certiﬁcate of analysis - columbia care...(method sop.t.40.043) if a pathogenic escherichia coli,...

Certificate of Analysis1000 MG CBD OIL LOT: 42719N/A Page 1 of 5

Columbia Care New York212 E 14th Street Bryant IsonCMO |Columbia Care [email protected] o: (212) 634-7100 m:(609) 240-2838NY, USA 10003(212) [email protected]

SAMPLE:DA90628009-004Sample is BELOW 0.3% THC

Ordered: 06/28/19 Sampled:06/28/19Completed: 07/02/19 Expires: 07/02/20

Image Safety

Pesticides - PassedMicrobials - PassedMycotoxins - PassedHeavy Metals - PassedTerpenes - NOT TestedResidual-Solvents - PassedFilth - PassedWater Activity - NOT TestedMoisture - NOT Tested

Cannabinoids

0.162%Total THC

3.800%Total CBD

48.60 mgTHC/Container

1142.10 mgCBD/Container

CannabinoidsAnalyte Weight(%) mg/gD9-THC 0.162 1.620

THCA ND ND

CBD 3.800 38.000

CBDA ND ND

CBN ND ND

CBDV 0.025 0.250

D8-THC ND ND

THCV ND ND

CBG 0.076 0.760

CBGA ND ND

CBC 0.125 1.250

TOTAL THC 0.162 1.620

TOTAL CBD 3.800 38.000

0.162 ND

3.800

ND ND 0.025 ND ND 0.076 ND 0.125 0.162

3.800

D9-THC THCa CBD CBDa CBN CBDV D8-THC THCV CBG CBGa CBC Total THC Total CBD

4131 SW 47th AVENUE SUITE1408DAVIE, FL [email protected] ___________________

Jorge SegredoLab Director

State License # n/aISO Accreditation #97164

This report shall not be reproduced, unless in its entirety, without written approval from EVIO Labs. This report is an EVIO Labs certification. The results relate only to the material or product analyzed.Test results are confidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batch material may vary depending on sampling error. IC=In-control QCparameter, NC=Non-controlled QC parameter, ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) and Limit Of Quantitation (LoQ) are termsused to describe the smallest concentration that can be reliably measured by an analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholds forhuman safety for consumption and/or inhalation.

Certificate of Analysis1000 MG CBD OIL LOT: 42719MN/A Page 2 of 5




Pesticides LOQ Action Level Units ResultDIMETHOATE 0.01 0.05 ppm NDABAMECTIN B1A 0.02 0.1 ppm NDPENTACHLORONITROBENZENE 0.01 0.2 ppm NDMETHYL PARATHION 0.05 0.2 PPM NDCYFLUTHRIN 0.05 1 PPM NDACEPHATE 0.01 0.1 ppm NDDIMETHOMORPH 0.005 0.05 ppm NDETHOPROPHOS 0.01 0.05 ppm NDACEQUINOCYL 0.05 0.1 ppm NDACETAMIPRID 0.01 0.05 ppm NDETOFENPROX 0.01 0.05 ppm NDALDICARB 0.02 0.05 ppm NDETOXAZOLE 0.01 0.05 ppm NDAZOXYSTROBIN 0.01 0.05 ppm NDFENHEXAMID 0.01 0.1 ppm NDBIFENAZATE 0.01 0.01 ppm NDFENOXYCARB 0.01 0.05 ppm NDFENPYROXIMATE 0.01 0.5 ppm NDBIFENTHRIN 0.01 0.1 ppm NDCARBARYL 0.01 ppm NDFIPRONIL 0.02 0.05 ppm NDFLONICAMID 0.01 0.4 ppm NDCARBOFURAN 0.01 ppm NDCHLORANTRANILIPROLE 0.01 ppm NDFLUDIOXONIL 0.01 0.1 ppm NDHEXYTHIAZOX 0.01 0.25 ppm NDCHLORFENAPYR 0.01 0.05 ppm NDIMAZALIL 0.01 0.05 ppm NDCHLORPYRIFOS 0.01 0.1 ppm NDIMIDACLOPRID 0.01 0.1 ppm NDCLOFENTEZINE 0.01 0.2 ppm NDKRESOXIM-METHYL 0.01 0.1 ppm NDCOUMAPHOS 0.005 0.05 ppm ND

Pesticides LOQ ActionLevel

Units Result

MALATHION 0.01 0.05 ppm NDCYPERMETHRIN 0.02 0.5 ppm NDDAMINOZIDE 0.02 0.5 ppm NDMETALAXYL 0.01 0.05 ppm NDDICHLORVOS 0.05 0.1 ppm NDMETHIOCARB 0.01 0.05 ppm NDMETHOMYL 0.01 0.1 ppm NDDIAZANON 0.01 0.05 ppm NDMEVINPHOS 0.01 0.05 ppm NDMYCLOBUTANIL 0.01 0.1 ppm NDNALED 0.01 0.25 ppm NDOXAMYL 0.01 0.25 ppm NDPACLOBUTRAZOL 0.01 0.05 ppm NDPERMETHRINS 0.05 0.1 ppm NDPHOSMET 0.01 0.1 ppm NDPIPERONYL BUTOXIDE 0.01 3 ppm NDPRALLETHRIN 0.05 0.1 ppm NDPROPICONAZOLE 0.01 0.1 ppm NDPROPOXUR 0.01 0.1 ppm NDPYRETHRINS (PYRETHRIN I) 0.01 0.5 ppm NDPYRIDABEN 0.01 0.2 ppm NDSPINOSAD (SPINOSYN A) 0.01 0.1 ppm NDSPINOSAD (SPINOSYN D) 0.01 0.1 ppm NDSPIROMESIFEN 0.01 0.1 ppm NDSPIROTETRAMAT 0.02 0.1 ppm NDSPIROXAMINE 0.01 0.05 ppm NDTEBUCONAZOLE 0.01 0.05 ppm NDTHIACLOPRID 0.01 0.05 ppm NDTHIAMETHOXAM 0.01 0.05 ppm NDTRIFLOXYSTROBIN 0.01 0.1 ppm ND









