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M560/565Melting Point
en
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The latest generation of Buchi Melting Point Apparatus once again sets the futures gold
standard of exact melting and boiling point determinations. The standard instrument, manual
Melting Point M560, and the video camera equipped instrument, fully automated Melting Point
M565, are both high quality and precise pieces of laboratory equipment. Equipped with a
precision magnifying lens to detect the slightest change in the capillaries and an intuitive menu
structure on a bright colour display, the instruments guarantee fast and reliable results from
the first run onward. In combination with the Sample Loader M569, the time consuming
procedure of loading samples into the capillaries is now easy, homogeneous and reproducible.
Melting Point M560 and Melting Point M565
Facile determinations of melting points and
boiling points
Highlights of the Melting Point Line Choose between manual or auto-matic instrument or Melting andBoiling Point determinationIncreased temperature range romroom temperature up to 400 CAll instruments are equipped withmagniying lens or visual controlUnchanged approved coating o theheating block or ast cleaning and along lietime
Compliant with Pharmacopeia asPH. EUR. 6.1.2.2.60, USP XXI 741and JPGLP/GMP compliant protocols eitherwith printer or on PC.IQ/OQ or Melting Point M-565available
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The attractively priced Melting Point M-560 for the manual determination of melting and
boiling points is designed for all laboratories with a moderate requirement of sample
processing in a non-regulated environment.
Basic Set: Melting Point M560
Manual melting point determination for
universities and research laboratories
Increase your efficiency of the Melting Point M-560 and M-565
Delivery content
The Basic Set consists o the instrumentand accessories or the installation,reliable calibration and convenient
determination o the irst 100 meltingpoints.
Melting Point M-560 Instrument
100 Melting Point Capillaries
10 Boiling Point Capillaries
10 Boiling Point Tubes
Calibration Set M-560 / M-565 or theirst installation
Packing wire or samples with a waxy
consistence
Sample Holder or the conusion reepreparation o 12 melting point and4 boiling point samples
Mini KeyboardFor the convenient, straightorward inputo parameters.
Serial Printer
For documenting the results ocalibration, melting and boiling point
determinations.
Sample Loader M-569
Instrument or the homogenous loadingo samples into Buchi melting point
capillaries.
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Exclusive Accessory of the Melting Point M-565
Delivery content
The Proessional Set consists o thetwo instruments and a wide range oaccessories or the installation, reliable
calibration and convenient determinationo the irst 100 melting points.
Melting Point M-565 Instrument
Sample Loader M-569 Instrument
100 Melting Point Capillaries
10 Boiling Point Capillaries
10 Boiling Point Tubes
Calibration Set M-560 / M-565 or theirst installation
Packing wire or samples with a waxyconsistence
Sample Holder or the conusion reepreparation o 12 melting point and4 boiling point samples
The video camera equipped Melting Point M565 for the automatic determination of
melting and boiling points is designed for true, professional quality control. When used in
combination with the Sample Loader M569, determinations are achieved with unrivalled
reproducibility. Optional, comprehensive IQ/OQ documentation is available in five different
languages for customers working in a regulated environment. Intuitive PC software is also
available for the handling of large amounts of user, method and result data generated.
Professional Set: Melting Point M565 and
Sample Loader M569 Automatic melting point
determination for higher sample throughputs
MeltingPoint Monitor Software
Sotware or the easy and convenientmanagement o user, method and result
data.
IQ/OQ Documentation
Installation Qualiication needed orthe initial installation o the Melting
Point M-565, either ater shipmentor movement to a new workplace.Including Operational Qualiicationto guarantee the instrument meetspredeined speciications.
OQ Documentation
Repeating operational qualiication toguarantee that the instrument meets
predeined speciication.
