cimarron corpora tion letter of transmittaldepartment's march 30 letter concerning the cover...

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CIMARRON CORPORA TION LETTER OF TRANSMITTAL I DATE: March 3,2004 TO: U.S. Nuclear Regulatory Commission Document Control Desk Washington, D.C. 20555 FROM: Quality Assurance Coordinator Cimarron Corporation P.O. BOX 315 Crescent, OK 73028 o Frst Class Mail E/Overnight-Fed Ex o Second Day-Fed Ex o Internal 0 UniShippers 0 Other O Overnight-UPS o Second Day Air-UPS iCOPY DATE DEiSC' . RIPTIO -- N; I March 3, 2004 Letter and Attachments to U.S. Nuclear Regulatory Commission re: Docket No. 70-925; License No. SNM-928 License Condition 22(c) These are transmitted as checked below: O For Approval 0 Approved as submitted I For your use O As requested 0 Returned for corrections 0 Return corrected prints o Disapproved 0 For review and comment 0 Controlled copy REMARKS:The above item(s) is for your use. Please sign and return transmittal letter. NOTE: SIGNATURE: ) ACKNOWLEDGMENT OF RECEIPT PLEASE RETURN ONE SIGNED COPV TO SENDER I HAVE RECEIVED TI1E DOCUMENTS IDENTIFIED ABOVE AND TIE PRIOR REVISIONS OF THESE HAVE BEEN DESTROYED N/A VOIDED N/A - PRINTED NAME OF RECIPIENT: | SIGNATURE OF RECIPIENT: l DATE RECEIVED: l If enclosures are not noted, kindly notify Cimarron Corporation at once. )JIlb's 0 (

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Page 1: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

CIMARRON CORPORA TION LETTER OF TRANSMITTAL

I DATE: March 3,2004

TO: U.S. Nuclear Regulatory CommissionDocument Control DeskWashington, D.C. 20555

FROM: Quality Assurance CoordinatorCimarron CorporationP.O. BOX 315Crescent, OK 73028

o Frst Class MailE/Overnight-Fed Exo Second Day-Fed Ex

o Internal0 UniShippers0 Other

O Overnight-UPSo Second Day Air-UPS

iCOPY DATE DEiSC' . RIPTIO --N;

I March 3, 2004 Letter and Attachments to U.S. Nuclear Regulatory Commission re: DocketNo. 70-925; License No. SNM-928 License Condition 22(c)

These are transmitted as checked below:O For Approval 0 Approved as submitted I For your useO As requested 0 Returned for corrections 0 Return corrected printso Disapproved 0 For review and comment 0 Controlled copy

REMARKS:The above item(s) is for your use. Please sign and return transmittal letter.

NOTE:

SIGNATURE: )

ACKNOWLEDGMENT OF RECEIPT PLEASE RETURN ONE SIGNED COPV TO SENDER

I HAVE RECEIVED TI1E DOCUMENTS IDENTIFIED ABOVE AND TIE PRIOR REVISIONS OF THESE HAVEBEEN DESTROYED N/A VOIDED N/A -

PRINTED NAME OF RECIPIENT: |

SIGNATURE OF RECIPIENT: l

DATE RECEIVED: l

If enclosures are not noted, kindly notify Cimarron Corporation at once.

)JIlb's 0 (

Page 2: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

CIMARRON CORPORATIONP.O. BOX315 * CRESCENT.OK73028

March 3, 2004

Mr. Kenneth KalmanLow-Level Waste & Decommissioning Projects BranchDivision of Waste ManagementOffice of Nuclear Materials Safety & SafeguardsU. S. Nuclear Regulatory CommissionWashington, D.C. 20555

Re: Docket No. 70-925; License No. SNM-928License Condition 22(c)

Dear Mr. Kalman:

In August 2003, Cimarron Corporation (Cimarron) submitted a license amendmentrequest proposing the deletion of License Condition 22. Condition 22(c), which wasissued with License Amendment #9 (dated December 30, 1992) reads, "CimarronCorporation (Kerr-McGee) shall provide to the Oklahoma State Department ofHealth whatever information is required to satisfy state requirements on thepresence/absence of potentially toxic substances or any other nonradioactiveconstituents of the fill and cover soil." NRC recently requested documentationdemonstrating that Cimarron has fulfilled this license condition.

