dfs high resolution gc/ms - high performance magnetic ... · product specifications the thermo...
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Pro
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The Thermo Scientific DFS high resolution GC/MS is the highest performance, most efficient and simple to operate magnetic sector mass spectrometer ever built.
M A S S S P E C T R O M E T R Y
DFS High Resolution GC/MS High Performance Magnetic Sector GC/MS
• Performance-Moderninnovationsinionoptics,magnetandelectricsectordesign,provideindustryleadingspeci-ficityfortracetargetcompoundanalysis;whilstdeliveringunrivalledsignaltonoisecharacteristicsforreliablepeakintegrationandquantification.
• Simplicity-TheDFSmassspectrometerissimpletooperateandfeelslikeabenchtopGC/MS.Automatedtuneandmasscalibrationeaseadoptionofthetechnologyintothelaboratory,whilstfreeingtheanalystforothertasks.
• Efficiency-Lowestinclassrunningcosts,combinedwithhighthroughputcapabilitiesofdualGCconfigurations,significantlyincreaselaboratorysamplecapacitywhilstreducingcostpersample.
DFS Mass SpectrometerTheDFSisahighresolutionmagneticsectormassspectrometerlikenonebefore.Ithasbeendesignedfromthegrounduptobenefitfromnewinnovationsandmodernproductiontechniques.Cumulativeadvancesinmoderncomponentdesignandmanufacture,combinetoprovidethemostpowerfulhighresolutionGC/MSeverforthemostdemandingconfirmatoryPOPsanalyses.
2 Hardware Specifications
Ion SourceThe ion source has been designed with special emphasis on sensitivity and durability for increased productivity, low maintenance and increased uptime.
• Plug-inionsourcewithoptimizedboxdesignforquickexchangeincludingbuiltinionextractionlensforeaseofmaintenance
• Exchangeofionvolumeandfilamentwithout venting
• OptimizedlonglifetimefilamentsforEIandCI
• Independentsourcetemperaturecontrol
• Simplesourcedesign-cleanquickly
• Inertcomposition-cleanlessfrequently
Reference InletAn independent reference calibrant system that is continuously flow adjustable and can beindividuallyevacuated.Itallowssyringeintroduction of liquid or gaseous samples. By separating the reference inlet from the GC interface, maintainance is reduced and uptimemaximized.
Vacuum InterlockTheDFSmassspectrometerisequippedwithavacuuminterlockforquickexchangeofionizationvolumesandfilamentswithoutventing.
• Pneumaticallyactuatedbysystemcontrol
• Eliminatesimpropermanualoperation
TuningTheDFSsystemusesthesameThermoScientifictuningsoftwarefoundonotherThermoScientificGC/MS&LC/MSinstruments;TunePlus™. Designed with automation and simplicity in mind; the tuningprocess,experimentandsequenceset-upisintuitiveandrapid.TheDFSmassspectro-meterenablesthereliable,routineuseofAUTOTUNEinallionizationmodeswithout restrictions, including slit control and automated resolution settings.
Mass CalibrationThermoFisherScientificinventedthefieldcalibration method of scanning magnetic massspectrometers.TheDFSsystemoffersfulldatasystemcontroloffieldcalibrationscanning.
The mass scale needs to be calibrated only once. The operator can change mass range and scan speed without the need for recalibration.ItisthesameapproachandhandlingasknownfrombenchtopGC/MSsystems.
• Constantmasscalibrationbasedonmagneticfieldmeasurement
• Calibrationindependentofmassrange,scan speed, scan mode (including linked scanMS/MS),ionpolarityandionizationtechnique
• Norecalibrationrequiredafterchangeofionvolumeorionizationtechnique
3
AnalyzerThenewlydesignedDFSanalyzerhasvirtuallynoimageaberrations.Itisperfectlydouble focusing; employing an ultra high precisiontoroidalelectrostaticanalyzerandacarefullyrefinedmagneticanalyzer.This directly translates into stability and ruggedness.
