final analytical report for delatte metalsthis final report should only be reproduced in full. the...

9T5BCC03

p "z •"}"" j \ { c nUnited States Environmental Protection Agency

Region (6,-EpviFpnrnental, Services Branch Laboratory16325 Fallstoni'NoUstori, Texas 77099

U f, S t 1 ?! ' ••» ;"-i «. • ! f\ 1 ;YR>,!A>s^i.wtl . - . .Final Analytical Report

ooi—»>^b->CO

Site Name . . . . . . . . . . . . . . . . .

CERCLIS Number . . . . . . . . . .

Sample Collection Date . . . . . .

Laboratory Sample Identification

Contact . . . . . . . . . . . . . . . . . . .

Report Date . . . . . . . . . . . . . . .

Report Narrative:

. . . . . . . . . . Delatte Metals

. . . . . . . . . LAD052510344

. . . . . January 27-28,1999

. . . . . . . . . . . . 9T5BCC03

Stephen Tzhone (6SF-LP)

. . . . . . . . . . March 2, 1999

Standard procedures for quality assurance and quality control were followed inthe analysis and reporting of the sample results. The results apply only to thesamples tested. This final report should only be reproduced in full.

The laboratory routinely disposes of samples 90 days after all analysis has beencompleted. If you have a need to hold these samples in custody longer than 90days, please send an e-mail to Sylvia Gorostiza (gorostiza-sylvia) within the next30 days briefly stating your need to hold these samples in custody.

Report Approvao ' <^==^\^J^€^^6^/(^^/U___<^^^

Mike DaggettDeputy Branch Chief

Douglas A. j^ka TRegion 6 Laooratory Branch Chief

142915

BWALKER

*142915*

9T5BCC03

^eosB^

i t' SB®"? i^^1^^o^

STATION NUMBER

25-TB01B . . . . . . .

WW-05B . . . . . . . .

WW-06B . . . . . . . .

WW-07B . . . . . . . .

WW-04B . . . . . . . .

WW-03B . . . . . . . .

WW-02B . . . . . . . .

WW-S4B . . . . . . .

WW-01B . . . . . . . . .

25-FB01B . . . . . . .

25-FB02B . . . . . . .

25-TB03B . . . . . . .

WW-08B . . . . . . . .

Chain of Custody DC

UnitedRegion 6

10(

)cuments

States Environmental Protection AgencyEnvironmental Services Branch Laboratory325 Fallstone, Houston, Texas 77099

Final Analytical Report

Report Contents

LABORATORY SAMPLE NUMBER

.... 9T5BCC03-01 . . . . . . . . . . . . . . . . .

. . . . 9T5BCC03-02 . . . . . . . . . . . . . . . . .

.... 9T5BCC03-03 . . . . . . . . . . . . . . . . .

. . . . 9T5BCC03-04 . . . . . . . . . . . . . . . . .

.... 9T5BCC03-05 . . . . . . . . . . . . . . . . .

.... 9T5BCC03-06 . . . . . . . . . . . . . . . . .

.... 9T5BCC03-07 . . . . . . . . . . . . . . . . .

. . . . 9T5BCC03-08 . . . . . . . . . . . . . . . . .

. . . . 9T5BCC03-09 .. . . . . . . . . . . . . . . .

. . . . 9T5BCC03-10. . . . . . . . . . . . . . . . .

.... 9T5BCC03-11 . . . . . . . . . . . . . . . . .

. . . . 9T5BCC03-12 . . . . . . . . . . . . . . . . .

. . . . 9T5BCC03-13 . . . . . . . . . . . . . . . . .

PAGE(S)

. . . . . . . . . 3-5

. . . . . . . .6-10

. . . . . . . 1 1 - 1 6

. . . . . . . 17-21

. . . . . . . 22-27

. . . . . . . 28-33

. . . . . . . 34-38

. . . . . . . 39-44

. . . . . . . 45-49

. . . . . . . 50-51

. . . . . . . 52-53

. . . . . . . 54-56

. . . . . . . 57-61

. . . . . . . 62-67

0o

9T5BCC03

o0

U. S. Environmental Protection Agency ^ •L )

Region 6 Houston Laboratory o

Report For Sample Number 9T5BCC03 01

Source: DELATTE METALS

Site Description: sTA.25.TB01 B

Date/Time Received: 1/28/1999 09:30 AM Date Completed 3/1/1999

Date/Time Collected: 1/27/1999 07:05 PM

Sample Type: LIQUID

Comments:

Parameter DescriptionVOA VOLATILE ORGANIC ANALYSIS

9T5BCC03

00I—I

'--10^

ORGANIC ANALYSIS DATA

Sample Number: 9T5BCC03-01 Date Extracted: 3-Feb.-99

Site Name: Delatte Metals Date Analyzed: 3-Feb.-99

VOLATILE COMPOUNDS BY METHOD 624

units - microgram/liter - ug/lCompound Name

ace one

hrr^mf^mpthfinf^ •* —•— • • •—————•••• — — • w

carbon disulfide————————————————————————————/""trhnn "frff'i'i^h Ir^rirl/^ ^—•••••.•..••••-••••-•••-••-•••Mi—-———•••—•• ——•••••———•

dibromochloromethane-""""---"---""--"—""""-"—————-""—"———1,1-dichloroethane"--"-----"-"---""""""----""-----"""------"-""--""---"----""1,1 -dichloroethene---"--------"---"-"""""""""""--"-"-""-"-—————•—-—

cis -1,2-dichloroethene————————————————————————

/"ne .•\ Q /4tr*hlftrrtnmn&nQ — >•——.—- -

1 1 ^ f) fofra^hlnrnothano •••—•••••—•••••••••«—•—•——• ••——•••-

+riphlnmpthono———— ———.>••.-—>.—•. ——..—.— ——.—

nffi a.. dY\(\le\v mfs'f'a —w/lorto - •.

* ND —• Means not detected above the listed detection limits.

Results*

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

Detection Limits

n Û.vJ

0.5n ^n'?U.%J

n £;0.5n Û.*J

n ^0.5n t;u.«^

0.5n ^n û.»^

0.5n ^n t;u.\^

0.5n '5U.%J

0.50.5n Û.«J

0.50.50.50.50.50.50.5n ^w.*J

0.50.50.50.50.50.5

9T5BCC03




TENTATIVELY IDENTIFIED VOLATILE COMPOUNDS BY METHOD 624*

001—^

><1OJto

Number of tentatively identified compounds reported-———1

units - IJQ/ITIC CAS NumberNo.

Compound Name

tetrahydro-Furan

RT Estimated **(min.) Concentration

1 000109-99-9

2

3

4

5

6

7

8

9

10

9.00 6.4

* Analyst's Note. The compounds listed are tentatively identified by the best match with theNIST/EPA/Wiley mass spectral data base, and/or by manual interpretation.Standards were not used for confirmation.

** Estimated concentration is obtained by quantitation using the nearest internal standard.Since no external standard is used, a response factor of 1.0 is assumed.

9T5BCC03

A-doar^"• — ^

U. S. Environmental Protection AgencyRegion 6 Houston Laboratory

Report For Sample Number 9T5BCC0302


Site Description; 3^ , g

oo•<iuOJ



Sample Type: LIQUID

Comments:

ParameterABMCMMAAMHG

MICPS04

TDSVOA

DescriptionACID/BASE NEUTRALSCYANIDEGFAAS METALSMERCURYICP METALSSULFATETOTAL DISSOLVED SOLIDSVOLATILE ORGANIC ANALYSIS

9T5BCC03


Sample Number: 9T5BCC03-02

Site Name: Delatte Metals


Date Extracted: 3-Feb.-99

Date Analyzed: 3-Feb.-99

units - microgram/liter - (JQ/I

00>—*--3UJ•

Compound Name Results* Detection Limits

acetone——————————————————————————————— ND 0.5ht^rt7^nQ_—•—•.—•—•——••••—<•••••••••—•——.————••———••••———————•»—_ • Mf^ n Ud HLVl [^-•>————————— ————————————— - ————— _ ———r——— |\L«/ \J,*-f

bromodichloromethane———————————————————————— ND 0.5bromoform————————————————————————————— ND 0.52-butanone————————————————————————————•- ND 0.5bromomethane—————————————————————————— ND 0.5carbondisulfide——————————————————————————— ND 0.5carbontetrachloride———————————————————————— ND 0.5chlorobenzene——————————————————————————— ND 0.5critoroGtncinG~~"~~~~~~~"*~~~"~*~~~~~"~~*~"~~"~""~~~"~~~~"~~~~~~~~"~~~"~"**~~"~~"~"~~~'"''''''' INL^ u.ochloroform————————————————————————————— ND 0.5chloromethane-———————————————————————————— ND 0.5dibromochloromethane—————————————————————— ND 0.51,1-dichloroethane————————————————————————— ND 0.51.1-dichioroethene————————————————————————— ND ' 0.51.2-dichloroethane———————-—•————————————————— ND 0.5c/s-1,2-dichloroethene————————————————————————— ND 0.5frans-1,2-dichloroethene—————————————————————— ND 0.51,2-dichloropropane————————————————————————— ND 0.5c/s-1,3-dichloropropene——————————————————————— ND 0.5frans-1,3-dichloropropene—————————————————————— ND 0.5ethylbenzene-—————————————————————————— ND 0.52-hexanone———————————————————————————— ND 0.5methylene chloride————————————————————————— ND 0.54-metriyl-2-pentanone——————————————————————— ND 0.5styrene—————————————————————————————— ND 0.51,1,2,2-tetrachloroethane—————————————————————— ND 0.5tetrachloroethene—————————————————————————— ND 0.5toluene——————————————————————————————— ND 0.51.1.1-trichloroethane————————————————————————— ND 0.51.1.2-trichloroethane—————————————————————————- ND 0.5trichloroethene——————————————————————————— ND 0.5vinyl chloride———————————————————————————— ND 0.5ort/io-xylene———————————————————————————— ND 0.5para- and/or meta-xy\ene—————————————————————— ND 0.5

* ND — Means not detected above the listed detection limits.

