from sample to vial · ables the ple to operate virtually leak and clog free. modular construction...

From Sample to VialAutomated Sample Prep Solutions

Extraction • Cleanup • Concentration

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Extraction SystemsSolid Samples PLE - Pressurized Liquid Extraction ..........................................................................................6

Liquid Samples EconoTrace - Automated Solid Phase Extraction Positive Pressure, Parallel processing 1 to 8 channels .............................................................10

TurboTrace - High Speed Solid Phase Extraction Vacuum/Positive Pressure, Parallel processing 1 to 8 channels ...............................................13

TurboTrace Sequential - Solid Phase Extraction Parallel/ Sequential processing 1 to 2 modules, 5 to 10 samples .............................................16

TurboTrace ABN - Multi Cartridge/Multi Fraction Solid Phase Extraction Vacuum/Positive Pressure/Multi Cartridge/ Multi Fraction/ Parallel processing ........................19

TurboTrace PFC - A Solid Phase Extraction system for PerfluoralkylatedSubstances ....................................................................................................22

NanoTrace - Small volume Solid Phase Extraction Parallel/ Sequential processing 1 to 2 modules, 5 to 10 samples .............................................25

Sample Clean-Up SystemsPowerPrep - High Speed Multi Column Sample Clean- Up and Fractionation Parallel processing 1 to 8 channel ...............................................................28

PowerPrep/EPH Single Column Sample Clean-Up and Fractionation System Parallel/Sequential processing ....................................................................31

PowerPrep/GPC Parallel and Sequential Gel Permeation Chromatography processing ..........................................................................................................33

Concentration/Evaporation/Solvent Recovery SystemsSuperVap/6 6 Position 250ml Concentration Direct to Vial ...........................................................37

SuperVap/12 12 Position 50ml Concentration Direct to Vial ........................................................38

SuperVap/12 12 Position 20, 40, 60ml Vial Concentration ....................................................39 - 41

SuperVap/24 24 Position 2, 4ml Vial Concentration ..............................................................42 - 43

SuperVap Solvent Recovery System Solvent Recovery for Concentration and Evaporation Systems ..................................................................................45

Extraction - Clean-up - ConcentrationTRP – Total Rapid Prep SystemThreesampleprocessescombinedintooneExtraction,Clean-upandConcentrationSystem .....46

Table of Contents

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Founded in 1985, Fluid Management Systems, Inc. head-quartered in Watertown, MA USA designs, manufactures,

andsupportsanalyticalinstrumentsusedbyscientiststoper-form extraction, cleanup, fractionation and concentration of samples prior to chemical analysis. Some of the industries that rely on our sample preparation systems are Agricultural, Chemical, Environmental, Food, Life Sciences and Pharma-ceutical.

Automated sample preparation systems from FMS are de-signed to replace outdated, labor-intensive techniques thathinder laboratoryproductivity.OurTotalSamplePreparationsystems improve the efficiency of both laboratory person-nel and expensive instrumentation. Our automated samplepreparation systems allow laboratory personnel to reducecosts, shorten sample turnaround time and improve the quali-tyandconsistencyoftheirresultsbyeliminatingthevariabilityinherent with manual sample preparation methods.

We support our sample preparation systems with an ever increasing network of field sales, service, and applicationsexpertise.FMSsystemsaresoldworldwidebydirectsalesforce,independentrepresentatives,anddistributors.After29years inbusiness,FMShasestablished itself as theworldleader in providing automated sample preparation systems inthefieldofPersistentOrganicPollutants(POPs)analysis.

Improving Laboratory Productivity While Reducing Costs

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Guaranteed Quality Products and ConsumablesOurManufacturing/Cleanroom

FMS proudly designs and

manufactures all of its products in the United

States of America. Within our 125,000 sq. foot facility is a 25,000 sq. foot custom high speedCNClatheandmillingshopthatquicklymanufacturesparts and prototypes for FMS automated sample prep sys-tems.Ourmanufacturingassembly,qualitycontrolandR&Doccupy 35,000 sq. ft. and 30,000 sq. ft. is dedicated to our laboratories.ThisallowsFMStohavegreatercontroloveritsqualityprocessandabilitytodeliverqualityproducts.

FMSmanufacturesallofitsconsumablesin1,000classclean room environments. The clean room manufacturing facility delivers guaranteed contaminant free products. This iscriticalforlaboratoriesperforminganalyticaltestingandeven more mission critical to those performing trace analysis withhighresolutionmassspectrometry(HRMS).EachlotiscontrolledandtestedbytheISO17025accreditedlaboratory.FMSoffersitscustomerstheabilitytoordertheirconsum-ablesfromonelot.Thisallowsthelaboratorytoreducecostsofqualifyingnewconsumablesmultipletimesinaprojectortimeperiod.Prepackagedconsumableseliminatethe possibilityofoutsidecontaminationoftheconsumable cartridges or columns used in sample preparation.

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Our Lab

ThelaboratorylocatedinWatertown,Massachusettsoccupiesa30,000squarefootspace.Thelaboratoryhastapped into 30 years of expertise in advanced sample preparationandautomation,makingourlaboneofthemostadvancedintheworld.Ourlabutilizesfullyautomat-ed sample preparation instrumentation, high resolution massspectrometers(HRGC/HRMS),TripleQuadGC/MS,SingleQuadGC/MS,TripleQuadUPLC,UPLC,HPLCand GC to demonstrate, quality results, faster turnaround, and lower cost to perform analysis of a variety of matrices inmanymarketsegmentsincluding:

•Biological Samples WholeBlood,BloodSerum,BreastMilk,Urine•Food & Feed Samples Fish, Shell Fish, Meat, Feed, Tissue•Environmental Samples

Soil, Air, Sediments, Building products, Fly ash•Water Samples Drinkingwater,GroundWater,WasteWater

• Pharmaceutical Drug development

We’re experts in POPs analysis, equipped with advanced automation, accredited in ISO 17025 to provide you with faster and less costly quality results. ThelaboratoryisISO17025accreditedprovidinghigh qualityanalyticaltestingofPersistentOrganicPollutants(POPs).OurapplicationslaboratoryfocusisPOPsandoth-eremergingcontaminants.Thelaboratoryusesthepowerofadvancedanalyticalinstrumentationcombinedwithautomat-ed sample preparation to create the world’s fastest, lowest cost, highest quality solutions for testing results focusing on thefollowingcompounds:

•Dioxin anddioxinlikecompounds• PCBs - PolyChlorinated Biphenyls•PAHs-PolyaromaticHydrocarbons•PBDEs - PolyBrominated Biphenyl Ethers•PFCs - PerFluorinated Compounds•OCPs-OrganoChlorinePesticides AllFMSproductsaretestedandcertifiedbytheISO 17025laboratory

We understand what you have to do

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PLE® Automated High Speed Pressurized Liquid Extraction

PLE® is a high speed Pressurized Liquid Extraction sys-tem, designed to perform the extraction of multiple samples simultaneously in minutes rather than hours, producing high recoveries and excellent precision for all analytes. Very inexpensive stainless steel extraction cells and end cap filtrationkeeptheoperationalcostataminimum.The optionaldisposableendcapfiltrationincreasesproductivityandsavesvaluabletime.

Moreefficientandcosteffectivethantraditional processing methods.

One Step Extraction & Clean-up OptionalIncellCleanupallowsfortheentireextractionandclean-upprocesstohappeninonestep.Thereby,increasingspeed&reducingthecostofsampleprep.Extraction Cell Size 5 - 150ml Run small to large sample sizes with the same basicsystem.Modular, Expandable & Affordable With the modular PLE design, one can purchase a 1 samplesystemataveryaffordableprice.Thesystemcanbeexpandedtoa6samplesystemasthe laboratory’sworkloadgrows.Reduces Operating Cost Rapidextraction&clean-up,alongwithreduced solvent use and waste, it reduces operating costs byasmuchas70percent.Increases Productivity Theentireextraction&clean-upmaybeperformedin lessthan30minutes.Traditionalmethodscouldtake 10 - 16 hours.Reduces Solvent Waste PLEreducessolventwastethroughefficientuse of solvents.Reduces Solvent Cost Uses as little as 15ml of solvent as compared to more than 500ml of solvent required to perform Soxhlet extractions.ApplicationsSolid and Semi Solid Material, Food and Feed,PackagingMaterialsSupports EPA MethodsMethod3545A SemiVolatiles,Organophosphorous Pesticides,OrganochlorinePesti cides,ChlorinatedHerbicides, PCBs,PCDDs/PCDFs,DROMethod 1613 Dioxin and FuransMethod 1668 Chlorinated Biphenyl CongenersSW-846 Methods for Solid Waste

The PLE is expandable from one to six modules to meet your laboratories needs as it grows

The PLE is a modular system that can grow with your laboratory

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Lower Your Re-Extraction Rate

5 to 150ml Extraction Cell Sizes PLE offers 5 - 150ml low cost stainless steel extractioncellswithTeflonendcapfiltration.Thiswide range of extraction cells allows the use of the same unit for all sample sizes, even in the same runCross Contamination Free OptionallowcostextractioncellsizesandTeflonendcapsfiltrationensuretroublefreeextractionwithno cross contamination.Automatic Operation & Documentation Real time software allows 6 channels of pressure and6channelsoftemperaturedatatobeplottedsimultaneously. This powerful feature allows automat-ic documentation of the entire extraction data. The temperatureandpressuredatacanbesuperimposedandprintedingraphicortabularformatandstoredforfuture reference.Patented One-Step Extraction & Clean-up The PLE patented one step extraction and clean-up designhastheflexibilitytoperformextractionaswellas clean-up in one run. Depending on the sample sizeandtheextentofclean-up,threeconfigurationsareavailable.In-line Column Clean-up An optional In-line clean-up module allows addition-alclean-upcolumnstobeaddedtotheoutputofextraction cells for cleaning the sample prior to GC/MS analysis. This powerful feature of PLE saves time and money while producing excellent recoveries and precise results for all analytes. FMS offers a wide varietyofdisposableTefloncolumnsfrom0.25to50grams capacity.Column Clean-up With PLE system, the entire ex-tractionandclean-upcanbedoneinonestepusingpackingmaterialsuchassilicaandcarbon. This feature allows for rapid extraction and cleanup all in one step.PLE/Power-Prep Dual Extraction & Clean-up System The Dual PLE/PowerPrep consists of two systems in oneeconomicalpackageandistrulythenewfrontierinrapidsamplepreparationforPOPsanalysis.Thesystemcanbeusedtoperformextraction,clean-uporbothextractionandclean-up.Themodularand

compactdesignofthesystemsenabletheusertoexpand from one to six modules. The user can there-fore, start off with a single sample system and expand up to a six module system as throughput demand increases.Complete Control & Monitoring by PC TheDMS-6000Editorallowsmultiplemethodstobestored. In each method parameters such as time, solvent,volumeandfinaltemperaturecanbesetfor each step. Pressure and temperature as well as dispensed volumes are displayed every second and stored for future reference. Six channels of pressure andsixchannelsoftemperaturearealsobeplottedin real time. This powerful feature allows automatic documentation of the entire extraction data.Multiple Extraction Programmingofvariablepressureandtemperatureallows extraction of a variety of different compounds.A Versatile Method Development Tool The powerful DMS 6000 real time software along with a large variety of extraction cell capacities and the abilitytoselectmultiplesolvents,differenttempera-turesettings,aswellasstorageofdatamakesthePLE the perfect development tool.Leak & Clog Free Operation Simpledesignalongwithlargeboreplumbingen-ablesthePLEtooperatevirtuallyleakandclogfree.Modular Construction Provides for Easy MaintenanceThePLEmodularunitsaswellasexposedplumbingconstructionmakesforefficientsystemmaintenance.The PLE module is designed to operate independent-ly, should one module fail the others will continue to perform. This versatility ensures ease of replacement with no down time.Multiple Method Storage The entire extraction process is PC controlled allowingthelaboratorytechniciantostoreandeditextraction protocols, as well as monitor and store extraction data.

