folleto m-565 buchi

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    M560/565Melting Point

    en

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    The latest generation of Buchi Melting Point Apparatus once again sets the futures gold

    standard of exact melting and boiling point determinations. The standard instrument, manual

    Melting Point M560, and the video camera equipped instrument, fully automated Melting Point

    M565, are both high quality and precise pieces of laboratory equipment. Equipped with a

    precision magnifying lens to detect the slightest change in the capillaries and an intuitive menu

    structure on a bright colour display, the instruments guarantee fast and reliable results from

    the first run onward. In combination with the Sample Loader M569, the time consuming

    procedure of loading samples into the capillaries is now easy, homogeneous and reproducible.

    Melting Point M560 and Melting Point M565

    Facile determinations of melting points and

    boiling points

    Highlights of the Melting Point Line Choose between manual or auto-matic instrument or Melting andBoiling Point determinationIncreased temperature range romroom temperature up to 400 CAll instruments are equipped withmagniying lens or visual controlUnchanged approved coating o theheating block or ast cleaning and along lietime

    Compliant with Pharmacopeia asPH. EUR. 6.1.2.2.60, USP XXI 741and JPGLP/GMP compliant protocols eitherwith printer or on PC.IQ/OQ or Melting Point M-565available

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    The attractively priced Melting Point M-560 for the manual determination of melting and

    boiling points is designed for all laboratories with a moderate requirement of sample

    processing in a non-regulated environment.

    Basic Set: Melting Point M560

    Manual melting point determination for

    universities and research laboratories

    Increase your efficiency of the Melting Point M-560 and M-565

    Delivery content

    The Basic Set consists o the instrumentand accessories or the installation,reliable calibration and convenient

    determination o the irst 100 meltingpoints.

    Melting Point M-560 Instrument

    100 Melting Point Capillaries

    10 Boiling Point Capillaries

    10 Boiling Point Tubes

    Calibration Set M-560 / M-565 or theirst installation

    Packing wire or samples with a waxy

    consistence

    Sample Holder or the conusion reepreparation o 12 melting point and4 boiling point samples

    Mini KeyboardFor the convenient, straightorward inputo parameters.

    Serial Printer

    For documenting the results ocalibration, melting and boiling point

    determinations.

    Sample Loader M-569

    Instrument or the homogenous loadingo samples into Buchi melting point

    capillaries.

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    Exclusive Accessory of the Melting Point M-565

    Delivery content

    The Proessional Set consists o thetwo instruments and a wide range oaccessories or the installation, reliable

    calibration and convenient determinationo the irst 100 melting points.

    Melting Point M-565 Instrument

    Sample Loader M-569 Instrument

    100 Melting Point Capillaries

    10 Boiling Point Capillaries

    10 Boiling Point Tubes

    Calibration Set M-560 / M-565 or theirst installation

    Packing wire or samples with a waxyconsistence

    Sample Holder or the conusion reepreparation o 12 melting point and4 boiling point samples

    The video camera equipped Melting Point M565 for the automatic determination of

    melting and boiling points is designed for true, professional quality control. When used in

    combination with the Sample Loader M569, determinations are achieved with unrivalled

    reproducibility. Optional, comprehensive IQ/OQ documentation is available in five different

    languages for customers working in a regulated environment. Intuitive PC software is also

    available for the handling of large amounts of user, method and result data generated.

    Professional Set: Melting Point M565 and

    Sample Loader M569 Automatic melting point

    determination for higher sample throughputs

    MeltingPoint Monitor Software

    Sotware or the easy and convenientmanagement o user, method and result

    data.

    IQ/OQ Documentation

    Installation Qualiication needed orthe initial installation o the Melting

    Point M-565, either ater shipmentor movement to a new workplace.Including Operational Qualiicationto guarantee the instrument meetspredeined speciications.

    OQ Documentation

    Repeating operational qualiication toguarantee that the instrument meets

    predeined speciication.