• NovelionopticsdesignisbasedontheprovenreverseNier-Johnsongeometry
• Massindependentfocuswithuniformresolution throughout the mass range
• Ionopticsoptimizedforanaccelerationvoltage of 5 kV
• Allionizationtechniquesoperationalwithfull acceleration voltage
• Highprecision,datasystemcontrolled,continuously variable Tantalum entrance andexitslitsforfastresponseandlonglifetime
• Lowhysteresis,radiallylaminatedH-typemagnet of special metal alloy with mass independent focal length, deflection radius 350 mm, deflection angle 65°
• InnovativeRogowskymagnetentrancepole pieces for optimum sensitivity regardlessofionizationmethod
• Novelelectrostaticanalyzer(ESA)usingacomputeroptimizedtoroidaldesignfor highest mass precision and ion transmission with virtually no image errors
• Allfocusinganddetectionelementshoused in a single monoblock vacuum chamber
• EntireDFSanalyzerassembledonanintegrated shock mounted platform for isolation from floor vibration
Performance Characteristics• Sensitivity(EIGC/MS):
>200:1 for 20 fg 2378TCDD at m/z322,R=10,000,S/N=PtP4SD.
• Massaccuracy<2ppm
• Resolution(static)>60,000(10%valley)
• Scanrates0.1to10,000seconds/decade(continuouslyvariable)
• Massrange2-6000Da; 2-1200Daatfullacceleratingvoltage
Detection SystemThe long lifetime secondary electron multiplieroftheDFSanalyzeralwaysprovidesoptimalsignalamplificationforallionizationmodesincludingnegativeCI.
• Longlifetimeoffaxissecondaryelectronmultiplier detection system
• Post-acceleration/conversiondynode,variable to ± 20 kV
• Quickchangemountonanindividualflange
Vacuum System
The clean high vacuum background produced by turbomolecular pumps enables theDFSsystemtoachievelowerdetectionlimits routinely.
• Ultrafastpumpdowntimes;reducesinstallationandmaintainencetime-maximizingproductivity
• Oil-freehighvacuumturbomolecularpumps reduce the high chemical background observed with other pumping technologies
• Directlycoupledhighspeeddifferentialpumping system with three turbo molecular pumps
• Push-buttoncontrol
• Automatedprotectionsystem
Electronics CabinetIntegratedelectronicscabinetforlowspacerequirements.Optimizedairflowforefficientcoolingofmagnetpowersupply.Effectivepotentialdecouplingbetweendigitalelectronics and mass spectrometer high voltage and power supplies.
• Universalinput/outputforReady/Startcommunicationwithexternaldevicesusing programmable signal logic
• Analogin
• Digitalin/out
Direct Inlet Options
Direct Probe Base Unit (optional)• Portfordirectinsertionprobe
• Requiredtoattachanyofthefollowingprobe options
• Containsexchangelockandprobeelectronics
Water Cooled DI Probe (DI / DIP)(optional)• Directinsertionprobe
• Datasystemcontrolled,liquidcooled
• Usingdisposablealuminumcrucibles
• Heatingrates:20°Cto200°Cin30s,
200 °C to 300 °C in 30 s
• Temperaturerangefrom10°Caboveambient
• Maximumtemperature350°C
DCI Probe (optional)• Directchemicalionizationprobe
• Fulldatasystemcontrol
• Usingreusablefilaments
• Ultrafastheatingratesof>500°C/s
• Maximumtemperature1600°C
• HightemperaturetipforDCIprobe(optional)
• Usingreusablequartzcrucibles
• Maximumtemperature800°C
4 Software Specifications
Thermo Scientific Xcalibur Data SystemXcalibur™ is the uniform software platform forsystemcontroloftheThermoScientificGC/MSandLC/MSsystems.
TheDFSmassspectrometerusestheXcalibur instrument control software for high and low resolution operation, multiple iondetectionMID,selectionofpositiveornegative ions, linked scans, peak matching, andfullcontrolofanalyzerandinletsystemssupportingthefollowingcapabilities:
• INTENSITYAUTOTUNE:automatedoptimizationoftunepeakformaximumsenstivity
• RESOLUTIONAUTOTUNE:computercontrolledslitsettingsformaximumselectivity
• Controlofstandardandoptionalinletsystems
• Instrumentdiagnostics:fulladvancedsuite of instrument diagnostics including integrated parameter logging
• Xcaliburapplicationsoftware,incorporating all mass spectrometry processing tasks such as chromatogram andspectrumdisplay,integratedNISTlibrarysearch,CMASSforaccuratemassconversion and averaging, elemental composition and isotopic pattern calculation.
