hygieneering inc - phase ii environmental soil
TRANSCRIPT
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Phase II Environmental Soil Investigation Report1840 South 54th Avenue in Cicero, Illinois
Cicero, Illinois
Prepared for:J. Sterling Morton High School District 201
Prepared by:Hygieneering, Inc.7575 Plaza Court September 28, 2001Willowbrook, Illinois 60521 Project No. 200 i -3628
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Table of Contents
Executive Summary 1Discussion 2
Background .-.-. 2Methodology 2Results 3
Conclusion 9Appendices 10
Appendices
Appendix A: Soil Boring LocationsAppendix B: Soil Boring LogsAppendix C: Laboratory Analytical Results
Phase II InvestigationSchool District 2012/28/2001-3628
PHASE II ENVIRONMENTAL SOIL INVESTIGATION1840 SOUTH 54TH AVENUE
CICERO, ILLINOISOCTOBER 19,2000
Executive Summary
J. Sterling Morton High School District 201 (School District 201) retained Hygieneering, Inc.(Hygieneering) to perform a Phase II Environmental Soil Investigation of the property located at1840 South 54th Avenue in Cicero, Illinois (the Property). This project was conducted to attemptto determine the presence of contaminated soil potentially caused from the historical use of theProperty.
Hygieneering and its subcontractor, Rock & Soil Drilling Corporation of St. Charles, Illinois,performed the following tasks as a part of this project:
• Advanced 37 soil borings (in three separate phases) to variable depths inside thesouthern portion of the building and outside the building on the Property.
• Conducted continuous sampling on each boring and screened samples for organicvapors in the field with a photo-ionization detector (PID).
• Submitted the one sample from each boring that displayed the highest organicvapor reading for analysis of VOCs (volatile organic compounds), BTEX(benzene, toluene, ethyl benzene, and xylenes), PNAs (polynuclear aromaticcompounds), and RCRA (Resource Conservation and Recovery Act) metals. Theparameters listed were not all analyzed for each sample, rather for selectedparameters from this list based on historical uses of different areas of theProperty and adjoining properties.
• Interpreted the results and compared the contaminant concentration levels to themost stringent cleanup objectives listed in the Tiered Approach to CorrectiveAction Objectives (TACO): IL Adm. Code Part 742.
Hygieneering did not advance soil borings in the central and northern portions of the building dueto access issues and the presence of active operations being performed by Economail.
The results of our investigation indicate the presence of high concentrations of variouschlorinated solvents under and adjacent to the southwestern portion of the building on theProperty. Trichloroethylene, perchloroethylene, cis-l,2-dichloroethylene, and vinyl chloridewere the main contaminants of concern that were present in soil and groundwater above the moststringent cleanup objectives listed in TACO. The affected area appeared to be approximately 100feet by 150 feet, with contamination detected at depths of up to 30 feet below the ground surface(bgs).
1840 South 54Ih Ave Soil InvestigationSchool District 201Project Number 2001-3628
Discussion
Background
Hygieneering conducted a Phase I Environmental Site Assessment of the Property anddetermined the Property and the adjoining properties have been used for industrial purposes sincethe early 1900s. These uses include the use of the Property as for manufacturing electricalconnectors and components.
Hygieneering observed the presence of three underground storage tanks under the southwesternportion of the building during our Phase I Environmental Site Assessment. In addition, SanbornFire Insurance Maps indicated that a plating room was located on the southwest corner of thebuilding.
Hygieneering performed a Phase II Environmental Soil Investigation in an attempt to determinethe presence of VOCs, BTEX, PNAs, and RCRA metals, on different areas of the Property.VOCs were analyzed for in areas where a broad range of possible contaminants was suspected,including solvents, degreasers, and fuels. BTEX and PNAs were analyzed for in areas that weremost likely to be locations of fuel oil USTs (near the former boiler room). Hygieneeringcollected samples that were analyzed for metals near the plating area on the Property. A drawingshowing the sample locations is included in Appendix A.
Methodology
Hygieneering and its subcontractor, Rock & Soil Drilling, advanced thirty-seven soil borings witha Bobcat mounted Geoprobe rig on the Property to a depths of twelve feet to thirty feet on May25, 31, June 3, July 9 and 13, 2001. In addition, six monitoring wells were installed, three insideand three outside the building during this project.
Hygieneering performed continuous sampling on each boring using a PID to screen for organicvapors. Samples were collected at two-foot intervals and the screening sample with the highestPID reading was submitted to the laboratory. In addition, Hygieneering collected a secondsample from selected borings inside the building in the main contaminated area in an attempt todefine the vertical extent of contamination. Copies of the soil boring logs are included inAppendix B. \ *, > f?
•/ y f /•\ % •< .*Boring locations B4, B18, B21, B26, and B37 were converted into monitoring wells. B4 was atemporary well that was removed on the same day it was installed.
Hygieneering collected VOC samples using the SW-846 method with field preservation included.Samples were stored in a cooler on ice until they reached the laboratory at the end of the day.
Great Lakes Analytical analyzed the VOC, BTEX, and PNA samples using the EPA Method5035/8260B, and RCRA metals samples by EPA 6000/7000 Series Methods. Copies of theanalytical reports are included in Appendix C.
1840 South 54Ih Ave Soil InvestigationSchool District 201Project Number 2001-3628
Results
Hygieneering interpreted the results and compared the contaminant concentrations to those listedin Illinois Administrative Code Part 742 (TACO). Hygieneering used the most stringent cleanupobjectives: Tier 1 Soil Remediation Objectives for Residential Properties, Soil Component of theClass I Groundwater Ingestion Exposure Route, except for RCRA metals. Hygieneeringattempted to compare these results to pH specific cleanup objectives, however, the pH of the soilwas greater than 8.0, which prevents this comparison from being made. Therefore, Hygieneeringcompared these levels to the concentrations of inorganic chemicals in background soils listed inAppendix A Table G of TACO.
The following table summarizes the results of the VOC, BTEX, RCRA metals (whereapplicable), and PNA (where applicable) laboratory analysis performed on the soil samplescollected.
BoringNo.
Bl
B4
B5
B7BIO
Bl l
Depth
6'
7'
8'
6'9'
ir
Contaminant
C ^!
Benzene 2 i.1 , 1 -Dichloroethane ' 1 ,2-Dichloroethane , °fi1,1-DCE ^Cis 1,2-DCE '-^Trans- 1,2-DCE 3" Ethyl benzene :; ':•Methylene ChlorideTolueneVinyl Chloride .' /Xylenes r 1 0No VOCs detectedPNAs:FluoranthenePhenanthrene1,1 Dichloroethane1,2-Dichloroethane1,1-DCEcis- 1,2-DCE1,1,1-TrichloroethaneTCE ' i-Vinyl ChlorideNo VOCs detectedCarbon Disulfide1,2-Dichlorore thanecis- 1,2-DCEPERCTCEVinyl ChlorideLeadBenzene(Only BTEX and PNAsanalyzed)
Concentration(mg/kg)
0.04271.1100.008250.0190.9020.2560.01510.0376130 ^0.8610.0441NA
1.0401.600230.07250.04625.5300.2478.1600.261NA0.008580.2050.01120.01710.005021.0600.0271 mg/L0.0406
Soil Comp ofGW Ingestion
Objective0.03230.020.060.40.7130.02120.01150NA
4,300NA230.020.060.420.060.01NA320.020.40.060.060.010.0075 mg/L0.03
Inhalation /Ingestion*Objective
0.813000.47007801600400136500.03410
3100NA13000.4700780120050.03NA7200.47801150.03400 mg/kg0.8
-
1840 South 54Ih Ave Soil InvestigationSchool District 201Project Number 2001-3628
BoringNo.
B12
B13
B14
B15
B16
B17
B18B18
B19
B19
B20
B20B21
B22
B22
B23
Depth
10'
11'
3'
10'
2'
9'
8'32'
5'
9'
4'
14'15'
3'
15'
9'
Contaminant
FluoranthenePhenanthrenePyrene(Only BTEX and PNAsanalyzed)PERC -2SrTCE ~-^LeadCis- 1,2-DCETCE ^LeadCis- 1,2-DCE ''-&TCECis- 1,2-DCETCELeadBenzene(Only BTEX and PNAsanalyzed)AcetoneAcetoneMethylene ChlorideAcetone2-ButanoneMethylene ChlorideChloroethane1,1 -Dichloroethanecis- 1,2-DCEVinyl ChlorideAcetoneChloroethaneAnthracenePhenanthreneNo VOCs detectedCis- 1,2-DCEMethylene ChloridePERCTCEVinyl ChlorideCis- 1,2-DCETCEVinyl ChlorideCis- 1,2-DCEMethylene ChlorideTCECis- 1,2-DCETrans- 1,2-DCEMethylene ChlorideTCEVinyl Chloride
Concentration(mg/kg)
0.3530.4200.221
1020 ^42200.020 mg/L34.674.80.0104 mg/L43.924.834.33.690.0385 mg/L0.0292
0.03420.03210.005230.1030.01990.005150.01220.007150.005680.005410.04340.01070.1640.205NA3.6500.8450.9715911.3300.4114.7500.5110.009450.005980.14921.300.3970.4310.3422.530
Soil Comp ofGW Ingestion
Objective4,300No objective4,200
0.060.060.0075 mg/L0.40.060.0075 mg/L0.40.060.40.060.0075 mg/L0.03
16160.0216No objective0.02No objective230.40.0116No objective12,000No objectiveNA0.40.020.060.060.010.40.060.010.40.020.060.40.70.020.060.01
Inhalation /Ingestion*Objective
3100NA2300
115400 mg/kg7805400 mg/kg78057805400 mg/kg0.8
78007800137800NA13NA13007800.037800NA23,000NANA780131150.0378050.0378013578016001350.03
1840 South 54'h Ave Soil InvestigationSchool District 201Project Number 2001-3628
BoringNo.
B24
B25
B26
B27B28B28B29
B30
B30
B31
B32
B32
B34
B34
B35
B35
Depth
12'
7'
7'
13'4'13'10'
11'
25'
4'
3'
15'
5'
15'
6'
15'
Contaminant
Cis- 1,2-DCETrans- 1,2-DCEMethylene ChlorideTCEVinyl ChlorideCis- 1,2-DCEMethylene ChlorideTCEVinyl Chloride1,1 -Dichloroethane1,1-DCEcis- 1,2-DCEtrans- 1,2-DCEMethylene ChlorideTCEVinyl ChlorideTfi^*'TCENo VOCs detectedCis- 1,2-DCETCECis- 1,2-DCEMethylene ChloridePERCTCEVinyl ChlorideMethylene ChlorideTCEAcetoneMethylene ChlorideTCEAcetone15 PNAs detected, noneabove cleanup objectives.(PNA analysis only)AcetoneMethylene ChlorideAcetone2-Butanone13 PNAs detected, noneabove cleanup objectives.(PNA analysis only)AcetoneMethylene ChlorideNo PNAs detectedAcetoneMethylene ChlorideAcetoneMethylene Chloride
Concentration(mg/kg)
5.5900.4380.8391560.000.4600.0370.006320.0840.1460.02330.0082711.800.5240.01150.006652.2300.007080.0115NA0.005990.036721.900.9384.8301160.001.2400.8359.9502.5200.8311.2100.0891See lab report
0.05270.005270.1020.0128See lab report
0.0790.00560NA0.07060.00560.05240.00525
Soil Comp ofGW Ingestion
Objective0.40.70.020.060.010.40.020.060.01230.060.40.70.020.060.010.060.06NA0.40.060.40.020.060.060.010.020.06160.020.0616NA
160.0216No objectiveNA
160.02NA160.02160.02
Inhalation/Ingestion*
>'• Objective78016001350.037801350.03130070078016001350.0355NA7805780131150.0313578001357800NA
7800137800NANA
780013NA780013780013
1840 South 54th Ave Soil InvestigationSchool District 201Project Number 2001-3628
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BoringNo.
B36
B36
B37
B37
Depth
3'
15'
6'
19'
Contaminant
Acetone2-ButanoneMethylene ChlorideAcetoneMethylene ChlorideChloroform1 , 1 -Dichloroethane1,1-DCEcis- 1,2-DCEtrans- 1,2-DCEMethylene ChloridePERC1,1,1 -TrichloroethaneTCEVinyl ChlorideAcetoneChloroformCis- 1,2-DCETrans- 1,2-DCEMethylene chlorideTCEVinyl Chloride
Concentration(mg/kg)
0.1720.01730.007080.06020.005170.8800.2080.06482.3300.2030.006840.01720.01118.2300.5230.08260.03070.1980.009060.019771.1000.00602
Soil Comp ofGW Ingestion
Objective16No objective0.02160.020.6230.060.40.70.020.0620.060.01160.60.40.70.020.060.01
Inhalation /Jngestioii*
"" Objective7800NA137800130.3130070078016001311120050.0378000.378016001350.03
Bold value indicates an exceedance of the TACO Tier 1 Soil Component of the Groundwater Ingestions ExposureRoute Remediation Objective1,1-DCE: 1,1-dichloroethylene *More stringent value listedCis-1,2-DCE: cis-1,2-dichloroethyleneTrans-1,2-DCE trans-1,2-dichloroethylenePERC: TetrachloroethyleneTCE: Trichloroethylene
These results indicate the presence of chlorinated solvent impacted soil under the southwesternportion of the building and the area immediately adjacent to the southwest corner of the building.Several samples contained concentrations of PERC, TCE, cis-1,2-DCE, and vinyl chloride thatexceeded the soil component of the groundwater ingestion exposure route values (most stringent)and the ingestion and inhalation exposure route values listed in the TACO soil remediationobjectives for residential properties. In addition, the concentrations for lead in all of the boringsanalyzed for TCLP RCRA metals exceeded the most stringent cleanup objective.
The following table summarizes laboratory analysis of water samples collected during thisinvestigation.
Monitoring Well No.
Temp- 1
Boring Location
B4
Contaminant
No VOCs detectedBenzo(a)pyreneBenzo(b)fluorantheneBenzo(k)fluorantheneChryseneFluoranthenelndeno( 1 ,2,3-cd)pyrenePhenanthrene
Concentration(rag/L)
0.003250.004160.001130.01000.04810.002010.0618 J
J ; CleanupObjective
NA0.00020.000180.000170.00150.280.00043No objective
1840 South 54th Ave Soil InvestigationSchool District 201Project Number 2001-3628
Monitoring Well No.
MW1MW2
MW3
Boring Location
B18B14
B21
Contaminant
AcetoneBenzeneChloroethane1,1 -Dichloroethane1 ,2-Dichloroethane1,1-DCEcis- 1,2-DCEtrans- 1,2-DCETCEVinyl Chloride1,1 -Dichloroethanecis- 1,2-DCEtrans- 1,2-DCETCEVinyl Chloride
Concentration(mg/L)
0.05460.002590.02962.5800.04240.0853242.0002.58047.10014.0000.63232.2000.954937.0006.560
CleanupObjective
0.70.005No objective0.70.0050.0070.070.10.0050.0020.70.070.10.0050.002
Bold value indicates an exceedance of the TACO Tier 1 Groundwater Remediation Objective
Tier 1 groundwater remediation objectives were exceeded for PNAs in temporary well 1, whichwas located in the parking lot approximately 50 feet south of the building. The presence of PNAssuggest the contamination is from heating oil, that may have been generated from the formerStrom Steel Ball Plant that was formerly located on the southern portion of the Property.
Tier 1 groundwater remediation objectives were exceeded for several chlorinated solvents inwells MW2 and MW3, which are located inside the southwestern portion of the building.
Future Land Use ConsiderationsIllinois has set up a voluntary cleanup program known as the Site Remediation Program, or SRP.The program allows the use of a risk-based approach to remediation (Tiered Approach toCorrective Action Objectives, or TACO), including creating site-specific cleanup objectives thatare based on the risk of individuals ingesting or inhaling contaminants. The remedial objectivesreferred to in the table above represent the most stringent objectives listed in TACO. Thosevalues may be changed through the use of risk-based equations or through the elimination of theexposure route (soil component of the groundwater ingestion exposure route). This program alsoallows property owners to leave contamination in place if they can demonstrate that all of therisks and potential exposure routes have been addressed. In order for contamination to be left inplace, the Illinois Environmental Protection Agency will sometimes place some conditions orrequirements on properties to allow this. These conditions may include deed restrictions,groundwater use ordinances, and installation of engineered barriers.
This investigation has confirmed the presence of chlorinated solvent impacted soil under andaround the southwest portion of the building. The contamination extends from the near surfacesoil to depths of at least 30 feet below the ground surface. The nature of the contaminationrequires that excavated soil be handled as hazardous waste. Due to the high cost of hazardouswaste disposal, the best future land use options for this site would be ones that involve the leastamount of excavation. However, the presence of the contaminants in the soil would require theinstallation of an engineered barrier to prevent exposure to potential future occupants of theproperty. An example of an engineered barrier is an asphalt parking lot.
1840 South 54Ih Ave Soil InvestigationSchool District 201Project Number 2001-3628
Hygieneering believes that through the use of the risk-based approach outlined in TACO, most, ifnot all of the contamination on the property may be left in place. The only material that wouldhave to be removed and disposed of as hazardous waste would be those materials excavated tofacilitate construction activities. Therefore, Hygieneering would recommend the installation ofan asphalt parking lot over the contaminated area in a manner that would only require theminimum amount of soil to be excavated from the site.
1840 South 54th Ave Soil InvestigationSchool District 201Project Number 2001-3628
Conclusion
The results of this Phase II Environmental Soil Investigation indicate the presence of significantchlorinated solvent contamination under and around the southwest portion of the building on theproperty. The contamination has impacted both soil and groundwater at concentrations thatexceed the most stringent cleanup objectives listed in TACO.
Recommendations
J. Sterling Morton High School District 201 intends on using this parcel as part of a futurecampus area. Hygieneering recommends the submission of this property into the Illinois SiteRemediation Program (SRP) so that site-specific cleanup objectives can be developed for theproperty and approved by the IEPA. Hygieneering also recommends that the contaminated areabe covered with an engineered barrier, specifically an asphalt parking lot, in order to minimizethe costs associated with disposing of soil that will be classified as hazardous waste from theproperty.
We appreciate the opportunity to assist you on this important project. If you have any questionsor require additional information, please do not hesitate to contact us.
Respectfully submitted,Hygieneering, Inc.
Garrick J. Milkeris, CHMMEnvironmental Assessments Manager
ohn Feller, CIH, CSPVice President
Progress/Gary M/Morton PII 00-2782/Morton PH.doc
1840 South 54th Ave Soil InvestigationSchool District 201Project Number 2001-3628
II* Appendices
• APPendi*A: B°ri"g Location Drawings
Appendix B: Soil Boring Logs
| APpendix c: Laboratoly Analytica]
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1840 South 54th Ave Soil Investigation J OSchool District 201Project Number 2001-3628
ii
Appendix A:
Boring Location Drawings
B954th Avenue
B8
eB7
eB6 I
~e ~[HIP
e82
n a
LD
eB3
eB5
B4 CD
e
< RAILROAD EASEMENT >
SITE PLAN
(NOT DRAWN TO SCALE)
Hygieneering, Inc.7575 Plaza Court
Willowbrook, IL 60521
CLIENT:
J. Sterling MortonHigh School District#201
PROJECT:
First Round OutdoorBorings1840 South 54th AvenueCicero, Illinois
PROJECT NO.:
2001-3628-E
Appendix B:
Soil Boring Logs
1 i>^1 l
\ Project Name: EconoMail
R^> Project Number: 2001-3495
f^P Project Location: 1834 South 54th Avenue
Samples Taken By: CD
^^ Ambient Air Tem p: 60F
a. HYGIENEERING. INC. start/stop Time:8:0° am - 4:0°Pm
1
1
1
1
4I1111
Boring Number: 3495-B1Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location: GPS Coord.
Date: 05/29/01
c-3O>_c
f "5.
«• iQ W
0 -j
-1 -
-2-
-3-
-4-
-5-**-o
-7-
-8-
-9-
-10-
-11-
-12-
-13-
-14-
If?
__ •>
— ' '
0
1E3z «« a"5- »E o
c(0o
CO £
Q 2.^ S Lithology Data Q. &
CONCRETE:M \
CLAY: Grey, Soft, Tracegravel.Noodor/discolorat
M
A CLAY: Grey/Tan, Hard,Trace gravel, Noodor/discoloration
W
W
J^^^^ l/ ^^^^^H — -ion ^^^1 108 ~ f ~2
^^^^^H .4
^•^ - -5
^^^^Hs98 .. ^
^H ^--*^^^^^1 — - -9
^ 1 --1°^^^^^H — -11H^ ^ ^HH ' . _
95---13
---14
•fl T-JO
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".
§ Boring was backfilled with bentonite chips. Photo-kmizatton Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated
1
1
1
1
1
1
_ ^\ Project Name: EconoMail
g K^^^C l Project Number: 2001-3495
^y^ Project Location: 1834 South
t Samples Taken By: CD
• ^ ^^ Ambient Air Temp: 70F
Boring Number: 3495-BIDrilling Company: Rock & Soil
54th AvenueDrilling Method: Geoprobe
Type of Sampling: Soil
Borinq Location: GPS Coord.^ HYGIENEERING, INC. start/St°P Time:8:00 am - 4:00pm• Date: 05/29/01
I S 1O Er*J
? z «
I = 0 D£ 0 - 0 . «\ 1 E o2 t5 5 2
1 00 -. ,: cu-1 - - W ^0
|-2-LS" ~ sAj? •^~r8f A
I "4 -- : CL/"* ~ r fe> w 9rai
gt ^ r" . * "
1 -7 - - ~ j£*F f
-8 U-
-9 -^
1--*••* ••
-^r-11-- ;
^_ HO—• -12: . w• -13:r
-14
1 .-"-1.
10o
CO ^Q a
Lithology Data Q. Q
kY: Grey, Gravel, Soft, No | ^ ^ lr/discoloration ^^^^^^1 -1
1:: ;Of: Grey, Hard, Trace ^^^^H/el.Noodor/discoloration ^^^^^^1 -5
^^^^Ho.o IT"6
^H ^-'i^^^^H ---9^^H -~-™^ • ^H — -11^^^^^^^^H ~~ . _
o.o - -12
-13
---14
•IT-JO
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".
1Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 1 0.8 eV lamp.Moisture symbols: D= dry, D/M=slightty moist, M=moist. M/W=very moist, W=wet, S=saturated.
1
1
1
1
1
1
IIIIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: EconoMail
Project Number: 2001-3495
Project Location: 1834 South 54th Avenue
Samples Taken By: CD
Ambient Air Temp: 70F
Start/Stop Time:8:00 am - 4:00pm
Date: 05/29/01
Boring Number: 3495-B3Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location: GPS Coord.
0) «
o cMg> z g i
j= 's. ~ -2 co £f c E E 1 O S .Q w 5 2 Lithology Data (L g
—
-1 -
-2-
-3-
-4-
-5-
-6-
-7-
-8-n-y
-10-
-11-
-12-
-13-
-14-
nftipH
tfIPR
IIv'tT:
A
W
W
W
w
NO RECOVERY:
SAND AND CLAY: Yellowsand, Well sorted/graded,Tan clay, Trace gravel,
/ / / / /
/////_/^ ,/1.8
\ Loose.Noodor/discoloration/ ^^^^B\ /muBiCLAY AND SILT: Grey/Tan, ^^^^B °'°Firm, Trace gravel, No HBI Bl
. odor/discoloration >r ^^^^^^\ /
— v
--2
--3
--4
--5
- -6
--7
- -8
o-y
- -10
— 11— -12
--13
--14
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled O'-IO' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=sligritly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number: 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 05/24/2001
i I
Boring Number: B-4Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
I *CO CO
oLithology Data
oCOQEL
o-1-2-3-4-5-6-7-8-9-10---11
-1;
-i-18-+-
-20---2-2-23-+--2-25+--261-
-28—
-30-3-3:-33-+--3*-35
B4-7
D
D
M
M
W
W
W
GRAVEL:Asphaltoverlayingfill Gravel
CLAY AND SILT: Grey SiltyClay. Soft. Very strong odor
CLAY AND SAND: Very littlerecovery. Very soft Gry Claywith Gravel. Strong petrolodor
CLAY AND SAND: Very softGrey Clay with trace graveland sand. Visible oil andsheen on exposed surface.Very strong petrol odor
CLAY AND SILT: Tan andGrey softSilty Clay with tracesand and gravel. No odor
CLAY AND SAND: Very softGrey Clay with trace sandand gravel. No odor. Wellplaced at 13'depth. EOB
0-1-2-3-4-5•6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28-29-30
--31--32--33--34--35
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-tonization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightty moist, M=moist, M/W=very moist, W=wet, S=saturated.
I VW^i _ HYGIENEE
1
1
1
1
1
1
1
1
1
\ ^ Project Name: EconoMail BoHng Number 3495-B(mr> Project Number 2001-3495 Drj||jng ^ Roc(< &
p W Project Location: 1 834 South 54th Avenue H T M H- r
^ Samples Taken By: CD T , . . . . , . .^ J Type of Sampling: Soil• Ambient Air Temp: 70F
^ Boring Location: GPS Coord.:RING INC Start/Stop Time:8:00 am -4:00pm
Date: 05/29/01
0)
o
t ECOCO
0 -
-1 -
-2-
-3-
.-5-
-6-
-7-
-9-
-10-
-11-
-12-
-13-
-14-
1C
- Iti >«
%— " -i— -
_ -
0
i
! i *E "5 Q
« «CO
W
W
A
W
W
z Lithology Data Q.
CLAY: Tan/Black, Trace ^^^^Hgravel, Soft, Loose, No ^^^^^^1odor/discoloration ^^^^^^1
^^^^^^^^HCLAY: Grey/Tan, Trace ^^^^^Hgravel, Firm, No ^^^^H 28 8
odor/discoloration ^^^^^^1
I334^^^^^^^BmpuppnCLAY AND SILT: Grey, Soft, ||tj|im|No odor/discoloration ^^^^^^B
•fl1'5^B^ HE IBfl1 5I
feQ
---1
---2
---3A-4
---5
---6
---7
-o
---9*e\
-\\j
---11._
---13
A f— — -15
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".
•
Boring was backfilled with bentonite chips. Photcnonizatkxi Detector (P.I.O.) scan performed using a Mini Rae equipped with a 1 0.8 eV lamp.Moisture symbols: D= dry, D/M=sligritly moist, M=moist, M/W=very moist, W=wet, S=saturated.
1
1
1
1
1
1
IIIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: EconoMail
Project Number: 2001-3495
Project Location: 1834 South 54th Avenue
Samples Taken By: CD
Ambient Air Temp: 70F
Start/Stop Time:8:00 am - 4:00pm
Date: 05/29/01
Boring Number: 3495-B6Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location: GPS Coord.
I ?f i t0) TO «Q co co i Lithology Data
ucoQQ.
u —
-1 --2-
-3-J
-5-
-6-
-7-
-8-
-9-
-10-
-11-
1*>£T
-13-
•1C
„
~"
' '
1 1_
»
„
_
J-
A
D
D
M
M
CLAY: Grey, Gravel, Firm,No odor/discoloration
CLAY: Grey, Tracegravel/Silt, Noodor/discoloration
0
-1-2
-3
-4
-5
-6
-7
-8
-9
-10
-11
-12
-13
-14
-15
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: EconoMail
Project Number: 2001-3495
Project Location: 1834 South 54th Avenue
Samples Taken By: CD
Ambient Air Temp: 70F
Start/Stop Time:8:00 am - 4:00pm
Date: 05/29/01
Boring Number: 3495-B7Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location: GPS Coord.
Ia.9co
3
»a.aco
<aoco
i Lithology Data
0
-1-2
-3
•4
-5
-6
-7
-8
-9
-10-+-
-11-
-12
-1*
-14-
M
M
CLAY: Grey, Trace gravel,Some Silt, Soft, Noodor/discoloration
CLAY: Grey, Some Si It, Firm,No odor/discoloration
NO RECOVERY:
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-kmization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.
Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number: 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 05/31/2001
Boring Number: B-10Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
w
I
Ia«jco
JS3
0)a.a
CO
Iio
Lithology Data
(0uCOoQ.
B-10
D
D
W
W
W
CEMENT: Concrete floor
ASPHALT:ThinAsphattlayer
CLAY: Stiff Grey Clay. Noodor
CLAY: Very soft Grey Clay.Mild petrol odor
BLANK: Refusal at 10'depth.Thick concrete layer. EOB
0-1-2-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28-29-30-31-32-33-34-35
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled O'-IO1 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 06/04/2001
Boring Number: B-11Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
aa
CO
«a.«to
(0(JCO
Lithology Data
0-1-2-3-4-5-6-7-8-9-11-1-1;
-1-1-1-1-1-2-2-2
-3-3-3
-[-_
—
—_
--o1
•H21
31
A4
S1
61
•h-
81
91
JO1
5-H521
53-1
J41
IS1
l^IT2
IB1
291
301
3-H
32-
33-
34-?c
B-11
D
M
M
W
W
W
W
CEMENT: Concrete and\ wood floor /
CLAY: Very soft Grey Claywith trace gravel. No odor.High plasticity
CLAY: Stiff Grey Clay. Noodor. High plasticity. EOB
-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28-29-30-31-32-33-34-35
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number: 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 06/04/2001
o 5c £
* I
| I |
« I 2
Boring Number: B-12Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
Lithology Data
3cooQ.
-10--
-26--
-33--
B-12
D
D
D
D
D
W
W
CEMENT: Concrete andwood floor
CLAY: Soft Tan Clay. Slightchemical odor. Highplasticity
CLAY: Black-stained Claywith trace silt. Very Soft.Slight chemical odor. Highplasticity
CLAY: Very soft Tan andBlack Clay. No odor. Highplasticity
CLAY: Very soft Grey Claywith gravel. No odor
CLAY: Very stiff Grey Clay.No odor. EOB
0-1-2-3-4-5-6-7-8
-9-10-11-12-13-14-15-16-17-18-19-20-21-22
-f--23
-24-25-26-27-28-29-30-31-32-33-34-35
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled (M O1 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated
.HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number: 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 06/04/2001
Boring Number: B-13Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
I
I
I
I
I
I
I
IIIIIIII
I *I I£1"o
co co Lithology Data
tooCOgQ.
B-13
CEMENT: Concrete andwood floor
BLANK: No Recovery
CLAY AND SILT: Very softTan/Grey Silty Clay withtrace gravel. Some blackdiscoloration. Strongchemical odor. Highplasticity
CLAY: Very soft Grey Clay.Very strong chemical odor.Very high plasticity. EOB /
3500>10,000
435
0-1-2-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28-29-30-31-32-33-34-35
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled CMO1 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=sligntly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number: 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 06/04/2001
Boring Number: B-14Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
Z i!•3 1f \ 1 8
£ o. 1 « w £$ E E | Q "S.Q to to s Lithology Data a. £
O ft
-1 --2--3--4--5-J-b --7--8--9 J
-1O1
-1-H-121
-131
-14--151
-16^•IT
-181
-19--201
-21-22^-23^-241
-251
-26-1
-27-1
-2&1
-29^-301
-3-H-321
-331
-34^-tlV-
-
B-14
W-14(water)
D
D
D
D
D
D
D
W
W
k CEMENT: Concrete floor ,\ /
CLAY: Very soft black-i stained Clay. StrongI chemical odor. High J\ plasticity j
I CLAY AND SILT: Soft Black II Silty Clay. Strong chemical II odor. High plasticity I
CLAY AND SILT: Soft jI Tan/Grey Silty Clay with |I trace gravel. No odor. Low i\ plasticity |
CLAY: Soft Grey Clay. Noodor. High plasticity. Wellplaced at 17'depth.Groundwaterencountered at
\ 13' depth. EOB /
IQQQCQQQEi
^^^H^^^H
0
>400>400
35
>100
>150
20
20
10
u
--1--2--3L-4~--5- -6--7
^-8— --10I- -11L-12L-13--14--15--16
r-174 ft-TO
--19--20--21
oo
--23^ -24--25--26--27--28--29^--30
O-f-0 1
--32L -33- -34
•JC
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".
Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 06/04/2001
Boring Number: B-15Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
Lithology Data
§COaE
B-15
W
CEMENT: Concrete andwood floor
BLANK: No Recovery
CLAY AND SILT: Soft BlackSilty Clay. Slight chemicalodor. High plasticity
CLAY: Soft Tan/G<ey Claywith trace silt and gravel.Mild chemical odor
CLAY AND SILT: Stiff BrownSilty Clay with trace gravel.No odor
CLAY: Grey Clay. Slightpetrol odor. High plasticity.EOB
0-1-2
• -3-4•6-6-7-8•9-10-11-12-13-14-15-16-17-18-19-20-21-22
-f--23-24-25-26-27-28-29-30-31-32-33-34-35
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightty moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIIIIIII1IIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number: 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 06/04/2001
Boring Number: B-16Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
o
f,o> a
I f t<B (8 mQ CO (0
oLithology Data
oCOoQ.
0-1-2-3-4-5-6-7-8-9-1(-1'-1:-1:-1.-1!-11-r-11-1!
-21-2
-2-2-2-2-2-2-3-3-3-3
O1
21
*-51
fr
7-1
tV91
O1
I1
2^
s1
51
&1
7-8^91
0^1-2-3-(4->K
B-16
D
D
D
D
W
W
W
CEMENT: Concrete and jwood floor n
CLAY: Stiff Grey Clay withtrace gravel. Strong Ichemical odor /I
CLAY AND SILT: Black Silty IClay. Slight chemical odor. /High plasticity /
CLAY: Very Soft Grey Clay. INo odor. High plasticity /]
CLAY AND SILT: Stiff GreyClay. No odor. High ,plasticity. EOB /
0-1-2-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28-29-30-31-32-33-34-35
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-1ff with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.6 eV lamp.Moisture symbols: D= dry, D/M=sligrrtly moist, M=moist, M/W=very moist, W=wet, S=saturated.
.HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number: 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time: 7am-3:30pm
Date: 06/04/2001
Boring Number: B-17Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
«J5
I Eco co
•8"5
Lithology Data
sCOaQ.
0-1-2-3-4-5-6-7-8-9-11-1-1;-1:-1--11-11-r-11-1!-21-2
-3-3:-3-3-35
—
—
—
——n <
•H2^
41
5-j6--h-tV91
O1
-K2^
31
41
51
6-1
IV
&1
to1
CH\2^\^
M--»K
' *Xt
--,
^ .
B-17
D
M
M
W
W
Ww
CEMENT: Concrete and\ wood floor /
CLAY: Soft Brown Clay withtrace silt and gravel. No
.odor. High plasticity
CLAY: Soft Brown Clay withtrace silt and gravel. Strongpetrol odor odor. High
^plasticity i
CLAY: Soft Grey Clay. No\odor. High plasticity /
CLAY AND SILT: Stiff GreyClay. No odor, medium
\ plasticity. EOB /
0-1-2-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28-29-30-31-32-33-34-35
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-101 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIiIiiiiIiiiiIIii
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number: 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time: 7am-3:30pm
Date: 07/09/2001
Boring Number: B-18Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
IIfl) «O CO
*
I
•5Lithology Data
oCOQa
o —.1 _~ 1
-2--3-^-4 —e _•o
-6 —-7--8-^
4 A_-10--11—11
10J—
-154ft—-10
-17-
«A-20-
oo
-23^-241
-25--26^-27-1
-28--29--30--31--32--33--34—1C-
'
B18-8
B18-32
D
D
D
D
W
W
W
W
W
CLAY: Black silty Clay.Petroleum odor
CLAY: Green/Brown Claywith interbedded gravel.Petrol odor
,
CLAY: Brown Clay withinterbedded gravel. No odor
CLAY: Soft Grey Clay withtrace gravel. No odor
CLAY: Hard Grey Clay withtrace gravel. No odor. Wellplaced at 28* depth. EOB
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIII1IIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 07/09/2001
Boring Number: B-19Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
a.E
a.E
S%o
Lithology Data
8COQ0.
-10--
-13--
-23--
-26--
B19-5
B19-9
BLANK: No Recovery
CLAY AND SILT: Brown andGrey Silty Soft Clay. Blackdiscoloration. Visible oil onexposed soil. Very strongpetrol odor
CLAY AND SILT: Brown andGrey Silty Soft Clay. Blackdiscoloration. Slight petrolodor
CLAY: Very soft Grey Claywith Brown Silt and tracegravel. No odor
CLAY: Soft Grey Clay withBrown Sift and trace gravel.No odor
CLAY: Stiff Grey Silty Claywith trace gravel. No odor
CLAY: Soft Grey Clay withtrace gravel. No odor. EOB
0-1-2-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28-29-30-31-32-33-34-35
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".
Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
III1IIIIIIiiIIilIii
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number. 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time: 7am-3:30pm
Date: 07/09/2001
Boring Number: B-20Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
J!
«a
oN
I I
i i
fii"6
Lithology Data
§COQE
o-1-2-3-4-5-6-7-8
-1
-1;-1:-1.-1!-11-1:-11
-3-3;-3:-3-35
H
3-
frj
T2
(
Ih12^31
^
tW7^8^91
O1
•H2-3-1
4-1
K-
1
^J "*"
it,
TS&
~
B20-4
B20-14
D
D
M
M
M
M
M
M
CEMENT: Concrete surface/
CLAY AND SAND: Black iGravelly Clay. Strong petrol /odor /
BLANK: No Recovery f
CLAY AND SILT: Soft Brownand GreySilty Clay with tracegravel. Black discoloration. Jvisible oil on exposed |surfaces. Very strong petrolodor
BLANK: No Recovery
CLAY AND SILT: Brown SiltyClay. Soft. No odor
CLAY: Stiff Grey. Clay. No 1odor. EOB 1
•s.vo
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled a-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonfte chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
I
I
I
I
I
I
I
I
t
I
I
I
I
I
I
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number. 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 07/10/2001
Boring Number: B-21Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
III
I
s ! tCO CO Lithology Data
§COQQ.
CEMENT: Concrete andwood floor
CLAY AND SILT: Black SiltyClay. Strong organic odor
CLAY AND SILT: Brown andGrey Silty Clay. Soft. Strongchemical odor
BLANK: No Recovery
CLAY: Brown Silty Clay.Soft. Strong chemical odor
BLANK: No Recovery
>10,000
>400
>10,000
>10,000
BLANK: Wet sludge. >80%liquid. Very strong chemicalodor
CLAY: Stiff Grey Clay.Strong chemical odor. Wellplaced at 21'depth. EOB
>10,000>10,000
0
-1
-2-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28-29-30-31-32-33-34-35
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled ff-101 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number: 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 07/10/2001
Boring Number: B-22Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
I *N I c^ bJ? Z « (0•S 0) 3 AJ
1 I * I Q |Q 5 co s Lrthology Data a. £
0 * »
-
-3--4-
-5--6-7-^-8--9--10
-12—-13^-14^
•IP-TO
-17-18-19--201
1«i_-21--22^-231
-241
-251
-26^-27^-2&1
-291
-301
-3-H-32^-331
-34^•**-
B22-3
B22-15
D
D
W
CEMENT: Concrete and S88888888Iwood floor 1888888883
^ nHBHEila 150CLAY AND SILT: Black Silty ^^^^9 >150
, Clay. Soft. Strong chemical ^^^^^^^9\odor IjBHI
CLAY AND SILT: Brown and BKBP >30°i Grey Silty Clay. Soft. Strong iBBBB|\ chemical odor / ^^^ l >200
\ ' ^^^^^MCLAY AND SAND: Very soft BBBEw Brown Sircy/Sandy Clay with ^^^^H
\ trace gravel. Very strong / ^^^^H|W I \chemical odor /^^^ l80
w I CLAY: Stiff Grey Clay with ^^^^H1 tracegravel. Slightchemical I ^ ^H1 odor . HHHHM
W 11 «^ 11| CLAY: Watery Clay. No odor |
| CLAY: Stiff Grey Clay. No ||odor. EOB
30
W
— -1
— -2--3--4--5— -6
~- -7— -8— -9--10--11— -12— -13--14--15
r-16
— -17--18--19
r-20
O<i— -21--22--23L-24L-25L-26- -27--2B--29--30L-31L-32- -33
r-34— 7K
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 07/10/2001
Boring Number: B-23Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
2 &•3 1O> Z 4) (0C M 3 0
f i t ! o fa co 5 s Lithology Data Q. &
0 »«
-1 --2--3--4-
-5~-6 —-7--8--9--101
-1-H-121
-13-141
-151
-16-1
-17--1ft1
-191
-2Q1
-2-H-2Z1
-23^-24^-251
-261
-27--2&1
-291
-301
-3V-321
-331
-34-•»«-
;V :
J'-
- i
B23-9
D
D
D
M
M
M
W
W
W
W
CEMENT: Concrete andwood floor
/CLAY AND SILT: Black SiltyClay. Soft. Strong chemicalodor ,
CLAY AND SILT: Brown andGrey Silty Clay with tracegravel. Soft. Slight chemical jodor /
CLAY AND SAND: Brownand Grey Silty Clay with jSand and trace gravel. Stiff. 1No odor i
ICLAY AND SAND: Very Soft jGrey Sandy Clay. No odor /i
fCLAY AND SAND: Brown jand Grey Silty Clay withSand and trace gravel. Stiff.No odor
CLAY: Soft Grey Clay withtrace sand and gravel. Noodor
CLAY: Stiff Grey Clay withtrace sand and gravel. Noodor. EOB
^SSSSSSSSL50
100
100
>300
300
100
40
3015
50
--1--2--3- -4]--5
-6--7--8
r-8
in
--11--12
r~13
— -14--15--16--17r-18
4A-13
r-20
-21i— -22L-23L-24--25L-26L-27--28L-29L-30L-31--32--337-34— 1C
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-101 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
tHYGIENEERING, INC.
