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The Thermo Scientific DFS high resolution GC/MS is the highest performance, most efficient and simple to operate magnetic sector mass spectrometer ever built.

M A S S S P E C T R O M E T R Y

DFS High Resolution GC/MS High Performance Magnetic Sector GC/MS

• Performance-Moderninnovationsinionoptics,magnetandelectricsectordesign,provideindustryleadingspeci-ficityfortracetargetcompoundanalysis;whilstdeliveringunrivalledsignaltonoisecharacteristicsforreliablepeakintegrationandquantification.

• Simplicity-TheDFSmassspectrometerissimpletooperateandfeelslikeabenchtopGC/MS.Automatedtuneandmasscalibrationeaseadoptionofthetechnologyintothelaboratory,whilstfreeingtheanalystforothertasks.

• Efficiency-Lowestinclassrunningcosts,combinedwithhighthroughputcapabilitiesofdualGCconfigurations,significantlyincreaselaboratorysamplecapacitywhilstreducingcostpersample.

DFS Mass SpectrometerTheDFSisahighresolutionmagneticsectormassspectrometerlikenonebefore.Ithasbeendesignedfromthegrounduptobenefitfromnewinnovationsandmodernproductiontechniques.Cumulativeadvancesinmoderncomponentdesignandmanufacture,combinetoprovidethemostpowerfulhighresolutionGC/MSeverforthemostdemandingconfirmatoryPOPsanalyses.

2 Hardware Specifications

Ion SourceThe ion source has been designed with special emphasis on sensitivity and durability for increased productivity, low maintenance and increased uptime.

• Plug-inionsourcewithoptimizedboxdesignforquickexchangeincludingbuiltinionextractionlensforeaseofmaintenance

• Exchangeofionvolumeandfilamentwithout venting

• OptimizedlonglifetimefilamentsforEIandCI

• Independentsourcetemperaturecontrol

• Simplesourcedesign-cleanquickly

• Inertcomposition-cleanlessfrequently

Reference InletAn independent reference calibrant system that is continuously flow adjustable and can beindividuallyevacuated.Itallowssyringeintroduction of liquid or gaseous samples. By separating the reference inlet from the GC interface, maintainance is reduced and uptimemaximized.

Vacuum InterlockTheDFSmassspectrometerisequippedwithavacuuminterlockforquickexchangeofionizationvolumesandfilamentswithoutventing.

• Pneumaticallyactuatedbysystemcontrol

• Eliminatesimpropermanualoperation

TuningTheDFSsystemusesthesameThermoScientifictuningsoftwarefoundonotherThermoScientificGC/MS&LC/MSinstruments;TunePlus™. Designed with automation and simplicity in mind; the tuningprocess,experimentandsequenceset-upisintuitiveandrapid.TheDFSmassspectro-meterenablesthereliable,routineuseofAUTOTUNEinallionizationmodeswithout restrictions, including slit control and automated resolution settings.

Mass CalibrationThermoFisherScientificinventedthefieldcalibration method of scanning magnetic massspectrometers.TheDFSsystemoffersfulldatasystemcontroloffieldcalibrationscanning.

The mass scale needs to be calibrated only once. The operator can change mass range and scan speed without the need for recalibration.ItisthesameapproachandhandlingasknownfrombenchtopGC/MSsystems.

• Constantmasscalibrationbasedonmagneticfieldmeasurement

• Calibrationindependentofmassrange,scan speed, scan mode (including linked scanMS/MS),ionpolarityandionizationtechnique

• Norecalibrationrequiredafterchangeofionvolumeorionizationtechnique

3

AnalyzerThenewlydesignedDFSanalyzerhasvirtuallynoimageaberrations.Itisperfectlydouble focusing; employing an ultra high precisiontoroidalelectrostaticanalyzerandacarefullyrefinedmagneticanalyzer.This directly translates into stability and ruggedness.

