clean air engineeringcae project no: 5815-1 summary introduction clean air engineering was...

Clean Air Engineering

REPORT ONVOLATILE ORGANICS TESTING

Performed for:VERTAC SITE CONTRACTORS

Conducted at:VERTAC CHEMICAL CORPORATION

SUPERFUND SITEJACKSONVILLE, ARKANSAS

CAE Project No: 5815-1December 1 1 , 1 9 9 1

VOLUME I

VERTAC SITE CONTRACTORSCAE Project No: 5815-1

CONTENTS

VOLUME I

1. SUMMARYINTRODUCTIONSUMMARY OF TEST RESULTS

2. DESCRIPTION OF INSTALLATION

3. SUMMARY OF PROCEDURESSAMPLING PROCEDURESANALYTICAL PROCEDURESQUALITY CONTROL PROCEDURES

4. COMMENTS

5. APPENDIXNOMENCLATURESAMPLE CALCULATIONSPARAMETERSCALIBRATION DATAFIELD DATACHAIN OF CUSTODY

VOLUME II

5. APPENDIXLABORATORY DATA


SUMMARY

INTRODUCTION

Clean Air Engineering was contracted by Vertac Site Contractors to determinethe levels of volatile organics emissions at the Vertac Chemical CorporationSuperfund site located in Jacksonville, Arkansas in support of their trial bum.

The testing took place at the Stack on October 10, 1991. Coordinating the fieldtesting were;

R. Apa - Vertac Site ContractorsP. Schwindt - US EPAM. McCorkle • State of Arkansas Department of Pollution

Control and EcologyC. Young - Independent Quality Assurance AdvisorJ. Chapman - Clean Air Engineering

SUMMARY OF TEST RESULTS

The test conditions and results of analysis are presented in Tables 1 A through1 C on pages 1 -2 through 1 -4.

To the best of our knowledge, the data presented in this report are accurateand complete.

Respectfully submitted,

CLEAN AIR ENGINEERING

- ' " ' . "h,'-^^ .A/;;-^•''/ ' •• /7 • / /Kimberiy Kempt L'Manager, Technical Communications

John ChapmanVice PresidentResearch and Development


SW-846 Method 00Volatile OrganlcsStack

Run No.1

Date (1991)Start Time (approx.)Stop Time (approx.)

Gas Conditions2

Temperature (°F)Moisture (volume %)Oz (dry voluma %)COz (dry volume %)

Volumetric Flow Rate2acfmdscim

Volatile Organic*

Chloromethane ^o ^ug/dscmppbIb/hr

Bromomethane iug/dscmppbIb/hr

Methylene Chloride '''•,.--:ug/dscmppbIb/hr -^.•.

Acetone 1 '•'•ug/dscmppbIb/hr

1,1-Dichloroethene 7 "ug/dscmppbIb/hr \ . . • > • - -

Chloroform " •ug/dscmppbIb/hr

"* Run 3 samples were2 The gas conditions a

sampling train.ND indicates that the o

the average.

lary of Test Re

1

October 102:19 PM2:29 PM

20143.01 1 . 17.9

28,10011 ,940

^1065.0

5074.76E-02

(<0,205) ND(<0)

(<8.16E-07)..••

1717.5486

1.32E-06

310.2129

2.00E-03^'A

21.75

2.52E-05

386.978

3.14E-05

not analyzed, seend volumetric flow

ompound was not

suits

2

October 10 C2:48 PM3:08 PM

20143.01 1 . 17.9

26,10011,940

218.9104

9.79E-03

5.61

4.63E-06

288.482

6.10E-06

9.44

1.02E-05

2.31

8.00E-08

78.516

6.64E-07

Comments, page 41.rate data was obtained f

detected. Non-detected

4

>ctober 103:56 PM4:16 PM

20143.01 1 . 17.9

26,10011,940

254.1121

1.14E-02

7.22

6.81 E-06

238.968

6.41 E-06

12.85

1.15E-05

3.61

1.72E-07

106.521

1.43E-06

rom the concurrent

values were not inc

Average

20143.01 1 . 17.9

26.10011,940

512.7244

2.29E-02

6.42

5.72E-06

748.3212

4.61 E-06

110 .846

6.72E-04

9.22

8.48E-06

190.638

1.12E-05

MM5

;luded in


SW-846 Method 0030Volatile OrganlcsStackRun No.1

Date (1991)Start Time (approx.)Stop Time (approx.)