Project Name: Morton High Schools
Project Number 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time: 7am-3:30pm
Date: 07/10/2001
Boring Number: B-24Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
o cN 1 C
S 5 ! J_ •— mZ u CO <—
U E 1" - Q U0 to 5 ^ Lrthology Data E S
0 1— r
--2--3--4--5--6 —-7--8-
-8~•irk—-ii/
. -~ •*
-13--14^•llv—
-1«/
-1ft—
-171
-1ft1
-19--201
-2-H-22^
-23--24^-2B1
-2^-27--2ft1
-29--301
-3-H-32--331
-341
•»R-
*j ^
,
r
1
824-Pff"l
12
D
D
W
W
W
W
CEMENT: Concrete and |£88888888iwood floor (888888888
•MI HBMI 550CLAY AND SILT: Black Sitty ^^^^HClay. Soft. Strong chemical ^^^^^Hgenodor , ^ ^ ^1
/ ^^^^•sooCLAY AND SILT: Brown and ^^^HGrey Silty Clay with trace J^^^^^B 10°gravel. Soft. Slightchemical / ^^^^^H
odor ll ^H^SOCLAY AND SAND: Brown l ^^ l 16°Sandy Clay. Stiff. No odor /^^^^•600
/ ^^^^^^^^^^^^H QQflCLAY: Stiff Grey Clay with i ^^^B 50trace gravel. No odor / ^^^^^H
CLAY AND SAND: Stiff Grey HiJ^ B50
Clay with trace sand and igravel. No odor. EOB /
20
V
— -1— -2--3J--4
A— -6~--7- -8'- -9
in- IU
— -11— -121 A
--13
I"'14
4C— -TO
--17--18--19--20--21— -22--23--24- -25--26--27--28--29--30L-31L-32L-33
r-34
— IK
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIriiiiiiiiiiiiiiii
YGIENEERING, INC.
Project Name: Morton High Schools
Project Number 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time: 7am-3:30pm
Date: 07/10/2001
Boring Number: B-25Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
= «
! t5 CBco coo
Lithology Data
8COoQ.
0-1-2-3-4-5-6-7-a-9-1-1-1-1-1-1-1-1
-2
-2;-2
-3-3:-3
—
—
-—
——
o1
•H21
31
4-
5^0
7^8-9:
Vh'•H•21
!3I41
'51
'61
J71
5ft1
591
JO1
J1-1
J2-1
J31
J4^»«-!
•y
' >
B25-7
D
D
M
M
M
M
M
CEMENT: Concrete and Iwood floor n
\CLAY AND SILT: Black Silty 1Clay. Soft. Strong chemical 1
^odor I
CLAY: Soft Grey Clay. Slight j\odor /
CLAY AND SILT: Stiff 1Brown/Grey Sirty Clay. No
\odor /
BLANK: No Recovery
CLAY AND SILT: Brown andGrey Silty Clay with someblackdiscoloration. Stiff. No
I odor. EOB j
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled O'-IO1 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".
Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIII1IIIIIIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number: 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 07/10/2001
Boring Number: B-26Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
^ 3 C
I « 1 st ™~ OB M — fc ^rf
E E o 9 9 -Q to to s Lithology Data Q. 3
0 «
-1--2--3--4--5--6 —
-8--9-
-1-K-12-1
-131
-14--151
-1ft1
-17-1
-1fr
-20--2-H-22--231
-241
-251
-261
-27-1
-28^-29^-301
-3-H-321
-33^-34-1
i -
'">; .
-
B26-7
D
D
D
D
W
W
W
W
W
CEMENT: Concrete andwood floor /
CLAY AND SILT: Black SiltyClay. Stiff. Slight chemicalodor
CLAY AND SILT: Brown andGrey Silty Clay with trace ,gravel. Soft. No odor /
CLAY AND SILT: Brown andGrey Silty Clay with trace ,sand and gravel. Soft. No Iodor |
CLAY AND SAND: BlackSandy Clay with Gravel.Hard. No odor
CLAY: Very soft Grey Clay.No odor
CLAY: Stiff Grey Clay. No 1odor /
CLAY: Hard Grey Clay. Noodor. Well placed at22'depth. EOB
•
I
--2
^-3
--5J--6
7
--6--9--10--11--12--13--14--15
r-16
— -17--18--19
r-20
— -22--23L-24— -25L-26--27L-28L-29--30--31--32L-33--34— IK
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number: 2001-3495
Project Location: Economail
Samples Taken By: GPAmbient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 07/10/2001
« q>c jo
N i! 1
Boring Number: B-27Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
Lithology Data
oWaE
o-1-2-3-4-5-6-7-8-9-11-1-1:-13-i-1-i-1
-3-3;-3-3-35
H21
^^
7^ft1
a1
0^•H2^3^41
S1
ft1
71
Q2
Q2
O1
•H21
31
41
f?
B27-13
D
D
W
W
W
W
W
CEMENT: Concrete and Iwood floor n
CLAY AND SILT: Brown and JGrey Sirty Clay. Soft. Slight j\chemical odor fl
CLAY AND SILT: Black Silty IIClay. Stiff. Strong chemicalodor
CLAY AND SILT: Brown andGrey Silty Clay. Stiff. No \odor /
CLAY: Stiff Grey Clay. Noodor. EOB /
0-1-2-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23-24-25-26-27-28-29-30-31-32-33-34-35
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled O'-IO1 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".
Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.
Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number: 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 07/10/2001
Boring Number: B-28Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
|
f0)D
SI f! t(0 CBCO CO
2
"5Lithology Data
COoQ.
0-1-2-3-4-5-6-7-8-9-11-1-1:-1:-1.
-r-11-1!-21-2
-3-3:-3
—
—
—
—
—
Q1
-H
21
41
61
T1
ft1
91
O1
•H•2^
4-1
.51
•6-1
•71
5ft1
59^>o-J-HJ2-1
J3-1
J41
>C-
- B28-4
B28-13
D
M
M
W
CEMENT: Concrete and I\ wood floor j\
CLAY AND SILT: Black SiltyClay w'rth trace gravel. Soft, j
\ Slight chemical odor /]
CLAY: Soft Grey Clay. No
yodor ^CLAY AND SILT: Brown and IGrey Silty Clay with tracesnad and gravel. Soft. No j
\odor A-» I
CLAY: Stiff Grey Clay. No ,\odor. EOB /
0-1-2-3-4-5-6-7-ft-9-10-11-12-13-14-15-16-17-18-19-20-21-22
-+--23-24-25-26-27-28-29-30-31-32-33-34-35
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled O'-IO1 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time: 7am-3:30pm
Date: 07/10/2001
2 1
Boring Number: B-29Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
• 3 Cg, Z £ «
f i l l S ia 3) to s Lithology Data o. £
0 /\—
_
-2--3 J
-4-je
-O
_
-8--9--10
-11-
-12:•!*»-U
-14-1
-15:-16--171
-1ft1
-191
-201
-21-1
-22^-23^-241
-251
-261
-27—-2ft1
-29--301
-31--32--33--34-
* >
-
-'
B29-10
D
D
M
W
W
W
CEMENT: Concrete and VSSS&SSSSkwood floor /• H^HH\ /•BMICLAY AND SILT: Black Silty ^^^^BClay. Soft. No odor / ^^^^ l
CLAY: Brown and Grey Silty ^^^^HClay. Very soft. No odor. IIB BEOB /
\ /
— -2r-3— -4
e-O
-_ ~*--8— -9
r-10
- -11--12--13--14- -15--16--17--18--19--20--21--22--23--24--25--26~— -27
— -28L-29--30- -31L -32- -33- -34— _7K
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled ff-IO1 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number: 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 07/10/2001
Boring Number: B-30Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
Lithology Data
c18U
COoQ.
-10--
-20--
B30-M
M
CEMENT: Concrete andwood floor
CLAY AND SILT: Black SiltyClay. Soft. Very strongchemical odor
CLAY AND SILT: Brown andGrey Silty Clay with tracegravel. Stiff. Very strongchemical odor
CLAY AND SAND: BrownSandy Clay with tracegravel.Stiff. Strong chemical odor
CLAY: Stiff Grey Clay. Verystrong chemical odor. EOB
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled ff-101 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
HYGIENEERING, INC.
Project Name: EconoMail
Project Number: 2001-3495
Project Location: 1834 South 54th Avenue
Samples Taken By: CD
Ambient Air Temp: 60F
Start/Stop Time:8:00 am - 4:00pm
Date: 07/13/01
Boring Number: 3495-B31Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location: GPS Coord.
No>
a
a«to
I
"oLithology Data
(0o
CO9a.
u —
-1 --2-
-3-
.-5-
-6-
-7-
-a--9-
-10-
1*ȣ.
-13-
-14-
•tK-
' »
. j
^ A
M
M
CONCRETE:
CLAY: Grey, Soft, Tracegravel, Noodor/discoloration
REFUSAL: Unable toadvance boring
o-1-2
-3
-5
-6-7
-9
-10
-11
-12
-13
-14
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled Of-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time: 7am-3:30pm
Date: 07/13/2001
Boring Number: B-32Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
• ^ 3 C0) 2 « (0
1 1 ! 1 z %Q co co S Lithology Data Q. £
O A
-1 --2--3--4--5--6-7 _
-8--9--101
-1-H
-12:
-14-1
-154 A—
-17^
-19--201
-2-H-221
-23^-24-1
-25--26-1
-27-1
-28^-291
-301
-3-H-321
-331
-341
-
B32-3
B32-15
D
D
D
D
D
W
W
W
CEMENT: Concrete andwood floor /
CLAY AND SILT: Black SiltyClay. Soft. Visible oil onexposedsurf ace. Very strongchemical odor /
CLAY AND SILT: Brown andGrey Silty CNy with tracegravel. Soft. Visible sheen Ion exposed surface. Very Istrong chemical odor I
CLAY AND SILT: Brown and IGrey Silty Clay with tracegravel. Soft. No odor I
CLAY AND SAND: Brownand Grey Silty Clay withgravel. Soft. No odor
CLAY AND SILT: Brown andGrey Silty Clay with tracegravel. Soft. No odor
CLAY: Soft Grey Clay. Noodor
CLAY: Soft Gravelly Clay.Well-sorted. Poorly-graded.Coarse. No odor
CLAY: Grey Clay with tracegravel. Soft. Slight petrolodor. EOB
s«1
1
5
--1--2--3--4--5--6— .7
--8--9--10--11--12--13
r-14•fC
--16--17--18--19--20
r-21— -22
--23--24--25--26L-27L-28--29
~ -30
tl
- -32L-33
r-34
— •*•;
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled O'-lff with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".
Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
III1IIIIIIIIIIIIIII
HYGIENEERING, INC
Project Name: Morton High Schools Boring Number: B-33
Project Number: 2001-3495 Drj|ljng Company; Roc|< &
Project Location: Economail ^.^ ^ ^
Samples Taken By : GP _ , _ . . _ . .Type of Sampling: SoilAmbient Air Temp: 80 F
Boring Location:Start/Stop Time:7am-3:30pm
Date: 07/1 3/2001
£ £•3 1W Z £ CO
t i l l a iS co co ^ Lrthology Data Q. Q
0 «~[
-1 --2--3--4--5--6--7--8--9 -
-10:-1-H-121
-13-j-14^-15^
-17--18--191
-201
-2-H-221
-231
-241
-251
Oft^
-27--2&1
-29^-301
-311
-321
-331
-341
.':*=-^it&-
i)•*"
%
«.
CEMENT: Concrete. Refusaly at 11 depth. EOB /
^KKfZKKGi --1
--2--3--4--5--6--7--8--9--10- -11- -12--13--14
r-15
--17--18--19--20
r-21
--23*)A-24
--2S--26--27--28--29--30L-31--32L-33L-34
•JC
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0"-101 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number: 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 07/13/2001
Boring Number: B-34Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
1I s
- 1 t * " £o- E E "o Q Q.Q co w 2 Lithology Data £ Q
-2--3--4--5--6-7 _
-8--9--101
-1-H-121
-13--141
-15:
-17-
-19^-201
-2V-22^-231
-241
-251
-26-1
-27-1
-281
-291
-3Q1
-31--32--331
-34^j»^-
B34-5
B34-15
D
D
M
W
W
W
W
W
CEMENT: Concrete andAsphalt floor /
CLAY AND SILT: Brown andGrey Sitty Clay with tracegravel. Soft. Visible oil onexposedsurface.Verystrong jpetrol odor f
CLAY AND SILT: Black SittyClay with trace gravel. VerySoft. Visible thick oil and Isheen on exposed surface. IVery strong petrol odor I
CLAY AND SILT: Brown andGrey Silty Clay with tracesand and gravel. Soft. Slightpetrol odor
CLAY AND SAND: BrownClay with compact sand andtrace gravel. Stiff. Slightpetrol odor
CLAY AND SILT: Brown andGrey Sitty Clay with tracesand and gravel. Soft. Slightpetrol odor
CLAY: Grey Clay with tracegravel. Soft. No odor
CLAY: Grey Clay with tracesand and gravel. Soft. Slightpetrol odor. EOB
^^^^•30
15
2.5
5.0
V
--1--2--3--4~--5
--8--9--10--11--12--13--14
r-15
_ "1"— -17--18--19
r-20
— -22--23L-24— -25--26- -27--28--29'--30
-
-oo
'--34— «
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number: 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time: 7am-3:30pm
Date: 07/13/2001
Boring Number: B-35Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
o>
"5.nV)
J!
Q.
CBCO
Iio
Lrthology Data
<Bo(0oQ.
CEMENT: Concrete floor
CLAY AND SILT: Black SittyClay with trace sand andgravel. Soft. Visible oil onexposedsurface.Verystrongpetrol odor
CLAY AND SILT: Brown andGrey Sitty Clay with tracegravel. Very Soft. Visiblethick oil and sheen onexposedsurface.Verystrongpetrol odor
CLAY AND SILT: Brown andGrey Sitty Clay with tracesand and gravel. Soft. Slightpetrol odor
BLANK: No Recovery
CLAY: Grey Clay with tracesand and gravel. Soft. Slightpetrol odor. EOB
o>Q
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled O'-IO1 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
IIIIIIIIIIIIIIIIIII
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number. 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 07/13/2001
Boring Number: B-36Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
g> Z £ «J
t i l l S fQ to co s Ltthology Data Q. Q
O A—
-1 --2--3--4--5--6-
TT-f
•8-
-9--101
-1-H-121
-131
-141
-15-j<4C_-16-
.-18--19--201
-2-H
-23^-24^-251
-2&1
-27--28^-291
-3rP0*-Oj
-32^-331
-341
7B-
B36-3
B36-15
D
D
W
W
W
W
CEMENT: Concrete floor ^SSSSSSKS^
CLAY AND SILT: Black Sitty ^^^HClay. Soft. Visible oil on HjHHj 120exposedsurface.Verystrong J ^H^ Bpetrol odor /j ^H|H|
CLAY AND SILT: Brown and j ^BHj60
Grey Sitty Clay wtth trace fffmgravel. Very Soft. Visible j ^^^Bthick oil and sheen on I ^ I H 15exposedsurface.Verystrong I ^^^^^Bpetrol odor f^^^^^H
CLAY AND SILT: Brown and j ^^ lGrey Sitty Clay with trace f^^^^Hsand and gravel. Soft. Slightpetrol odor
CLAY: Grey Soft Clay wtthtrace Gravel. No odor
CLAY: Grey Clay with tracesand and gravel. Soft. Slightpetrol odor. EOB
mmmrnHHflHI15
— u
--2--3~--4
r-5
r -®-i-i- -8--9- -10--11--12--13--14
r-15A £-16
— 17- 1 1--18--19--20
r -21
— -22--23--24--25~ -26— -27--28
r ~29L-30
L-32- -33
QC
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-10' with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slightly moist, M=moist, M/W=very moist, W=wet, S=saturated.
HYGIENEERING, INC.
Project Name: Morton High Schools
Project Number 2001-3495
Project Location: Economail
Samples Taken By: GP
Ambient Air Temp: 80 F
Start/Stop Time:7am-3:30pm
Date: 07/13/2001
Boring Number: B-37Drilling Company: Rock & Soil
Drilling Method: Geoprobe
Type of Sampling: Soil
Boring Location:
O C
f fI ! t* w aa co «
£3
Lithology Data
(0o(0QQ.
f0)Q
u
-1 --2--3-j-4 —•5--6--7--8--9--101
-1-H-1-13-1
-14-1
-151
-161
-17-1
-181O-
-201
-2-H-22—
-231
-2*i2K..
-26^
-27-
-281
-291
-301
-3-H
-32^
-33-
-341
.as-
" r
"
B37-6
B37-19
D I
°D
D
D
D
D
D
D
D
SAND AND SILT: Brown fineSilt with Sand. Loose. Well- jsorted. Poorly-graded. No /I odor /I
, CLAY AND SILT: Black Sitty II Clay wtth trace sand and II gravel. Soft. No odor I
CLAY AND SILT: Brown andGrey Sitty Clay wtth trace Isand and gravel. Soft. No Iodor
CLAY: Soft Grey Clay. No Iodor I
CLAY: Stiff Grey Clay wtthtrace gravel. No odor i
SAND AND SILT: Verticallense of Sand and Silt in stiffGrey soil. No odor. EOB
I
••I— — — _
15
10
160
99
85
5
1.5
u
--1
--2
- -3— .4
— •5- -6
--7
- -8
--9--10
I" -11- -12
r-13
— -14
--15
--16
--17
r-18
•10-|!»
--20--21
--23'--24
-25L-26L-27L-28L-29
--3QL-31L-32
--33
- -34tc
II
COMMENTS: Borehole drilling using Macro Core Type Sampler. Sampled 0'-101 with PVC Liner- O.D. 1 3/4" / I.D. 1 5/8".
Boring was backfilled with bentonite chips. Photo-ionization Detector (P.I.D.) scan performed using a Mini Rae equipped with a 10.8 eV lamp.Moisture symbols: D= dry, D/M=slJghtly moist, M=moist, M/W=very moist, W=wet, S=saturated.
B37/MW5$
B38/MW6
BIO
B-
Hygieneering, Inc.7575 Plaza Court
Willowbrook, IL 60521(630) 654-2550
Scale: 1 "=7-1/2'
KEY PLAN
CLIENT:
J. Sterling Morton HighSchool District #201
PROJECT:
Phase II Assessment1840 South 54th AvenueCicero, Illinois
PROJECT NO.:
2001-3628-EBORING LOCATION DRAWING:
1 OF2
Appendix C:
Laboratory Analytical Reports
GREAT
ANALYTICAL1380 Busch Parkway
Buffalo Grove, Illinois 60089Email: [email protected]
(847)808-7766 FAX (847) 808-7772
June 21, 2001
Chris DePaolaHygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
RE: 2001-3495
Dear Chris DePaola
Enclosed are the results of analyses for sample(s) received by the laboratory on June 13, 2001. If you have anyquestions concerning this report, please feel free to contact me.
Sincerely,
Andy JohnsonProject Manager
-A-J GREAT•ll| LAKES-"-^ANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/'A
Project Manager: Chris DePaola
Sampled: 5/29/01Received: 6/13/01Reported: 6/21/01 14:00
ANALYTICAL REPORT FOR SAMPLES:
Sample Description Laboratory Sample Number Sample Matrix Date Sampled
3495-B4 B106231-01 Soil 5/29/01
Great Lakes Analytical
Andy'Jonnson, Project Manager
The results in this report appl\' to the samples anatvzed in accordance with the chain of custody documentThis analytical report must be reproduced in us entirely
Page 1 of
»». lli,. •viml±1
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
I Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL60521
Project: 2001-3495Project Number: N/A
Project Manager: Chris DePaola
Sampled: 5-29/01Received: 6,13/01Reported: 6/21/01 14:00
Total Petroleum Hydrocarbons as Diesel by EPA 8015MGreat Lakes Analytical—Oak Creek
• Analyte
*3495-B4Diesel
BatchNumber
1060038
DatePrepared
6/18/01
DateAnalyzed
SurrogateLimits
B106231-016/18/01
ReportingLimit
255
Result
708
Units
Soilmg/kg
Notes*
G1.G12.G15T10J15J8
Great Lakes Analytical *Refer to end of report lor text of notes and definitions.
Andy Johnson, Project Manager Page 2 of 5
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook.IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Chris DePaola
Sampled: 5/29,01Received: 6/13/01Reported: 6/21/01 14:00
Dry Weight DeterminationGreat Lakes Analytical
Sample Name
3495-B4
Lab ID
B106231-01
Matrix
Soil
Result Units
90.0 %
Great Lakes Analytical
Andy Jonnson, Project Manager Page 3 of
. •GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project:Project Number:
Project Manager:
2001-3495N/AChris DePaola
Sampled: 5,29,01Received: 6.13/01Reported: 6,21/01 14:00
Total Petroleum Hydrocarbons as Diesel by EPA 8015M/Quality Control' Great Lakes Analytical—Oak Creek
I Analyte
'Batch: 1060038Blank| Diesel
LCS
1Diesel
Matrix SpikeDiesel
[ Matrix Spike PupDiesel
Date SpikeAnalyzed Level
Date Prepared: 6/18/011060038-BLK16/18/01
1060038-BS16/18/01 37.1
SampleResult
QCResult Units
ReportingRecov.
LimitLimits
Recov. RPD RPD% Limit % Notes*
Extraction Method: EPA 3550B
ND
30.8
nig/kg
mg/kg
5.00
36.0-120 83.0
1060038-MS1 B106231-016/18/01 35.4 708
1060038-MSD1 B106231-016/18/01 34.4 708
461
366
mg/kg
mg/kg
10.0-160
10.0-160
NR
NR 30.0 -35
GrealftLakes Analytical
Andy Johnson, Project Manager
'Refer lo end of report for text of notes anil definitions.
Page 4 of 5
GREATLAI\to 1380 Busch Parkway Email: [email protected] Buffalo Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772
Hygieneering, Inc. Project: 2001-3495 Sampled: 5/29/017575 Plaza Court Project Number: N/A Received: 6,13/01Willowbrook, IL 60521 Project Manager: Chris DePaola Reported: 6.21/01 14:00
Notes and Definitions
Note
Gl The recovery of one or more analytes in the matrix QC (MS/MSD) associated with this sample is above the laboratory's establishedacceptance criteria. Refer to the included QC reports for more detail.
Gl 2 The reporting limit of this sample/analyte is elevated due to sample matrix and/or other effects.
G15 The relative percent difference (RPD) of one or more analytes in the matrix QC (MS/MSD) associated with this sample is above thelaboratory's established acceptance limits. Refer to the included QC reports for more detail.
T10 Diesel Range
Tl 5 Late Elevated Baseline
T8 Diesel Pattern
DET Analyte DETECTED
ND Analyte NOT DETECTED at or above the reporting l imit
NR Not Reported
dry Sample results reported on a dry weight basis
Recov. Recovery
RPD Relative Percent Difference
Great Lakes Analytical
Andy Johnson. Project Manager Page 5 of
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847)808-7766 FAX (847) 808-7772
June 12, 2001
Chris DePaolaHygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
RE: 200 1-3495
Dear Chris DePaola
Enclosed are the results or analyses for sample(s) received by the laboratory on May 30, 2001 . If you have anyquestions concerning this report, please feel free to contact me.
Sincerely,
Andy JohnsonProject Manager
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089jfjalo
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Chris DePaola
Sampled: 5,29,01Received: 5/30/01Reported: 6/12/01 13:57
ANALYTICAL REPORT FOR SAMPLES:
Sample Description Laboratory Sample Number Sample Matrix Date Sampled
3495-B1
3495-B4
3495-B5
3495-B7
B105425-01
Bl05425-02
B105425-03
B105425-04
Soil
Soil
Soil
Soil
5,29,01
5/29/01
5,29/01
5,29/01
Great Ivikes Analytical
I\LAndy Johnson, Project Manager
The results in this report apply to the samples analyzed in accordance \\ith the chain of custody documentThis analytical report must be reproduced in its entirety
Page 1 of 2
-_±^t*it.'iAi>*. ^H
$1_;;«• GREAT
LAKES(ANALYTICAL 1380 Busch Parkway
Buffalo Grove, Illinois 60089Email: [email protected]
(847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 5/31/01Received: 6/1/01Reported: 6/13/01 07:44
TCLP Metals by EPA 1311/6000/7000 Series MethodsGreat Lakes Analytical
Analyte
B-10 Sign ShopArsenicBariumCadmiumChromiumSeleniumSilverLeadMercury
BatchNumber
DatePrepared
DateAnalyzed
SpecificMethod
ReportingLimit Result
B106039-021060130n
"tit >""1060137
6/8/0111
"""11
11
6/12/01
6/U/01"«""11
6/8/016/12/01
EPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 7421EPA 7470A
0.1001.00
0.00500O.I 000.100
0.05000.00500
0.000200
ND.NDNDNDNDND
0.0271ND
Units
Soilmg/111
""""11
"
Notes
G15.G
I
I
I Great Lakes Analytical
And Johnson, Project Manager
*Refer to end of report for text of notes and definitions
Page 2 of 2
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
I1JHygieneering, Inc.
7575 Plaza CourtWillowbrook. IL 60521
Analvte
3495-B1Arsenic
1BariumCadmiumChromiumLead
1SeleniumSilverMercury
I3495-B4ArsenicBarium
1CadmiumChromiumLeadSelenium
•SilverMercury
^3495-65•Arsenic
BariumCadmium
1ChromiumLeadSeleniumSilver
•Mercury
3495-B7•ArseniciBarium
CadmiumChromium
iLead^Selenium
Silver•Mercury
I*Great Lafces Analytical
I/ i A/ l /U-
Project: 2001-3495Project Number: N/A
Project Manager: Chris DePaola
Total Metals by EPA 6000/7000 SeriesGreat Lakes Analytical
Batch Date Date SpecificNumber Prepared Analyzed Method
Bl 05425-011050635 5/31/01 5/31/01 EPA6010B
EPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OB
1060077 6/6/01 6/6/01 EPA7471A
Bl 05425-021050635 5/31/01 5/31/01 EPA6010B
EPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OB
1060077 6/6/01 6/6/01 EPA7471A
B105425-031050635 5/31/01 5/31/01 EPA60IOB
EPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OB
1060077 6/6/01 6/6/01 E P A 7 4 7 1 A
Bl 05425-041050635 5 ,31 /01 5,31/01 EPA6010B
EPA 601 OBEPA 601 OBEPA 601 OBEPA 6(11 OBEPA 601 OBEPA 601 OB
1060077 6 /601 6,6,01 E P A 7 4 7 1 A
Methods
ReportingLimit
2.5025.0
0.5000.500
1.002.502.50
0.0400
2.5025.0
0.5000.500
1.002.502.50
0.0400
2.5025.0
0.5000.500
1 .002.502.50
0.0400
2.5025.0
0.5000.500
1.002.502.5(1
0.0400
Sampled: 5/29/01Received. 530/01Reported: 6/12/01 13:57
Result Units Notes*
SoilND mg/kgNDND
9.1912.0NDND " G2ND " G15
SoilND mg/kg
59.8ND
8.9879.6 - "NDND " G2
0.119 " G15
SoilND mg/kgNDND12.36.62NDND " G2ND " G15
SoilND mg/kgNDND
13.09.67NDND " G2ND " G15
*Refer to end of report for text of notes and definitions
"Andy Jonnson, Project Manager Page 2 of 21
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Analvte
3495-B4AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
Project: 2001-3495Project Number: N/A
Project Manager. Chris DePaola
Polynuclear Aromatic Compounds by EPA Method 8310Great Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B105425-021060031 6/4/01 6/5/01 1000
200010001000900
1000100010001000900
100010001000100010001000
29.0-132
Sampled: 5,29,01Received: 5/30/01Reported: 6,12.01 13:57
Result Units Note?
Soil G12ND ug/kgNDNDNDNDNDNDNDNDND
1040NDNDND
1600NDAT? % O5
Great Lafces Analytical
Andy Johnson, Project Manager
'Refer to end of report for text of notes and definino
Page 3 ol
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
11
I Hygieneering, Inc.J 75 75 Plaza Court•JWillowbrook. IL 60521
•
Analvte
3495-B1Acetone
1BenzeneBromodichloromethaneBromoformBromomethane
12-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzene
•ChlorodibromomethaneIchloroethane
Chloroform
IChloromethane1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethene
|cis-l,2-Dichloroethenetrans-l,2-Dichloroethene1 ,2-Dichloropropane
Icis-l,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-Hexanone
1Methylene chloride
4-Methyl-2-pentanoneStyrene1,1 ,2.2-Tetrachloroethane
jTetrachloroethene[Toluene
1,1,1-Trichloroethane
11 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetate
fVinyl chloride[Total XylenesSurrogate: DibromofluoromellianeSurrogate: 1 . 2-Dichtoroethuiw-d4
Project: 2001-3495Project Number: N/'A
Project Manager: Chris DePaola
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
Bl 05425-011060024 6/1/01 6/2/01 25.0
5.005.005.005.0010.05.005.005.005.002505.005.00250
5.005.002505.005.005.005.005.0010.05.0010.05.005.005.00
250005.005.005.0(15.0010.0250
5.0081.2-1*45U.X-I45
Sampled: 5,29,01Received: 530/01Reported: 6,12,01 13:57
Result Units Notes*
Soil45.7 ug/kg A42.7NDNDND
36.3 " 1NDNDNDND
4410 " G12NDND
1110 " G128.2519.1902 " G12256NDNDND15.1ND
37.6 " 2NDNDNDND
130000 " G1226.1 " G3NDNDNDND861 " G12
44.1114 "/:,
115
'Great Lakes^Airalvtical
And>'Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 4 of 21
£.-«w._ Hsv&mliil
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495 Sampled: 5,29/01Project Number: N/A Received: 5/30/01
Project Manager: Chris DePaola Reported: 6 / 1 2 0 1 1 3 : 5 7
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Analvte
3495-B1 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units Notes*
B105425-01 SoilJ 060024 6/1/01 6/2/01 82.0-121 101 %
76.8-113 73.4 " O4
Great Lakes Analytical
And>'Johnson. Project Manager
"Refer to end of report for text of notes and definition:
Page 5 of!
I GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
11
Hygieneering, Inc.7575 Plaza Court| Willowbrook. IL 605211
Analvte
1 3495-B4Acetone
_ BenzeneM Bromodichloromethane• Bromoform
Bromomethane
12-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzene
I chlorodibromomethaneChloroethaneChloroform
IChloromethane1.1 -Dichloroethane1 ,2-Dichloroethane1 ,1 -Dichloroethene
I cis-1 ,2-Dichloroethenetrans- 1 ,2-Dichloroethene1 ,2-Dichloropropane
. cis-l,3-Dichloropropene| trans- 1 ,3-Dichloropropene1 Ethylbenzene
2-Hexanone• Methylene chloride
1 4-Methyl-2-pentanoneStyrenc1 , 1 ,2,2-Tetrachloroethane
i Tetrachloroethene[ Toluene
1,1.1 -Trich loroethane• 1,1 ,2-Trichloroethane1 Trichloroethene' Trichlorofluoromethane
Vinyl acetateVinyl chlorideTotal XylenusSurrogate: DibromofluoromethaneSurrogate: 1 .2-DicMoroelhane-d4
\ ,. .. .
Project: 2001-3495Project Number: N/A
Project Manager: Chris DePaola
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
Bl 05425-021060024 6/1/01 6/7/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-1*450.K-I4?
Sampled: 5,29/01Received: 5,30/01Reported: 6,12,01 13:57
Result Units Notes*
Soil36.7 ug/kg ANDNDNDND15.7 " 1NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND " G3NDNDNDNDNDND12(1 "/„
120
Great Lakes Analyticalrcat Lak
Andy Johnson. Project Manager
"Refer l<> end of report for text of notes and definitions.
Page 6 of 21
. H|l
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.75 75 Plaza CourtWillowbrook, IL60521
Analyte
3495-B4 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
Project: 2001-3495 Sampled: 5/29,01Project Number: N/A Received: 5,30/01
Project Manager: Chris DePaola Reported: 6 /120113 :57
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units Notes"
B105425-02 Soil1060024 6/1/01 6/7/01 82.0-121 105 %
76.8-113 93.5
Great Lakfls Analytical
Andy Johnson, Project Manager
Refer to end of report for text of notes and definition
Page 7 of :
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847)808-7766 FAX (847) 808-7772
iHygieneering, Inc.7575 Plaza CourtWillowbrook.IL 60521
11
lAnalvte
•3495-B5Acetone
1BenzeneBromodichloromethaneBromoformBromomethane
l2-Butanone(Carbon disulfide
Carbon tetrachloride-Chlorobenzene•Chlorodibromomethane•Chloroethane
Chloroform
IChloromethane1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethene
|cis-l,2-Dichloroethenetrans-l,2-Dichloroethene1 ,2-Dichloropropane
|Cis-l,3-DichloropropeneItrans- 1 ,3-Dichloropropene*Ethylbenzene2-Hexanone
iMethylene chloride|4-Methyl-2-pentanoneStyrene1 ,1 ,2.2-Tetrachloroethane
[Tetrachloroethene•Toluene1,1,1-Trichloroethane11,1,2-TrichloroethaneJTrichloroetheneTrichlorofluoromethaneVinyl acetate[Vinyl chloride[Total XylenesSurrogate: DibromofluoromethaneSurrogate: 1 . 2-Dichloroelhane-d4
Project: 2001-3495Project Number: N/A
Project Manager: Chris DePaola
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B105425-031060024 6/1/01 6/2/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.002505.005.002505.005.005.005.005.0010.05.0010.05.005.005.005.005.005.002505.0010.05.005.00
81.2-1*450.8-145
Sampled: 5,29/01Received: 5/30/01Reported: 6.12/01 13:57
Result Units Notes*
SoilND ug/kgNDNDNDND
18.5 " INDNDNDNDNDNDND
2300 " G127.2546.25530 " G12230NDNDNDNDNDNDNDNDNDNDND247 " G3ND
8160 " G12NDND261ND112 "/„in
Great Lal/es Analytical
Andy JVnmson, Project Manager
"Refer to end <>/ report for text of notes and definitions.
Page 8 of 21
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL60521
Project: 2001-3495Project Number: N/A
Project Manager: Chris DePaola
Sampled:Received:Reported:
5,29/015/30/016,' 12/01 13:57
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Analvte
3495-B5 (continued^Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B105425-03~~1060024 6/1/01 6/2/01 82.0-121
76.8-11*
Result
86.373.0
Units Notes*
Soil%
04
Great Uakes Analytical "Refer to end of report for text of notes and definnioi.
And\ l Johnson, Project Manager Page 9 of
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
I1
j Hygieneering, Inc.J 75 75 Plaza CourtBJWillowbrook, IL6052I
•
Analvte
3495-B7Acetone
_ Benzene• Bromodichloromethane• Bromoform
Bromomethane
12-ButanoneCarbon disulfldeCarbon tetrachlorideChlorobenzene
HChlorodibromomethane• Chloroethane
Chloroform
tChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethene
Icis- 1 ,2-Dichloroethenetrans- 1 ,2-Dichloroethene1 ,2-Dichloropropane
Icis-1 ,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-Hexanone
1Methylene chloride
4-Methyl-2-pentanoneStyrene1 .1 ,2,2-Tetrachloroethane
ITetrachloroetheneToluene1,1,1 -Trichloroethane
11,1.2-TrichIoroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetate
(Vinyl chlorideTotal XylenesSurrogate: Dibromofluoroinelliane
-Surrogate: 1 .2-Dichloroethane-d4
Project: 2001-3495Project Number: N/A
Project Manager: Chris DePaola
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B105425-041060024 6/1/01 6/2/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
X 1.2 -1*4
50. 8- 145
Sampled: 5,29,01Received: 5,30/01Reported: 6 12,01 13:57
Result Units Notes*
SoilND ug/kgNDNDNDND
12.8 " 1NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND " G3NDNDNDNDNDND112 "/„1/2
Great Stakes Analytical "Refer to end of report for text of notes and definition*.
Andy Johnson. Project Manager Page 10 of 21
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
.Email: [email protected](847)808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL60521
Project: 2001-3495Project Number: N/A
Project Manaeer: Chris DePaola
Sampled:Received:Reported:
5,29/015/30/016/12.01 13:57
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Analvte
3495-B7 (continued)Surrogate: Toluene-d8Surrogate: 4-Broinofluorobenzene
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B105425-041060024 6/1/01 6/2/01 82.0-121
76.8-113
Result
92. 189.2
Units Notes*
Soil%
Great Lakes Analytical
Andy Johnson. Project Manager
"Refer to end of report for text of notes and definition
Page 1 1 of
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
iI Hygieneering, Inc.
•7575 Plaza CourtJWillowbrook. IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Chris DePaola
Sampled: 5,29/01Received: 530/01Reported: 6 12/01 13:57
IDry Weight Determination
Great Lakes Analytical
lampleName Lab ID Matrix Result Units
I
I
I
I
I
I
I
I
I
B105425-01
Bl 05425-02
B105425-03
B105425-04
Soil
Soil
Soil
Soil
80.9
90.0
78.9
83.0
Great Lakes Analytical
I //A-AnuV JoTinson, Project Manager
I
Pane 12 of 21
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook.IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Chris DePaola
Sampled: 5,29,01Received: 5,30,01Reported: 6,12,01 13:57
Total Metals by EPA 6000/7000 Series Methods/Quality ControlGreat Lakes Analytical
Analvte
Batch: 1050635
DateAnalyzed
Date Prepa
SpikeLevel
red: 5/31/0
SampleResult
1
QCResult
Reporting Limit Recov.Units Recov. Limits %
Extraction Method: EPA 3050B
RPDLimit
RPD% Notes*
BlankArsenicBariumCadmiumChromiumLeadSeleniumSilver
1050635-BLK15/31/01
ArsenicBariumCadmiumChromiumLeadSeleniumSilver
Matrix SpikeArsenicBariumCadmiumChromiumLeadSeleniumSilver
Matrix Spike PupArsenicBariumCadmiumChromiumLeadSeleniumSilver
1050635-BS15/31/01 106
20020020020156.0200
1050635-MS15/31/01 105
198198198199
55.4198
Bl 05382-01ND
36.1ND
9.465.66NDND
1050635-MSD15/31/01 106
200200200
20156.0200
B 105382-01
ND36.1ND
9.465.66NDND
NDNDNDNDNDNDND
10819820019720155.2147
77.9191146159156
41.618.7
84.3202155169167
44.1I 1.8
mg/kg
mg/kg
mg/kg
mg,kg
2.5025.0
0.5000.500
1.002.502.50
81.1-12172.9-12174.3-11872.2-12172.2-12173.1-12010.0-155
53.1-11754.3-11152.5-10843.3-11543.3-11547.3-11310.0-117
10299.0100
98.5100
98.673.5
74.278.273.775.575.575:1
9.44
53.1-54.3-52.5-43.3-43.3-47.3-10.0-
17110815151317
79.583.077.579.880.378.75.90
26.728.824.924.1
24.125.347.0
6.905.965.035.546.164.6846.2
Great LAkes Analytical "Refer to end of report for text of notes and definitions.
An/ly Johnson, Project Manager Page 13 of 21
I
I
aSL. ,«a-- •vAmH
SSlGREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
I Hygieneering, Inc.J?575 Plaza Court•Willowbrook.lL 60521
•
Project: 2001-3495Project Number: N/A
Project Manager: Chris DePaola
Sampled: 5/29/01Received: 530/01Reported: 6,12/01 13:57
Total Metals by EPA 6000/7000 Series Methods/Quality Control
lAnalyte
•Batch: 1060077Blank
1Mercury
LCSMercury
Matrix SpikeMercury
Great Lakes Analytical
Date Spike Sample QCAnalvzed Level Result Result
Date Prepared: 6/6/011060077-BLK16/6/01 ND
1060077-BS16/6/01 0.200 0.188
1060077-MS1 B105425-016/6/01 0.200 ND 0.274
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*
Extraction Method: EPA 7471 A
mg/kg 0.0400
mg/kg 71.9-126 94.0
mg/kg 38.3-154 137
•M
I
I
I
I
I
I
I
Matrix Spike Pup
reat Latfes Analyt ical
1060077-MSD1 B105425-016/6/01 0.156 ND 0.173 mg/kg 38.3-154 111 9.52 21.0
IAndy Johnson. Project Manager
Refer to end of report for text of notes and definitions.
Page 14 of 21
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL60521
Analvte
Batch: 1060031BlankAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1 ,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
LCSAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
t
Project: 2001-3495Project Number: N/A
Project Manager: Chris DePaola
Polynuclear Aromatic Compounds byGreat Lakes
Date Spike SampleAnalyzed Level Result
Date Prepared: 6/4/011060031-BLK16/5/0111
11
""ii"11
n11
11
n"n
11
"
' 17.1
1 06003 1-BS16/5/01 67.0
67.067.067.067.067.067.067.067.067.067.067.067.067.067.067.016.7
EPA MethodAnalytical
QCResult
Sampled: 5,29,01Received: 5/3001Reported: 6,12,01 13:57
8310/Quality Control
Reporting LimitUnits Recov. Limits
Recov. RPD RPD% Limit % Notes'
Extraction Method: EPA 3550B
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
9.28
58.495.066.266.251.072.572.562.268.774.660.736.469.558.166.374.115.2
ug/kg 100200100100
90.0100100100100
90.0100100100100100100
29.0-132
ug/kg 30.8-12038.9-15832.9-12240.5-12531.2-12845.0-13238.7-13753.4-12546.5-12942.8-13437.1-11640.8-10851.0-11522.7-11629.5-12344.5-11829.0-132
54.3
87.2142
98.898.876.1108I OK
92.81031 1 1
90.654.3104
86.799.0
I I I91.0
GreatX-.akes Analytical
A»dy Johnson, Project Manager
"Refer to end of report for text of notes and definition*
Page 15 of 2
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
11
Hygieneering, Inc.7575 Plaza Court
• Willowbrook, IL 60521
1*\
(Analvte
Matrix SpikeAcenaphthene
1AcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyrene
1Benzo (b) ttuorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChrysene
I Dibenz (a,h) anthracene• Fluoranthene
Fluorene
1Indeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyrene
( Surrogate: Carbazole
Matrix Spike Pup
1AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthracene
1Benzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluoranthene
• Chrysene• Dibenz (a,h) anthracene
Fluoranthene
1FluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrene
1PyreneSurrogate: Carbazole
1 <
Project: 2001-3495Project Number: N/'A
Project Manager: Chris DePaola
Sampled: 5,29/01Received: 5,30/01Reported: 6 12/01 13:57
Polynuclear Aromatic Compounds by EPA Method 8310/Quality ControlGreat Lakes Analytical
Date SpikeAnalyzed Level
SampleResult
QC Reporting LimitResult Units Recov. Limits
Recov. RPDLimit
RPD% Notes*
1060031-MS1 B105439-016/5/01 64.6
64.664.664.664.664.664.664.664.664.664.664.664.664.664.664.616.2
1 06003 1-MSD16/5/01 67.6
67.667.667.667.667.667.667.667.667.667.667.667.667.667.667.616.9
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
B 105439-01NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
36.0 ug/kg84.841.136.635.243.437.640.348.042.640.342.534.040.444.836.511.5
49.8 ug/kg104
54.148.449.356.244.055.670.057.562.560.047.454.456.549.614.6
10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145
29.0-132
10.0-15410.0-17610.0-1 1410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145
29.0-132
55.7131
63.656.754.567.258.262.474.365.962.465.852.662.569.356.571.0
73.7154
80.071.672.983.165.182.2104
85.192.588.870.180.583.673.4N6.4
66.465.767.157.854.551.965.959.365.249.858.753.955.862.557.456.6
27.816.122.823.228.921.211.227.433.325.438.929.828.525.218.726.0
'Great ,tibkes Analytical
\AAndy Johnson. Project Manager
"Refer to end of report for text of notes ami definitions.