• NovelionopticsdesignisbasedontheprovenreverseNier-Johnsongeometry

• Massindependentfocuswithuniformresolution throughout the mass range

• Ionopticsoptimizedforanaccelerationvoltage of 5 kV

• Allionizationtechniquesoperationalwithfull acceleration voltage

• Highprecision,datasystemcontrolled,continuously variable Tantalum entrance andexitslitsforfastresponseandlonglifetime

• Lowhysteresis,radiallylaminatedH-typemagnet of special metal alloy with mass independent focal length, deflection radius 350 mm, deflection angle 65°

• InnovativeRogowskymagnetentrancepole pieces for optimum sensitivity regardlessofionizationmethod

• Novelelectrostaticanalyzer(ESA)usingacomputeroptimizedtoroidaldesignfor highest mass precision and ion transmission with virtually no image errors

• Allfocusinganddetectionelementshoused in a single monoblock vacuum chamber

• EntireDFSanalyzerassembledonanintegrated shock mounted platform for isolation from floor vibration

Performance Characteristics• Sensitivity(EIGC/MS):

>200:1 for 20 fg 2378TCDD at m/z322,R=10,000,S/N=PtP4SD.

• Massaccuracy<2ppm

• Resolution(static)>60,000(10%valley)

• Scanrates0.1to10,000seconds/decade(continuouslyvariable)

• Massrange2-6000Da; 2-1200Daatfullacceleratingvoltage

Detection SystemThe long lifetime secondary electron multiplieroftheDFSanalyzeralwaysprovidesoptimalsignalamplificationforallionizationmodesincludingnegativeCI.

• Longlifetimeoffaxissecondaryelectronmultiplier detection system

• Post-acceleration/conversiondynode,variable to ± 20 kV

• Quickchangemountonanindividualflange

Vacuum System

The clean high vacuum background produced by turbomolecular pumps enables theDFSsystemtoachievelowerdetectionlimits routinely.

• Ultrafastpumpdowntimes;reducesinstallationandmaintainencetime-maximizingproductivity

• Oil-freehighvacuumturbomolecularpumps reduce the high chemical background observed with other pumping technologies

• Directlycoupledhighspeeddifferentialpumping system with three turbo molecular pumps

• Push-buttoncontrol

• Automatedprotectionsystem

Electronics CabinetIntegratedelectronicscabinetforlowspacerequirements.Optimizedairflowforefficientcoolingofmagnetpowersupply.Effectivepotentialdecouplingbetweendigitalelectronics and mass spectrometer high voltage and power supplies.

• Universalinput/outputforReady/Startcommunicationwithexternaldevicesusing programmable signal logic

• Analogin

• Digitalin/out

Direct Inlet Options

Direct Probe Base Unit (optional)• Portfordirectinsertionprobe

• Requiredtoattachanyofthefollowingprobe options

• Containsexchangelockandprobeelectronics

Water Cooled DI Probe (DI / DIP)(optional)• Directinsertionprobe

• Datasystemcontrolled,liquidcooled

• Usingdisposablealuminumcrucibles

• Heatingrates:20°Cto200°Cin30s,

200 °C to 300 °C in 30 s

• Temperaturerangefrom10°Caboveambient

• Maximumtemperature350°C

DCI Probe (optional)• Directchemicalionizationprobe

• Fulldatasystemcontrol

• Usingreusablefilaments

• Ultrafastheatingratesof>500°C/s

• Maximumtemperature1600°C

• HightemperaturetipforDCIprobe(optional)

• Usingreusablequartzcrucibles

• Maximumtemperature800°C

4 Software Specifications

Thermo Scientific Xcalibur Data SystemXcalibur™ is the uniform software platform forsystemcontroloftheThermoScientificGC/MSandLC/MSsystems.

TheDFSmassspectrometerusestheXcalibur instrument control software for high and low resolution operation, multiple iondetectionMID,selectionofpositiveornegative ions, linked scans, peak matching, andfullcontrolofanalyzerandinletsystemssupportingthefollowingcapabilities:

• INTENSITYAUTOTUNE:automatedoptimizationoftunepeakformaximumsenstivity

• RESOLUTIONAUTOTUNE:computercontrolledslitsettingsformaximumselectivity

• Controlofstandardandoptionalinletsystems

• Instrumentdiagnostics:fulladvancedsuite of instrument diagnostics including integrated parameter logging

• Xcaliburapplicationsoftware,incorporating all mass spectrometry processing tasks such as chromatogram andspectrumdisplay,integratedNISTlibrarysearch,CMASSforaccuratemassconversion and averaging, elemental composition and isotopic pattern calculation.