PLE

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SpecificationsDimensions:

PLE1=15”(38cm)WX35”(90cm)HX18”(45cm)DPLE2=23”(58cm)WX35”(90cm)HX18”(45cm)DPLE3=31”(78cm)WX35”(90cm)HX18”(45cm)DPLE4=39”(98cm)WX35”(90cm)HX18”(45cm)DPLE5=47”(118cm)WX35”(90cm)HX18”(45cm)DPLE6=55”(138cm)WX35”(90cm)HX18”(45cm)D Ordering InformationPLE Extraction CellsPart number Description

PLE-ECEL-SS20 20ml stainless steel extraction cellPLE-ECEL-SS40 40ml stainless steel extraction cellPLE-ECEL-SS100 100ml stainless steel extraction cell

PLE Filtration CapsPart number Description

PLE-FLT-TEF-OAR TeflonEndcapfiltrationwitho-ringfor 100,40,20,10, 5ml cellPLE-FLT-100M-TEF Teflon,Endcapfiltrationfor 100, 40, 20, 10, 5ml cellPLE-FLT-100M-SS StainlesssteelReusableEndcapfiltrationfor 100,40 20, 10, 5ml cell

PLE Extraction Cell and CapPart number Description

PLE-CAR100-FLT10 100ml stainless steel extraction cell with two end capfiltrationPLE-CAR40-FLT10 40ml stainless steel extraction cell with two end capfiltrationPLE-CAR20-FLT10 20ml stainless steel extraction cell with two end capfiltration

PLE System Configurations Part Number Description

PLE 1 Modular one sample extraction system. This system Processes one samplePLE 2 Modular two sample extraction system. This system Processes two samples simultaneouslyPLE 3 Modular three sample extraction system. This system Processes three samples simultaneouslyPLE 4 Modular four sample extraction system. This system Processes four samples simultaneouslyPLE5 Modularfivesampleextractionsystem.This systemProcessesfivesamplessimultaneouslyPLE 6 Modular six sample extraction system. This system Processes six samples simultaneously

PLE AccessoriesPart number Description

PLE-HTB-SM SmallHeaterblocksfor5-40mlextractioncellPLE-HTB-MD MediumHeaterblockfor100mlextractioncellPLE-HTB-LG LargeHeaterblockfor250mlextractioncell

PLE ModulesPart number Description

PLE-CNT-MD PLE Control modulePLE-HPR-MD High Pressure pump modulePLE-SMP-MD Sample processing modulePLE-COL-MD Columnmodule

Portable Cart & Spill TrayPart number Description

SPILL-TRY Spill TrayPORT-CRT PortableCart

ConsumablesPart number Description

PLE-CAR-SS05 5ml Stainless Steel CartridgePLE-CAR-SS10 10ml Stainless Steel CartridgePLE-CAR-SS100 100ml Stainless Steel CartridgePLE-CAR-SS20 20ml Stainless Steel CartridgePLE-CAR-SS40 40ml Stainless Steel CartridgePLE-FLT-100M-SS ReusableEndcapfiltrationfor100,40,20,10,5ml cell - Stainless steelPLE-FLT-100M-SS-NP ReusableEndCapFiltrationfor100,40,20,10, 5ml Cell - Stainless Steel Non-PolarPLE-FLT-100M-SS-P ReusableEndCapFiltrationfor100,40,20,10, 5ml Cell - Stainless Steel PolarPLE-FLT-100M-SS-U ReusableEndCapFiltrationfor100,40,20,10, 5ml Cell - Stainless Steel UniversalPLE-FLT-100M-TEF-NP TeflonCapFiltrationfor100,40m20,10,5ml Cell Non PolarPLE-FLT-100M-TEF-P TeflonCapFiltrationfor100,40m20,10,5ml Cell PolarPLE-FLT-100M-TEF-U TeflonCapFiltrationfor100,40m20,10,5ml Cell UniversalPLE-FLT-INCL3-NP Non-Polar In Cell Cleanup End Cap 3 gm capacityPLE-FLT-INCL3-P Polar In Cell Cleanup End Cap 3 gm capacityPLE-FLT-INCL3-U Universal In Cell Cleanup End Cap 3 gm capacityPLE-FLT-INCL6-NP Non-Polar In Cell Cleanup End Cap 6 gm capacityPLE-FLT-INCL6-P Polar In Cell Cleanup End Cap 6 gm capacityPLE-FLT-TEF TeflonCapFiltrationfor100,40m20,10,5ml

Extraction, InCell Cleanup with Direct to GC vial Sample PrepPLE

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Consumables (contd.)Part number Description

PLE-FLT-INCL6-U Universal In Cell Cleanup End Cap 6 gm capacityPLE-OR-ETP-ST VitonETP(Universal)OringsSet:014,017,116PLE-OR-NEO-ST Neoprene(Polar)OringsSet:014,017,116PLE-OR-VIT-ST Viton(Non-Polar)OringsSet:014,017,116PLE-SS-CAP-100M ReusableEndCapFittingBodyfor100,40, 20, 10, 5ml CellPLE-SS-FLT-10 Stainless Steel FilterPLE-SS-RET Retaining Ring

High Throughput, Robust Pressurized Liquid ExtractionPLE

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EconoTrace® Parallel SPE System

The EconoTrace Parallel SPE System is designed to streamlineyourlaboratory’sworkflowandincreasepro-ductivitybyautomatingthemanualstepsinyoursamplepreparation process. The EconoTrace Parallel SPE system automates existing manual SPE techniques and replaces older manual Liquid-Liquid Extraction techniques and out-dated semi-automated instruments.

The EconoTrace Parallel SPE system is the only SPE systemthatcombinesextraction,dryingandconcentrationinto one step – providing a truly automated total sample prepsolutionforthelaboratory.Simplyloadsamplesontothe EconoTrace Parallel SPE system and trigger the auto-mated extraction process. After loading the sample onto the SPEcartridgeattheprogrammedflowrate,thedryingstepis accomplished using Nitrogen. This drying step replaces manual techniques. The analytes of interest are then eluted directly to the SuperVap Concentrator where the concentra-tionprocessautomaticallybringstheextracttofinalvolumeinanautosamplervial,readyforfinalanalysis.Automatingthese processes into one step ensures the highest quality resultsintheshortestamountoftimeandeliminatesbothhumanerrorandthepossibilityofcontamination.

Reduces Errors and CostsOne-stepautomatedSPEandconcentrationeliminateshumanerror,saveslaborcostsandreducessolventusage while increasing your sample throughput.Fully AutomatedHyphenates the entire sample prep process– extraction, drying and concentration steps into a one process. Runs up to eight samples simultaneously. Automaticsamplebottlerinse.Concentrates samples up to 250ml directly to a GC vial.High SpeedThefastestautomatedsampleprocessingavailablefor SPE cartridges and columns of all sizes.Runs up to eight samples simultaneously.Positive pressure pumping for fast, simultaneous loading of samples. ApplicationsDrinkingWaterSupports EPA Methods506 Phthalates and Adipate Esters508.1 ChlorinatedPesticides,Herbicides,and Organohalides515.2 Chlorinated Acids521 Nitrosamines525.2 Semi-volatiles526 Semi-volatiles527 Selected Pesticides and Flame Retardants528 Phenols529 Explosives532 Phenylurea Compounds535 Chloroacetanilide and other Acetamide Herbicides548.1 Endothall549.2 Diquat and Paraquat550.1 PAH’s552.1 Haloacetic Acids and Dalapon553 Benzidines and Nitrogen Containing Pesticides

The EconoTrace runs two samples per module in parallel. It is expandable from one to four modules to grow with your laboratory giving you up to 8 extractions simultaneously.

1010

High Throughput Solid Phase Extraction for Drinking Water, Beverages, Urine and Blood

The EconoTrace Parallel SPE system uses positive pres-sure pumping for precise and accurate delivery of the sam-ple as well as conditioning, washing and elution solvents. Thesystemisspecificallydesignedtoisolateanalytesofinterest from a wide variety of liquid matrices such as urine, blood,water,milk,andbeverages.Samplesizesrangefrom2mltoLitersandusesthesamebottlethesamplewascol-lectedin.Sampleloadingratesareprogrammable.A positive pressure pump is used to load samples onto any SPEcartridgeorcolumnavailableonthemarketandit easilyhandlesbothcleanandtoughsamplematrices.

The EconoTrace Parallel SPE/SuperVap system concen-trates samples up to 250ml directly to a GC vial. For guar-anteed results, especially when dealing with low limits of detection, we recommend using FMS cartridges. Sample ProcessingModulescaneasilybereplacedforservicewhichmeansyourlabwillexperiencezerodowntime.

The EconoTrace System is expandable from one to four modules

Measurements - Concentration / Evaporation vessels in 500 µL, 1ml, and direct to a GC Vial or to dryness.

Automatic time-based or endpoint detection for nitrogen shut off for each vessel

System control is accomplished via an easy-to-use touch screen.

The SuperVap® Concentrator is where the concentration process automatically brings the extract to final volume in an autosampler vial, ready for final analysis.

EconoTrace

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SpecificationsDimensions:15”Wx18”Dx35”HWeight:65lbs.GasRequirements:Nitrogen-20PSIminimumPump:PistonDisplacementFlowrate:0.2to15ml/minuteElectricalInput:110/220Volts,50/60HZController:IntegratedTouchScreenControl

Ordering Information Part number DescriptionEconoTrace/1 EconoTraceSPEsystemfor2samples(1Module)EconoTrace/2 EconoTraceSPEsystemfor4samples(2Modules)EconoTrace/3 EconoTraceSPEsystemfor6samples(3Modules)EconoTrace/4 EconoTraceSPEsystemfor8samples(4Modules)ECONO-EXP EconoTraceExpansionModule

ConsumablesPart number Description SPE-ADP-1 SPE 1ml Cartridge AdapterSPE-ADP-20 SPE 20ml Cartridge AdapterSPE-ADP-3 SPE 3ml Cartridge AdapterSPE-ADP-6 SPE 6ml Cartridge AdapterSPE-BT.5L SPE Sample Bottle 500mlSPE-BT1 SPE Sample Bottle 1LSPE-BT1.25L SPE Sample Bottle 1250mlSPE-BTRC SPE Sample Bottle Rinse CapSPE-CAP-1L SPE Bottle Cap with Loading and SampleRinseTubingsandAdapters,1LSPE-CAP-2L SPE Bottle Cap with Loading and SampleRinseTubingsandAdapters,2LSPE-CAR1-C18 SPE Cartridge 1 gram C18SPE-CAR1-DVB SPE Cartridge 1 gram DVBSPE-CAR5-C18 SPE Cartridge 5 gram C18SPE-CAR6-DVB SPE Cartridge 6 gram DVB

SPE Accessories Part number Description SPE-CART-TRY SPEPortableCartandTray

Economic Automated Solid Phase ExtractionEconoTrace

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TurboTrace® Parallel SPE System

TheTurboTraceParallelSPEsystemisdesignedtostream-lineyourlaboratory’sworkflowandincreaseproductivitybyautomating the manual steps in your sample preparation process. It is designed for high throughput and tough sample matrices.TheTurboTraceParallelSPEsystemautomatesexisting manual SPE techniques and replaces older manual Liquid-Liquid Extraction techniques and outdated semi-auto-mated instruments.

TheTurboTraceParallelSPEsystemcombinesextraction,drying and concentration into one step -- providing a truly automatedtotalsampleprepsolutionforthelaboratory.Sim-plyloadsamplesontotheTurboTraceParallelSPEsystem,use the touch screen to trigger the automated extraction process. After loading the sample onto the SPE cartridge, the drying step is accomplished using vacuum or nitrogen orboth.Thisdryingstepreplacesmanualtechniquessuchas sodium sulfate drying. The analytes of interest are then eluted directly to the SuperVap Concentrator where the con-centrationprocessautomaticallybringstheextracttofinalvolumeinanautosamplervial,readyforfinalanalysis.Au-tomating these processes into one step ensures the highest quality results in the shortest amount of time and eliminates bothhumanerrorandthepossibilityofcontamination.