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    Features of the

    M560 and M565

    Additional

    Features of

    the M565

    Sample Loader M-569 World Novelty

    Unique system or the loading o melting point capillariesReproducible results due to consistent, homogeneous packing qualityLoading times substantially reduced when compared to conventional methodsEasy and sae handling o samples and capillaries:

    No risk o cross contaminations as with the glass tube procedureNo Risk o breaking capillary eliminated when compared to manual knocking method

    Compact design with a stable standThree position switch or permanent operation or operation during pressing

    Invaluable when packing large numbers o capillariesIn the delivery content o Melting Point M-565Optional accessory or Melting Point M-560 and previous Buchi Melting Pointinstruments

    Precision lens with 2.5 times magniica-tion or a precise determination o thesamples

    Optimised design o theheating block allowsaster cooling times andthereore higher samplethroughput per hour

    Brilliant large colourdisplay with a high

    resolution or com-ortable control othe instrument

    Fully menu guided, exactingcalibrations when using the BuchiCalibration Standards

    Optional Keyboard and Printer or a astinput o sample parameters and a direct,standardised output o results

    Optional Melting Point Monitor Sotwareor easy and sae management o user,methods and results data

    Optional IQ/OQ Documentation or

    customers in a regulated environment.No need to create validation documents.

    Available in ive languages

    Video movie o de-terminations allowsthe review o each

    measurement. Varia-ble speed playbackrom single rameslow motion throughto 100x real time

    Relaxed, atigue reeobservation o thephase transition on the6x magniied colourdisplay

    Automatic determination o melting andboiling point or a higher eiciency

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    Melting point orboiling point video

    Actual temperatureaccording to videoplay time

    Melting or boiling point curves

    Method and Result database Overview o automatic and manuallydetermined results

    For the intuitive, user friendly management of user, methods and results data in combination

    with the ability to observe the melting and boiling point determination movies, MeltingPoint

    Monitor software is essential for non-tolerant, routine work, for example, as found in quality

    control. Subsequent observation of the melting curves and melting video after the

    determination identifies any failures in packing of the capillary, combustion of the substance

    or presence of excess impurities and subsequently reduces the repetition of

    measurements.

    MeltingPoint Monitor

    Professional PCSoftware for the

    Melting Point M565

    Method and Result Management

    Comortable database structure or easyarchiving and recovery o previousmeasurements. Various sort unctionsby name, user and date.

    Overview of Results

    Succinct overview o the automaticallydetected results, showing the averagevalue and standard deviation, allowsinterpretation rom one view. Additional,manually determined results are shown

    below.

    Melting Point and Boiling Point

    Screen video display

    Ater the measurement, any previousmovie can be reviewed at various speedsrom single rame advancing to 100xactual speed. Moving the scrollbar to the

    start point o a melting process reducesthe observation time.

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    Accuracy Competence Meets Quality

    To reduce the time spent preparing documents and test plans, completedocumentation is provided in ive dierent languages. The qualiication packagealso includes speciically certiied calibration and veriication standards which canbe traced back to the international temperature scale ITS-90 and comply with thestrictest requirements.I the quality o your Instrument has to comply with very strict audit requirementsthen Buchi can oer the installation, calibration and qualiication o your instrumentby a ully certiied service technician.

    You save time and only need to approve the qualiication o your instrument on thecompletion o all work.

    Complete Qualification Packages

    The initial qualiication covers the Instru-ment Qualiication (IQ) and the OperationQualiication (OQ). The IQ veriies that theinstrument is correctly installed and in

    good working order. The OQ demon-strates the unctioning o the instrumentwithin its working speciications.For the Melting Point M-565 Buchi oersan IQ/OQ package or the initial installa-tion and an OQ renewal or the routineveriication that the instrument still ulilsits speciications.

    Analytical instruments must be calibrated and verified at regular intervals according to a

    written procedure. The necessary accuracy is ensured by this instrument and the Operation

    Qualification.

    GLP/GMP compliant IQ/OQ for

    Melting Point M565

    IQ/OQ Package for Melting Point

    M-565

    Instrument LogbookIQ documentationOQ documentationOQ labelCalibration kit M-565Veriication kit M-565

    100 melting point capillariesAvailable in E, D, F, I, ES

    OQ renewal for Melting Point M-565

    IQ documentationOQ documentationOQ labelCalibration kit M-565Veriication kit M-565100 melting poit capillariesAvailable in E, D, F, I, ES

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    A B

    Overview of Ordering Information

    Basic Set: Melting Point M-560

    Economic Instrument or themanual detection o melting andboiling points.100 V240 V, 50/60 Hz

    Order no. 051999

    Instruments

    Sample Loader M-569

    Instrument or a ast and homo-genous loading o samples intomelting capillaries.100 V240 V, 50/60 Hz

    Order no. 051997

    Professional Set: Melting Point M-565 and Sample Loader M-569

    High end Melting Point M-565 or the automatic and manual detection omelting and boiling points. Includes the Sample Loader M-569 or an eec-tive packing o samples into melting capillaries.100 V240 V, 50/60 Hz

    Order no. 051998

    Mini Keyboard

    For convenient straightorwardinput o parameters.