9T5BCC03

00t—t

•o

L»Ji

ORGAHIC ANALYSIS DATA6MD-HO Sample HO: 9T5BCC03-02

Analyst: B. Schuppener

SEMI-VOLATILE COMPOUNDS BY METHOD 625

(continuous extractor)units: ug/L

Date Reported: 22-Feb-99

Sample Type: WATER

units: ug/L

Compound Name Results* | Det Limits Compound Name Results* | Det Limits

Acenaphthene ...............Acenaphthylene .............

Anthracene .................

Benzole Acid ...............

Benzo (a)Anthracene .........

Benzo(a)Pyrene .............Benzo(b)Fluoranthene .......

Benzo(g, h, i)Perylene .......

Benzo(k)Fluoranthene .......

Benzyl Alcohol .............

bis(2-Chloroethoxy)Methane .

bis(2-Chloroethy].) Ether ...

bis(2-chloroisopropyl)Ether

bis- (2-EthylhexyDPhthalate

4-Bromophenylphenyl Ether ..

Butylbenzylphthalate .......Carbazole ..................

4-Chloroaniline ............

2-Chloronaphthalene ........

2-Chlorophenol .............

4-Cttlorophenylphenyl Ether .

4-Chloro-3-Methylphenol ....

Chrysene ...................Dibenzofuran ...............

Dibenzo(a,h)Anthracene .....

1.2-Dichlorobenzene ........1.3-Dichlorobenzene ........

1.4-Dichlorobenzene ........

3,3'-Dichlorobenzidine .....2,4-Dichlorophenol .........

Diethylphthalate ...........

2,4-Dimethylphenol .........

DimethylPhthalate ..........

NDNDNDNDMDNDNDNDNDKDNDNDNDMDHDNDMDHDHDNDNDNDMDNDNDNDMDNDNDMDNDNDND

2

22

10

8

0.2

8

8

8

4

2

2

2

4

8

4

24

2

4

8

8

82

8

3

3

3

10

6

2

2,4-Dinitrophenol . . . . . . . . .2,4-Dinitrotoluene . . . . . . . .2,6-Dinitrotoluene . . . . . . . .4,S-Dinitro-2-MethylphenolDi-n-Butylphthalate . . . . . . .Di-n-Ootyl Phthalate . . . . . .Fluoranthene . . . . . . . . . . . . . .Fluorene . . . . . . . . . . . . . . . . . .Hexachlorobenzene . . . . . . . . .Hexachlorobutadiene . . . . . . .Hexachlorocyclopentadiene .Hexachloroethane . . . . . . . . . .Indeno(l,2,3-cd) Pyrene . . .Isophorone . . . . . . . . . . . . . . . .2-Methylnaphthalene . . . . . . .2-Methylphenol . . . . . . . . . . . .4-Methylphenol . . . . . . . . . . . .Naphthalene . . . . . . . . . . . . . . .2-Nitroaniline . . . . . . . . . . . .3-Nitroaniline . . . . . . . . . . . .4-Nitroaniline . . . . . . . . . . . .Nitrobenzene . . . . . . . . . . . . . .2-Nitrophenol . . . . . . . . . . . . .4-Nitrophenol . . . . . . . . . . . . .N-Nitrosodiphenylamine . . . .N-Nitroso-Di-n-PropylaminePentachlorophenol . . . . . . . . .Phenanthrene . . . . . . . . . . . . . .Phenol . . . . . . . . . . . . . . . . . . . .Pyrene . . . . . . . . . . . . . . . . . . . .1,2,4-Trichlorobenzene . . . .

_ 2,4,5-Trichlorophenol2,4,6-Trichlorophenol

NDNDNDNDNDHDNDNDNDNDNDNDNDNDNDNDNDNDNDNDMDNDNDNDMDNDNDNDMDNDNDNDND

3066202422151038426S2888210134612422066

( * ) ND = Not detected above the listed detection limit. ( * ) ND = Not detected above the listed detection limit.

Analyst Notes; none

9T5BCC03 US EPA REGION 6 LABORATORY

SAMPLE #:

SOURCE:MATRIX

ANALYSTS:

PARAMETER

ALUMINUMANTIMONYARSENICBARIUMBERYLLIUMCADMIUMCALCIUMCHROMIUMCOBALTCOPPERIRONLEADMAGNESIUMMANGANESEMERCURYNICKELPOTASSIUMSELENIUMSILVERSODIUMTHALLIUMVANADIUMZINC

9T5BCC03-02

DELATTE METALLIQUID

KD. TS, BB

CONCENTRATION

NDNDNDNDNDND

948NDNDNDND10NDNDNDNDNDNDND

69400NDNDND

S

DETECTIONLIMIT <=

10022

1022

150222

252

1502

0.22

10002

10500

22

20

DATERECEIVED:

DATES ANALYZED:03-FEB-99 1

DATEREPORTED:

UNITS

UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L

28-JAN-99

-0 25-FEB-99

26-FEB-99

METHOD

200.7200.8200.8200.7200.8200.8200.7200.8200.8200.8200.7200.8200.7200.8245.1200.8200.7200.8200.7200.7200.8200.8200.7

ND: LESS THAN DETECTION LIMIT

00I—A

---It-^0\

. . , 9T5BCC03 TNRCC Laboratory ^

S|gg Report of Analysis Sj--j

TNRCC Sampler: 9900617 GroupS:19990167 Chain of Custody #: 9T5BCC03-02 Region: 0Program Code: EPA Sample Matrix: LIQUID Sample Depth: Station ID:Sample Collected: 1/27/99 02:29 pm Sample Recieved: 1/29/99 Sample Collector; EPACollection Site: Delatte Metals

Storet Parameter Name Result Unit Prepared Analyzed Method00720 Cyanide, Total 0.02 mg/L N/A 2/3/99 16:05 335.270300 Total Dissolved Solids 174 mg/L N/A 1/29/9914:00 160.100945 Sulfate,ic 11.0 mg/L N/A 2/1/9911:08 300.0

Comments: End of Data for TNRCC Sampled :9900617

/Laboratory Approval: J,AG ———-7-r" ^^JJ^V Approval Date: ll-Feb-1999

RPISFVm 2«0ctl99» // '

9T5BCC03




Site Description: 3^ ^gg

ooi—t•~-iU)00



Sample Type: LIQUID

Comments:

ParameterABM

CH

MAA

MHG

MICP

S04

TDS

VGA


9T5BCC03





units - microgram/liter - M9/I

00i—k0(-'

Compound Name Results* Detection Limits

cir^o^nno __ _•___• _u .i_____ii.___—.•_—..—_——•_o____________wwf ___________•>•________—>i- _> _ MF" 0 ^\aL*c?iuno —.—.—«- INL./ u.w

benzene—————————————————————————————— ND 0.5bromodichloromethane———————————————————————— ND 0.5bromoform———————————————————————————— ND 0.52-butanone———————————————————————————— ND 0.5bromomethane—————————————————————————— ND 0.5carbon disulfide——————————————————————————— ND 0.5carbon tetrachloride————————————————————————— ND 0.5chlorobenzene———————————————————————————— ND 0.5chloroethane———————————————————————————— ND 0.5chloroform——————————————————————————— ND 0.5chloromethane——————————————————————————— ND 0.5dibromochloromethane—--—-———-———————————-- ————— ND 0.51,1-dichloroethane—————————————————————————— ND 0.51,1 -dichloroethene—————————————————————————— ND 0.5•1,2-dichloroethane—————————————————————————— ND 0.5o/'s-1,2-dichloroethene———————————————————————— ND 0.5fr-ans-1,2-dichloroethene——————————————————————— ND 0.51,2-dichloropropane————————————————————————— ND 0.5G/'s-1,3-dichloropropene——————————————————————— ND 0.5trans -1,3-dichloropropene—————————————————————— ND 0.5ethylbenzene———————————————————————————— ND 0.52-hexanone—————————————————————————————— ND 0.5methylene chloride-———————————————————————— ND 0.54-methyl-2-pentanone——————————————————————— ND 0.5styrene—————————————————————————————— ND 0.51,1,2,2-tetrachloroethane——————————————————————— ND 0.5tetrachloroethene—————————————————————————— ND 0.5

1.1.1-trichloroethane———————————————————————— ND 0.51.1.2-trichloroethane———————————————————————— ND 0.5trichloroethene——————————————————————————— ND 0.5vinylchloride——————————————————————————— ND 0.5o/t/io-xylene———————————————————————————— ND 0.5para- and/or me^a-xylene————————————————————— ND 0.5


9T5BCC03

ORGANIC ANALYSIS DATA6MD-HO Sample NO: 9T5BCC03-03 Date Reported: 22-Feb-99

Analyst: B. Schuppener Sample Type: WATER

SEMI-VOLATILE COMPOUNDS BY METHOD 625(continuous extractor)

units; ug/L units; ug/L

Compound Name

bis(2-Chloroethyl) Ether ....

bis-(2-EthylhexyDPhthalate .

Diethylphthalate ............