• QuanBrowser:quantificationpackage
• MSdataimportandexportusingtheANDI/netCDFformats,conversionfromFinniganMassLabdatafileformats,ASCIItextexport
• StandardizedoutputtoLIMSsystems
Thermo Scientific TargetQuan Software Suite (optional)ThespecialXcaliburDFSsoftwarepackagefor automated data evaluation on target compoundsincluding:
• Dioxinmethodsetup
• Supportofinstrumentandquantitation
• Responsefileandreportingprograms
• Dataevaluationforisotopedilutionmethods as well as relative response factors
• CompliantwiththepublishedEPAmethodsfordioxinmeasurementsanddataevaluationaccordinge.g.EPA1613,EPA8280,EPA8290,EPA23,EPA513,EN1948andequivalentJISmethods
• CompliantwiththerequirementforTEQlow-med-upperboundreporting
• StandardizedoutputtoLIMSsystems
Library Options• NISTLibrary
• WileyLibrary
• Pfleger-Maurer-WeberLibrary
• ThermoScientificPesticideLibrary
Software LicensesTheDFSXcalibursoftwarelicensesaresupplied for instrument control as well as reprocessing.
Newinstrumentsoftwarereleasesaresuppliedfreeofchargewithin12monthafterdelivery.
Data System
Personal Computer in the following minimumconfiguration*:DellOptiplex990MTCorei3-2100
• 3.1GHzProcessor
• MiniTowercase
• 4096MB800MHzDDR2RAM
• 1TBSATAIIharddisk
• DVD-RWdrive
• DVIAdd-incard
• Networkcard10/100
• 2PCIand1PCI-Expressslotspace
• 1parallelport
• 2serialports
• 12USB2.0
• Graphicschiponboard,upto128MBofmemory
• 10/100/1000Ethernetchiponboard
• U.S.keyboardblack
• DellUSB6-ButtonOpticalMouseBlack
• MicrosoftWindows7ProfessionalOperatingsystem(32BitOS)
• MicrosoftOffice2010Professional
• MouseandKeyboard
• Highresolution22inchTFTcolormonitor
• Optionallaserprinter,BW, 1200x1200dpi,upto25pages/min
*Minimumdatasystemspecificationsmay change without prior notice in case of technological improvement. Call for latest configuration.
5Gas Chromatography Options
Thermo Scientific TRACE 1310 Gas ChromatographTheTRACE™1300SeriesGCconsistsoftwomodelsdesignedtomeetthespecificneedsofalllaboratories.TheTRACE1310GCfeaturesacompleteicon-driventouch-screenuserinterfaceidealfordirectinstrument control in larger routine and method development laboratories. The TRACE1300GCisthebudget-consciousinvestment for the basic routine laboratory lookingforanintuitivesingle-buttonsystem,that provides ease of use with minimal instrument interaction. Both instruments offerthesameuser-exchangeable,instantconnect injector and detector modules and fastovenperformancewithexceptionalretention time stability to reach an incredibly high lab productivity at reduced cost of ownership.
Performance Specifications•TypicalRetentionTimeRepeatability:<0.0008min
•TypicalPeakAreaRepeatability:<0.5%RSD
Oven Specifications•ColumnOven(H×W×D):27×27×17.7cm;12.9L
•OperatingTemperatureRange:ambient+3°Cto450°C
•CryogenicOptionMinimumTemperature:-100°CwithliquidNitrogen;-50withliquidCO
2
•TemperatureSetPointResolution:0.1°C
•NumberofRamps/Plateaus:32/33
•MaximumHeatingRate:125°C/min
T Range °C Heating Rate °C/min
Model:220Volts Model:110Volts
50to70 125 90
70to115 100 65
115to175 80 50
175to300 50 30
300to450 35 20
•OvenCool-Down(22°Cambient):450°Cto50°Cin<4minutes
•AmbientRejection:<0.01°Cper1°C
IEC (Integrated Electronic Control)Gas Specification
•Upto18channelsofintegratedelectronic gas control
•PressureSetPointsMinimumIncrements: 0.01kPa-0.001psiinallranges
Carrier Gas Control Common to all Injectors•SplitRatio:Upto12500:1
•PressureRange:0–1000kPa(0–145PSI)
•Modes:Constantandprogrammedpressures and flows
•TotalFlowSetting:
– Control of split flow in 1 mL/min from 0 to 1250 mL/min
– Purge flow from 0 to 50 mL/min
Optional Instant Connect Auxiliary Gas Module•Allowsforthecontrolofthreeadditional
gas channels
Injectors•MaximumNumberInjectorsInstalled:2
•AvailableasInstantConnect,user-exchangeablemodules
Instant Connect Split/Splitless•Suitableforallcapillarycolumns (50μmto530μmi.d.)