• QuanBrowser:quantificationpackage

• MSdataimportandexportusingtheANDI/netCDFformats,conversionfromFinniganMassLabdatafileformats,ASCIItextexport

• StandardizedoutputtoLIMSsystems

Thermo Scientific TargetQuan Software Suite (optional)ThespecialXcaliburDFSsoftwarepackagefor automated data evaluation on target compoundsincluding:

• Dioxinmethodsetup

• Supportofinstrumentandquantitation

• Responsefileandreportingprograms

• Dataevaluationforisotopedilutionmethods as well as relative response factors

• CompliantwiththepublishedEPAmethodsfordioxinmeasurementsanddataevaluationaccordinge.g.EPA1613,EPA8280,EPA8290,EPA23,EPA513,EN1948andequivalentJISmethods

• CompliantwiththerequirementforTEQlow-med-upperboundreporting

• StandardizedoutputtoLIMSsystems

Library Options• NISTLibrary

• WileyLibrary

• Pfleger-Maurer-WeberLibrary

• ThermoScientificPesticideLibrary

Software LicensesTheDFSXcalibursoftwarelicensesaresupplied for instrument control as well as reprocessing.

Newinstrumentsoftwarereleasesaresuppliedfreeofchargewithin12monthafterdelivery.

Data System

Personal Computer in the following minimumconfiguration*:DellOptiplex990MTCorei3-2100

• 3.1GHzProcessor

• MiniTowercase

• 4096MB800MHzDDR2RAM

• 1TBSATAIIharddisk

• DVD-RWdrive

• DVIAdd-incard

• Networkcard10/100

• 2PCIand1PCI-Expressslotspace

• 1parallelport

• 2serialports

• 12USB2.0

• Graphicschiponboard,upto128MBofmemory

• 10/100/1000Ethernetchiponboard

• U.S.keyboardblack

• DellUSB6-ButtonOpticalMouseBlack

• MicrosoftWindows7ProfessionalOperatingsystem(32BitOS)

• MicrosoftOffice2010Professional

• MouseandKeyboard

• Highresolution22inchTFTcolormonitor

• Optionallaserprinter,BW, 1200x1200dpi,upto25pages/min

*Minimumdatasystemspecificationsmay change without prior notice in case of technological improvement. Call for latest configuration.

5Gas Chromatography Options

Thermo Scientific TRACE 1310 Gas ChromatographTheTRACE™1300SeriesGCconsistsoftwomodelsdesignedtomeetthespecificneedsofalllaboratories.TheTRACE1310GCfeaturesacompleteicon-driventouch-screenuserinterfaceidealfordirectinstrument control in larger routine and method development laboratories. The TRACE1300GCisthebudget-consciousinvestment for the basic routine laboratory lookingforanintuitivesingle-buttonsystem,that provides ease of use with minimal instrument interaction. Both instruments offerthesameuser-exchangeable,instantconnect injector and detector modules and fastovenperformancewithexceptionalretention time stability to reach an incredibly high lab productivity at reduced cost of ownership.

Performance Specifications•TypicalRetentionTimeRepeatability:<0.0008min

•TypicalPeakAreaRepeatability:<0.5%RSD

Oven Specifications•ColumnOven(H×W×D):27×27×17.7cm;12.9L

•OperatingTemperatureRange:ambient+3°Cto450°C

•CryogenicOptionMinimumTemperature:-100°CwithliquidNitrogen;-50withliquidCO

2

•TemperatureSetPointResolution:0.1°C

•NumberofRamps/Plateaus:32/33

•MaximumHeatingRate:125°C/min

T Range °C Heating Rate °C/min

Model:220Volts Model:110Volts

50to70 125 90

70to115 100 65

115to175 80 50

175to300 50 30

300to450 35 20

•OvenCool-Down(22°Cambient):450°Cto50°Cin<4minutes

•AmbientRejection:<0.01°Cper1°C

IEC (Integrated Electronic Control)Gas Specification

•Upto18channelsofintegratedelectronic gas control

•PressureSetPointsMinimumIncrements: 0.01kPa-0.001psiinallranges

Carrier Gas Control Common to all Injectors•SplitRatio:Upto12500:1

•PressureRange:0–1000kPa(0–145PSI)

•Modes:Constantandprogrammedpressures and flows

•TotalFlowSetting:

– Control of split flow in 1 mL/min from 0 to 1250 mL/min

– Purge flow from 0 to 50 mL/min

Optional Instant Connect Auxiliary Gas Module•Allowsforthecontrolofthreeadditional

gas channels

Injectors•MaximumNumberInjectorsInstalled:2

•AvailableasInstantConnect,user-exchangeablemodules

Instant Connect Split/Splitless•Suitableforallcapillarycolumns (50μmto530μmi.d.)