DimethylPhthalate ............

j Results*

........ MD -

........ MD

........ KD

........ ND

........ HD

........ ND

........ ND

........ HD....... HD....... MD....... ND....... MD....... MD....... ND....... MD....... MD....... MD....... ND....... ND....... MD....... MD....... ND....... ND....... MD....... ND....... ND....... ND....... MD....... ND....... ND....... MD....... ND....... ND

| Det Limits

222

108

0.288842224842424

2

333

106262

Compound Name

Di-n-Octyl Phthalate ...............

2-Mitroaniline .....................3-Nitroaniline .....................

| Results*

MDMDMDMDNDNDHDNDNDMDKDNDNDNDNDNDNDNDMD

.. ' NDNDNDMDMDMDNDNDNDNDMDMDMDND

Det Limits

3066

20242215

1038'

4

6628

82

1013461242

2066

(*) ND = Not detected above the listed detection limit.

lalyst Notes: none

(*) ND - Mot detected above the listed detection limit.

9T5BCC03

ORGANIC ANALYSIS DATA6MD-H Sample NO;9T5BCC03-03

Analyst; B. Schuppener

TENTATIVELY IDENTIFIED SEMI-VOLATILE COMPOUNDS BY METHOD 625

00I—t•<l

Date Reported: 22-Feb-99 -

Matrix: WATER

units s ug/L

RT (min)

6 . 3

---————-----

(* ) ANALYSTS HOTspectral dat

(**) Estimated c

CAS #

E: The compoundsa base or by man

oncentratlon is

• COMPOUND NAME (*)

Unknown

listed are tentatively identified by the best match with the NISual interpretation.

based on a Response Factor of 1.0 to the nearest internal standar

EstimatedConcentration (**)

1

————————J

T/EPA/Wiley mass

d.

.

SAMPLE #:

SOURCE:MATRIX

ANALYSTS:

PARAMETER C


ND: LESS THAN

US

9T5BCC03-03

DELATTE METALSLIQUID

KD,TS, BB

ONCENTRAT10N

NDNDNDNDNDND

1990NDNDND5410

84826NDNDNDNDND

67400NDNDND

DETECTION LIMIT

S EPA REGION

DETECTIONLIMIT <=

10022

1022

150222

252

1502

0.22

10002

10500

22

20

6 LABORATORY

DATERECEIVED:

DATES ANALYZED:03-FEB-99 T

DATEREPORTED:

UNITS


9

28-JAN-99

'0 25-FEB-99

26-FEB-99

METHOD

200.7200.8200.8200.7200.8200.8200.7200.8200.8200.8200.7200.8200.7200.8245.1200.8200.7200.8200.7200.7200.8200.8200.7

9T5BCC03

00I—I

--J4^10

"5s ^s

TNRGGTNRCC Sampler: 9900618Program Code: EPASample Collected: 1/27/99 02:42 pmCollection Site: Delatte Metals

Storet Parameter Name00720 Cyanide, Total70300 Total Dissolved Solids00945 Sulfate, ic

Comments:

Laboratory Approval: flA <'—RP18FYNI. 2tOctlS98 /

TNRCC LabReport of Ai(

GroupS:19990167Sample Matrix: LIQUIDSample Recieved: 1/29/99

Result Unit<0.02 mg/L

166 mg/L7.0 mg/L

End of Data for TNRCC Sarr

)oratorynalysis

Chain of Custody,!Sample Depth:Sample Collector:

PreparedN/AN/AN/A

^ple#:9900618

^~\ ft /

Wf/ry^-

s:

f

12

9

9T5BCCO:

EPA

Analyzed-/3/99 16:05/29/99 14:00-/1/99 11:31

Approval

T5BCC03 00)—1

>--!4^

3-03 Region: 0Station ID:

Method335.2160.1300.0

Date: ll-Feb-1999

9T5BCC03




Site Description: sTA.WW.07B

o0»—l

S



Sample Type: LIQUID

Comments:

ParameterABMCNMAAMHG

MICPS04

TDS

VGA

DescriptionACID/BASE MEUTRALSCYANIDEGPAAS METALSMERCURYICP METALSSULB-ATETOTAL DISSOLVED SOLIDSVOLATILE ORGANIC ANALYSIS

9T5BCC03

ORGANIC ANALYSIS DATA00>--l

Sample Number: 9T5BCC03-04 Date Extracted: 3-Feb.-99 ^



_________________________________units - microgram/liter- IJQ/ICompound Name Results* Detection Limits

acetone——————————————————————————————— ND 0.5benzene————————————————————————————— ND 0.5bromodichloromethane——————————————————————— ND 0.5bromoform——————————————————————————— N D 0.5

bromomethane—————————————————————————— ND 0.5carbondisulfide———————————————————————————— ND 0.5carbontetrachloride————————————————————————— ND 0.5chlorobenzene——————————————————————————— ND 0.5chloroethane———————————————————————-————- ND 0.5chloroform————————————————————————————— ND 0.5chloromethane——————————————————————————— ND 0.5dibromochloromethane—————————————————————— ND 0.51,1-diGhloroethane————————————————————————— ND 0.51.1-dichloroethene————————————————————————— ND 0.51.2-dichioroethane——————————————————————-——- ND 0.5cis -1,2-dichloroethene-——————————————————————— ND 0.5fr-ans-1,2-dichloroethene—————————————————————— ND 0.51,2-diGhloropropane———————————————————————— ND 0.5c;/s-1,3-dichloropropene-—————————————————————— ND 0.5//•ans-1,3-dichloropropene—————————————————————— ND 0.5ethylbenzene———————————————————————————— ND 0.52-hexanone————————————————————————————— ND 0.5methylene chloride————————————————————————— ND 0.54-methyl-2-pentanone———-——-—————————————————— ND 0.5styrene—————————————————————————————— ND 0.51,1,2,2-tetrachloroethane——————————————————————— ND 0.5tetrachloroethene————————————————————————— ND 0.5

1.1.1-trichloroethane———————————————————————— ND 0.51.1.2-trichloroethane—————————————————— -—————- ND 0.5trichloroethene——————————————————————————— ND 0.5vinyl chloride———————————————————————————— ND 0.5orf/io-xylene——————————————————————————— ND 0.5para- and/or /neta-xylehe—————————————————————— ND 0.5


9T5BCC03

6MD-HO Sample NO: 9T5BCC03-04


Compound Name

bis(2-Chloroethyl) Ether .........

bis-(2-Ethylhexyl)Phthalate ......

SB

units:

I Results*

HDNDNDMDMDNDNDHDMDMD

• NDKDHDMDNDMDNDMDMD

HDND

KDHDNDNDNDND .NDND

NDNDNDND

ORGANIC 1

•MI-VOLATILE COt(continuol

ug/L

| Det Limits

222

108

0.288842224842424

333

106262

ANALYSIS DATA

WOUNDS BY METHOD 625us extractor)

Compound Name

4,6-Dinifcro-2-Methylphe

Di-n-Octyl Phthalate ..

2-Methylphenol ........

3-Nitroaniline ........4-Mitroaniline ........

2-Hitrophenol .........

Date Reported:

Sample Type:

units

| Results

.......... MD

.......... ND

.......... ND

....;..... ND

.......... MD

.......... MD

.......... MD

.......... MD

.......... ND

.......... MD

.......... ND

.......... ND

.......... MD

.......... MD

.......... ND

.......... ND

.......... MD

.......... ND

.......... MD

.......... ND

.......... ND

.......... MD

.......... ND

.......... ND

.......... ND

.......... ND

.......... MD

.......... MD

.......... ND

.......... MD

.......... ND

.......... ND

.......... ND

*

00t—t

--I4^G^

22-Feb-SS

WATER

ug/L

| Det Limits

3066

20242215

1038426628882

1013

461242

2066

(*) MD ° Not detected above the listed detection limit.

lalyst Notes: none

(*) MD = Mot detected above the listed detection limit.

SAMPLE #:

SOURCE:MATRIX

ANALYSTS:

PARAMETER


ND: LESS THA

U

9T5BCC03-04


KD, TS, BB

CONCENTRATION

NDNDNDNDNDND

586NDNDND3411ND

4NDNDNDNDND

67400NDNDND

N DETECTION LIMIT

S EPA REGION

DETECTIONLIMIT <=

10022

1022

150222

252

1502

0.22

10002

10500

22

20

6 LABORATORY

DATERECEIVED:

DATES ANALYZEC03-FEB-99

DATEREPORTED:

UNITS


9T5BCC03

28-JAN-99

):TO 25-FEB-99 —

26-FEB-9902 ,

METHOD ^<1

200.7 &—200.8200.8200.7200.8200.8200.7200.8200.8200.8200.7200.8200.7200.8245.1200.8200.7200.8200.7200.7200.8200.8200.7

TNRGG

TNRCC LaboratoryReport of Analysis

9T5BCC03

TNRCC Sample #: 9900619Program Code: EPASample Collected: 1/27/99 03:08 pmCollection Site: Delatte Metals


Comments:

Laboratory Approval: |{/[(RP15FYNL ZBOctlMt

Groupfe 1999016Sample Matrix: ISample Recieved:

Result<0.02

1569.0

End of Data for I

... -————-6

7LIQUID

1/29/99

Unitmg/Lmg/Lmg/L

FNRCC Saa

Chain of Custody^Sample Depth:Sample Collector:

PreparedN/AN/AN/A

nple#:9900619

A/y

»:

/i

9T5BCCO:

EPA

Analyzed'/3/99 16:05/29/99 14:002/1/99 15:43

Approval

3-04 Region:Station II

Metho335.2160.1300.0

Date: 11-Ff

0D:

d

2b-1999

001—1

00

9T5BCC03


Report For Sample Number 9T5BCCO 3 0 5


Site Description: g- ^3


Date/Time Collected: 1/27/1999 11:07PM

Sample Type: LIQUID

Comments:

00»—i

^

ParameterABCT

CN

MAAMHO

MICPS04

TDSVOA


9T5BCC03







units - microgram/liter - [Jg/1Compound Name Results* Detection Limits

acetone———————————————————————————————— ND . 0.5benzene——————————————————————————————— ND 0.5bromodichloromethane——————————————————————— ND 0.5bromoform---———————————————————————————— ND 0.52-butanone——————————————————————————— ND 0.5bromomethane—————————————————————————— ND 0.5carbon disulfide——————————————————————————— ND 0.5carbon tetrachloride——————————————————————— ND o.5chlorobenzene—————————————————————————— ND 0.5chloroethane——————————————————————————— ND 0.5chloroform———————————————————————————— ND 0.5chloromethane——————————————————————————— ND 0.5dibromochloroiTiethane—------——————————————————-—— ND 0.51,1-dichloroethane———————————-————-—————————— ND 0.51.1-dichloroethene————————————————————————— ND 0.51.2-dichloroethane————————————————————————— ND 0.5c/s-1,2-dichloroethene———————————————————————— ND 0.5trans -1,2-dichloroethene—————————————————————— ND 0.51,2-dichloropropane———————————————————————— ND 0.5cis -1,3-dichloropropene-——————————————————————— ND 0.5trans -1,3-dichloropropene—————————————————————— ND 0.5ethylbenzene——————————————————————————— ND 0.52-hexanone———————————————————————————— ND 0.5methylene chloride————————————————————————— ND 0.54-methyl-2-pentanone——————————————————————— ND 0.5styrene—————————————————————————————— ND 0.51,1,2,2-tetrachloroethane—————————————————————— ND 0.5totrQ^'hlor/^othonQ —••••—_•_._• _ —•r—.r _ • _ ———•••—• MF"^ C\ ^\Ldt ClUI IIUI UGLI Id ic'"'"""'"""'"'"""""'"•—•-—•—•—————"———-"•———————-—"- •"—"——————*•——»— 1NL/ U.iJ

1.1.1-trichloroethane————————————————————————— ND 0.51.1.2-tricriloroetriane———————————————————————— ND 0.5trichloroethene——————————————————————————— ND 0.5vinyl chloride——————————————————————————— ND 0.5o/f/io-xylene———————————————————————————— ND 0.5para- and/or mera-xylene————————————————————— ND 0.5


9T5BCC03

ORGANIC ANALYSIS DATA6MD-HO Sample NO: 9T5BCC03-05 Date Reported: 22-Feb-SS

Analyst; B. Schuppener Sample Type: WATER

Compound Name

bis(2-Chloroetayl) Ether ..

bia-(2-Ethylhexyl)Phthalate

Diethylphthalate ..........

) DimethylPhthalate .........

1

(*) ND = Not detected above

Analyst Notes: none

SB

units:

( Results*

.......... ND

.......... ' ND -

.......... ND

.......... ND

.......... ND

.......... ND

.......... ND

.......... ND

.......... ND

.......... ND

.......... ND

.......... ND......... ND......... ND......... ND......... ND

.......... ND......... ND......... ND......... ND......... ND......... ND......... ND......... ND......... ND......... ND......... ND......... ND......... ND......... ND......... ND......... ND......... ND

the listed detection

MI-VOLATILE CO(continue!

ug/L

Det Limits

2'2

210

80.2

S8842224

. 84242488

2

333

106262

limit.

MPOONDS BY METHOD 625us extractor)

Compound Name

Di-n-Octyl Phthalate ..........

2-Mltroaniline ................3-Nitroaniline ................

Phenol ........................

i*) ND = Not detected above the

units: ug/L

| Results* | Det

....... ND

....... ND

....... ND

....... ND

....... ND

....... MD

....... ND

....... ND

....... ND

....... ND

....... ND

....... ND '

....... ND

....... MD

....... ND

....... ND

....... ND Q...... ND 0

....... ND ^...... ND <- 1

1—l....... ND...... ND...... ND...... ND...... ND...... ND...... ND

...... ND

...... ND

...... ND

...... HD

listed detection limit.

Limits

3066

2024221

510

3— ~B

4--2-

6" 6^V

"""8"'88

,. ^-2: 10..••13

461

2-42

20

66

9T5BCC03

ORGANIC ANALYSIS DATA6MD-H Sample NOs9T5BCC03-05




Matrix: WATER

units: ug/L

RT (min)

9 . 4

——————————

(*) ANALYSTS N01spectral dat

(**) Estimated c

CAS #

85449

CE: The compoundsa base or by man

oncentration is

COMPOUND NAME ( * )

Phthalic anhydride4

listed are tentatively identified by the best match with the NISlual interpretation.

based on a Response Factor of 1.0 to the nearest internal standar

EstimatedConcentration (**)

1

•

00

L/i——————.———.-——— -———.^J

------——--—-----—

T/EPA/Wiley mass

-d.

SAMPLE #:

SOURCE:MATRIX

ANALYSTS:

PARAMETER


ND: LESS THA

US

9T5BCC03-05


KD.TS, BB

CONCENTRATION

NDNDNDNDNDND


70600NDNDND

<N DETECTION LIMIT

3 EPA REGIOIS

DETECTIONLIMIT <=

10022

1022

150222

252

1502

0.22

10002

10500

22

20

j 6 LABORATORY

DATERECEIVED:


DATEREPORTED:

UNITS


9T5BCC03

28-JAN-99

0 25-FEB-99

26-FEB-99

METHOD

200.7200.8200.8200.7200.8 "200.8 0 . :200.7 2 : '200.8 ^200.8 ^200.8 ——200.7 -200.8200.7200.8245.1200.8200.7200.8200.7200.7200.8200.8200.7

TNRGGTNRCC Sample #: 9900620Program Code: EPASample Collected: 1/27/99 11Collection Site: Delatte Metals


Comments:

/Laboratory Approval; f

RP15PYN1. 280C11SM V

:07

u<

am

ft

TNRCC LabReport of Ai

i

GroupS; 19990.167Sample Matrix: LIQUIDSample Recieved: 1/29/99

Result Unit0.02 mg/L

172 mg/L11.0 mg/L

End of Data for TNRCC San

. ^

moratorynalysis

Chain of CustodySample Depth:Sample Collector:

PreparedN/AN/AN/A

nple# :9900620

A/H——

#:

/

12

9T5

9T5BCC03-05

EPA

Analyzed-/3/99 16:05/29/99 14:00/10/99 15:44

Approval Dat

BCC03

Region: 0Station ID:

Method335.2160.1300.0

e: ll-Feb-1999

9T5BCC03




Site Description: 3^ ^


Date/Time Collected: 1/27/1999 10:34PM

Sample Type: LIQUID

Comments:

ParameterABN

CN

MAAMHG

MICPS04

TDS

VOA


00>—i0^1

9T5BCC03





_________________________________units - microgram/liter - w/\Compound Name Results* Detection Limits

DGnZGnG"''"'1""'"'"*""'"'*'''''"'"""'""""'"'''*'"'"''""""""""""'''''"'''"''"'""""""'""'"'"""""^""'"'""""""""""""""'""'"'""""'""'"'"" IN Li/ u.O

bromodichloromethane———————————————————————— ND 0.5brom oform————————————————————————————— N D 0.52-butanone—————————————————————————————- ND 0.5bromomethane———————————————————————-——— ND 0.5carbondisulfide—————————————————————-———-—— ND 0.5carbontetrachloride————————————————————————— ND 0.5chlorobenzene——————————————————————————— ND 0.5chloroethane———————————————————————————— ND 0.5chloroform————————————————————————————— ND 0.5chloromethane——————————————————————————— ND 0.5dibromochloromethane———————————————————————— ND 0.51,1 -dichloroethane—————————————————————————— ND 0.51,1 -diGhloroetriene————————————————————————— ND 0.51,2-dichloroethane—————————————————————————— ND 0.5G/'s-1,2-dichloroethene———————————————————————— ND 0.5fr-ans-1,2-dichloroethene——————————————————————— ND 0.51,2-d i chloropropane———————————————————————— N D 0.5c/s-1,3-dichloropropene——————————————————————— ND 0.5&-ans-1,3-dicriloropropene——————————————————————— ND 0.5ethylbenzene———————————————————————————— ND 0.52-hexanone————————————————————————————— ND 0.5rnethylene chloride————————————————————————— ND 0.54-methyl-2-pentanone-—————————————————————— ND 0.5

1,1,2,2-tetrachloroethane————————————————————— ND 0.5tetrachloroethene————————————————————————— ND 0.5

1.1.1-trichloroethane———————————————————————— ND 0.51.1.2-trichloroethane———————————————————————— ND 0.5trichloroethene——————————————————————————— ND 0.5vinyl chloride———————————————————————————— ND 0.5ort/io-xylene———————————————————————————— ND 0.5para- and/or mefa-xylene———————————————————.——-— ND 0.5


0 „_o w-^I—I

-<!i

0\



Compound Name |

bis(2-Chloroethyl) Ether ............

bis-(2-Ethylhexyl)Phthalate .........

4-Chloro-3-Methylpbenol .............

| Diethylphthalate ....................

(*) MD = Not detected above the listed

toalyst Notes: none

SE1

units:

Results*

MDNDNDNDKDMDNDMDMDMDMDNDMDMDMDNDMDMDMDMDMDMDNDNDMDNDMDNDMDMDMDNDMD

detection

ORGANIC 1

MI-VOLATILE COt(continuol

ug/L

Det Limits

2

22

10e

0.288

422248424248885

333

10626

limit.