pas Condltions2Temperature ("F)Moisture (volume %)Oz (dry volume %)COz (dry volume %)

Volumetric Flow Rate2

actmdscfm

Volatile Organic*Trichlorofluoromethane '

ug/dscmppbIb/hr

2-Butanona "- ' , .>• .pg/dscmppbIb/hr

1.1,1-Trlchloroethane v^;ug/dscmppbIb/hr

Carbon Tetrachloride ''^r'ug/dscmppbIb/hr

Bromdichloromethaneug/dscmppbIb/hr

Trichloroethene / r ' - . t / v^ug/dscm v

ppbIb/hr

1 Run 3 samples were no2 The gas conditions and

y of Test Re

i


20143.01 1 . 17.9

26,10011,940

J" .' l'*-

47.98

6.94E-05

64.11 0

1.15E-05•'\

105.419

2.53 E-05i

67.21 1

2.65E-05

256.938

6.47E-05

3.8 E1

3.64E-06

t analyzed, seevolumetric flow

suits

2


20143.01 1 . 17.9

26,10011,940

14.22

4.17E-06

(<0.154) ND(<0)

(<8.18E-09)

44.58

2.57E-08

52.18

8.68E-06

79.212 •

1.55E-05

4.01

1.19E-06

Comments, page 41.rate data was obtaine

4


20143.01 1 . 17.9

26,10011,940

5.51

2.19E-06

(<0.570) ND(<0)

(<1.17E-08)

29.25

6.24 E-08

1 1 1 . 817

1.22E-05

115.217

4.82E-05

4.61

1.97E-06

d from the concurrc

Average

20143.01 1 . 17.9

26,10011,940

22.54

2.52E-05

64.110

1.15E-05

59.71 1

8.47E-06

77.012

1.58E-05

150.422

4.28E-05

4.11

2.27 E-06

Bnt MM5

1-3

r-0'.—r i00

sampling train.NO indicates that the compound was not detected. Non-detected values were not included in

the average.

•

3

1


20143.01 1 . 17.9

26,10011,940

39.85

5.64E-07

5.12

7.62E-07

(<0.205) ND(<0)

(<3.92E-09)

2.7 E0

2.04E-09

13.74

1.37E-07

(<0.102) ND(<0)

(<5.25E-09)

! analyzed, see. volumetric flow

suits

2


20143.01 1 . 17.9

26,10011,940

103.512

1.55E-06

3.01

1.17E-06

129.112

1.46E-06

5.11

2.46E-06

1.8 E0

3.52E-08

3.11

2.13E-08

Comments, page 41.rate data was obtaine

4

Octobsr 103:56 PM4:16 PM

20143.01 1 . 17.9

26,10011,940

161 .219

2.75E-06

3.91

2.38E-06

192.018

2.83E-06

5.41

3.92E-06

2.2 E1

4.44E-08

2.81

2.28E-08

d from the concurrent

Average

20143.01 1 . 1

7.9

26,10011.940

101.512

1.62E-06

4.01

1.44E-06

160.51 5

2.15E-06

4.41

2.13E-06

5.92

7.21 E-08

2.91

2.21 E-08

MM5

1-4

000

m00

pound was not detected. Non-detected values were not included in


DESCRIPTION OF INSTALLATION 2-1

Vertac Site Contractors operates a transportable rotary kiln thermaldestruction unit (TDU) which is used to destroy hazardous wastes. The TDUis custom built specifically to process and destroy 2,4-Dichloropnenoxyaceticacid (2,4-D) still bottom and pesticide waste material located at the VertacChemical Corporation superfund site. The primary components include arotary kiln (primary combustion chamber), a hot cyclone, an after burner(secondary combustion chamber), a spray dryer/quench tower, fourbaghouses, a venturi/baffle plate absorber, an induced draft fan and a stack.

The testing reported in this document was performed at the Stack.

A schematic of the process is shown below.