•Compatiblewith1/8”and1/16”packedcolumnusingadapters.SupportsP&T/TD/HSbyspecialadapter.CompatibleMerlinMicroseal™ septum.

•Dedicatedsplit/splitlessinjectorwithintegrated backflush capabilities

•MaximumTemperature:400°C

Instant Connect Programmable Temperature Vaporizer•Supportshot/coldsplitandsplitless

modes as well as large volume injections (solventsplit)andOnColumn(TPOC).CompatibleMerlinMicrosealseptum.

•DedicatedPTVinjectorwithintegratedbackflush capabilities

•TemperatureRange:Airforcedcoolingtoambient+5°Cupto450°C

•CryogenicOptionMinimumTemperature:-100°Cwithliquidnitrogen;-50°CwithCO

2

•Temperatureprogrammingofupto3rampsatupto870°C/min

Detectors

•DetectorsAvailable:FlameIonizationDetector, Thermal Conductivity Detector, ElectronCaptureDetector,NitrogenPhosphorusDetector,fullrangeofThermoScientificmassspectrometers

•AvailableasInstantConnect,user-exchangeablemodules

•MaximumnumberInstalled:3includingamass spectrometers on the same oven

•FastDataAcquisitionRate:upto300HzforFID,TCD,ECD,andNPD

Instant Connect Flame Ionization Detector•Capillarycolumnoptimizedcompatiblewith1/8”and1/16”packedcolumn

•Flameoutdetectionandautomaticre-ignition

•MDL:<1.8pgC/s

•Sensitivity:>0.03Coulombs/gC

•LinearDynamicRange:>107(±10%)

•MaximumTemperature:450°Cinstepsof0.1°C

•IEC:

– Air: 0–500 mL/min in 0.1 steps

– H2: 0–100 mL/min in 0.1 steps

– Makeup gas (N2 or He) 0–50 mL/min in 0.1 steps

Instant Connect Thermal Conductivity Detector•Capillarycolumnoptimized(microTCD)compatiblewith1/8”and1/16”packedcolumn

• MaximumTemperature:400°Cinstepsof0.1°C

•MDL:<400pgtridecane/mLwithHecarrieror<20pgtridecane/swithatotalflowthroughthecellof3mL/min

•LinearDynamicRange:105

6 Thermo ScientificTriPlus RSH AutosamplerTheThermoScientificTriPlusRSHAutosampleroffersexceptionalprecision,flexibility,andproductivityinrobotic,sample-handlingsolutions.CompatiblewithThermoScientificGCandGC/MSsystems,the autosampler sets new standards in automationandprovidesadvancedliquid-handling cycles that enable automated functionality beyond traditional liquid, headspace,andsolid-phasemicroextraction(SPME*)injections.

Integrated Sampling SystemTheTriPlus™RSHautosamplerexpandsautomated capabilities beyond sample injectionstoadvancedsample-handlingcycles. Automating the whole workflow, from sample preparation to injection, increases precision and reproducibility and enables unprecedentedflexibilityandproductivityinGCandGC-MSsampling.

Ultimate ProductivityDesignedforexpandedproductivity,thisintegrated sampling system accommodates large sample capacities supporting full, unattended24/7operation.Asanexample,amaximumof972,2mLvialscombinedwithmultiple100mLwash/wastebottlesenableweek-endlongunattendedoperations–agoalnotattainablewithmostothersampling systems currently on the market.

Unmatched FlexibilityTheTriPlusRSHroboticsample-handlingsystem offers liquid, headspace, and solidphasemicroextraction–capabilitiesyouexpectasbeingastandardpartofamulti-axisautosampler.Inthesemodes,thesampling system delivers the precision you demandforachievingexceptionalresults.ScalablecapabilitiesenableexpandedGCandGC-MSapplicationranges,accuratemicro-sampleinjections,andthematchingoftechniques to sample types.