ANALYSIS DATA

MPOUNDS BY METHOD 625as extractor)

Compound Mame

Di-n-Octyl Phthalate ......

2-Mitroaniline ............3-Nitroaniline ............4-Nitroaniline ............

2-Mitrophenol .............

Phenol ....................

(*) ND « Mot detected above

9T5BCC03

Date Reported:

Sample Type:

units:

| Results*

........... ND

........... ND

........... MD

........... MD

........... MD

........... MD

........... ND

........... ND

........... ND

........... MD

........... ND

........... MD

........... MD

........... ND

........... MD

........... ND

........... ND

........... KD

........... ND

........... ND

........... MD

........... MD

........... ND

........... ND

........... MD

........... ND

..... . . . . . . MD

........... ND

........... ND

........... MD

........... MD

........... ND

........... MD

the listed detection 1

22-Peb-99

WATER

ug/L

Det Limits

306

• 620

2422

,... 3.

0 ~s0 -10^ -,U-l 8

-~1

2

6628

21013461

242

2066

imit.

^

9T5BCC03

ORGANIC ANALYSIS DATA6MD-H Sample NO:9T5BCC03-06

Analyst: B. Schuppener .


Date Reported: 22-Feb-9.9.

Matrix: WATER

units: ug/L

EstimatedRT (min) CAS ft COMPOUND NAME (*) Concentration (**) |

14.0 Unknown ' 3 |———————— ————————— ——————————————————————————————————————————— -——.--.-.--.——————]

14.1 83688862 2-Methyl-6-tridecylpiperidine 2 j———————— ————————— ————————————.——————————————————————————————— ————————————.-.- j

15.0 Unknown 6 ' |———————— —————————— —————————————————————————————————————————— ———————————————I

15.1 Unknown 2

- - —— Q0

.-—————————————————__————.. —-——-—--—-- -— .^—^

^———————————————— ——————<-^

00

(*) ANALYSTS NOTE: The compounds listed are tentatively identified by the best match with the NIST/EPA/Wiley massspectral data base or by manual interpretation.

(**) Estimated concentration is based on a Response Factor of 1.0 to the nearest internal standard.

SAMPLE #:

SOURCE:MATRIX

ANALYSTS:

PARAMETER


1.

9T5BCC03-06

DELATTE METALLIQUID

KD,TS, BB

CONCENTRATION

NDNDNDNDNDND

1200NDNDND4710

257NDNDNDNDNDND

70000NDNDND

JS EPA REGIOts

S

DETECTIONLIMIT <=

10022

1022

150222

252

1502

0.22

10002

10500

22

20

^ 6 LABORATORY

DATERECEIVED:


DATEREPORTED:

UNITS


9T5BCC03

28-JAN-99

-0 25-FEB-99

26-FEB-99

METHOD

200.7200.8 :200.8 0 .„:200.7 ' 2 E

200.8 ^200.8 ^0 --—200.7200.8200.8200.8200.7200.8200.7200.8245.1200.8200.7200.8200.7200.7200.8200.8200.7


S3%RGGTNRCC Sampler: 9900621Program Code: EPASample Collected: 1/27/99 10:34 amCollection Site: Delatte Metals

Storet Parameter Name00720. Cyanide, Total70300 Total Dissolved Solids00945 Sulfate, ic

Comments:

Laboratory Approval: j [ /^C-RP15FYNL 2aOct)S»» '

•

TNRCC Laboratory ^BCOOS pagessReport of Analysis

Groupff: 19990167 Chain of Custody #: 9T5BCC03-06 Region: 0Sample Matrix; LIQUID Sample Depth: Station ID:Sample Recieved: 1/29/99 Sample Collector: EPA

Result Unit Prepared Analyzed Method<0.02 mg/L N/A 2/3/9916:05 335.2

168 mg/L N/A 1/29/9914:00 . 160.111.0 mg/L N/A 2/1/9915:45 300.0

End of Data for TNRCC Sampled :9900621

, ,——————^— ~^^y/yy Approval Date: ll-Feb-1999// \ f f • " " l•^

v

001—*•oa\0

9T5BCC03




Site Description: sTA.VWV.02B

00I—I

--ja\Date/Time Received: 1/28/1999 09:30 AM Date Completed 3/1/1999

Date/Time Collected: 1/27/1999 10:03 AM

Sample Type: LIQUID

Comments:

ParameterABNCN

MAAMHG

MICPS04

TDS

VOA


9T5BCC03





_________________________________units - microgram/liter - |JQ/ICompound Name Results* Detection Limits

ar'ofnnPr—— »—•<•••.•.—•»•._—..•- —_- __•.——•.—_•••.••••—•———•——————————.————————— MF^C1UCLUI ic ~ " ————»•..—...—-—.—— - — |\L/

benzene—————————————————————————————— NDbromodichloromethane———————————————————————— NDbromoform————————————————————————————— ND2-butanone————————————————————————————— NDbromomethane——————————————————————————— NDcarbon disulfide——————————————————————————— NDcarbon tetrachloride—————————— -——————————————— NDchlorobenzene——————————————————————————— NDchloroethane———————————————————————————— NDchloroform———————————————————————————— NDchloromethane———————————————————————————— NDdibromochloromethane———————————————————————— ND1,1 -dichloroethane—————————————————————————— ND1,1 -dicriloroethene——————————————————————-———— ND1,2-dichloroethane—————————————————————————— NDCT's-1,2-dichloroethene-—-——--——————————————————— NDfr8/7s"1,2-dichloroethene——-———-—--------———————-————-— ND1,2-dichloropropane———————————————————————— NDG/s-1,3-dichloropropene——————————————————————— NDfr"ans-1,3-dichloropropene——————-——————————————— NDethylbenzene———————————————————————————— ND2-hexanone————————————————————————————— NDmethylene chloride————————————————————————— ND4-methyl-2-pentanone— ————— ————— ————— ——————-— NDstyrene——————————————————————————————— ND1,1,2,2-tetrachloroethane——————————————————————— NDtetrachloroethene—————————————————————————— ND

1,1,1 -trichloroethane————————————————————————— ND1,1,2-trichloroethane————————————————————————— NDtrichloroethene——————————————————————————— NDvinyl chloride———————————————————————————— NDorf/po-xylene———————————————————————————— NDpara - and/or meta -xylene—————————————————————— ND


0.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.5

A



Compound Name |

bis(2-Chlorosthyl) Ether ............


DimethylPhthalate ...................

(*) MD = Not detected above the listed

toalyst Notes: none

SB

units:

Results*

NDNDNDNDMDMD

NDNDNDNDNDMDHDMDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

detection

ORGANIC 1


ug/L

| Det Limits.

222

108

0.2888

42

224842

4 -

4

2

3

33

106262

limit.

ANALYSIS DATA

IPOONDS BY METHOD 625as extractor)

Compound Name


2-Methylphenol ............

2-Nitrophenol .............

Phenol ....................

(*) ND = Mot detected above

9T5BCC03

Date Reported:

Sample Type:

units:

] Results*

........... MD

........... MD

........... ND

........... ND

........... ND

. . . . . . . . . . . ND

........... MD

........... ND

........... ND

........... ND

........... MD

........... MD

........... KD

........... MD

........... MD

........... ND

........... MD

........... MD

........... MD

........... MD.......... ND

........... MD.......... MD

........... ND.......... MD.......... MD.......... MD.......... MD.......... ND.......... MD.......... ND

.......... ND

.......... ND

the listed detection

22-Feb-99

WATER

ug/L

| Det Limits

3066

202

- 4

- .2: 2|Ei

§ -s^——/ ——

^ -10-<1 ...,...0\ 3

LO -a4266

28882

1013461242

2066

1

limit.

SAMPLE #:

SOURCE:MATRIX

ANALYSTS:

PARAMETER


L

9T5BCC03-07

DELATTE METALLIQUID

KD, TS,BB

CONCENTRATION

NDNDNDNDNDNDNDNDNDNDND12ND1 1NDNDNDNDND

966NDNDND

JS EPA REGIOh

S

DETECTIONLIMIT <=

10022

1022

150222

252

1502

0.22

10002

10500

22

20

^ 6 LABORATORY

DATERECEIVED:


DATEREPORTED:

UNITS


9T5BCC03

28-JAN-99

"0 25-FEB-99

26-FEB-99

METHOD

200.7200.8200.8200.7200.8 — -200.8200.7200.8 § ^200.8 ^ .--.--200.8 0 .200.7 ^ ——200.8 ———-200.7 -200.8245.1200.8200.7200.8200.7200.7200.8200.8200.7


TiiSccTNRCC Sample#: 9900622Program Code: EPASample Collected: 1/27/99 10:03 amCollection Site: Delatte Metals

Storet Parameter Name00720 Cyanide, Total703 00 Total Dissolved Solids00945 Sulfate, ic

Comments:

jj j /Laboratory Approval: 1 Ai—" A A .——//'U' '•————

RP15FYNL 2»0ct1898 V


i,

Group;?: 19990167 Chain of CustodySample Matrix: LIQUID Sample Depth:Sample Recieved: 1/29/99 Sample Collector:

Result Unit Prepared<0.02 mg/L N/A

202 mg/L N/A7.0 mg/L N/A

End of Data for TNRCC Sample# :9900622

? , Gx^J.... ....... ... ,.,- ... ...-„. ^^L.r/.^—

9

S: 9T5BCCO

EPA

Analyzed2/3/99 16:051/29/99 14:002/1/99 15:46

Approval

T5BCC03

3-07 Region: 0Station ID:

Method335.2160.1300.0

Date: ll-Feb-1999

9T5BCC03




Site Description: 3^ ^g



Sample Type: LIQUID

Comments: 00>—i•<!0-Na\

ParameterABKTCN

MAAMHGMICP

S04

TDS

VOA


9T5BCC03





___________________________________units - microgram/liter - ug/1JR^ults* | Detection LimitsCompound Name

hQri'7Qri&——————— • ————————————————————-—•.—•———--—__-. Mn n ^Ud 1&.GI 1C'""—-"•—-—"—•—•.—————» - • • • • 1 1 L / U.U

bromodichloromethane———————————————————————— ND 0.5bromoform————————————————————————————— ND 0.52-butanone————————————————————————————— ND 0.5bromomethane——————————————————————————— ND 0.5carbondisulfide—————————————————————————— ND 0.5carbontetrachloride————————————————————————— ND 0.5chlorobenzene———————————————————————————— ND 0.5chloroethane———————————————————————————— ND 0.5chloroform———————————————————————————— ND 0.5chloromethane——————————————————————————— ND 0.5dibromochloromethane-——————————————————————— ND 0.51,1 -dichloroethane————————————————————-———— ND 0.51,1 -dichloroethene—————————————————————————— ND 0.51,2-dichloroethane—————————————————————————— ND 0.5c/s-1,2-dichloroethene———————————————————————— ND 0.5frans-1,2-dichloroethene—————————————————————— ND 0.51,2-dichloropropane———————————————————————— ND 0.5c/s-1,3-dichloropropene——————————————————————— ND 0.5fr-ans-1,3-dichloropropene—————————————————————— ND 0.5ethylbenzene———————————————————————————— ND 0.52-hexanone-———————————————————————————- ND 0.5methylenechloride————————————————————————— ND 0.54-methyl-2-pentanone———————————————————————— ND 0.5styrene——————————————————————————————— ND 0.51,1,2,2-tetrachloroethane——————————————————————— ND 0.5tetrachloroethene-————————————————————————— ND 0.5toluene——————————————————————————————— ND 0.51 , 1 , 1 -trichloroethane————————————————————————— ND 0.51,1,2-trichloroethane————————————————————— ——.-- ND 0.5trichloroethene——————————————————————————— ND 0.5vinyl chloride——————————————————————————— ND 0.5

para- and/or mefa-xylene————————————————————— ND 0.5

; ND — Means not detected above the listed detection limits.

00I—I

~-j0>^

6MD-HO Sample HO: 9T5BCC03-08

analyst; B. Schuppener

Compound Name I




(*) ND - Not detected above the listed

Analyst Notes: none

SE

units:

Results*

NDMDNDMDNDNDNDNDKDHDNDNDNDNDNDNDNDNDNDKDNDNDNDKDNDNDNDMDHDNDNDNDND

detection

•

ORGANIC 1


ug/L

| Det Limits

222

108

0.28884223

484

424

2

333

106262

limit.

MTALYSIS DATA


Compound Name


2-Methylphenol ............4-Methylphenol ............

4-Nitroaniline ............

(*) MD " Mot detected above

9T5BCC03

Date Reported;

Sample Type:

units:

| Results*

........... ND

........... ND

........... ND

........... ND

........... ND

........... MD

........... ND

........... MD

........... ND

........... ND

........... ND

........... MD

........... ND

........... ND

........... MD

........... ND

........... ND

........... MD

........... NS

........... MD

........... ND

........... MD.......... NO

........... ND.......... ND.......... MD.......... ND.......... ND.......... MD.......... MD.......... MD.......... MD.......... ND


23-Peb-99

WATER

ug/L

Det Limits

3066

20- 2--4

0 ; 2

-0 - 5 1

S 1°3

" 4

26628882

101346

1242

20S6

imit.

9T5BCC03

ORGANIC ANALYSIS DATA6MD-H Sample NO:9T5BCC03-08

Analyst; ' B. Schuppener



Matrix: HATER

units: ug/L

EstimatedRT (min) CAS # COMPOUND NAME (*) Concentration (**) |

5.9 105431 3-Methyl-pentanoic acid 1 |------------ --------------- ---------------------------------------------------------------- -------------------_—i

9.4 85449 Phthalic anhydride 1

——.————————————————.——.—————————————— —————————————— ^ ^

0 ——--------------------------------—------------------ ----------------- - ^__^ ___

<1 -

———————————————————— ———————— 0\\0 [_ -

——————————————————— -—————-—— —

(*) AMALYSTS NOTE: The compounds listed are tentatively identified by the best match with the NIST/EPA/Wiley massspectral data base or by manual interpretation.

(**) Estimated concentration is based on a Response Factor of 1.0 to the nearest internal standard.


SAMPLE #:

SOURCE:MATRIX

ANALYSTS:

PARAMETER


9T5BCC03-08

DELATTE METAL!LIQUID

KD, TS, BB

CONCENTRATION

NDNDNDNDNDND


70300NDNDND

S

DETECTIONLIMIT <=

10022

1022

150222

252

1502

0.22

10002

10500

22

20

DATERECEIVED:

DATES ANALYZED:03-PEB-99 1

DATEREPORTED:

UNITS


28-JAN-99

'0 25-FEB-99

26-FEB-99

METHOD

200.7200.8200.8200.7200.8200.8200.7200.8200.8200.8200.7200.8200.7200.8245.1200.8200.7200.8200.7200.7200.8200.8200.7


00»—*

•o•<!0

TNRGG


9T5BCC03

TNRCC Sample #: 9900623Program Code: EPASample Collected: 1/27/99 11:07 amCollection Site; Delatte Metals

Group#:19990167Sample Matrix; LIQUIDSample Recieved: 1/29/99

Chain of Custody #: 9T5BCC03-08 Region: 0Sample Depth: Station ID:Sample Collector: EPA

Storet Parameter Name Result Unit Prepared Analyzed Method00720 Cyanide, Total 2/3/99 16:05 <0.02 mg/L 335.2 N/A70300 Total Dissolved Solids 1/29/99 14:00 mg/L 160.1 N/A 17800945 Sulfate, ic 2/1/99 15:46 mg/L 300.0 11.0 N/A

Comments: End of Data for TNRCC Sampled :9900623

Laboratory Approval:RPWYNt. 28001988____________

Approval Date: ll-Feb-1999

o0 :^1-=-;I—I _ 1-1

•<l -

~<1

9T5BCC03




Site Description: sTA.WW.01B


00)—t

^1-j^


Sample Type: LIQUID

Comments:

ParameterABM

CHMAA

MHGMICPS04

TDSVGA


9T5BCC03







units - microgram/liter - pg/1'I Results* | Detection LimitsCompound Name

acetone—————————————————————————————— ND 0.5hon7<an& —•»•.•• •_-.- __ »——————••—————————••••——_———•———.... NtPi n UCI I Ld 1C;"""" " —.——-——»——— - — —. - •—— — INl-/ U,»J

bromodichloromethane———————————————————————— ND 0.5bromoform———————————————————————————— ND 0.52-butanone————————————————————————————— ND 0.5bromomethane———————————————————————————- ND . 0.5carbon disulfide——————————————————————————— ND 0.5carbon tetrachloride———————————————————— -——— ND 0.5chlorobenzene——————————————————————————— ND 0.5chloroethane———————————————————————————-— ND 0.5chloroform-———————————————————————————— ND 0.5chloromethane——————————————————————————— ND 0.5dibromochloroiriethane--————————————————————————- ND 0.51,1-dichloroethane—————————————————————————— ND 0.51.1-dichloroethene—————————————————————————— ND 0.51.2-dichloroethane—————————————————————————— ND 0.5cis -1,2-dichioroethene———————————————————————— ND 0.5trans -1,2-dichloroethene————————————————————— ND 0.51,2-dichloropropane————————————————————————— ND 0.5cfe-1,3-dichloropropene——————————————————————— ND 0.5frans -1,3-dichloropropene—————————————————————— ND 0.5ethylbenzene———————————————————————————— ND 0.52-hexanone————————————————————————————— ND 0.5methylene chloride————————————————————————— ND 0.54-methyl-2-pentanone———————————————————————— ND 0.5styrene——————————————————————————————— ND 0.51,1,2,2-tetrachloroethane———————————————————————— ND 0.5tetrachloroethene—————————————————————————— ND 0.5toluene——————————————————————————————— ND 0.51,1 ,l-trichloroethane—————————————————————————— ND 0.51,1,2-trichloroethane————————————————————————— ND 0.5trichloroethene——————————————————————————— ND 0.5vinyl chloride———•-—-—————————————————————— ND 0.5orf/io-xylene———————————————————————————— ND 0.5para- and/or meta-xy\ene—————————————————————— ND 0.5


00i—»-<lUJ

1 , t.



) Compound Name |


bis-(2-Efchylhexyl)Phthalate .........


(*) ND « Not detected above the listed

analyst Notes: none

SE

units:

Results*

ND

MDNDNDNDNDNDNDNDNDNDNDNDNDMDNDNDNDMDNDNDNDNDNDNDMDNDMDNDNDNDNDMD

detection

ORGANIC 1

MI-VOLATILE COr

(continuolug/L

| Det Limits

222

108

0.28 |8842224842424

2

333

106262

limit.

RMALYSIS DATA

IPOUNDS BY METHOD 625us extractor)

Compound Name

2-Methylphenol ............

4-Nitroaniline ............