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Features of the
M560 and M565
Additional
Features of
the M565
Sample Loader M-569 World Novelty
Unique system or the loading o melting point capillariesReproducible results due to consistent, homogeneous packing qualityLoading times substantially reduced when compared to conventional methodsEasy and sae handling o samples and capillaries:
No risk o cross contaminations as with the glass tube procedureNo Risk o breaking capillary eliminated when compared to manual knocking method
Compact design with a stable standThree position switch or permanent operation or operation during pressing
Invaluable when packing large numbers o capillariesIn the delivery content o Melting Point M-565Optional accessory or Melting Point M-560 and previous Buchi Melting Pointinstruments
Precision lens with 2.5 times magniica-tion or a precise determination o thesamples
Optimised design o theheating block allowsaster cooling times andthereore higher samplethroughput per hour
Brilliant large colourdisplay with a high
resolution or com-ortable control othe instrument
Fully menu guided, exactingcalibrations when using the BuchiCalibration Standards
Optional Keyboard and Printer or a astinput o sample parameters and a direct,standardised output o results
Optional Melting Point Monitor Sotwareor easy and sae management o user,methods and results data
Optional IQ/OQ Documentation or
customers in a regulated environment.No need to create validation documents.
Available in ive languages
Video movie o de-terminations allowsthe review o each
measurement. Varia-ble speed playbackrom single rameslow motion throughto 100x real time
Relaxed, atigue reeobservation o thephase transition on the6x magniied colourdisplay
Automatic determination o melting andboiling point or a higher eiciency
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Melting point orboiling point video
Actual temperatureaccording to videoplay time
Melting or boiling point curves
Method and Result database Overview o automatic and manuallydetermined results
For the intuitive, user friendly management of user, methods and results data in combination
with the ability to observe the melting and boiling point determination movies, MeltingPoint
Monitor software is essential for non-tolerant, routine work, for example, as found in quality
control. Subsequent observation of the melting curves and melting video after the
determination identifies any failures in packing of the capillary, combustion of the substance
or presence of excess impurities and subsequently reduces the repetition of
measurements.
MeltingPoint Monitor
Professional PCSoftware for the
Melting Point M565
Method and Result Management
Comortable database structure or easyarchiving and recovery o previousmeasurements. Various sort unctionsby name, user and date.
Overview of Results
Succinct overview o the automaticallydetected results, showing the averagevalue and standard deviation, allowsinterpretation rom one view. Additional,manually determined results are shown
below.
Melting Point and Boiling Point
Screen video display
Ater the measurement, any previousmovie can be reviewed at various speedsrom single rame advancing to 100xactual speed. Moving the scrollbar to the
start point o a melting process reducesthe observation time.
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Accuracy Competence Meets Quality
To reduce the time spent preparing documents and test plans, completedocumentation is provided in ive dierent languages. The qualiication packagealso includes speciically certiied calibration and veriication standards which canbe traced back to the international temperature scale ITS-90 and comply with thestrictest requirements.I the quality o your Instrument has to comply with very strict audit requirementsthen Buchi can oer the installation, calibration and qualiication o your instrumentby a ully certiied service technician.
You save time and only need to approve the qualiication o your instrument on thecompletion o all work.
Complete Qualification Packages
The initial qualiication covers the Instru-ment Qualiication (IQ) and the OperationQualiication (OQ). The IQ veriies that theinstrument is correctly installed and in
good working order. The OQ demon-strates the unctioning o the instrumentwithin its working speciications.For the Melting Point M-565 Buchi oersan IQ/OQ package or the initial installa-tion and an OQ renewal or the routineveriication that the instrument still ulilsits speciications.
Analytical instruments must be calibrated and verified at regular intervals according to a
written procedure. The necessary accuracy is ensured by this instrument and the Operation
Qualification.
GLP/GMP compliant IQ/OQ for
Melting Point M565
IQ/OQ Package for Melting Point
M-565
Instrument LogbookIQ documentationOQ documentationOQ labelCalibration kit M-565Veriication kit M-565
100 melting point capillariesAvailable in E, D, F, I, ES
OQ renewal for Melting Point M-565
IQ documentationOQ documentationOQ labelCalibration kit M-565Veriication kit M-565100 melting poit capillariesAvailable in E, D, F, I, ES
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A B
Overview of Ordering Information
Basic Set: Melting Point M-560
Economic Instrument or themanual detection o melting andboiling points.100 V240 V, 50/60 Hz
Order no. 051999
Instruments
Sample Loader M-569
Instrument or a ast and homo-genous loading o samples intomelting capillaries.100 V240 V, 50/60 Hz
Order no. 051997
Professional Set: Melting Point M-565 and Sample Loader M-569
High end Melting Point M-565 or the automatic and manual detection omelting and boiling points. Includes the Sample Loader M-569 or an eec-tive packing o samples into melting capillaries.100 V240 V, 50/60 Hz
Order no. 051998
Mini Keyboard
For convenient straightorwardinput o parameters.