Seamless Operation

Accurate automation of a multitude of traditionally manual tasks is enabled by a new and innovative ATC (Automatic Tool Change)capability.TheATCfeatureenablesthe user to set up a sequence using up to sixdifferentsyringes,automaticallyloadedby the autosampler to accurately perform dilutions, calibrations, and sample injections. Theabilitytoexchangesyringesfordifferenttasksenableshigh-precisionsamplehandling in a single, unattended sequence prior to automated sample injection.

TriPlus RSH ConfigurationsTheTriPlusRSHAutosamplerisavailableinthefollowingconfigurations:

•TriPlusRSHforautomatedliquidsampling

•TriPlusRSHforstaticheadspaceautomation

•TriPlusRSHforautomatedliquidandheadspace sampling and injection

Additional upgrade kits are available totransformexistingversionsintomultitechnique platforms.

DescriptionlXYZroboticsamplehandlingapparatus with automatic syringe switch concept.Whentheoptionalaccessoriesare installed, the system is capable of automating sample preparation steps like standard dilution, standard addition, sequentialdilution,derivatizationandvortexing.

CommunicationlTwoindependentLAN

Local User InterfacelLEDstatusindicators.Optionalcontrolpanelwith4keys,roundknob,andgraphicalLCDdisplay.

Instrument ControllThermoScientificchromatography data systems integrated with Virtual Terminal software to completely mimic the physical controller

Teaching FunctionslManualwithoutusingtoolsorexternaldevices

Injector Compatibility l Compatible with on-column,programmabletemperaturevaporizing,packed,purgedpacked,split-splitless injectors

High Throughput Configuration DualGCset-upwithDoubleProandConfirmationmodes:SingleTriPlusRSHservingtwoindependentGCorGC/MSsystems,forliquid,HSorSPMEsampleinjection or for sample preparation, using the same or two different software systems. Two different methods can be used.RapidModestartsthesyringe

Instant Connect Electron Capture Detector•RadioactiveSource:370MBqequalto10mCi,63Ni

•MDL:<6fg/slindane

•LinearDynamicRange:>104withlindane

•MaximumTemperature:400°Cin0.1°Csteps

•IEC:0to500mL/minmakeupin0.1steps

•Make-upGas:Nitrogenor95%argon/5%methane

Instant Connect Nitrogen Phosphorus Detector•NPDavailablewithceramicbeadsandcompatiblewithelement-specificsources

•MDL:<20fgP/sand<100fgN/swithstandard ceramic bead

•Selectivity:gP/gC=200000;gN/gC=80000

•LinearDynamicRange:104

•MaximumTemperature:450°Cinstepsof0.1°C

•IEC:

– Air: 0–500 mL/min in 0.1 steps

– H2: 0–10 mL/min in 0.1 steps

– Makeup gas (Nitrogen): 0–50 mL/min in 0.1 steps

General Specifications

•HeatedZones:Upto7

•TimeEvents:63.Supportupto8valves

•OperatingAltitude:Upto3500mabovesea level

•Dimensions(H×W×D):45×44×67cm

•Weight(Kg):35Kgmainunitplus 0.8Kgeachmodule

CertificationsConforms to the following safety standards:

– International Electrotechnical Commission (IEC): 61010-1:2001 - 61010-2-010:2003 - 61010-2-081:2001 + A1:(2003)

– CAN/CSA C22.2 No. 61010-1 and UL 61010-1

– EuroNorm (EN): 61010-1:2001 - 61010-2-010:2004 - 61010-2-081:2002

Conforms to the following regulations on Electromagnetic Compatibility (EMC) and Radio Frequency Interference (RFI):

– CISPR 11/EN 55011: Group 1 Class A

– IEC/EN 61326-1:2006

* Sold under license from Supelco®

7 washing cycle during the current GC cooling phase.

Barcode Reader l Two active laser scanners for all standard vials using 1-dimensionbarcodesinahorizontalorientation.