Residual solvent Action Level(ppm) Pass/Fail Results(ppm)1,2-DICHLOROETHANE 2 Pass ND1,2-DICHLOROETHENE 8 Pass ND1,4-DIOXANE Pass ND2-BUTANOL Pass ND2-ETHOXYETHANOL Pass ND2-PROPANOL 500 Pass NDACETONE 750 Pass NDACETONITRILE 60 Pass NDBENZENE 1 Pass NDBUTANES (ISO-BUTANE) 2000 Pass NDBUTANES (N-BUTANE) Pass NDCHLOROFORM 2 Pass NDCYCLOHEXANE Pass NDETHANOL 5000 Pass NDETHYL ACETATE 400 Pass NDDICHLOROMETHANE Pass NDETHYL ETHER 500 Pass NDETHYLENE OXIDE 5 Pass NDETHYLBENZENE Pass NDHEPTANE 500 Pass NDHEXANES (2,2-DIMETHYLBUTANE) 60 Pass NDHEXANES (2,3-DIMETHYLBUTANE) 60 Pass NDHEXANES (2-METHYLPENTANE) 60 Pass NDHEXANES (3-METHYLPENTANE) 60 Pass NDISOPROPYL ACETATE Pass NDMETHALENE CHLORIDE 125 Pass NDMETHANOL 250 Pass NDN-HEXANE Pass NDPENTANES (ISO-PENTANE) Pass NDPENTANES (N-PENTANE) 750 Pass NDPENTANES (NEO-PENTANE) Pass NDPROPANE 100 Pass NDTETRAHYDROFURAN Pass NDTOLUENE 150 Pass NDTOTAL XYLENES 150 Pass NDTRICHLOROETHYLENE 25 Pass ND









Cannabinoid Profile Test Result-Analysis Method :SOP.T.40.020, SOP.T.30.050 Analytical Batch:DA004383

Reagent LOT ID Dilution Consumables Id062719.R03 10 181205062819.R08 1929V5454

Reagent LOT ID Dilution Consumables Id062719.R02 849C4-849AK

910C6 - 910H

Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 for sample prep and Shimadzu High Sensitivity MethodSOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).

Filth and foreign Materials-Analysis Method :SOP.T.40.013This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing waste and by-products. An SH-2B/T Stereo Microscope is use for inspection.

Mycotoxin Analysis-Analysis Method :SOP.T.30.065, SOP.T.40.065 Analytical Batch:DA004380Analyte Results Action LevelAFLATOXIN_G2 ND 0.02AFLATOXIN_G1 ND 0.02AFLATOXIN_B2 ND 0.02AFLATOXIN_B1 ND 0.02OCHRATOXIN_A ND 0.02Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using LC-MS. (Method: SOP.T.30.065 for Sample Preparation and SOP.T40.065 Procedure for Mycotoxins Quantification Using LCMS. LOQ 1.0 ppb). TotalAflatoxins (Aflotoxin B1, B2, G1, G2) must be





Pesticide Analysis-Analysis Method:SOP.T.30.065, SOP.T.40.065 Analytical Batch :DA004379Reagent LOT/ID Dilution Consumables ID062819.R01 1 181205

Reagent LOT/ID Dilution Consumables ID280653964

Pesticide screen is performed using LC-MS which can screen down to below single digit ppb concentrations for regulated Pesticides. Currently we analyze for 57 Pesticides. (Method: SOP.T.30.065 SamplePreparation for Pesticides Analysis via LCMSMS and SOP.T40.065 Procedure for Pesticide Quantification Using LCMS).Heavy Metals Analysis-Analysis-Method:SOP.T.40.050, SOP.T.30.052 Analytical Batch: DA004378Reagent LOT/ID Dilution Consumables ID

50

Reagent LOT/ID Dilution Consumables ID

Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – Mass Spectrometer) which can screen down to below single digit ppb concentrations for regulated heavy metals usingMethod SOP.T.30.052 Sample Preparation for Heavy Metals Analysis via ICP-MS and SOP.T.40.050 Heavy Metals Analysis via ICP-MS.Metal Result Action-LevelARSENIC ND 0.2CADMIUM ND 0.2LEAD 0.038 0.5MERCURY ND 0.1

Abbreviation:ppm=Parts Per MillionResidual SolventsAnalysis Method:SOP.T.40.032 Analytical Batch :DA004390Reagent LOT ID Dilution Consumables Id

1

Reagent LOT ID Dilution Consumables Id

Residual solvents screening is performed using GC-MS which can detect below single digit ppm concentrations. Currently we analyze for 34 Residual solvents. (Method: SOP.T.30.042 Residual SolventsAnalysis via GC-MS).





certiﬁcate of analysis - columbia care...(method sop.t.40.043) if a pathogenic escherichia coli,...

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