Order no.German (CH) 029509English (USA) 029508
IQ/OQ M-565 Order no.English 11055 004
German 11055 005French 11055 006Spanish 11055 007Italian 11055 008
OQ M-565 Order no.English 11055 009
German 11055 010French 11055 011Spanish 11055 012Italian 11055 013
Melting point capillaries
The precision glass capillariesensure highly reproducible meltingpoint determinations.
Order no.
100 pieces 0178081000 pieces 001759
Calibration Kit M-560/5
Consists o our Buchi certiiedstandards or the calibration o theMelting Point M-560 or the MeltingPoint M-565.Order no. 11055018
Certification and Installation
service offer
Installation, calibration and certii-cation perormed by a Buchi certii-cated service technician.
Order no.or Switzerland 900402
For other countries please contactyour local distributor
Verification Kit M-560/M-565
Consists o three Buchi certiiedstandards or the veriication o theMelting Point M-560 or the MeltingPoint M-565.
Order no. 11055019
Sample Holder
For the conusion ree preparationo 12 melting point and 4 boilingpoint samples.
Order no. 11055014
MeltingPoint Monitor Software
Sotware CD, Tutorial and single
PC license. For installation underWindows Vista or Windows XP.
Order no. 11055 332
Agate Mortar and Pestle
For high purity sample crushing. Thepolished surace is easy to clean,preventing cross-contamination
Order no. 041867
Accessories for Melting Point M-560 and Melting Point M-565
Exclusive Accessories for Melting Point M-565
Serial Printer
For the documentation o resultso calibration, melting and boilingpoint determinations.100 V240 V, 50/60 HzOrder no. 11055 438
Boiling Point Tube A
Boiling Point Capillary B
The precision capillaries B gen-erate perect gas bubbles withintube A or reproducible boilingpoint determinations.Order no. A B10 pieces 019697 051850
100 pieces 019007 051890
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Technical data9
Melting Point M-560 Melting Point M-565 Sample Loader M-569
Manual melting point determination
Manual boiling point determination
Automatic melting point determination
Automatic boiling point determination
Homogeneous sample loading
Positions or melting capillaries 3 3 3
Positions or boiling capillaries 1 1
Precision magniying lens Magniication o lens 2.5 x 2.5 x
Digital camera
Video unction
Magniication, Display 6 x
Display Colour, TFT, 320 x 240, 3.5
Determination temperature range ambient to 400 C
Temperature resolution 0.1 C
Accuracy up to 100 Cup to 250 Cup to 400 C
+/ 0,3 C+/ 0,5 C+/ 0,8 C
Temperature gradients, C/min 0.1, 0.2, 0.5, 1, 2, 3, 5, 10, 20
Heat-up time (50 C 350 C) ~ 4 min
Cool-down time (350 C 50 C) ~ 10 min
Electrical supply 100240 V (10%), 5060 Hz 100240 V
Power consumption 150 W 15 W
Contact termination L, N, PE L, N
Approval CE, UL
Dimensions (W x H x D), mm 190 x 200 x 370 70 x 86 x 130
Weight, kg 4.5 0.5
Environmental conditions For indoor use only
Temperature 540 C
Altitude up to 2000 m
Humidity Maximum relative humidity 80% or temperatures up to 31 C, decreasing linerly to50% relative humidity at 40 C
Overvoltage category II
Degree o protection IP20
Pollution degree 2
System requirements MeltingPoint Monitor Software
Processor 32-or 64-bit Processor with 1 GHz
Memory 512 MB (RAM)
Hard disk 40 GB hard disk with at least 15 GB ree
Operating system Windows XP Proessional SP2 or higherWindows Vista Ultimate (32-bit version)Windows Vista Business (32-bit version)
Drive CD ROM
Serial interace 1 x USB 2.0
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Evolution of Melting Point Instruments
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