On February 25, 1993, Cimarron met with Oklahoma State Department of Health(OSDH) personnel to discuss metal concentration data that had been provided toOSDH. OSDH required additional sampling and analysis for organic compounds.This meeting and the data needs were documented by OSDH in a letter dated March30, 1992 (it is erroneously dated 1992).

On April 7, 1993, Cimarron personnel met with OSDH to identify the specificsamples needed, and to develop a list of the compounds for which they would beanalyzed. Cimarron documented that meeting in a letter dated April 8, 1993.

Page 3: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

The samples were collected on May 4, 1993 and submitted to Armstrong ForensicLaboratory for analysis. Cimarron reported the results of the sampling and analysis,and submitted the laboratory analytical report to OSDH on June 1, 1993.

Cimarron has enclosed a copy of all three letters and the laboratory data package,which demonstrate that license condition 22(c) has been fulfilled. If you havequestions or comments, please call me at 405-642-5152.

Sincerely,

Jeff LuxProject Manager

xc: D. Blair Spitzberg, NRC Region IVDavid Cates, Oklahoma Department of Environmental Quality

Attachments

Page 4: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

.ciomas D. Peace, Ph.D. OKLP.. _OMA STATE < so

- Cjommissioner DEPARTMENT OF HEALTH .

Board of Health 1000 NE TENTH - >John B. Carmichael, D.D.S Gordon H. Deckert, M.D. OKLAHOMA CITY, OKPresident Dan H. Fieker, D.O. 73117-1299 EmEarnest D. Martin, R.Ph. Walter Scott Mason, IIIVice President Lee W. PadenBurdge F. Green, M.D. R. Brent Smith, M.D. A.' QUAL O-PR7W:4;Y _ECY=ERSecretary-Treasurer Orange Welbom, M.D.

March 30, 1992

Dr. Ed Still, D.V.M.Vice President and DirectorEnvironment and Health Management Division, Kerr McGeeKerr McGee CenterOklahoma City, OK 73125

Dear Dr. Still:

This letter is to confirm the Solid Waste Management Service's (SWMS) position regardingthe soil you intend to use for the closure of the "Burial Ground" and the "Old SanitaryLagoon" at the Cimarron Corporation's Cresent, Oklahoma site that we discussed in ourFebruary 25th meeting at the Oklahoma State Department of Health.

The Solid Waste Management Service's involvement in this closure is primarily to satisfyparagraph C of Condition 22 of Cimarron Corporation's Nuclear Regulatory License #SNM-928. The selection of an undeveloped area of the Cresent site as a source of cover materialfor the closure of its "Burial Ground:" and "Old Sanitary Lagoon" greatly simplifys the SolidWaste Management Service's task of determining "the presence/absence of potentially toxicsubstances or any other nonradioactive constituents of the fill and cover soil."

The metals analysis of the proposed "fill and cover soils" that Kerr McGee has providedindicates that the metals content of the proposed "fill and cover soils" are not contaminatedwith quantity of metals that would be considered toxic. However, the Solid WasteManagement Service would like a more detailed description of the location where the "filland cover soils" will be obtained and the activities which have occurred in that area in thepast to verify the validity of this conclusion.

The anylisis that has been provided to the SWMS to date, does not fully adress the potentialfor the presence of organic constituants in the "burial ground", the "old sanitary lagoon", orin the proposed "fill and cover soils". The SWMS requests that you obtain representativesamples of the soil currently left in the "burial ground" and "old sanitary lagoon" areas aswell as your proposed "fill and cover soils" and preform a GC/MS scan to determine if thereare any potentialy toxic constituants present.

tW rer..:..2 -Uane,

Page 5: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

Dr. Ed StillVice President and DirectorEnvironment and Health Management Division, Kerr McGeeKerr McGee CenterOklahoma City, OK 73125Page 2

Upon receipt of the above mentioned anylisis and a description of the methedology utilizedto collect the representative samples requested, we will determine if it is possible for theSolid Waste Management Service to indicate to the NRC that there are no potentialy toxicconstituents present in the proposed " fill and cover soils" or the areas to be filled.

If you have any questions or if we may be of any assistance in this matter please feel freeto contact Glen Wheat of my staff at (405) 271-7038.