•Compatiblewith1/8”and1/16”packedcolumnusingadapters.SupportsP&T/TD/HSbyspecialadapter.CompatibleMerlinMicroseal™ septum.
•Dedicatedsplit/splitlessinjectorwithintegrated backflush capabilities
•MaximumTemperature:400°C
Instant Connect Programmable Temperature Vaporizer•Supportshot/coldsplitandsplitless
modes as well as large volume injections (solventsplit)andOnColumn(TPOC).CompatibleMerlinMicrosealseptum.
•DedicatedPTVinjectorwithintegratedbackflush capabilities
•TemperatureRange:Airforcedcoolingtoambient+5°Cupto450°C
•CryogenicOptionMinimumTemperature:-100°Cwithliquidnitrogen;-50°CwithCO
2
•Temperatureprogrammingofupto3rampsatupto870°C/min
Detectors
•DetectorsAvailable:FlameIonizationDetector, Thermal Conductivity Detector, ElectronCaptureDetector,NitrogenPhosphorusDetector,fullrangeofThermoScientificmassspectrometers
•AvailableasInstantConnect,user-exchangeablemodules
•MaximumnumberInstalled:3includingamass spectrometers on the same oven
•FastDataAcquisitionRate:upto300HzforFID,TCD,ECD,andNPD
Instant Connect Flame Ionization Detector•Capillarycolumnoptimizedcompatiblewith1/8”and1/16”packedcolumn
•Flameoutdetectionandautomaticre-ignition
•MDL:<1.8pgC/s
•Sensitivity:>0.03Coulombs/gC
•LinearDynamicRange:>107(±10%)
•MaximumTemperature:450°Cinstepsof0.1°C
•IEC:
– Air: 0–500 mL/min in 0.1 steps
– H2: 0–100 mL/min in 0.1 steps
– Makeup gas (N2 or He) 0–50 mL/min in 0.1 steps
Instant Connect Thermal Conductivity Detector•Capillarycolumnoptimized(microTCD)compatiblewith1/8”and1/16”packedcolumn
• MaximumTemperature:400°Cinstepsof0.1°C
•MDL:<400pgtridecane/mLwithHecarrieror<20pgtridecane/swithatotalflowthroughthecellof3mL/min
•LinearDynamicRange:105
6 Thermo ScientificTriPlus RSH AutosamplerTheThermoScientificTriPlusRSHAutosampleroffersexceptionalprecision,flexibility,andproductivityinrobotic,sample-handlingsolutions.CompatiblewithThermoScientificGCandGC/MSsystems,the autosampler sets new standards in automationandprovidesadvancedliquid-handling cycles that enable automated functionality beyond traditional liquid, headspace,andsolid-phasemicroextraction(SPME*)injections.
Integrated Sampling SystemTheTriPlus™RSHautosamplerexpandsautomated capabilities beyond sample injectionstoadvancedsample-handlingcycles. Automating the whole workflow, from sample preparation to injection, increases precision and reproducibility and enables unprecedentedflexibilityandproductivityinGCandGC-MSsampling.
Ultimate ProductivityDesignedforexpandedproductivity,thisintegrated sampling system accommodates large sample capacities supporting full, unattended24/7operation.Asanexample,amaximumof972,2mLvialscombinedwithmultiple100mLwash/wastebottlesenableweek-endlongunattendedoperations–agoalnotattainablewithmostothersampling systems currently on the market.
Unmatched FlexibilityTheTriPlusRSHroboticsample-handlingsystem offers liquid, headspace, and solidphasemicroextraction–capabilitiesyouexpectasbeingastandardpartofamulti-axisautosampler.Inthesemodes,thesampling system delivers the precision you demandforachievingexceptionalresults.ScalablecapabilitiesenableexpandedGCandGC-MSapplicationranges,accuratemicro-sampleinjections,andthematchingoftechniques to sample types.