The TurboTrace Parallel system is modular and can run up to 8 samples in parallel providing direct-to-vial concentration and delivering unmatched throughput in solid phase extraction

Reduces Errors and CostsOne-stepautomatedSPEandconcentrationeliminateshumanerror,saveslaborcostsandreducessolventusage while increasing your sample throughputFully AutomatedHyphenates the entire sample prep process-- extraction, drying and concentration steps--into a one step process.Runs up to 8 samples simultaneously Sample Liquid Level Sensors to detect when the SamplehasfinishedloadingandwasteoverflowAutomaticSamplebottlerinseConcentrates samples up to 250ml directly to a GC vialHigh SpeedThefastestautomatedsampleprocessingavailablefor SPE cartridges and columnsRun up to eight samples simultaneouslyVacuum for fast loading of large volume samples ApplicationsDrinkingWater,WasteWater,Blood, MilkandBeveragesEPA Methods608 Chlorinated Pesticides and PCB’s1613 Dioxin1664AOilandGreaseandSGT-HEM1668AToxicPCB’sbyIsotopeDilutionandGC/MS1694 Pharmaceutical and Personal Care Products8061 Phthalate esters8081 TCLPOrganochlorinepesticides8082 PCB’s8095 Explosives8141 Organophosphoruspesticides8321 TCLPPhenoxyacidherbicides8330 Nitroaromatics / NitraminesCompliantComplies with existing methods that require vacuum,positive pressure pumping for the precise delivery ofsample and solvents

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High Speed, High Throughput Automated Solid Phase Extraction for Difficult Samples

TheTurboTraceParallelSPEsystemincorporatesvacuumor positive pressure pump to load samples for compliance with all SPE methods. It uses positive pressure pumping for precise and accurate delivery of conditioning, washing andelutionsolvents.TheTurboTraceParallelSPEsystemisspecificallydesignedtoisolateanalytesofinterestfromawidevarietyofliquidmatricessuchasurine,blood,water,milk,beverages.Samplesizesrangefrom2mlto8Landusethesamebottlethesamplewascollectedin.Manysampleloadingratesareprogrammable.Avacuumorpositive pressure pump is used to load samples onto the SPE cartridges and columns at unprecedented speeds and it easilyhandlesbothcleanandtoughsamplematrices.Aliquidsensordetectswhenthesamplehasbeenloaded,triggeringthesystemtoinitiatenextsteps.TheTurboTraceParallel SPE system concentrates samples up to 250ml directly to a GC vial. The Sample Processing Module is designed to use all standard formats of SPE cartridges and columnsonthemarkettoday.Forguaranteedresults, especially when dealing with low limits of detection, we recommendFMSpre-packedcolumnsandcartridges.

TurboTrace System is expandable from one to eight modules.





TurboTraceParallel

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SpecificationsDimensions:15”Wx18”Dx35”HWeight:65lbs.GasRequirements:Nitrogen-20PSIminimumVacuumRequirements:25”HgminimumPump:PistonDisplacementFlowrate:0.2to15ml/minuteElectricalInput:110/220Volts,50/60HZController:IntegratedTouchScreenControl

Ordering InformationPart number Description TurboTrace/1 TurboTraceSPEparallelsystemfor1sampleTurboTrace/2 TurboTraceSPEparallelsystemfor2samplesTurboTrace/3 TurboTraceSPEparallelsystemfor3samplesTurboTrace/4 TurboTraceSPEparallelsystemfor4samplesTurboTrace/5 TurboTraceSPEparallelsystemfor5samplesTurboTrace/6 TurboTraceSPEparallelsystemfor6samplesTurboTrace/7 TurboTraceSPEparallelsystemfor7samplesTurboTrace/8 TurboTraceSPEparallelsystemfor8samplesTurboTrace-EXP TurboTraceExpansionModule

ConsumablesPart number Description SPE-ADP-1 SPE 1ml Cartridge AdapterSPE-ADP-20 SPE 20ml Cartridge AdapterSPE-ADP-3 SPE 3ml Cartridge AdapterSPE-ADP-6 SPE 6ml Cartridge AdapterSPE-BT.05L SPE Sample Bottle 500mlSPE-BT1 SPE Sample Bottle 1LSPE-BT1.25L SPE Sample Bottle 1250mlSPE-BTRC SPE Sample Bottle Rinse CapSPE-CAP-1L SPE Bottle Cap with Loading and Sample Rinse TubingsandAdapters,1LSPE-CAP-2L SPE Bottle Cap with Loading and Sample Rinse TubingsandAdapters,2LSPE-CAR1-C18 SPE Cartridge 1 gram C18SPE-CAR1-DVB SPE Cartridge 1 gram DVBSPE-CAR5-C18 SPE Cartridge 5 gram C18SPE-CAR6-DVB SPE Cartridge 6 gram DVB

SPE Accessories Part number DescriptionSPE-CART-TRY SPEPortableCartandTray

Truly Compliant Automated Solid Phase ExtractionTurboTraceParallel

TurboTrace® Sequential SPE System

TheTurboTrace®SequentialSPEAutomatedOne-StepExtraction and Concentration System is designed to stream-lineyourlaboratory’sworkflowandincreaseproductivitybyautomating the manual steps in your sample preparation process.TheTurboTrace Sequential SPE system automates existing manual SPE techniques and replaces older manual Liquid-Liquid Extraction techniques and outdated semi- automated instruments.

TheTurboTraceSequentialSPEsystemistheonlySPE systemthatcombinesextraction,dryingandconcentrationinto one step -- providing a truly automated total sample prepsolutionforthelaboratory.SimplyloadsamplesontotheTurboTraceSequentialSPEsystemtostartthe automated extraction process. After loading the sample onto the SPE cartridge, the drying step is accomplished using Nitrogen. This drying step replaces manual techniques. The analytes of interest are then eluted directly to the SuperVap Concentrator where the concentration process automatical-lybringstheextracttofinalvolumeinanautosamplervial,readyforfinalanalysis.Automatingtheseprocessesintoone step ensures the highest quality results in the shortest amountoftimeandeliminatesbothhumanerrorandthepossibilityofcontamination.

The TurboTrace Sequential module is capable of readying five samples running one at a time.

Reduces ErrorsOne-stepautomatedSPEandconcentrationeliminateshumanerror,saveslaborcostsandreducessolventusage while increasing your sample throughputFully Automated Hyphenates the entire sample prep process-- extraction, drying and concentration steps--into a one step program. Runs up to 5 different methods/sample matrices sequentially Concentrates samples up to 250ml directly to a GC vial.AutomaticSamplebottlerinseHigh SpeedThefastestautomatedsampleprocessingavailablefor SPE cartridges and columnsRun up to four samples simultaneously, up to 20 samples totalVacuum for fast loading of large volume samples ApplicationsDrinkingWater,WasteWater,Blood, MilkandBeveragesEPA Methods500 Series600 Series1600 Series8000 SeriesCompliantComplies with existing methods that require vacuum, positive pressure pumping for the precise delivery of sample and solventsDispensesuptofivesolventsusinganHPLCpumptodeliverprecisevolumesandflowratesforcondi-tioning and elutionEasy DocumentationProgramsandstoresanunlimitednumberof methods and runsEasy-to-use software

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Automated Solid Phase Extraction and Direct to Vial Concentration

TheTurboTrace® Sequential SPE system uses positive pressure pumping for precise and accurate delivery of conditioning,washingandelutionsolvents.TheTurboTrace® SequentialSPEsystemisspecificallydesignedtoisolateanalytes of interest from a wide variety of liquid matrices suchasurine,blood,water,milk,beverages.Samplesizesrangefrom2mlto8Landusethesamebottlethesamplewascollectedin.Sampleloadingratesareprogrammable.Avacuum or positive pressure pump is used to load samples onto the SPE cartridges and columns at unprecedented speedsanditeasilyhandlesbothcleanandtoughsamplematrices.TheTurboTrace® Sequential SPE system con-centrates samples up to 250ml directly to a GC vial. The Sample Processing Module is designed to use all standard formatsofSPEcartridgesandcolumnsonthemarkettoday.For guaranteed results, especially when dealing with low limitsofdetection,werecommendFMSpre-packedcolumnsandcartridges.SampleProcessingModulescanbeeasilyreplaced to perform cleanup column chemistries allowingthelabtomultipurposetheTurboTrace® to automate other sample prep processes.

The TurboTrace Sequential System is expandable from one to four modules to grow with your lab.





TurboTraceSequential

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Ordering InformationPart number Description TurboTrace/SEQ/1 TurboTraceSequentialsystemfor5samplesTurboTrace/SEQ/2 TurboTraceSequentialsystemfor10samplesTurboTrace/SEQ/3 TurboTraceSequentialsystemfor15samplesTurboTrace/SEQ/4 TurboTraceSequentialsystemfor20samplesTurboTraceSEQ-EXP TurboTraceSequentialExpansionModule ConsumablesPart number Description SPE-ADP-1 SPE 1ml Cartridge AdapterSPE-ADP-20 SPE 20ml Cartridge AdapterSPE-ADP-3 SPE 3ml Cartridge AdapterSPE-ADP-6 SPE 6ml Cartridge AdapterSPE-BT.05L SPE Sample Bottle 500mlSPE-BT1 SPE Sample Bottle 1 LSPE-BT1.25L SPE Sample Bottle 1250mlSPE-BTRC SPE Sample Bottle Rinse CapSPE-CAP-1L SPE Bottle Cap with Loading and SampleRinseTubingsandAdapters,1LSPE-CAP-2L SPE Bottle Cap with Loading and SampleRinseTubingsandAdapters,2LSPE-CAR1-C18 SPE Cartridge 1 gram C18SPE-CAR1-DVB SPE Cartridge 1 gram DVBSPE-CAR5-C18 SPE Cartridge 5 gram C18SPE-CAR6-DVB SPE Cartridge 6 gram DVB


TurboTraceSequential

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Reduces ErrorsOne-stepautomatedSPEandconcentrationeliminateshumanerror,saveslaborcostsandreducessolventusage while increasing your sample throughputFully Automated Hyphenates the entire sample prep process-- extraction, drying and concentration steps--into a one step program.Runs up to 6 samples, simultaneously Sample Liquid Level Sensor to detect when the SamplehasfinishedloadingAutomaticSamplebottlerinseConcentrates samples up to 250ml directly to a GC vialWasteliquidlevelsensortopreventwasteoverflowDual Cartridge extraction and fractionation of Acid/Base/Neutral analytesHigh SpeedThefastestautomatedsampleprocessingavailablefor ABN methods using SPE cartridges and columns ready for analysis in hours versus days Run up to eight samples simultaneouslyVacuum for fast loading of large volume samples VersatileHandles a wide range of sample sizes and all matrix typesDual Cartridge allows for many other types of multi cartridge applicationsUp to 3 fractions per runSample Sizes 2ml to many litersSample Liquid Level Sensor to detect when the SamplehasfinishedloadingExpandablefrom1to6modulesApplications DrinkingWater,WasteWater,Blood, MilkandBeveragesEPA Methods 625 Semi-Volatiles 8270 TCLP Semi-volatiles 500, 600, 1600, 8000 Series

TurboTrace® ABN SPE System

TheTurboTraceABNSPEsystemisdesignedtostream-lineyourlaboratory’sworkflowandincreaseproductivitybyautomating the manual steps in your sample preparation process.TheTurboTraceABNSPEsystemautomatesexisting manual SPE techniques and replaces older manual Liquid-Liquid Extraction techniques and outdated semi-auto-mated instruments.

TheTurboTraceABNSPEsystemistheonlySPEsystemthatcombinesDualCartridgeextraction,fractionation,drying and concentration into one step -- providing a truly automatedtotalsampleprepsolutionforthelaboratory.Sim-plyloadsamplesontotheTurboTraceABNSPEsystemandtrigger the automated extraction process. After loading the sample onto the SPE cartridges, the drying step is accom-plished using Nitrogen. This drying step replaces manual techniques. The analytes of interest are then eluted directly to the SuperVap Concentrator where the concentration processautomaticallybringstheextracttofinalvolumeinanautosamplervial,readyforfinalanalysis.Automatingtheseprocesses into one step ensures the highest quality results intheshortestamountoftimeandeliminatesbothhumanerrorandthepossibilityofcontamination.Thefullprocessiscompleteinjustover1hourversus16to18hrsandcutssolventconsumptionby70%.

The TurboTrace ABN System is expandable from one to eight modules.

CompliantComplies with existing methods that require vacuum, positive pressure pumping for the precise delivery of sample and solventsDispensesuptofivesolventsusinganHPLCpumptodeliverprecisevolumesandflowratesfor conditioning and elutionEasy DocumentationProgramsandstoresanunlimitednumberof methods and runs on an SD Card for Easy method transferEasy-to-use software

The First Automated Multi Cartridge MultiFraction Solid Phase Extraction System

The TurboTrace System is expandable from one to eight modules.