Page 16 of 21
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Chris DePaola
Sampled: 5/29/01Received: 5/30/01Reported: 6,12/01 13:57
Volatile Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical
Date Spike SampleAnalvte Analyzed Level Result
Batch: 1060024 Date Prepared: 6/1/01Blank 1060024-BLK1Acetone 6/1/01Benzene "Bromodichloromethane "Bromoform "Bromomethane "2-Butanone "Carbon disulfide "Carbon tetrachlorideChlorobenzene "Chlorodibromomethane "Chloroethane "Chloroform "Chloromethane "1,1 -Dichloroethane "1,2-Dichloroethane "1,1-Dichloroethene "cis-l,2-Dichloroethene "trans- 1,2-Dichloroethene "1 ,2-Dichloropropane "cis-1 ,3-Dichloropropene "trans- 1,3-Dichloropropene "Ethylbenzene2-HexanoneMethylene chloride "4-Methyl-2-pentanone "Styrene "1,1,2,2-Tetrachloroethane "Tetrachloroethene "Toluene "1,1,1-Trichloroethane "1 , 1 ,2-Trichloroethane "Trichloroethene "Trichlorottuoromethane "Vinyl acetate "Vinyl chlorideTotal XylenesSurrogate: Dibrotnofluoromethane " 50.0
QCResult
NDNDNDNDND
11.6NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
8.71NDNDNDNDNDNDNDNDNDNDNDND
52. 1
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notc<
Extraction Method: EPA 5035B [P/T]
ug/kg 25.05.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-1*4 104
Great Lakes Analytical Refer to end of report for text of notes and definition.
AndV Johnson, Project Manager Page 17 of!
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email. info@glalabs com(847) 808-7766 FAX (847) 808-7772
11
Hygieneering, Inc.7575 Plaza Court| Willowbrook. 1L 60521
•
Project: 2001-3495Project Number: N/A
Project Manager: Chris DePaola
Sampled: 5/29/01Received: 5,30/01Reported: 6,12/01 13:57
Volatile Organic Compounds by EPA Method 5035/8260B/Quality Control
Analvte
1 Blank (continued)Surrogate: 1 . 2-Dichloroethane-d4
1Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
LCS
1AcetoneBenzeneBromodichloromethaneBromoform
H BromomethaneH 2-Butanone
Carbon disultlde
1Carbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethane
1ChloroformChloromethane1,1 -Dichloroethane
11 ,2-Dichloroethane1 , 1 -Dichloroethenecis-1 ,2-Dichloroethenetrans- 1 ,2-Dichloroethene
11 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene
• 2-Hexanone• Methylene chloride
4-Methyl-2-pentanone
ISryrene1 , 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene
11,1,1 -Trichloroethane1,1,2-TrichloroethaneTrichloroethenc
_ Trichlorofluoromethane
Great Lakes
Date Spike SampleAnalyzed Level Result
1060024-BLK16/1/01 50.0
50.050.0
1060024-BS16/1/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0
Analytical
QCResult
48.446.946.0
45.545.150.749.558.655.050.762.858.353.4115
55.036.650.360.454.555.361.246.647.650.051.217.752.934.655.443.155.748.264.248.X53.161.4
Reporting LimitUnits Recov. Limits
ug/kg 50.8-14582.0-12176.8-11*
ug/kg 10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-142641-13460.0-13476.4-12561.8-132140-241
Recov. RPD RPD% Limit % Notes*
96.893.892.0
91.090.2101
99.01 1 7110101126117107NR110
73.210112110911 1122
93.295.2100102
35.4106
69.21 1 1
86.21 1 1
964128
97.6106123
1 Great Ldkes Analytical
IAndy Johnson, Project Manager
I
"Refer to end of report /or text of notes and definitions.
Page 18 of 21
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Chris DePaola
Sampled: 5,29,01Received: 530,01Reported: 6 12.01 13:57
Volatile Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical
Analyte
LCS (continued)Vinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 , 2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
LCS PupAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1.1-Dichloroethenecis- 1 ,2-Dichloroethenetrans- 1 ,2-Dichloroethene1 ,2-Dichloropropanecis-l,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 .1 ,2.2-TetrachloroethaneTetrachloroetheneToluene
Date Spike SampleAnalyzed Level Result
1060024-BS16/1/01 50.0
50.0150
50.050.050.050.0
1060024-BSD16/2/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.05(1.0
QC Reporting LimitResult Units
29.3 ug/kg41.5168
'53.752.948.045.3
39.8 ug/kg49.355.052.158.454.157.868.460.857.5119
59.335.257.862.160.060.267.751.250.15 1 . 153.617.259.735.957.046.958.152.1
Recov. Limits
10.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113
10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-1752X.4-14910.0-1X864.6-1366X.4-13757.6-14264.1-134
riecov.%
58.683.0112107106
96.090.6
79.698.6110104117108116137122115NR119
70.4l l t >124120120135102100102107
34.41 19
7 1 . X1 14
93.X1 1 6104
RPDLimit
34541.442.057.461.9173126
43.539.041.690.343.571.841.868.647.539.343.038.141.557.242.7
I 2 X67.4
1 1 937.254.646.342. (i
RPD% Notes'
13.48.908.534.93
01.8313.88.374.187.213.427.863.9013.82.459.617.7910.19.024.921.984.782.X71 1 . 63.692.d78.444.417.5X
Great Lakes Analytical "Refer to end of report for text of notes and definitions.
_LAndy Johnson, Project Manager Page 19 of 2
GREAT^^ 1380 Busch Parkway Email: [email protected]
ANALYTICAL Buffalo Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772
I
I
I
Hygieneering, Inc.7575 Plaza CourtWillowbrook.IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Chris DePaola
Sampled: 5,29/01Received: 5,30/01Reported: 6,12/01 13:57
Volatile Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical
•J Analyte
* LCS Pup (continued)1,1,1 -Tri Chloroethane
11 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane
_ Vinyl acetate• Vinyl chlorideB Total Xylenes
Surrogate: DibromofluoromethaneISurrogi. 'e: 1 ,2-Dichloroethane-d4
Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
1
1
1
1
1
1
1
1Great Lakts Analytical
1 /L—1 , __
Andy Johnson. Project Manager
1
Date Spike Sample QC Reporting Limit Recov. RPD RPDAnalyzed Level Result Result Units Recov. Limits % Limit % Notes
1060024-BSD16/2/01 50.0 68.7 ug/kg 60.0-134 137 44.2 6.79
50.0 52.9 " 76.4-125 106 53.2 8.2550.0 57.3 " 61.8-132 115 43.5 8.1450.0 56.7 " 14.6-241 113 115 8.4750.0 31.2 " 10.0-161 62.4 92.1 6.2850.0 40.2 " 57.9-143 80.4 81.0 3.18150 174 " 60.0-141 116 40.1 3.51
50.0 54.4 " 81.2-1*4 10950.0 50.9 " 50.8-145 10250.0 48.1 " 82.0-121 96.250.0 45.8 " 76.8-113 91.6
"Refer to end of report for text of notes and definitions
Page 20 of 2
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook.IL 60521
Project: 2001-3495Project Number: N/'A
Project Manager: Chris DePaola
Sampled: 5,29/01Received: 530-01Reported: 6.1201 13:57
Notes and Definitions
Note
A The concentration of the analyte detected in the sample is characteristic of a laboratory artifact.
G12 The reporting limit of this sample/analyte is elevated due to sample matrix and/or other effects.
G15 The relative percent difference (RPD) of one or more analytes in the matrix QC (MS/MSD) associated with this sample is above thelaboratory's established acceptance limits. Refer to the included QC reports for more detail.
G2 The recovery of one or more analytes in the matrix QC (MS/MSD) associated with this sample is below the laboratory's establishedacceptance criteria. Refer to the included QC reports for more detail.
G3 The recovery of one or more analytes in the laboratory control QC (BS/BSD) associated with this sample is above the laboratory'.'established acceptance criteria. Refer to the included QC reports for more detail.
04 The recovery for this analyte is below the laboratory's established acceptance criteria.
05 The recovery for this analyte is above the laboratory's established acceptance criteria.
1 The method blank associated with this sample contains 11.6ppb of this analyte.
2 The method blank associated with this sample contains 8.71ppb of this analyte.
DET Analyte DETECTED
ND Analyte NOT DETECTED at or above the reporting l imit
NR Not Reported
dry Sample results reported on a dry weight basis
Recov. Recovery
RPD Relative Percent Difference
Great LakeyAnalytical,
And^Johnson, Project Manager Page 21 of 21
GREATLHl\CO
ANALYTICAL1380 Busch Parkway
Buffalo Grove, Illinois 60089Email: info@glalabs com
(847) 808-7766 FAX (847) 808-7772
June 13, 2001
Gary MilkerisHygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
—
•
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RE: 2001 -3495
Dear Gary Milkeris
Enclosed are the results of analyses for sample(s) received by the laboratory on June 1 , 2001 . If you have anyquestions concerning this report, please feel free to contact me.
Sincerely,
Andy JohnsonProject Manager
&.*L . i £v_ ^H
ivAviB
•§••
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWiliowbrook. IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 5,31/01Received: 6.1/01Reported: 613-0107:44
ANALYTICAL REPORT FOR SAMPLES:
Sample Description Laboratory Sample Number Sample Matrix Date Sampled
B-4 Outside Parking Lot
B-10 Sign Shop
B106039-01
Bl 06039-02
Water
Soil
5,31/01
5/31/01
Greatf Lakes Analytical The results in this report apply to the samples analyzed in accordance \vilh the chain of custody document.This analytical report must be reproduced in us entirety.
Andy Johnson, Project Manager Page 1 of 2
LAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
11
1 Hygieneering, Inc.J 75 75 Plaza Court•Willowbrook. IL 60521
•
•
| Analyte
^B-4 Outside Parking LotAcetone
^Benzene•Bromodichloromethane•Bromoform
Bromomethane•2-ButanoneBCarbon disultlde
Carbon tetrachloride—Chlorobenzene•Chlorodibromomethane•Chloroethane
Chloroform
f hloromethane1 -Dichloroethane
i ,2-Dichloroethane1,1-Dichloroethene
§is- 1 ,2-Dichloroethene•ans-1 ,2-Dichloroethene
1 ,2-Dichloropropane^;is-l ,3-Dichloropropene«rans-l ,3-Dichloropropene^fethylbenzene
2-Hexanone
Fethylene chlorideMethyl-2-pentanone
Styrene1 , 1 ,2,2-Tetrachloroethane
•1 etrachloroethene•Toluene
1,1 ,1 -TrichloroethaneM! , 1 ,2-Trichloroethane•Trich 1 oroeth en c^^"rich lorofl uoromethane
Vinyl acetate
§inyl chlorideotal Xylenes
Surrogate: Dibromofluoromelhane^surrogate: l.2-Dichloroethane-d4
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
Bl 06039-011060128 6/7/01 6/8/01 10.0
2.002.002.002.0010.02.002.002.002.002.002.002.002.002.002.002.002.002.002.002.002.0010.02.0010.02.002.002.002.002.002.002.002.002.002.002.00
9 1 . / - / I I
X5.I-IM
Sampled: 5/31/01Received: 6. 1/01Reported: 6,13/01 07:44
Result Units Notes*
Water G15ND ug,INDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDitr %HI 5 " O5
rcat L; kes Analytical
iAndy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 3 of 2 1
I
femal
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 5,31,01Received: 61 /01Reported: 6.13,01 07:44
Volatile Organic Compounds by EPA Method 8260BGreat Lakes Analytical
AnalvteBatchNumber
DatePrepared
DateAnalyzed
SurrogateLimits
ReportingLimit Result Units Notes*
B-4 Outside Parking Lot (continued')Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
1060128 6/7/01B106039-01
6/8/01 95.1-10589.6-105
Water106
99.4
CIS05
Great/Lakes Analytical "Refer to end of report for text of notes and definitions.
Andy Johnson, Project Manager Page 4 of 21
1 K:,A<~| GREATfill LAKES
- •&•• ANALYTICAL•11
1 Hygieneering, Inc.J?575 Plaza Court•Willowbrook, IL 60521
•
Analvte
B-4 Outside Parking LotAcenaphthene
•Acenaphthylene•Anthracene*Benz (a) anthracene
Benzo (a) pyrene•Benzo (b) fluoranthenejBenzo (ghi) perylene
Benzo (k) fluoranthene^Chrysene•Dibenz (a,h) anthraceneBpluoranthene
Fluorene•Indeno (1,2,3-cd) pyrene•Naphthalene^rhenanthrene
Pyrene•Surrogate: Carbazole
1
1
1
1
1
••brapt Lakes Analytical
1380 Busch Parkway Email: [email protected] Grove, I l l inois 60089 (847) 808-7766 FAX (847) 808-7772
Project: 2001-3495 Sampled: 5 3 1 , 0 1Project Number: N/A Received: 6/1/01
Project Manager: Gary Milkeris Reported: 6/130107:44
Polynuclear Aromatic Compounds by EPA Method 8310Great Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units Notes*
B106039-01 Water G12.G31060075 6/6/01 6/7/01 25.0 ND ug,l
25.0 ND25.0 ND
0.500 ND0.500 3.250.500 4.16
25.0 ND0.500 1.13
5.00 10.00.500 ND
25.0 48.125.0 ND1.00 2.0125.0 ND25.0 61.825.0 ND
24.5-122 93.2 "A,
"Refer to end of report for text of notes and definitions.
Andy Johnson, Project Manager Page 5 of 21
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Analyte
B-10 Sign ShopAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 , 1 -Dichloroethane1,2-Dichloroethane1 , 1 -Dichloroethenecis-l,2-Dichloroethenetrans- 1 ,2-Dichloroethene1 ,2-Dichloropropanecis-l,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-M ethy 1-2-pentanoneStyrene1 , 1 ,2.2-TetrachloroethaneTetrach loroetheneToluene1.1,1 -Trichloroethane1 , 1 ,2-TrichIoroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 .2-Dichloroelhane-d4
Project: 2001-3495Project Number: N/AProject Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B106039-021060123 6/7/01 6/9/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.02505.00
81.2-1*450. N- 145
Sampled: 5/31.01Received: 6.1/01Reported: 6 /13 01 07:44
Result Units Notes*
Soil66.0 ug/kg ANDNDNDND14.0 " A8.58NDNDNDNDNDNDND205ND11.2NDNDNDNDNDNDNDNDNDND17.1NDNDND
5.02NDND
1060 " G12ND104 "/,,108
Great Lakes Analytical
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions
Page 6 of 2
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email [email protected](847) 808-7766 FAX (847) 808-7772
IHygieneering, Inc.
J7575 Plaza CourtWillowbrook. IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 5,31-01Received: 6,1,01Reported: 6 13,01 07:44
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units Notes*
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Sign Shop (continued')Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
1060123 6/7/01Bl 06039-02
6/9/01 82.0-12176.8-113
98.975.8
Soil%
O4
Great Makes Analytical
I/
I
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 7 of 21
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 5,31/01Received: 6.1/01Reported: 6,13/01 07:44
TCLP Metals by EPA 1311/6000/7000 Series Methods/Quality ControlGreat Lakes Analytical
Analvte
Batch: 1060130BlankArsenicBariumCadmiumChromiumSeleniumSilverLead
Date Spike SampleAnalyzed Level Result
Date Prepared: 6/8/011060130-BLK16/11/01
""""
6/8/01
QCResult
NDNDNDNDNDNDND
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*
Extraction Method: EPA 3015
mg/1 0.1001.00
0.005000.1000.100
0.05000.00500
LCSArsenicBariumCadmiumChromiumSeleniumSilverLead
Matrix SpikeArsenicBariumCadmiumChromiumSeleniumSilverLead
Matrix Spike PupArsenicBariumCadmiumChromiumSeleniumSilverLead
1060130-BS16/11/01 2.00
2.001 .002.001 .001 .00
6/8/01 0.0240
1060130-MS16/11/01 2.00
2.001.002.001.001 .00
6/8/01 0.0240
1060130-MSD16/11/01 2.00
2.001.002.001 .001.00
6/8/01 0.0240
Bl 06023-01NDND
0.0528NDNDND
0.281
Bl 06023-01NDND
0.0528NDNDND
0.281
2.092.071.012.041.02
0.9720.0255
2.103.071.062.011.09
0.3600.253
2.083.021.031.971.07
0.4940.266
mg/
mg,' I
72.8-13981.6-12676.7-13179.3-13069.9-13583.2-13759.9-152
10410310110210297.2106
82.8-13567.1-15466.3-15367.1-14966.1-15019.6-17635.2-176
105
153
101
100
109
36.0NR
82.8-13567.1-15466.3-15367.1-14966.1-15019.6-17635.2-176
104151
97.798.5107
49.4NR
19.316.023.813.X21.835.835.3
0.9571.323.321.511.8531.4
Great
Andy ohnson. Project Manager
"Refer to end of report for text of notes and definitions.
Page 8 of 21
' Rill LAKES. iSmm ANALYTICAL11
Hygieneering, Inc._ 7575 Plaza CourtI Willowbrook, IL 60521
1380 Busch ParkwayBuffalo Grove, I l l inois 60089
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Email, [email protected](847) 808-7766 FAX (847) 808-7772
Sampled: 5,31/01Received: 6/1/01Reported: 6,13/01 07:44
TCLP Metals by EPA 1311/6000/7000 Series Methods/Quality Control
Analvte
Im Batch: 1060137
Blank
1Mercury
LCSMercury
[ Matrix SpikeMercury
• Matrix Spike Pup
Great Lakes Analytical
Date Spike Sample QCAnalyzed Level Result Result
Date Prepared: 6/12/011060137-BLK16/12/01 ND
1060137-BS16/12/01 0.00100 0.000853
1060137-MS1 B106039-026/12/01 0.00100 ND 0.000879
1060137-MSD1 B106039-02
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*
Extraction Method: EPA 7470A
mg/1 0.000200
mg/1 73.9-123 85.3
mg/1 58.0-152 87.9
Mercury
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6/12/01 0.00100 ND 0.000875 mg/1 58.0-152 87.5 26.2 0.456
Great L ikes Analytical
Andy Jonnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 9 of 2!
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: info@glalabs com(847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 5/31/01Received: 6,1/01Reported: 6/13/01 07:44
Volatile Organic Compounds by EPA Method 8260B/Quality ControlGreat Lakes Analytical
Date Spike SampleAnalyte Analyzed Level Result
Batch: 1060128 Date Prepared: 6/7/01Blank 1060128-BLK1Acetone 6/7/01Benzene "Bromodichloromethane "Bromoform "Bromomethane "2-Butanone "Carbon disulfideCarbon tetrachloride "Chlorobenzene "Chlorodibromomethane "Chloroethane "Chloroform "Chloromethane "1,1 -Dichloroethane "1,2-Dichloroethane "1,1-Dichloroethene "cis- ,2-Dichioroethene "trans- 1,2-Dichloroethene "1 ,2-Dichloropropane "cis-l,3-Dichloropropene "trans- 1 ,3-DichloropropeneEthylbenzene "2-Hexanone "Methylene chloride "4-Methyl-2-pentanone "Styrene1 , 1 ,2,2-TetrachloroethaneTetrachloroethene "Toluene "1,1, -Trichloroethane "1,1,2-Trichloroethane "Trichloroethene "Trichlorofluoromethane "Vinyl acetate-Vinyl chlorideTotal XylenesSurrogate: Dibromofluoromeihane " 50.0
QCResult
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
50.*
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*
Extraction Method: EPA 5030B (P/T)
ug/ l 10.02.002.002.002.0010.02.002.002.002.002.002.002.002.002.002.002.002.002.002.002.002.0010.02.0010.02.002.002.002.002.002.002.002.002.002.002.00
91.1-111 101
Gre at Lakes Analytical
Andy Johnson. Project Manager
"Refer to end of report for text of notes and definitions
Page I Oof 2
I GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
11JHygieneering, Inc.
7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method
1*T
| Analyte
[| Blank (continued^Surrogate: 1 . 2-Dichloroethane-d4
_ Surrogate: Toluene-d8V Surrogate: 4-Bromofluorobenzene
LCS
1AcetoneBenzeneBromodichloromethaneBromoform
IBromomethane2-ButanoneCarbon disulfide
1Carbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethane
1ChloroformChloromethane
,1 -Dichloroethane^ ,2-Dichloroethane• ,1-DichloroetheneV cis-1 ,2-Dichloroethene
rans-1 ,2-Dichloroethene
1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthyl benzene
12-HexanoneMethylene chloride4-Methyl-2-pentanone
IStyrene1 , 1 ,2,2-TetrachloroethaneTetrach 1 oroetheneToluene
11,1 ,1-Trichloroethane1,1 ,2-TrichloroethaneTrichloroetheneTrichlorotluoromethane
• f
Great Lakes
Date Spike SampleAnalyzed Level Result
1060128-BLK16/7/01 50.0
50.050.0
10601 28-BS16/8/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0-50.0
Analytical
QCResult
53.052.049.9
58.350.053.357.047.854.155.850.855.257.151.951.146.945.750.048.555.747.852.753.955.156.350.150.052.660.338.65(5.1
55.552.956.9d().254.0
Sampled: 5,31/01Received: 6/1/01Reported: 6,13/01 07:44
8260B/Quality Control
Reporting LimitUnits Recov. Limits
ug/I 85.1-10495.1-10589.6-105
ug/1 10.0-19484.9-11574.3-13070.1-12010.0-25810.0-14743.4-14660.5-13885.4-11578.8-11610.0-45574.5-13478.7-12876.8-12066.7-12972.7-12587.0-12377.0-11988.3-11581.2-12075.2-12684.3-11921.4-14262.5-14038.2-14186.6-11713.2-19776.6-12086.3-12063.5-14684.5-12451.4-15310.0-586
Recov. RPD RPD% Limit % Notes*
106104
99.8
117100107114
95.6108112102110114104102
93.891.4100
97.0
I"95.6105108110113100100105121
77.21121 ) 1106114120108
I Great Lakes Analytical
I
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Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions
Page 1 I of 21
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 5/31/01Received: 6/1/01Reported: 6/13/01 07:44
Volatile Organic Compounds by EPA Method 82606/Quality ControlGreat Lakes Analytical
Analyte
LCS (continued)Vinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 ,2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
Matrix SpikeAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 , 1 -Dichloroethane1,2-Dichloroethane1 , 1 -Dichloroethenecis-l,2-Dichloroethenetrans- 1 ,2-Dichloroethene1 ,2-Dichloropropanecis- 1 ,3-Dichloropropenetrans- 1,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2.2-TetrachloroethaneTetrachloroetheneToluene
Date SpikeAnalyzed Level
1060128-BS16/8/01 50.0
50.0150
50.050.050.050.0
SampleResult
QC Reporting Limit Recov. RPD RPDResult Units Recov. Limits % Limit °/o Notes*
37.8 ug/l47.7173
49.747.451.551.9
10.0-21971.0-12088.3-11891.1-11185.1-10495.1-10589.6-105
75.695.4115
99.494.8103104
1060128-MS1 B106020-066/8/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
54.9 ug/l44.250.556.543.751.442.839.950.154.962.346.337.240.149.538.250.240.648.746.848.647.849.745.852.754.758.844.749.0
10.0-26971.4-11565.3-13454.6-13210.0-17610.0-20123.4-14326.3-13377.4-10872.8-11710.0-29370.8-12461.3-10963.3-11454.5-13736.1-11564.8-12954.7-11377.8-11467.3-11757.3-12468.3-11110.0-22545.6-15010.0-20849.7-12620.6-22345.1-11371.3-1 18
11088.4101113
87.4103
85.679.8100110125
92.674.480.299.076.4100
81.297.493.697.295.699.491.6105109118
89.498.0
Great L <es Analytical
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions
Page 12 of 2
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email, [email protected](847) 808-7766 FAX (847) 808-7772
JHygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Project:Project Number:
Project Manager:
2001-3495N/AGary Milkeris
Sampled: 5,31,01Received: 6/1/01Reported: 6,13/01 07:44
Volatile Organic Compounds by EPA Method 82606/Quality ControlIjt Great Lakes Analytical
1_jAnalyte
BlMatrix Spike (continued)1,1,1 -Trichloroethane
a»\ ,1 ,2-Trichloroethane•Trichloroethene^^"ri ch 1 orofl uorom ethan e
Vinyl acetate
f inyl chlorideotal Xylenes
Surrogate: Dibromofluoromethane^Surrogate: 1 . 2-Dichloroethane-d4^[Surrogate: Toluene-d8^Surrogate: 4-Bromofluorobenzene
•Matrix Spike PupBAcetone
BenzeneBromodichloromethane
tromoformromomethane
2-Butanone•Carbon disulfide•Carbon tetrachloride^Chlorobenzene
Chlorodibromomethane
f hloroethanehloroform
Chloromethane
— 1 , 1 -Dichloroethane• I ,2-Dichloroethane9\ , 1 -Dichloroethene
cis- 1 ,2-Dichloroethene
Krans- ,2-Dichloroethene,2-Dichloropropane
cis- 1 ,3-Dichloropropenetrans- ,3-Dichloropropene
Kthylbenzene-Hcxanone
Methylene chloride
|
4-Methvl-2-pentanone'
Great ,akes Analytical
Andv ohnson. Project Manager
Date SpikeAnalyzed Level
SampleResult
QCResult
Reporting Limit Recov.Units Recov. Limits %
RPDLimit
RPD 1°/o Notcs*|
1060128-MS1 B106020-066/8/01 50.0
50.050.050.050.050.0150
50.050.050.050.0
NDND12.1NDNDNDND
41.855.649.244.650.235.8151
50.650.351.950.9
ug/l 42.5-12870.1-13953.5-10610.0-41710.0-23937.4-11370.8-1119 1.1-1 II85.1-10495.1-10589.6-105
83.6111
74.289.2100
71.6101101101104102
1060128-MSD1 B106020-066/8/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
59.937.044.950.643.860.834.834.339.048.046.240.032.334.546.332.442.734.042.639.643.037.558.640.152.7
ug/l 10.0-26971.4-11565.3-13454.6-13210.0-17610.0-20123.4-14326.3-13377.4-10872.8-11710.0-29370.8-12461.3-10963.3-11454.5-13736.1-11564.8-12954.7-11377.8-11467.3-11757.3-12468.3-11110.0-22545.6-15010.0-20S
"Refer to end of report
12074.089.8101
87.6122
69.668.678.096.092.480.064.669.092.664.885.468.085.279.286.075.0117
80.2105
for text
73.819.115.636.245.761.623.626.212.223.936.910.620.112.727.223.019.617.416.415.726.313.558.311.469.7
of notes
8.7017.711.711.2
0.22916.920.615.124.713.630.014.614.115.06.6816.41S.717.713.416.712.224.216.313.3
0
and definitions
Page 1 3 of 2 1
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 5/31/01Received: 6/1/01Reported: 6-13/0107:44
Volatile Organic Compounds by EPA Method 82608/Quality ControlGreat Lakes Analytical
AnalvteDateAnalyzed
SpikeLevel
SampleResult
QCResult Units
ReportingRecov.
LimitLimits
Recov. RPDLimit
RPDNotes*
Matrix Spike Pup (continued)Styrene1,1,2,2-TetrachloroethaneTetrach I oroeth en eToluene1,1,1 -Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1.2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
1060128-MSD1 B106020-066/8/01 50.0
50.050.050.050.050.050.050.050.050.0150
50.050.050.050.0
NDNDNDNDNDND12.1NDNDNDND
42.255.336.939.435.650.741.339.642.430.5119
50.349.951.250.7
ug/: 49.7-12620.6-22345.1-11371.3-118
42.5-12870.1-139
53.5-10610.0-41710.0-239
37.4-11370.8-11191. 1-11185.1-104
95.1-10589.6-105
84.411173.878.871.210158.479.284.861.079.310199.8102101
18.650.317.619.418.432.520.929.234.523.512.4
25.46.1119.121.716.09.4323.811.916.516.024.1
Array Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 14 of 2'
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
11JHygieneering, Inc.
75 75 Plaza CourtWillowbrook. IL 60521
11
1 Analyte
• Batch: 1060075Blank
IAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthracene
1Benzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) perylene
— Benzo (k) fluoranthene• Chrysene• Dibenz (a,h) anthracene
Fluoranthene
tFluoreneIndeno ( 1 ,2,3-cd) pyreneNaphthalenePhenanthrene
1PyreneSurrogate: Carbazole
§LCSAcenaphtheneAcenaphthyleneAnthracene
IBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluoranthene
— Benzo (ghi) perylene• Benzo (k) fluoranthene^Chrysene
Dibenz (a,h) anthracene
1FluorantheneFluoreneIndeno ( 1 ,2,3-cd) pyreneNaphthalene
1PhenanthrenePyreneSurrogate: Carbazole
I"Great Laka^ Analytical
1 /
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Polynuclear Aromatic Compounds byGreat Lakes
Date Spike SampleAnalyzed Level Result
Date Prepared: 6/6/011060075-BLK16/6/0111
11
"ii
""••11
""»""»
0.500
1060075-BS16/6/01 2.00
2.002.002.002.002.002.002.002.002.002.002.002.002.002.002.00
0.50(1
Sampled: 5/31/01Received: 6/1/01Reported: 6.13/01 07:44
EPA Method 8310/Quality ControlAnalytical
QCResult
Reporting LimitUnits Recov. Limits
Recov. RPD RPD% Limit % Notes"
Extraction Method: EPA3510C
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
0.423
.69
.732.10
.75
.74
.91
.96
.63
.84
.89
.68
.69
.76
.58
.881 .9(i
0.474
ug/l 5.005.005.00
0.1000.1000.100
5.000.100
1.000.1005.005.00
0.2005.005.005.00
24.5-122
ug/ l 23.9-10721.6-10124.8-10732.9-10023.5-11334.5-12635.7-97.542.9-11339.9-11031.3-92.536.1-10536.6-99.641.5-95.722.0-99.825.8-1153 1 . 5 - 1 1 224.5-122
84.6
84.586.5105
87.587.095.598.081.592.094.584.084.588.079.094.098.094.8
"Refer to end of report for text of notes and definitions.
Anay Johnson. Project Manager Page 15 of 2
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 5,31/01Received: 6,1/01Reported: 6/13/01 07:44
Polynuclear Aromatic Compounds by EPA Method 8310/Quality Control
Analvte
LCS PupAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) ttuorantheneChryseneDibenz (a,h) anthraceneFiuorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
Great Lakes Analytical
Date Spike Sample QCAnalyzed Level Result Result
1060075-BSD16/6/01 2.00 1.68
2.00 1.712.00 2.042.002.002.002.002.002.002.002.002.002.002.002.00
.74
.71
.87
.88
.66
.88
.841.06.71.72.59.92
2.00 2.06• • - - r - - Q500 Q408
Reporting LimitUnits Recov. Limits
ug/l 23.9-10721.6-10124.8-10732.9-10023.5-11334.5-126
35.7-97.542.9-11339.9-110
31.3-92.536.1-105
36.6-99.641.5-95.722.0-99.825.8-11531.5-11224.5-122
Recov.%
84.085.5102
87.085.593.594.083.094.092.0103
85.586.079.596.0103
81.6
RPDLimit
62.560.747.447.445.252.445.449.651.753.258.852.545.857.255.950.0
RPD% Notes*
0.5931.162.90
0.5731.742.124.171.822.152.6820.31.182.30
0.63 12.114.98
Great La/es Analytical
Andy Johnson, Project Manager
Refer to end of report for text of notes and definitions.
Page 16 of 21
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
I
JHygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 5/31-01Received: 6/1/01Reported: 6 13/01 07:44
Volatile Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical
^ Date Spike SamplelAnalyte Analyzed Level Result
• Batch: 1060123 Date Prepared: 6/7/01Blank 1060123-BLK1
IAcetone 6/7/01Benzene "Bromodichloromethane "Bromoform "
IBromomethane "2-Butanone "Carbon disulfide
— Carbon tetrachloride "• Chlorobenzene "WChlorodibromomethane "
Chloroethane "
1Chloroform "Chloromethane "1,1 -Dichloroethane "1 ,2-Dichloroethane "
11,1-Dichloroethene "cis-l,2-Dichloroethene "trans- 1,2-Dichloroethene "
11 ,2-Dichloropropane "cis-l,3-Dichloropropene "trans- 1 ,3-Dichloropropene "Ethylbenzene "
12-Hexanone "Methylene chloride "4-Methyl-2-pentanone "Styrene "
• 1,1 ,2,2-Tetrachloroethane "BlTetrachloroethene "
Toluene "
11,1,1-Tri chloroethane "1,1 ,2-Trichloroethane "TrichloroetheneTrichlorofluoromethane "
1Vinyl acetateVinyl chloride "Total Xylenes
1Surrogate: Dibromofluoromethane " 50.0
/Great Lakes/Analytical
QCResult
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
50.5
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*
Extraction Method: EPA 5035B [P/T1
ug/kg 25.05.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
HI. 2- 134 101
"Refer to end of report for text of notes and definitions.
IAndy Johnson, Project Manager
I
Page I 7 of 21
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.75 75 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 5,31/01Received: 6/1/01Reported: 6/13,01 07:44
Volatile Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical
Analvte
Blank (continued)Surrogate: 1 ,2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
LCSAcetoneBenzeneBromodichloromethane3romotbrmBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 , 1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethenecis-l,2-Dichloroethenetrans- 1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene1.1,1-Trichloroethane1 ,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane
Date Spike Sample QC Reporting Limit Recov. RPD RPDAnalyzed Level Result Result Units Recov. Limits % Limit % Notes'
1060123-BLK16/7/01 50.0
50.050.0
1060123-BS16/7/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0
48.3 ug/kg52.849.0
87.5 ug/kg55.657.254.257.759.564.358.956.353.688.055.457.154.656.655.756.855.657.257.660.555.860.048.761.855.752.059.360.25h.l57.957.561.8
50.8-14582.0-12176.8-113
10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-13460.0-13476.4-12561.8-13214.6-241
96.6106
98.0
1751 1 11141081151191291181131071761 1 11141091131 1 11141 1 1114115121112120
97.41241 1 11041 1 9120112116115124
Ajrfdy Johnson, Project Manager
"Refer to end of report for text of notes and definition:
Page 18 of 2
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email, [email protected](847) 808-7766 FAX (847) 808-7772
I1
1 Hygieneering, Inc.7575 Plaza Court
HWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 5/31,01Received: 6,1/01Reported: 6 1 3 - 0 1 07:44
• Volatile Organic Compounds by EPA Method 5035/8260B/Quality Control! Great Lakes Analytical
Analvte
LCS (continued)Vinyl acetate
IVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 . 2-Dichloroethane-d4
( Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
LCS Pup• Acetone• Benzene
Bromodichloromethane
tBromoformBromomethane2-ButanoneCarbon disulfide
1Carbon tetrachlorideChlorobenzeneChlorodibromomethane
1ChloroethaneChloroformChloromethane1 , 1 -Dichloroethane
11,2-Dichloroethane1 .1 -Dichloroethenecis-1 ,2-Dichloroethenetrans- 1 ,2-Dichloroethene
• 1 ,2-DichloropropaneBcis-1 ,3-Dichloropropene
trans- 1,3-Dichloropropene
IEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanone
ISrs'rene-1 ,1 ,2,2-TetrachloroethaneTetrach 1 oroeth en e
— Toluene
Date Spike Sample QC Reporting Limit Recov.Analyzed Level Result Result Units Recov. Limits %
1060123-BS16/7/01 50.0
50.0150
50.050.050.050.0
1060123-BSD16/8/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0
58.5 ug/kg52.5166
49.951.853.248.3
51.5 ug/kg53.253.551.867.957.165.153.852.450.6106
53.967.452.552.255.058.055.454.552.954.252.458.148.260.552.354.953.656.1
10.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-11*
10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-134
1171051 1 1
99.8104106
96.6
103106107104136114130108105101NR1081351051041101161 1 1109106108105116
96.41211051 1 01071 12
RPDLimi t
34541.442.057.461.9173126
43.539.041.690.343.571.841.868.647.539.343.038.141.557.242.7128
67.4119
37.254.646.342. fi
RPD% Notes*
51.84.616.333.7716.74.29
0.7728.857.345.7718.62.7416.93.748.29
0.9051.74
04.488.141 1 . 46.453.391 .032.455.565.6110.66.90
nalytical
Anay Johnson, Project Manager
I
"Refer to end of report for text of notes and definitions
Page 19 of 21
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.75 75 Plaza CourtWillowbrook, IL60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 5.31-01Received: 6-1 ,01Reported: 6-13, ( ) l 07:44
Volatile Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical
AnalvteDateAnalyzed
SpikeLevel
SampleResult
QCResult Units
ReportingRecov.
LimitLimits
Recov. RPDLimit
RPD/() Notes"
LCS Pup (continued)1,1,1 -Tri chloroethane1,1,2-TrichIoroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1,2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
1060123-BSD16/8/01 50.0
50.050.050.050.050.0150
50.050.050.050.0
54.155.256.173.257.563.6156
51.951.054.249.9
ug/kg 60.0-13476.4-12561.8-13214.6-24110.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-11*
10811011214611512710410410210899.8
44.253.243.511592.181.040.1
3.645.312.6416.31.7219.06.51
Great La/es Analytical
A'ridy Johnson. Project Manager
"Refer to end of report for text of notes and definitions.
Page 20 of 2
1•
1
11
| GREAT
•MEH'-"^" 1380 Busch Parkway•BflP ANALYTICAL Buffalo Grove. Illinois 60089
Hygieneering, Inc. Project:7575 Plaza Court Project Number:Willowbrook. IL 6052 1 Project Manager:
2001-3495N/AGary Milkeris
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Sampled: 5,31,01Received: 6 1 / 0 1Reported: 6/13/01 07:44
Notes and Definitions
# Note
(A
G12
IGIS
I02
rO4
i«I
DET
ND
>NR
dry
f Recov.
RPD
IIII
The concentration of the analyte detected in the sample is characteristic of a laboratory artifact.
The reporting limit of this sample/analyte is elevated due to sample matrix and/or other effects.
The relative percent difference (RPD) of one or more analytes in the matrix QC (MS/MSD) associated with this sample is above thelaboratory's established acceptance limits. Refer to the included QC reports for more detail.
The recovery of one or more analytes in the matrix QC (MS/MSD) associated with this sample is below the laboratory's establishedacceptance criteria. Refer to the included QC reports for more detail.
The recovery of one or more analytes in the laboratory control QC (BS/BSD) associated with this sample is above the laboratory^established acceptance criteria. Refer to the included QC reports for more detail.
The recovery for this analyte is below the laboratory's established acceptance criteria.
The recovery for this analyte is above the laboratory's established acceptance criteria.
Analyte DETECTED
Analyte NOT DETECTED at or above the reporting limit
Not Reported
Sample results reported on a dry weight basis
Recovery'
Relative Percent Difference
"Great Lake's Analytical
1 /—Atfclv Johnson. Project Manager
1
Page 21 of 21
LAKttiANALYTICAL
(847) 808-7766FAX (847) 808-777
(414) 570-9460FAX (414) 570-9461
TAT: (SID. \ 4 DAY 3 DAY 2 DAY 1 DAY < 24 HRSO YES - TAT is critical
D NO - TAT is not critical
TEMPERATURE UPON RECEIPT: OH OC£LSfafe <SProgram:
Deliverable Package Needed:D SID D Other
Project: bG\- 349-5T # of Soff/esPreservative Used
PO/Quote #: JOI - J- LABORATORYID NUMBERHELD /D, LOCATION
RELINQUISHED
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
IIII1II
July 26, 2001
Gary MilkerisHygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
RE: 2001 -3495
Dear Gary Milkeris
Enclosed are the results of analyses for sampie(s) received by the laboratory on July 13, 2001 . If you have anyquestions concerning this report, please feel free to contact me.