Seamless Operation
Accurate automation of a multitude of traditionally manual tasks is enabled by a new and innovative ATC (Automatic Tool Change)capability.TheATCfeatureenablesthe user to set up a sequence using up to sixdifferentsyringes,automaticallyloadedby the autosampler to accurately perform dilutions, calibrations, and sample injections. Theabilitytoexchangesyringesfordifferenttasksenableshigh-precisionsamplehandling in a single, unattended sequence prior to automated sample injection.
TriPlus RSH ConfigurationsTheTriPlusRSHAutosamplerisavailableinthefollowingconfigurations:
•TriPlusRSHforautomatedliquidsampling
•TriPlusRSHforstaticheadspaceautomation
•TriPlusRSHforautomatedliquidandheadspace sampling and injection
Additional upgrade kits are available totransformexistingversionsintomultitechnique platforms.
DescriptionlXYZroboticsamplehandlingapparatus with automatic syringe switch concept.Whentheoptionalaccessoriesare installed, the system is capable of automating sample preparation steps like standard dilution, standard addition, sequentialdilution,derivatizationandvortexing.
CommunicationlTwoindependentLAN
Local User InterfacelLEDstatusindicators.Optionalcontrolpanelwith4keys,roundknob,andgraphicalLCDdisplay.
Instrument ControllThermoScientificchromatography data systems integrated with Virtual Terminal software to completely mimic the physical controller
Teaching FunctionslManualwithoutusingtoolsorexternaldevices
Injector Compatibility l Compatible with on-column,programmabletemperaturevaporizing,packed,purgedpacked,split-splitless injectors
High Throughput Configuration DualGCset-upwithDoubleProandConfirmationmodes:SingleTriPlusRSHservingtwoindependentGCorGC/MSsystems,forliquid,HSorSPMEsampleinjection or for sample preparation, using the same or two different software systems. Two different methods can be used.RapidModestartsthesyringe
Instant Connect Electron Capture Detector•RadioactiveSource:370MBqequalto10mCi,63Ni
•MDL:<6fg/slindane
•LinearDynamicRange:>104withlindane
•MaximumTemperature:400°Cin0.1°Csteps
•IEC:0to500mL/minmakeupin0.1steps
•Make-upGas:Nitrogenor95%argon/5%methane
Instant Connect Nitrogen Phosphorus Detector•NPDavailablewithceramicbeadsandcompatiblewithelement-specificsources
•MDL:<20fgP/sand<100fgN/swithstandard ceramic bead
•Selectivity:gP/gC=200000;gN/gC=80000
•LinearDynamicRange:104
•MaximumTemperature:450°Cinstepsof0.1°C
•IEC:
– Air: 0–500 mL/min in 0.1 steps
– H2: 0–10 mL/min in 0.1 steps
– Makeup gas (Nitrogen): 0–50 mL/min in 0.1 steps
General Specifications
•HeatedZones:Upto7
•TimeEvents:63.Supportupto8valves
•OperatingAltitude:Upto3500mabovesea level
•Dimensions(H×W×D):45×44×67cm
•Weight(Kg):35Kgmainunitplus 0.8Kgeachmodule
CertificationsConforms to the following safety standards:
– International Electrotechnical Commission (IEC): 61010-1:2001 - 61010-2-010:2003 - 61010-2-081:2001 + A1:(2003)
– CAN/CSA C22.2 No. 61010-1 and UL 61010-1
– EuroNorm (EN): 61010-1:2001 - 61010-2-010:2004 - 61010-2-081:2002
Conforms to the following regulations on Electromagnetic Compatibility (EMC) and Radio Frequency Interference (RFI):
– CISPR 11/EN 55011: Group 1 Class A
– IEC/EN 61326-1:2006
* Sold under license from Supelco®
7 washing cycle during the current GC cooling phase.
Barcode Reader l Two active laser scanners for all standard vials using 1-dimensionbarcodesinahorizontalorientation.