Sincerely,

R. Fenton Rood, ChiefSolid Waste Management Service

cc: pJ. L Kegi, Cimarron CorporationGary L Ammon, Oklahoma State Department of HealthTommy Stambeck, RS #287, Logan County Health Dept.Bill Warden, RS, District Sanitarian

C0330303

Page 6: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

rorK KERR-MCGEE CORPOR-ATIN* - KERR-McGES CENTER . OKLAHOMA Cird. OKLAHOMA 73125

ENVIRCNMEIT AtJD "EALT H MANAGEMENT CIVISICN

EDWIN . STILL. CVMVICE PqESICENT ANO DlRECrCA

April 8, 1993

Mr. Michael S. HoutsSolid Waste Management ServiceOklahoma State Department of Health1000 NE 10thOklahoma City, OK 73117-1299

Re: Cimarron Facility, Crescent, Oklahoma

Dear Mr. Houts:

Thank you for meeting with me on April 7 to discuss theDepartment's March 30 letter concerning the cover and fill of theformer sanitary lagoons and waste burial area at the Cimarronfacility. As summarized below, the additional information theOklahoma State Department of Health (Department) would likeCimarron to provide was clarified and acceptable sampling andanalytical procedures were defined.

Additional Information

The Department acknowledges adequate sampling has been done todemonstrate the absence of radiological and most non-radiologicalsubstances of potential concern. The Department notes, however,that the extensive sampling and analytical program has not focusedon certain organic substances, such as hydrocarbons and solvents.Thus, before backfilling the structures, the Department would liketo have soil from the bottom of the lagoons and the burial trencharea analyzed for volatile constituents that were or may have beenused in the facility operation. The backfill material also will beanalyzed for these constituents. Cimarron agrees to analyze soilfrom these locations and provide the results to the Department.

Samplino and Analysis

A random number table will be used to select aidintersections in the lagoons and burial area at which aliauots ofsoil will be removed and comDosited to provide separate samples foreach.. The area from which necessary backfill material will beobtained will also be sampled similarly.

The three comoosite samples will be taken in accordance withEPA approved Procedures as described in 'PA SW-846. The sampleswill be submitted so a laboratory meeting QA/QC requirements as

Page 7: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

Michael S. H-outsRage 2p-.ril 8, 1.993

specified by EPA Method 8240. The analysis will be performed usingthe TCLP and Method 8240 for volatile organics. The attached liststhe substances that will be analyzed.

Cimarron will inform the Department at least a day in advanceof collecting the samples. The Department may at its conveniencehave a representative present when the samples are obtained.However, a Department representative is not a requirement.

I hope this accurately reflects our discussion and that thesubstances listed will provide you with the necessary information.

Sincerely,

ETS:lld

Attachment

Page 8: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

SOIL ANALYSIS LISTCIMARRON FACILITY

Sample Type:

Soil Composite

Analytical Methods:

TCLP-ZHE (EPA Method 1311)GC/MS (EPA Method 8240)

Substances to be Analyzed:

RCRA Volatile Organics

BenzeneCarbon tetrachlorideChlorobenzeneChloroform1,4-Dichlorobenzene1,2-Dichloroethane1,1-DichloroethyleneMethyl ethyl ketoneTetrachloroethyleneTrichloroethyleneVinyl Chloride

Page 9: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

KERR-MCGEE COR P.n -4 lI-VKERR-McGEE CENTER * OKLAHOMA CITY. OKLAHOMA 73125

ENVIRONMENT AND HEALTH MANAGEME'NT DIVISION

EOWIN T. STILL DVM

VICE PRESIDENT AND DIRECTOR June 1, 1993

Mr. Michael S. HoutsSolid Waste Management ServiceOklahoma State Department of Health1000 NE 10thOklahoma City, OK 73117-1299

Re: Cimarron Facility, Crescent, Oklahoma

Dear Mr. Houts:

Cimarron Corporation has completed the soil testing discussedwith you on April 7, 1993 and summarized in my letter to you onApril 8, 1993. The results of the analyses are attached for thesamples from the two lagoons, the former waste burial area and thedesignated backfill material area.