Sincerely
/Andy JohnsonProject Manager
_,«• GREATLAKES
[ANALYTICAL1380 Busch Parkway
Buffalo Grove, Illinois 60089Email: [email protected]
(847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.75 75 Plaza CourtWillowbrook, IL 60521
Sample Description
B32-3
B32-15
B34-5
B34-15
B35-6
B35-15
B36-3
B36-15
B37-6
B37-19
Project: 2001-3495Project Number: 200 1 -3495
Project Manager: Gary Milkeris
ANALYTICAL REPORT FOR
Laboratory Sample Number
B107171-01
B107171-02
B107171-03
B107171-04
B107171-05
B107171-06
B107171-07
B107171-08
B107171-09
B107171-IO
SAMPLES:
Sample Matrix
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Date Sampled
7/13/01
7/13/01
7/13/01
7/13/01
7/13/01
7/13/01
7/13/01
7/13/01
7/13/01
7/13/01
JGreat Lal#es Analytical
'?Andy Johnson, Project Manager
The results in tins report apply to the samples analyzed in accordance with the chain of custody docuniiThis analytical report must be reproduced in its enlir
Page 1 c
|
-^| GREAT•All LAKES•&•• ANALYTICAL•1
fHygieneering, Inc.7575 Plaza Court
• Willowbrook, IL 60521
*
Analyte
IMMAcenaphthene
«AcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyrene
1Benzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChrysene
• Dibenz (a,h) anthraceneV Fluoranthene
Fluorene
1Indeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePvrene
t _ . _ . . _Surrogate: Carbazole
B34-5
t AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthracene
1Benzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) perylene
, Benzo (k) fluoranthene
f ChryseneDibenz (a,h) anthraceneFluoranthene
1FluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrene
( PyreneSurrogate: Carbazole
I
1380 Busch ParkwayBuffalo Grove, I l l inois 60089 (847)
Project: 2001-3495Project Number: 200 1 -3495
Project Manager: Gary Milkeris
Polynuclear Aromatic Compounds by EPA Method 8310Great Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107171-011070317 7/17/01 7/21/01 100
200100100
90.0100100100100
90.01000
100100100100
1000~~" "" """""" 29.0-132
B107171-031070364 7/19/01 7/21/01 100
10001000
10090.0100100100100
90.010001000
100100
10001000
,29.0-132
Email: [email protected] FAX (847) 808-7772
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Result Units Notes"
Soil G_l1050 ug/kg831717
1430467767681299
1150623
3900 " G12682364ND737
9650 " G12165 % OS
SoilND ug/kg
1330 " G122000 " G121520
ND968929574
166011808600 " G I 21860 " G12
179ND
5320 " G1210500 " G12
78.2 %
' Great Lakes Analytical
Andy Johnson, Project Manager Page 2 of 3'
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Analyte
B34-15AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1 ,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
B35-6AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
\
Project: 2001-3495Project Number: 2001-3495
Project Manager. Gary Milkeris
Polynuclear Aromatic Compounds by EPA Method 8310Great Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107171-041070364 7/19/01 7/21/01 100
200100100
90.0100100100100
90.0100100100100100100
29.0-132
B107171-051070364 7/19/01 7/23/01 100
200100100
90.0100100100100
90.0100100100100100500
29.0-132
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Result Units Notes*
SoilND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
" "68.3 %
SoilND ug/kg386355NDNDNDNDNDNDND
1050415NDND380
2760 " G1260.5 %
Greit Lakes Analytical
\
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions
Page 3 of 2
|
«, | GREAT•ill LAKES
_ •&• ANALYTICAL•11
Hygieneering, Inc.— 7575 Plaza Court• Willowbrook, IL 60521
|Analvte
• B35-15Acenaphthene
1AcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyrene
1Benzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluoranthene
_ Chrysene• Dibenz (a,h) anthraceneB» Fluoranthene
Fluorene» Indeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyrene
B Surrogate: Carbazole
B36-3
1AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthracene
K Benzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) perylene
-^ Benzo (k) fluoranthene• Chrysene9 Dibenz (a,h) anthracene
Fluoranthene^ Fluorene• Indeno (1,2,3-cd) pyrene
NaphthalenePhenanthrene
1 Pyrene| Surrogate: Carbazole
1
1380 Busch ParkwayBuffalo Grove, I l l inois 60089 (847)
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Polynuclear Aromatic Compounds by EPA Method 8310Great Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107171-061070336 7/18/01 7/22/01 100
200100100
90.0100100100100
90.0100100100100100100
29.0-132
B107171-071070336 7/18/01 7/22/01 100
200100100
90.0100100100100
90.0100500100100100500
29.0-132
Email: [email protected] FAX (847) 808-7772
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Result Units Notes*
SoilND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
83. 1 %
SoilND ug/kg
1590801NDNDNDNDNDNDNDND788 " G 1 2NDND
13702040 " G I 283.0 %
Grekt Lakes Analytical
I
I
Andy\JoTinson, Project Manager
"Refer to end oj report for text of notes and definitions.
Page 4 of" 3 7
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Polynuclear Aromatic Compounds by EPA Method 8310Great Lakes Analytical
Analyte
B36-15AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1 ,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107171-081070336 7/18/01 7/26/01 100
200100100
90.0100100100100
90.0100100100100100100
29.0-132
Result Units Notes*
SoilND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
78.0 %
Great Lakes Analytical "Refer to end oj report for text of notes and definition
Andy Johnson, Project Manager Page 5 of
1111
-.-•GREAT•|!| LAKES•Bll ANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project:Project Number:
Project Manager:
2001-34952001-3495Garv Milkeris
Sampled:Received:Reported:
7/13/017/13/017/26/01 12:15
I
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
9 B32-3 B107171-01Acetone 1070359 7/17/01 7/19/01
fBenzene " " "Bromodichloromethane " " "Bromoform " " "Bromomethane " " "
f 2-Butanone " " "Carbon disultlde " " "Carbon tetrachloride " " "
» Chlorobenzene " " "Chlorodibromomethane " " "Chloroethane " " "Chloroform " " "
I Chloromethane " " "1,1 -Dichloroethane " " "1 ,2-Dichloroethane "1,1-Dichloroethene
M cis-l,2-Dichloroethene " " "^ trans- 1 ,2-Dichloroethene " " "
1,2-Dichloropropane " " "
§cis-l,3-Dichloropropene " " "trans- 1 ,3-Dichloropropene " " "Ethylbenzene " " "2-Hexanone " " "
f Methylene chloride " " "4-Methyl-2-pentanone " " "Styrene
^ 1,1,2,2-Tetrachloroethane " " "• Tetrachloroethene " " "V Toluene " " "
1,1,1-Trichloroethane " " "
t l,l,2-Trichloroethane " " "Trichloroethene " " "Trichlorofluoromethane " " "Vinyl acetate "
• Vinyl chloride " " "|| Total Xylenes
Surrogate: Dibromofluoromethane " " " 81.2-134
« Surrogate: 1.2-Dichloroelhane-d4 " " " 50.8-145
. Greit Lakes Analytical
25.05.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
"Refer to end i
Soil G19.G3.G^89.1 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND108 %153 " 05
fjf report for text of notes and definitions.
Andj| Johnson. Project Manager Page 6 of 37
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
B32-3 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
AnalyteBatchNumber
DatePrepared
DateAnalyzed
SurrogateLimits
ReportingLimit Result Units Notes'
B107171-01 Soil G19.G3.C1070359 7/17/01 7/19/01 82.0-121
76.8-113~10385.2
Great Lakes Analytical
Andy Johnson, Project Manager
"Refer to end of report for text of notes and dcfinitio,
Page 7 of
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
1I
Hygieneering, Inc.75 75 Plaza Court
1 Willowbrook, IL 60521
P
•
Analvte
E B32-1SAcetone
_ BenzeneB Bromodichloromethane™ Bromoform
Bromomethane
K 2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzene
|c.hlorodibromomethaneChloroethaneChloroform
I Chloromethane1,1 -Dichloroethane1 ,2 -Dichloroethane1,1-Dichloroethene
I cis-1 ,2-Dichloroethenetrans- 1 ,2-Dichloroethene1 ,2-Dichloropropane
^ cis-1, 3-Dichloropropene• trans-1 ,3-Dichloropropene™ Ethylbenzene
2-Hexanone
I Methylene chloride
4-Methyl-2-pentanoneStyrene1,1,2,2-Tetrachloroethane
I Tetrachloroethenef Toluene
1,1,1 -Trichloroethane
» 1 ,1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetate
t Vinyl chloride•• Total Xylenes
Surrogate: Dibromofluoromethaneg Surrogate: 1.2-Dichloroethane-d4
Project: 2001-3495Project Number: 200 1 -3495
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107171-021070359 7/17/01 7/19/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-13450.8-145
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Result Units Notes*
Soil G19.G3.G452.7 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
5.27 " ANDNDNDNDNDNDNDNDNDNDNDND112 "/„140
"Refer to end of report for text of notes and definitions
IAndy JMinson, Project Manager Page8 of 3 7
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL60521
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
AnalvteBatchNumber
DatePrepared
DateAnalyzed
SurrogateLimits
ReportingLimit Result Units Notes*
B32-15 (continued^Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
6107171-02^1070359 7/17/01 " 7/79/07:" " " 82.0-121
76.8-113
Soil G19.G3.G-"99.3 %71.1 " O4
GreatiLakes Analytical
KAndy Johnson, Project Manager
"Refer to end of report for text of notes and definitioi
Page 9 ol
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
11
Hygieneering, Inc._ 7575 Plaza Court• Willowbrook. IL 60521f
|Analvte
1 834^5Acetone
1BenzeneBromodichloromethaneBromoformBromomethane» 2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzene
• Chlorodibromomethane™ Chloroethane
Chloroform
IChloromethane1,1 -Dichloroethane
- 1 ,2-Dichloroethane1,1-Dichloroethene
• cis-1 ,2-Dichloroethene| trans- 1 ,2-Dichloroethene
1 ,2-Dichloropropane
§cis-1 ,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-Hexanone
f Methylene chloride4-M ethyl -2-pentanoneStyrene1 ,1 ,2,2-Tetrachloroethane
• TetrachloroetheneR Toluene
1,1,1 -Tri chloroethane
11 , 1 ,2-Tri ch 1 oroethaneTrichloroetheneTrichlorofluoromethane
. . V i n y l acetateB Vinyl chloride• Total Xylenes
Surrogate: Dibromofluoromethane— Surrogate: l.2-Dichloroelhane-d4
• 1
Project: 2001-3495Project Number: 2001-3495Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107171-031070359 7/17/01 7/19/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.00
" " " 10.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-13450.8-145
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Result Units Notes*
Soil G19.G3.G4102 ug/kg ANDNDNDND
12.8 " ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND107 %149 " OS
'Great Lpkes Analytical
IAndy Johnson, Project Manager
"Refer to end of report lor text of notes and definitions
Page 10 of 37
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: 2001 -3495
Project Manager: Gary Milkeris
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
AnalvteBatchNumber
DatePrepared
DateAnalyzed
SurrogateLimits
ReportingLimit Result Units Notes*
B34-5 (continued^Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
1070359 7/17/01Bl07171-03
"7/79/0; 82.0-12776.8-113
Soil105 %
76.3
G19.G3.G
O4
tlfeGreat Lpkes Analytical "Refer to end of report for text of notes and definitions
\
Andy Johnson, Project Manager Page 1 1 of 3
I "—- - H G R EATF|Sl LAKES•fill ANALYTICAL
•1
|Hygieneering, Inc.7575 Plaza Court
f willowbrook, IL 60521
mI
1| Analyte
JB34-15Acetone
_ Benzene• Bromodichloromethane^ Bromoform
Bromomethane
12-ButanoneCarbon disulfideCarbon tetrachloride
. Chlorobenzene
IchlorodibromomethaneChloroethaneChloroform
tChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethene
1cis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis- 1 ,3-Dichloropropene
• trans-1 ,3-Dichloropropene™Ethylbenzene
2-Hexanone
fMethylene chloride4-Methyl-2-pentanoneStyrene1 ,1 ,2,2-Tetrachloroethane
ITetrach 1 oroeth eneToluene1,1,1 -Trichloroethane
§1 ,1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetate
§Vinyl chlorideTotal XylenesSurrogate: Dibromofluoromethane
^Surrogate: 1 . 2-Dichloroethane-d4
1380 Busch ParkwayBuffalo Grove, I l l inois 60089 (847)
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107171-041070359 7/17/01 7/19/01 25.0
5.005.005.005.001 0.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-13450.8-145
Email: [email protected] FAX (847) 808-7772
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Result Units Notes*
Soil G19.G3.G479.3 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
5.60 " ANDNDNDNDNDNDNDNDNDNDNDND115 %144
Grea Lakes Analytical
i\Andyl Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 12 of 37
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: 200 1 -3495
Project Manager: Gary Milkens
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
AnalvteBatchNumber
DatePrepared
DateAnalyzed
SurrogateLimits
ReportingLimit Result Units Notes*
B34-15 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
1070359 7/17/01B107171-04
'7/19/01 ~~~ 8'2.0-lYr76.8-113
Soil94.071.7
G19.G3.G
04
IGreat Likes Analytical
Andy Jdhnson, Project Manager
"Refer to end of report for text of notes and definition.
Page 13 of!
I ^.^B GREAT'KM LAKES•&• ANALYTICAL
1Hygieneering, Inc.
_ 7575 Plaza Court• Willowbrook, IL 60521P
. Analyte
• B35-6Acetone
1BenzeneBromodichloromethane
_ BromoformBromomethane
I 2-ButanoneCarbon disultldeCarbon tetrachloride
^ ChlorobenzeneH Chlorodibromomethane9 Chloroethane
Chloroform
IChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethene
• cis-1 ,2-Dichloroethenejj trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
§cis-1 ,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-Hexanone
tMethylene chloride4-Methyl-2-pentanoneStyrene1,1,2,2-Tetrachloroethane
• Tetrachloroethene••Toluene
1,1,1 -Tri chloroethane
11 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetate
f Vinyl chlorideTotal XylenesSurrogate: Dibromofluoromethane
— Surrogate: 1 .2-Dichloroethane-d4
1380 Busch ParkwayBuffalo Grove, I l l inois 60089 (847)
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107171-051070359 7/17/01 7/19/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-13450.8-145
Email: [email protected] FAX (847) 808-7772
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Result Units Notes*
Soil G19.G3.G470.6 ug/kg ' ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
5.06 " ANDNDNDNDNDNDNDNDNDNDNDND107 %148 " O5
Gredt Lakes Analytical
II
red
Andy Jonnson, Project Manager
"Refer to end of report for text of notes and definition.',.
Page 14 of 37
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
AnalyteBatchNumber
DatePrepared
DateAnalyzed
SurrogateLimits
ReportingLimit Result Units Notes"
B35-6 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
1070359 7/17/01_B107171-05
~~7/19/6T~ '82.0-12176.8-113
Soil G19.G3.G705 %
91.0
Great Lakes Analytical "Refer to end of report for text of notes and definition.
Andy Johnson, Project Manager Page 15 of.
|
~..,| GREATyam LAKES•&•• ANALYTICAL•1
1Hygieneering, Inc.
|7575 Plaza CourtBwillowbrook.IL 60521
'
Analyte
B35-15Acetone
— Benzene•Bromodichloromethane^Bromoform
Bromomethane
I2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzene
IchlorodibromomethaneChloroethaneChloroform
fChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethene
>cis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropene
• trans-1 ,3-Dichloropropene^Ethylbenzene
2-Hexanone
IMethylene chloride4-Methyl-2-pentanoneStyrene1 ,1 ,2,2-Tetrachloroethane
ITetrachloroetheneToluene1,1,1 -Tri chloroethane
11 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetate»Vinyl chlorideTotal Xylenes
• - -- - • - - . . . _ . . . . _ _ .
Surrogate: DibromofluoromelhaneSurrogate: 1 . 2-Dichloroelhane-d4
I 1
1380 Busch ParkwayBuffalo Grove, I l l inois 60089 (847)
Project: 2001-3495Project Number: 2001-3495
Project Manager: Garv Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107171-061070359 7/18/01 7/19/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
" " " 81.2-13450.8-145
Email: [email protected] FAX (847) 808-7772
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Result Units Notes*
Soil G19.G3.G452.4 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
5.25 " ANDNDNDNDNDNDNDNDNDNDNDND102 %136
Lakes Analytical
IAndyUohnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 16 of 37
I
ilGREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Analvte
B35-15 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
Project: 2001-3495Project Number: 2001-3495Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107171-06;070359 7/18/01 7/19/01 82.0-121
76.8-113
Sampled:Received:Reported:
Result
96.975.7
7/13/017/13/017/26/01
Units
Soil%
12:15
Notes"
G19.G3.G
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definition.
Page 17 of'.'
I ^.^B GREAT•ill LAKES
_ iSmm ANALYTICAL•1I
Hygieneering, Inc.7575 Plaza Court
• Willowbrook, IL 60521
9
Analyte
B360Acetone
_ Benzene• Bromodichloromethane9 Bromoform
Bromomethane
t 2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzene
• Chlorodibromomethane• Chloroethane
Chloroform
IChloromethane1 , 1 -Dichloroethane
- 1 ,2-Dichloroethane1,1-Dichloroethene
1cis- 1 ,2-Dichloroethenetrans- 1 ,2-Dichloroethene1 ,2-Dichloropropane
_ cis-1 ,3-Dichloropropene•trans- 1 ,3-Dichloropropene9 Ethylbenzene
2-Hexanone
1Methylene chloride4-M ethyl-2-pentanoneStyrene1 , 1 ,2,2-Tetrachloroethane
ITetrachloroetheneToluene1,1,1 -Trichloroethane
11 , 1 .2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetate
§Vinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: l.2-Dichloroethane-d4
I
1380 Busch ParkwayBuffalo Grove, I l l inois 60089 (847)
Project: 2001-3495Project Number: 200 1 -3495
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107171-071070359 7/18/01 7/19/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.00
" ' " 5.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-13450.8-145
Email: [email protected] FAX (847) 808-7772
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Result Units Notes*G19.G3.G4.
Soil O2.O3172 ug/kg ANDNDNDND17J " ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
7.08 " ANDNDNDNDNDNDNDNDNDNDNDND121 %150 " O5
Great -akes Analytical
IAndyWohnson, Project Manager
"Refer to end of report for text of notes and definitions
Page 18 of 37
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.75 75 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Analyte
B36-3 (continued)
BatchNumber
DatePrepared
DateAnalyzed
SurrogateLimits
ReportingLimit
B107171-07
Result Units
SoilG19.G302.03
Notes*.G4.
Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
1070359 7/18/01 7/19/01 82.0-12176.8-113
90.3 %37.9 " O4
Groat Lakes Analytical "Refer to end of report for text of notes, and definitions
Andy Sofmson, Project Manager Page 19 of 3
I »*£*M GREAT•All LAKES•Ell ANALYTICAL•1
11 Hygieneering, Inc.
J 7575 Plaza CourtMl Willowbrook. IL 60521i
M
1
H1 Analyte
PB36-15Acetone
»BenzeneBromodichloromethaneBromoformBromomethane
12-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzene
• Chlorodibromomethane• Chloroethane
Chloroform
IChloromethane1 , 1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethene
1cis- 1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropane
_ cis-l,3-DichloropropeneM trans- 1,3-Dichloropropene9 Ethylbenzene
2-Hexanone
1Methylene chloride4-Methyl-2-pentanoneStyrene1 ,1 ,2,2-Tetrachloroethane
I TetrachloroetheneToluene1,1,1-Trichloroethane
11 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetate
1Vinyl chlorideTotal XylenesSurrogate: Dibromofluoromethane
^ Surrogate: 1.2-Dichloroethane-d4
I• GreatjLakes Analytical
1 1 _
1380 Busch ParkwayBuffalo Grove, I l l inois 60089 (847)
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107171-081070359 7/18/01 7/19/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-13450.8-145
Email: [email protected] FAX (847) 808-7772
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Result Units Notes*
Soil G19.G3.G460.2 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
5.17 " ANDNDNDNDNDNDNDNDNDNDNDND112 %137
"Refer to end of report for text of notes and definitions.
Andy Vohrrson, Project Manager Page 20 of 3 7
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495 Sampled: 7/13/01Project Number: 2001-3495 Received: 7/13/01
Project Manager: Gary Milkeris Reported: 7/26/01 12:15
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Analvte
B36-15 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzet
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units Notes'
B107171-08 Soil G19.G3.G;070159 7/18/01 7/19/01 82.0-121 96.3 %
le " " " 76.8-113 74.7 " O4
Great Lakes Analytical "Refer to end of report for text of notes and definition.
A^ndy Johnson, Project Manager Page 21 of.'
LAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
1I
Hygieneering, Inc.7575 Plaza Court
• Willowbrook, IL 60521
Analyte
•m^6Acetone
_ Benzene• Bromodichloromethane• Bromoform
Bromomethane
12-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzene
• Chlorodibromomethane• Chloroethane
Chloroform
I Chloromethane1,1-Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethene
1cis-1, 2-Dichloroethenetrans-1, 2-Dichloroethene1 ,2-Dichloropropane
— cis- 1 ,3-Dichloropropene• trans- 1 ,3-Dichloropropene9 Ethylbenzene
2-Hexanone
1Methylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-Tetrachloroethane
§TetrachloroetheneToluene1,1,1-Trichloroethane
11 ,1 ,2-TrichloroethaneTrichloroetheneTrichlorotluoromethaneVinyl acetate
1Vinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 ,2-Dichloroethane-d4
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107171-091070359 7/18/01 7/19/01 25.0
5.005.005.005.00
7/21/01 10.07/19/01 5.00
5.005.005.005.005.005.005.005.005.00
7/21/01 2507/19/01 5.00
5.005.005.005.0010.05.0010.05.005.005.005.005.005.00
7/21/01 25007/19/01 5.00
10.07/21/01 5.007/19/01 5.00
81.2-13450.8-145
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Result Units Notes*
Soil G19.G3.G82.6 ug/kg ANDNDNDNDNDNDNDNDNDND880 " END208ND
64.82330 " G12
203NDNDNDNDND
6.84 " ANDNDND
17.2ND11.1ND
8230 " G12NDND523 " END107 "/„151 " O5
I Grdat Lakes Analytical
And_y'Johnson, Project Manager
Refer to end of report for text of notes and definitions
Page 22 of 3
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Sampled: 7/13/01Received: 7/13/01 ,Reported: 7/26/01 12:15 1
B37-6 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
AnalvteBatchNumber
DatePrepared
DateAnalyzed
SurrogateLimits
ReportingLimit Result Units Notes*
1070359 7/18/01B107171-09
"7/7 9/07" 82.0-12176.8-113
Soil79.880.6
G19,G3.G4O4
Great Lakes Analytical "Refer to end of report for text of notes and definitions
Andy Johnson. Project Manager Page 23 of 3'
I ^.^B GREATf|5| LAKES
_ •&• ANALYTICAL•11
Hygieneering, Inc._ 7575 Plaza CourtBlWillowbrook, IL 60521
•
1i1 Analyte
• B37-19Acetone
•
BenzeneBromodichloromethaneBromoformBromomethane
12-ButanoneCarbon disulfideCarbon tetrachloride
_ ChlorobenzeneI Chlorodibromomethane9 Chloroethane
Chloroform
IChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1 ,1 -Dichloroethene»cis-1, 2-Dichloroethenetrans-1, 2-Dichloroethene1 ,2-Dichloropropane
|
Cis-l,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-Hexanone
§Methylene chloride4-Methyl-2-pentanoneStyrene1,1,2,2-Tetrachloroethane
• Tetrachloroethene• Toluene
1,1,1 -Trichloroethane
11 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorotluoromethaneVinyl acetate
1Vinyl chlorideTotal XylenesSurrogate: Dibromofluoromethane
_ Surrogate: 1.2-Dichloroethane-d4
1380 Busch ParkwayBuffalo Grove, Illinois 60089 (847)
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107171-101070359 7/18/01 7/19/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.00
7/23/01 5.007/19/01 5.00
10.05.0010.05.005.005.005.00
7/23/01 5.007/19/01 5.007/23/01 50007/19/01 5.00
10.05.005.00
81.2-13450.8-145
Email: [email protected] FAX (847) 808-7772
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Result Units Notes*
Soil G19.G3.G454J ug/kg ANDNDNDNDNDNDNDNDNDND
30.7NDNDNDND198
9.06NDNDNDNDND
19.7 " ANDNDNDNDNDNDND
71100 " G12NDND
6.02ND115 %159 " 05
' Great Lakps Analytical
I
I
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 24 of 3 7
I•III
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Analyte
B37-19 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA MethodGreat Lakes Analytical
Batch Date Date SurrogateNumber Prepared Analyzed Limits
B107171-101070359 7/18/01 7/19/01 82.0-121
76.8-113
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
5035/8260B
ReportingLimit Result Units Notes*
Soil G19.G3.G496. 6 %74. 1 " O4
4-Great Lakes Analytical "Refer to end of report for text of notes and definitions
Andy Johnson, Project Manager Page 25 of 3
I ^.^B GREATSASII LAKES• •B 1380 Busch Parkwayk^H ANALYTICAL Buffalo Grove, I l l inois 60089
1Hygieneering, Inc. Project:
17575 Plaza Court Project Number:Willowbrook, IL 60521 Project Manager:
Dry
2001-34952001-3495Gary Milkeris
Weight Determination
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
1 Great Lakes Analytical
1Sample Name Lab ID
B32-3 B107171-01
• B32-15 B107171-02
B34-5 B 1071 71 -03
BB34-15 B107171-04
B35-6 B107171-05
JB35-15 B107171-06
B36-3 B107171-07
• B36-15 B107171-08
I B37-6 B1071 71-09
B37-19 B107171-10
1
1
1
1
Matrix
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Result Units
73.7 %
77.5 %
75.8 %
84.2 %
83.1 %
79.6 %
70.1 %
82.0 %
87.7 %
83.5 %
II
Great Lqkes Analytical
1 i\ _Andy Johnson, Project Manager
1
Page 26 of 3
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: 2001 -3495
Project Manager: Gary Milkeris
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Polynuclear Aromatic Compounds by EPA Method 8310/Quality ControlGreat Lakes Analytical
Analyte
Batch: 1070317BlankAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
Date Spike SampleAnalyzed Level Result
Date Prepared: 7/17/011070317-BLKl7/22/01II
"
M
"
11
ii
"
n
11
11
"
11
11
n
n
"" ~" " 16.5
QCResult
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
11.4
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes
Extraction Method: EPA 3550B
ug/kg 100200100100
90.0100100100100
90.0100100100100100100
29.0-132 69.1
LCSAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
1070317-BS17/22/01 67.7
67.767.767.767.767.767.767.767.767.767.7
67.767.767.767.767.716.9
65.899.352.657.847.757.361.160.260.755.758.559.857.453.359.865.215.8
ug/kg 30.8-12038.9-15832.9-12240.5-12531.2-12845.0-13238.7-13753.4-12546.5-12942.8-13437.1-11640.8-10851.0-11522.7-11629.5-12344.5-11829.0-132
97.2147
77.785.470.584.690.388.989.782.386.488.384.878.788.396.393.5
Grebt Lakes Analytical
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definition.
Page 27 of'.'
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
IHygieneering, Inc.
_ 7575 Plaza Court| Willowbrook, IL 60521
•
Analyte
Matrix SpikeAcenaphthene
1AcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyrene
1Benzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluoranthene
_ Chrysene• Dibenz (a,h) anthracene9 Fluoranthene
Fluorene
1Indeno (1 ,2,3-cd) pyreneNaphthalenePhenanthrenePyrene
H Surrogate: Carbazole
Matrix Spike DUD
1AcenaphtheneAcenaphthyleneAnthraceneBenz fa) anthracene
1Benzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) perylene
^ Benzo (k) fluoranthene• Chrysene• Dibenz (a,h) anthracene
Fluoranthene
1FluoreneIndeno (1 ,2,3-cd) pyreneNaphthalenePhenanthrene
1PyreneSurrogate: Carbazole
1
Project: 2001-3495Project Number: 200 1 -3495
Project Manager: Gary Milkeris
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Polynuclear Aromatic Compounds by EPA Method 8310/Quality ControlGreat Lakes Analytical
Date SpikeAnalyzed Level
SampleResult
QC Reporting Limit Recov.Result Units Recov. Limits %
RPDLimit
RPD% Note
1070317-MS1 B107145-057/22/01 65.9
65.965.965.965.965.965.965.965.965.965.965.965.965.965.965.916.5
1070317-MSD17/22/01 68.4
68.468.468.468.468.468.468.468.468.468.468.468.468.468.468.417.1
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
B107145-05NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
76.3 ug/kg139
57.760.650.556.359.456.860.853.665.564.154.277.564.965.531.7
55.2 ug/kg83.743.644.335.442.843.743.346.741.247.949.842.955.449.448.012.4
10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145
29.0-132
10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145
29.0-132
116NR
87.692.076.685.490.186.292.381.399.497J82.2118
98.599.4192
80.7122
63.764.851.862.663.963J68.360.270.072.862.781.072.270.272.5
66.465.767.157.854.551.965.959.365.249.858.753.955.862.557.456.6
35.953.531.634.738.630.834.030.629.929.834.728.826.937.230.834.4
Gre^t Lakes Analytical
I
I
Johnson, Project Manager
Refer to end of report for text of notes and definitions
Page 28 of 3
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Polynuclear Aromatic Compounds by EPA Method 8310/Quality ControlGreat Lakes Analytical
LCSAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
Analyte
Batch: 1070336BlankAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1 ,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
Date Spike SampleAnalyzed Level Result
Date Prepared: 7/18/011070336-BLK17/21/0111
it"""11
11
n11
""it11
"n
16.6
QCResult
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
"15.8
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*
Extraction Method: EPA 3550B
ug/kg 100200100100
90.0100100100100
90.0100100100100100100
29.0-132 95.2
1070336-BS17/21/01 67.7
67.767.767.767.767.767.767.767.767.767.767.767.767.767.767.716.9
58.177.355.758.953.356.864.457.159.658.360.954.559.553.655.959.217.4
ug/kg 30.8-12038.9-15832.9-12240.5-12531.2-12845.0-13238.7-13753.4-12546.5-12942.8-13437.1-11640.8-10851.0-11522.7-11629.5-12344.5-11829.0-132
85.8114
82.387.078:7
83.995.184.388.086.190.080.587.979.282.687.4103
Great Lalfes Analytical "Refer to end of report for text of notes and definitions
Andy Johnkm^xProject Manager Page 29 of" '•
I GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
11
Hygieneering, Inc.7575 Plaza Court| Willowbrook, IL 60521
•
Analyte
Matrix SpikeAcenaphthene
1AcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyrene
1Benzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluoranthene
_ Chrysene• Dibenz (a,h) anthracene• Fluoranthene
Fluorene
1Indeno (1 ,2,3-cd) pyreneNaphthalenePhenanthrenePyrene
• Surrogate: Carbazole
Matrix Spike DUD
1AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthracene
1Benzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluoranthene
I Chrysene9 Dibenz (a,h) anthracene
Fluoranthene
1FluoreneIndeno ( 1 ,2,3-cd) pyreneNaphthalenePhenanthrene
I PvreneSurrogate: Carbazole
1
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Polynuclear Aromatic Compounds by EPA Method 8310/Quality ControlGreat Lakes Analytical
Date SpikeAnalyzed Level
SampleResult
QCResult
Reporting LimitUnits Recov. Limits
Recov.%
RPDLimit
RPD% Notes
1070336-MS1 B107171-067/21/01 66.4
66.466.466.466.466.466.466.466.466.466.466.466.466.466.466.416.6
1070336-MSD17/19/01 67.2
67.267.267.267.267.267.267.267.267.267.267.267.267.267.267.216.8
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
B107171-06NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
39.780.049.150.548.849.853.249.452.848.452.646.851.759.450.051.412.3
57.669.246.547.440.752.340.143.046.236.047.843.041.365.649.956.617.4
ug/kg 10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145
29.0-132
ug/kg 10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145
29.0-132
59.8120
73.976.173.575.080.174.479.572.979.270.577.989.575377.474.1
85.7103
69.270.560.677.859.764.068.853.671.164.061.597.674.384.2104
66.465.767.157.854.551.965.959.365.249.858.753.955.862.557.456.6
35.615.26.577.6419.23.6629.215.014.430.510.89.6723.58.661.348.42
II
Andy Johrrsfjn, Project Manager
"Refer to end of report for text of notes and definitions
Page 3 Oof 3 7
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Polynuclear Aromatic Compounds by EPA Method 8310/Quality ControlGreat Lakes Analytical
LCSAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
Analyte
Batch: 1070364BlankAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1 ,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
Date Spike Sample QCAnalyzed Level Result Result
Date Prepared: 7/19/011070364-BLK17/24/01 ND
NDNDNDNDNDNDNDNDNDNDNDNDNDNDND
" 16.5 "13.6
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*
Extraction Method: EPA 3550B
ug/kg 100200100100
90.0 !100100100100
90.0100100100100100100
29.0-132 82.4 \
1070364-BS17/24/01 65.9
65.965.965.965.965.965.965.965.965.965.965.965.965.965.965.9
16.5
49.463.343.446.543.247.451.048.249.749.345.645.246.640.545.646.911.0
ug/kg 30.8-12038.9-15832.9-12240.5-12531.2-12845.0-13238.7-13753.4-12546.5-12942.8-13437.1-11640.8-10851.0-11522.7-11629.5-12344.5-11829.0-132
75.096.165.970.665.671.9
77.473.175.474.869.268.670.761.569.271.266.7
Great Lakes Analytical "Refer to end of report for text of notes and definitions.
Andy Johnson, Project Manager Page 31 of 3'
I GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
11
Hygieneering, Inc._ 7575 Plaza Court| Willowbrook, IL 60521
•
|Analyte
| Matrix SpikeAcenaphthene
1AcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyrene
1Benzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluoranthene
_ Chrysene• Dibenz (a,h) anthraceneB Fluoranthene
Fluorene
1 Indeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyrene
• Surrogate: Carbazole
Matrix Spike DUD
1AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthracene
1Benzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluoranthene
• Chrysene• Dibenz (a,h) anthracene
Fluoranthene
1FluoreneIndeno ( 1 ,2,3-cd) pyreneNaphthalenePhenanthrene
1 PyreneSurrogate: Carbazole
1
Project: 2001-3495Project Number: 200 1 -3495
Project Manager: Gary Milkeris
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Polynuclear Aromatic Compounds by EPA Method 8310/Quality ControlGreat Lakes Analytical
Date SpikeAnalyzed Level
SampleResult
QC Reporting Limit Recov.Result Units Recov. Limits %
RPDLimit
RPD% Notes"
1070364-MS1 B107171-047/24/01 67.0
67.067.067.067.067.067.067.067.067.067.067.067.067.067.067.016.8
1070364-MSD17/24/01 67.6
67.667.667.667.667.667.667.667.667.667.667.667.667.667.667.616.9
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
B107171-04NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
44.2 ug/kg62.043.447.642.847.448.646.550.545.268.244.544.447.649.667.11 1.0
38.0 ug/kg76.444.446.343.046.952.043.553.246.966.144.344.548.548.769.310.1
10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145
29.0-132
10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145
29.0-132
66.092.564.871.063.970.772.569.475.467.5102
66.466371.074.0100
65.5
56.2113
65.768.563.669.476.964.378.769.497.865.565.871.772.0103
59.8
66.465.767.157.854.551.965.959.365.249.858.753.955.862.557.456.6
16.020.01.383.58
0.4711.865.897.634.282.784.201.36
0.7570.981
2.742.96
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 3 2 of 3 7
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Volatile Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical
Analyte
Batch: 1070359BlankAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 , 1 -Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethenecis- 1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-M ethy 1-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrach 1 oroethen eToluene1,1,1-Trichloroethane1 ,1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: Dibromofluoromethane
Date Spike Sample QCAnalyzed Level Result Result
Date Prepared: 7/18/011070359-BLK17/19/01 59.0
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
7.47NDNDNDNDNDNDNDNDNDNDNDND
50.0 54.0
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes"
Extraction Method: EPA 5035B 1P/T1
ug/kg 25.05.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-134 108
GreathLakes Analytical "Refer to end of report for text of notes and definitions.
\
Andy Johnson, Project Manager Page 3 3 of 3 7
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: 2001 -3495
Project Manager: Ganr Milkeris
Sampled: 7/13/01Received: 7/13/01Reported: 7/26/01 12:15
Volatile Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical
V1 Analyte
H Blank (continued)Surrogate: 1 , 2-Dich/oroethane-d4
1Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
LCS
1AcetoneBenzeneBromodichloromethaneBromoform
• Bromomethane• 2-Butanone
Carbon disulfide
1Carbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethane
1ChloroformChloromethane1,1 -Dichloroethane
11 ,2-Dichloroethane1,1-Dichloroethenecis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene
11 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene
12-HexanoneMethylene chloride4-Methyl-2-pentanone
IStyrene1.1 ,2,2-TetrachloroethaneTetrach 1 oroeth en eToluene
11,1,1-Trichloroethane1 , 1 ,2-TrichloroethaneTrichloroethene
_ Trichlorofluoromethane
Date Spike Sample QC Reporting Limit Recov. RPD RPDAnalyzed Level Result Result Units Recov. Limits % Limit % Notes-
1070359-BLK17/19/01 50.0
50.050.0
1070359-BS17/18/01 50.0
50.050.0
. " 50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0
68.9 ug/kg54.348.8
\ 1 0 ug/kg45.349.339.5171
55.638.840.639.641.858.945.832.743.851.242.943.940.049.150.656.440.964.345.660.741.153.137.242.944.748.144.1
191
50.8-14582.0-12176.8-113
10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-13460.0-13476.4-12561.8-13214.6-241
138109
97.6
NR90.698.679.0NR1 1 1
77.681.279.283.6118
91.665.487.6102
85.887.880.098.2101113
81.8129
91.2121
82.2106
74.485.889.496.288.2NR
Great Lakes Anjifytical
II
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 34 of 3 7
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
*!
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Sampled: Ii \ 3/0 1Received: 7/13/01Reported: 7/26/01 12:15
Volatile Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical
Analyte
LCS (continued)Vinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 , 2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
LCS PupAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethenecis-1 ,2-Dichloroethenetrans- 1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-M ethyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene
Date Spike SampleAnalyzed Level Result
1070359-BS17/18/01 50.0
50.0150
50.050.050.050.0
1070359-BSD17/19/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0
QC Reporting LimitResult Units
5 1 .4 ug/kg56.8203
44.055.245.441.5
1 34 ug/kg47.748.539.269.453.351.437.039.041.144.450.624.351.851.650.349.443.751.248.354.940.464.355.461.442.650.334.442.9
Recov. Limits
10.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113
10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-134
Recov.%
103114135
88.0110
90.883.0
NR95.497.078.4139107103
74.078.082.288.8101
48.6104103101
98.887.4102
96.6110
80.81291 1 1123
85.2101
68.885.8
RPDLimit
34541.442.057.461.9•173126
43.539.041.690.343.571.841.868.647.539.343.038.141.557.242.7128
67.4119
37.254.646.342.6
RPD% Notes*
19.75.161.64
0.76284.43.6728.19.281.531.6928.29.7629.517.1
0.97616.311.88.843.804.452.691.23
019.61.643.584.837.82
0
Great Lakes Analytical7
"Refer to end of report for text of notes and definitions
AndyjJohnson, Project Manager Page 35 of 3
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
IHygieneering, Inc.75 75 Plaza CourtWillowbrook, IL 60521
Project:Project Number:
Project Manager:
2001-34952001-3495Gary Milkeris
Sampled:Received:Reported:
7/13/017/13/017/26/01 12:15
IVolatile Organic Compounds by EPA Method 5035/8260B/Quality Control
Great Lakes Analytical
1Analyte
LCS Pup (continued)
DateAnalyzed
SpikeLevel
SampleResult
QCResult
Reporting Limit Recov.Units Recov. Limits %
RPDLimit
RPD% Notes
1070359-BSD1
I
I
I
I
I
I
I
I
I
I
II
I
I
1,1,1 -Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: l,2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
7/19/01 50.050.050.050.050.050.0_150_
~50.0~50.050.050.0
46.850.545.3197
41.647.9204
ug/kg
48.155.146.042.2
60.0-13476.4-12561.8-13214.6-24110.0-16157.9-14360.0-141'81.2-13450.8-14582.0-12176.8-113
93.6101
90.6NR
83.295.8136
96.2110
92.084.4
44.253.243.5115
92.181.040.1
4.594.872.683.0921.317.3
0.738
Great LakaS Analytical
And/ Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 36 of 3'
SL.fcS-HmGREAT
^ 1380 Busch Parkway Email: [email protected] Buffalo Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772
Hygieneering, Inc. Project: 2001-3495 Sampled: 7/13/017575 Plaza Court Project Number: 2001-3495 Received: 7/13/01Willowbrook, IL 60521 Project Manager: Gary Milkeris Reported: 7/26/01 12:15
Notes and Definitions
# Note
A The concentration of the analyte detected in the sample is characteristic of a laboratory artifact.
E This result is estimated. The analysis gave a final result that is above the calibration range
Gl The recovery of one or more analytes in the matrix QC (MS/MSD) associated with this sample is above the laboratory's establishedacceptance criteria. Refer to the included QC reports for more detail.
G12 The reporting limit of this sample/analyte is elevated due to sample matrix and/or other effects.
G19 The relative percent difference (RPD) of one or more analytes in the laboratory control QC (BS/BSD) associated with this sampleis above the laboratory's established acceptance limits. Refer to the included QC reports for more detail.
G3 The recovery of one or more analytes in the laboratory control QC (BS/BSD) associated with this sample is above the laboratory'sestablished acceptance criteria. Refer to the included QC reports for more detail.
G4 The recovery of one or more analytes in the laboratory control QC (BS/BSD) associated with this sample is below the laboratory';established acceptance criteria. Refer to the included QC reports for more detail.
02 One or more internal standard recoveries were below the method specified acceptance criteria.
03 One or more internal standard recoveries were above the method specified acceptance criteria.
04 The recovery for this analyte is below the laboratory's established acceptance criteria.
05 The recovery for this analyte is above the laboratory's established acceptance criteria.
DET Analyte DETECTED
ND Analyte NOT DETECTED at or above the reporting limit
NR Not Reported
dry Sample results reported on a dry weight basis
Recov. Recovery
RPD Relative Percent Difference
Great Lakes^Analvtical
Andy'Johnson, Project Manager Page 37 of 3
SP LAKESANALYTICAL
CHAIN OF CUSTODY REPORT (847) 808-7766FAX (847) 808-7772
531M(414) 570-9460
FAX (414) 570-9461
Client: e/// TO.- 3 DAY 2 DAY 1 DAY < 24 HRS.
-T ±-, -Address: /h?7!P
D YES^fAT is Critical
n N<"i - TAT is
D/irE RESULTS NEEDED:
TFMPFRATI 1RF 1 IPON RFC.FIPT « C«-
Report to:Phone *:Fax #:
Sfafe &Program:
P/ione #: f J Deliverable Package Needed:D STD D Other
Air Bill No.
^roject: <:
Sampler:
PO/Quote #:
FIELD ID, LOCATION
# of Boff/esPreservative Used
LABORATORYID NUMBER
-.•..•GREATILAKES 1380 Busch Parkway Email: [email protected]
ANALYTICAL Buffalo Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772
July 20, 2001
Gary MilkerisHygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
RE: 2001-3495
Dear Gary Milkeris
Enclosed are the results of analyses for sample(s) received by the laboratory on July 11, 2001. If you have anyquestions concerning this report, please feel free to contact me.