STACKSWL1HBPCHISi


SUMMARY OF PROCEDURES

SAMPLING PROCEDURES

The sampling followed procedures as detailed in U.S. Environmental ProtectionAgency (EPA) Solid Waste Method 0030. This method can be referenced inSW-846 "Test Methods for Evaluating Solid Waste, Volume 1A: Field Manualfor Physical/Chemical Methods." This methods is titled:

• SW-846 0030 — "Volatile Organics Sampling Train."

The sampling apparatus is shown in Fig 1 on page 3-2. The samplingequipment was designed and manufactured by Nutech Inc. and Clean AirEngineering to meet U.S. EPA standards. All equipment was calibrated at theClean Air Engineering laboratory prior to shipment to the job site.

Sampling Locations

The Stack has two ports. For volatile organics sampling a single point near thecenter of the stack was sampled for 20 minutes.


Figure 1

The SW-846 Method 0030 sampling apparatus is shown.

CONDENSER

PARTICULATEFILTER THERAOCOUPLE EXHAUST


SUMMARY OF PROCEDURES (Continued)

ANALYTICAL PROCEDURES

Volatile OrganicsThe VOST tubes were analyzed according to the guidelines of SW-846Methods 8240 and 5040. The contents of the sorbent cartridges were spikedwith internal and surrogate standards and thermally desorbed with a purge gasprior to analysis. The volatile organics were separated by temperature-programmed gas chromatography and detected by mass spectrometry, whichwas used to provide both qualitative and quantitative information.

QUALITY CONTROL PROCEDURES

Quality control procedures for all aspects of field sampling; samplepreservation and holding time; reagent quality; analytical method; analysttraining and safety; and instrument cleaning, calibration and safety werefollowed. These procedures are generally consistent with EPA guidelinesdocumented in "Quality Assurance Manuals for Air Pollution MeasurementSystems," Vol 3, "Stationary Source Specific Methods" (EPA-600/4-77-027b).


COMMENTS

The Run 3 samples were not analyzed as the data was lost during analysisdue to an electrical storm.

No deviations from standard U.S. EPA testing procedures were noted.


APPENDIX

NOMENCLATURESAMPLE CALCULATIONSPARAMETERSCALIBRATION DATAFIELD DATACHAIN OF CUSTODY


NOMENCLATURE


SAMPLE CALCULATIONS

VERTAC SITE CONTRACTORSCAE Project No : 5815-1

SAMPLE CALCULATIONS - RUN 1, STACK(Note: results are taken from computer analysis)

14. Chloromethane

casern .J^f35^fq(V^)l m3 J

=(10dlD (35.31)(0.35)

=1065.0HQ

ppb ——SL—f^ss^^YioooP^I(V. ) [453,590^) I MW A PpmJ

^1) fssil Y^oo^(0.35) [453,590^) I 50.49 A PPm

=507

Ib/hr fioooiis.1F-a^——- (dscfm) (60)

(V.,.,) [453,590^)10.411

fl 000^1= ———\—!aJ——^1 • 940)(60)

(0.35)[453,590^J=4.76x10-2


PARAMETERS

VERTAC SITE CONTRACTORSCAE Project No: 5518

VOLATILE ORGANICS

LOCATION STACK

RUN NO.Date (1991)

FIELD BLANKOct10

ChloromethaneM

BromomethaneM

Methylene ChlorideW

AcetoneM

1,1-DichloroetheneM

ChloroformM

TrichlorofluoromethaneM

2-ButanoneM

1,1,1-TrichloroethaneM

Carbon Tetrachloride48

BromdichloromethaneM

TrichloroetheneM

DibromochloromethaneM

Benzene49

BromoformW

TetrachloroetheneM

TolueneM

ChlorobenzeneM

0.053

(<0.001) ND

0.034 E

0.065

(<0.001) ND

0.005 E

(<0.001) ND

0.089

(<0.001) ND

(<0.001) ND

(<0.001) ND

(<0,001) ND

(<0.001) ND

(<0.001) ND

(<0.001) ND

(<0.001) ND

0.01 O E

(<0.001) ND

ND - not detectedE - estimated

VERTAG SITE CONTRACTORSCAE Project No: 5518

VOLATILE ORGANICS

LOCATION STACK

RUN NO.*Date (1991)Start Time (approx.)Stop Time (approx.)