TheTurboTraceABNSPEsystemusespositivepressurepumping for precise and accurate delivery of conditioning, washingandelutionsolvents.TheTurboTraceABNSPEsystemisspecificallydesignedtoisolateanalytesofin-terest from a wide variety of liquid matrices such as urine, blood,water,milk,beverages.Samplesizesrangefrom2mlto8Landusethesamebottlethesamplewascollectedin.Sampleloadingratesareprogrammable.Avacuumorpositive pressure pump is used to load samples onto the SPE cartridges and columns at unprecedented speeds and iteasilyhandlesbothcleanandtoughsamplematrices.TheTurboTraceABNSPEsystemconcentratessamplesupto250ml directly to a GC vial. The Sample Processing Module is designed to use all standard formats of SPE cartridges andcolumnsonthemarkettoday.Forguaranteedresults,especially when dealing with low limits of detection, we rec-ommendFMSpre-packedcolumnsandcartridges.

TheTurboTraceABNSPEsystemisaMultiCartridge,MultifractionationsystemthatcanbeusedforanySPEmethodrequiring more than one cartridge or fraction.

TurboTraceABN

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Ordering InformationPart number Description TurboTrace/ABN/1 TurboTraceABNSPEparallelsystemfor1sampleTurboTrace/ABN/2 TurboTraceABNSPEparallelsystemfor2samplesTurboTrace/ABN/3 TurboTraceABNSPEparallelsystemfor3samplesTurboTrace/ABN/4 TurboTraceABNSPEparallelsystemfor4samplesTurboTrace/ABN/5 TurboTraceABNSPEparallelsystemfor5samplesTurboTrace/ABN/6 TurboTraceABNSPEparallelsystemfor6samplesTurboTrace/ABN/-EXP TurboTraceABNExpansionModule

ConsumablesPart number Description SPE-ADP-1 SPE 1ml Cartridge AdapterSPE-ADP-20 SPE 20ml Cartridge AdapterSPE-ADP-3 SPE 3ml Cartridge AdapterSPE-ADP-6 SPE 6ml Cartridge AdapterSPE-BT.05L SPE Sample Bottle 500mlSPE-BT1 SPE Sample Bottle 1LSPE-BT1.25L SPE Sample Bottle 1250mlSPE-BTRC SPE Sample Bottle Rinse CapSPE-CAP-1L SPE Bottle Cap with Loading and SampleRinseTubingsandAdapters,1LSPE-CAP-2L SPE Bottle Cap with Loading and SampleRinseTubingsandAdapters,2LSPE-CAR1-C18 SPE Cartridge 1 gram C18SPE-CAR1-DVB SPE Cartridge 1 gram DVBSPE-CAR5-C18 SPE Cartridge 5 gram C18SPE-CAR6-DVB SPE Cartridge 6 gram DVB

SPE Accessories Part number DescriptionSPE-CART-TRY SPEPortableCartandTraySPE-CAR2 -ABN Kit SPE ABN Cartridge Kit, contains cartridges for ABN extraction

Prep ABN Samples Directly to a Vial in Hours Not DaysTurboTraceABN

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TurboTrace® PFC SPE System

TheTurboTracePFC(Perfluoralkylatedsubstances)SPEsystemisdesignedtostreamlineyourlaboratory’sworkflowandincreaseproductivitybyautomatingthemanualstepsin your sample preparation process. It is designed for high throughputandtoughsamplematrices.TheTurboTracePFC SPE system automates existing manual SPE tech-niques and replaces older manual Liquid-Liquid Extraction techniques and outdated semi-automated instruments.Perfluoralkylatedisageneraltermusedtodescribesub-stances which are largely comprised of or contain a per-fluorinatedorpolyfluorinatedcarbonchainmoietysuchasF(CF2)n-orF(CF2)n-(C2H4)n.Inrecentyears,therehasbeenincreasingconcernoverthelevelsofperfluorinatedandpolyfluorinatedchemicals,suchasPFOS(perfluorosul-fonate)andPFOA(perfluorooctanoicacid),intheglobalen-vironmentandtheirfateandpossibleadverseeffectsintheenvironment.PFOSisnowsubjecttovaryingbutincreasinglevelsofcontrolinanumberofcountries.TheTurboTracePFCSPEsystem,thefirstautomatedsolidphaseextractionsystemmadespecificallyforPFCextractionandconcentra-tion.Primarilyeffectiveatreducingbackgroundcontamina-tion.Extractionandconcentrationofaqueoussamplestakesless than two hours.

The TurboTrace PFC System runs in parallel and is expandable from one to eight modules.

TheTurboTracePFCSPEsystemcombinesextraction,drying and concentration into one step -- providing a truly automatedtotalsampleprepsolutionforthelaboratory.SimplyloadsamplesontotheTurboTracePFCSPEsystem,and use the touch screen to trigger the automated extraction process. After loading the sample onto the SPE cartridge, the drying step is accomplished using vacuum or nitrogen orboth.Thisdryingstepreplacesmanualtechniquessuchas sodium sulfate drying. The analytes of interest are then eluted directly to the SuperVap Concentrator where the con-centrationprocessautomaticallybringstheextracttofinalvolumeinanautosamplervial,readyforfinalanalysis.Au-tomating these processes into one step ensures the highest quality results in the shortest amount of time and eliminates bothhumanerrorandthepossibilityofcontamination.

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Reduces ErrorsOne-stepautomatedSPEandconcentrationeliminateshumanerror,saveslaborcostsandreducessolventusage while increasing your sample throughputReducesbackgroundContaminationFully AutomatedHyphenates the entire sample prep process--ex-traction, drying and concentration steps--into a one step program.Runs up to eight samples simultaneouslySample Liquid Level Sensors to detect when the Sample hasfinishedloadingandtopreventwasteoverflows.AutomaticSamplebottlerinseConcentrates samples up to 250ml directly to a GC vialHigh SpeedThefastestautomatedsampleprocessingavailablefor SPE cartridges and columnsRun up to eight samples simultaneouslyVacuum for fast loading of large volume samples Versatile Handles a wide range of sample sizes and all matrix typesSample Sizes 2ml to many litersSample Liquid Level Sensor to detect when the SamplehasfinishedloadingExpandablefrom1to8modulesEfficientUses all SPE cartridge and column sizesPositive pressure pumping for loading small volume samplesNitrogen drying CompliantComplies with existing methods that require vacuum, positive pressure pumping for the precise delivery of sample and solventsDispenses up to six solvents using an HPLC pump todeliverprecisevolumesandflowratesforcondi-tioning and elutionEasy DocumentationProgramsandstoresanunlimitednumberofmeth-ods and runs on an SD Card for Easy method transferEasy-to-use software - Touch screen operation

TheTurboTracePFCSPEsystemincorporatesvacuumor positive pressure pump to load samples for compliance with all SPE methods. It uses positive pressure pumping for precise and accurate delivery of conditioning, washing andelutionsolvents.TheTurboTracePFCSPEsystemisspecificallydesignedtoisolateanalytesofinterestfromawidevarietyofliquidmatricessuchasurine,blood,water,milk,beverages.Samplesizesrangefrom2mlto8Landusethesamebottlethesamplewascollectedin.Sampleloadingratesareprogrammable.Avacuumorpositivepressurepump is used to load samples onto the SPE cartridges and columns at unprecedented speeds and it easily handles bothcleanandtoughsamplematrices.Aliquidsensorde-tectswhenthesamplehasbeenloaded,triggeringthesys-temtoinitiatenextsteps.TheTurboTracePFCSPEsystemconcentrates samples up to 250ml directly to a GC vial. The Sample Processing Module is designed to use all standard formatsofSPEcartridgesandcolumnsonthemarkettoday.For guaranteed results, especially when dealing with low limitsofdetection,werecommendFMSpre-packedcolumnsandcartridges.SampleProcessingModulescanbeeasilyreplaced to perform cleanup column chemistries allowing thelabtomultipurposetheTurboTracePFCSPEsystemtoautomate other sample prep processes.

The TurboTrace PFC System is expandable from one to eight modules

The First Automated Solid Phase Extraction System Dedicated to Perfluoralkylated Substances TurboTracePFC

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Ordering InformationPart number Description TurboTrace/PFC/1 TurboTracePFCparallelsystemfor1sampleTurboTrace/PFC/2 TurboTracePFCparallelsystemfor2samplesTurboTrace/PFC/3 TurboTracePFCparallelsystemfor3samplesTurboTrace/PFC/4 TurboTracePFCparallelsystemfor4samplesTurboTrace/PFC/5 TurboTracePFCparallelsystemfor5samplesTurboTrace/PFC/6 TurboTracePFCparallelsystemfor6samplesTurboTrace/PFC/7 TurboTracePFCparallelsystemfor7samplesTurboTrace/PFC/8 TurboTracePFCparallelsystemfor8samplesTurboTracePFC-EXP TurboTracePFCExpansionModule

ConsumablesPart number Description SPE-ADP-1 SPE 1ml Cartridge AdapterSPE-ADP-20 SPE 20ml Cartridge AdapterSPE-ADP-3 SPE 3ml Cartridge AdapterSPE-ADP-6 SPE 6ml Cartridge AdapterSPE-BT.05L SPE Sample Bottle 500mlSPE-BT1 SPE Sample Bottle 1LSPE-BT1.25L SPE Sample Bottle 1250mlSPE-BTRC SPE Sample Bottle Rinse CapSPE-CAP-1L SPE Bottle Cap with Loading and SampleRinseTubingsandAdapters,1LSPE-CAP-2L SPE Bottle Cap with Loading and SampleRinseTubingsandAdapters,2L


An Automated Low Background, High Throughput method for a Tedious Manual Sample Prep TurboTracePFC





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NanoTrace® Small Volume SPE system

TheNanoTraceSmallVolumeSPEAutomatedOne-StepExtraction and Concentration System is designed to stream-lineyourlaboratory’sworkflowandincreaseproductivitybyautomating the manual steps in your sample preparation process. The NanoTrace Small Volume SPE system auto-mates existing manual SPE techniques and replaces older manual Liquid-Liquid Extraction techniques and outdated semi-automated instruments.

The NanoTrace Small Volume SPE system is the only small volumeSPEsystemthatcombinesextraction,dryingandconcentration into one step -- providing a truly automated totalsampleprepsolutionforthelaboratory.TheNano-Traceusessmallboretubingthroughouttominimizedeadvolume.Itisspecificallydesignedtouse1mlandlargerSPE cartridges. Simply load samples as small as 250ul onto the NanoTrace Small Volume SPE system and trigger the automated extraction process. After loading the sample onto the SPE cartridge, the drying step is accomplished using Nitrogen. This drying step replaces manual or vacuum techniques used in manifolds. The analytes of interest are then eluted directly to the SuperVap Concentrator where the concentrationprocessautomaticallybringstheextracttofinalvolumedirectlyintoanautosamplervial,readyforfinalanalysis. Automating these processes into one step ensures the highest quality results in the shortest amount of time and eliminatesbothhumanerrorandthepossibilityofcontami-

The NanoTrace Small Volume SPE system can run 5 samples sequentially per module and 2 modules in parallel

Reduces ErrorsOne-stepautomatedSPEandconcentrationeliminateshumanerror,saveslaborcostsandreducessolventusagewhile increasing your sample throughput.

Fully AutomatedHyphenates the entire sample prep process--extraction, drying and concentration steps--into a one step program.

Runsuptofivedifferentmethods/samplematrices sequentially

High SpeedThefastestautomatedsampleprocessingavailablefor1mland up SPE cartridges and columns

Run one sample at a time with a total of 5 in the ready mode

Expandablefromonetotwomodules,eachmodulehas5samples in the ready mode

Onetofoursamplessimultaneously,upto20samples total unattended

Positive Pressure pumping for low volume samples

VersatileHandles a wide range of sample sizes and all matrix types

Sample Sizes 250ul to liters

Expandablefrom1to2modules

5 samples per module sequentially

ApplicationsBlood, Serum, Urine, Pharmaceutical Products,BeveragesCompliantComplies with existing methods that require positive pres-sure pumping for the precise delivery of sample and solvents

DispensesuptofivesolventsusinganHPLCpumptodeliverprecisevolumesandflowratesforconditioning and elution

Easy DocumentationProgramsandstoresanunlimitednumberofmethodsonanSD card for method transfer and storage

Easy-to-use softwareTouch screen entry

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The NanoTrace is modular and expandable from one to four modules to grow with your Laboratory

Unattended Sample Preparation Produces Excellent ResultsNanoTrace

nation.The NanoTrace Small Volume SPE system uses positive pressure pumping for precise and accurate delivery of the sample, conditioning, washing and elution solvents. The NanoTraceSmallVolumeSPEsystemisspecifically designed to isolate analytes of interest from a wide vari-ety of liquid matrices such as pharmaceutical extracts and samples,urine,blood,water,milk,beverages.Samplesizesrangefrom250ultolitersandusethesamebottlethesample was collected in. Sample loading rates are program-mable.Apositivepressurepumpisusedtoloadsamplesonto the SPE cartridges and columns at unprecedented speeds and it easily handles small volume sample matrices. TheNanoTraceSmallVolumeSPEsystemcombinewiththe SuperVap 12 50ml system concentrates samples up to 50ml down to directly to a GC vial. The Sample Process-ing Module is designed to use all standard formats of SPE cartridgesandcolumnsonthemarkettoday.Forguaranteedresults, especially when dealing with low limits of detection, werecommendFMSpre-packedcolumnsandcartridges.