Sino
Andy JohnsonProject Manager
•
-.-•GREATMil LAKES•&•• ANALYTICAL
1
11 Hygieneering, Inc.
•7575 Plaza Court•Villowbrook, IL 60521
sample Description
ft 18-8
B 18-32
^19-5
J19-9
^20-4
«20-14
%21-15
^22-3
B22-15
K23-9
B24-12
^25-7
C26-7
27-13
128-4
28-13
•^29-10
B30-11
•30-25
B31
1Great/Lakes Analytical
1 \iu '
1380 Busch ParkwayBuffalo Grove, I l l inois 60089
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
(847)Email, [email protected] FAX (847) 808-7772
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41
ANALYTICAL REPORT FOR SAMPLES:
Laboratory Sample Number
B107129-01
B 107 129-02
B 107 129-03
B 107 129-04
B 107 129-05
B 107 129-06
B107129-07
B107129-08
B 107 129-09
B107129-10
B107129-11
B107129-12
B107129-I3
B107129-I4
B107129-15
B107129-16
B107129-17
B107129-18
BI07129-I9
B 107 129-20
The results in this report apply to the samples
Sample Matrix
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Date Sampled
7/9/01
7/9/01
7/9/01
7/9/01
7/9/01
7/9/01
7/10/01
7/10/01
7/10/01
7/10/01
7/10/01
7/10/01
7/10/01
7/10/01
7/10/01
7/10/01
7/10/01
7/10/01
7/10/01
7/10/01
analyzed in accordance with the chum of custody documentThis analvlicul report must he reproduced in its entirely.
Andy Johnson, Project Manager Page I of 70
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Analvte
B31AcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 , 1 -Dichloroethane1 ,2 -Dichloroethane1,1-Dichloroethenecis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrach 1 oroeth en eToluene1,1,1 -Tri chloroethane1 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1.2-Dichloroelhane-d4
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-201070323 7/18/01 7/18/01 2500
500500500500
1000500500500500500500500500500500500500500500500500
1000500
1000500500500500500500500500
1000500500
" " " 8 1.2- 1 3450.8-145
Sampled: 7/9/01 to 7/1 0/01Received: 7/11/01Reported: 7/20/01 13:41
Result Units Notes*
Soil G12.G3.G42520 ug/kg A
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND831 " ANDNDNDNDNDNDND
1210NDNDNDND130 %118
Great Lakes Analytical
Andy Johnson. Project Manager
*Refer to end of report tor text oj notes and de/inittons.
Page 2 of 70
GREATLAKES
NALYTICAL1380 Busch Parkway
Buffalo Grove, Illinois 60089Email, [email protected]
(847) 808-7766 FAX (847) 808-7772
I Hygieneering, Inc.^575 Plaza Court•Villowbrook. IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 7/9/01 to 7,10/01Received: 7/11/01Reported: 7/20/01 13:41
Volatile Organic Compounds by EPA Method 8260BGreat Lakes Analytical
AnalvteBatch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units Notes*
t31 (continued)Surrogate: Toluene-d8
m£urrogale: 4-Bromofluorobenzene
I
I
I
I
I
I
I
I
I
JO 703 2 3 7/18/01B107129-20
"7/AS/07 82.0-121"76.8-113
Soil G12.G3.G4126 % 05129 " OS
^read Lakes Analyt ical
1 Andy Johnson, Project Manager
1
*Refer to end of report fur left of notes and definition*.
Page 3 of 70
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Analyte
B19-5AcenaphtheneAcenaphthyleneAnilineAnthraceneBenzoic acidBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneBenzyl alcoholBis(2-chloroethoxy)methaneBis(2-chloroethyl)etherBis(2-chloroisopropyl)etherBis(2-ethylhexyl)phthalate4-Bromophenyl phenyl etherButyl benzyl phthalate4-Chloroaniline4-Chloro-3-methylphenol2-ChloronaphthaIene2-Chlorophenol4-Chlorophenyl phenyl etherChryseneDibenz (a,h) anthraceneDibenzofuran1 ,2-Dichlorobenzene1 ,3-Dichlorobenzene1 ,4-Dichlorobenzene3,3 '-Dichlorobenzidine2,4-DichlorophenolDiethyl phthalate2,4-DimethylphenolDimethyl phthalateDi-n-butyl phthalate4,6-Dinitro-2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-Dinitrotoluene
Great Lakes Analytical
lu' \ i \; \i •
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Semivolatile Organic Compounds by EPA Method 8270CGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-031070237 7/13/01 7/17/01 1000
1000100010005000100010001000100010001000100010001000330010001000100010001000100010001000100010001000100010005000100010001000100033005000500010001000
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41
Result Units Notes*
Soil G12.G15.G2.G4ND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
"Refer to end of report for text of notes and definitions
Andy'Johnson. Project Manager Page 4 of 7'
GREATLAKESANALYTICAL 1380 Busch Parkway
Buffalo Grove, Illinois 60089Email: info@glalabs com
(847) 808-7766 FAX (847) 808-7772
11
1 Hygieneering, Inc.JJ5 75 Plaza Court•Villowbrook, IL 60521
•
|TlAnalyte
•19-5 (continued)Di-n-octyl phthalate
(luorantheneluoreneexachlorobenzene
Hexachlorobutadiene
Eexachlorocyclopentadieneexachloroethane
Indeno (1,2,3-cd) pyrene^ophoronel-Methylnaphthalene"-Cresolm,p-Cresols
!
aphthalene•Nitroaniline•Nitroaniline
4-Nitroaniline
t itrobenzene•Nitrophenol
4-Nitrophenol
(-Nitrosodi-n-propylamine-Nitrosodiphenylamine
. entachlorophenolPhenanthrene
Khenolyrene
1 ,2,4-Trichlorobenzene^,4,5-Trichlorophenol•,4,6-Trichlorophenolmurrogate: 2-FluorophenolSurrogate: Phenol-d6
^Surrogate: Nitrobenzene-d5Wiurrogale: 2-FluorobiphenylSurrogate: 2.4,6-TribromophenolSurrogate: p-Terphenyl-d!4
1
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Semivolatile Organic Compounds by EPA Method 8270CGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-031070237 7/13/01 7/17/01 1000
100010001000100010001000100010001000100010001000500050005000100010005000100010005000100010001000100050001000
10.0-10910.0-11510.0-114/ 0.0- 10619.3-88.710.0-126
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41
Result Units Notes*
Soil G12.G15.G2.G4ND ug/kgNDNDNDNDNDNDNDND
3740NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND104 %
6.32 " O427.429.036.532.0
jrcat Lakes Analytical
Anthr Johnson, Project Manager
"Refer to end of report fur text of notes and definitions.
Page 5 of 70
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Analyte
B20-4AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Polynuclear Aromatic Compounds by EPAGreat Lakes Analytical
Batch Date Date SurrogateNumber Prepared Analyzed Limits
B107129-OS1070277 7/16/01 7/17/01II II M
II II II
II II II
II II II
II II II
tl II II
II II II
II It M
II II II
II II II
II II II
II II II
II II II
II II II
II II II
_ _._. ._. . . „ (..._. . . . 29.0-132
Method 8310
ReportingLimit
JOO200100100
90.0100100100100
90.0100100100100100100
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41
Result Units Notes*
Soil G1.G15.G4.O5ND ug/lcgND164NDNDNDNDNDNDNDNDNDNDND205NDAT? % 05
Lakes Analytical
, 1Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 6 of 70
1 -,,-«• GREATfill LAKES•BM ANALYTICAL•1
11 Hygieneering, Inc.
^75 75 Plaza Court•Willowbrook, IL 60521
•
|J_Analvte
1VI 8-8
Acetone•Benzenefcromodichloromethane^Jromoform
Bromomethane•i-ButanoneCarbon disulfide
Carbon tetrachloride^ThlorobenzenemThlorodibromomethaneBbhloroethane
ChloroformKhloromethane• , 1 -Dichloroethane
1,2-Dichloroethane1,1-Dichloroethene
B;is-l ,2-DichloroetheneBrans- 1 ,2-Dichloroethene
1 ,2-Dichloropropane•cis- 1 ,3-Dichloropropene•rans- 1 ,3-Dichloropropene^Ethylbenzene
2-Hexanone
tethylene chlorideMethyl-2-pentanone
Styrene^1,1 ,2,2-Tetrachloroethane•Tetrachloroethene•Toluene
1,1,1 -Trichloroethane•1 , 1 , 2 -Tri ch 1 oroeth an e•Trichloroethene^"richlorofluoromethane
Vinyl acetate•Vinyl chloride(Total Xylenes
Surrogate: DibromofluoromethanemSurrogate: 1 ,2-Dichloroethane-d4
1380 Busch ParkwayBuffalo Grove, I l l inois 60089 (847)
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-011070296 7/17/01 7/17/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
HI. 2-13450.8-145
Email: [email protected] FAX (847) 808-7772
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41
Result Units Notes*
Soil G3.G434.2 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND112 %122
I
jreat Lakes Analytical
AndyiJohnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 7 of 70
I
GREATLAKESANALYTICAL 1380 Busch Parkway
Buffalo Grove, Illinois 60089Email: [email protected]
(847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled:Received:Reported:
7/9/01 to 7/1 0/017/11/017/20/01 13:41
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Analyte
•B18-8 (continued)Surrogate: Toluene-dSSurrogate: 4-Bromofluorobenzene
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-011070296 7/17/01 7/17/01 82.0-121
76.8-113
Result
99.297.4
Units
Soil%
Notes*
G3.G4
Great Lakes Analytical
Andy Johnson, Project Manager
"Refer to end of report /or text of notes and definitions.
P a u e & o f 7<
i!-.-.B GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email, [email protected](847) 808-7766 FAX (847) 808-7772
1I
1 Hygieneering, Inc.A7575 Plaza CourtB^illowbrook, IL 605219
ITUnalyte
»18-32Acetone
^BenzeneBiromodichloromethane^Bromoform
Bromomethane
t-Butanonearbon disulfide
Carbon tetrachloride^ThlorobenzeneMThlorodibromomethane•Chloroethane
Chloroform•Chloromethane• ,1 -Dichloroethane
l ,2-Dichloroethane1,1-Dichloroethene
•is- 1 ,2-DichloroetheneBrans- 1 ,2-Dichloroethene
1 ,2-Dichloropropanejj£\s- 1 ,3-Dichloropropene•rans-1 ,3-Dichloropropene^tthylbenzene
2-Hexanone•blethylene chloride•p-Methyl-2-pentanone
Styrene_1 , 1 ,2,2-Tetrachloroethane•Tetrachloroethene^Toluene
1,1,1 -Tri chloroethane
t,l ,2-Trichloroethanerichloroethenerichlorottuoromethane
Vinyl acetate
t inyl chlorideotal Xylenes
Surrogate: Dibromofluoromethane
t arrogate: 1 ,2-Dichloroethane-d4
r4ai Lakes Analytical
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 503S/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-021070296 7/17/01 7/17/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.00
" " " 5.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-13450.8-145
Sampled: 7/9/01 to 7, 10/01Received: 7/11/01Reported: 7/20/01 13:41
Result Units Notes*
Soil G3.G432.1 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
5.23 " ANDNDNDNDNDNDNDNDNDNDNDND/ / / %125
"Refer to end of report for text of notes and definitions.
Artdy JohrisonT-Project Manager Page 9 of 70
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Analyte
B18-32 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-021070296 7/17/01 7/17/01 82.0-121
76.8-113
Sampled:Received:Reported:
Result
98.396.1
7/9/01 to 7/10/017/11/017/20/01 13:41
Units
Soil%
Notes*
G3.G4
Great Liikes Analytical Refer to end of report for text of notes and definitions.
Andy Johnson, Project Manager uc 10 of 70
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
1I
1 Hygieneering, Inc.J7575 Plaza CourtB\Villowbrook, IL 60521
•
|f
lAnalvte
•319-5• - ...
Acetone^Benzene•3romodichloromethane^feromoform
BromomethaneBte-ButanoneB^arbon disulfide
Carbon tetrachloride_Chlorobenzene•Chlorodibromomethane•Chloroethane
ChloroformHChloromethane•l , 1 -Dichloroethane
1 ,2-Dichloroethane1,1-Dichloroethene
tis- 1 ,2-Dichloroethene-ans-1 ,2-Dichloroethene
1 ,2-Dichloropropane^:is-l ,3-Dichloropropene•trans-1 ,3-Dichloropropene^Ethylbenzene
2-Hexanone•Methylene chloride
•4-Methyl-2-pentanoneStyrene1 ,1 ,2,2-Tetrachloroethane
•Tetrachloroethene•Toluene
1,1,1 -Trichloroethanem\ , 1 ,2-Trichloroethane•Trichloroethene^Trichlorofluoromethane
Vinyl acetateHVinyl chlorideJTotal Xylenes
Surrogate: Dibromofluoromethane^urrogale: 1 ,2-Dichloroelhane-d4
1 !
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-031070296 7/17/01 7/17/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.00
" 5.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-13450.8-145
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7,20/01 13:41
Result Units Notes*
Soil G3.G4.02103 ug/kg ANDNDNDND
19.9 " ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
5.15 " ANDNDNDNDNDNDNDNDNDNDNDND103 %118
I
jreaj Lakess Analytical
Andy Johnson, Project Manager
"Refer 10 end of report for text of notes and definition.'*.
Page 11 of 70
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: info@glalabs com(847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Analyte
B19-5 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzei
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-031070296 7/17/01 7/17/01 82.0-121
le " " " 76.8-113
Sampled:Received:Reported:
Result
94. 179.7
7/9/01 t7/11/017/20/01
Units
Soil%
07/10/01
13:41
Notes*
G3.G4.O2
Great Lakes Analytical "Refer to end of report for text of notes and definition
Andy Johnson, PToject Manager Page 12 of
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
11
1 Hygieneering, Inc.^7575 Plaza Court•Willowbrook, IL 605219
_JAnalyte
fcl9-9Acetone
^BenzeneBiromodichloromethane^Bromoform
Bromomethane
§-Butanonearbon disulfide
Carbon tetrachloride^Chlorobenzene•Chlorodibromomethane•Chloroethane
ChloroformfChloromethane•1,1-Dichloroethane
1 ,2-Dichloroethane1,1-Dichloroethene
»:is-l, 2-Dichloroethene^rans-1 ,2-Dichloroethene
1 ,2-DichloropropaneMpis-1 ,3-Dichloropropene•trans-1 ,3-Dichloropropene^Ethylbenzene
2-Hexanone•Methylene chloride•4-Methyl-2-pentanone
Styrene1 , 1 ,2,2-Tetrachloroethane
•Tetrach 1 oroeth en e•Toluene
1,1.1 -Trichloroethanemt\ ,1 ,2-Trichloroethane•Trichloroethene
1 richlorofluoromethaneVinyl acetate
t'inyl chlorideotal Xylenes
Surrogate: Dibromofluoromethane
( arrogate: / ,2-Dichloroethane-d4
rett Lakes Analytical
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-041070296 7/17/01 7/17/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-13450.8-145
"Refer to end of i
Sampled: 7/9/01 to 7/1 0/01Received: 7/11/01Reported: 7/20/01 13:41
Result Units Notes*
Soil G3.G4ND ug/kgNDNDNDNDNDNDNDNDND
12.2NDND
7.15NDND
5.68NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
5.41ND104 %128
•eport for text of notes and definitions.
I \.Andy\Johnson, Project Manager Page 13 of 70
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Analyte
B19-9 (continued)Surrogate: Toluene-dSSurrogate: 4-Bromofluorobenzene
Project: 2001-3495 Sampled: 7/9/01 to 7Project Number: N/A Received: 7,11/01
Project Manager: Gary Milkeris Reported: 7/20/01 13
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units
B107129-04 Soil1070296 7/17/01 7/17/01 82.0-121 97.8 %
76.8-113 91.4
10/01
41
Notes*
G3,G4
Grew Lakes Analytical "Refer to end of report for text of notes and definitions.
Andy Johnson. Project Manager Pace 14 of 70
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
1I
1 Hygieneering, Inc.^7575 Plaza CourtBw-illowbrook. IL 60521V
•1T_iAnalyte
luAcetone
•Benzene•Sromodichloromethane^Sromoform
Bromomethane
t-Butanonearbon disultlde
Carbon tetrachloride^Chlorobenzene•Chlorodibromomethane^Chloroethane
Chloroform•Chloromethanell , 1 -Dichloroethane
1 ,2-Dichloroethane^J ,1 -Dichloroethene•;is-l ,2-DichloroetheneBrans- 1 ,2-Dichloroethene
1 ,2-Dichloropropane•pis- 1 ,3-Dichloropropene•trans-1 ,3-Dichloropropene^Ethylbenzene
2-Hexanoner ethylene chlorideMethyl-2-pentanone
Styrene^1 ,1 ,2,2-Tetrachloroethane•Tetrach 1 oroethen e•Toluene
1,1,1 -Trichloroethane• 1 , 1 ,2-Trichloroethane•Trichloroethene^"richlorofluoromethane
Vinyl acetate•Vinyl chlorideIfTotal Xylenes
Surrogate: Dibromofluoromethane
C irrogale: 1.2-Dich/oroelhane-d4
reat ^.akes Analytical
Project: 2001-3495Project Number: N/A
Proj ect M anager: Gary M i Ikeri s
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-051070296 7/17/01 7/17/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-13450.8-145
"Refer to end of
Sampled:Received:Reported:
Result
43.4NDNDNDNDNDNDNDNDND10.7NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND103123
7/9/01 to 7/1 0/017/11/017/20/01 13:41
Units Notes*
Soil G3.G4ug/kg A11
11
11
"
:M"„n••**""""„"..n"""••"..%
report for text of notes and definitions.
IAndy Jphnson, Project Manager Page 15 of 70
I
&s*£-£(^_^|JTZT _r!rr H
$1GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 6052 1
Analvte
B20-4 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
Bl 07 129-051070296 7/17/01 7/17/01 82.0-121
76.8-113
Sampled:Received:Reported:
Result
99.592.1
7/9/01 to 77/11/017/20/01 13
Units
Soil%
10/01
41
Notes*
G3.G4
Great\Lakes Analytical "Refer to end of report for text of notes and definitions.
Andy lohrtson. Project Manager Page 16 of 70
GREATLAKES
(ANALYTICAL 1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
11iHygieneenng, Inc.^575 Plaza Court•Villowbrook, IL 60521I
§1TlAnalyte
•20-14Acetone
BenzeneRromodichloromethaneTiromoformBromomethane
t-Butanonearbon disulfide
Carbon tetrachloride^hlorobenzeneKhlorodibromomethanefthloroethane
Chloroformrhloromethane1 -Dichloroethane
,2-Dichloroethane1,1-Dichloroethene
R- 1 ,2-Dichloroethenens-1 ,2-Dichloroethene
1 ,2-Dichloropropane^is- 1 ,3-Dichloropropenetans-1 ,3-Dichloropropeneftthylbenzene2-Hexanoner ethytene chloride
Methyl-2-pentanoneStyreneJ ,1 ,2,2-Tetrachloroethane•"etrach 1 oroeth ene•"oluene
1,1,1 -Trichloroethaney ,1 ,2-Trichloroethane•"richloroetheneTrichlorofluoromethaneVinyl acetate
f invl chloride-otal Xylenes
Surrogate: DibromofluoromethaneSurrogate: l,2-Dichloroelhane-d4
I 1^jreat Lakes Analytical
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-061070296 7/17/01 7/17/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-13450.8-145
"Refer to end o
Sampled: 7/9/01 to 7/1 0/01Received: 7/11/01Reported: 7/20/01 13:41
Result Units Notes*
Soil G3.G4ND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND112 %121
f report for text of notes and definitions.
iAndy JoHnscMi, Project Manager Page 17 of 70
I
-.-•GREAT•All LAKES•Sil ANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Analvte
B20-14 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzet
Project: 2001-3495Project Number: N/A
Project Manager: Garv Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-061070296 7/17/01 7/17/01 82.0-121
te " " " 76.8-113
Sampled:Received:Reported:
Result
97.596. 1
7/9/01 to 7/1 0/017/11/017/20/01 13:41
Units
Soil%
Notes*
G3.G4
Great Lakes Analytical 'Refer to end of report for text of notes and definitions.
Andy Johnson. Project Manager Page I X of 70
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
11
1 Hygieneenng, Inc.^7575 Plaza CourtBWillowbrook, IL 605219
|
:
Acetone^Benzene•Bromodichloromethane^Bromoform
Bromomethaneto-Butanone•Carbon disulfide
Carbon tetrachloride^ Chlorobenzene•Chlorodibromomethane•Chloroethane
ChloroformMChloromethane•1 , 1 -Dichloroethane
1 ,2-Dichloroethane1,1-Dichloroethene
f s-l,2-Dichloroethenean s-1 ,2-Dichloroethene
1 ,2-Dichloropropanegpis-l,3-DichloropropeneBrans- 1 ,3-Dichloropropene^thylbenzene
2-Hexanone
tlethvlene chloride-Methyl-2-pentanone
Styrene1 , 1 ,2,2-Tetrachloroethane
•Tetrachloroethene•Toluene
1,1,1 -Trichloroethane•1 , 1 ,2 -Trichloroethane•TrichloroetheneTYichlorofluoromethane
Vinyl acetatePt'inyl chloride[Total XylenesSurrogate: Dibromofluoromethane
^urrogate: 1 . 2-Dichloroelhane-d4
1 <
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-071070323 7/18/01 7/17/01 2500
500500500500
1000500500500500500500500500500500500500500500500500
1000500
1000500500500500500500
10000500
1000500500
81.2-13450.8-145
Sampled: 7/9/01 to 7, 10/01Received: 7/11/01Reported: 7.20/01 13:41
Result Units Notes*
Soil GI2.G19.G3.G4ND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
3650NDNDNDNDNDND845 " ANDNDND971NDNDND
591000NDND
1330ND122 %1 10
jreat Lakes AnalyticalS
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 19 of 70
mGREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled:Received:Reported:
7/9/01 to 7/1 0/017/11/017/20/01 13:41
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Analyte
B2 1-15 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzei
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-071070323 7/18/01 7/17/01 82.0-121
te " " " 76.8-113
Result
113118
Units
Soil%
Notes*
C12.G19.G3.G4
O5
Great Lakfcs Analytical Refer to end of report for text of notes and definitions.
Andy Johrrson. Project Manager Page 20 of 70
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
11
1 Hygieneering, Inc.1?5 75 Plaza CourtpVillowbrook, IL 60521I
•T^Analvte
|22.3
AcetoneBenzeneBjromodichloromethaneTiromoform
Bromomethane
t-Butanonearbon disulfide
Carbon tetrachloride^ThlorobenzenethlorodibromomethanePfchloroethane
ChloroformfeChloromethane• ,1 -Dichloroethane~i ,2-Dichloroethane
1,1-DichloroetheneKs-l,2-Dichloroethene^rans-l ,2-Dichloroethene
1 ,2-Dichloropropane
El ,3-Dichloropropenes-1 ,3-Dich)oropropeneylbenzene
2-Hexanone•Methylene chloride•-M ethyl-2-pentanone
StyreneJ,l,2,2-Tetrachloroethane•"etrach 1 oroeth en e•"oluene
1,1,1 -Trichloroethane
(, 1 ,2-Trichloroethanerichloroethenerichlorotluoromethane
Vinyl acetate
f inyl chlorideotal Xylenes
Surrogate: Dibromofluoromethane^urrogate: 1 ,2-Dichloroethane-d4
Project: 2001-3495Project Number: N/A
Project Manager: Gary M ilkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
Bl 07 129-081070323 7/18/01 7/18/01 1250
250250250250500250250250250250250250250250250250250250250250250500250500250250250250250250250250
" " " 500250250
81.2-13450.8-145
Sampled: 7/9,01 to 7/1 0/01Received: 7/11/01Reported: 7/20/01 13:41
Result Units Notes*
Soil G12.CI9.G3.G4ND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDND411NDNDNDNDNDNDNDNDNDNDNDNDNDND
4750NDND511ND110 %
97.7
K5tt Lakes Analytical
Andly Jbhhson, Project Manager
"Refer to end of report for text of notes and definitions
Page 21 of 70
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: info@glalabs com(847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Analvte
B22-3 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzer
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-081070323 7/18/01 7/18/01 82.0-121
le " " " 76.8-113
Sampled:Received:Reported:
Result
98.597.9
7/9/01 t7/11/017,20/01
Units
Soil%
0 7 / 1 0 / 0 1
13:41
Notes*
G12.GI9.G3.G4
Great Lafces Analytical
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 22 of 7(
> -,-• GREAT•All LAKES•&•• ANALYTICAL
IHygieneenng, Inc.l?575 Plaza Court
BVillowbrook, IL 60521
9
|
T1
lAnalyte
y22-15Acetone
^Jenzene•Jromodichloromethane^Bromotorm
Bromomethane|K-Butanone•Tarbon disulfide
Carbon tetrachlorideChlorobenzene
thlorodibromomethanehloroethane
ChloroformWThloromethane•i ,1 -Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethene»is-l,2-Dichloroethene•ans- 1 ,2-Dichloroethene
1 ,2-Dichloropropane
E' -1,3-Dichloropropenens- 1 ,3-Dichloropropenenylbenzene
2-Hexanone
f lethylene chloride-Methyl-2-pentanonetyrene
1 , 1 ,2,2-Tetrachloroethane•Tetrach 1 oroeth ene^Toluene
1 , 1 ,1 -Trichloroethane
t, 1 ,2-Trichloroethanerichloroethenerichlorofluoromethane
Vinyl acetatefe/inyl chloride•Total Xylenes
Surrogate: Dibromofluoromethane^urrogate: 1 ,2-Dichloroethane-d4
1380 Busch ParkwayBuffalo Grove, Illinois 60089 (847)
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-091070296 7/17/01 7/17/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-13450.8-145
Email: [email protected] FAX (847) 808-7772
Sampled: 7/9/01 to 7, 10/01Received: 7/11/01Reported: 7/20/01 13:41
Result Units Notes*
Soil G3.G4.O243.5 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDND
9.45NDNDNDNDNDND
5.98 " ANDNDNDNDNDNDND149NDNDNDND/ 15 %124
Great Lakes AnalyticalI V
\Andy JihnVon, Project Manager
"Refer to end of report for text of notes and definitions
Page 23 of 7C
I
GREAT
1380 Busch Parkway Email: [email protected] Buffalo Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 7/9/01 to 7/10/01Received: 7/1 1/01Reported: 7/20/01 13:41
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
AnalyteBatchNumber
DatePrepared
DateAnalyzed
SurrogateLimits
ReportingLimit Result Units Notes*
B22-15 (continued) B107129-09 Soil G3.G4.O2Surrogate: Toluene-d8 1070296 7/77/07 7/77/01 82.0-121 "" 79.9 % O4Surrogate: 4-Bromofluorobenzene " " " 76.8-113 72.0 " O4
Great uftkes Analytical "Refer to end of report for text of notes and definitions.
Andy Johnson, Project Manager Page 24 of 70
I -.-B GREATf All LAKES
_ IBM ANALYTICAL•11
1 Hygieneering, Inc.^7575 Plaza CourtMvillowbrook, IL 60521V
1j
^Analvte
miM.Acetone
^Benzene•Jromodichloromethane^Jvomoform
Bromomethane
§-Butanonearbon disulfide
Carbon tetrachloride^Uhlorobenzene•ThlorodibromomethaneBfchloroethane
Chloroform•Chloromethane• ,1 -Dichloroethane^\ ,2-Dichloroethane
1 , 1 -Dichloroethene»is-l,2-Dichloroethenerans-l,2-Dichloroethene
1 ,2-Dichloropropane
E-l,3-Dichloropropenens- 1 ,3-Dichloropropenenylbenzene
2-Hexanone
f ethylene chlorideMethyl-2-pentanone
Styrene
f1 ,1,2,2-Tetrachloroethane
etrachloroetheneoluene
1,1,1 -Trichloroethane
t,l,2-Trichloroethanerichloroethenerichlorofluoromethane
Vinyl acetate»inyl chlorideotal Xylenes
" Surrogate: Dibromofluoromethane^Surrogate: 1.2-Dichloroethane-d4
•^jreal Lakes Analytical
1380 Busch ParkwayBuffalo Grove, I l l inois 60089 (847)
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-101070323 7/18/01 7/19/01 1250
7/17/01 250250250250500250250250250250250250250250250500250250250250250500250500250250250250250250250250500250250
81.2-13450.8-145
"Refer to end ofr
Email: [email protected] FAX (847) 808-7772
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41
Result Units Notes*
Soil G12.G19.G3.G4ND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
21300397NDNDNDND "ND431 " ANDNDNDNDNDNDND342NDND
2530ND159 % OS151 " 05
eport for text of notes and definitions.
IAndy Johnson, Project Manager Page 25 of 70
I
—,«• GREATtillLAKES
•&• ANALYTICAL1380 Busch Parkway
Buffalo Grove, Illinois 60089Email: [email protected]
(847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Analvte
B23-9 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-101070323 7/18/01 7/17/01 82.0-121
76.8-113
Sampled:Received:Reported:
Result
138148
7/9/01 to 7/1 0/017/1 1/017/20/01 13:41
Units Notes*
Soil G1iGI9.GJ.G4% O5
05
Great Lakes Analytical "Refer to end of report for text of notes and definitions.
Andy Jdbrtson, Project Manager Page 26 of 70
1 —^1 GREATi|S| LAKES•fill ANALYTICAL•1
Slygieneering, Inc.575 Plaza Court/illowbrook, IL 60521
|J.Analyte
»24-12Acetone
Benzene•Jromodichloromethane^Bromoform
Bromomethane
(•Butanonearbon disulfide
Carbon tetrachloride^Thlorobenzene•ThlorodibromomethaneHbhloroethane
Chloroform
(hloromethane,1 -Dichloroethane,2-DichIoroethane
1 , 1 -Dichloroethene•ris-l,2-Dichloroethene•rans-1, 2-Dichloroethene
1 ,2-Dichloropropane
Kis-1 ,3-Dichloropropeneans-1 ,3-Dichloropropenethylbenzene
2-Hexanone
Fethylene chlorideM ethy \-2-pentanone
StyreneJ ,1 ,2,2-Tetrachloroethane•TetrachloroetheneMfoluene
1,1,1 -TrichloroethaneM , 1 ,2-Trichloroethane•Trichloroethene^Trich lorofluoromethane
Vinyl acetate
t inyl chlorideotal Xylenes
Surrogate: Dibromofluoromethane^urro gale: 1 . 2-Dichloroethane-d4
1Wjreat Lakes Analytical
1380 Busch ParkwayBuffalo Grove, I l l inois 60089 (847)
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-111070323 7/18/01 7/17/01 1250
250250250250500250250250250250250250250250250250250250250250250500250500250250250250250250
Email: [email protected] FAX (847) 808-7772
Sampled:Received:Reported:
Result
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
5590438NDNDNDNDND839NDNDNDNDNDNDND
7/9/01 to 7 /1 0/017/11/017/20/01 13:41
Units Notes*
Soil G12.G19.G3.C4ug/kg11
"""
"11
)(
"
it
»
11
11
:M""""
A-""••"""
7.20/01 25000 15600007/17/01 250
500250250
81.2-13450.8-145
NDND460ND103
94.6
""••%"
"Refer to end of report for text of notes and definitions.
IAndy Jehnson, Project Manager Page 27 of 70
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847)808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled:Received:Reported:
7/9/01 to 7/1 0,017/11/017/20/01 13:41
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Analvte
B24-12 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-111070323 7/18/01 7/17/01 82.0-121
76.8-113
Result
96.3102
Units
Soil G12.G19%
Notes*
.C3.G4
Great Lakes AnalyticalT!
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 28 of 70
-;~1 GREATI LAKESI ANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
IHygieneering, Inc.
^575 Plaza Court•Villowbrook, IL 60521
Project: 2001-3495Project Number: N/AProject Manager: Gary Milkeris
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
T Batch Date Date SurrogatejAnalyte Number Prepared Analyzed Limits
•bs-7 B107129-12Acetone 1070323 7/18/01 7/18/01
BenzeneBiromodichloromethane " " "^Bromoform " " "
Bromomethane " " "
§-Butanone " " "arbon disulfide " " "
Carbon tetrachloride " " "^Thlorobenzene " " "m?hlorodibromomethane " " "•Chloroethane " " "
Chloroform " " "•Chloromethane " " "• ,1 -Dichloroethane " " "
1 ,2-Dichloroethane " " "1,1-Dichloroethene " " "
•is-1, 2-Dichloroethene " " "•Vans- 1, 2-Dichloroethene " " "
1,2-Dichloropropane " " "^is-l,3-Dichloropropene " " "Brans- 1,3-Dichloropropene " " "
Lithylbenzene " " "2-Hexanone " " "
Ilethylene chloride " "-Methyl-2-pentanone " " "
Styrene " " "«,l,2,2-Tetrachloroethane " "etrachloroethene "oluene " " "
1 ,1 ,1 -Trichloroethane
K l,2-Trichloroethane " " "richloroethene " "richlorofluoromethane " "
Vinyl acetate " "
f inyl chlorideotal Xylenes " " "
Surrogate: Dibromofluoromethane " " " 81.2-134^urrogale: 1.2-Dichloroethane-d4 " " " 50.8-145
^ireat/Lakes Analytical
ReportingLimit
25.05.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
"Refer to end oj
Result Units Notes*
Soil G19.G3.G481.7 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDND
37.0NDNDNDNDNDND
6.32 " ANDNDNDNDNDNDND
84.1NDND146ND137 % O5177 " 05
f report for text of notes and definitions.
Johnson, Project Manager Page 29 of 70
I
&3iWTIKUfi^ IB i
••• •••V i
^£l GREATLAKES
(ANALYTICAL1380 Busch Parkway
Buffalo Grove, Illinois 60089Email: [email protected]
(847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Analyte
B25-7 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzei
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-121070323 7/18/01 7/18/01 82.0-121
ie " " " 76.8-113
Sampled:Received:Reported:
Result
123107
7/9/01 to 7,7/11/017/20/01 13:
Units
Soil%
10/01
Notes*
G19,G3,G4OS
Great Lakes Analytical
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 30 of 7C
-.-•GREAT1LAKES
[ANALYTICAL1380 Busch Parkway
Buffalo Grove, Illinois 60089Email: info@glalabs com
(847) 808-7766 FAX (847) 808-7772
L_(Hygieneering, Inc.^575 Plaza Court
•Villowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
T Batch Date Date Surrogate^nalvte Number Prepared Analyzed Limits
^26-7 B107129-13Acetone 1070296 7/17/01 7/17/01
Benzene " " "•Jromodichloromethane " " "Hjromoform " " "
Bromomethane " " "•-Butanone " " "Karbon disulfide " " "
Carbon tetrachloride " " "_Chlorobenzene " " "
•Chlorodibromomethane " " "•Chloroethane " " "
Chloroform " " "
f^hloromethane,1-Dichloroethane " " ",2-Dichloroethane
1,1-Dichloroethene "•is-l,2-Dichloroethene " "^rans-1, 2-Dichloroethene " "
1,2-Dichloropropane " " "
E-l,3-Dichloropropene " " "ns-l,3-Dichloropropene " " "^ylbenzene " " "
2-Hexanone " " "
Klethylene chloride " " "-Methyl-2-pentanone " " "
btyrene " " "1 , 1 ,2,2-Tetrachloroethane "
Jetrachloroethene " " "oluene " " "
1,1,1 -Trichloroethane " " "
t, 1 ,2-Trichloroethane "richloroethene " " "richlorofluoromethane "
Vinyl acetate " " "
(inyl chloride " "otal Xylenes " "arrogate: Dibromofluoromethane " " " 81.2-134
^urrogate: 1.2-Dichloroethane-d4 " " " 50.8-145
ReportingLimit
25.05.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005005005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.0500
5.00
Result Units Notes*
Soil G3.G4.O2125 ug/kg ANDNDNDNDNDNDNDNDNDNDNDND23.3ND
8.2711800 " G12
524 " G12NDNDNDNDND11.5 " ANDNDNDNDNDNDND
6.65NDND
2230 " G12ND134 %145
ireat Lakes Analytical
indy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 31 of 70
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 6052 1
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled:Received:Reported:
7/9/01 to 7/1 0/017/11/017/20/01 13:41
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Analvte
B26-7 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzei
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-131070296 7/17/01 7/17/01 82.0-121
ie " " " 76.8-1/3
Result
77.662.0
Units
Soil%
Notes*
G3.G4.O2O404
Great Uakes Analytical "Refer to end of report for text of notes and definitions.
Andy Joimson, Project Manager Page 32 of 7<
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
1I
[Hygieneering, Inc.^75 75 Plaza Court^Villowbrook, IL 60521
i
M
I
T1 Analyte
•327-13Acetone
^BenzeneBfromodichloromethane^feromoform
Bromomethane
§-Butanonearbon disulfide
Carbon tetrachloride.Chlorobenzene
•Thlorodibromomethane•Thloroethane
Chloroform••ThloromethaneB ,1 -Dichloroethane^ ,2-Dichloroethane
1 ,1 -DichloroethenejAis-1 ,2-DichloroetheneJpans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
E-l,3-Dichloropropenens-1 ,3-Dichloropropenelylbenzene
2-Hexanone•dethylene chlorideBr-Methyl-2-pentanone
Styrene1 ,1 ,2,2-Tetrachloroethane
•TetrachloroetheneB^oluene
1,1,1 -Trichloroethane
K,l ,2-Trichloroethanerichloroethenerich 1 orofluoromethane
Vinyl acetate»inyl chloride
otal Xylenes- - - • — -Surrogate: Dibromofluoromethane
^urrogate: !,2-Dichloroethane-d4
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-141070296 7/17/01 7/17/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-13450.8-145
Sampled: 7/9/01 to 7,10/01Received: 7,11/01Reported: 7/20/01 13:41
Result Units Notes*
Soil G3.G4.O238.8 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
7.08NDNDNDND101 %116
•eit Lakes Analytical
Johnson, Project Manager
"Refer to end of report for text of notes and definitions
Page 33 of 70
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 7/9/01 to 7,10/01Received: 7/11/01Reported: 7/20/01 13:41
B27-13 (continued)
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
AnalvteBatchNumber
DatePrepared
DateAnalyzed
SurrogateLimits
ReportingLimit Result Units Notes*
Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
B107129-141070296 7/17/01 " 7/17/01 82JJ-J~2T
76.8-113
Soil84.070.3
G3.G4.O2
O4
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 34 of 70
|~^l GREAT•All LAKES•Sill ANALYTICAL•1
I| Hygieneering, Inc.
Jj5 75 Plaza Court•Viliowbrook, IL 60521m
tTJAnalyte
P28-4Acetone
BenzeneBromodichlorom ethane^Bromoform
BromomethaneV^Butanone•arbon disulfide
L'arbon tetrachlorideelorobenzenelorodibromomethaneloroethane
Chloroform•ChloromethaneV, 1 -Dichloroethane
n,2-Dichloroethane1,1-Dichloroethene
•is- 1 ,2-Dichloroethene(fans- 1 ,2-Dichloroethene
1 ,2-Dichloropropane
C-l,3-Dichloropropenens-1 ,3-Dichloropropenelylbenzene
2-Hexanone
Vethylene chlorideMethyl-2-pentanone
atyrene1 , 1 ,2,2-Tetrachloroethane
§etrachloroetheneoluene
1 ,1 ,1 -Trichloroethane
t l,2-Trichloroethanerichloroethenerichlorotluoromethane
Vinyl acetate
K inyl chlorideotal Xylenes
Surrogate: DibromofluoromethaneSurrogate: 1.2-Dichloroelhane-d4
I !**reaC:Lakes Analytical
M• i ^^ ~^~
1380 Busch ParkwayBuffalo Grove, I l l inois 60089 (847)
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-151070262 7/13/01 7/13/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
81. 2-13450.8-145
Email: [email protected] FAX (847) 808-7772
Sampled: 7/9/01 to 7, 10/01Received: 7 /11 /01Reported: 7/20/01 13:41
Result Units
Soil63.2 ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
11.5NDNDNDND113 %1 19
Notes* ''
G19.G4A
"Refer to end of report for text of notes and definitions.
\ndy Johnson, Project Manager Page 3 5 of 70
I
—.—•GREAT•AllLAKES
•&• ANALYTICAL1380 Busch Parkway
Buffalo Grove, Illinois 60089Email: [email protected]
(847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
AnalvteBatchNumber
DatePrepared
DateAnalyzed
SurrogateLimits
ReportingLimit Result Units Notes*
B28-4 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
1070262 7/13/01^6107129-15
i/imi " 82.0-ni76.8-113
Soil G19.G4104
89.5
dy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 3 6 of 70
§ -.«• GREAT•All LAKES•fill ANALYTICAL
1Hygieneering, Inc.7575 Plaza Court
•Willowbrook, IL 60521
•
JAnalyte
JB28-13Acetone
—Benzene•Bromodichloromethane^Bromoform
BromomethaneM2-Butanone•Carbon disulfide
Carbon tetrachlorideChlorobenzene
•Chlorodibromomethane•Chloroethane
Chloroform
(hloromethane,1 -Dichloroethane,2-Dichloroethane
1,1-Dichloroethene•:is-l ,2-DichloroetheneB^rans- 1 ,2-Dichloroetheme
1 ,2-Dichloropropane<pis- 1 ,3-Dichloropropene
Brans- 1 ,3-DichloropropeneBz thy (benzene
2-Hexanone•Methylene chloride^•t-Methyl-2-pentanone^ityrene
1 , 1 ,2,2-Tetrachloroethane
tetrachloroetheneoluene
1,1,1 -Trichloroethane1 , 1 ,2-Trichloroethane
•Trichloroethene"Trichlorofluoromethane
Vinyl acetate•Vinyl chloride•Total Xylenes
Surrogate: DibromofluoromethaneSurrogate: 1 . 2-Dichloroethane-d4
1 380 Busch ParkwayBuffalo Grove, I l l inois 60089 (847)
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260B .Great Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-161070262 7/13/01 7/13/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.00
" " " 10.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
" " " 81.2-13450.8-145
Email: [email protected] FAX (847) 808-7772
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41
Result Units Notes*
Soil G19.G429.6 ug/kg ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND119 %129
jreatlLakes Analytical
Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 3 7 of 70
I
GREATLAKESANALYTICAL 1380 Busch Parkway
Buffalo Grove, Illinois 60089Email: [email protected]
(847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled:Received:Reported:
7/9/01 to7 /10 /7/11/017/20/01 13:41
01
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Analvte
B28-13 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-161070262 7/13/01 7/13/01 82.0-121
76.8-113
Result
83.066.3
Units
Soil%
Notes*
G19.G4
O4
Great Bakes Analytical! \
"Refer to end of report for text of notes and definitions.