(*) ND - Not detected above

9T5BCC03

Date Reported:

Sample Type:

units:

| Results*

........... MD

........... ND

........... ND

........... MD

........... ND

........... MD

........... ND

........... ND

........... ND

........... ND

........... MB

........... ND

........... MB

........... ND

........... MD

........... ND

........... MD

........... ND

........... ND.......... ND

........... MD.......... ND.......... ND

........... ND.......... ND.......... MD.......... ND.......... MD.......... ND.......... ND.......... MD.......... ND.......... MD


22-Feb-99

HATER

ug/Ii

Det Limits

30

66

2024

-2

1o rs0 -•--•—l 10""' 3

S; .4

- 26628882

1013

46

1242

2066

imit.

,

SAMPLE #:

SOURCE:MATRIX

ANALYSTS:

PARAMETER


US

9T5BCC03-09


KD, TS, BB

CONCENTRATION

NDNDNDNDNDND

1410NDNDNDND11

44712NDNDNDNDND

70500NDNDND

3 EPA REGION

DETECTIONLIMIT <=

10022

1022

150222

252

1502

0.22

10002

10500

22

20

6 LABORATORY

DATERECEIVED:


DATEREPORTED:

UNITS

UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L .UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L

28-JAN-99

"0 25-FEB-99

26-FEB-99

METHOD

200.7200.8200.8200.7200.8200.8200.7200.8200.8200.8200.7200.8200.7200.8245.1200.8200.7200.8200.7200.7200.8200.8200.7


9T5BCC03

o0I—I

•o~>~1< l

TNRGG


9T5BCC03

TNRCC Sampled: 9900624Program Code; EPASample Collected: 1/27/99 08:47 am

Collection Site: Delatte Metals

GroupS:19990167Sample Matrix: LIQUIDSample Recieved: 1/29/99

Chain of Custody #: 9T5BCC03-09 Region; 0Sample Depth: Station 3D:Sample Collector: EPA

Storet Parameter Name Result Unit Prepared Analyzed Method

00720 Cyanide, Total 2/3/99 16:05 <0.02 mg/L 335.2 N/A70300 Total Dissolved Solids 1/29/99 14:00 mg/L 160.1 N/A 18200945 Sulfate, ic 8.0 mg/L N/A 2/1/99 15:47 300.0

End of Data for TNRCC Sample? :9900624Comments:

Laboratory Approval:,BP15FYMI. 280c>1998

Approval Date; ll-Feb-1999

00>—l

•<1

~<10\

9T5BCC03



oSource: DELATTE METALS_________ _______ 2

Site Description: sTA.25.FB01 B ^



Sample Type: LIQUID

Comments:


9T5BCC03





___________________________________units - microg ram/liter - |Jg/lCompound Name Results* Detection Limits

acetone—————————————————————————————— ND 0.5benzene-————————————————————————————— ND 0.5bromodichloromethane——————————————————————— ND 0.5bro m oform————————————————————————————— N D 0.52-butanone———————————————————————————— ND 0.5bromomethane———————————————————————————- ND 0.5carbon disulfide————————————————————————— ND 0.5carbontetrachioride————————————————————————— ND 0.5chlorobenzene——————————————————————————— ND 0.5chloroethane——————————————————————————— ND 0.5

chloromethane———————————————————————— ND 0.5dibromochloromethane——————————————————————— ND 0.51,1-dichloroethane—————————————————————————— ND 0.51,1 -dichloroethene—————————————————————————— ND 0.51,2-dichloroethane—————————————————————————— ND 0.5c/s-1,2-dichloroethene———————————————————————-— ND 0.5frans-1,2-dichloroethene——————————————————————— ND 0.51,2-dichloropropane———————————————————————— ND 0.5c/s-1,3-dichloropropene———————————————————————- ND 0.5trans -1,3-dichloropropene—————————————————————— ND 0.5ethylbenzene——————————————————————————— ND 0.52-hexanone———————————————————————————— ND 0.5methylene chloride-———————————————————————— ND 0.54-methyl-2-pentanone——————————————————————— ND 0.5styrene—————————————————————————————— ND 0.51,1,2,2-tetrachloroethane——————————————————————— ND 0.5tetrachloroethene—————————————————————————— ND 0.5toluene—————————————————————————————— 0.7 0.51,1,1 -trichloroethane————————————————————————— ND 0.51,1,2-trichloroethane————————————————————————— ND 0.5trichloroethene--———--———-——————————————————— ND 0.5vinyl chloride———————————————————————————— ND 0.5orfho -xyl en e———————————————————————————— 0.8 0.5para - and/or mefa-xylene-————————————————————— 1.5 0.5


9T5BCC03




Site Description: s-rA25-FB02B



Sample Type: LIQUID 0—————————— 0»—i

Comments: ^3——————————————————————— ^


9T5BCC03





___________________________________units - microgram/liter - pg/lCompound Name Results* Detection Limits

acetone—————————————————————————————— ND

bromodichloromethane——————————————————————— NDhrnmnfnrm—•*——•'•'••"'»•—»— ««»«»—»»™—f™———M——»•«•«——i—niir———i—» i—iir———•>•———•i—k—miR—,—*— Mr^2-butanone——————————————————————— —-——-—— NDbromomethane-—-————————————————————————- NDcarbon disulfide——————————————————————————— NDcarbontetrachloride————————————————————————— NDchlorobenzene——————————————————————————— NDchloroethane———--——————-—————————————————— ND

chloromethane——————————————————————————— NDdibromochloromethane———————————————————————— ND1,1 -dichloroethane—————————————————————————— ND1.1-dichloroethene—————————————————————————— ND1.2-dichloroethane—————————————————————————— NDc/s-1,2-dichloroethene———————————————————————— NDf/"ans-1,2-diGhloroethene——————————————————————— ND1,2-dichloropropane————————————————————————— ND(?/s-1,3-dichloropropene———————————————————————— NDfrans-1,3-dichloropropene—————————————————————— NDethylbenzene———————————————————————————— ND2-hexanone————————————————————————————— NDmethylene chloride————————————————————————— ND4-methyl-2-pentanone-——-—-——————————————————— ND

1,1,2,2-tetrachloroethane——-———•—————————————————— NDtetrachloroethene—————————————————————————— NDtoluene———————————————————————————————0.61 , 1 , 1 -triGhloroethane————————————————————————— ND1,1,2-trichloroethane——————————————————— --————- NDtrichloroethene——————————————————————————— NDvinylchloride———————————————————————————— NDort/io-xylene———————————————————————————-— 0.8para- and/or me^a-xylene—————————————————————— 1.4


0.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.5

9T5BCC03




Site Description: STA25-TB03B



Sample Type: LIQUID

Comments:


00»—1

•o00

9T5BCC03





units - microgram/liter - pg/lCompound Name Results* Detection Limits

acetone—————————————————————————————— ND 0.5benzene————————————————————————————-— ND 0.5bromodichloromethane——————————————————————— ND 0.5bromoform————————————————————————————— ND 0.52-butanone——————————————————————————— ND 0.5bromomethane—————————————————————————— ND 0.5carbondisulfide—————————————————————————— ND 0.5carbontetrachloride————————————————————————— ND 0.5chlorobenzene——————————————————————————— ND 0.5Ghloroethane————————————————————————-——— ND 0.5chloroform————————————————————————————— ND 0.5chloromethane——————————————————————————— ND 0.5dibromochloromethane—————————————————————— ND 0.51,1-dichloroethane-—-————————————————————————— ND 0.51,1 -dichloroethene—————————————————————————— ND 0.51,2-dichloroethane————————————————————————— ND 0.5G/s-1,2-dichloroethene———————————~———————————— ND 0.5fr-ans-1,2-dichloroethene——————————————————————— ND 0.51,2-dichloropropane———————————————————————— ND 0.5c/$-1,3-dichloropropene——————————————————————— ND 0.5fr-ans-1,3-dichloropropene—————————————————————— ND 0.5ethylbenzene—-———————————————————————— ND 0.52-hexanone———-—-—————————————————————— ND 0.5methylene chloride————————————————————————— ND 0.54-methyl-2-pentanone——————————————————————— ND 0.5

1,1,2,2-tetrachloroethane—————————————————————— ND 0.5tetrachloroethene———————————————————————— ND 0.5toluene——————————————————————————————— ND 0.51.1.1-trichloroethane———————————————————————— ND 0.51.1.2-trichloroethane———————————————————————— ND 0.5trichloroethene——————————————————————————- ND 0.5vinyl chloride—————————————————————————-—— ND 0.5o/f/io-xylene———————————————————————————— ND 0.5para - and/or meta -xylene—————————————————————— ND 0.5


9T5BCC03



Site Name: Delatte Metals.



TENTATIVELY IDENTIFIED VOLATILE COMPOUNDS BY METHOD 624*

Number of tentatively identified compounds reported—-——1

units -TIC CAS Number Compound Name RT EstimNo, (min.) Conce

1 000109-99-9 tetrahydro-Furan 9.01 6.6

2

3

4

5

6

7

8

9

10

MQ/Iated **'ntration

001—i

00u^

* Analyst's Note. The compounds listed are tentatively identified by the best match with theNIST/EPA/Wiley mass spectral data base, and/or by manual interpretation.Standards were not used for confirmation.

** Estimated concentration is obtained by quantitation using the nearest internal standard.Since no external standard is used, a response factor of 1.0 is assumed.