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SpecificationsDimensions:15”Wx18”Dx35”HWeight:65lbs.GasRequirements:Nitrogen-20PSIminimumPump:PistonDisplacementFlowrate:0.2to15ml/minuteElectricalInput:110/220Volts,50/60HZController:IntegratedTouchScreenControl

Ordering InformationPart number Description NanoTrace/1 NanoTracesystemfor5samples(SingleModule)NanoTrace/2 NanoTracesystemfor10samples(TwoModules)Nano-EXP NanoTraceExpansionModule

NanoTrace

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The Powerprep Multi Column Sample Cleanup system auto-mates error prone, complex, tedious, manual sample clean-upandfractionationinthelaboratory.Itreplacesolderman-ualtechniquesbyautomatingthesampleloading,washing,elution, fractionation and evaporation steps of the process increasingthelaboratoriesthroughputbyperformingsamplecleanup and fractionation in hours instead of days.

The PowerPrep Multi Column Sample Cleanup System is theonlyautomatedsampleprocessingsystemofitskindintoday’slaboratories.Theautomatedliquidchromatographysystem performs simultaneous sample processing automat-ically and unattended. The total sample prep process, sam-ple loading, washing, elution and fraction collection is done automatically.Builtbydesignspecificallytoreplacedifficult,errorprone,timeandlaborconsumingmanualprocessesin-volved in sample cleanup for trace analysis. The PowerPrep Multi Column Sample Cleanup System performs the sample cleanup process in hours versus days for the trace analysis ofPersistentOrganicPollutantsinallsamplematrices.

Versatile Rapid Sample Processing:The PowerPrep® system automates the entire manual sample cleanup process, unattended in hours versus days. The Sample Processing Modules canbeeasilyreplacedtoperformsinglecolumnsamplecleanupchemistriesallowingthelabto multipurpose the PowerPrep for automating other sample prep processes.Cost Effective & Reliable Unattended Operation:Performs the entire column chromatography, au-tomatically and unattended achieving consistent, reproduciblerecoveriesforallanalytes.Unattendedoperationofthesystemsaveslaborandtime,re-ducingglasswareandsolvents.Itautomatesdifficultmanualsamplecleanupproceduresspecificallyforthe trace analysis of Dioxins, BFRs, PCBs, Pesti-cides and PAHs.High Recovery of all Analytes:FMScolumnsarecertifiedandguaranteedforthecleanup of samples for the trace analysis of Dioxins, PAHs, PBDEs, and PCBs producing the highest recoveries for all analytes of interest.Modular, Expandable, Affordable, Easy to Maintain:ThePowerPrepsystemismodularandcanbeExpanded from 1 to 8 Samples. Both expansion andmodulereplacementaredoneviaFMS’squickconnect modules. Reducing system down time, in-creasinglaboratorythroughputandeliminatingcrosscontamination from sample to sample.ApplicationsLiquids,Milk,Oil,Serum,Water,WasteWater,Solids, Fish, Feed, Meat, Soil, Fly AshSupported EPA MethodsMethod 1613 Dioxin and FuransMethod 1614 Brominated Diphenyl Ethers in Water, Soil, Sediment and TissueMethod 1668A Clorinated Bipenyl CongenersSW - 846 Test Methods for Solid Waste40CFR136 MethodsforPOPsanalysis

PowerPrep® MultiColumn Sample Cleanup for Trace Analysis

The PowerPrep Multicolumn Cleanup system runs 1 to 8 samples in parallel performing sample cleanup and fractionation with direct to vial concentration

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Disposable Columns:The PowerPrep System uses FMS proprietary columnsthataremadefromteflonandcontain packing’ssuchasmulti-layerABNsilica,acidicsilica,basicsilica,neutralsilica,alumina,carbonandflorisil.FMScolumnsaretestedforpurityandperformance.Priortoshipmenttheyarecertifiedandguaranteed.FMScolumnsareCertifiedandGuaran-teed for the cleanup of sample for the Trace Analysis of Dioxins, PAHs, PBDEs, and PCBs producing the Highest Recoveries for all analytes of interestEasy Documentation:Programs and stores an unlimited amount of methods and runs.

Samples are cleaned up and directly fractionated to the SuperVap Concentrator for unattended concen-tration directly to a vial.

PowerPrep

The PowerPrep Multicolumn Cleanup system is modular and is expandable from 1 to 8 samples to meet your laboratories throughput

SpecificationsDimensions:15”Wx18”Dx35”HWeight:65lbs.Pump:PistonDisplacementFlowrate:0.2to15ml/minuteElectricalInput:110/220Volts,50/60HZ

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FMS pre-packed Columns for guaranteed purity.

Optional SuperVap concentration for one step sample cleanup and concentration for Dioxin and PCBs analysis

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PowerPrep

PowerPrep ConsumablesPart Number Description Low capacity ColumnsLCDS-ABN-STD LowCapacityDisposableSilicaABNColumnLCDA-BAS-006 LowCapacityDisposableBasicAluminaColumnCLDC-CCE-034 DisposableCarbon/Celite(.34g)Column Low Capacity PCB Free ColumnsPCBL-ABN-STD PCBFreeLowCapacityDisposableSilica ABN ColumnPCBL-BAS-006 PCBFreeLowCapacityDisposableAlumina (6g)ColumnPCBC-CCE-034 PCBFreeClassicalDisposableCarbon/celite Column .34g Low Capacity PBDE free columnsPBDEL-BAS-006 PBDEFreeLowCapacityDisposableAlumina(6g) ColumnPBDEL-ABN-STD PBDEFreeLowCapacityDisposableSilicaABN ColumnPBDEL-CCE-034 PBDEFreelowcapacityDisposableCarbon/Celite column .34 g Classical ColumnsCLDS-ABN-STD ClassicalDisposableSilicaABNColumnCLDA-BAS-011 DisposableBasicAlumina(11g)ColumnCLDC-CCE-034 DisposableCarbon/Celite(.34g)ColumnHCDS-ABN-STD HighCapacityDisposableABNSilicaColumnHCDS-ACD-STD HighCapacityDisposableAcidicSilicaColumnHCDS-ABN-STD-TFC HighCapacityDisposableABNSilicaColumnwith TeflonChipHCDS-ACD-STD-TFC HighCapacityDisposableAcidicSilicaColumnwith TeflonChip PCB Free classical ColumnsPCBS-ABN-STD PCBFreeClassicalDisposableSilicaABNColumnPCBA-BAS-011 PCBFreeDisposableAlumina(11g)ColumnPCBC-CCE-034 PCBFreeClassicalDisposableCarbonColumnPCB-HCDS-ABN PCBFreeHighCapacityDisposableABN Silica ColumnPCB-HCDS-ACD PCBFreeHighCapacityDisposableAcidic Silica ColumnPCB-HCDS-ABN-TFC PCBFreeHighCapacityDisposableABNSilica ColumnwithTeflonChipPCB-HCDS-ACD-TFC PCBFreeHighCapacityDisposableAcidicSilica ColumnwithTeflonChip PBDE Free classical columnsPBDES-ABN-STD PBDEFreeClassicalDisposableSilicaABNColumnPBDEA-BAS-011 PBDEFreeDisposableAlumina(11g)ColumnPBDEC-CCE-034 PBDEFreeClassicalDisposableCarbon/Celite ColumnPBDE-HCDS-ABN PBDEFreeHighCapacityDisposableABNSilica ColumnPBDE-HCDS-ACD PBDE Free High Capacity

Part Number Description

Disposable Acidic Silica ColumnPBDE-HCDS-ABN-TFC PBDEFreeHighCapacityDisposableABNSilica ColumnwithTeflonChipPBDE-HCDS-ACD-TFC PBDEFreeHighCapacityDisposableAcidicSilica ColumnwithTeflonChip Silver Nitrate /Silica columnsCLDS-ABN-SNT ClassicalDisposableABNSilica+SilverNitrate ColumnPCBS-ABN-SNT PCBFreeClassicalDisposableABNSilica+ Silver Nitrate ColumnPBDES-ABN-SNT PBDEFreeClassicalDisposableABNSilica+ Silver Nitrate ColumnHCDS-ABN-SNT HighCapacityDisposableABNSilica+Silver Nitrate Column Carbon/Silica columnsCLDC-CSI-002 DisposableCarbon/Silica(2g)ColumnPCBC-CSI-002 PCBFreeDisposableCarbon/Silica(2g)ColumnPBDEC-CSI-002 PBDEFreeDisposableCarbon/Silica(2g)Column

Miscellaneous columnsCLDF-FLR-705 ClassicalDisposableFlorisil(7.5g)ColumnCLDS-ACD-008 ClassicalDisposableAcidicSilica(8g)ColumnCLDS-NSS-060 ClassicalDisposableNeutralSilica(6g)ColumnPCBA-5BAS-011 PCBFreeDisposable0.5%DeactivatedAlumina (11g)ColumnPBDEA-5BAS-011 PBDEFreeDisposable0.5%DeactivatedAlumina (11g)Column Hex FittingsCLTF-FIT-000 FittingTeflonHexForClassicalTeflonColumnsCLTF-FIT-025 FittingTeflonHexForHighCapacityColumns Tefzel fittingsUNI-TFZ-028 FittingTefzelUnionMLU-TFZ-028 FittingTefzelMaleLuerFLU-TFZ-028 FittingTefzelFemaleLuer Delrin FittingsUNI-DEL-028 Fitting Delrin UnionMLU-DEL-028 Fitting Delrin Male LuerFLU-DEL-028 Fitting Delrin Female Luer

FritzFRZ-TFE-678 SmallFritzFRZ-TFE-901 LargeFritz Vial & SyringeTUBE-CEN-015 Glass Sample Vials With Caps 15mlSYRI-POL-010 PolypropyleneSyringes

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The PowerPrep® EPH Fractionation system performs fractionation and sample cleanup for up to 30 samples in less than one hour, producing the highest recoveries and bestresultsforaliphaticandaromatichydrocarboncontent.With the PowerPrep EPH system you have the option of expandingfromonemodule,thatwillperformfivesamplefractionationandcleanups,toasixmodulesystemcapableof performing 30 sample fractionation and cleanups.

ThePowerPrepEPHsystemdeliversthereproducibilityyoudemandbyconsistentlyconditioningthecolumns,deliveringthe sample performing the sample cleanup and fractionation. The PowerPrep EPH system increases sample throughput while reducing errors. It eliminates poor recoveries and providesacleanerbackgroundwhileeliminatingcontamina-tion. This system uses FMS’s high quality and inexpensive, Polypropylenebased,pre-packed,disposablecolumnsthatdeliver high recoveries and eliminate the errors and time spentonmanualcolumnpacking,gravimetricchromatogra-phy and glassware cleanup.

Separates Aliphatic and Aromatic HydrocarbonsFractionation is accomplished using either polypro-pylenecartridgespre-packedwithsilicagelorglasscolumnsmanuallypackedwithconditionedsilicagel.Whileitisdifficulttoachievethehighaliphaticandaromatic compounds recovery, the manual collection offractionsbyusingpoly-propylenecartridgesormanuallypackedglasscolumnsrequiresadditionaltimeforcolumnpreparationandcalibration.FMSoffers a precise method that is automatically con-trolledbyaprogrammableworkstationwithpatentedpre-packedandpre-conditionedcolumns.Together,they guarantee a consistent level of fractionation and recoveries of targeted compounds.Fast turnaround: 30 Samples in One HourThe PowerPrep EPH system increases sample throughput while reducing errors and poor recoveries.Produces Consistent, Reproducible Results Withjustafewkeystrokes,thePowerPrepEPHsys-tem performs an entire column chromatography, au-tomatically achieving high recoveries for all analytes.Ready-to-Use, Conditioned Columns From FMSThePowerPrepEPHsystemusespre-packeddis-posablecolumnsmadefromTeflonandsilica.FMS’scolumns are tested for purity and performance prior to shipment.Automates in compliance with Methods MADEP EPH, TNRCC Method 1005-1006The PowerPrep EPH system is changing high speed sampleprocessingintoday’slaboratories.Youneedonlytoloadyoursamples,snaponyourpre-packedcolumnsandpressthestartkey.Thesystemper-forms the entire sample cleanup and fractionation according to the MADEP EPH, TNRCC Method 1005-1006makingcomplianceeasy.