Andy Johnson, Project Manager Page 3 8 of 70
•—.—•GREAT•All LAKES
_ •&• ANALYTICAL11
1 Hygieneering, Inc.J7575 Plaza Court•vVillowbrook, IL 60521
•
|
lAnalvte
•329-10Acetone
•BenzeneBjromodichloromethane'^Bromoform
Bromomethane
§-Butanonearbon disulfide
Carbon tetrachloride_ChlorobenzeneB^hlorodibromomethane•Chloroethane
Chloroform•ChloromethaneB , 1 -Dichloroethane
1 ,2-Di chloroethane1,1-Dichloroethene
M:is-l, 2-DichloroetheneBrans- 1 ,2-Dichloroethene
1 ,2-Dichloropropane
K s-l ,3-Dichloropropeneans-1 ,3-Dichloropropenethylbenzene
2-Hexanone
f ethylene chlorideMethyl-2-pentanone
Styrene1 , 1 ,2,2-Tetrachloroethane
BretrachloroetheneBfoluene
1,1,1 -Trichloroethane
t l ,2-Trichloroethanerichloroethene
i richlorofluoromethaneVinyl acetate
§inyl chlorideotal Xylenes
Surrogate: DibromofluoromethaneSurrogate: 1 ,2-Dichloroethane-d4
I >^jredt Lakes Analytical
f\
l\
1 iV~- —
1380 Busch ParkwayBuffalo Grove, I l l inois 60089 (847)
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-171070296 7/17/01 7/17/01 25.0
5.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-13450.8-145
Email: [email protected] FAX (847) 808-7772
Sampled: 7/9/01 to 7, 10,01Received: 7/11/01Reported: 7/20/01 13:41
Result Units
Soil41.7 ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
5.99NDNDNDNDNDNDNDNDNDNDNDNDNDND
36.7NDNDNDND113 %118
Notes*
G3.G4A
"Refer to end of report for text of notes and definitions.
Andy Johnson, Project Manager Page 39 of 70
I
k«=**-*W;V BH
MGREATLArXLo 1380 Busch Parkway Email: [email protected] Buffalo Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Analvte
B29-10 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-171070296 7/17/01 7/17/01 82.0-121
76.8-113
Sampled:Received:Reported:
Result
93.880.3
7/9/01 to 7/1 0/017/11/017/20/01 13:41
Units
Soil
y°
Notes*
G3.G4
Great Lakes Analytical "Refer to end of report for text of notes and definitions.
Andy Johnson, Project Manager Page 40 of 70
I ^.^H GREAT•All LAKES•Hii ANALYTICAL
1"THygieneering, Inc.
17575 Plaza Court•Willowbrook, IL 60521I
11
JAnalyte
BB30-11l B^ '"•
Acetone—BenzeneBjromodichloromethane•Bromotorm
Bromomethane•2-Butanone•Carbon disulfide
Carbon tetrachlorideChlorobenzene
•Chlorodibromomethane•Chloroethane
ChloroformMjChloromethane•! , 1 -Dichloroethane™1 ,2-Dichloroethane
1,1-Dichloroethene•cis-1, 2-DichloroetheneBran s-1 ,2-Dichloroethene
1 ,2-Dichloropropane^f is- 1 ,3-Dichloropropene•rans-1 ,3-Dichloropropene•Ethylbenzene
2-Hexanone
f lethylene chloride-Methyl-2-pentanonetyrene
1 , 1 ,2,2-Tetrachloroethane•TetrachloroetheneBjoluene
1,1,1 -Trichloroethane•1 , 1 ,2-TrichloroethaneBrrichloroethene•Trichlorofluoromethane
Vinyl acetate
f inyl chlorideotal Xylenes
Surrogate: Dibromofluoromethane^urrogate: l.2-Dichloroelhane-d4
m- I•Jniit Lakes Analytical
• \
1 1 \i \/^
1380 Busch ParkwayBuffalo Grove, Il l inois 60089 (847)
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-181070323 7/18/01 7/17/01 2500
500500500500
1000500500500500500500500500500500
7/20/01 5007/17/01 500
500500500500
1000500
1000500500500500500500
Email: [email protected] FAX (847) 808-7772
Sampled: 7/9/01 to 7. 10/01 !
Received: 7/11/01Reported: 7/20/01 13:41
Result Units Notes*
Soil G12.GI9.G.1.G42580 ug/kg A
NDNDNDNDNDNDNDNDNDNDNDNDNDNDND
21900NDNDNDNDNDND938 " ANDNDND
4830NDNDND
25000 1160000500
1000500500
81.2-13450.8-145
NDND
1240ND139 % O5125
"Refer to end of report for text of notes and definitions.
Andy Johnson, Project Manager Page 41 of 70
I
-.«• GREAT•All LAKES•Sll ANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.75 75 Plaza CourtWillowbrook, IL 60521
Analvte
B30-11 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-181070323 7/18/01 7/17/01 82.0-121
76.8-113
Sampled:Received:Reported:
Result
129138
7/9/01 t7/11/017/20/01
Units
Soil%
o7/10/01
13:41
Notes*
G12.G19.G3.G4O5O5
Great llakes Analytical
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 42 of 70
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
11Hygieneenng, Inc.75 75 Plaza Court[Willowbrook, IL 605211
|[Analyte
1830-25Acetone•BenzenebromodichloromethanewomoformBromomethane|2-ButanoneJGarbon disulfideCarbon tetrachlorideChlorobenzene
IChlorodibromomethaneChloroethaneChloroform
iChloromethanell , I -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethene
fcis-1 ,2-Dichloroethenefrans- 1 ,2-Dichloroethene
1 ,2-Dichloropropaneg:is-l ,3-Dichloropropene•rans-1 ,3-Dichloropropenetthylbenzene2-Hexanone
•Methylene chlorideR-M ethy 1-2-pentanoneStyrene1 , 1 ,2,2-Tetrachloroethane
•Tetrachloroethene•Toluene
1 ,1 ,1 -Trichloroethane
( , 1 ,2-Trichloroethanefrichloroethenerrichlorofluoromethane
Vinyl acetate
§'inyl chloride'otal Xylenes
Surrogate: Dibromofluoromethane^urrogate: 1 . 2-Dichloroethane-d4
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107129-191070323 7/18/01 7/17/01 2500
500500500500
1000500500500500500500500500500500500500500500500500
1000500
1000500500500500500500500500
1000500500
81.2-13450.8-145
Sampled:Received:Reported:
Result
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND835NDNDNDNDNDNDND
9950NDNDNDND165166
7/9/01 to 7, 10, 017/11/017/20/01 13:41
Units Notes*
Soil GI2.GI9.G3.C4ug/kg11
"""
»"»11
11
"n
••"""
n
11
A
11
"11
"""11
"
"% 05
O5
jjeat Lakes AnalyticalA
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 43 of 7t
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Project: 2001-3495Project Number: N/'A
Proj ect M an ag er: Gary M i 1 k eri s
Sampled: 7/9/01 to 7,10/01Received: 7/11/01Reported: 7/20/01 13:41
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
AnalyteBatchNumber
DatePrepared
DateAnalyzed
SurrogateLimits
ReportingLimit Result Units Notes*
B30-25 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
1070323 7/18/01B107129-19
"7/77/07 82.0-12176.8-113
Soil G12.GI9.G3.G4154 % O5161 " 05
Great Lakes Analytical
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 44 of 70
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
I Hygieneering, Inc.•7575 Plaza CourtJwillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 7/9/01 to 7/10/01Received: 7,11/01Reported: 7/20/01 13:41
Dry Weight DeterminationGreat Lakes Analytical
gample Name Lab ID Matrix Result Units
J19-5
320-4
B31
B107129-03
B107129-05
Bl 07129-20
Soil
Soil
Soil
77.3
78.4
80.0
Great'jLaldes Analytical
Andy) Johnson, Project Manager Page 45 of 70
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41
Volatile Organic Compounds by EPA Method 8260B/Quality ControlGreat Lakes Analytical
Date Spike SampleAnalyte Analyzed Level Result
Batch: 1070323 Date Prepared: 7/18/01Blank 1070323-BLK1Acetone 7/20/01Benzene "Bromodichloromethane "Bromoform "Bromomethane "2-Butanone "Carbon disulfide "Carbon tetrachloride "Chlorobenzene "Chlorodibromomethane "Chloroethane "Chloroform "Chloromethane "1,1 -Dichloroethane "1 ,2-Dichloroethane "1,1-Dichloroethene "cis- 1 ,2-Dichloroethene "trans-1, 2-Dichloroethene "1 ,2-Dichloropropane "cis-l,3-Dichloropropene "trans- 1,3-Dichloropropene "Ethylbenzene "2-Hexanone "Methylene chloride "4-Methyl-2-pentanone "Styrene "1,1,2,2-Tetrachloroethane "Tetrachloroethene "Toluene "1,1,1 -Trichloroethane "1,1,2-Trichloroethane "Trichloroethene "Trichlorofluoromethane "Vinyl acetate "Vinyl chloride "Total Xylenes "Surrogate: Dibromofluoromethane " 50.0
1Great Lkkek Analytical
QCResult
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
57..?
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*
Extraction Method: EPA 5035B 1P/T1
ug/kg 1250250250250250500250250250250250250250250250250250250250250250250500250500250250250250250250250250500250250
81.2-134 115
"Refer to end of report for text of notes and definitions.
Andy Jdhnson, Project Manager Page 46 of 70
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
1iHygieneenng, Inc.JJ575 Plaza Court•Villowbrook, IL 60521
•
Project: 2001-3495Project Number: N/AProject Manager: Gary Milkeris
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41
Volatile Organic Compounds by EPA Method 8260B/Qualiry ControlGreat Lakes Analytical
T1 Analyte
Hilank (continued)Surrogate: 1.2-Dichloroethane-d4
^urrogate: Toluene-dS^Surrogate: 4-Bromofluorobenzene
LCS»cctoneenzene
Bromodichloromethane^BromoformBjromomethaneB-Butanone
Carbon disulfide•parbon tetrachlorideBrhlorobenzene^Thlorodibromomethane
Chloroethane
§hloroformhloromethane
1,1 -Dichloroethane
t1 ,2-Dichloroethane, I -Dichloroetheneis- 1 ,2-Dichloroethene
trans- 1 ,2-Dichloroethene
1,2-Dichloropropaneis- 1 ,3-Dichloropropene
trans- 1 ,3-DichloropropeneEthylbenzene
B-HexanoneB^ethylene chloride
4-Methyl-2-pentanone
("tyrene,1 ,2,2-Tetrachloroethaneetrachloroethene
Toluene
1,1,1 -Trichloroethane, 1 ,2-Trichloroethane
TrichloroetheneJYichlorofluoromethane
1 I•jreat Laket AnalyticalA f \
Date Spike SampleAnalyzed Level Result
1070323-BLK17/20/01 50.0
50.050.0
1070323-BS17/20/01 2500
2500250025GO25002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500
QCResult
51.049.945.8
334030102590209032103930127023202200214033703500584
35902170200032002800311026503000232037902860333023202090218028002820281025402690
Reporting Limit Recov. RPD RPDUnits Recov. Limits
ug/kg 50.8-14582.0-12176.8-113
ug/kg 10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-13460.0-13476.4-12561.8-13214.6-241
% Limit % Notes*
70299.891.6
134120104
83.6128157
50.892.888.085.6135140
23.4144
86.880.0128112124106120
92.8152114133
92.883.687.2112113112102108
"Refer to end of report for text of notes and definitions.
^ndy'Johnson, Project Manager Page 4 7 of 70
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/AProject Manager: Gary Milkeris
Sampled:Received:Reported:
7/9/01 107/10/017/11/017/20/01 13:41
Volatile Organic Compounds by EPA Method 8260B/Quality ControlGreat Lakes Analytical
Analvte
LCS (continued)Vinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 , 2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
LCS PUPAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 , 1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethenecis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 ,1 ,2,2-TetrachloroethaneTetrachloroetheneToluene
'Great Ldkas Analytical
u. \ j\
Date Spike SampleAnalyzed Level Result
1070323-BS17/20/01 2500
2500750050.050.050.050.0
1070323-BSP17/20/01 2500
2500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500
QCResult
40301110728084.558.164.252.1
55903220303021902780430029002860233022702760396038803480275030603610329034102870315024503990309035702440220024203020
Reporting LimitUnits Recov. Limits
ug/kg 10.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113
ug/kg 10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-134
Recov.%
16144.497.1169116128104
NR129121
87.61 1 1172116114
93.290.8110158155139110122144132136115126
98.0160124143
97.688.096.8121
"Refer to end of report for text
RPDLimit
34541.442.057.461.9173126
43.539.041.690.343.571.841.868.647.539.343.038.141.557.242.7128
67.4119
37.254.646.342.6
of notes
RPD% Notes*
50.37.2315.14.6714.29,1278.220.55.745.9020.412.1148
3.5323.641.611.816.49.238.144.885.455.138.407.255.045.1310.47.73
and definitions.
Page 4 8 of 70
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
I Hygieneering, Inc.JJS 75 Plaza CourtKvillowbrook. IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41
Volatile Organic Compounds by EPA Method 8260B/Quality ControlGreat Lakes Analytical
T DatelAnalyte Analyzed
Spike SampleLevel Result
QC Reporting Limit Recov.Result Units Recov. Limits %
RPDLimit
RPD% Notes*
B.CS DUD (continued) 1070323-BSD11,1,1 -Trichloroethane 7/20/01
t, 1 ,2 -Trichloroethane "richloroethene "richlorofluoromethane "
Vinyl acetate "Byinyl chloride "Bfotal Xylenes "
Surrogate: Dibromofluoromethane "^Surrogate: 1 ,2-Dichloroethane-d4 "•Surrogate; Toluene-d8 "^Surrogate: 4-Bromofluorobenzene "
250025002500250025002500750050.050.050.050.0
3430 ug/kg29602780265038304280762059.670.566.252.8
60.0-13476.4-12561.8-13214.6-24110.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113
1371181 1 1106153171102779141132106
44.253.243.5115
92.181.040.1
19.25.228.451.875.10118
4.92
IIIIIIIIireat Lakes Analytical
IAndy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 49 of 70
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.75 75 Plaza CourtWillowbrook. IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41
Semivolatile Organic Compounds by EPA Method 8270C/Qualiry ControlGreat Lakes Analytical
Analvte
Batch: 1070237BlankAcenaphtheneAcenaphthyleneAnilineAnthraceneBenzoic acidBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneBenzyl alcoholBis(2-chloroethoxy)methaneBis(2-chloroethyl)etherBis(2-chloroisopropyl)etherBis(2-ethylhexyl)phthalate4-Bromophenyl phenyl etherButyl benzyl phthalate4-ChIoroaniline4-Chloro-3-methylphenol2-Chloronaphthalene2-Chlorophenol4-Chlorophenyl phenyl etherChryseneDibenz (a,h) anthraceneDibenzofuran1 ,2-Dichlorobenzene1 ,3-Dichlorobenzene1 ,4-Dichlorobenzene3,3 '-Dichlorobenzidine2,4-DichlorophenolDiethyl phthalate2,4-DimethylphenolDimethyl phthalateDi-n-butyl phthalate4.6-Dinitro-2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene
Date Spike Sample QCAnalyzed Level Result Result
Date Prepared: 7/13/011070237-BLK17/17/01 ND
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*
Extraction Method: EPA 3550B
ug/kg 100100100100500100100100100100100100100100330100100100100100100100100100100100100100500100100100100330500500100
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions .
Page 50 of 70
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
1THygieneering, Inc.
J7575 Plaza Court•Willowbrook, IL 60521
•
Project:Project Number:
Project Manager:
2001-3495N/AGarv Milkeris
Sampled:Received:Reported:
7/9/01 to7/10/7/11/017/20/01 13:41
01
Semivolatile Organic Compounds by EPA Method 8270C/Quality ControlGreat Lakes Analytical
| Date Spike Sample QC1 Analyte Analyzed Level Result Result
Blank (continued) 1070237-BLK12,6-Dinitrotoluene 7/17/01
J3i-n-octyl phthalate "•fluoranthene "^•'luorene "
Hexachlorobenzene "•hexachlorobutadiene "B-Iexachlorocyclopentadiene "
Hexachloroethane "Jndeno ( 1 ,2,3-cd) pyrene "Bsophorone "B2-Methylnaphthalene "
o-Cresol "•rn.p-Cresols "•Naphthalene "^^-Nitroaniline "
3-Nitroaniline "
K-Nitroaniline "itrobenzene "
2-Nitrophenol "^1-Nitrophenol "BvI-Nitrosodi-n-propylamine "^J-Nitrosodiphenylamine "
Pentachlorophenol "
(henanthrene "henolyrene "
1,2,4-Trichlorobenzene "•2, 4,5-TrichlorophenolB?,4,6-Trichlorophenol "
Surrogate: 2-Fluorophenol " 3400mSurrogate: Phenol-d6 " 3400USurrogate: Nitrobenzene-d5 " 1710^Surrogate: 2-Fluorobiphenyl " 1710
Surrogate: 2.4,6-Tribromophenol " 3400fKurrogate: p-Terphenvl-d 1 4 " 1710
LCS 1070237-BS1Acenaphthene 7/17/01 1690
^jreat Lakes Analytical
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
438109157179229312
611
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*
ug/kg 100100100100100100100100100100100100100100500500500100100500100100500100100100100500100
10.0-109 12.910.0-1/5 3.2110.0-114 9.1810.0-106 10.519.3-88.7 6.7410.0-126 18.2
ug/kg 29.4-110 36.2
"Refer to end of report for text of notes and definitions.
IAndy Johnson, Project Manager
I
Page 51 of 70
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Semivolatile Organic Compounds by EPA Method
Analvte
LCS (continued)AcenaphthyleneAnilineAnthraceneBenzoic acidBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneBenzyl alcoholBis(2-chloroethoxy)methaneBis(2-chloroethyl)etherBis(2-chloroisopropyl)etherBis(2-ethylhexyl)phthalate4-Bromophenyl phenyl etherButyl benzyl phthalate4-Chloroaniline4-Ch!oro-3-methy!phenol2-Chloronaphthalene2-Chlorophenol4-Chlorophenyl phenyl etherChryseneDibenz (a.h) anthraceneDibenzofuran1 ,2-Dichlorobenzene1 ,3-Dichlorobenzene1 .4-Dichlorobenzene3,3'-Dichlorobenzidine2,4-DichlorophenolDiethyl phthalate2,4-DimethylphenolDimethyl phthalateDi-n-butyl phthalate4,6-Dinitro-2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-ocryl phthalate
1—
Great Lakes
Date Spike SampleAnalyzed Level Result
1070237-BS17/17/01 1690
1 69016901690169016901690169016901690169016901690169016901 690169016901690169016901 6901 6901 69016901 69016901690169016901 6901 69016901 6901 6901 69016901 690
Analytical
QCResult
605ND589212629750759774828613639636627
104063872918.9657665776657590796735671661662216695591624646475554526680691643
Sampled: 7/9/01 to 7/1 0/01Received: 7/11/01Reported: 7.20/01 13:41
8270C7Quality Control
Reporting LimitUnits Recov. Limits
ug/kg 31.0-1105.00-11032.9-1105.00-11035.9-11040.3-11041.9-11015.0-11039.6-11029.1-11027.8-11010.8-11016.5-1105.00-13132.6-1105.00-1595.00-11033.5-11017.0-11030.6-11015.2-11036.1-11030.5-11015.3-11015.6-11016.2-11016.3-1105.00-11016.9-11015.8-11016.1-11015.3-11032.0-1106.14-1105.00-11032.1-11034.2-1105.00-124
Recov. RPD RPD% Limit °/o Notes*
35.8NR
34.912.537.244.444.945.849.036.337.837.637.161.537.843.11.1238.939.345.938.934.947.143.539.739.139.212.841.135.036.938.228.132.831.140.240.938.0
Great Lako^ Analytical
Andy/Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 5 2 of 7(
GREATLAKESANALYTICAL 1380 Busch Parkway
Buffalo Grove, Illinois 60089Email: [email protected]
(847) 808-7766 FAX (847) 808-7772
JHygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 7/9/01 to 7, 10/01Received: 7/11/01Reported: 7/20/01 13:41
Semivolatile Organic Compounds by EPA Method 8270C/Quality ControlGreat Lakes Analytical
JAnalyte
f r<* (continued)Fluoranthene
^Fluorene•Hexachlorobenzene^iexachlorobutadiene
Hexachlorocyclopentadiene•lexachloroethane•ndeno (1,2,3-cd) pyrene
Isophorone2-Methylnaphthalene
•s-CresolBn,p-Cresols
Naphthalene•p-Nitroaniline•3-Nitroaniline
4-NitroanilineNitrobenzene
tNitrophenolNitrophenol
N-Nitrosodi-n-propylamineJ'J-Nitrosodiphenylamine•"entaehlorophenol•"henanthrene
Phenol•PyreneB ,2,4-Trichlorobenzene
2,4,5-Trichlorophenol2,4,6-Trichlorophenol
mSurrogate: 2-FluorophenolIfurrogale: Phenol-d6
Surrogate: Nitrobenzene-d5mSurrogate: 2-FluorobiphenylmSurrogate: 2.4.6- Tribromophenol^Surrogate: p-Terphenyl-d 1 4
•Klatrix Spike(Acenaphthene
Acenaphthylene—Aniline
I•treat La/es Analytical
Date Spike SampleAnalyzed Level Result
1070237-BS17/17/01 1690
16901 69016901690169016901690169016901690169016901690169016901 69016901 690169016901 6901 69016901 69016901 690
~"" 536033607690/69033601690
1070237-MS1 B1071 15-127/17/01 1700 ND
1700 ND1700 ND
QCResult
552631639635374679793513773653596613662360589623687561647494594606654
1170652632678
14001150640729
12701280
566561106
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*
ug/kg 15.0-11030.1-11031.8-11011.1-1107.46-11010.6-11011.3-11828.0-11031.8-11020.3-1105.00-11027.0-11012.0-1105.00-1105.00-11027.3-11029.7-11010.4-11032.4-11031.2-1105.00-11035.4-11015.8-1105.00-16614.3-11014.3-11030.9-11010.0-10910.0-11510.0-11410.0-10619.3-88.710.0-126
ug/kg 5.00-1405.00-1315.00-110
"Refer to end ofrepor
32.737.337.837.622.140.246.930.445.738.635.336.339.221.334.936.940.733.2 '38.329.235.135.938.769.238.637.440.141.734.237.943.137.875.7
33.333.06.24
for text of notes and definitions.
Anuy Johnson, Project Manager Page 53 of 70
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Project:Project Number:
Project Manager:
2001-3495N/AGarv Milkeris
Sampled: 7/9/01 to 7/1 0/01Received: 7/11/01Reported: 7/20/01 13:41
Semivolatile Organic Compounds by EPA Method 8270C/Quality ControlGreat Lakes Analytical
Analvte
Matrix Spike (continued)AnthraceneBenzoic acidBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneBenzyl alcoholBis(2-chloroethoxy)methaneBis(2-chloroethyl)etherBis(2-chloroisopropyl)etherBis(2-ethylhexyl)phthalate4-Bromophenyl phenyl etherButyl benzyl phthalate4-Chloroaniline4-Chloro-3-methylphenol2-Chloronaphthalene2-Chloropheno!4-Chlorophenyl phenyl etherChryseneDibenz (a,h) anthraceneDibenzofuran1 ,2-Dichlorobenzene1 ,3-Dichlorobenzene1 ,4-Dichlorobenzene3,3 '-Dichlorobenzidine2,4-DichlorophenolDiethyl phthalate2,4-DimethylphenolDimethyl phthalateDi-n-butyl phthalate4,6-Dinitro-2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-octyl phthalateFluorantheneFluorene
Date SpikeAnalyzed Level
SampleResult
QC Reporting Limit Recov. RPD RPDResult Units Recov. Limits % Limit % Notes*
1070237-MS1 B107115-127/17/01 1700
1 7001 7001 7001 7001 70017001 7001 7001 70017001 7001 70017001 7001 7001 7001 7001 7001 7001 70017001 7001700170017001 7001 7001 7001 70017001 7001 7001 7001 70017001 7001 700
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
542 ug/kg442572665671696749619630609591997
588689275693610778604540732674627619622263734586655636498590583654661653504572
5.00-1465.00-1495.00-1495.00-1345.00-1275.00-2235.00-1208.91-11023.1-11016.6-11014.5-1105.00-1535.00-1525.00-2165.00-11017.8-1105.00-1175.03-1285.00-1105.00-1555.00-1645.00-1335.00-1175.00-1105.00-1105.00-11021.5-1105.00-1125.00-12214.4-1145.00-1175.00-1265.00-14016.2-1105.00-1355.00-1705.00-1105.00-130
31.926.033.639.139.540.944.136.437.135.834.858.634.640.516.240.835.945.835.531.843.139.636.936.436.615.543.234.538.537.429.334.734.338.538.938.429.633.6
Great Lakes Analytical
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 54 of 70
ANALYTICAL1380 Busch Parkway
Buffalo Grove, Illinois 60089Email: [email protected]
(847) 808-7766 FAX (847) 808-7772
11
1 Hygieneering, Inc.J75 75 Plaza CourtMvillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 7/9/01 to 7/10/01Received: 7/1 1/01Reported: 7/20/01 13:41
• Semivolatile Organic Compounds by EPA Method 8270C7Quality Control! Great Lakes Analytical
.nalvte
latrix Spike (continued)Hexachlorobenzene
Kexachlorobutadieneexachlorocyclopentadieneexachloroethane
Indeno (1,2,3-cd) pyrene»sophorone-Methylnaphthalene
o-Cresol
f,p-Cresols>r
aphthalene•Nitroaniline
3-NitroanilineMt-NitroanilineBjitrobenzene^-Nitrophenol
4-NitrophenolBk•^•Nitrosodi-n-propylamine^J-Nitrosodiphenylamine
Pentachlorophenol^fhenanthreneVhenol^"yrene
1 ,2,4-Trichlorobenzene
1,4,5-Trichlorophenol,4,6-Trichlorophenol
Surrogate: 2-Fluorophenol^urrogate: Phenol-d6^Surrogate: Nilrobenzene-d5^Surrogate: 2-Fluorobiphenyl
Surrogate: 2.4.6- Tribromophenolmfurrogale: p-Terphenvl-d 1 4
I~1atrix Soike DUDAcenaphthene
tcenaphthyleneni l ine
Anthracene^Jenzoic acid
Date Spike SampleAnalyzed Level Result
QC Reporting Limit Recov.Result Units Recov. Limits %
RPD RPDLimit % Notes*
1070237-MS1 B107115-127/17/01 1700
1 7001 70017001 7001 7001 7001 7001 7001 7001 70017001 7001 7001 7001 7001 7001 7001 7001 7001 7001 7001 70017001 700339033901 700170033901700
1070237-MSD1 B10717/17/01 1670
16701 67016701670
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
15-12NDNDNDNDND
582 ug/kg601321622709538714667624579633535625599717646622501661549679
1090627688697
14501280600574
12201120
218 ug/kg221
26.4208168
5.00-1175.00-1105.00-1105.00-1105.00-16923.1-1105.00-1375.00-1285.00-1315.00-12618.1-1105.00-11015.8-11014.4-1105.00-1205.00-12423.2-1105.00-1275.00-1145.00-13723.7-1105.00-4025.00-11011.6-11318.8-11010.0-10910.0-11510.0-11410.0-10619.3-88.710.0-126
5.00-1405.00-1315.00-1105.00-1465.00-149
34.235.418.936.641.731.642.039.236.734.137.231.536.835.242.238.036.629.538.932.339.964.136.940.541.042.837.835.333.836.065.9
13.113.21.5812.510.1
81.8 87.173.0 85.7116 119
98.1 87.478.8 88.1
Ijreat Lakerf Analytical
// 'i
Andy^Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 5 5 of 70
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project:Project Number:
Project Manager:
2001-3495N/AGary Milkeris
Sampled: 7/9/01 to 7/1 0/01Received: 7/11/01Reported: 7/20/01 13:41
Semivolatile Organic Compounds by EPA Method 8270C/Quality ControlGreat Lakes Analytical
Analyte
Matrix Spike DUD (continued)Benz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneBenzyl alcoholBis(2-chloroethoxy)methaneBis(2-chloroethyl)etherBis(2-chloroisopropyl)etherBis(2-ethylhexyl)phthalate4-BromophenyI phenyl etherButyl benzyl phthalate4-Chloroaniline4-Chloro-3-methylphenol2-Chloronaphthalene2-Chlorophenol4-Chlorophenyl phenyl etherChryseneDibenz (a,h) anthraceneDibenzofuran1 ,2-Dichlorobenzene1 ,3-Dichlorobenzene1 ,4-Dichlorobenzene3,3 '-Dichlorobenzidine2.4-DichlorophenolDiethyl phthalate2,4-DimethylphenolDimethyl phthalateDi-n-butyl phthalate4,6-Dinitro-2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-octyl phthalateFluorantheneFluoreneH ex ach 1 oroben zeneHexachlorobutadiene
Date SpikeAnalyzed Level
SampleResult
QC Reporting Limit Recov.Result Units Recov. Limits %
RPDLimit
RPD% Notes*
1070237-MSD1 B1071 15-127/17/01 1670
16701670167016701670167016701 670167016701670167016701670167016701670167016701670167016701670167016701 6701670167016701670167016701 6701 6701 67016701670
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
227 ug/kg243267229
324270262266265852222222
94.4294238281238208227267258254263220247174332237119260310273268349
200228219
220
5.00-1495.00-1345.00-1275.00-2235.00-1208.91-11023.1-11016.6-11014.5-1105.00-1535.00-1525.00-2165.00-11017.8-1105.00-1175.03-1285.00-1105.00-1555.00-1645.00-1335.00-1175.00-1105.00-1105.00-11021.5-1105.00-1125.00-12214.4-1145.00-1175.00-1265.00-14016.2-1105.00-1355.00-1705.00-1105.00-1305.00-1175.00-110
13.614.616.013.719.416.215.715.915.951.013.313.35.6517.614.316.814.312.513.616.015.415.215.713.214.810.419.914.27.1315.618.616.316.020.912.013.713.113.2
124124121121107103
86.083.480.8115
70.792.3196100
77.777.473.0122105
76.284.984.086.6146
81.075.8145
77.1107
97.425.685.789.676.1142
79.579.582.0
84.791.284.799.677.876.881.177.074.613.988.9101
96.679.586.192.785.187.1104
84.982.282.279.916.097.9107
63.789.9122
75.959.481.083.459.084.684.189.291.4
Great Lakes Analytical
Andy JoKnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 56 of 71
I tzssm GREAT•All LAKES•fill ANALYTICAL
1
11 Hygieneering, Inc.
^7575 Plaza Court•Villowbrook, IL 60521
1380 Busch ParkwayBuffalo Grove, Il l inois 60089
Project:Project Number:
Project Manager:
2001-3495N/AGar,' Milkeris
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41
BSemivolatile Organic Compounds by EPA Method 8270C/Quality Control
1 Great Lakes Analytical
.nalvte
latrix Spike Pup (continued)Hexachlorocyclopentadiene«exachloroethane
ideno (1,2,3-cd) pyreneophorone
2-Methylnaphthalene
tCresol,p-Cresols
Naphthalene^2-NitroanilineB-NitroanilineBl-Nitroaniline
Nitrobenzened£-NitrophenolB-Nitrophenol
r4-Nitrosodi-n-propylamineN-Nitrosodiphenylamine
f entachlorophenolhenanthrene
PhenolJyreneB ,2,4-Trichlorobenzene^1,4,5-Trichlorophenol
2,4,6-Trichlorophenol
f arrogate: 2-Fluorophenolurrogate: Phenol-d6urrogate: Nitrobenzene-dS
Surrogate: 2-Fluorobiphenyl^turrogate: 2,4.6- TribromophenolB-urrogafe: p-Terphenyl-d!4
1
1
I*Creat LakesAnalvtical
1 ///
Date SpikeAnalyzed Level
SampleResult
QCResult
Reporting LimitUnits Recov. Limits
Recov.%
RPDLimit
RPD% Notes*
1070237-MSD1 B107115-127/17/01 1670
1670167016701670167016701670167016701670167016701670167016701670167016701670167016701670
334033401670167033401670
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
155259236142284190173237253218302257317264193127304
.220240438238270318677418250184507377
ug/kg 5.00-1105.00-1105.00-16923.1-1105.00-1375.00-1285.00-1315.00-12618.1-1105.00-11015.8-11014.4-1 105.00-1205.00-12423.2-1105.00-1275.00-1145.00-13723.7-1105.00-4025.00-11011.6-11318.8-11070.0-70910.0-11510.0-11410.0-106
19.3-88.710.0-126
9.2815.514.18.5017.011.410.414.215.113.118.115.419.015.811.67.6018.213.214.426.214J16.219.020. 112.515.011.015.222.6
71.290.3107
84.671.786.192.875.689.31 1 1
99.984.285.155.293.574.370.7141
88.0157
76.779.388.2
68.381.098.9115
84.7110112
82.484.582.568.178.375.882.5104118
72.584.093.983.988.385.773.3
"Refer to end of report for text of notes and definitions.
Andy Johnson, Project Manager Page 5 7 of 70
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41
Polynuclear Aromatic Compounds by EPA Method 8310/Quality ControlGreat Lakes Analytical
Analvte
Batch: 1070277BlankAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
Date Spike Sample QCAnalyzed Level Result Result
Date Prepared: 7/16/011070277-BLK17/17/01 ND
NDNDNDNDNDNDNDNDNDNDNDNDNDNDND
76.6 16.0
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*
Extraction Method: EPA 3550B
ug/kg 100200100100
90.0100100100100
90.0100100100100100100
29.0-132 96.4
LCSAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
1070277-BS17/17/01 67.2
67.267.267.267.267.267.267.267.267.267.267.267.267.267.267.216.8
16.7 ug/kg81.650.860.551.658.060.861.861.659.652.749.761.872.757. Q9.6914.2
30.8-12038.9-15832.9-12240.5-12531.2-12845.0-13238.7-13753.4-12546.5-12942.8-13437.1-11640.8-10851.0-11522.7-11629.5-12344.5-11829.0-132
24.9121
75.690.076.886.390.592.091.788.778.474.092.0108
86.214.4
84.5
Great Lake* Analyticalke» Anal;
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 58 of 7(
LAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
11 Hygieneering, Inc.
^7575 Plaza Court•Willowbrook, IL 60521B
Project:Project Number:
Project Manager:
2001-3495N/AGarv Milkeris
Sampled:Received:Reported:
7/9,01 to 7, 107/11/017/20/01 13:41
01
Polynuclear Aromatic Compounds by EPA Method 8310/Quality ControlGreat Lakes Analytical
Unalyte
•Matrix SoikeAcenaphthene
^Acenaphthylene•Anthracene^feenz (a) anthracene
Benzo (a) pyrene
f enzo (b) fluorantheneenzo (ghi) perylene
Benzo (k) fluoranthene^Zhrysene•Dibenz (a,h) anthraceneB^luoranthene
Fluorene| ndeno (1 ,2,3-cd) pyrene
•Naphthalenei^henanthrenePyrene
VKurrogate: Carbazole
Matrix Spike DUD—Acenaphthene•Acenaphthylene"Anthracene
Benz (a) anthracene•Benzo (a) pyrene•Benzo (b) fluoranthene
Benzo (ghi) peryleneBenzo (k) fluoranthene
BrhryseneB)ibenz (a,h) anthracene
Fluoranthene•rluorene•ndeno (1,2,3-cd) pyrene^Japhthalene
Phenanthrene
§yreneurrogate: Carbazole
Date SpikeAnalyzed Level
SampleResult
QC Reporting Limit Recov.Result Units Recov. Limits %
RPDLimit
RPD% Notes*
1070277-MS1 B1071 15-057/17/01 68.4
68.468.468.468.468.468.468.468.468.468.468.468.468.468.468.4
" ~ 77.7
1070277-1MSD17/17/01 64.9
64.964.964.964.964.964.964.964.964.964.964.964.964.964.964.916.2
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
Bl 07 11 5-05NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
45.3 ug/kg103
55.4119
54.957.647.357.967.049.678.351.460.180.358.176.4Tl.8
25.5 ug/kg39.443.256.347.747.043.446.269.346.570.345.959.781.253.381.49.33
10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145
29.0-132
10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145
29.0-132
66.2151
81.017480384.269.284.698.072.5114
75.187.9117
84.9112
69.0
39360.766.686.773.572.466.971.2107
71.6108
70.792.0125
82.1125
57.6
66.465.767.157.854.551.965.959.365.249.858.753.955.862.557.456.6
51.085.319.567.08.8415.13.3817.28.781.255.416.044.566.613.3511.0
jreat Lakes Anlajytical
IAnd/ Johnson, Project Manager
I
"Refer to end of report for text of notes and definitions
Page 59 of 70
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/AProject Manager: Garv Milkeris
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41
Volatile Organic Compounds by EPA Method 503578260B/Qualiry ControlGreat Lakes Analytical
Date Spike SampleAnalvte Analyzed Level Result
Batch: 1070262 Date Prepared: 7/13/01Blank 1070262-BLK1Acetone 7/13/01Benzene "Bromodichloromethane "Bromoform "Bromomethane "2-Butanone "Carbon disulfide "Carbon tetrachloride "Chlorobenzene "Chlorodibromomethane "Chloroethane "Chloroform "Chloromethane "1,1 -Dichloroethane "1,2-Dichloroethane "1,1-Dichloroethenecis-1, 2-Dichloroethene "trans- 1 ,2 -Dichloroethene "1 ,2-Dichloropropane "cis-l,3-Dichloropropene "trans- 1 ,3-Dichloropropene "Ethylbenzene "2-Hexanone "Methylene chloride "4-Methyl-2-pentanone "Styrene "1.1.2,2-Tetrachloroethane "Tetrachloroethene "Toluene "1 ,1 ,1 -Trichloroethane "1,1,2-Trichloroethane "Trichloroethene "Trichlorofluoromethane "Vinyl acetate "Vinyl chloride "Total Xylenes "Surrogate: Dibromofluoromethane " 50.0
QCResult
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
53.0
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*
Extraction Method: EPA S035B IP/T1
ug/kg 25.05.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.0010.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-134 106
Great LakeyAnalytical
///
"Refer to end of report for text of notes and definitions.
Andy Johnson, Project Manager Page 60 of 71
GREATLAKES
ANALYTICAL1380 Busch Parkway
Buffalo Grove, Illinois 60089Email: [email protected]
(847) 808-7766 FAX (847) 808-7772
1I
1 Hygieneering, Inc.J75 75 Plaza Court•Willowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 7/9/01 to 7/1 0/01Received: 7/11/01Reported: 7,20/01 13:41
• Volatile Organic Compounds by EPA Method 5035/8260B/Quality Control• Great Lakes Analytical
^J Analyte
B3lank (continued)Surrogate: 1.2-Dichloroethane-d4
^^urrogate: Toluene-d8^Surrogate: 4-Bromofluorobenzene
LCS•Acetone^Benzene
Bromodichloromethane^romoform•BromomethaneB2-Butanone
Carbon disulfideg«Carbon tetrachlorideBrhlorobenzene^-hlorodibromomethane
ChloroethaneBChloroformBrhloromethane
1,1 -Dichloroethane
I1 ,2-Dichloroethane, 1 -Dichloroetheneis- 1 ,2-Dichloroethene
trans-1 . 2-Dichloroethene
§,2-Dichloropropaneis- 1 ,3-Dichloropropene
trans-1 ,3-DichloropropeneEthvlbenzene
B--HexanoneBviethylene chloride
4-Methyl-2-pentanoneMftyrene|l , 1 ,2,2-Tetrachloroethane
1 etrachloroetheneToluene
§,1 ,1 -Trichloroethane, 1 ,2-Trichloroethane
Trichloroethene^Trichlorofluoromethane
1 ,•breat La/es Analytical
Date Spike SampleAnalyzed Level Result
1070262-BLK17/73/07 50.0
50.050.0
1070262-BS17/13/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0
QCResult
54.052.357.3
57.953.057.857.826.164.447.754.056.659.440.049.121.843.956.150.248.744.454.358.566.152.860.045.358.953.356.458.051.851.455.552.7194
Reporting LimitUnits Recov. Limits
ug/kg 50.8-14582.0-12176.8-113
ug/kg 10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-13460.0-13476.4-12561.8-13214.6-241
"Refer to end of report
Recov. RPD RPD% Limit % Notes*
705705703
116106116116
52.2129
95.4108113119
80.098.243.687.8112100
97.488.8109117132106120
90.61181071131161041031 1 1105NR
r for text of notes and definitions./ 4//L
Antiy Johnson, Project Manager
I
Page 61 of 70
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Project:Project Number:
Project Manager:
2001-3495N/AGan.' Milkeris
Sampled: 7/9/01 to 7/1 0/01Received: 7/1 1/01Reported: 7/20/01 13:41
Volatile Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical
Analvte
LCS (continued)Vinyl acetateVinyl chlorideTotal XvlenesSurrogate: DibromofluoromethaneSurrogate: I,2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
LCS PupAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethenecis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- 1,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTerrachloroetheneToluene
ti — _ — .
Date SpikeAnalyzed Level
1070262-BS17/13/01 50.0
50.0150
50.050.050.050.0
1070262-BSDl7/17/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0
Sample QC Reporting Limit Recov.Result Result Units
48.6 ug/kg53.5269
~' 47.3 "51.051.051.6
83.1 ug/kg49.849.355.563.450.946.734.452.455.434.946.918.443.647.950.650.545.950.849.755.149.955.554.755.750.155.451.X45.1
Recov. Limits
10.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113
10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-134
%
97.2107179
94.6102102103
16699.698.6
111127102
93.468.81051 1 1
69.893.836.887.295.8101101
91.8102
99.4110
99.81 1 11091 1 11001 1 1104
90.2
RPDLimit
34541.442.057.461.9173126
43.539.041.690.343.571.841.868.647.539.343.038.141.557.242.7128
67.4119
37.254.646.342.6
RPD% Notes*
35.56.2316.24.4183.523.42.1244.37.346.9613.64.5816.9
0.68615.6
0.9953.633.326.6416.318.26.037.79
. 18.46 .116.761.7910.914.2
"Refer to end of report for text of notes and definitions.