9T5BCC03




Site Description: sTAWW-OSB


00i—i<1004^


Sample Type: LIQUID

Comments:

ParameterABNcarMAA

MHG

MICP

S04TDSVOA


9T5BCC03





___________________________________units - microgram/liter - pg/lCompound Name Results* Detection Limits

acetone——————————————————————————————— ND 0.5benzene—————————————————————————————— ND 0.5bromodichloromethane——————————————————————— ND 0.5bro mofo rm———————————————————————————— N D 0.52-butanone-———————————————————————————— ND 0.5bromomethane——————————————————————————— ND 0.5carbondisulfide—————————————————————————-— ND 0.5carbontetrachloride———————————————————————— ND 0.5fhIf^rr^hotTyono • _ — _—r__u_k———••••—•——•——••—••—••——•r—.r-k——•—•_>f ••-•_••—_•________ MF" 0 ^wl HUl UUd 1&.C71 ic ——..>•- 11LJ U.U

chloroethane—————————————————————————— ND 0.5chloroform-—————-—-————————————————————— ND 0.5chloromethane——————————————————————————— ND 0.5dibromochloromethane——————————————————————-— ND 0.51,1-dichloroethane—————————————————————————— ND 0.51.1-dichloroethene————————————————————————— ND 0.51.2-dichloroethane—————————————————————————— ND 0.5cis -1,2-dichloroethene———————————————————————— ND 0.5trans -1,2-dicnloroethene——————————————————————— ND 0.51,2-dichloropropane————————————————————————— ND 0.5c/'s-1,3-diGhloropropene——————————————————————— ND 0.5trans -1,3-dichloropropene—————————————————————— ND 0.5ethylbenzene———————————————————————————— ND 0.52-hexanone———————————————————————————— ND 0.5methylene chloride————————————————————————— ND 0.54-methyl-2-pentanone———————————————————————— ND 0.5styrene—————————————————————————————— ND 0.51,1,2,2-tetrachloroethane——————————————————————— ND 0.5tetrachloroethene—————————————————————————— ND 0.5toluene—————————————————————————————— ND 0.51,1 ,1 -frichloroethane————————————————————————— ND 0.51,1,2-trichloroethane———————————————————————— ND 0.5trichloroethene—————————————————————————— ND 0.5vinyl chloride——————————————————————————— ND 0.5ortyio-xylene——————————————————————————— ND 0.5para- and/or mefa-xylene—————————————————————— ND 0.5


00»—k

•<!00U)

ORGANIC ;6MD-HO Sample NO: 9T5BCC03-13


SEMI-VOLATILE CCt(continuol

units: ug/L

Compound Name j Results* ] Det Limits

bi»(2-Chloroethyl) Ether . . . . . . . . . . . . ND 2

bis-(2-Ethylhexyl)Phthalate . . . . . . . . . ND 4

Diethylphthalate . . . . . . . . . . . . . . . . . . . . ND 2

| DimethylPhthalate . . . . . . . . . . . . . . . . . . . ND 2

(*) ND » Not detected above the listed detection limit.

9T5BCC03

ftHALYSIS DATADate Reported: 22-Feb-99

Sample Type; WATER


units: ug/L

Compound Name 1 Results* | Det Limits

4,6-Dinitro-2-Methylphenol . . . . . . . . . . . ND 20Di-n-Butylphthalate " . . . . . . . . . . . . . . . . . . ND 2Di-n-Octyl Phthalate . . . . . . . . . . . . . . . . . ND "~ 4

Hexachloroethane . . . . . . . . . . . . . . . . . . . . . MD 0\ s 3

2-Methylphenol . . . . . . . . . . . . . . . . . . . . . . . ND 6

2-Nitroaniline . . . . . . . . . . . . . . . . . . . . . . . ND 83-Nitroaniline . . . . . . . . . . . . . . . . . . . . . . . ND 84-Nitroaniline . . . . . . . . . . . . . . . . . . . . . . . MD 8

2-Nitrophenol . . . . . . . . . . . . . . . . . . . . . . . . MD 104-Nltrophenol . . . . . . . . . . . . . . . . . . . . . . . . ND 13

(*) ND " Not detected above the listed detection limit.


SAMPLE #:

SOURCE:MATRIX

ANALYSTS:

PARAMETER


9T5BCC03-13

DELATTE METAL)LIQUID

KD,TS, BB

CONCENTRATION

NDNDNDNDNDND

1 1 1 0NDNDND6314

46660NDNDNDNDND

66900NDNDND

S

DETECTIONLIMIT <=

10022

1022

150222

252

1502

0.22

10002

10500

22

20

DATERECEIVED:

DATES ANALYZED:03-FEB-99 TO

DATEREPORTED:

UNITS M


28-JAN-99

25-FEB-99

26-FEB-99

ETHOD

200.7200.8200.8200.7200.8200.8200.7200.8200.8200.8200.7200.8200.7200.8245.1200.8200.7200.8200.7200.7200.8200.8200.7


001—1

-000•<!

TNRGG


9T5BCC03

TNRCC Sampled: 9900625Program Code: EPASample Collected: 1/27/99 08:42 amCollection Site: Delatte Metals

Groupff:19990167Sample Matrix: LIQUIDSample Recieved: 1/29/99

Chain of Custody #: 9T5BCC03-13 Region: 0Sample Depth: Station DO:Sample Collector: EPA

Storet Parameter Name Result Unit Prepared Analyzed Method00720 Cyanide. Total 2/3/99 16:05 0.02 mg/L 335.2 N/A70300 Total Dissolved Solids 168 mg/L N/A 1/29/99 14:00 160.100945 Sulfate, ic 2/1/99 15:48 mg/L 300.0 N/A 6.0

Comments: End of Data for TNRCC Sample# :9900625

Laboratory Approval:RP15FYNL 280CU99B_____________

Approval Date: ll-Feb-1999

oo

0000

001789 ENVIRONMENTAL PROTECTION AGENCYOFFICIAL

CHAIN OF CUSTODY RECORDPROJ.NO. PROJECT NAME .

^UU v^Us NO.

OFSAMPLERS: {Signature)

CON-TAINERS

TIME STATION LOCATION8STA.NO. DATE

REMARKS

xX

'ki| UQI

X.J^n^J ~\^} (2

4

Relinquished by: (Signature) Date /Time Received by: (Signature!FEhG^-^

Relinquished by: {Signature) Date /Time Received by: (Signature)

Relinquished by: (Signature) Date /Time Received by: {Signature) Relinquished by: {Signature) Date /Time Received by: Signature)

Relinquished by: {Signature) Date/Time Received for{Signature) „/

or iLabi

Shipped by: / ^ Airbill Number 5fc86

/ Date /TimeW^^-f^

Remarks

EPA 7500-531•^^ / n c \

Distribution; White Accompanies Shipment; Pink to Coordinator Field Files;Green to Report; Yellow Returns with Warrant 6" 07003


CHAIN OF CUSTODY RECORDPROJ.NO. PROJECT NAMEl 1 (Md^ ^4^>

SAMPLERS: ISianature)

t S0 C0 0

STATION LOCATIONSTA. NO. DATE TIME

NO.

OF

CON-TAINERS

REMARKS

5

Relinquished by: {Signature) Date/Time

^(^ 1630

Received by: {Signature) Relinquished by: {Signature) Date /Time Received by: (Signature)

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Relinquished by: ISismtum) Date /Time Receivedfqf IfliboratoryHy: ;e /Time Remarks| ISismtur,

Shipped by: ]fc:g~ jg\_ Airbill Number: 'g. •^ <, J y i 3 <J"$

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Distribution; White Accompanies Shipment; Pink to Coordinator Field Files;Green to Report; Yellow Returns with Warrant 6" 07004

001791ENVIRONMENTAL PROTECTION AGENCY

OFFICIALCHAIN OF CUSTODY RECORD

PROJ. NO. PROJECT NAME

"]>^^dJs NO.

OFSAMPLERS: (Signature

CON-TAINERS

STATION LOCATIONSTA. NO. DATE TIME8

REMARKS

Relinquished by: (Signaturef Date/Time

^nf^l^'i'oReceived by: {Signature)

f€h^Relinquished by: (Signaiure) Date/Time Received by: {Signature}

Relinquished by: {Signsturfi Date /Time Received by: (Signature) Relinquished by: (Signature) Date /Time Received by: (Signature)

Relinquished by: (Sisnsun) Date /Time Received for LiISiarnturf)^

'ate /Time

Shipped by:^ I •w

Airbill Number ;0.<g-<»^<a/ ? S'

Remarks

EPA 7500-53/ i i /nc \

Distribution: White Accompanies Shipment; Pink to Coordinator Field Files;Green to Report; Yellow Returns with Warrant 6- 07005


CHAIN OF CUSTODY RECORDPROJECT NAMEPROJ. NO.^^-A-'n~<s /s/^-rA^s

SAMPLERS: ISigiutwtl ^

S TÔT^/YÔ^^

o: caa <o lieS oSTATION LOCATIONSTA. NO. DATE TIME

^( ^7/^<2fe^7_K v/vA^/g^W) /

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Relinquished by: (Signsnu»)

Shipped by: ? ) _^

Date /Time Received mi Laborajteyy by:/? // Rate /Time Remarks______^'ÛÎP^^ \ ^30

\ Airbill Number: ^ ^V^^

EPA 7500-53Mi /o^

Distribution; White Accompanies Shipment; Pink to Coordinator Field Files;Green to Report; Yellow Returns with Warrant 6- 07006


CHAIN OP CUSTODY RECORDPROJ. NO- PROJECT NAME

SAMPLERS: (Signature)

STA. NO. DATE TIME 8 STATION LOCATION

NO.

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CON-TAINERS

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REMARKS

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Relinquished by: (Signatural

Shipped by: /^>^ f^C

Date/Time Received Mfi-Laborafcry by •.n , 1 Date /Time RemarksI isi^w^^^^u. \Wm\ ^••jpI Airbill Nuni er: ^^^y/3q^

EPA 7500-53fn/qfi\

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CHAIN OF CUSTODY RECORD

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final analytical report for delatte metalsthis final report should only be reproduced in full. the...

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