The analyses show listed RCRA volatile organics are notdetectable. In addition, priority pollutant volatile organics arenot detectable, with the exception of 1,1,1- Trichloroethane, whichwas indicated in three of the four samples at 0.03 to 0.05 partsper million (ppm).

To our knowledge, 1,1,1- Trichloroethane was not used in theprocessing activities previously carried out at the Cimarronfacility. The very low levels noted also are far below the U.S.Environmental Protection Agency's lifetime health advisory level of0.2 ppm for drinking water.

In light of these data, we plan to proceed with backfillingthe lagoons and former waste burial area in accordance with theU.S. Nuclear Regulatory Commission license amendment previouslyprovided to you.

Please contact me at your early convenience if you havequestions about this matter.

Sincerely,

ETS:11dX

Attachment

Page 10: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

A Armstronrg Forensic Ca6cratory, Inc.330 Loch'n Green Trail * Arlington, Texas 76012 * 817.275-2691 .A.T. Armstrong, Ph.D.

Certified Chemist, AICFellow AAFS

Fellow AICIAAI

AIHAACSMay 19, 1993

Mr. J. L. KeginCimarron CorporationP.O. Box 315Crescent, OK 73028

Site: Cimarron Facility

LABORATORY REPORT:

Received: May 5, 1993Submitted: 4 Soils

93EN1393

Sample No: 1Client No: Burial Ground [-Sample Type: SoilTCLP-ZHE Extraction: EPA Method 1311

PRIORITY POLLUTANT VOLATILE ORGANICS: EPA Method 8010

ResultspDpb (ua/1

Det Limitnnb (ua/l IOrqanic ComDound

BenzeneBromodichloromethaneBromoformBromomethaneCarbon tetrachlorideChlorobenzeneChloroethane2-Chloroethylvinyl etherChloroformChloromethaneDibromochloromethane

bdlbdlbdlbdlbdlbdlbdlbdlbdlbdlbdl

0.23.7.

10.3.0.2

10.1.8.

10.4.

bdl - below detection limits

Page 11: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

'Armstrong Forensic Laboratory, Inc.Report 93EN1393Page 2

Sample No: 1Client No: Burial GroundSample Type: SoilTCLP-ZHE Extraction: EPA Method 1311

PRIORITY POLLUTANT VOLATILE ORGANICS: EPA Method 8010 (continued)

Results Det LimitOrganic Compound ppb( pq/l) ppb(pq/1)

1,2-Dichlorobenzene bdl 0.31,3-Dichlorobenzene bdl 0.31,4-Dichlorobenzene bdl 0.31,1-Dichloroethane bdl 0.61,2-Dichloroethane bdl 0.91,1-Dichloroethylene bdl 0.41,2-Dichloroethylene-trans bdl 0.21,2-Dichloropropane bdl 0.41,3-Dichloropropene-cis bdl 0.61,3-Dichloropropene-trans bdl 1.Ethyl benzene bdl 0.2Methylene chloride bdl 1.1,1,2,2-Tetrachloroethane bdl 2.Tetrachloroethylene bdl 1.Toluene bdl 0.21,1,1-Trichloroethane bdl. 0.91,1,2-Trichloroethane bdl 1.Trichloroethylene bdl 0.8Trichlorofluoromethane bdl 3.Vinyl chloride bdl 10.

bdl - below detection limits

------------------------------------------------------------------------------------

Page 12: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

..Armstrong Forensic Laboratory, Inc.Report 93EN1393Page 3

Sample No: 2Client ID: DA Dirt PileSample Type: SoilTCLP-ZHE Extraction: EPA Method 1311

PRIORITY POLLUTANT VOLATILE ORGANICS: EPA Method 8010

Results Det LimitOrganic Compound ppb(pg/l) ppb(pg/l)

Benzene bdl 0.2Bromodichloromethane bdl 3.Bromoform bdl 7.Bromomethane bdl 10.Carbon tetrachloride bdl 3.Chlorobenzene bdl 0.2Chloroethane bdl 10.2-Chloroethylvinyl ether bdl 1.Chloroform bdl 8.Chloromethane bdl 10.Dibromochloromethane bdl 4.1,2-Dichlorobenzene bdl 0.3