VortexerlIntensivemixingof0.5,0.7,2,5,10,or20mLvialswithanagitationspeedup to 2000 rpm
Vial TrayslHeatedandcooledtraysexpandthe range of available applications from sampleinjectiontosample/standardpreparation
GC Mounting KitslThermoScientificTRACE1300GC,TRACE1310GC,TRACEGCUltraandFOCUSGC
Configuration for Liquid SamplingVial Volumesl300μLfixedinsertvials,0.5,0.7,2,2.5,10,and20mL.96/384MicrotiterorDeepWellplateswithAutomatic Foil Cutter to pierce alumina or plastic foils prior the needle penetration
Bottom-Sensing Vials l Capable of liquid injectionstartingfromsmall-volumesamples. Capability to inject from samples aslowas5µLintoavial.Possibilityofperforminguptothree1µLinjectionsfroma5µLsample,dependingonvialtype.
Height from Vial Bottom l User selectable between0.1and32mmin0.1mmsteps
Injection Speed for Liquid Samples Selectablefrom0.1μL/secupto2000μL/secandfullyprogrammable
Sample Capacity (Depending on autosampler, GC and MS configurations)•Upto4608wellplatesor6912wellplateswithextendedX-arm
•Upto8400.5/0.7mLvialsor12600.5/0.7mLvialswiththeextendedX-arm
•Upto6482mLsamplevialsor9722mLvialswiththeextendedX-arm
•Upto24010mLor20mLvialsor36010mLor20mLvialswiththeextendedX-arm
Syringes (Capable of handling liquid volumes in the range 0.1 μL – 10 mL) Capableofusing0.5μL,1.0μL,5μL,10μL(standard),25μL,50μL,100μL,250μL,500μL,1000μL,10000μLsyringesforsampleinjectionand/orvolumetransfer
Syringe CleaninglWashstationsforupto4differentsolventsforatotalof40mL(standard).Optionallargewashingstationsforupto3×100mLsolventbottles.Waste:1×10mLordraintoexternalwastebottle.Possibilitytoinstallmultiplesolventstationstoexpandsolventandwaste volumes.
Options•Upgradetoheadspaceoptionanditsown
accessories
•UpgradetoSPMEoption(withorwithoutheadspaceoption)
•Peltier-controlleddrawerforwellplates,300μLfixedinsertvials,2and10mLvials. Temperature selectable between 0 and40°C
•Cooledtrayholdersforwellplates,300μLfixedinsertvials,2,10and20mLvials.Temperatureselectablebetween4and70°C.Requiresexternalcirculatorbath.
•Solvent/reagentreservoir
•LargeVolumeWashStation
Injection VolumelRangefrom0.1to10,000μLin0.1μLstepsto100μLand1μLstepsbetween100μLand10mL.Needlelengths:57mmor85mmLiquidInjectionModes–8fullycustomizablemethod-specificpresetmenusavailable:
•Basicenrichment
•Enrichmentneedlesolventwash
•Internalstandarddouble
•Internalstandardpost
•Needlesolventwash
•Solventflushdouble
•Solventflushpost
Typical Performance –≤0.3RSD%obtainedunderThermoScientificstandardconditions
Configuration for HeadspaceVial Volumesl2,10and20mL
Syringe Sizesl1,2.5,and5mL
Sample Capacity (Depending on autosampler, GC and MS configurations)lUpto18010or20mLvialsor30010or20mLvialswiththeextendedX-arm
Injection Volume Rangel0.1to5mLin0.1mLstepsdependingonsyringe
Syringe TemperaturelOFFor40°Cto150°Cin1°Csteps
Incubation Oven Capacity l 6 vials
Incubation Oven Temperature Range 40to200°Cin1°Csteps,withagitation
Incubation Timel0.1to600.0minin0.1min increments
Syringe Flush CapabilitylWithinertgas
Solvent Syringe CleaninglOptionalwashingstations(4×10mLor2×100mLvials)
Multiple Headspace Extraction Yes(optionalaccessory)
Enrichment SamplinglYeswithoptionalkit for cold trap
Injection Speedl1to100mL/min,in1mL/minincrements
Typical Performancel≤0.7RSD%underThermoScientificstandardconditions
Needle Lengths l 65 mm, compatible with every injector port
Options•UpgradetoLiquidoption
•UpgradetoSPMEoption
•Peltier-cooledtrayholderfor300μLfixedinsertvials,2and10mLvials;temperature selectable between 0 °C and 40°C
•Cooledtrayholdersfor300μLfixedinsertvials,2,10and20mLvials;requiresexternalcirculatorbath;temperatureselectablebetween4°Cand70°C
•SPMEFiberCleaningStation
•Solvent/reagentreservoir
•LargeVolumeWashStation
Solid Phase Micro Extraction OptionVial Volumesl2,10and20mL
Sample Capacity l Depending on Autosampler,GCandMSconfigurations:
•Upto8400.5/0.7mLvialsor12600.5/0.7mLvialswiththeextendedX-arm
•Upto6482mLsamplevialsor9722mLvialswiththeextendedX-arm
•Upto18010or20mLvialsor30010or20mLvialswiththeextendedX-arm
Incubation Oven Capacity l 6 vials
Incubation Oven Temperature Range 40°Cto200°Cin1°Csteps,withagitation
Vial Penetration DepthlStandardorcustom between 5 mm and 20 mm, suitableforliquidorheadspaceextraction
Fiber Conditioning StationlOptional,2-portsandaneedleguide,40-350°C,inertgaspurged.Fiber:23gauge.Onefiberholdertoautomateallfibers.