    Order no.German (CH) 029509English (USA) 029508

    IQ/OQ M-565 Order no.English 11055 004

    German 11055 005French 11055 006Spanish 11055 007Italian 11055 008

    OQ M-565 Order no.English 11055 009

    German 11055 010French 11055 011Spanish 11055 012Italian 11055 013

    Melting point capillaries

    The precision glass capillariesensure highly reproducible meltingpoint determinations.

    Order no.

    100 pieces 0178081000 pieces 001759

    Calibration Kit M-560/5

    Consists o our Buchi certiiedstandards or the calibration o theMelting Point M-560 or the MeltingPoint M-565.Order no. 11055018

    Certification and Installation

    service offer

    Installation, calibration and certii-cation perormed by a Buchi certii-cated service technician.

    Order no.or Switzerland 900402

    For other countries please contactyour local distributor

    Verification Kit M-560/M-565

    Consists o three Buchi certiiedstandards or the veriication o theMelting Point M-560 or the MeltingPoint M-565.

    Order no. 11055019

    Sample Holder

    For the conusion ree preparationo 12 melting point and 4 boilingpoint samples.

    Order no. 11055014

    MeltingPoint Monitor Software

    Sotware CD, Tutorial and single

    PC license. For installation underWindows Vista or Windows XP.

    Order no. 11055 332

    Agate Mortar and Pestle

    For high purity sample crushing. Thepolished surace is easy to clean,preventing cross-contamination

    Order no. 041867

    Accessories for Melting Point M-560 and Melting Point M-565

    Exclusive Accessories for Melting Point M-565

    Serial Printer

    For the documentation o resultso calibration, melting and boilingpoint determinations.100 V240 V, 50/60 HzOrder no. 11055 438

    Boiling Point Tube A

    Boiling Point Capillary B

    The precision capillaries B gen-erate perect gas bubbles withintube A or reproducible boilingpoint determinations.Order no. A B10 pieces 019697 051850

    100 pieces 019007 051890

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    Technical data9

    Melting Point M-560 Melting Point M-565 Sample Loader M-569

    Manual melting point determination

    Manual boiling point determination

    Automatic melting point determination

    Automatic boiling point determination

    Homogeneous sample loading

    Positions or melting capillaries 3 3 3

    Positions or boiling capillaries 1 1

    Precision magniying lens Magniication o lens 2.5 x 2.5 x

    Digital camera

    Video unction

    Magniication, Display 6 x

    Display Colour, TFT, 320 x 240, 3.5

    Determination temperature range ambient to 400 C

    Temperature resolution 0.1 C

    Accuracy up to 100 Cup to 250 Cup to 400 C

    +/ 0,3 C+/ 0,5 C+/ 0,8 C

    Temperature gradients, C/min 0.1, 0.2, 0.5, 1, 2, 3, 5, 10, 20

    Heat-up time (50 C 350 C) ~ 4 min

    Cool-down time (350 C 50 C) ~ 10 min

    Electrical supply 100240 V (10%), 5060 Hz 100240 V

    Power consumption 150 W 15 W

    Contact termination L, N, PE L, N

    Approval CE, UL

    Dimensions (W x H x D), mm 190 x 200 x 370 70 x 86 x 130

    Weight, kg 4.5 0.5

    Environmental conditions For indoor use only

    Temperature 540 C

    Altitude up to 2000 m

    Humidity Maximum relative humidity 80% or temperatures up to 31 C, decreasing linerly to50% relative humidity at 40 C

    Overvoltage category II

    Degree o protection IP20

    Pollution degree 2

    System requirements MeltingPoint Monitor Software

    Processor 32-or 64-bit Processor with 1 GHz

    Memory 512 MB (RAM)

    Hard disk 40 GB hard disk with at least 15 GB ree

    Operating system Windows XP Proessional SP2 or higherWindows Vista Ultimate (32-bit version)Windows Vista Business (32-bit version)

    Drive CD ROM

    Serial interace 1 x USB 2.0

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    T +33 1 56 70 62 50F +33 1 46 86 00 [email protected]

    We are represented by more than 100 distributionpartners worldwide. Find your local representative at

    www.buchi.com

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