Pb (in. Hg)Vm (LITERS)Vm (ft3)DHYdTm

CALCULATED RESULTS

Vmstddscfm**

ChloromethaneMVUQ/dscmppbIb/hr

BromomethaneMug/dscmppbIb/hr

Methylene ChlorideMug/dscmPPbIb/hr

AcetoneUSug/dscmppbIb/hr

1,1-DichloroetheneMug/dscmppbIb/hr

ChloroformU9ug/dscmppbIb/hr

1Oct10

2:19 PM2:29 PM

30.0010.000.351.50

0.999983

0.3511,940

10.4111065.0

5074.76E-02

(<0.002) ND(<0)(<0)

(<8.16E-07)

16.7891717.5

4861.32E-06

3.032310.2

1292.00E-03

0.21221.7

52.52E-05

3.782386.9

783.14E-05

2Oct10

2:48 PM3:08 PM

30.0019.990.711.50

0.999985

0.6911,940

4.264218.9

1049.79E-03

0.1105.6

14.63E-06

5.618288.4

826.10E-06

0.1849.4

41.02E-05

0.044 E2.3

18.00E-08

1.52978.5

166.64E-07

4Oct10

3:56 PM4:16 PM

30.0020.01

0.711.75

0999991

0.6811,940

4.900254.1

1211.14E-02

0.1387.2

26.81 E-06

4.608238.9

686.41 E-06

0.24712.8

51.15E-05

0.0693.6

11.72E-07

2.054106.5

211.43E-06

AVERAGE

MW= 50.496.525512.7

2442.29E-02

MW= 94.940.124

6.42

5.72E-06MW= 84.94

9.005748.3

2124.61 E-06

MW= 58.051.154110.8

466.72E-04

MW= 96.940.108

9.22

8.48E-06MW = 119.38

2.455190.6

381.12E-05

* Run No. 3 was not analyzed. The samples were tost due to an electrical storm."The flow rate was taken from the corresponding MM5 run.ND - not detectedE - estimatedNon-detected values were not included in the average.


VOLATILE ORGANICS

LOCATION STACK

RUN NO." 1 2 4 AVERAGEDate (1991) Oct10 Oct10 Oct10Start Time (approx.) 2:19 PM 2:48 PM 3:56 PMStop Time (approx.) 2:29 PM 3:08 PM 4:16 PM


30.0010.000.351.50

0.999983

30.0019.99

0.711.50

0999985

30.0020.01

0.711.75

0.999991

CALCULATED RESULTS

Vmstd 0.35dscfrn" 11,940

0.6911,940

0.6811,940

TrichlorofluoromelhaneMug/dscmppbIb/hr

2-ButanoneMug/dscmppbIb/hr

1,1,1-TrichloroethaneMtig/dscmppbIb/hr

Carbon TetrachlorideMug/dscmppbIb/hr

BromdichloromethaneMug/dscmppbIb/hr

TrichloroetheneMug/dscmppbIb/hr

MW = 137.400.468 0.276 0.106 0.28347.9 14.2 5.5 22.5

8 2 1 46.94E-05 4.17E-06 2.19E-06 2.52E-05

MW= 148,210.627 (<0.003)ND (<0.011)ND 0.627

64.1 (<0) (<1) 64.110 (<0) (<0) 10

1.15E-05 (<8.18E-09) (<1.17E-08) 1.15E-05MW a 133.41

1.030 0.886 0.563 0.826105.4 45.5 29.2 60.0

19 8 5 1 12.53E-05 2.62E-08 6.24E-08 8.47E-06

MW = 153.820.657 1.015 2.156 1.27667.2 52.1 111 .8 77.0

1 1 8 17 122.65E-05 8.88E-06 1.22E-05 1.59E-05

MW= 163.832.511 1.543 2.221 2.092256.9 79.2 115.2 150.4

38 12 17 226.47E-05 1.55E-05 4.82E-05 4.28E-05

MW= 131.390.037 E 0.078 0.088 0.068

3.8 4.0 4.6 4.11 1 1 1

3.64E-06 1.19E-06 1.97E-06 2.27E-06

* Run No. 3 was not analyzed. The samples were tost due to an electrical storm."The flow rate was taken from the corresponding MM5 run.ND - not detectedE - estimatedNon-detected values were not included in the average.