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PS30096_E07/12G
Pro
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sInstallation Requirements
Detailed installation requirements are providedintheDFSPreinstallationRequirementsGuidePN/1194630
Recirculating Water ChillerTheDFSmassspectrometercanbeconfiguredwiththeoptionalThermoScientificNESLABThermoFlexTF25recirculating chiller. The chiller is compact, quietandefficient.TheThermoFlexTF25isavailableinbothair-cooledandwatercooledconfigurations,foraquietlaboratoryfor stable and precise cooling of magnet and turbo molecular pumps. The cooler is controlled by a temperature sensor mounted ontheDFSmagnet.
• Precisetemperaturecontrolandtemperaturestabilityofupto±0.1°C
• Adjustablehighandlowtemperaturesafeties with audible alarm
• Environmentally-friendlyCFC-freeair-cooledrefrigerationsystemThermoFlexTF25-79.6Kg.44x67x73cm
Supplies
PowerTheDFSmassspectrometerisdesignedtooperate at a nominal voltage of 230 V AC, 50/60Hz.Theminimumandmaximumvoltage tolerances are in compliance with IEC950,Amend2,1993.Approximateconsumptionvaluesforregularoperationare:
• 0,9kWforGCoperation
• 1,9kWforMSoperation
• 1,6kWforchiller
HeliumForGCcarriergas:99.996%,ultra-highpurity. Total hydrocarbons should be less than 2.0 ppm.
Compressed AirCompressed air with a pressure of 6 bar (87psi)isrequiredtooperatethepneumaticvalves of the instrument. A suitable compressor can be ordered from Thermo FisherScientific(PartNo.0261850).
Space Requirement
DFS Mass Spectrometer• HxD140.6cm(55.4”)x156.8cm(62.5”)
• WidthwithoneGCinstalled
161.1cm(63.5”)
• WidthwithtwoGCsinstalled
209.1cm(82.4”)
• MSconsolewithanalyzerandmagnet900kg(2000lb)
• Datasystem130kg(<290lb)
• GCwithconsole35kg(78lb)
TRACE 1310 GC• Dimensions(H×W×D):45×44×67
cm
• Weight(Kg):35Kgmainunitplus0.8Kgeachmodule(78lb)
• ColumnOven(H×W×D):27×27×17.7cm;12.9L
TriPlus RSH AutosamplerOveralldimensionsontheGC:
• Length(Xaxis)80cm Theextendedextendedmodellength is120cm
• Heightapproximately70cm,dependenton mounting kit
CPU: 42x18x44.5cm(16.5x7x17”)Monitor: 42x40x43cm(16.5x16x17”) Keyboard: 2.5x47x18cm(1x18x7“)
Environment
Room TemperatureLaboratoryroomtemperaturemustbemaintainedbetween15°Cand26°C (59°Fand79°F).Theoptimumoperationtemperatureisbetween18°Cand21°C (65°Fand70°F).
Air Conditioning LoadThe average power dissipation during analysisoperationforabasicDFSsystem,including gas chromatograph and data system,isapproximately4.7kW(4.5BTU/s).FordualGCconfiguration,theaverageairconditioningloadamountsapproximately to4.9kW(4.7BTU/s).
HumidityThe relative humidity of the operating environmentmustbebetween30%and70%,withnocondensation.
Recommended Instrument Clearences and Weight Distribution