PowerPrep® EPH Single Column Cleanup and Fractionation System

The PowerPrep EPH Single Column Cleanup and Fractionation System system runs 5 samples sequentially and in parallel while providing direct-to-vial concentration

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PowerPrep EPH

Reduce solvent and glassware usageFMSpre-packeddisposablecolumnseliminatewashing glassware and the solvents to clean that glassware.Dramatically Cuts Operation CostsUnattendedoperationofthesystemsaveslaborandvaluabletime.FMSpre-packedcolumns reducetheneedtoQCtestinthelabaswellaserrors caused from manual fractionation.Modular and expandableWith the PowerPrep EPH Fractionation system you have the option to expand from one module, which willperformfivesamplefractionationandcleanups,a six module system which will perform 30 sample fractionation and cleanups.Robust and Easy to MaintainBoth system expansion and module replacement areperformedviaFMS’squickconnectmodules.This feature reduces system down time and increaseslaboratorythroughput.Cookbook MethodFMS’spowerfulwindows-basedmonitoringandcontrol software offers a rich set of features and flexibility,includingmethodsdevelopmentandoptimization.Oncethemethodisoptimizeditissaved and used for each run, eliminating the need to create a new method each time the system is run.Inputparametersincludeflowrates,volumes,column selection, sample size, solvent selection and fraction collection.

SpecificationsDimensions:15”Wx18”Dx35”HWeight:130lbs.Pump:PistonDisplacementFlowrate:0.2to15ml/minuteElectricalInput:110/220Volts,50/60HZController:PCbased

The SuperVap® Small Volume is a standalone automated direct-to-vial concentration system

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The PowerPrep GPC® system is a low cost automated Gel Permeation Chromatography system designed to separate synthetic macromolecules such as pesticides, PCBs, PAHs etc.frominterferingcompounds.Itusesglassortefloncolumnspackedwithstyrene-divinylbenzeneresinbeadstoperform sample clean-up using size exclusion chromatog-raphy technique. The samples are loaded onto the column, then washed and collected in the appropriate fraction ves-sels.ThePowerPrepGPCsystemgreatlysimplifiessamplecleanup through its unattended operation, increased speed andprecision.Optionssuchasdifferenttypesofcolumns,UV detector and a PC allow versatility in a sample type, automaticmonitoring,datarecordingandprogrammablecontrol over all aspects of the separation procedure.

The PowerPrep GPC system can automate pesticide samplecleanupproceduresspecifiedbytheUSEPAandFDA methods. The modularity and expansion features of the GPC-Prep allow the user to expand the system for use in other applications such as the separation of Dioxins and PCBsfromenvironmentalandbiologicalsamples.

ApplicationsPesticides, PCBs, PAHs, Dioxins, FuransSupported EPA MethodsMethos 3649 Gel Permeation CleanupCost Effective Expandable Systems ThePowerPrepGPCsystemfitsintothesmallestbudget.Withitsmodulardesign,youcancosteffec-tively automate your sample clean-up procedure bypurchasingonemoduleandexpanditto5,10,15or up to 40 samples as needed.

ThePowerPrepGPCsystemprovidesmajorsavingsin solvents and glassware as compared with the amounts typically required in manual procedures. WithFMS’slowcostpre-packedTefloncolumnsthesavingsbecomemoresubstantial.

PowerPrep® GPC

The PowerPrep GPC/ Parallel System is mod-ular & expandable from one to four modules processing 2 to 8 samples simultaneously

PowerPrep GPC /Sequential system processes 5 samples sequentially

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SuperVap concentration system for one step GPC clean-up and concentration for fast analysis

The PowerPrep Parallel GPC System is expandable from one to four modules and can process eight samples at the same time.

PowerPrep GPC system includes: •MainController •SampleProcessingModule •UVdetector •Pre-packedTeflonorGlassColumn

Easy Monitoring With The UV detector UVdetectorwitha254nmflowcellisusedforeasycolumncalibrationandmonitoringtheelutionprofile.Enhanced Monitoring & Real Time Plotting ThePowerPrepGPCcontrolsallthefluidhandling,including the pump, valves and columns. The entire separation procedure, including sample loading, columnwashing,elutionandpeakseparation,iscoordinatedbytheGPCcontroller.TheEditorfunc-tion allows the operator to create, review and run various separation protocols. The PowerPrep GPC also plots, displays and stores the separation data. Column CalibrationFlow:5ml/minDetector:UV,254mmColumns:

450 x 25 mm Glass column 300x20mmPre-PackedTefloncolumn150x20mmPre-PackedTefloncolumn

Standard CLP Calibration Standard •Cornoil(125mg)•Diethylphthalate(5mg) •Methoxychlor(1mg)•Perylene(0.1mg)•Sulfur(0.4mg)

System Configurations:PowerPrep GPC /P Parallel System Thissystemismodularandexpandablefrom2to8 samples. The samples are loaded and processed simultaneouslyPowerPrep GPC /S Sequential system ThePowerPrepGPCbasicsystemconsistsofoneor more modules where each module can sequen-tiallyprocessuptofivesamplesautomaticallyandunattended. By upgrading from one to up to eight modules,youcanexpandthesystem’scapabilityfrom 5 to up to 40 samples, where all modules are processed in parallel.

Gel Permeation Chromatography is a size exclusion technique. Large compounds, greater than the molecular exclusion limit, pass through the column unhindered, where-as small compounds, within the molecular weight operating range,willberetainedinthecolumn.Thesmallcompoundspermeatetheporesofthestyrene-divinylbenzenebeads,andthustheytakelongertopassthroughthecolumn.

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SpecificationsDimensions:15”Wx18”Dx35”HWeight:65lbs.Pump:PistonDisplacementFlowrate:0.2to15ml/minuteElectricalInput:110/220Volts,50/60HZ Controller:PCIntegratedTouchScreenControl

Ordering informationPowerPrep GPC / ParallelPartnumberDescriptionPowerPrep GPC/P2 2 sample GPC, 1 modulePowerPrep GPC/P4 4 sample GPC, 2 modulesPowerPrep GPC/P6 6 sample GPC, 3 modulesPowerPrep GPC/P8 8 sample GPC, 4 modules

PowerPrep GPC/SequentialPowerPrep GPC/S5 5 sample GPC ,1 modulePowerPrep GPC/S10 10 sample GPC, 2 modulesPowerPrep GPC/S15 15 sample GPC, 3 modulesPowerPrep GPC/S20 20 sample GPC, 4 modulesPowerPrep GPC/S25 25 sample GPC, 5 modulesPowerPrep GPC/S30 30 sample GPC, 6 modulesPowerPrep GPC/S35 35 sample GPC, 7 modulesPowerPrep GPC/S40 40 sample GPC, 8 modules

GPC Columns & AccessoriesGPC-UV-254 UV detector, 254 nmTEF-COL-300GPCPre-packedTefloncolumn300x20mmTEF-COL-150GPCPre-packedTefloncolumn150x20mmGLS-COL-450GPCGlasscolumn450x25mmmSTR-DVI-100Styrene-divinylebenzene Copolymer,100 grams

Columns:Glass Columns ThesecolumnsarepackedwithSDVBresinbeads.Theinnovativedesignoftheseglasscolumnsallowsyoutoadjustthegelbedheightforbetterreliabilityandturbulence-freeapplications.

Teflon Columns FMS’spre-packeddisposableTefloncolumnsemployaproprietarydesignthatallowsuptoa70%solventreduction.Thesecolumnsareeasytouseand dramatically reduce elution time.

PowerPrep GPC

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SuperVap® Family of Automated Direct-to-Vial Concentration and Evaporation

The SuperVap® Small Volume is a standalone automated direct-to-vial concentration system that replaces older, man-ualtechniquessuchasKD,nitrogenblowdownandwaterbaths.TheSuperVapSmallVolumedirect-to-vialconcen-tration system is designed to simplify, improve and increase laboratoryproductivitybyautomatingthemanualstepsinyour sample evaporation/concentration process. It auto-mates the time consuming steps involved in manual sample concentration,lowerslaborcostsandeliminateserrors.

The SuperVap concentrator sets a new standard for automating rapid sample evaporation and concentra- tionforproducingconsistent,reliableresults.The SuperVap automated concentration system is ideal for the analysisofpesticides,herbicides,

persistent organic pollutants, PCBs

HEPA/carbon filter eliminates outside contamination

Uses no water, dry heating

assembly makes solvent

recovery simple

Concentrates up to 12 20ml, 40ml, 60ml vials or 50ml concentration vessels with tips.

Concentrates up to 24 2ml or 4ml vials.

Measurements-Concentration/Evaporation Vessels in 500 µL, 1ml, and direct-to-a GC Vial or to dryness

Automatic time-based or endpoint detection for nitrogen shut off

for each vessel

Sample sizes from 1ml to 50ml

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Sample sizes from 1ml to 50ml

SuperVap® 6 250ml

The SuperVap® system is an automated, standalone, di-rect-to-vial concentrator that replaces older techniques such asKD,nitrogenblowdownandwaterbaths.Byautomatingwhat were once manual evaporation and concentration processes, the SuperVap concentration system accelerates yoursamplethroughput,lowerslaborcosts,andimprovestheconsistencyofyourresultsbyeliminatingthevariabilityinherent in manual sample prep procedures.

The SuperVap concentrator sets new a standard for con-sistency,speed,andreliabilityofresultsforanautomatedsample evaporation and concentration system. It is ideal for theanalysisofpesticides,herbicides,PersistentOrganicPollutants(POPs),PCBs,PAHs,pharmaceuticalbyprod-ucts,andpersonalcarebyproductsaswellasmanyotherapplications.TheprogrammableSuperVapconcentratorisa dry, waterless concentrator that can preheat as well as rampuptofinaltemperature.Itautomaticallysenseswhentheextractisbeingdeliveredtoeachvessel,startstheblowdownandthenshutsoffthenitrogenwhenfinalvolumeisachieved. The concentrated samples are then automatically transferred directly to a vial, eliminating the errors that occur during manual transfer.

Easy-to-UseThe SuperVap concentration system uses a touch screen display for programming, storing, and running methods. Real-time plotting of temperature readings are displayed throughout the process. Simply touch a point on the plot and instantly see the temperature of that point.Reduces ErrorsThe SuperVap system performs the entire evapora-tion and concentration process, automatically, deliv-eringconsistent,reproduciblyhighrecoveriesforallanalytes. Unattended operation of the sample prep processsavestime,reduceslaborcosts,glasswareand solvents.High Recovery of All AnalytesThe SuperVap system provides direct-to-vial concen-tration with automatic endpoint detection and Nitro-gen shut off for each vesselUses No WaterUsesarobustwaterless,drybathwithnoelectron-icssubmergedinwater.Iteasilyandinexpensivelycaptures solvents.Concentrates up to 6 SamplesSample Sizes up to 250ml. Compact SizeMinimizes ContaminationAnintegratedHEPA/Carbonfiltereliminatesoutsidecontamination.Inexpensive GlasswareEconomically priced vessels with 500 µL, 1ml and direct-to-vial endpoints. Fully AutomatedAutomatic endpoint detection, nitrogen shutoff, and alarmforeachvessel.Programmableheatrampandnitrogen settings for precise control of the concentra-tion and evaporation process.DocumentationEvery method and run is documented and stored on the SuperVap system for easy retrieval for documen-tation. A temperature log for each run is also saved andmaybedownloadedtoaPCviaaUSBport.Stand Alone or IntegratedTheSuperVapconcentratorcanbeeasilyintegratedinto existing FMS sample preparation systems. IntegrationallowsforPC-basedcontroland automatic solvent exchange.

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SuperVap® 12 50ml

The SuperVap® system is an automated, standalone, di-rect-to-vial concentrator that replaces older techniques such asKD,nitrogenblowdownandwaterbaths.Byautomatingwhat were once manual evaporation and concentration processes, the SuperVap concentration system accelerates yoursamplethroughput,lowerslaborcosts,andimprovestheconsistencyofyourresultsbyeliminatingthevariabilityinherent in manual sample prep procedures.