VortexerlIntensivemixingof0.5,0.7,2,5,10,or20mLvialswithanagitationspeedup to 2000 rpm

Vial TrayslHeatedandcooledtraysexpandthe range of available applications from sampleinjectiontosample/standardpreparation

GC Mounting KitslThermoScientificTRACE1300GC,TRACE1310GC,TRACEGCUltraandFOCUSGC

Configuration for Liquid SamplingVial Volumesl300μLfixedinsertvials,0.5,0.7,2,2.5,10,and20mL.96/384MicrotiterorDeepWellplateswithAutomatic Foil Cutter to pierce alumina or plastic foils prior the needle penetration

Bottom-Sensing Vials l Capable of liquid injectionstartingfromsmall-volumesamples. Capability to inject from samples aslowas5µLintoavial.Possibilityofperforminguptothree1µLinjectionsfroma5µLsample,dependingonvialtype.

Height from Vial Bottom l User selectable between0.1and32mmin0.1mmsteps

Injection Speed for Liquid Samples Selectablefrom0.1μL/secupto2000μL/secandfullyprogrammable

Sample Capacity (Depending on autosampler, GC and MS configurations)•Upto4608wellplatesor6912wellplateswithextendedX-arm

•Upto8400.5/0.7mLvialsor12600.5/0.7mLvialswiththeextendedX-arm

•Upto6482mLsamplevialsor9722mLvialswiththeextendedX-arm

•Upto24010mLor20mLvialsor36010mLor20mLvialswiththeextendedX-arm

Syringes (Capable of handling liquid volumes in the range 0.1 μL – 10 mL) Capableofusing0.5μL,1.0μL,5μL,10μL(standard),25μL,50μL,100μL,250μL,500μL,1000μL,10000μLsyringesforsampleinjectionand/orvolumetransfer

Syringe CleaninglWashstationsforupto4differentsolventsforatotalof40mL(standard).Optionallargewashingstationsforupto3×100mLsolventbottles.Waste:1×10mLordraintoexternalwastebottle.Possibilitytoinstallmultiplesolventstationstoexpandsolventandwaste volumes.

Options•Upgradetoheadspaceoptionanditsown

accessories

•UpgradetoSPMEoption(withorwithoutheadspaceoption)

•Peltier-controlleddrawerforwellplates,300μLfixedinsertvials,2and10mLvials. Temperature selectable between 0 and40°C

•Cooledtrayholdersforwellplates,300μLfixedinsertvials,2,10and20mLvials.Temperatureselectablebetween4and70°C.Requiresexternalcirculatorbath.

•Solvent/reagentreservoir

•LargeVolumeWashStation

Injection VolumelRangefrom0.1to10,000μLin0.1μLstepsto100μLand1μLstepsbetween100μLand10mL.Needlelengths:57mmor85mmLiquidInjectionModes–8fullycustomizablemethod-specificpresetmenusavailable:

•Basicenrichment

•Enrichmentneedlesolventwash

•Internalstandarddouble

•Internalstandardpost

•Needlesolventwash

•Solventflushdouble

•Solventflushpost

Typical Performance –≤0.3RSD%obtainedunderThermoScientificstandardconditions

Configuration for HeadspaceVial Volumesl2,10and20mL

Syringe Sizesl1,2.5,and5mL

Sample Capacity (Depending on autosampler, GC and MS configurations)lUpto18010or20mLvialsor30010or20mLvialswiththeextendedX-arm

Injection Volume Rangel0.1to5mLin0.1mLstepsdependingonsyringe

Syringe TemperaturelOFFor40°Cto150°Cin1°Csteps

Incubation Oven Capacity l 6 vials

Incubation Oven Temperature Range 40to200°Cin1°Csteps,withagitation

Incubation Timel0.1to600.0minin0.1min increments

Syringe Flush CapabilitylWithinertgas

Solvent Syringe CleaninglOptionalwashingstations(4×10mLor2×100mLvials)

Multiple Headspace Extraction Yes(optionalaccessory)

Enrichment SamplinglYeswithoptionalkit for cold trap

Injection Speedl1to100mL/min,in1mL/minincrements

Typical Performancel≤0.7RSD%underThermoScientificstandardconditions

Needle Lengths l 65 mm, compatible with every injector port

Options•UpgradetoLiquidoption

•UpgradetoSPMEoption

•Peltier-cooledtrayholderfor300μLfixedinsertvials,2and10mLvials;temperature selectable between 0 °C and 40°C

•Cooledtrayholdersfor300μLfixedinsertvials,2,10and20mLvials;requiresexternalcirculatorbath;temperatureselectablebetween4°Cand70°C

