j56861-2 std tal l2 final report - mdeq · 2017-06-09 · job narrative 680-56861-2 receipt all...

ANALYTICAL REPORT

Job Number: 680-56861-2

Job Description: Hattiesburg Sludge TCLP APR 2010

For:Ashland Inc.

500 Hercules RoadWilmington, DE 19894

Attention: Timothy Hassett

_____________________________________________

Approved for release.Lidya GuliziaProject Manager I5/13/2010 12:05 PM

Lidya GuliziaProject Manager I

[email protected]/13/2010

cc: Craig Derouen

The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This reportmay not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to theperson who signed this report.

Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; AZ: AZ0741; CA: 03217CA;CO; CT: PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KYUST; LA DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; MI: 9925; MS; NFESC: 249; NV:GA00006; NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LAO00244;SC: 98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WVDHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q

TestAmerica Laboratories, Inc.

TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404

Tel (912) 354-7858 Fax (912) 352-0165 www.testamericainc.com

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mailto:[email protected]

http://www.testamericainc.com

Job Narrative

680-56861-2

Receipt

All samples were received in good condition within temperature requirements.

GC/MS VOA

No analytical or quality issues were noted.

GC/MS Semi VOA

Method(s) 8270C: Pyridine recovery is not calculated in sample 680-56861-3 MSD because the result is below the reporting limit for the

analyte.

Method(s) 8270C: The following sample(s) was diluted due to the abundance of target analytes: IBS-1-LS (680-56861-1), IBS-4-LS

(680-56861-5), IBS-7-LS (680-56861-15), IBS-7-US (680-56861-16). Elevated reporting limits (RLs) are provided.

Method(s) 8270C: The following sample(s) contained one acid and/or one base surrogate outside acceptance limits: IBS-1-LS

(680-56861-1). The laboratory's SOP allows one acid surrogate and/or one base surrogate to be outside acceptance limits; therefore,

re-extraction/re-analysis was not performed. These results have been reported and qualified.

No other analytical or quality issues were noted.

GC Semi VOA

Method(s) 8081A_8082: Two surrogates are used for this analysis. The laboratory's SOP allows one of these surrogates to be outside

acceptance criteria without performing re-extraction/re-analysis. The following sample(s) contained an allowable number of surrogate

compounds outside limits: IBS-1-LS (680-56861-1) and the associated MS/MSD samples (680-56861-1 MS and 680-56861-1 MSD).

These results have been reported and qualified.

Method(s) 8151A: This method incorporates the use of second column confirmation. Corrective action for unacceptable percent recovery

is not taken for surrogate or spike compounds unless the results from both columns are outside criteria. Any results which fall outside

criteria are qualified and reported.


Metals

No analytical or quality issues were noted.

General Chemistry

Method(s) 1030: The following sample(s) did not ignite: IBS-1-LS (680-56861-1), IBS-1-US (680-56861-20), IBS-2-LS (680-56861-22),

IBS-2-US (680-56861-23), IBS-3-LS (680-56861-3), IBS-3-US (680-56861-6), IBS-4-LS (680-56861-5), IBS-4-US (680-56861-9),

IBS-5-LS (680-56861-8), IBS-5-US (680-56861-12), IBS-6-LS (680-56861-11), IBS-6-US (680-56861-13), IBS-7-LS (680-56861-15),

IBS-7-US (680-56861-16), IBS-8-LS (680-56861-18), IBS-8-US (680-56861-19); therefore, an ignitability value could not be obtained.

The result has been reported as "No Burn" (NB).

Method(s) 9012A: The matrix spike / matrix spike duplicate (MS/MSD) recoveries associated with batch 166379 were outside control

limits. Matrix interference is suspected.

Method(s) 9034: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for sample 680-56861-22 (680-56861-22 MS),

(680-56861-22 MSD) were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria.


Comments

No additional comments.

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METHOD SUMMARY

Job Number: 680-56861-2Client: Ashland Inc.