The SuperVap, 12 position, 50ml Direct-to-vial Evapora-tion/Concentration system is the ideal sample preparation solutionforSolidPhaseExtraction(SPE)andPressurizedLiquidExtraction(PLE)methodsrequiringtheevaporationand concentration of liquid extracts. Typical extractions needingevaporationand/orconcentrationtofinalvolumearethosefromdrinkingwater,wastewater,juice,milk,urine,and human serum. The system uses evaporation/concentra-tion vessels that handle liquid extraction volumes from 1ml to40mlwithfinalvolumetipsof500µLor1ml,oryoucanchoose GC vials. The SuperVap Evaporation/Concentration system is designed to automatically evaporate and concen-trate 12 samples simultaneously. Sensors detect when the end point is reached and shut off each individual position whiletriggeringanaudiblealarmtoalerttheuser.

Easy-to-UseThe SuperVap concentration system uses a touch screen display for programming, storing, and running methods. Real-time plotting of temperature readings are displayed throughout the process. Simply touch a point on the plot and instantly see the temperature of that point.Reduces ErrorsThe SuperVap system performs the entire evapora-tion and concentration process, automatically, deliv-eringconsistent,reproduciblyhighrecoveriesforallanalytes. Unattended operation of the sample prep processsavestime,reduceslaborcosts,glasswareand solvents.High Recovery of All AnalytesThe SuperVap system performs the entire evapora-tion and concentration process, automatically, deliv-eringconsistent,reproduciblyhighrecoveriesforallanalytes. Unattended operation of the sample prep processsavestime,reduceslaborcosts,glasswareand solvents.Uses No WaterUsesarobustwaterless,drybathwithnoelectron-icssubmergedinwater.Iteasilyandinexpensivelycaptures solvents.Concentrates up to 12 SamplesSample Sizes up to 50ml in a concentration vessel. Compact SizeMinimizes ContaminationAnintegratedHEPA/Carbonfiltereliminatesoutsidecontamination.Inexpensive GlasswareEconomically priced vessels in with 500 µL, 1ml and direct-to-vial endpoints.Fully AutomatedAutomatic endpoint detection, nitrogen shutoff, and alarmforeachvessel.Programmableheatrampandnitrogen settings for precise control of the concentra-tion and evaporation process.DocumentationEvery method and run is documented and stored on the SuperVap system for easy retrieval for electronic documentation. A temperature log for each run is alsosavedandmaybedownloadedtoaPCviaaUSB port.Stand Alone or IntegratedTheSuperVapconcentratorcanbeeasilyintegratedinto existing FMS sample preparation systems. In-tegrationallowsforPC-basedcontrolandautomaticsolvent exchange.

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SuperVap® 12 20ml

The SuperVap®, 12 position, 20ml vial, Evaporation/Concen-trationsystemistheidealsolutionforperformingthefinalevaporation and concentration step for solid phase ex-traction(SPE)andpressurizedliquidextraction(PLE)(ASE)sample preparation methods. Typical extractions requiring evaporationorconcentrationtofinalvolumearedrinkingwater,wastewater,juice,milk,urine,andhumanserum.The system uses 20ml evaporation/concentration vials that handle liquid extract volumes up to 20ml. The system is de-signed to automatically evaporate and concentrate 12 sam-ples simultaneously and will shut off when the programmed endtimeisreached,whichalsotriggersanaudiblealarm.

Easy-to-UseThe SuperVap concentration system uses a touch screen display for programming, storing, and running methods. Real-time plotting of temperature readings are displayed throughout the process. Simply touch a point on the plot and instantly see the temperature of that point.Reduces ErrorsThe SuperVap system performs the entire evapora-tion and concentration process, automatically, deliv-eringconsistent,reproduciblyhighrecoveriesforallanalytes. Unattended operation of the sample prep processsavestime,reduceslaborcosts,glasswareand solvents.High Recovery of All AnalytesThe SuperVap system provides concentration with automatic endpoint detection and Nitrogen shut off for each vessel.Uses No WaterUsesarobustwaterless,drybathwithnoelectron-icssubmergedinwater.Iteasilyandinexpensivelycaptures solvents.Concentrates up to 12 SamplesSample Sizes up to 20ml.Compact SizeMinimizes ContaminationAnintegratedHEPA/Carbonfiltereliminatesoutsidecontamination.Inexpensive GlasswareEconomically priced vessels, 20ml VialFully AutomatedAutomatic nitrogen shutoff, and alarm for vessel. Programmableheatrampandnitrogensettingsforprecise control of the concentration and evaporation process.DocumentationEvery method and run is documented and stored on the SuperVap system for easy retrieval for documen-tation. A temperature log for each run is also saved andmaybedownloadedtoaPCviaaUSBport.Stand Alone or IntegratedTheSuperVapconcentratorcanbeeasilyintegratedinto existing FMS sample preparation systems. In-tegrationallowsforPC-basedcontrolandautomaticsolvent exchange.

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SuperVap® 12 40ml

The SuperVap® 12 position 40ml vial Evaporation/Concen-trationsystemistheidealsolutionforperformingthefinalevaporation and concentration step for solid phase ex-traction(SPE)andpressurizedliquidextraction(PLE)(ASE)sample preparation methods. Typical extractions requiring evaporationorconcentrationtofinalvolumearedrinkingwater,wastewater,juice,milk,urine,andhumanserum.Thesystem uses 40ml evaporation/concentration vials that han-dleliquidextractionvolumesupto40ml,withfinalvolumesbetweendrynessand40ml.Thefinalvolumeisreachedau-tomaticallybyprogramminganendpointtime.Thesystemis designed to automatically evaporate and concentrate 12 samples simultaneously and will shut off when the programmed end time is reached, which also triggersanaudiblealarm.

Easy-to-UseThe SuperVap concentration system uses a touch screen display for programming, storing, and running methods. Real-time plotting of temperature readings are displayed throughout the process. Simply touch a point on the plot and instantly see the temperature of that point.Reduces ErrorsThe SuperVap system performs the entire evapora-tion and concentration process, automatically, deliv-eringconsistent,reproduciblyhighrecoveriesforallanalytes. Unattended operation of the sample prep processsavestime,reduceslaborcosts,glasswareand solvents.High Recovery of All AnalytesThe SuperVap system provides concentration with automatic endpoint detection and Nitrogen shut off for each vessel.Uses No WaterUsesarobustwaterless,drybathwithnoelectron-icssubmergedinwater.Iteasilyandinexpensivelycaptures solvents.Concentrates up to 12 SamplesSample Sizes up to 40ml.Compact SizeMinimizes ContaminationAnintegratedHEPA/Carbonfiltereliminatesoutsidecontamination.Inexpensive GlasswareEconomically priced vessels in 40ml Vial Fully AutomatedAutomatic nitrogen shutoff, and alarm for each ves-sel.Programmableheatrampandnitrogensettingsfor precise control of the concentration and evapora-tion processDocumentationEvery method and run is documented and stored on the SuperVap system for easy retrieval for documen-tation. A temperature log for each run is also saved andmaybedownloadedtoaPCviaaUSBport.Stand Alone or IntegratedTheSuperVapconcentratorcanbeeasilyintegratedinto existing FMS sample preparation systems. In-tegrationallowsforPC-basedcontrolandautomaticsolvent exchange.

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SuperVap® 12 60ml

The SuperVap® 12 position 60ml vial Evaporation/Concen-trationsystemistheidealsolutionforthefinalevaporationand concentration step for ASE types of liquid sample preparation. Typical extractions requiring evaporation or concentrationtoafinalvolumearedrinkingwater,wastewater,juice,milk,urine,andhumanserum.Thesystemuses60ml vials for evaporation/ concentration and can handle liquidextractvolumesupto60mlwithfinalvolumes.The finalvolumeisreachedautomaticallybyprogramminganend time. The system is designed to automatically evap-orate and concentrate 12 samples simultaneously and will shut off when the programmed end time is reached, which triggersanaudiblealarm.

Easy-to-UseThe SuperVap concentration system uses a touch screen display for programming, storing, and running methods. Real-time plotting of temperature readings are displayed throughout the process. Simply touch a point on the plot and instantly see the temperature of that point.Reduces ErrorsThe SuperVap system performs the entire evapora-tion and concentration process, automatically, deliv-eringconsistent,reproduciblyhighrecoveriesforallanalytes. Unattended operation of the sample prep processsavestime,reduceslaborcosts,glasswareand solvents.High Recovery of All AnalytesThe SuperVap system provides concentration with automatic endpoint detection and Nitrogen shut off for each vessel.Uses No WaterUsesarobustwaterless,drybathwithnoelectron-icssubmergedinwater.Iteasilyandinexpensivelycaptures solvents.Concentrates up to 12 SamplesSample Sizes up to 60ml.Compact SizeMinimizes ContaminationAnintegratedHEPA/Carbonfiltereliminatesoutsidecontamination.Inexpensive GlasswareEconomically priced vessels, 60ml Vial.Fully AutomatedAutomatic nitrogen shutoff, and alarm for each vessel.Programmableheatrampandnitrogen settings for precise control of the concentration and evaporation process.DocumentationEvery method and run is documented and stored on the SuperVap system for easy retrieval for documen-tation. A temperature log for each run is also saved andmaybedownloadedtoaPCviaaUSBport.Stand Alone or IntegratedTheSuperVapconcentratorcanbeeasilyintegratedinto existing FMS sample preparation systems. IntegrationallowsforPC-basedcontroland automatic solvent exchange.

SuperVap® 24 2ml

The SuperVap® 24 position, 2ml vial Evaporation/Concentra-tionsystemistheidealsolutionforthefinalevaporationandconcentration step for many sample preparation methods. The system uses 2ml vials that handle liquid extractvolumesupto2mlwithfinalvolumestofinaldrynessorapre-determinedvolume.Thefinalvolumeisachievedwhenthe system automatically reaches the end of its programmed time. Typical extractions requiring evaporation or concen-trationtofinalvolumeareMetabolomics,POPs,oranyextractionwhereafinalvolumemanualevaporationtech-niquesarerequiredtofinishtheprocess.Thesystemisde-signed to automatically evaporate and concentrate 24 sam-ples simultaneously. Shut off occurs when the programmed endpointtimeisreachedwhichtriggersanaudiblealarm.

Easy-to-UseThe SuperVap concentration system uses a touch screen display for programming, storing, and running methods. Real-time plotting of temperature readings are displayed throughout the process. Simply touch a point on the plot and instantly see the temperature of that point.Reduces ErrorsThe SuperVap system performs the entire evapora-tion and concentration process, automatically, deliv-eringconsistent,reproduciblyhighrecoveriesforallanalytes. Unattended operation of the sample prep processsavestime,reduceslaborcosts,glasswareand solvents.High Recovery of All AnalytesThe SuperVap system provides concentration with automatic endpoint detection and Nitrogen shut off for each vessel.Uses No WaterUsesarobustwaterless,drybathwithnoelectron-icssubmergedinwater.Iteasilyandinexpensivelycaptures solvents.Concentrates up to 24 SamplesSample Sizes up to 2ml.Compact SizeMinimizes ContaminationAnintegratedHEPA/Carbonfiltereliminatesoutsidecontamination.Inexpensive GlasswareEconomically priced vessels, 2ml GC VialsFully AutomatedAutomatic nitrogen shutoff, and alarm for each ves-sel.Programmableheatrampandnitrogensettingsfor precise control of the concentration and evapora-tion process.DocumentationEvery method and run is documented and stored on the SuperVap system for easy retrieval for documen-tation. A temperature log for each run is also saved andmaybedownloadedtoaPCviaaUSBport.Stand Alone or IntegratedTheSuperVapconcentratorcanbeeasilyintegratedinto existing FMS sample preparation systems. In-tegrationallowsforPC-basedcontrolandautomaticsolvent exchange.

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SuperVap® 24 4ml

The SuperVap® 24 position, 4ml vial, Evaporation/Concen-trationsystemistheidealsolutionforperformingthefinalevaporation and concentration step for a variety of sample preparation methods. The system uses 4ml vials that handle liquidextractvolumesupto4mlwithfinalvolumestofinaldrynessorapredeterminedvolume.Thefinalvolumeisautomatically achieved when the system reaches the end of its programmed time. Typical extractions requiring evap-orationorconcentrationtofinalvolumeareMetabolomics,POPs,oranyextractionwherefinalvolumemanualevap-orationtechniquesarerequiredtofinishtheprocess.Thesystem is designed to automatically evaporate and concen-trate 24 samples simultaneously. Shut off occurs when the programmed end point time is reached which triggers an audiblealarm.