1,3-Dichlorobenzene bdl 0.31,4-Dichlorobenzene bdl 0.31,1-Dichloroethane bdl 0.61,2-Dichloroethane bdl 0.91,1-Dichloroethylene bdl 0.41,2-Dichloroethylene-trans bdl 0.21,2-Dichloropropane bdl 0.41,3-Dichloropropene-cis bdl 0.61,3-Dichloropropene-trans bdl 1.Ethyl benzene bdl 0.2Methylene chloride bdl 1.1,1,2,2-Tetrachloroethane bdl 2.Tetrachloroethylene bdl 1.Toluene bdl 0.21,1,1-Trichloroethane 45.4 0.91,1,2-Trichloroethane bdl 1.Trichloroethylene bdl 0.8Trichlorofluoromethane bdl 3.Vinyl chloride bdl 10.

bdl - below detection limits

------------------------------------------------------------------------------------

Page 13: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

..Armstrong Forensic Laboratory, Inc.Report 93EN1393Page 4

Sample No: 3Client ID: East Sanitary LagoonSample Type: SoilTCLP-ZHE Extraction: EPA Method 1311

PRIORITY POLLUTANT VOLATILE ORGANICS: EPA Method 8010

Results Det LimitOrcanic Comuound ppb(yg/l) ppb(pg/l)

Benzene bdl 0.2Bromodichloromethane bdl 3.Bromoform bdl 7.Bromomethane bdl 10.Carbon tetrachloride bdl 3.Chlorobenzene bdl 0.2Chloroethane bdl 10.2-Chloroethylvinyl ether bdl 1.Chloroform bdl 8.Chloromethane bdl 10.Dibromochloromethane bdl 4.1,2-Dichlorobenzene bdl 0.31,3-Dichlorobenzene bdl 0.31,4-Dichlorobenzene bdl 0.31,l-Dichloroethane bdl 0.61,2-Dichloroethane bdl 0.9l,l-Dichloroethylene bdl 0.41,2-Dichloroethylene-trans bdl 0.21,2-Dichloropropane bdl 0.41,3-Dichloropropene-cis bdl 0.61,3-Dichloropropene-trans bdl 1.Ethyl benzene bdl 0.2Methylene chloride bdl 1.1,1,2,2-Tetrachloroethane bdl 2.Tetrachloroethylene bdl 1.Toluene bdl 0.21,1,1-Trichloroethane 32.6 0.91,1,2-Trichloroethane bdl 1.Trichloroethylene bdl 0.8Trichlorofluoromethane bdl 3.Vinyl chloride bdl 10.

bdl - below detection limits

------------------------------------------------------------------------------------

Page 14: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

-Armstrong Forensic Laboratory, Inc.Report 53EN1393Page 5

Sample No: 4Client ID: West Sanitary LagoonSample Type: SoilTCLP-ZHE Extraction: EPA Method 1311

PRIORITY POLLUTANT VOLATILE ORGANICS: EPA Method 8010

Results Det LimitOrganic Compound ppb(pg/1) ppb(p2/1)

Benzene bdl 0.2Bromodichloromethane bdl 3.Bromoform bdl 7.Bromomethane bdl 10.Carbon tetrachloride bdl 3.Chlorobenzene bdl 0.2Chloroethane bdl 10.2-chloroethylvinyl ether bdl 1.Chloroform bdl 8.Chloromethane bdl 10.Dibromochloromethane bdl 4.1,2-Dichlorobenzene bdl 0.31,3-Dichlorobenzene bdl 0.31,4-Dichlorobenzene bdl 0.31,1-Dichloroethane bdl 0.61,2-Dichloroethane bdl 0.91,1-Dichloroethylene bdl 0.41,2-Dichloroethylene-trans bdl 0.21,2-Dichloropropane bdl 0.41,3-Dichloropropene-cis bdl 0.61,3-Dichloropropene-trans bdl 1.Ethyl benzene bdl 0.2Methylene chloride bdl 1.1,1,2,2-Tetrachloroethane bdl 2.Tetrachloroethylene bdl 1.Toluene bdl 0.21,1,1-Trichloroethane 34.4 0.91,1,2-Trichloroethane bdl 1.Trichloroethylene bdl 0.8Trichlorofluoromethane bdl 3.Vinyl chloride bdl 10.

bdl - below detection limits

Jo i/M. Corn, MSSenkor ChemistAIY'A Accreditation: 363

Page 15: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

ARMSTRONG FORENSIC LABORATORY, INC.

