLATOXIN_B1 ND 0.02OCHRATOXIN_A ND 0.02Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using LC-MS. (Method: SOP.T.30.065 for Sample Preparation and SOP.T40.065 Procedure for Mycotoxins Quantification Using LCMS. LOQ 1.0 ppb). TotalAflatoxins (Aflotoxin B1, B2, G1, G2) must be


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Pesticide Analysis-Analysis Method:SOP.T.30.065, SOP.T.40.065 Analytical Batch :DA005486Reagent LOT/ID Dilution Consumables ID

1

Reagent LOT/ID Dilution Consumables ID

Pesticide screen is performed using LC-MS which can screen down to below single digit ppb concentrations for regulated Pesticides. Currently we analyze for 57 Pesticides. (Method: SOP.T.30.065 SamplePreparation for Pesticides Analysis via LCMSMS and SOP.T40.065 Procedure for Pesticide Quantification Using LCMS).Heavy Metals Analysis-Analysis-Method:SOP.T.40.050, SOP.T.30.052 Analytical Batch: DA005499Reagent LOT/ID Dilution Consumables ID

50

Reagent LOT/ID Dilution Consumables ID

Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – Mass Spectrometer) which can screen down to below single digit ppb concentrations for regulated heavy metals usingMethod SOP.T.30.052 Sample Preparation for Heavy Metals Analysis via ICP-MS and SOP.T.40.050 Heavy Metals Analysis via ICP-MS.Metal Result Action-LevelARSENIC 0.002 0.2CADMIUM ND 0.2LEAD ND 0.5MERCURY ND 0.1

Abbreviation:ppm=Parts Per MillionResidual SolventsAnalysis Method:SOP.T.40.032 Analytical Batch :DA005508Reagent LOT ID Dilution Consumables Id

1 00268767161040-1

Reagent LOT ID Dilution Consumables Id24151940

Residual solvents screening is performed using GC-MS which can detect below single digit ppm concentrations. Currently we analyze for 34 Residual solvents. (Method: SOP.T.30.042 Residual SolventsAnalysis via GC-MS).





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