Andy Johnsort, Prdject Manager Page 62 of 7 C
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
1~J Hygieneering, Inc.J 75 75 Plaza Court•Willowbrook, IL 60521
•
Project: 2001-3495Project Number: N/A
Project Manager: Garv Milkeris
Sampled: 7/9/01 to 7/1 0,01Received: 7/1 1/01Reported: 7,20/01 13:41
Volatile Organic Compounds by EPA Method 5035/8260B/Quality Control
1•| Analyte
jpLCS DUD (continued')1,1,1 -Trichloroethane
f1 , 1 ,2-Trichloroethane
richloroethenerichlorofluoromethane
Vinyl acetate•Vinyl chloride•Total Xylenes
Surrogate: DibromofluoromethaneSurrogate: 1 , 2-Dichloroethane-d4
^Surrogate: Toluene-d8^Surrogate: 4-Bromofluorobenzene
•Batch: 1070296•Blank^Acetone
BenzeneBBromodichloromethaneBSromoform
Bromomethane^2-Butanone•Carbon disulfideBcarbon tetrachloride
Chlorobenzene•Chlorodibromomethane•Chloroethane
ChloroformChloromethane
11 , 1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethene
^cis- 1 . 2-DichloroetheneBtrans-1 ,2-Dichloroethene™1 ,2-Dichloropropane
cis-1 ,3-Dichloropropene•trans-1 ,3-Dichloropropene•Ethylbenzene
2-Hexanone_Methylene chloride
Great Lakes f
Date Spike SampleAnalyzed Level Result
1070262-BSP17/17/01 50.0
50.050.050.050.050.0150
" "" " " "50.050.050.050.0
Date Prepared: 7/17/011070296-BLK17/17/01"""n
"
»
..11
"
„11
ii»"11
..11
Analytical
QCResult
42.251.047.9162
57.233.6205
50.257.749.349.7
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*
ug/kg 60.0-134 84.4 44.2 19.976.4-125 102 53.2 8.4561.8-132 95.8 43.5 9.1614.6-241 NR 115 18.010.0-161 114 92.1 15.957.9-143 67.2 81.0 45.760.0-141 137 40.1 26.681.2-134 10050.8-145 Iu382.0-121 98.676.8-113 99.4
Extraction Method: EPA 503SB tP/TI
ug/kg 25.05.005.005.005.0010.05.005.005.005.005.005.005.005.005.005.005.005.005.005.005.005.0010.05.00
I
ircat Uakes Analytical
,' I/i/1
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 63 of 70
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Volatile
Analvte
Blank (continued)4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene1 , 1 ,1 -Trichloroethane1 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 . 2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
LCSAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 ,1 -Dichloroethane1 ,2-Dichloroethane1 . 1 -Dichloroethenecis-1 . 2-Dichloroethenetrans-1, 2-Dichloroethene1 ,2-Dichloropropanecis- 1 ,3-Dichloropropene
Project:Project Number:
Project Manager:
2001-3495N/AGarv Milkeris
Sampled: 7/9/01 to 7,10/01Received: 7/11/01Reported: 7/20/01 13:41
Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical
Date SpikeAnalvzed Level
1070296-BLK17/17/0111
"nn11
"""ii11
11
" 50.0~'50.050.050.0
1070296-BS17/17/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0
Sample QC Reporting Limit Recov. RPD RPDResult Result Units
ND ug/kgNDNDNDNDNDNDNDNDNDNDND
' 55.0 "55.357.652.5
83.8 ug/kg51.251.753.247.966.346.247.351.152.033.847.434.044.649.249.650.446.951.854.5
Recov. Limits
10.05.005.005.005.005.005.005.005.0010.05.005.00
81.2-~13450.8-14582.0-12176.8-113
10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-124
°/o Limit % Notes*
7/0/ / /703705
168102103106
95.8133
92.494.6102104
67.694.868.089.298.499.2
10193.8104109
Great Lakes/\nalytical "Refer to end of report for text of notes and definitions
Andy Johnson, Project Manager Paue64 of 7<
*-AKE5
ANALYTICAL1380 Busch Parkway
Buffalo Grove. Illinois 60089Email: [email protected]
(847) 808-7766 FAX (847) 808-7772
1fHygieneering, Inc.
J7575 Plaza Court•Willowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 7Received: 7Reported: 7
\
/9/OI to 7. 10/01/1 1/01/20/01 13:41
• Volatile Organic Compounds by EPA Method 5035/8260B/Quality Control• Great Lakes Analytical
_[Analvte
I '•XS (continued)
trans-1 ,3-Dichloropropene^Ethylbenzene•2-Hexanone•vlethylene chloride
4-Methyl-2-pentanone
ttyrene, 1 ,2,2-Tetrachloroethane
TetrachloroetheneToluene
Bl ,1,1 -TrichloroethaneBl , 1 ,2-Trichloroethane
TrichloroetheneMjTrichlorofluoromethane•Vinyl acetate^^/inyl chloride
Total Xylenes
f urrogate: Dibromofluoromelhaneurrogate: 1 . 2-Dichloroethane-d4
Surrogate: Toluene-d8
C arrogate: 4-Bromofluorobenzene
CSDuDAcetone
•Benzene^promodichloromethane
Bromoform^Bromomethane•2-ButanoneBCarbon disulfide
Carbon tetrachlorideaChlorobenzeneBrhlorodibromomethane^3hloroethane
Chloroform
ff hloromethane,1 -Dichloroethane
1 ,2-Dichloroethane^1 , 1 -Dichloroethene
Date Spike Sample QC Reporting Limit Recov.Analyzed Level Result Result Units Recov. Limits %
1070296-BS17/17/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.0150
50.050.050.050.0
1070296-BSD17/17/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0
62.6 ug/lcg48.459.947.558.049.753.252.348.247.454.649.2170
31.258.5253
50.257.657.552.4
82.1 ug/lcg52.252.560.667.557.746.338.056.460.344.949.118.745.151.749.8
63.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-13460.0-13476.4-12561.8-13214.6-24110.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113
10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-129
12596.8120
95.0116
99.4106105
96.494.8109
98.4NR
62.4117169100103103105
164104105121135115
92.676.0113121
89.898.237.490.2103
99.6
RPDLimit
34541.442.057.461.9173126
43.539.041.690.343.571.84 1 . X68.647.5
RPD% Notes*
2.411.941.9213.234.014.5
0.21621.810.215.128.23.5258.11 . 1 !4.57
0.402
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 65 of 70
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/AProject Manager: Gary Milkeris
Sampled:Received:Reported:
7/9/01 to 7/1 0/017/11/017,20/01 13:41
Volatile Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical
Analyte
LCS Pup (continued)cis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene1 ,1 ,1 -Trichloroethane1 ,1 ,2-TrichloroethaneTrichloroetheneTrichiorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 ,2-Dichloroethdne-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
Batch: 1070323BlankAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethane
Date Spike SampleAnalyzed Level Result
1070296-BSD17/17/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0150
50.050.050.050.0
Date Prepared: 7/18/011070323-BLK17/20/01"11
"11
""-""
QCResult
53.746.754.353.658.652.660.656.060.852.962.154.147.643.356.749.391.160.935.6269
50.357.649.049.3
Reporting LimitUnits Recov. Limits
ug/lcg 64.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-13460.0-13476.4-12561.8-13214.6-24110.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113
Recov.%
10793.4109107117105121112122106124108
95.286.6113
98.6182122
71.2179101103
98.098.6
Extraction Method: EPA 5035B
NDNDNDNDNDNDNDNDNDNDND
ug/kg 1250250250250250500250250250250250
RPDLimit
39.343.038.141.557.242.7128
67.4119
37.254.646.342.644.253.243.5115
92.181.040.1
[P/T1
RPD% Notes*
5.770.427
4.691.856.618.13
0.83016.45.046.4315.72.821.259.043.60
0.20360.564.648.75.75
Great LakesAnalyticalesAnalytic
/i
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 66 of 70
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
IJ Hygieneering, Inc.
^7575 Plaza CourtpVillowbrook, IL60521
•
Project:Project Number:
Project Manager:
2001-3495N/AGarv Milkeris
Sampled:Received:Reported:
7/9/01 to 7/1 0/017/11/017,20/01 13:41
Volatile Organic Compounds by EPA Method 5035/8260B7Quality ControlGreat Lakes Analytical
T Date Spike Sample_|_Analyte Analyzed Level Result
Blank (continued) 1070323-BLK1Chloroform 7/20/01
jChloromethane "B , 1 -Dichloroethane "™ ,2-Dichloroethane "
1,1-Dichloroethene "
(is- 1, 2-Dichloroethene "-ans- 1 ,2-Dichloroethene "
1 ,2-Dichloropropane "^;is-l,3-Dichloropropene "Brans- 1 ,3-Dichloropropene "Btthylbenzene "
2-Hexanone "||vlethylene chloride "•l-Methyl-2-pentanone "^Styrene "
1 , 1 ,2,2-Tetrachloroethane "
tetrachloroethene "oluene "
1,1,1 -Trichloroethane "J , 1 ,2-Trich 1 oroethane "•Trichloroethene "^Trichlorofluoromethane "
Vinyl acetate "
f inyl chloride "otal Xylenes "
Surrogate: Dibromofluoromethane " 50.0^urrogate: 1.2-Dichloroethane-d4 " 50.0^Kurrogate: Toluene-d8 " 50.0Wfurrogate: 4-Bromofluorobenzene " 50.0
QCResult
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
57.351.049.945.8
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*
ug/kg 250250250250250250250250250250250500250500250250250250250250250250500250250
81.2-134 11550.8-145 10282.0-121 99.876.8-113 91.6
•LCS•\cetone^Benzene
Bromodichloromethane»romoformromomethane
2-Butanone^Tarbon disulfide
1070323-BS17/20/01 2500
250025002500250025002500
3340301025902090321039301270
ug/kg 10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-175
13412010483.612815750.8
jreat LaWs Analvtical
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 67 of 70
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Project: 2001-3495Project Number: N/'A
Project Manager: Gary Milkeris
Sampled: 7/9/01 to 7/10/01Received: 7/11/01Reported: 7/20/01 13:41
Volatile Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical
Analvte
LCS (continued)Carbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 ,1 -Dichloroethane1 ,2-Dichloroethane1 ,1 -Dichloroethenecis-1, 2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrach 1 oroeth eneToluene1,1,1 -Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1.2-Dichloroelhane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
LCS DimAcetoneBenzeneBromodichloromethane
Date Spike SampleAnalvzed Level Result
1070323-BS17/20/01 2500
250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500750050.050.050.050.0
1070323-BSD17/20/01 2500
25002500
QC Reporting Limit Recov. RPD RPDResult Units
2320 ug/kg2200214033703500
5843590217020003200280031102650300023203790286033302320209021802800282028102540269040301 1 1 0728084.558. 164.252. 1
5590 ug/kg32203030
Recov. Limits
51.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-13460.0-13476.4-12561.8-13214.6-24110.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113
10.0-16662.1-13864.3-125
% Limit % Notes*
92.888.085.6135140
23.4144
86.880.0 .128112124106120
92.8152114133
92.883.687.2112113112102108161
44.497.1169116128104
NR 345 50.3129 41.4 7.23121 42.0 15 .1
Great LaJ/es Analytical
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 68 of 70
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
1IHygieneering, Inc.17575 Plaza Court[Willowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 7/9/0 1 to 7, 1 0/0 1Received: 7 /11 /01Reported: 7,20/01 13:41
Volatile Organic Compounds by EPA Method 5035/8260B/Quality Control
1
Cnalyte
CS Pup (continued)Bromoformbromomethanep-ButanoneCarbon disulfideCarbon tetrachloride[ChlorobenzenefchlorodibromomethaneChloroethane•ChloroformjChloromethane1 , 1 -Dichloroethane1 ,2-DichIoroethane
11 , 1 -Dichloroethene|eis-l ,2-Dichloroethenetrans-1 ,2-Dichloroethene|) ,2-Dichloropropanepis-1 ,3-DichloropropeneTrans-1 ,3-DichloropropeneEthylbenzene
fc-HexanoneIvlethylene chloride4-Methyl-2-pentanone
^tyrene
1 , 1 ,2,2-Tetrachloroethaneiretrach 1 oroeth en eToluene
•1,1,1 -Trichloroethane•1 , 1 ,2-TrichloroethaneTrichloroethene
TrichlorofluoromethanePv'inyl acetatetyinyl chlorideTotal Xylenes
^urrogate: Dibromofluoromethane^Surrogate: 1.2-Dichloroethane-d4^Surrogate: Toluene-d8Surro gate: 4-Bromofluorobenzene
1Great Lake/ Analytical
Great Lakes Analytical
Date Spike SampleAnalyzed Level Result
1070323-BSD17/20/01 2500
2500250025002500250025002500250025002500250025002500250025002500250025002500250025002500
250025002500250025002500250025002500750050.050.050.050.0
QCResult
21902780430029002860233022702760396038803480275030603610329034102870315024503990309035702440220024203020343029602780265038304280762089.670.566.252.8
Reporting LimitUnits Recov. Limits
ug/kg 47.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-13460.0-13476.4-12561.8-13214.6-24110.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113
Recov.%
87.61 1 1172116114
93.290.8110158155139110122144132136115126
98.0160124143
97.6
88.096.8121137118111106153171102179141132106
"Refer to end of report for text
RPDLimit
57.461.9173126
43.539.041.690.343.571.841.868.647.539.343.038.141.557.242.7128
67.4119
37.254.646.342.644.253.243.5
11592.181.040.1
of notes
RPD% Notes*
4.6714.29.1278.220.55.745.9020.412.1148
3.5323.641.611.816.49.238.144.885.455.138.407.255.045.1310.47.7319.25.228.451.875.10118
4.92
and definitions
Andy Johnson, Project Manager Page 69 of 70
I
GREAT
1380 Busch Parkway Email: [email protected] Buffalo Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772
Hygieneering, Inc. Project: 2001-3495 Sampled: 7/9,01 to 7 10.017575 Plaza Court Project Number: N/A Received: 7/11/01Willowbrook, IL 60521 Project Manager: Gary Milkeris Reported: 7,20/01 13:41
Notes and Definitions
_# Note
A The concentration of the analyte detected in the sample is characteristic of a laboratory artifact.
Gl The recovery of one or more analytes in the matrix QC (MS/MSD) associated with this sample is above the laboratory's establishedacceptance criteria. Refer to the included QC reports for more detail.
G12 The reporting limit of this sample/analyte is elevated due to sample matrix and/or other effects.
Gl 5 The relative percent difference (RPD) of one or more analytes in the matrix QC (MS/MSD) associated with this sample is above thelaboratory's established acceptance limits. Refer to the included QC reports for more detail.
G19 The relative percent difference (RPD) of one or more anaiytes in the laboratory control QC (BS/BSD) associated with this sampleis above the laboratory's established acceptance limits. Refer to the included QC reports for more detail.
G2 The recovery of one or more analytes in the matrix QC (MS/MSD) associated with this sample is below the laboratory's establishedacceptance criteria. Refer to the included QC reports for more detail.
G3 The recovery of one or more analytes in the laboratory control QC (BS/BSD) associated with this sample is above the laboratory'sestablished acceptance criteria. Refer to the included QC reports for more detail.
G4 The recovery of one or more analytes in the laboratory control QC (BS/BSD) associated with this sample is below the laboratory';established acceptance criteria. Refer to the included QC reports for more detail.
O2 One or more internal standard recoveries were below the method specified acceptance criteria.
04 The recovery for this analyle is below the laboratory's established acceptance criteria.
05 The recovery for this analyte is above the laboratory's established acceptance criteria.
DET Analyte DETECTED
ND Analyte NOT DETECTED at or above the reporting limit
NR Not Reported
dry Sample results reported on a dry weight basis
Recov. Recovery
RPD Relative Percent Difference
Great La^es AnalyticalT /
Andy Johnson, Project Manager Page 70 of 70
ESI LAKESANALYTICAL
(847) 808-7766FAX (847) 808-7772
(414) 570-9460FAX (414) 570-9461
LAKhS
ANALYTICAL(847) 808-7766
FAX (847) 808-7772(414) 570-9460
FAX (414) 570-9461
Client: H£lflVff/n* B/// To: TAT: (STO/ 4 DAY 3 DAY 2 DAY 1 DAY 4 HRS
Address: 7^7 Address:D YES - TAT is critical
D NO - TAT is not critical
DATE RESULTS NEEDED:
I L - i ;pnw RFC.FIPT
Report to: QPhone »:Fa**:
State &Program:
Phone #: f JFax #: ? )
Deliverable Package Needed:D STD D Oilier
Air Bill No.
Project: 2cc4> - . 34 -5"
Sampler:
not BottlesPreservative Used
PO/Quote #:
JJF/ELD /D, LOCATION
LABOnATORYID NUMBER
^L
-^LPID-(fOP
7-10-0)
PID: 2-CO
3
X-~7
p/0-'7^IT - 13
P/D:
5J
P/D: 3XIT
P/D: XU -b
P/D:
UPID: ^10,000
X'U ftTcr- 2:5
PfD-g>.OOQ-7
10J
P/D: .f?a//A/QV*SH£
PL /
RECEIVED RECEIVED
COMMENTS:
RAGE " 2- OF
I
I
I
I
I
I
I
I
i
GREATLAI\CO 1380 Busch Parkway Email: [email protected] Buffalo Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772
July 31, 2001
I
Gary MilkerisHygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
RE: 2001-3495
Dear Gary Milkeris
Enclosed ars the results of analyses for sample(s) received by the laboratory on July 19, 2001. If you have anyquestions concerning this report, please feel free to contact me.
Sincerely,
7,Andy JohnsonProject Manager
»,„• GREAT1LAKES
ANALYTICAL1380 Busch Parkway
Buffalo Grove, Illinois 60089Email: [email protected]
(847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Sampled: 7/13/01Received: 7/19/01Reported: 7/31/01 11:52
ANALYTICAL REPORT FOR SAMPLES:
Sample Description Laboratory Sample Number Sample Matrix Date Sampled
B18
B21
B107244-01
B107244-02
Water
Water
7/13/01
7/13/01
GreatA-aKes Analytical
Andy Johnson, Project Manager
The results in this report apply to the samples analyzed in accordance with the chain of custody document.Tins analytical report must be reproduced in its entirety.
Page 1 of 1
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
1i
Hygieneering, Inc.
— 7575 Pla2a Court• Willowbrook, IL 60521f
1*T
1 Analyte
IBISAcetone
»BenzeneBromodichloromethaneBromoformBromomethane
12-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzene
• Chlorodibromomethane• Chloroethane
Chloroform
IChloromethane1 , 1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethene
Icis- 1 ,2-Dichloroethenetrans-1, 2-Dichloroethene1 ,2-Dichloropropane
— cis- 1 ,3-Dichloropropene• trans-1 ,3-DichloropropeneW Ethylbenzene
2-Hexanone
1Methylene chloride4-Methyl-2-pentanoneStyrene1 ,1 ,2,2-Tetrachloroethane
• TetrachloroetheneQ Toluene
1,1,1 -Trichloroethane
§1 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetate
§Vinyl chlorideTotal XylenesSurrogate: Dibromofluoromethane
« Surrogate: \.2-Dichloroethane-d4
I
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B107244-011070436 7/23/01 7/30/01 10.0
2.002.002.002.0010.02.002.002.002.002.002.002.002.002.002.002.002.002.002.002.002.0010.02.0010.02.002.002.002.002.002.002.002.002.002.002.00
91.1 '-11185.1-104
Sampled: 7/13/01Received: 7/19/01Reported: 7/31/01 11:52
Result Units Notes*
Water G1S.G2.G20.G?54.6 ug/l ANDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND " 'NDNDNDNDNDNDNDNDNDNDNDNDNDND
91.2 %IDS " O5
• Great Likes Analytical
IAndy lohnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 2 of 11
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Sampled: 7/13/01Received: 7/19/01Reported: 7/31/01 11:52
Volatile Organic Compounds by EPA Method 8260BGreat Lakes Analytical
Analvte-BatchNumber
DatePrepared
DateAnalyzed
SurrogateLimits
ReportingLimit Result Units Notes*
B18 (continuedSurrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
1070436 7/23/01B107244-01
7/30/01 ~95.1-10589.6-105
Water G15.G2.G20.G3"108 % OS105
Greht Lakes Analytical
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 3 of 1
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
111
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Project:Project Number:
Project Manager:
2001-34952001-3495Garv Milkeris
Sampled:Received:Reported:
7/13/017/19/017,31/01 11:52
Volatile Organic Compounds by EPA Method 8260BGreat Lakes Analytical
gB21 Bl 07244-02Acetone 1070436 7/23/01 7/24/01
_ BenzeneH Bromodichloromethane " " "9 Bromoform " " "
Bromomethane " " "
12-Butanone " " "Carbon disulfide " " "Carbon tetrachloride " " "Chlorobenzene " " "
1Chlorodibromomethane " " "Chloroethane " " "Chloroform " " "
I Chloromethane " " "1,1-Dichloroethane1 ,2-Dichloroethane " "1,1-Dichloroethene
t cis-l,2-Dichloroethenetrans-1, 2-Dichloroethene " " "1 ,2-Dichloropropane " " "cis-l,3-Dichloropropene " " "
H trans- 1 ,3-Dichloropropene " " "1 Ethylbenzene " " "
2-Hexanone " " "
1Methylene chloride "4-Methyl-2-pentanone " " "Styrene1,1,2,2-Tetrachloroethane " " "
1Tetrachloroethene " " "Toluene " " "1,1,1 -Trichloroethane " " "
t l,l,2-Trichloroethane " "Trichloroethene "Trichlorofluoromethane " " "Vinyl acetate " " "
§Vinyl chloride " "Total XylenesSurrogate: Dibromofluoromethane " " " 9 I.I - I I I
-Surrogate: 1 .2-Dichloroethane-d4 " " " 85.I-HI4
I /
2000400400400400
2000400400400400400400400400400400400400400400400400
2000400
2000400400400400400400
10000400400400400
NDNDNDNDNDNDNDNDNDNDNDNDND632NDND
32200954NDNDNDNDNDNDNDNDNDNDNDNDND
937000NDND
6560ND
98.897.4
Water G12.G15.G2.G3ug/l11
..11
"""
11
:"""I!
"
G17G17
""
»11
"i,
"11
G17""
G16"
11
G17
%
'Great Lfikes/Analytical
^ 'l-i
"Refer to end of report for text (if notes and dc'finilu
AndyiJorrhson, Project Manager Page 4 of
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL60521
Project: 2001-3495Project Number: 2001 -3495
Project Manager: Gary Milkeris
Sampled: 7/13/01Received: 7/19/01Reported: 7/31/01 11:52
Volatile Organic Compounds by EPA Method S260BGreat Lakes Analytical
AnalyteBatchNumber
DatePrepared
DateAnalyzed
SurrogateLimits
ReportingLimit Result Units Notes*
B21 (continued^ Bl 07244-02Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
1070436 7/23/01 7/24/01 95.1-10589.6-105
10996.2
Water C12.C15.G2.G3% O5
Great L^kes Analytical
Andy JoVnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 5 of 1
1111
—.—•GREAT•All LAKES•&• ANALYTICAL
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Project:Project Number:
Project Manager:
2001-34952001-3495Gary Milkeris
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Sampled:Received:Reported:
7/13/017/19/017/31/01 11:52
Volatile Organic Compounds by EPA Method 8260B/Quality ControlGreat Lakes Analytical
^ Date Spike SampleAnalvte Analyzed Level Result
• Batch: 1070436 Date Prepared: 7/23/01Blank 1070436-BLK1
_ Acetone 7/23/01B Benzene "™ Bromodichloromethane "
Bromotbrm "
1Bromomethane . "2-Butanone "Carbon disulfide "Carbon tetrachloride "
• Chlorobenzene "• Chlorodibromomethane "
Chloroethane "
1Chloroform "Chloromethane "1,1 -Dichloroethane "1 ,2-Dichloroethane "
11,1-Dichloroethene "cis- 1 ,2-Dichloroethene "trans- 1 ,2-Dichloroethene "
_ 1,2-Dichloropropane "• cis-1 ,3-Dichloropropene "™ trans- 1 ,3-Dichloropropene "
Ethylbenzene "to 2-Hexanone "• Methylene chloride "
4-Methyl-2-pentanoneStyrene "
• 1,1,2,2-Tetrachloroethane "P Tetrachloroethene "
Toluene
11, 1,1 -Trichloroethane "1 ,1 ,2-TrichloroethaneTrichloroethene "Trichlorofluoromethane "
• Vinyl acetate "• Vinyl chloride "
Total Xylenes "^Surrogate: Dibromofluoromethane " 50.0
1 f
QCResult
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
46.8
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*
Extraction Method: EPA S030B (P/T)
ug/l 10.02.002.002.002.0010.02.002.002.002.002.002.002.002.002.002.002.002.002.002.002.002.0010.02.0010.02.002.002.002.002.002.002.002.002.002.002.00
91. 1-1 II 93.6
i Great Lakes Analytical
I
I
Anay Johnson, Project Manager Page 6 of 1 1
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
I
1Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method
Analvte
Blank (continued)Surrogate: 1 . 2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
LCSAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethenecis-1, 2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis- 1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 .1 ,2,2-TetrachloroethaneTetrachloroetheneToluene1.1,1 -Trichloroethane1 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane
Great Lakes
Date Spike SampleAnalyzed Level Result
1070436-BLK17/23/01 50.0
50.050.0
1070436-BS17/23/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0
Analytical
QCResult
45.653.948.9
89.658.054.847.641.553.599.645.348.046.742.354.640.960.650.075.455.159.864.159.565.851.870.071.760.350.545.543.053.846.152.753.362.3
Sampled: 7/13/01Received: 7/19/01Reported: 7/31/01 11:52
8260B/Quality Control
Reporting LimitUnits Recov. Limits
ug/l 85.1-10495.1-10589.6-105
ug/l 10.0-19484.9-11574.3-13070.1-12010.0-25810.0-14743.4-14660.5-13885.4-11578.8-11610.0-45574.5-13478.7-12876.8-12066.7-12972.7-12587.0-12377.9-11988.3-11581.2-12075.2-12684.3-11921.4-14262.5-14038.2-14186.6-11713.2-19776.6-12086.3-12063.5-14684.5-12451.4-15310.0-586
i
Recov. RPD RPD% Limit % Notes*
i
91.2108
97.8
179116110
95.283.0107199
90.696.093.484.6109
81.8'121100151110120128119132104140143121101
91.086.0108
92.2105107125
Great Lak^ Analytical
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 7 of 1 1
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
I1
Hygieneering, Inc._ 7575 Plaza Court• Willowbrook, IL 60521
•
Project:Project Number:
Project Manager:
2001-34952001-3495Gary Milkeris
Sampled: 7/13/01Received: 7/19/01Reported: 7/31/01 11:52
Volatile Organic Compounds by EPA Method 8260B/Quality Control
1^_ Analvte
1 '• LCS (continued)
Vinyl acetate
§Vinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 ,2-Dichloroethane-d4
1Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
_ Matrix Spike• Acetone• Benzene
Bromodichloromethane
t BromoformBromomethane2-ButanoneCarbon disulfide
• Carbon tetrachloride• Chlorobenzene
Chlorodibromomethane
IChloroethaneChloroformChloromethane1 , 1 -Dichloroethane
t l ,2-Dichloroethane1 ,1 -Dichloroethenecis-1 ,2-Dichloroethene
^ trans-1, 2-Dichloroethene• 1,2-DichloropropaneB cis-l,3-Dichloropropene
trans-1 ,3-Dichloropropene
I Ethylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanone
• Styrene• 1 . 1 ,2,2-Tetrachloroethane
Tetrach 1 oroethene^ Toluene
Great Lakes
Date SpikeAnalyzed Level
1070436-BS17/23/01 50.0
50.0150
50.050.050.050.0
SampleResult
Analytical
QCResult
39.443.7153
44.744.846.345.0
Reporting LimitUnits Recov. Limits
ug/l 10.0-21971.0-12088.3-11891.1-11185.1-10495.1-10589.6-105
Recov. RPD RPD% Limit % Notes*
78.887.4102
89.489.692.690.0
1070436-MS1 B107220-017/26/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0
52.6NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
66.448.448.941.014.140.151.137.049.345.768.149.327.944.849.015.451.442.549.944.936.949.849.344.750.049.352.148.449.4
ug/l 10.0-26971.4-11565.3-13454.6-13210.0-17610.0-20123.4-14326.3-13377.4-10872.8-11710.0-29370.8-12461.3-10963.3-11454.5-13736.1-11564.8-12954.7-11377.8-11467.3-11757.3-12468.3-11110.0-22545.6-15010.0-20849.7-12620.6-22345.1-11371.3-118
27.696.897.882.028.280.2102
74.098.691.4136
98.655.889.698.030.8103
85.099.889.873.899.698.689.4100
98.6104
96.898.8
kes Analytical
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 8 of 11
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.75 75 Plaza CourtWillowbrook. IL 60521
Project:Project Number:
Project Manager:
2001-34952001-3495Gary Milkeris
Sampled: 7/13/01Received: 7/19/01Reported: 7/31/01 1:52
Volatile Organic Compounds by EPA Method 8260B/QuaIity ControlGreat Lakes Analytical
Analvte
Matrix Spike (continued)1,1,1 -Trichloroethane1 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 ,2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
Matrix Spike DUDAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethenecis-1, 2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis- 1 ,3-Dichloropropenetrans- 1,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-M ethy 1-2-pentanone
Date SpikeAnalyzed Level
SampleResult
QC Reporting LimitResult Units Recov. Limits
Recov.%
RPDLimit
RPD% Notes'
1070436-MS1 B107220-017/26/01 50.0
50.050.050.050.050.0150
50.050.050.050.0
NDNDNDNDNDNDND
48.7 ug/l51.941.649.840.129.4156
44.944.544.845.6
42.5-12870.1-13953.5-10610.0-41710.0-23937.4-11370.8-11191.1-11185.1-10495.1-10589.6-105
97.4104
83.299.680.258.8104
89.889.089.691.2
1070436-MSD1 B107220-017/26/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0
52.6NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
59.1 ug/l48.348.741.814.239.651.237.848.845.757.047.727.443.448.420.050.742.249.444.438.050.046.244.347.1
10.0-26971.4-11565.3-13454.6-13210.0-17610.0-20123.4-14326.3-13377.4-10872.8-11710.0-29370.8-12461.3-10963.3-11454.5-13736.1-11564.8-12954.7-11377.8-11467.3-11757.3-12468.3-11110.0-22545.6-15010.0-208
13.096.697.483.628.479.2102
75.697.691.4114
95.454.886.896.840.0101
84.498.888.876.0100
92.488.694.2
73.819.115.636.245.761.623.626.212.223.936.910.620.112.727.223.019.617.416.415.726.313.558.311.469.7
71.90.2070.410
1.930.707
1.250
2.141.02
017.63.301.813.171.2326.01.96
0.7081.011.122.94
0.4016.49
0.8995.97
Great Lakp Analytical
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 9 of 1
LAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
I1
Hygieneering, Inc.
17575 Plaza CourtWillowbrook, IL 60521
1
«Analyte
Matrix Spike Pup (continued)Styrene
11 , 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene1,1,1 -Trichloroethane
M 1,1,2-Trichloroethane• Trichloroethene
Trichlorofluoromethane
1Vinyl acetateVinyl chlorideTotal XylenesSurrogate: Dibromofluoromethane
1Surrogate: 1 . 2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
1
1
1
1
1
1
|Great L«(kes Analytical
1 ,/_-_Andy Johnson, Project Manager
1
Project: 2001-3495Project Number: 2001-3495
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA MethodGreat Lakes Analytical
Date Spike Sample QCAnalyzed Level Result Result
1070436-MSD1 B107220-017/26/01 50.0 ND 49.1
50.0 ND 50.550.0 ND 48.350.0 ND 49.550.0 ND 47.850.0 ND 51.050.0 ND 39.350.0 ND 50.550.0 ND 38.550.0 ND 30.8150 ND 155
50.0 43.350.0 44.150.0 44.350.0 45.3
Sampled: 7/13/01Received: 7/19/01Reported: 7/31/01 11:52
8260B/Quality Control
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes1
ug/l 49.7-126 98.2 18.6 0.40720.6-223 101 50.3 2.9345.1-113 96.6 17.6 0.20771.3-118 99.0 19.4 0.20242.5-128 95.6 18.4 1.8770.1-139 102 32.5 1.9453.5-106 78.6 20.9 5.6910.0-417 101 29.2 1.4010.0-239 77.0 34.5 4.0737.4-113 61.6 23.5 4.6570.8-111 103 12.4 0.96691.1-111 86.685.1-104 88.295.1-105 88.689.6-105 90.6
"Refer to end of report for tc.rl of notes and definitions
Page 1 0 of 1 1
mLAKF9fnrvt'J 1380 Busch Parkway Email: [email protected] Buffalo Grove, Illinois 60089 (847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc. Project: 2001-3495 Sampled: 7/13/017575 Plaza Court Project Number: 2001-3495 Received: 7/19/01Willowbrook. IL 60521 Project Manager: Gary Milkeris Reported: 7/31/01 11:52
Notes and Definitions
# Note
A The concentration of the analyte detected in the sample is characteristic of a laboratory artifact.
G12 The reporting limit of this sample/analyte is elevated due to sample matrix and/or other effects.
G15 The relative percent difference (RPD) of one or more analytes in the matrix QC (MS/MSD) associated with this sample is above thelaboratory's established acceptance limits. Refer to the included QC reports for more detail.
Gl 6 The percent recovery of the internal standard used to quantitate this analyte is below the method specified limits.
Gl 7 The percent recovery of the internal standard used to quantitate this analyte is above the method specified limits.
G2 The recovery of one or more analytes in the matrix QC (MS/MSD) associated with this sample is below the laboratory's establishedacceptance criteria. Refer to the included QC reports for more detail.
G20 This analyte was initially analyzed within holdtime; however, reanalysis at a dilution was performed outside the method specifiedholdtime.
G3 The recovery of one or more analytes in the laboratory control QC (BS/BSD) associated with this sample is above the laboratory's-established acceptance criteria. Refer to the included QC reports for more detail.
OS The recovery for this analyte is above the laboratory's established acceptance criteria.
DET Analyte DETECTED
ND Analyte NOT DETECTED at or above the reporting limit
NR Not Reported
dry Sample results reported on a dry weight basis
Recov. Recovery
RPD Relative Percent Difference
Great Lakas Analytical
A/dy Johnson, Project Manager Page I I of 1
mM LAKESANALYTICAL FAX (84?) 808-7772 FAX (414) 570-9461
Client: Bill To: 4 DAY 3 DAY 2 DAY 1 DAY < 24 HRS
Address: /Address:D YEST^TAT is critical
n NO . TAT is nn( cnli
DATE RESULTS NEEDED:
U \i-kuufcfiuot IL TFMPERATURF IPON RFCEIPT
Report to: Q .Phone #: State &
Program:Phone #: fFa**: (.
Deliverable Package Needed:D STD D Other
Air Bill No.
Project: 2c& \ - ^
Sampler:
» of BottlesPreservative Used
PO/Quote #:
JTF/ELD /D, LOCATION
SAMPLE/CONTROL
LABORATORY'^NUMBER
Li -02,PID:
ITP/D:
5J
P/D:
P/D:
UP/D:
8J
P/D:
UP/D:
P/D:1-2D'0\
^2^sffn- vx£e-^LINQUISHEDRELINQUISHED RELINQUIS
COMMENTS:
R4GE OF
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
June 18, 2001
Gary MilkerisHygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
RE: 2001-3495
Dear Gary Milkeris
Enclosed are the results of analyses for sample(s) received by the laboratory on June 5, 2001. If you i.gve anyquestions concerning this report, please feel free to contact me.
Sincerely,
Andy JohnsonProject Manager
siau, • i'iuis* ^HurAwl
•§51GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
I Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 6/4/01Received: 6/5/01Reported: 6,18/01 16:18
ANALYTICAL REPORT FOR SAMPLES:
[Sample Description Laboratory Sample Number Sample Matrix Date Sampled
IV
I
I!i;iiiiiiii
lB-14Central-3'
W-14 Central-17'
|B-15
.B-16
IB-17
IB-11
B-12
IB-13
B106065-01
B106065-02
B106065-03
B106065-04
B106065-05
B106065-06
B106065-07
B106065-08
Soil
Water
Soil
Soil
Soil
Soil
Soil
Soil
6/4/01
6/4/01
6/4/01
6/4/01
6/4/01
6/4/01
6/4/01
6/4/01
Great
I
Lakes Analytical
Andy'Johnson, Project Manager
Tltt' result!: in this report apply to ill? samples analyzed in accordance with the chain of custody document.This analytical report must be reproduced in us entirely.
Page 1 ot"34
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 200)-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 6/4/01Received: 6/5/01Reported: 6'18/01 16:18
Total Metals by EPA 6000/7000 Series MethodsGreat Lakes Analytical
Analvte
W-14 Central-lTArsenicBariumCadmiumChromiumSeleniumSilverLeadMercury
Batch Date DateNumber Prepared Analyzed
SpecificMethod
ReportingLimit
B106065-021060181 6/12/01 6/12/01.i n M,in., ., nnn .i i i
1060196 6/13/01 6/13/01
EPA 601 OBE P A 6 0 I O BEPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 7421EPA 7470A
0.05000.500
0.005000.01000.05000.0500
0.005000.000200
Result Units Note
WaterND mg/1NDNDNDNDNDNDND
Grt^it Lakes Analytical *Refer to end of report for text oj notes and dcfmuioi
Andy Johnson. Project Manager Page 2 of
I GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
11JHygieneering, Inc.
75 75 Plaza CourtWillowbrook. IL 60521
Analyte
B-14 Central-3'Arsenic
1BariumCadmiumChromiumSelenium
•
SilverLeadMercury
ArsenicBarium
1CadmiumChromiumSeleniumSilver
•LeadMercury
— B-16• Arsenic^ Barium
Cadmium
1ChromiumSeleniumSilverLead
• Mercury
B-13
1ArsenicBariumCadmiumChromium
1SeleniumSilverLead
— MercuryI '
"Great Lakes Analytical\ \
1 '-K-
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
TCLP Metals by EPA 1311/6000/7000 SeriesGreat Lakes Analytical
Batch Date Date SpecificNumber Prepared Analyzed Method
B 106065-011060182 6/12/01 6/12/01 EPA6010B
EPA 601 OBEPA 601 OBEPA 601 OBEPA6010BEPA 601 OBEPA 7421
1060137 " " EPA7470A
B106065-031060182 6/12/01 6/12/01 EPA6010B" , " " EPA 601 OB
EPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 7421
1060137 " " EPA7470A
Bl 06065-041060182 6/12/01 6/12/01 EPA60IOB
EPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 7421
1060137 " " EPA7470A
Bl 06065-081060182 6,12,01 6,12/01 EPA6010B
EPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 601 OBEPA 7421
1 OWI1 37 " " EPA 7470A
Methods
ReportingLimit
0.1001.00
0.005000.1000.100
0.05000.00500
0.000200
0.1001.00
0.005000.1000.100
0.05000.00500
0.000200
0.1001.00
0.005000.1000.100
0.05000.00500
0.000200
0.1001.00
0.005000.1000 100
0.05000.00500
0.000200
Sampled: 6/4/01Received: 6/5/01Reported: 6/18/01 16:18
Result Units Notes*
SoilND mg/1NDNDNDNDND
0.0104ND
SoilND mg/1NDNDNDNDND
0.0385ND
SoilND mg/1NDNDNDNDND
0.0278ND
SoilND mg/1NDNDNDNDND
0.0200ND
*Re/er to end of report /or le.rl of notes uiul definitions.
Andy Johnson, Project Manager Page 3 of 34
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Analvte
W-14Central-lTAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethenecis-l,2-Dichloroethenetrans-l,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene1 .1 ,1 -Trichloroethane1 . 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 .2-Dichloroetliane-d4
Project: 2001-3495Project Number: N/A
Project Manaeer: Garv Milkeris
Volatile Organic Compounds by EPA Method 8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analvzed Limits Limit
B106065-021060148 6/8/01 6/9/01 10.0
2.002.002.002.0010.02.002.002.002.002.002.002.00
20002.002.00200020002.002.002.002.0010.02.0010.02.002.002.002.002.002.0020002.002.0020002.00
Vl.l-lll85.1-104
Sampled: 6/4/01Received: 6/5/01Reported: 6 18/01 16:18
Result Units Notes"
Water G15.G2.G3.O'ND ug/l
2.59NDNDNDNDNDNDNDND
29.6NDND
2580 " G1242.485.3
242000 " G122580 " G12
NDNDNDNDNDNDNDNDNDNDNDNDND
47100 " GI2NDND
14000 " G12ND
91.2 %111) " O5
Grca| Lakes Analytical
^ \,'< \ \
"Refer lo end of report lor text of notes and definition:
Andy (Johnson. Project Manager Page 4 of '•
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
I Hygieneering, Inc.75 75 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 6/4/01Received: 6/5/01Reported: 6/18/01 16:18
Volatile Organic Compounds by EPA Method 8260BGreat Lakes Analytical
JAnalvteBatch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units Notes*
iw-14Central-17' (continued)Surrogate: Toluene-d8
• Surrogate: 4-Bromofluorobenzene1060148 6/8/01
B106065-026/9/01 95.1-105
89.6-105
Water G15,G2,G3.O9100 %102
I
I
I
I
I
I
I
I
I
IGreat Lpkes Analytical
IAndy Jo+mson, Project Manager
*Rc/cr to end of report for text of notes and definition!,
Page 5 of" 34
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Analyte
B-17AcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno ( 1 ,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
B-llAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno ( 1 ,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Polynuclear Aromatic Compounds by EPA Method 8310Great Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B106065-051060134 6/8/01 6/12/01 100
200100100
90.0100100100100
90.0100100100100100100
29.0-132
Bl 06065-061060134 6/8/01 6,11/01 100
200100100
90.0100100100100
90.0100100100100100100
29.0-132
Sampled: 6/4/01Received: 6/5/01Reported: 6/18/01 16:18
Result Units Notes:
SoilND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
44.8 %
SoilND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
84.9 %
Great bakes Analytical *Refer to end of report for text of notes and definition.
Andy Johnson, Project Manager Page 6 of '.