VOLATILE ORGANICS

LOCATION STACK

RUN NO.*Date (1991)Start Time (approx.)Stop Time (approx.)


CALCULATED RESULTS

Vmstddscfrn"

DibromochloromethaneMug/dscmppbIb/hr

BenzeneWug/dscmppbIb/hr

Bromoformuglig/dscmppbIb/hr

TetrachloroetheneMug/dscmppbIb/hr

TolueneWug/dscmppbIb/hr

ChlorobenzeneMug/dscmppbIb/hr

1Oct10

2:19 PM2:29 PM

30.0010.000.351.50

0.999983

0.3511,940

0.38939.8

55.64E-07

0.0505.1

27.62E-07

(<0.002) ND(<0)(<0)

(<3,92E-09)

0.026 E2.7

02.04E-09

0.13413.7

41.37E-07

(<0.001) ND(<0)(<0)

(<5.25E-09)

2Oct10

2:48 PM3:08 PM

30.0019.99

0.711.50

0.999985

0.6911,940

2.016103.5

121.55E-06

0.0593.0

11.17E-06

2.514129.1

121.46E-06

0.0995.1

12.46E-06

0.036 E1.8

03.52E-08

0.0603.1

12.13E-08

4Oct10

3:56 PM4:16 PM

30.0020.01

0.711.75

0.999991

0.6811,940

3.108161.2

192.75E-06

0.0763.9

12.38E-06

3.703192.0

182.83E-06

0.1055.4

13.92E-06

0.042 E2.2

14.44E-08

0.0542.8

12.28E-08

* Run No. 3 was not analyzed. The samples were lost due to an electrical storm."The flow rate was taken from the corresponding MM5 run.ND-not detectedE - estimatedNon-detected values were not included in the average.

AVERAGE

MW = 208.291.838101.5

121.62E-06

MW=78.120.062

4.01

1.44E-06MW = 252.75

3.109160.5

152.15E-06

MW= 165.830.077

4.41

2.13E-06MW=92.13

0.0715.9

27.21 E-08

MW a 112.560.057

2.91

2.21 E-08

VERTAC SITE CONTRACTORSCAE Project No; 5518

VOLATILE ORGANICS

LOCATION

RUN NO.Date (1991)Start Time (approx.)Stop Time (approx.)

AUDIT CYCLINDER 470

470-1Oct10

5:08 PM5:18 PM

470-2Oct10

5:29 PM5:49 PM

470-3Oct10

5:52 PM6:02 PM

AVERAGE


30.0010.020.351.75

0.999986

30.0010.020.351.75

0.999986

30.0010.040.351,75

0.999986

CALCULATED RESULTS

Vmstd 0.34 0,34 0,35

ChloromethaneWpg/dscmppb

Vinyl ChlorideMpg/dscmppb

Methylene ChlorideWpg/dscmppb

AcetoneWpg/dscmppb

ChloroformWpg/dscmppb

TrichlorofluoromethaneWpg/dscmppb

1,1,1-Trichloroethanempg/dscmppb

Carbon Tetrachloridepgpg/dscmppb

BenzeneVQpg/dscmppb

TetrachloroetheneWpg/dscmppb

(<0.001) ND(<0.1)

(<0)

0.44645.7

18

6.709687.9

195

0.13613.9

6

1.706174.9

35

0.32533.3

6

1.178120.8

22

0.66868.5

11

0.80882.8

26

1.074110.1

16

1.308134.1

64

0.36537.4

14

6.346650.7

184

0.12012.3

5

1.656169.8

34

0.23824.4

4

0.95197.5

18

0.67268.9

11

0.81583.6

26

1.049107.6

16

1.396142.9

68

0.30331.0

12

6.338648.6

184

0.10110.3

4

1.534157.0

32

0.22523.0

4

0.57558.8

11

0.60161.5

10

0.72674.3

23

0.96598.8

14

MW= 50.490.902

9244

MW= 62.500.371

3815

MW a 84.946.464

662188

MW» 58.050.119

125MW= 119,38

1.63216734

MWs 137.400.263

275MWs 133.41

0.9019217

MW> 153.820.647

6610

MW» 78.120.783

8025

MWs 165.831.029

10515

ND - not detectedNon-detected values were not included in the average.