Easy-to-UseThe SuperVap concentration system uses a touch screen display for programming, storing, and running methods. Real-time plotting of temperature readings are displayed throughout the process. Simply touch a point on the plot and instantly see the temperature of that point.Reduces ErrorsThe SuperVap system performs the entire evapora-tion and concentration process, automatically, deliv-eringconsistent,reproduciblyhighrecoveriesforallanalytes. Unattended operation of the sample prep processsavestime,reduceslaborcosts,glasswareand solvents.High Recovery of All AnalytesThe SuperVap system provides direct-to-vial concentration with automatic endpoint detection and Nitrogen shut off for each vessel.Uses No WaterUsesarobustwaterless,drybathwithnoelectron-icssubmergedinwater.Iteasilyandinexpensivelycaptures solvents.Concentrates up to 24 SamplesSample Sizes up to 4ml.Compact SizeMinimizes ContaminationAnintegratedHEPA/Carbonfiltereliminatesoutsidecontamination.Inexpensive GlasswareEconomically priced vessels, 4ml VialsFully AutomatedAutomatic nitrogen shutoff, and alarm for each vessel.Programmableheatrampandnitrogen settings for precise control of the concentration and evaporation process.DocumentationAutomatic endpoint detection, nitrogen shutoff, and alarmforeachvessel.Programmableheatrampandnitrogen settings for precise control of the concentra-tion and evaporation process.Stand Alone or IntegratedTheSuperVapconcentratorcanbeeasilyintegratedinto existing FMS sample preparation systems. In-tegrationallowsforPC-basedcontrolandautomaticsolvent exchange.

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47

SuperVap® Family

SpecificationsDimensions: 13”Wx13”Dx12”HWeight: 20lbs.Gasrequirements: Nitrogen-20PSIminimumElectricalinput: 110/220Volts,50/60HZController: IntegratedTouchScreenControlBath: Dry

Ordering informationConcentrator and AccessoriesPart Number Description SuperVap Concentrator Standalone SuperVap-6/SC 6 Position with 250ml concentration tubesSVAP-TUB-200M-1000250mlconcentratortube,1mltipSVAP-TUB-200M-500 250mlconcentratortube,standard500µLtipSVAP-TUB-200M-GC 250mlconcentratortube,standardGCvialtipSVAP-UNI-TFZ TefzelGCvialunionSVAP-UNI-WSR TeflonGCvialunionwasher,packof100SVAP-VIAL-GC GC vialFMS-TR-2006 6Positionconcentratortuberackfor250mltubeFMS-TR-2012 12Positionconcentratortuberackfor250mltubeHEP-FIL-200 HepafilterCAR-FIL-200 Carbonfilter

SuperVap Concentrator Standalone SuperVap-12/SC 12 Position with 50ml concentration tubesSVAP-TUB-060M-1000 50mlconcentratortube,1mltipSVAP-TUB-060M-500 50mlconcentratortube,standard500µLtipSVAP-TUB-060M-GC 50mlconcentratortube,standard GC vial tip

Easy-to-use touch screen programming

Programmable heat ramp and nitrogen settings to precisely control the concentration and evaporation process

In order from left to right50ml tube with tip50ml tube with tip40ml vial20ml vial2ml vial

SuperVap Concentrator Standalone SuperVap-12/SV 12 Position for 20, 40, 60ml vials (no block)SVAP-BLK-12-020 SuperVapconcentratorblock-12positionwith 20ml concentration vialsSVAP-BLK-12-040 SuperVapconcentratorblock-12positionwith 40ml concentration vialsSVAP-BLK-12-060 SuperVapconcentratorblock-12positionwith 60ml concentration vialsSVAP-VIA-020M-000 20mLconcentratorvial,packof500SVAP-VIA-040M-000 40mlconcentratorvial,packof500SVAP-VIA-060M-000 60mlconcentratorvial,packof500

SuperVap Concentrator Standalone SuperVap-24/SV 24 Position for 2 & 4ml vials (no block)SVAP-BLK-24-002 SuperVapconcentratorblock-24positionwith 2ml concentration vialsSVAP-BLK-24-004 SuperVapconcentratorblock-24positionwith 4ml concentration vialsSVAP-VIA-002M-000 2mlconcentratorvial,packof100SVAP-VIA-004M-000 4mlconcentratorvial,packof100

44 4844

SuperVap® Solvent Recovery System

The SuperVap Solvent Recovery System is designed to recover solvents from the SuperVap family of Concentrators/Evaporators. It uses no refrigerant. It uses solvent resistant bottlesforcapturingtherecoveredsolventfordisposal.Ithasabuiltinstorageareaforthesolventrecoverybottle.Some of the solvents that it can recover are Acetone, Acetonitrile, Benzene, Ethanol, Ethyl Acetate, Hexane, Methanol, Methylene Chloride, MTBE, Petroleum Ether, and Toluene.

Ordering InformationSVAP - SRS – 110 SuperVap Solvent Recovery System 110VSVAP - SRS – 220 SuperVap Solvent Recovery System 220V

Reduce the laboratory’s solvent vapor emissions aiding in regulatory compliance Allows solvents to be captured for recycling saving on disposal costsReduce exposure to harmful solvent vaporsRequires no refrigerantSmall footprint saving valuable spaceRecovered solvent storage areaTemperature Display

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TotalPrep® Family of Total Sample Prep SolutionsIntegrated Sample Extraction, Cleanup, and Concentration Systems

Imagine performing the total sample preparation process for liquids and solids automatically, in a fraction of the time it takes today. FMS introduces a new family of integrated, economical “TotalSolution”samplepreparationsystemsthatcombinethree sample prep steps into one automated process. Total-Prep systems perform extraction, cleanup, and concentra-tion for eight samples simultaneously in less than two hours, whiledeliveringthehighestrecoveriesandbestresultsfor all target analytes. The systems are programmed and controlled via an easy-to-use touch screen and methods are stored on SD cards. Running a single sample preparation step, such as extraction, sample cleanup or concentration is also an option.

The TotalPrep® S system for solid samplesPLE® Pressurized Liquid Extraction Module PowerPrep® Multi-column Sample Cleanup ModuleSuperVap® Evaporation and Solvent Exchange Module

Simultaneously perform eight sample extractions, cleanups, and concentrations in less than two hours.The TotalPrep systems are integrated, economical samplepreparationsystemsthatcombinethesam-ple extraction, cleanup, and evaporation steps into one automated process. Unattended sample preparation.Load a solid sample into the extraction cell, or car-tridge in the case of liquid samples, install the cleanup columnsonthesystem,pushthe“Run”buttonandwalkaway.TheTotalPrepsystemswillautomaticallyperform the entire sample preparation process unat-tended,invirtuallyonestep.ThefinalfractionisreadyforanalysisbyGC,LC,orGC/LC/MS.

Same day turn around for multiple samples.Becausetheyprocesseightsamplesinparallel−simultaneous extraction, cleanup, and concentration −TotalPrepsystemsareabletoturnaroundupto24samples in a day.

The TotalPrep® L system for solid samplesTurboTrace r parallel solid phase extraction system PowerPrep® Multi-column Sample Cleanup ModuleSuperVap® Evaporation and Solvent Exchange Module

46 5046

TotalPrep Family

Easy sample preparation for POP analysis TotalPrep systems perform complete sample preparation for eightsamplesautomaticallyandunattendedproducingthefinalextract for GC, LC, and GC/LC/MS analysis. They use pre-packeddisposablecleanupcolumnsaswellasready-to-usedisposableextractioncellendcaps.TheintegrateddesignofTotalPrep systems means there is no need transfer samples from one system to another for additional processing. These features allow for “Raw sample in, GC, LC, and GC/LC/MS ready fraction out”, and minimize the need to wash glassware.

Automates EPA SW846 and 40 CFR 136 methodsTotalPrepsystemshavebeenapprovedbytheUSEPAasanautomated alternative to SW- 846 and 40 CFR 136 methods for POPsanalysis.

Reduce solvent and glassware usageByusinginexpensive,pre-packed,disposableclean-up columns,filtrationcartridges,andconcentrationtubesthesesystemsalsousedisposableextractioncellendcaps,greatlyreducingtheamountofcontaminatedpartsthatneedtobewashed.ThegreaterefficiencywithwhichtheTotalPrepsystemsperform extraction and cleanup reduces solvent consumption.

Dramatic savings in time and resourcesTotalPrep systems perform the complete preparation of eight samplesinjustafewhours,insteadofdays.Thiscapabilityresultsintimeandlaborsavings.

Low background automated sample prepTheadvanced,closedloopsystemdesigncombinedwithpre-packed,disposablecolumnsdelivercleanerbackgroundsandeliminate cross contamination.

Wide range of inexpensive extraction cell sizesA wide range of inexpensive stainless steel extraction cell sizes areavailableforTotalPrepsystems.Currentlyavailablesizesinclude 5ml, 10ml, 20ml, 40ml, and 100ml. They are made of either316stainlesssteel,orthespecialacidandalkaliresistantalloystainlesssteel.Withtheirflexibledesignandconstruc-tion, TotalPrep Systems can accommodate the whole range of extraction cell sizes; from the 5ml cell all the way to the 100ml, in the same system.

Wide range of pre-packed, disposable cleanup columnsAwidevarietyofeconomical,pre-packed,disposablecleanupcolumnsareavailableforusewithTotalPrepsystems.Thesecolumnsareconfiguredinavarietyofsizesandpackingmaterialtypes−fromstandardmulti-layeredA-B-Nsilicatocustom made columns.

Disposable Columns used for Dioxins and PCBs, PBDEs analysis:

1. Multi-layered A-B-N silica 2. Alumina 3.Carbon4.Highcapacityacidsilica(optionalusedforfattysamples, this column removes 3-5 grams fat

Disposable or reusable extraction filtration end capsInhigh-throughputlaboratorieswherefastsampleturnaroundisthegoal,disposableTeflonendcapseliminatetheneedtowashandassembleendcaps.Reusablestainlesssteelendcapsmaybeusedwhensavingtimeandlaborisnotthe overriding issue.

Modular and expandableTotalPrepsystemsaremodularandcanbeconfiguredinfromonetosixsampleconfigurations.TheflexibledesignofTotal-Prepsystemsallowslaboratoriestoacquireasinglesampleconfigurationinexpensivelyandthenexpandittotwo,three,four,five,orasixsampleconfigurationassamplethroughputdemandgrows.Laboratorystaffcaneasilyconnectexpansionmodules to the existing system in less than an hour. This design andconstructionmakeTotalPrepsystemseasytoexpand and maintain.

Ideal for method development TotalPrep Systems are the ideal method development tool fortoday’slaboratories.Becausetheyutilizeawiderangeofextraction cell sizes, cleanup columns, and multiple solvent selectionvalvestheyareextremelycapabletoolsforexperi-mentingwithdifferentsamplesizes,solvents,flowrates,clean-uppackingmaterials,extractionpressures,andtemperatures.

Robust and maintainable Themodular,flexibledesignofTotalPrepsystemsvirtuallyeliminatesdowntimeandmakesthemthemosteasytomain-tainsystemsintoday’slaboratories.Eachsystemchanneloperates independently of the other channels, so if one channelmalfunctionstheothersstillwork.Shouldamodulemalfunction,laboratorypersonnelcanreplaceiton-siteandtheexposedconstructionmakespartsaccessibleforeasyre-placement.Thelarge-boreplumbingoftheextractionmodulemakesitvirtuallyclogfree

Ordering InformationTRP/1 Total Rapid Prep System TRP 1 for one SampleTRP/2 Total Rapid Prep System TRP 2 for two SamplesTRP/3 Total Rapid Prep System TRP 3 for three SamplesTRP/4 Total Rapid Prep System TRP 4 for four SamplesTRP/5 TotalRapidPrepSystemTRP5forfiveSamplesTRP/6 Total Rapid Prep System TRP 6 for six Samples

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Fluid Management Systems 580 Pleasant Street, Watertown MA 02427

Tel: 617 393 2396 Fax: 617 393 0194

[email protected]

Total Solution Sample Prep

PLE® Pressurized Liquid Extraction

PowerPrep® Multi-Column Cleanup System

SPE Solid Phase Extraction

TRP® System Total Rapid Prep

TotalPrep® S TotalPrep® L

From Sample to Vial

Extraction • Cleanup • Concentration

from sample to vial · ables the ple to operate virtually leak and clog free. modular construction...

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