I ^^B GREATI All LAKES
. •&•• ANALYTICAL•11
1 Hygieneering, Inc.J 75 75 Plaza Court• Willowbrook, IL 60521
•
Analyte
B-,2Acenaphthene
1AcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyrene
1Benzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluoranthene
— Chrysene1 Dibenz (a,h) anthracene• Fluoranthene
Fluorene
1Indeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyrene
• Surrogate: Carbazole
1
1
1
1
1
1— Grefct Lakes Analytical
i W/-
1380 Busch Parkway Email: [email protected] Grove, I l l ino is 60089 (847) 808-7766 FAX (847) 808-7772
Project: 2001-3495 Sampled: 6/4/01Project Number: N/A Received: 6/5/01
Project Manager: Garv Milkeris Reported: 618/01 16:
Polynuclear Aromatic Compounds by EPA Method 8310Great Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units
Bl 06065-07 Soil1060134 6/8/01 6/11/01 100 ND ug/kg
200 ND100 ND100 ND
90.0 ND100 ND100 ND100 ND100 ND
90.0 ND100 353100 ND100 ND100 ND100 420100 221
29.0-132 AT? %
•18
Notes
05
'Refer to end of report for text of notes and definition
AndyVIohnson, Project Manager Page 7 of:
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Analyte
B-14 Central-3'AcetoneBenzeneBromodichloromethaneBromotbrmBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 ,1 -Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethenecis-1, 2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-l,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 . 1 ,2.2-TetrachloroethaneTetrachloroetheneToluene1,1.1 -Trichloroethane1 . 1 .2-TrichloroethaneTrichloroetheneTrichlorotluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 .2-Dichloroethane-d4
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B 106065-011060197 6/12/01 6/13/01 25000
5000500050005000
100005000500050005000500050005000500050005000500050005000500050005000
100005000
1000050005000500050005000500050005000
1000050005000
81.2-1345(1.8-145
Sampled: 6/4/0 iReceived: 6/5/01Reported: 6/18/01 16:18
Result Units Notes*
Soil G4ND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
34600 " G 1 2NDNDNDNDNDNDNDNDNDNDNDNDNDND
74800 " I . G 1 2NDNDNDND
96.6 "/:,
12-
Gruat Lakes Analytical *Refer to end of report for lext of notes uiul definitions
An<Jy Johnson. Project Manager Page X of 3
I
I£\
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: info@glalabs com(847) 808-7766 FAX (847) 808-7772
1 Hygieneering, Inc.7575 Plaza Court
BJWillowbrook, IL 60521
•
11 Analyte
[JB-14Central-3' (continued)Surrogate: Toluene-d8
_ Surrogate: 4-Bromofluorobenzene
1
1
1
1
1
1
1
1
1
IHi Great Lakes Analytical
Andy Johnson. Project Manager
1
Project: 2001-3495 Sampled: 6,4-01Project Number: N/A Received: 6,5/01
Project Manager: Gary Milkeris Reported: 618/01 lb :18
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units Notes*
B 106065-01 Soil G41060197 6/12/01 6/13/01 82.0-121 100 %
76.8-113 108
"Refer 10 end of report for text of notes and definitions.
Page 9 of 34
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
-
Analvte
MSAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1,1 -Dichloroethane1 ,2-Dichloroethane1,1-Dichloroethenecis-1, 2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- 1,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 . 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene1,1,1 -Trichloroethane1 ,1 ,2 -TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 . 2-Dichloroethane-d4
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B106065-031060197 6/12/01 6/13/01 25000
5000500050005000
100005000500050005000500050005000500050005000500050005000500050005000
100005000
1000050005000500050005000500050005000
1000050005000
8 1.2- 13450.8-145
Sampled: 6/4/01Received: 6/5/01Reported: 6,18/01 16:18
Result Units Notes"
Soil G4ND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
43900 " G\2NDNDNDNDNDNDNDNDNDNDNDNDNDND
24800 " 1.GI2NDNDNDND
93. 7 %127
Great Lpkes Analytical "Refer to end of report for text of notes and de/iniltons
Andy Johnson. Project Manager Page 10 of 3
III
ISal
GREAT1380 Busch Parkway Email: [email protected]
ANALYTICAL Buffalo Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772
IHygieneering, Inc. Project: 2001-3495 Sampled: 6/4/017575 Plaza Court Project Number: N/A Received: 6/5/01Willowbrook. IL 60521 Project Manager: Gary Milkeris Reported: 6/18/01 16:18
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingI Analyte Number Prepared Analyzed Limits Limit Result Units Notes*
I B-15 (continued^ B106065-03 Soil G4Surrogate: Toluene-d8 ~ 1060197 6/12/01 6/13/01 82.0-121 101 %
• Surrogate: 4-Bromofluorobenzene " " " 76.8-113 109
I
I
I
I
I
I
I
I
I
IGreat Lakes Analytical "Refer to end of report for text of notes and definitions.\
\\Andy J\>hnson, Project Manager Page 1 1 of 34
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 6/4/01Received: 6/5/01Reported: 6/18/01 16:18
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Analvte
B-16AcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 , 1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethenecis-1, 2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 ,1 ,2,2-TetrachloroethaneTetrach 1 oroeth en eToluene1,1 ,1 -Trichloroethane1 , 1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 . 2-Dichloroelhane-d4
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
Bl 06065-041060197 6/12/01 6/13/01 12500
25002500250025005000250025002500250025002500250025002500250025002500250025002500250050002500500025002500250025002500250025002500500025002500
81.2-13450.8-145
Result Units Notes*
Soil G4ND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
34300 " G12NDNDNDNDNDNDNDNDNDNDNDNDNDND
3690 " G 1 2NDNDNDND
97.2 %127
GreatJLakes Analytical "Refer 10 end of report for text of notes and definitions
Andj' Johnson, Project Manager Page 12 of 3'
II
„-..••A* ISSl
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
I Hygieneering, Inc.75 75 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 6,4/01Received: 6/5/01Reported: 6/18/01 16:18
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
lAnalvteBatch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units Notes*
I
I
I
I
I
I
I
I
I
I
I
B-16 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
1060197 6/12/01B106065-04
6/13/01 82.0-12176.8-113
99.7108
Soil%
G4
Gre|it Lakes Analytical
II JAndy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Pane 13 of 3-
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Analvte
BdlAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 , 1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethenecis-1, 2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-l,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-M ethy 1-2-pentanoneStyrene1,1.2,2-TetrachloroethaneTetrach loroeth en eToluene1,1 ,1 -Trichloroethane1 . 1 .2-TrichloroethaneTrichloroetheneTri ch 1 orott uoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromelhaneSurrogate: 1.2-Dichloroeiliane-d4
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B106065-081060197 6/12/01 6/13/01 1250000
250000250000250000250000500000250000250000250000250000250000250000250000250000250000250000250000250000250000250000250000250000500000250000500000250000250000250000250000250000250000250000250000500000250000250000
81.2-13450.8-145
Sampled: 6/4/01Received: 6/5/01Reported: 6,18/01 16:18
Result Units Notes*
Soil G4ND ug/kgNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
1020000 " G12NDNDND
4220000 " 2.G12NDNDNDND
93.4 "/„142
Great Ltikes Analytical "Refer to end of report lor texl of notes and definitions
Andy Johnson, Project Manager Page 14 of 3-
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
I Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 6,4/01Received: 6,5/01Reported: 6 18/01 16:18
JAnalyte
Volatile Organic Compounds by EPA Method 5035/8260BGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit Result Units Notes*
I
I
I
I
I
I
I
I
I
I
I
I
B-13 (continued)Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
1060197 6/12/01B106065-08
6/13/01 82.0-12176.8-113
Soil G4
98.5111
Great Lajces Analytical
Antly Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 15 of
I
I GREATurAwBi Aifcc••••UMrvco 1380 Busch Parkway Email: [email protected]•fill ANALYTICAL Buffalo Grove, I l l inois 60089 (847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Analvte
B-17BenzeneTolueneEthylbenzeneTotal XylenesSurrogate: 4-BFB
B-llBenzeneTolueneEthylbenzeneTotal XylenesSurrogate: 4-BFB
B-12BenzeneTolueneEthylbenzeneTotal XylenesSurrogate: 4-BFB
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
BTEX by EPA Method 5035/802 IBGreat Lakes Analytical
Batch Date Date Surrogate ReportingNumber Prepared Analyzed Limits Limit
B 106065-051060153 6/8/01 6/11/01 25.0
250250250
" ~ " " 35.1-140
B 106065-061060153 6/8/01 6/11/01 25.0
250250250
35.1-140
B106065-071060153 6/8/01 6/11/01 25.0
250250250
35.1-140
Sampled:Received:Reported:
Result
29.2NDNDND
23.8
40.6NDNDND
34. 1
NDNDNDND
21.8
6,4,016/5/016,18/01 16:18
Units Notes*
Soil G4.O3ug/kg11
11
"
% O4
Soil G4.O3ug/kg"
11
"
% O4
Soil G4.O3ug/kg"""
% O4
Andy Johnson, Project Manager
"Refer lo end of report for text of notes and definitions.
Page 16 of 34
1 g*slGREAT
•All LAKto 1380 Buscri Parkway_ •fifll ANALYTICAL Buffalo Grove, Il l inois 60089•1
11 Hygieneering, Inc. Project: 2001-3495
• 7575 Plaza Court Project Number: N/A•Willowbrook, IL 60521 Project Manager: Gary Milkeris
Dry Weight DeterminationI Great Lakes Analytical
BJSampleName Lab ID Matrix1^B-14Central-3- B106065-01 Soil
• B-15 B106065-03 Soil
B-16 B106065-04 Soil
• B-17 B106065-05 Soil
B- l l B 106065-06 Soil
|B-12 B106065-07 Soil
,_B-13 Bl 06065-08 Soil
1
1
1
1
1
1
1
1Great Lakes Analytical
1 /1A^
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Sampled: 6/4,01Received: 6/5/01Reported: 6,18/01 16:18
Result Units
75.5 %
72.9 %
81.0 %
81.2 %
81.1 %
76.3 %
75.3 %
I
Andy Johnson, Project Manager Page 17 of 34
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
iHygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N,A
Project Manager: Gar,- Milkeris
Sampled: 6,4/01Received: 6.5/01Reported: 6 18/01 16:18
Total Metals by EPA 6000/7000 Series Methods/Quality ControlGreat Lakes Analytical
Analvte
Batch: 1060181BlankArsenicBariumCadmiumChromiumSeleniumSilverLead
LCSArsenicBariumCadmiumChromiumSeleniumSilverLead
Matrix SpikeArsenicBariumCadmiumChromiumSeleniumSilverLead
Matrix Spike PupArsenicBariumCadmiumChromiumSeleniumSilverLead
Date Spike SampleAnalyzed Level Result
Date Prepared: 6/12/011060181-BLK16/12/01
""""11
1060181-BS16/12/01 2.00
2.001.002.001 .001.00
0.0240
1060181-MS1 B106070-016/12/01 2.00 ND
2.00 ND1 .00 ND2.00 0.03471.00 ND1.00 ND
0.0240 0.0249
1060181-MSD1 B106070-016/12/01 2.00 ND
2.00 ND1.00 ND2.00 0.03471.00 ND1.00 ND
0.0240 0.0249
QCResult
NDNDNDNDNDNDND
2.082.081.012.061.001.10
0.0309
2.062.15
0.9972.061.03
0.6880.0505
2.022.13
0.9732.021.02
0.4970.0502
Reporting Limit Recov.Units Recov. Limits %
Extraction Method: EPA
mg/1 0.05000.500
0.005000.01000.05000.0500
0.00500
mg/1 78.6-12677.1-11878.2-11679.1-11676.2-12425.7-16964.1-149
mg/1 74.0-12372.0-12673.7-12055.6-13431..5-15710.0-14142.0-184
mg/1 74.0-12372.0-12673.7-12055.6-13431.5-15710.0-14142.0-184
3015
104104101103100110129
103108
99.7101103
68.8107
101107
97.399.3102
49.7105
i
RPD RPDLimit % Notes*
20.5 1.961 7.0 0.93014.2 2.4414. S 1.7036.2 0.97677.9 32.232. S 1.89
Great Likes Analytical
An0y Johnson. Project Manager
"Refer to end of report for text of notes and definition.'*.
Page I K of 3'
I ^^.BGREATfill LAKES
B WSmm ANALYTICAL1380 Busch Parkway
Buffalo Grove, Illinois 60089Email: [email protected]
(847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.J7575 Plaza CourtIwillowbrook, IL60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 6,4/01Received: 6/5/01Reported: 6.18/01 16:18
I Batch: 1060196Blank
i Mercury
'LCSMercury
[Matrix SpikeMercury
I Matrix Spike PupMercury
I
I
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I
I
I
I
I
I
Total Metals by EPA 6000/7000 Series Methods/Quality ControlGreat Lakes Analytical
Date Spike Sample QC Reporting Limit Recov. RPD RPDlAnalvte Analyzed Level Result Result Units Recov. Limits % Limit % Notes*
Pate Prepared: 6/13/011060196-BLK16/13/01
1060196-BS16/13/01 0.0200
1060196-MS1 Bl 06070-016/13/01 0.0200 ND
1060196-MSP1 Bl 06070-016/13/01 0.0200 ND
NP
Extraction Method: EPA 7470A
mg/1 0.000200
0.0218 mg/I
0.0200 mg/1
0.0196 mg/1
73.4-125 109
42.2-148 100
42.2-148 98.0 27.5 2.02
Great Lqkes Analytical
AndyjJohnson. Project Manager
"Refer in end of report for text of notes and definitions
Page 19 of 34
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 6,4/01Received: 6,5/01Reported: 6.18/01 16:18
TCLP Metals by EPA 1311/6000/7000 Series Methods/Quality ControlGreat Lakes Analytical
Analvte
Batch: 1060137BlankMercury
LCSMercury
Matrix SpikeMercury
Matrix Spike PupMercury
Batch: 1060182BlankArsenicBariumCadmiumChromiumSeleniumSilverLead
LCSArsenicBariumCadmiumChromiumSeleniumSilverLead
Matrix SpikeArsenicBariumCadmiumChromiumSeleniumSilver ,
Date Spike SampleAnalyzed Level Result
Date Prepared:1060137-BLK16/12/01
1060137-BS1
6/12/01
6/12/01 0.00100
1060137-MS1 B 10603 9-026/12/01 0.00100 ND
1060137-MSP1 Bl 06039-026/12/01 0.00100 ND
Pate Prepared:1060182-BLK16/12/01""11
"11
11
1060182-BS16/12/01"""11
n
6/12/01
2.002.001.002.001.001.00
0.0240
1060182-MS16/12/0111
"""
B106062-012.00 ND2.00 ND1.00 ND2.00 ND1.00 ND1.00 ND
QCResult
NP
0.000853
0.000879
0.000875
NRNPNPNPNPNPNP
2.012.02
0.9901.99
0.97S0.986
0.0297
1.952.71
0.9671.911.01
O.S93
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*
Extraction Method: EPA
mg/1 0.000200
mg/1 73.9-123
mg/1 58.0-152
mg/1 58.0-152
Extraction Method: EPA
mg/1 0.1001.00
0.005000.1000.100
0.05000.00500
mg.l 72.8-13981.6-12676.7-13179.3-13069.9-13583.2-13759.9-152
mg/1 82.8-13567.1-15466.3-15367.1-14966.1-15019.6-176
7470A
85.3
87.9
87.5 26.2 0.456
3015
100101
99.099.597.898.6124
97.5136
96.795.5101
89.3
Great Liakt$ Analytical "Refer to end of report for text of notes and definition
AndyUohnson, Project Manager Page 20 of
111
;n-~»\e.w.B
ti&Aml
•III(GREAT(LAKES(ANALYTICAL
1380 Busch Parkway Email: [email protected] Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772
IHygieneering, Inc.75 75 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Pro j ect Manager: Gary Milkeris
Sampled: 6,4/01Received: 6/5/01Reported: 6,18/01 16:18
TCLP Metals by EPA 1311/6000/7000 Series Methods/Quality ControlGreat Lakes Analytical
[AnalyteDate Spike Sample QC Reporting Limit Recov. RPD RPDAnalyzed Level Result Result Units Recov. Limits % Limit u/o Notes
I
I
I
I
I
I
I
I
I
I
I
I
I
[Matrix Spike (continued)Lead
Matrix Spike PupArsenicBariumCadmiumChromiumSeleniumSilverLead
1060182-MS1 Bl 06062-016/12/01 0.0240 ND 0.0303
6/12/01 2.002.001.002.001.001 .00
0.0240
NDNDNDNDNDNDND
1.972.72
0.9661.911.01
0.9990.0310
mg/1
mg/1
35.2-176 126
82.8-13567.1-15466.3-15367.1-14966.1-15019.6-17635.2-176
98.5136
96.695.5101
99.9129
19.316.023.813.821.835.835.3
1.020
0.10300
11.22.35
Great Lakds Analytical
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definitions.
Page 21 of 3'
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project:Project Number:
Project Manager:
2001-3495N/AGary Milkeris
Sampled:Received:Reported:
6/4/016/5/016/18/01 16:18
Volatile Organic Compounds by EPA Method 82606/Quality ControlGreat Lakes Analytical
Date Spike Sample QCAnalyte Analyzed Level Result Result
Batch: 1060148 Pate Prepared: 6/8/01Blank 1060148-BLK1Acetone 6/8/01Benzene "Bromodichloromethane "Bromoform "Bromomethane "2-Butanone "Carbon disulfide "Carbon tetrachloride "Chlorobenzene "Chlorodibromomethane "Chloroethane "Chloroform "Chloromethane "1 , 1 -Dichloroethane "1 ,2-Dichloroethane "1,1-Dichloroethene "cis-1, 2-Dichloroethene "trans-1, 2-Dichloroethene "1 ,2-Dichloropropane "cis-l,3-Dichloropropene "trans- 1 ,3-Dichloropropene "Ethylbenzene "2-HexanoneMethylene chloride "4-Methyl-2-pentanone "Styrene "1 . 1 ,2,2-Tetrachloroethane "Tetrachloroethene "Toluene1,1,1 -Trichloroethane "1 , 1 ,2-Trichloroethane "Trichloroethene "Trichlorotluoromethane "Vinyl acetate "Vinyl chloride "Total Xylenes "Surrogate: Dibromofluoromethane " 50 .1)
— i
NPNPNPNPNPNPNPNDNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNDNPNP
46.1
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit "/o Notes*
Extraction Method: EPA 5030B (P/T)
ug/l 10.02.002.002.002.0010.02.002.002.002.002.002.002.002.002.002.002.002.002.002.002.002.0010.02.0010.02.002.002.002.002.002.002.002.002.002.002.00
91.1-111 92.2
Great t\akes Analytical
\iArrdy Johnson, Project Manager
"Refer lo end of report for text of notes and definitions
Page 22 of 3^
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
IwHygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Project:Project Number:
Project Manager:
2001-3495N/AGary Milkeris
Sampled:Received:Reported:
6/6/6,
4/015/0118/01 16 18
Volatile Organic Compounds by EPA Method 8260B/Quality ControlGreat Lakes Analytical
•1Analvte
H Blank (continued)Surrogate: 1 .2-Dichloroethane-d4
_ Surrogate: Toluene-d8• Surrogate: 4-Bromofluorobenzene
LCS
1AcetoneBenzeneBromodichloromethaneBromoform
H Bromomethane• 2-Butanone
Carbon disulfide
1Carbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethane
1ChloroformChloromethane1 , 1 -Dichloroethane
11 ,2-Dichloroethane1,1-Dichloroethenecis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene
11 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene
12-HexanoneMethylene chloride4-Methyl-2-pentanone
IStyrene1 , 1 .2,2-TetrachloroethaneTetrachloroetheneToluene
11, 1.1 -Trichloroethane1 , 1 ,2-TrichloroethaneTrichloroethene
_ Trichlorofluoromethane
Date Spike SampleAnalyzed Level Result
1060148-BLK1"~6/87oi" 50.0
50.050.0
1060148-BS16/8/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0
- 50.0
QCResult
39 J50.749.6
38.849.755.058.663.446.354.755.657.258.954.549.850.644.251.250.653.147.850.654.857.658.142.446.445.961.057.461.455.953.254.550.263.1
Reporting LimitUnits Recov. Limits
ug/l 85.1-10495.1-10589.6-105
ug/l 10.0-19484.9-11574.3-13070.1-12010.0-25810.0-14743.4-14660.5-13885.4-11578.8-11610.0-45574.5-13478.7-12876.8-12066.7-12972.7-12587.0-12377.9-11988.3-11581.2-12075.2-12684.3-11921.4-14262.5-14038.2-14186.6-11713.2-19776.6-120X6.3-12063.5-14684.5-12451.4-15310.0-586
Recov. RPD RPD% Limit % Notes'
78.2101
99.2
77.699.4110117127
92.61091 1 1114118109
99.6101
88.4102101106
95.61011 10115116
84.892.891.81221151231 1 210610910012(3
Great Lakes Analytical
1Andy Johnson, Project Manager
I
"Refer to end of report for text of notes and definitions
Page 23 of 34
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Volatile Organic Compounds by EPA Method
Analvte
LCS (continued)Vinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1 .2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
Matrix SpikeAcetoneBenzeneBromodichloromethaneBromofbrmBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethaneChloroformChloromethane1 .1 -Dichloroethane1 ,2-Dichloroethane1 , 1 -Dichloroethenecis- 1 ,2-Dichloroethenetrans-1, 2-Dichloroethene1 ,2-Dichloropropanecis- 1 .3-Dichloropropenetrans- 1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene
Great Lakes
Date Spike SampleAnalyzed Level Result
1060148-BS16/8/01 50.0
50.0150
-- - „ 500
50.050.050.0
1060148-MS1 B106046-016/9/01 50.0 ND
50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 12.450.0 ND50.0 ND50.0 29550.0 6.4150.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND50.0 ND
Analytical
QCResult
12154.1179
48.849.650.650.1
50.045.252.457.546.962.241.039.751.356.240.946.231.551.049.834.3280
43.449.448.251.549.450.045.353.155.759. S46.249.5
Sampled: 6,4/01Received: 6/5/01Reported: 6/18/01 16:18
8260B/Quality Control
Reporting LimitUnits Recov. Limits
ug/l 10.0-21971.0-12088.3-11891.1-11185.1-10495.1-10589.6-105
ug/l 10.0-26971.4-11565.3-13454.6-13210.0-17610.0-20123.4-14326.3-13377.4-10872.8-11710.0-29370.8-12461.3-10963.3-11454.5-13736.1-11564.8-12954.7-11377.8-11467.3-11757.3-12468.3-11110.0-22545.6-1501 0.0-20849.7-12620.6-22345 .1-11371.3-118
Recov. RPD RPD% Limit % Note;
NR108119
97.699.2101100
10090.4105115
93.8124
82.079.4103112
81.892.463.077.299.668.6NR
74.098.896.4103
98.8100
90.6106111120
92.499.0
Griit Lakes Anaivtical "Refer to end of report for text of notes and definition.'
\
Anj\ly Johnson, Project Manager Page 24 of 3
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
11
1 Hygieneering, Inc.J7575 Plaza Court• Willowbrook, IL 60521
Project:Project Number:
Project Manager:
2001-3495N/AGary Milkeris
Sampled: 6/4/01Received: 65/01Reported: 6,18/01 16:18
• Volatile Organic Compounds by EPA Method 8260B/Quality Controlm Great Lakes Analytical
T~[Analvte
1^ Matrix Spike (continued)
1 ,1 ,1 -Trichloroethane
11 ,1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetate
1Vinyl chlorideTotal XylenesSurrogate: Dibromofluoromethane
^ Surrogate: 1.2-Dichloroethane-d4H Surrogate: Toluene-d8• Surrogate: 4-Bromofluorobenzene
1Matrix Spike PupAcetoneBenzeneBromodichloromethane
IBromofbrmBromomethane2-Butanone
1Carbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethane
1ChloroethaneChloroformChloromethane
_ 1,1 -Dichloroethane• 1 ,2-DichloroethaneU 1 , 1 -Dichloroethene
cis-1, 2-Dichloroethene
1trans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1 ,3-Dichloropropenetrans- 1 ,3-Dichloropropene
I Ethylbenzene2-HexanoneMethylene chloride
|
4-Methyl-2-pentanone1 '
Date SpikeAnalyzed Level
SampleResult
QC Reporting Limit Recov.Result Units Recov. Limits %
RPDLimit
RPD% Notes
1060148-MS1 B 106046-016/9/01 50.0
50.050.050.050.050.0150
" "~"~ " 50.050.050.050.0
NDND
3.36NDND
35.2ND
41.4 ug/l57.550.842.180.646.1154
'50.549.951.751.4
42.5-12870.1-13953.5-10610.0-41710.0-23937.4-11370.8-11191.1-11185.1-10495.1-10589.6-105
82.8115
94.984.2161
21.8103101
99.8103103
1060148-MSP1 B 106046-016/9/01 50.0
50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0
NDNDNDNDNDNDNDNDNDNDNDNDND12.4NDND295
6.41NDNDNDNDNDNDND
45.0 ug/l44.251.655.951.644.841.539.851.255.444.745.635.647.748.934.4274
44.247.247.149.949.044.344.746.1
10.0-26971.4-11565.3-13454.6-13210.0-17610.0-20123.4-14326.3-13377.4-10872.8-11710.0-29370.8-12461.3-10963.3-11454.5-13736.1-11564.8-12954.7-11377.8-11467.3-11757.3-12468.3-1 1 110.0-22545.6-15010.0-208
90.088.4103112103
89.683.079.6102111
89.491.271.270.697.868.8NR
75.694.494.299.898.088.689.492.2
73.819.115.636.245.761.623.626.212.223.936.910.620.112.727.223.019.617.416.415.726.313.558.311.469.7
10.52.241.922.649.3532.21.21
0.2520.9760.897
8.881.3112.28.931.82
0.291
2.144.552.313.16
0.81312.11.3313.9
' Great. Lakes Analytical
I
I
Andy Johnson, Project Manager Page 25 of 3-
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 6/4/01Received: 6/5/01Reported: 6/18/01 16:18
Volatile Organic Compounds by EPA Method 8260B/Quality ControlGreat Lakes Analytical
AnalvteDateAnalyzed
SpikeLevel
SampleResult
QCResult Units
ReportingRecov.
LimitLimits
Recov. RPDLimit
RPDu/o Notes
Matrix Spike Pup (continued)Styrene1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1,1,1 -Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1.2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
1060148-MSD1 B106046-016/9/01 50.0
50.050.050.050.050.050.050.050.050.0150
50.050.050.050.0
NDNDNDNDNDND
3.36NDND
35.2ND
55.756.646.648.341.954.845.543.7.'3.753.3153
49.750.050.650.8
ug/l 49.7-12620.6-22345.1-11371.3-11842.5-12870.1-139
53.5-10610.0-41710.0-239
37.4-11370.8-11191.1-1/1
85.1-10495.1-10589.6-105
11111393.296.683.811084387.414736.2102
99.4.100101102
18.650.317.619.418.432.520.929.234.523.512.4
06.010.862
2.451.204.4411.83.739.0949.70.976
Great\Lakes Analytical• \
\"Refer to end of report for text of notes and definitions
Andy Johnson, Project Manager Page 26 of 3
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email. info@glalabs com(847)808-7766 FAX (847) 808-7772
1I"iHygieneering, Inc.J?575 Plaza Court
•Willowbrook, IL 60521I
nalvte
atch: 1060134Blank
—Acenaphthene•Acenaphthylene•Anthracene
Benz (a) anthracene•Benzo (a) pyrene•Benzo (b) fluoranthene
Benzo (ghi) peryleneBenzo (k) fluoranthene
•Chrysene•Dibenz (a,h) anthracene
Fluoranthene••Fluorene•Indeno ( 1 ,2,3-cd) pyrene^Naphthalene
Phenanthrene•PyreneJfSurrogate: Carbazole
^LCS•Acenaphthene"Acenaphthylene
Anthracene
Eenz( a) anthraceneenzo (a) pyrene
" Benzo (b) fluoranthene^Benzo (ghi) peryleneVBenzo (k) fluoranthene•Chrysene
Dibenz (a,h) anthracene
f luorantheneluoreneideno ( 1 ,2,3-cd) pyrene
NaphthaleneIBPhenanthreneJP'yrene
Surrogate: Carbazole
1
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Polynuclear Aromatic Compounds byGreat Lakes
Date Spike SampleAnalvzed Level Result
Pate Prepared: 6/8/011060134-BLK16/11/01
""11
nn
it"M
»
76.7
1060134-BS16/11/01 64.9
64.964.964.964.964.964.964.964.964.964.964.964.964.964.964.916.2
EPA MethodAnalytical
QCResult
Sampled: 6/4/01Received: 6/5/01Reported: 6/18/01 16:18
8310/Quality Control
Reporting LimitUnits Recov. Limits
Recov. RPD RPD% Limit % Note>
Extraction Method: EPA 3550B
NPNPNPNPNRNPNPNPNPNPNPNPNPNPNPNP
15.4
49.680.747.352.143.259.948.855.255.248.454.149.148.643.453.164.212.6
ug/kg 100200100100
90.0100100100100
90.0100100100100100100
29.0-132
ug/kg 30.8-12038.9-15832.9-12240.5-12531.2-12845.0-13238.7-13753.4-12546.5-12942.8-13437.1-11640.8-10851.0-11522.7-11629.5-12344.5-11829.11-132
92.2
76.4124
72.980.366.692.375.285.185.174.683.475.774.966.981.898977.8
jreal Lakes Analytical
IAndyVlohnson, Project Manager
I
"Refer to end of report for text of notes and definitions.
Page 27 of 3'
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook. IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 6/4/01Received: 6,5/01Reported: 6,18,01 16:18
Polynuclear Aromatic Compounds by EPA Method 8310/Quality ControlGreat Lakes Analytical
Analvte
Matrix SpikeAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno (1,2,3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
Matrix Spike PupAcenaphtheneAcenaphthyleneAnthraceneBenz (a) anthraceneBenzo (a) pyreneBenzo (b) fluorantheneBenzo (ghi) peryleneBenzo (k) fluorantheneChryseneDibenz (a,h) anthraceneFluorantheneFluoreneIndeno ( 1 ,2.3-cd) pyreneNaphthalenePhenanthrenePyreneSurrogate: Carbazole
\
Date SpikeAnalyzed Level
SampleResult
QC Reporting LimitResult Units Recov. Limits
^ecov.%
RPDLimit
RPD% Notes
1060134-MS1 B106061-076/12/01 67.0
67.067.067.067.067.067.067.067.067.067.067.067.067.067.067.016.8
1060134-MSP16/12/01 68.5
68.568.568.568.568.568.568.568.568.568.568.56S.568.568.568.517.1
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
B106061-07NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
48.9 ug/kg66.751.637.238.043.929.033.253.021.265.337.130.837.349.275.610. 7
44.9 ug/kg68.958.036.038.044.431.336.566.827.052.539.332.235.536.263. S12.7
10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145
29.0-132
10.0-15410.0-17610.0-11410.0-11810.0-13310.0-12610.0-10310.0-11210.0-12113.9-10110.0-12310.0-14410.0-10310.0-13210.0-13010.0-145
29.0-132
73.099.677.055.556.765.543.349.679.131.697.555.446.055.773.4113
63. 7
65.5101
84.752.655.564.845.753.397.539.476.657.447.051.852.893.174.3
66.465.767.157.854.551.965.959.365.249.858.753.955.862.557.456.6
10.81.409.525.372.141.075.397.1920.822.024.03.552.157.2632.619.3
Great \Lakes Analytical
Andy Johnson, Project Manager
"Refer to end of report for text of notes and definition
Page 28 of
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
II Hygieneering, Inc.
_7575 Plaza Court• Willowbrook. IL 6052 1
•
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled. 6/4/01Received: 6/5/01Reported: 6/18/01 16:18
VolatUe Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical
| Date Spike SamplejAnalyte Analyzed Level Result
M Batch: 1060197 Pate Prepared: 6/12/01Blank 1060197-BLK1
1Acetone 6/14/01Benzene "Bromodichloromethane "Bromoform "
1Bromomethane "2-Butanone "Carbon disulfide "Carbon tetrachloride "
• Chlorobenzene "•Chlorodibromomethane "
Chloroethane "
1ChloroformChloromethane "1,1 -Dichloroethane1 ,2-Dichloroethane "
• l,l-Dichloroethene "B'-is-l, 2-Dichloroethene "
trans-1, 2-Dichloroethene "
K1. ,2-Dichloropropane "ois-l,3-Dichloropropene "irans- 1 ,3-Dichloropropene "Ethylbenzene "
|
.'-Hexanone "Methylene chloride "4-Methyl-2-pentanone "
^Styrene "• 1 ,1 ,2,2-Tetrachloroethane•-Tetrachloroethene
Toluene "
I', 1,1 -Trichloroethane "1,1 ,2-Trichloroethane "frichloroethene "Trichlorotluoromethane "
KVinyl acetate "Vinyl chloride "Total Xylenes "
•
^urrogate: Dibromofluoromelhane " 50.0
^ortsot Lakes Analytical
QCResult
NPNPNDNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNPNDNPNPNPNPNPNPNPNPNPNPNRNP
46. 8
Reporting Limit Recov. RPD RPDUnits Recov. Limits % Limit % Notes*
Extraction Method: EPA 5035B fP/Tl
ug/kg 1250250250250250500250250250250250250250250250250250250250250250250500250500250250250250250250250250500250250
81.2-134 93.6
"Refer lo end of report for text of notes and def inn ions.
\Andy Jbimson, Project Manager
I
Page 29 of 34
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 6/4/01Received: 6/5/01Reported: 6/18/01 16:18
Volatile Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical
Analyte
Blank (continued)Surrogate: 1 . 2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
LCSAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChioroethaneChloroformChloromethane1 , 1 -Dichloroethane1,2-Dichloroethane1 , 1 -Dichloroethenecis-1, 2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropanecis-1,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1 , 1 ,2,2-TetrachloroethaneTetrachloroetheneToluene1 , 1 , 1 -Trichloroethane1 ,1 ,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane
1
Date Spike SampleAnalyzed Level Result
1060197-BLK16/14/01 50.0
50.050.0
1060197-BS16/14/01 2500
25002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500
QC Reporting Limit Recov. RPD RPDResult Units
69.9 ug/kg46.348.0
3320 ug/kg18202580262025602200139030402330268031602140
9371560269018301 9601710168020702360241012201 550852
23901380292022402630208024501130
Recov. Limits
50.8-14582.0-12176.8-113
10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-13668.4-13757.6-14264.1-13460.0-13476.4-125h i . 8-13214.6-241
% Limit % Notes
14092.696.0
13372.8103105102
88.055.6122
93.2107126
85.637.562.4108
73.278.468.467.282.894.496.448.862.034.195.655.21 1 7
89.6105
83.298.045.2
Gnjat Lakes Analytical "Refer to end of report for text of notes and de/initioi,
Andy Johnson, Project Manager Page 30 of
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
11
1 Hygieneering, Inc.J 75 75 Plaza CourtI Willowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 6-4,01Received: 6 .501Reported: 61801 16:18
1Volatile Organic Compounds by EPA Method 5035/8260B/Quality Control
1Great Lakes Analytical
Analvte
LCS (continued)Vinyl acetate
1Vinyl chlorideTotal Xylenes
-. - . .
Surrogate: DibromofluoromethaneSurrogate: / , 2-Dichloroethane-d4
1Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
LCS PUDB AcetoneB Benzene
Bromodichloromethane
IBromoformBromomethane2-ButanoneCarbon disulfide
B Carbon tetrachlorideBCh lorobenzene
Chlorodibromomethane
1ChloroethaneChloroformChloromethane1 .1 -Dichloroethane
11,2-Dichloroethane1 .1 -Dichloroethenecis- 1 ,2-Dichloroethene
-trans-1, 2-DichloroetheneB 1 .2-Dichloropropane• cis-1 ,3-Dichloropropene
trans-1 ,3-Dichloropropene
IEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanone
J stvrene•1 , 1 ,2,2-TetrachloroethaneTetrachloroethene
1Toluene
1Great Lakes Analytical
1 :l,~
Date Spike SampleAnalyzed Level Result
1060197-BS16/14/01 2500
25007500
" 50.050.050.050.0
1060197-BSP16/14/01 2500
2500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500
QCResult
10101640725050.071.748.649.6
338019002860274027402200146033302390281030002260
7961600305017801940178018102210255024701750159099S
2480141029502390
Reporting LimitUnits Reeov. Limits
ug/kg 10.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113
ug/kg 10.0-16662.1-13864.3-12547.5-12449.2-19810.0-21410.0-17551.1-13463.5-13567.5-12110.0-53769.2-12467.4-16263.0-12757.5-12559.9-12964.4-13759.0-13666.3-13267.9-12463.6-12460.0-14110.0-17528.4-14910.0-18864.6-1366S.4-13757.6-14264.1-134
"Refer 10 end of report
Recov.%
40.465.696.7100143
97.299.2
13576.0114110110
88.058.4133
95.6112120
90.431.864.0
12271.277.671.272.488.4102
98.870.063 639.999.256.4I I S
95.6
for text
RPDLimit
34541.442.057.461.9173126
43.539.041.690.343.571.841.868.647.539.343.038.141.557.242.7128
67.41 1 9
37.254646.342.6
of notes
RPD% Notes*
1.494.3010.14.657.55
04.918.632.544.574.885.4516.52.5312.22.771.034.017.456.547.742.4635.72.5515.73.702.15
O.X516.4S
and definitions.
Andy Johnson, Project Manager Page 31 of 34
I
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 6/4,01Received: 6/5/01Reported: 6/18/01 16:18
Volatile Organic Compounds by EPA Method 5035/8260B/Quality ControlGreat Lakes Analytical
AnalvteDateAnalyzed
SpikeLevel
SampleResult
QCResult Units
ReportingRecov.
LimitLimits
Recov. RPDLimit
RPDNote;
LCS Pup (continued)1,1,1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl acetateVinyl chlorideTotal XylenesSurrogate: DibromofluoromethaneSurrogate: 1.2-Dichloroethane-d4Surrogate: Toluene-d8Surrogate: 4-Bromofluorobenzene
1060197-BSP16/14/01 2500
25002500250025002500750050.050.050.050.0
272022402700109010901370737051.376.750.451.7
ug/kg 60.0-13476.4-12561.8-13214.6-24110.0-16157.9-14360.0-14181.2-13450.8-14582.0-12176.8-113
10989.610843.643.6' 54.898.3103153101103
44.253.243.511592.181.040.1
3.747.419.713.607.6217.91.64
Grcat/Lakes Analytical Refer to end of report for text of notes and definition'
Andy Johnson. Project Manager Page 32 of:
1 i**|GREATBMBH*-""^^ 1380 Busch Parkway Email: [email protected]^BjBJ ANALYTICAL Buffalo Grove, Illinois 60089 (847)808-7766 FAX (847) 808-7772
1
1iHygieneering, Inc.
• 75 75 Plaza Court• Willowbrook, IL 60521
1J Analyte
1 '•Batch: 1060153
Blank
1BenzeneTolueneEthylbenzeneTotal Xylenes
• Surrogate: 4-BFB
I CSLt*~ <J
1BenzeneTolueneEthylbenzeneTotal Xylenes
•Surrogate: 4-BFB
LCS Pup
1BenzeneTolueneEthylbenzeneTotal Xylenes
•Surrogate: 4-BFB
1
1
1
1
GreatlLakes Analytical
i XAndv Johnson. Project Manaeer
1
Project: 2001-3495 Sampled: 64,01Project Number: N/A Received: 65/01
Project Manager: Gary Milkeris Reported: 6 1 8 0 1 16:18
BTEX by EPA Method 5035/802 IB/Quality ControlGreat Lakes Analytical
Date Spike Sample QC Reporting Limit Recov. RPD RPDAnalyzed Level Result Result Units Recov. Limits % Limit % Notes
Pate Prepared: 6/8/01 Extraction Method: EPA 5035B [P/T11060153-BLK16/11/01 NP ug/kg 25.0
NP " 250NP " 250NP " 250
1000 829 " 35.1-140 82.9
1060153-BS16/11/01 1000 610 ug/kg 77.6-105 61.0
1000 842 " 65.0-131 84.21000 960 " 82.7-115 96.03000 2780 " 86.7-115 92.71000 1000 " 35.1-140 100
1060153-BSP16/11/01 1000 665 ug/kg 77.6-105 66.5 15.4 8.63
1000 858 " 65.0-131 85.8 18.9 1.881000 950 " 82.7-115 95.0 19.8 1.053000 2740 " 86.7-115 91.3 19.8 1.521000 933 " 35.1-140 93.3
"Refer to end of report (or text of notes find definitions.
Page 33 of 34
GREATLAKESANALYTICAL
1380 Busch ParkwayBuffalo Grove, Illinois 60089
Email: [email protected](847) 808-7766 FAX (847) 808-7772
Hygieneering, Inc.7575 Plaza CourtWillowbrook, IL 60521
Project: 2001-3495Project Number: N/A
Project Manager: Gary Milkeris
Sampled: 6/4/01Received: 6,5/01Reported: 6/18/01 16:18
Notes and Definitions
Note
Gl 2 The reporting limit of this sample/analyte is elevated due to sample matrix and/or other effects.
Gl 5 The relative percent difference (RPD) of one or more analytes in the matrix QC (MS/MSD) associated with this sample is above thelaboratory's established acceptance limits. Refer to the included QC reports for more detail.
G2 The recovery of one or more analytes in the matrix QC (MS/MSD) associated with this sample is below the laboratory's establishedacceptance criteria. Refer to the included QC reports for more detail.
G3 The recovery of one or more analytes in the laboratory control QC (BS/BSD) associated with this sample is above the laboratory'sestablished acceptance criteria. Refer to the included QC reports for more detail.
G4 The recovery of one or more analytes in the laboratory control QC (BS/BSD) associated with this sample is below the laboratory'.'established acceptance criteria. Refer to the included QC reports for more detail.
03 One or more internal standard recoveries were above the method specified acceptance criteria.
04 The recovery for this analyte is below the laboratory's established acceptance criteria.
05 The recovery for this analyte is above the laboratory's established acceptance criteria.
O9 The pH of this volatile sample was checked prior to analysis and was found to be above the method specified pH of 2.
1 The method blank associated with this sample contains 7800 ug/L of this analyte
2 The method blank associated with this sample contains 200,500 ug/ L of this analyte.
DET Analyte DETECTED
ND Analyte NOT DETECTED at or above the reporting limit
NR Not Reported
dry Sample results reported on a dry weight basis
Recov. Recovery
RPD Relative Percent Difference
Great Lakes Analytical\vAndyJonnson, Project Manager Page 34 of 3-
ANALYTICAL\\J-TI ) U'U^j i i OU
FAX (847) 808-7772 FAX (414) 570-9461
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D NO - TAT is not critical
DATE RESULTS NEEDED:
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