VOLATILE ORGANICS

LOCATION AUDIT CYCLINDER 471

RUN NO. 471-1 471-2 471-3 AVERAGEDate (1991) Oct10 Oct10 Oct10Start Time (approx.) 6:13 PM 6:33 PM 6:50 PMStop Time (approx,) 6:23 PM 6:43 PM 7:00 PM


30.0010.020.351.75

0.999984

30.0010.000.351.75

0.999984

30.0010.010.351.75

0.999984

CALCULATED RESULTS

Vmstd 0.35 0.34 0.35

Chloromethane49 1.038ug/dscm 106.1ppb 51

Methylene ChlorideHg 6.532ug/dscm 667.6ppb 189

Acetoneug 0.324ug/dscm 33.1ppb 14

1,1-Dichloroetheneug 0.484Ug/dscm 49.5ppb 12

Trichlocofluoromethaneug 0.209ug/dscm 21.4ppb 4

2-Butanonepg 0.080ug/dscm 8.2ppb 1

1.1,1-TrichtoroethaneM 0.469ug/dscm 47.9ppb 9

Toluenepg 0.440ug/dscm 45.0ppb 12

ChlorobenzeneM 0.502ug/dscm 51.3ppb 11

1.643168.2

80

8.184838.1

237

0.31632.4

13

0.54455.7

14

0.22923.5

4

0.0545.5I

0.34735.5

6

0.42343.3II

0.48950.1

1 1

2.117216.6

103

6.758691.4

196

0.23323.8

10

0.45146.1

1 1

0.12713.0

2

0.0687.0I

0.31131.8

6

0.40541.4II

0.51352.5

11

MW = 50.491.599

16478

MW= 84.947.158

732207

MW = 58.050.291

3012

MW = 96.940.493

5013

MW = 137.400.188

193MW = 148.21

0.0808IMW = 133.41

0.376387MW s92.13

0.42343II

MW= 112.560.501

5111


CALIBRATION DATA

^»- *- »*• **•» • ww <\^»-»-. w^s-ri . i^* . h_nw<

Proof RecordWV^H COHP.

MJ«HfrHr N.C.

company M«fr Number

Amwrlonn &TM-115*nC iTiTiJQ Ttf-^/Cy

H 000469

UiXEtH R1.3A

Overall Avrifl* yaa,-

4l hBll311Lbi'..ir\,i>< • W • • • • • • • ' -i .' '

i

1•i

. •

1——————

1

•

•' ' '.••.itf.fiilk "102 S. MaWSffifi •

C

AV.

MePi

0

Yd=

Poat.ll

"^Co.

^P«xl <

asu0 flrti

E

'"branfl

14-A.S

t ; ll-

irenr007

F

-ov

.999

Jfoxtra

»c>^

A^

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'lov

Tismilla

^

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H

jmomoFrom

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.

troiifirwil

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Mk A/^

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' (^w

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L

W

(<

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M PURCHASE Of

* 8091

.99965

v0—"—————^

m^0

•

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REMARKS

T>J NOT ».^Ac- ( -7 fc fi.^t4^-

d.^fi 2.

(2.JN 3

flunrr ^ ^ 0 - 1

4'»-»- 2-

*^ '.";•'

R«Ml«wl by: JSUMlw^ ^

T^l ?<P.

nelinqutehod by: (Slynatun) Oaf/Tim*

RMiriMd by: (S(9M«k« ReUnqulihad by: (SJgnffumJ

RellnquWtMt by: fitoiMlUKtf

>tf MARKS:

Dale/Tim*

-< ^^/ '•-/-L^ iL.^1^ \ JM^ (^ ( t ^ N i > ^ . - ^ A,^^A- ^.zfr-^f) Clean Air Engln—ring

500 W. Wood StrestPalatine. IL 60067708/991-3300

/•USTOMER COPV

clean air engineeringcae project no: 5815-1 summary introduction clean air engineering was...

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