QA/QC ATTACHMENT REPORT: 93EN1393

PRIORITY POLLUTANT VOLATILE ORGANICS: EPA Method 8010

Technician:Extraction Date:

Date Analyzed:QC Date:

QC Sample Number:

EB5/6/935/14/935/19/93VOC-1

Extraction Method:Matrix Spike Recovery:Sample Duplicate RPD:

Method Blank:Blank Spike Recovery:

EPA 1311100. %

0.0 %0.009 Pig

100. %

BlankLaOrcanic Compound

BenzeneBromodichloromethaneBromoformBromomethaneCarbon tetrachlorideChlorobenzeneChloroethane2-Chloroethylvinyl etherChloroformChloromethaneDibromochloromethane1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-Dichlorobenzene1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethylene1,2-Dichloroethylene-trans1,2-Dichloropropane1,3-Dichloropropene-cis1,3-Dichloropropene-transEthyl benzeneMethylene chloride1,1,2,2-TetrachloroethaneTetrachloroethyleneToluene1,1,1-Trichloroethane1,1,2-TrichloroethaneTrichloroethyleneTrichlorofluoromethaneVinyl chloride

<0. 001<0.015<0.035<0.005<0.015<0.001<0.050<0.005<0.040<0.050<0.020<0.002<0.002<0.002<0.003<0.005<0.002<0.001<0.002<0.003<0.005<0. 001<0.005<0.010<0.005<0. 001<0.005<0.005<0.004<0.015<0.050

Page 16: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

ZIrmstrong Forensic Cagoratory, Inc.330 Loch'n Green Trail - Arlington, Texas 76012 * 817-275.2691

May 19, 1993A.T. Armstrong, Ph.D.

Certified Chemist, AICFellow AAFS

Fellow AICIAAI

AIHAACS

Mr. J. L. KeginCimarron CorporationP.O. Box 315Crescent, OK 73028

Site: Cimarron Facility Received: May 5, 1993Submitted: 4 Soils

LABORATORY REPORT: 93EN1393-2

Sample No: 1Client ID: Burial GroundSample Type: SoilTCLP-ZHE Extraction: EPA Method 1311

RCRA VOLATILE ORGANICS: EPA Method 8010

Resultsnnhil"/l I

Det. LimitTnnhhitryl/1 IOrqanic Comnound

----- *--------- w_ ,y

Benzene

Carbon tetrachloride

Chlorobenzene

Chloroform

1,4-Dichlorobenzene

1,2-Dichloroethane

1,1-Dichloroethylene

Methyl ethyl ketone

Tetrachloroethylene

Trichloroethylene

Vinyl chloride

bdl

bdl

bdl

bdl

bdl

bdl

bdl

bdl

bdl

bdl

bdl

0.2

23.

0.2

8.

0.3

0.9

0.4

1.7

1.

0.8

10.

bdl - below detection limits

____________________________________________________________________________________

Page 17: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

* Armstrong Forensic Laboratory, Inc.Report 93EN1393-2Page 2

____________________________________________________________________________________

Sample No:Client ID:Sample Type:TCLP-ZHE Extraction:

RCRA VOLATILE ORGANICS

2DA Dirt PileSoilEPA Method 1311

;: EPA Method 8010

ResultsOrganic Compound ppb(p/l)

Det. Limitppb (qll)

Benzene

Carbon tetrachloride

Chlorobenzene

Chloroform

1,4-Dichlorobenzene

1,2-Dichloroethane

1,1-Dichloroethylene

Methyl ethyl ketone

Tetrachloroethylene

Trichloroethylene

Vinyl chloride

bdl

bdl

bdl

bdl

bdl

bdl

bdl

bdl

bdl

bdl

bdl

0.2

3.

0.2

8.

0.3

0.9

0.4

1.7

1.