•SPMEFiberCleaningStation

•Solvent/reagentreservoir

•LargeVolumeWashStation

Solid Phase Micro Extraction OptionVial Volumesl2,10and20mL

Sample Capacity l Depending on Autosampler,GCandMSconfigurations:

•Upto8400.5/0.7mLvialsor12600.5/0.7mLvialswiththeextendedX-arm

•Upto6482mLsamplevialsor9722mLvialswiththeextendedX-arm

•Upto18010or20mLvialsor30010or20mLvialswiththeextendedX-arm

Incubation Oven Capacity l 6 vials

Incubation Oven Temperature Range 40°Cto200°Cin1°Csteps,withagitation

Vial Penetration DepthlStandardorcustom between 5 mm and 20 mm, suitableforliquidorheadspaceextraction

Fiber Conditioning StationlOptional,2-portsandaneedleguide,40-350°C,inertgaspurged.Fiber:23gauge.Onefiberholdertoautomateallfibers.

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PS30096_E07/12G

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sInstallation Requirements

Detailed installation requirements are providedintheDFSPreinstallationRequirementsGuidePN/1194630

Recirculating Water ChillerTheDFSmassspectrometercanbeconfiguredwiththeoptionalThermoScientificNESLABThermoFlexTF25recirculating chiller. The chiller is compact, quietandefficient.TheThermoFlexTF25isavailableinbothair-cooledandwatercooledconfigurations,foraquietlaboratoryfor stable and precise cooling of magnet and turbo molecular pumps. The cooler is controlled by a temperature sensor mounted ontheDFSmagnet.

• Precisetemperaturecontrolandtemperaturestabilityofupto±0.1°C

• Adjustablehighandlowtemperaturesafeties with audible alarm

• Environmentally-friendlyCFC-freeair-cooledrefrigerationsystemThermoFlexTF25-79.6Kg.44x67x73cm

Supplies

PowerTheDFSmassspectrometerisdesignedtooperate at a nominal voltage of 230 V AC, 50/60Hz.Theminimumandmaximumvoltage tolerances are in compliance with IEC950,Amend2,1993.Approximateconsumptionvaluesforregularoperationare:

• 0,9kWforGCoperation

• 1,9kWforMSoperation

• 1,6kWforchiller

HeliumForGCcarriergas:99.996%,ultra-highpurity. Total hydrocarbons should be less than 2.0 ppm.

Compressed AirCompressed air with a pressure of 6 bar (87psi)isrequiredtooperatethepneumaticvalves of the instrument. A suitable compressor can be ordered from Thermo FisherScientific(PartNo.0261850).

Space Requirement

DFS Mass Spectrometer• HxD140.6cm(55.4”)x156.8cm(62.5”)

• WidthwithoneGCinstalled

161.1cm(63.5”)

• WidthwithtwoGCsinstalled

209.1cm(82.4”)

• MSconsolewithanalyzerandmagnet900kg(2000lb)

• Datasystem130kg(<290lb)

• GCwithconsole35kg(78lb)

TRACE 1310 GC• Dimensions(H×W×D):45×44×67

cm

• Weight(Kg):35Kgmainunitplus0.8Kgeachmodule(78lb)

• ColumnOven(H×W×D):27×27×17.7cm;12.9L

TriPlus RSH AutosamplerOveralldimensionsontheGC:

• Length(Xaxis)80cm Theextendedextendedmodellength is120cm

• Heightapproximately70cm,dependenton mounting kit

CPU: 42x18x44.5cm(16.5x7x17”)Monitor: 42x40x43cm(16.5x16x17”) Keyboard: 2.5x47x18cm(1x18x7“)

Environment

Room TemperatureLaboratoryroomtemperaturemustbemaintainedbetween15°Cand26°C (59°Fand79°F).Theoptimumoperationtemperatureisbetween18°Cand21°C (65°Fand70°F).

Air Conditioning LoadThe average power dissipation during analysisoperationforabasicDFSsystem,including gas chromatograph and data system,isapproximately4.7kW(4.5BTU/s).FordualGCconfiguration,theaverageairconditioningloadamountsapproximately to4.9kW(4.7BTU/s).

HumidityThe relative humidity of the operating environmentmustbebetween30%and70%,withnocondensation.

Recommended Instrument Clearences and Weight Distribution

Thermo Fisher Scientific (Bremen) GmbH Management System Registered to ISO 9001:2008