0.8

10.

bdl - below detection limits

Page 18: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

* Armstrong Forensic Laboratory, Inc.Report'93EN1393-2Page 3

____________________________________________________________________________________

Sample No:Client ID:Sample Type:TCLP-ZHE Extraction:

RCRA VOLATILE ORGANICS

3East Sanitary LagoonSoilEPA Method 1311

,: EPA Method 8010

ResultsnDh ( tir/1 I

Det. Limittn~nb It irr/I iOrganic Compound

,- _ - -I

Benzene

Carbon tetrachloride

Chlorobenzene

Chloroform

1,4-Dichlorobenzene

1,2-Dichloroethane

1,l-Dichloroethylene

Methyl ethyl ketone

Tetrachloroethylene

Trichloroethylene

Vinyl chloride

bdl

bdl

bdl

bdl

bdl

bdl

bdl

bdl

bdl

bdl

bdl

0.2

3.

0.2

8.

0.3

0.9

0.4

1.7

1.

0.8

10.

bdl - below detection limits

___________________________________________________________________________________

Page 19: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

- Armstrong Forensic Laboratory, Inc.Report '93EN1393-2Page 4

____________________________________________________________________________________

Sample No:Client ID:Sample Type:TCLP-ZHE Extraction:

RCRA VOLATILE ORGANICS

4West Sanitary LagoonSoilEPA Method 1311

,: EPA Method 8010

Results

Orqanic Compound ppb (u/l)

Det. Limit

ppb(uq/)

Benzene

Carbon tetrachloride

Chlorobenzene

chloroform

1,4-Dichlorobenzene

1,2-Dichloroethane

1,1-Dichloroethylene

Methyl ethyl ketone

Tetrachloroethylene

Trichloroethylene

Vinyl chloride

bdl - below detection limits

Jo ri;M. Corn, MSSe'ni'or ChemistArfA Accreditation: 363

bdl

bdl

bdl

bdl

bdl

bdl

bdl

bdl

bdl

bdl

bdl

0.2

3.

0.2

8.

0.3

0.9

0.4

1.7

1.

0.8

10.

Page 20: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

ARMSTRONG FORENSIC LABORATORY, INC.

QA/QC ATTACHMENT REPORT: 93EN1393-2

RCRA VOLATILE ORGANICS: EPA Method 8010

Technician:Extraction Date:

Date Analyzed:QC Date:

QC Sample Number:

EB5/6/935/14/935/19/93VOC-1

Extraction Method:Matrix Spike Recovery:Sample Duplicate RPD:

Method Blank:Blank Spike Recovery:

EPA 1311100. %

0.0 %0.009 pg

100. %

BlankuaOraanic Compound

BenzeneCarbon tetrachlorideChlorobenzeneChloroform1,4-Dichlorobenzene1,2-Dichloroethane1,1-DichloroethyleneMethyl ethyl ketoneTetrachloroethyleneTrichloroethyleneVinyl chloride

<0.001<0.015<0.001<0.040<0.002<0.005<0.002<0.050<0.005<0.004<0.050

Page 21: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

93EN1393INVOICE

* **** ********** **

No: 017979

Date of Invoice: May 19, 1993

To: Mr. J. L. KeginCimarron CorporationP.O. Box 315Crescent, OK 73028405-282-2935

From: Armstrong Forensic Laboratory, Inc.330 Loch'n Green TrailArlington, Texas 76012TIN: 75-175-9877

Site: Cimarron FacilityLab File: 93EN1393

Laboratory Analysis

TCLP Priority Pollutant VOCs

Cost/Sample

$240

NoSamples

4 $960.00

Total Invoice $960.00

Client Copy

Account balance is due upon receipt of invoice.

Page 22: CIMARRON CORPORA TION LETTER OF TRANSMITTALDepartment's March 30 letter concerning the cover and fill of the former sanitary lagoons and waste burial area at the Cimarron facility

INVOICE93EN1393-2

No: 018024

Date of Invoice: May 19, 1993

To: Mr. J. L. KeginCimarron CorporationP.O. Box 315Crescent, OK 73028405-282-2935

From: Armstrong Forensic Laboratory, Inc.330 Loch'n Green TrailArlington, Texas 76012TIN: 75-175-9877

Site: Cimarron FacilityLab File: 93EN1393-2

Laboratory AnalysisCost/Sample

NoSamples

TCLP RCRA VOCs

Total Invoice

$200 4 $800.00

$800.00

Client Copy

Account balance is due upon receipt of invoice.