Preparation MethodMethodLab LocationDescription

Matrix: Solid

SW846 8260BVolatile Organic Compounds (GC/MS) TAL SAV

SW846 1311TAL SAVTCLP Extraction

SW846 5030BTAL SAVPurge and Trap

SW846 8270CSemivolatile Compounds by Gas Chromatography/Mass

Spectrometry (GC/MS)

TAL SAV


SW846 3520CTAL SAVLiquid-Liquid Extraction (Continuous)

SW846 8081A_8082Organochlorine Pesticides & PCBs (GC) TAL SAV


SW846 3520CTAL SAVLiquid-Liquid Extraction (Continuous)

SW846 8151AHerbicides (GC) TAL SAV


SW846 8151ATAL SAVExtraction (Herbicides)

SW846 6010BMetals (ICP) TAL SAV


SW846 3010ATAL SAVPreparation, Total Metals

SW846 7470AMercury (CVAA) TAL SAV


SW846 7470ATAL SAVPreparation, Mercury

SW846 1030Ignitability, Solids TAL SAV

SW846 9012ACyanide, Total and/or Amenable TAL SAV

SW846 9012ATAL SAVCyanide, Total and/or Amenable, Distillation

SW846 9034Sulfide, Acid Soluble and Insoluble (Titrimetric) TAL SAV

SW846 9030BTAL SAVSulfide, Distillation (Acid Soluble and Insoluble)

SW846 9045CpH TAL SAV

Lab References:

TAL SAV = TestAmerica Savannah

Method References:

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Savannah

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METHOD / ANALYST SUMMARY

Client: Ashland Inc. Job Number: 680-56861-2

Method Analyst Analyst ID

Cowart, Judson WJCSW846 8260B

Lanier, Carolyn CLSW846 8260B

Davis, Nancy NDSW846 8270C

Haynes, Carion CRHSW846 8270C

Kellar, Joshua JKSW846 8081A_8082

Smith, Crystal CASSW846 8151A

Bland, Brian BCBSW846 6010B

Eaton, Cliff CESW846 7470A

Jackson, Michelle S MSJSW846 1030

McDonald, Debbie DAMSW846 9012A

Vasquez, Juana JVSW846 9034

Jackson, Michelle S MSJSW846 9045C


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SAMPLE SUMMARY


Client Sample IDLab Sample ID Client Matrix

Date/Time

Sampled

Date/Time

Received

04/14/2010 0950 04/17/2010 1045IBS-1-LS680-56861-1 Solid

04/14/2010 1255 04/17/2010 1045IBS-3-LS680-56861-3 Solid

04/14/2010 1735 04/17/2010 1045IBS-4-LS680-56861-5 Solid

04/15/2010 0845 04/17/2010 1045IBS-3-US680-56861-6 Solid

04/15/2010 1005 04/17/2010 1045IBS-5-LS680-56861-8 Solid

04/15/2010 1100 04/17/2010 1045IBS-4-US680-56861-9 Solid

04/15/2010 1110 04/17/2010 1045IBS-6-LS680-56861-11 Solid

04/15/2010 1145 04/17/2010 1045IBS-5-US680-56861-12 Solid

04/15/2010 1415 04/17/2010 1045IBS-6-US680-56861-13 Solid

04/15/2010 1520 04/17/2010 1045IBS-7-LS680-56861-15 Solid

04/15/2010 1525 04/17/2010 1045IBS-7-US680-56861-16 Solid

04/15/2010 1615 04/17/2010 1045IBS-8-LS680-56861-18 Solid

04/15/2010 1620 04/17/2010 1045IBS-8-US680-56861-19 Solid

04/15/2010 1700 04/17/2010 1045IBS-1-US680-56861-20 Solid

04/16/2010 0850 04/17/2010 1045IBS-2-LS680-56861-22 Solid

04/16/2010 0930 04/17/2010 1045IBS-2-US680-56861-23 Solid


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SAMPLE RESULTS


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Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-LS

Client Matrix:

680-56861-1

Solid

Date Sampled: 04/14/2010 0950

Date Received: 04/17/2010 1045

8260B Volatile Organic Compounds (GC/MS)-TCLP

Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 2124

04/22/2010 2124

20

8260B Analysis Batch: 680-166481

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID:

a379.d

5 mL

5 mL

Leachate Batch: 680-166366

5030B

MSA

Date Leached: 04/21/2010 1605

Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL

0.21 0.0200.020Benzene

0.020 U 0.0200.020Carbon tetrachloride

0.020 U 0.0200.020Chlorobenzene

0.020 U 0.0200.020Chloroform

0.020 U 0.0200.0201,2-Dichloroethane

0.020 U 0.0200.0201,1-Dichloroethene

0.20 U 0.200.202-Butanone (MEK)

0.020 U 0.0200.020Tetrachloroethene

0.020 U 0.0200.020Trichloroethene

0.020 U 0.0200.020Vinyl chloride

Surrogate %Rec Acceptance LimitsQualifier

97 75 - 1204-Bromofluorobenzene

94 75 - 121Dibromofluoromethane

99 75 - 120Toluene-d8 (Surr)

TestAmerica Savannah of 173

Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-LS

Client Matrix:

680-56861-3

Solid

Date Sampled: 04/14/2010 1255



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 2153

04/22/2010 2153

20




Lab File ID:

Instrument ID:

a381.d

5 mL

5 mL


5030B

MSA

Date Leached: 04/21/2010 1605


0.96 0.0200.020Benzene



0.020 U 0.0200.020Chloroform



0.20 U 0.200.202-Butanone (MEK)









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-LS

Client Matrix:

680-56861-5

Solid

Date Sampled: 04/14/2010 1735



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 2222

04/22/2010 2222

20




Lab File ID:

Instrument ID:

a383.d

5 mL

5 mL


5030B

MSA

Date Leached: 04/21/2010 1605


0.052 0.0200.020Benzene



0.020 U 0.0200.020Chloroform



0.20 U 0.200.202-Butanone (MEK)









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-US

Client Matrix:

680-56861-6

Solid

Date Sampled: 04/15/2010 0845



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 2251

04/22/2010 2251

20




Lab File ID:

Instrument ID:

a385.d

5 mL

5 mL


5030B

MSA

Date Leached: 04/21/2010 1605


0.12 0.0200.020Benzene



0.020 U 0.0200.020Chloroform



0.20 U 0.200.202-Butanone (MEK)









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-LS

Client Matrix:

680-56861-8

Solid

Date Sampled: 04/15/2010 1005



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 2320

04/22/2010 2320

20




Lab File ID:

Instrument ID:

a387.d

5 mL

5 mL


5030B

MSA

Date Leached: 04/21/2010 1605


0.043 0.0200.020Benzene



0.020 U 0.0200.020Chloroform



0.20 U 0.200.202-Butanone (MEK)









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-US

Client Matrix:

680-56861-9

Solid

Date Sampled: 04/15/2010 1100



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 2349

04/22/2010 2349

20




Lab File ID:

Instrument ID:

a389.d

5 mL

5 mL


5030B

MSA

Date Leached: 04/21/2010 1605


0.038 0.0200.020Benzene



0.020 U 0.0200.020Chloroform



0.20 U 0.200.202-Butanone (MEK)









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-LS

Client Matrix:

680-56861-11

Solid

Date Sampled: 04/15/2010 1110



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/23/2010 0018

04/23/2010 0018

20




Lab File ID:

Instrument ID:

a391.d

5 mL

5 mL


5030B

MSA

Date Leached: 04/21/2010 1605


0.14 0.0200.020Benzene



0.020 U 0.0200.020Chloroform



0.20 U 0.200.202-Butanone (MEK)









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-US

Client Matrix:

680-56861-12

Solid

Date Sampled: 04/15/2010 1145



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/23/2010 0047

04/23/2010 0047

20




Lab File ID:

Instrument ID:

a393.d

5 mL

5 mL


5030B

MSA

Date Leached: 04/21/2010 1605


0.025 0.0200.020Benzene



0.020 U 0.0200.020Chloroform



0.20 U 0.200.202-Butanone (MEK)









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-US

Client Matrix:

680-56861-13

Solid

Date Sampled: 04/15/2010 1415



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/23/2010 0116

04/23/2010 0116

20




Lab File ID:

Instrument ID:

a395.d

5 mL

5 mL


5030B

MSA

Date Leached: 04/21/2010 1605


0.020 U 0.0200.020Benzene



0.020 U 0.0200.020Chloroform



0.20 U 0.200.202-Butanone (MEK)









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-LS

Client Matrix:

680-56861-15

Solid

Date Sampled: 04/15/2010 1520



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 2306

04/22/2010 2306

20




Lab File ID:

Instrument ID:

a386.d

5 mL

5 mL


5030B

MSA2

Date Leached: 04/21/2010 1605


1.3 0.0200.020Benzene



0.020 U 0.0200.020Chloroform



0.20 U 0.200.202-Butanone (MEK)









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-US

Client Matrix:

680-56861-16

Solid

Date Sampled: 04/15/2010 1525



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/26/2010 1659

04/26/2010 1659

20




Lab File ID:

Instrument ID:

p0244.d

5 mL

5 mL


5030B

MSP2

Date Leached: 04/22/2010 1610


0.020 U 0.0200.020Benzene



0.020 U 0.0200.020Chloroform



0.20 U 0.200.202-Butanone (MEK)









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-LS

Client Matrix:

680-56861-18

Solid

Date Sampled: 04/15/2010 1615



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/26/2010 1729

04/26/2010 1729

20




Lab File ID:

Instrument ID:

p0246.d

5 mL

5 mL


5030B

MSP2

Date Leached: 04/22/2010 1610


0.10 0.0200.020Benzene



0.020 U 0.0200.020Chloroform



0.20 U 0.200.202-Butanone (MEK)









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-US

Client Matrix:

680-56861-19

Solid

Date Sampled: 04/15/2010 1620



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/26/2010 1759

04/26/2010 1759

20




Lab File ID:

Instrument ID:

p0248.d

5 mL

5 mL


5030B

MSP2

Date Leached: 04/22/2010 1610


0.020 U 0.0200.020Benzene



0.020 U 0.0200.020Chloroform



0.20 U 0.200.202-Butanone (MEK)









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-US

Client Matrix:

680-56861-20

Solid

Date Sampled: 04/15/2010 1700



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/26/2010 1830

04/26/2010 1830

20




Lab File ID:

Instrument ID:

p0250.d

5 mL

5 mL


5030B

MSP2

Date Leached: 04/22/2010 1610


0.55 0.0200.020Benzene



0.020 U 0.0200.020Chloroform



0.20 U 0.200.202-Butanone (MEK)









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-LS

Client Matrix:

680-56861-22

Solid

Date Sampled: 04/16/2010 0850



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/26/2010 1900

04/26/2010 1900

20




Lab File ID:

Instrument ID:

p0252.d

5 mL

5 mL


5030B

MSP2

Date Leached: 04/22/2010 1610


0.13 0.0200.020Benzene



0.020 U 0.0200.020Chloroform



0.20 U 0.200.202-Butanone (MEK)









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-US

Client Matrix:

680-56861-23

Solid

Date Sampled: 04/16/2010 0930



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/26/2010 1931

04/26/2010 1931

20




Lab File ID:

Instrument ID:

p0254.d

5 mL

5 mL


5030B

MSP2

Date Leached: 04/22/2010 1610


0.058 0.0200.020Benzene



0.020 U 0.0200.020Chloroform



0.20 U 0.200.202-Butanone (MEK)









Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-LS

Client Matrix:

680-56861-1

Solid

Date Sampled: 04/14/2010 0950


8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)-TCLP

Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 1439

05/04/2010 1705

5.0

8270C Analysis Batch: 680-167473

Prep Batch: 680-166414

Injection Volume:



Lab File ID:

Instrument ID:

g1030.d

200 mL

1 mL

1 uL


3520C

MSG

Date Leached: 04/19/2010 1917


0.25 U 0.250.251,4-Dichlorobenzene

0.25 U 0.250.252,4-Dinitrotoluene

0.25 U 0.250.25Hexachloroethane

0.25 U 0.250.25Hexachlorobenzene

0.25 U 0.250.25Hexachlorobutadiene

1.4 0.500.50Methyl Phenols,Total

0.25 U 0.250.25Nitrobenzene

1.2 U 1.21.2Pentachlorophenol

1.2 U 1.21.2Pyridine

0.25 U 0.250.252,4,5-Trichlorophenol



108 40 - 1392,4,6-Tribromophenol

85 50 - 1132-Fluorobiphenyl

27 36 - 110X2-Fluorophenol

99 45 - 112Nitrobenzene-d5

69 38 - 116Phenol-d5

69 10 - 121Terphenyl-d14


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-LS

Client Matrix:

680-56861-3

Solid

Date Sampled: 04/14/2010 1255



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 1439

04/28/2010 1735

1.0



Injection Volume:



Lab File ID:

Instrument ID:

g0892.d

200 mL

1 mL

1 uL


3520C

MSG

Date Leached: 04/19/2010 1917










0.25 U 0.250.25Pyridine






53 36 - 1102-Fluorophenol


62 38 - 116Phenol-d5



Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-LS

Client Matrix:

680-56861-5

Solid

Date Sampled: 04/14/2010 1735



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 1439

05/04/2010 1728

5.0



Injection Volume:



Lab File ID:

Instrument ID:

g1031.d

200 mL

1 mL

1 uL


3520C

MSG

Date Leached: 04/19/2010 1917


















55 38 - 116Phenol-d5



Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-US

Client Matrix:

680-56861-6

Solid

Date Sampled: 04/15/2010 0845



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 1439

04/28/2010 1822

1.0



Injection Volume:



Lab File ID:

Instrument ID:

g0894.d

200 mL

1 mL

1 uL


3520C

MSG

Date Leached: 04/19/2010 1917










0.25 U 0.250.25Pyridine








58 38 - 116Phenol-d5



Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-LS

Client Matrix:

680-56861-8

Solid

Date Sampled: 04/15/2010 1005



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 1439

04/28/2010 1900

1.0



Injection Volume:



Lab File ID:

Instrument ID:

n7170.d

200 mL

1 mL

1 uL


3520C

MSN

Date Leached: 04/19/2010 1917










0.25 U 0.250.25Pyridine








57 38 - 116Phenol-d5



Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-US

Client Matrix:

680-56861-9

Solid

Date Sampled: 04/15/2010 1100



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 1439

04/28/2010 1924

1.0



Injection Volume:



Lab File ID:

Instrument ID:

n7171.d

200 mL

1 mL

1 uL


3520C

MSN

Date Leached: 04/19/2010 1917










0.25 U 0.250.25Pyridine








65 38 - 116Phenol-d5



Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-LS

Client Matrix:

680-56861-11

Solid

Date Sampled: 04/15/2010 1110



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 1439

04/28/2010 1504

1.0



Injection Volume:



Lab File ID:

Instrument ID:

n7160.d

200 mL

1 mL

1 uL


3520C

MSN

Date Leached: 04/19/2010 1917










0.25 U 0.250.25Pyridine








48 38 - 116Phenol-d5



Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-US

Client Matrix:

680-56861-12

Solid

Date Sampled: 04/15/2010 1145



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 1439

04/28/2010 1528

1.0



Injection Volume:



Lab File ID:

Instrument ID:

n7161.d

200 mL

1 mL

1 uL


3520C

MSN

Date Leached: 04/19/2010 1917










0.25 U 0.250.25Pyridine








62 38 - 116Phenol-d5



Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-US

Client Matrix:

680-56861-13

Solid

Date Sampled: 04/15/2010 1415



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 1439

04/28/2010 1552

1.0



Injection Volume:



Lab File ID:

Instrument ID:

n7162.d

200 mL

1 mL

1 uL


3520C

MSN

Date Leached: 04/19/2010 1917










0.25 U 0.250.25Pyridine








58 38 - 116Phenol-d5



Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-LS

Client Matrix:

680-56861-15

Solid

Date Sampled: 04/15/2010 1520



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 1439

05/03/2010 1933

5.0



Injection Volume:



Lab File ID:

Instrument ID:

t1713.d

200 mL

1 mL

1 uL


3520C

MST

Date Leached: 04/19/2010 1917


















73 38 - 116Phenol-d5



Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-US

Client Matrix:

680-56861-16

Solid

Date Sampled: 04/15/2010 1525



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 1439

05/03/2010 2021

5.0



Injection Volume:



Lab File ID:

Instrument ID:

t1714.d

200 mL

1 mL

1 uL


3520C

MST

Date Leached: 04/19/2010 1917


















65 38 - 116Phenol-d5



Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-LS

Client Matrix:

680-56861-18

Solid

Date Sampled: 04/15/2010 1615



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 1439

04/28/2010 1702

1.0



Injection Volume:



Lab File ID:

Instrument ID:

n7165.d

200 mL

1 mL

1 uL


3520C

MSN

Date Leached: 04/19/2010 1917










0.25 U 0.250.25Pyridine








71 38 - 116Phenol-d5



Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-US

Client Matrix:

680-56861-19

Solid

Date Sampled: 04/15/2010 1620



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 1439

04/28/2010 1726

1.0



Injection Volume:



Lab File ID:

Instrument ID:

n7166.d

200 mL

1 mL

1 uL


3520C

MSN

Date Leached: 04/19/2010 1917










0.25 U 0.250.25Pyridine








56 38 - 116Phenol-d5



Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-US

Client Matrix:

680-56861-20

Solid

Date Sampled: 04/15/2010 1700



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 1439

04/28/2010 1749

1.0



Injection Volume:



Lab File ID:

Instrument ID:

n7167.d

200 mL

1 mL

1 uL


3520C

MSN

Date Leached: 04/19/2010 1917










0.25 U 0.250.25Pyridine








73 38 - 116Phenol-d5



Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-LS

Client Matrix:

680-56861-22

Solid

Date Sampled: 04/16/2010 0850



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 1439

04/28/2010 1813

1.0



Injection Volume:



Lab File ID:

Instrument ID:

n7168.d

200 mL

1 mL

1 uL


3520C

MSN

Date Leached: 04/19/2010 1917










0.25 U 0.250.25Pyridine








68 38 - 116Phenol-d5



Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-US

Client Matrix:

680-56861-23

Solid

Date Sampled: 04/16/2010 0930



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

04/22/2010 1439

04/28/2010 1837

1.0



Injection Volume:



Lab File ID:

Instrument ID:

n7169.d

200 mL

1 mL

1 uL


3520C

MSN

Date Leached: 04/19/2010 1917










0.25 U 0.250.25Pyridine








63 38 - 116Phenol-d5



Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-LS

Client Matrix:

680-56861-1

Solid

Date Sampled: 04/14/2010 0950


Method:

8081A_8082 Organochlorine Pesticides & PCBs (GC)-TCLP

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1654

04/21/2010 1423

Analysis Batch: 680-166545



Instrument ID:



Injection Volume:

Result Type: PRIMARY

20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917


0.025 U 0.0250.025Chlordane (technical)

0.0050 U 0.00500.0050Endrin

0.0025 U 0.00250.0025gamma-BHC (Lindane)

0.0025 U 0.00250.0025Heptachlor

0.0025 U 0.00250.0025Heptachlor epoxide

0.0025 U 0.00250.0025Methoxychlor

0.25 U 0.250.25Toxaphene


105 14 - 115DCB Decachlorobiphenyl

78 35 - 120Tetrachloro-m-xylene


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-LS

Client Matrix:

680-56861-1

Solid

Date Sampled: 04/14/2010 0950


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1654

04/21/2010 1423




Instrument ID:



Injection Volume:

Result Type: SECONDARY

20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-LS

Client Matrix:

680-56861-3

Solid

Date Sampled: 04/14/2010 1255


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1713

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917



0.0050 U 0.00500.0050Endrin


0.0025 U 0.00250.0025Heptachlor


0.0025 U 0.00250.0025Methoxychlor






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-LS

Client Matrix:

680-56861-3

Solid

Date Sampled: 04/14/2010 1255


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1713

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-LS

Client Matrix:

680-56861-5

Solid

Date Sampled: 04/14/2010 1735


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1732

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917



0.0050 U 0.00500.0050Endrin


0.0025 U 0.00250.0025Heptachlor


0.0025 U 0.00250.0025Methoxychlor



65 14 - 115pDCB Decachlorobiphenyl



Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-LS

Client Matrix:

680-56861-5

Solid

Date Sampled: 04/14/2010 1735


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1732

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-US

Client Matrix:

680-56861-6

Solid

Date Sampled: 04/15/2010 0845


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1752

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917



0.0050 U 0.00500.0050Endrin


0.0025 U 0.00250.0025Heptachlor


0.0025 U 0.00250.0025Methoxychlor






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-US

Client Matrix:

680-56861-6

Solid

Date Sampled: 04/15/2010 0845


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1752

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-LS

Client Matrix:

680-56861-8

Solid

Date Sampled: 04/15/2010 1005


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1811

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917



0.0050 U 0.00500.0050Endrin


0.0025 U 0.00250.0025Heptachlor


0.0025 U 0.00250.0025Methoxychlor






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-LS

Client Matrix:

680-56861-8

Solid

Date Sampled: 04/15/2010 1005


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1811

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-US

Client Matrix:

680-56861-9

Solid

Date Sampled: 04/15/2010 1100


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1830

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917



0.0050 U 0.00500.0050Endrin


0.0025 U 0.00250.0025Heptachlor


0.0025 U 0.00250.0025Methoxychlor






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-US

Client Matrix:

680-56861-9

Solid

Date Sampled: 04/15/2010 1100


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1830

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-LS

Client Matrix:

680-56861-11

Solid

Date Sampled: 04/15/2010 1110


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1850

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917



0.0050 U 0.00500.0050Endrin


0.0025 U 0.00250.0025Heptachlor


0.0025 U 0.00250.0025Methoxychlor






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-LS

Client Matrix:

680-56861-11

Solid

Date Sampled: 04/15/2010 1110


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1850

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-US

Client Matrix:

680-56861-12

Solid

Date Sampled: 04/15/2010 1145


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1909

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917



0.0050 U 0.00500.0050Endrin


0.0025 U 0.00250.0025Heptachlor


0.0025 U 0.00250.0025Methoxychlor






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-US

Client Matrix:

680-56861-12

Solid

Date Sampled: 04/15/2010 1145


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1909

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-US

Client Matrix:

680-56861-13

Solid

Date Sampled: 04/15/2010 1415


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1929

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917



0.0050 U 0.00500.0050Endrin


0.0025 U 0.00250.0025Heptachlor


0.0025 U 0.00250.0025Methoxychlor






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-US

Client Matrix:

680-56861-13

Solid

Date Sampled: 04/15/2010 1415


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1929

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-LS

Client Matrix:

680-56861-15

Solid

Date Sampled: 04/15/2010 1520


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1948

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917



0.0050 U 0.00500.0050Endrin


0.0025 U 0.00250.0025Heptachlor


0.0025 U 0.00250.0025Methoxychlor






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-LS

Client Matrix:

680-56861-15

Solid

Date Sampled: 04/15/2010 1520


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 1948

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-US

Client Matrix:

680-56861-16

Solid

Date Sampled: 04/15/2010 1525


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 2007

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917



0.0050 U 0.00500.0050Endrin


0.0025 U 0.00250.0025Heptachlor


0.0025 U 0.00250.0025Methoxychlor






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-US

Client Matrix:

680-56861-16

Solid

Date Sampled: 04/15/2010 1525


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 2007

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-LS

Client Matrix:

680-56861-18

Solid

Date Sampled: 04/15/2010 1615


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 2027

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917



0.0050 U 0.00500.0050Endrin


0.0025 U 0.00250.0025Heptachlor


0.0025 U 0.00250.0025Methoxychlor



47 14 - 115pDCB Decachlorobiphenyl

66 35 - 120pTetrachloro-m-xylene


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-LS

Client Matrix:

680-56861-18

Solid

Date Sampled: 04/15/2010 1615


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 2027

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-US

Client Matrix:

680-56861-19

Solid

Date Sampled: 04/15/2010 1620


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 2046

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917



0.0050 U 0.00500.0050Endrin


0.0025 U 0.00250.0025Heptachlor


0.0025 U 0.00250.0025Methoxychlor






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-US

Client Matrix:

680-56861-19

Solid

Date Sampled: 04/15/2010 1620


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 2046

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-US

Client Matrix:

680-56861-20

Solid

Date Sampled: 04/15/2010 1700


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 2106

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917



0.0050 U 0.00500.0050Endrin


0.0025 U 0.00250.0025Heptachlor


0.0025 U 0.00250.0025Methoxychlor






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-US

Client Matrix:

680-56861-20

Solid

Date Sampled: 04/15/2010 1700


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 2106

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-LS

Client Matrix:

680-56861-22

Solid

Date Sampled: 04/16/2010 0850


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 2125

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917



0.0050 U 0.00500.0050Endrin


0.0025 U 0.00250.0025Heptachlor


0.0025 U 0.00250.0025Methoxychlor




47 35 - 120pTetrachloro-m-xylene


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-LS

Client Matrix:

680-56861-22

Solid

Date Sampled: 04/16/2010 0850


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 2125

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-US

Client Matrix:

680-56861-23

Solid

Date Sampled: 04/16/2010 0930


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 2144

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917



0.0050 U 0.00500.0050Endrin


0.0025 U 0.00250.0025Heptachlor


0.0025 U 0.00250.0025Methoxychlor






Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-US

Client Matrix:

680-56861-23

Solid

Date Sampled: 04/16/2010 0930


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A_8082

3520C

1.0

04/22/2010 2144

04/21/2010 1423




Instrument ID:



Injection Volume:


20 mL

10 mL

2 uL

SGM

Date Leached: 04/19/2010 1917





Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-LS

Client Matrix:

680-56861-1

Solid

Date Sampled: 04/14/2010 0950


Method:

8151A Herbicides (GC)-TCLP

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1618

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


0.050 U 0.0500.0502,4-D

0.050 U 0.0500.050Silvex (2,4,5-TP)


90 50 - 150pDCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-LS

Client Matrix:

680-56861-1

Solid

Date Sampled: 04/14/2010 0950


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1618

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


161 50 - 150XDCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-LS

Client Matrix:

680-56861-3

Solid

Date Sampled: 04/14/2010 1255


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1636

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


0.050 U 0.0500.0502,4-D

0.050 U 0.0500.050Silvex (2,4,5-TP)


114 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-LS

Client Matrix:

680-56861-3

Solid

Date Sampled: 04/14/2010 1255


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1636

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


84 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-LS

Client Matrix:

680-56861-5

Solid

Date Sampled: 04/14/2010 1735


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1655

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


0.050 U 0.0500.0502,4-D

0.050 U 0.0500.050Silvex (2,4,5-TP)


86 50 - 150pDCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-LS

Client Matrix:

680-56861-5

Solid

Date Sampled: 04/14/2010 1735


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1655

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


135 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-US

Client Matrix:

680-56861-6

Solid

Date Sampled: 04/15/2010 0845


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1714

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


0.050 U 0.0500.0502,4-D

0.050 U 0.0500.050Silvex (2,4,5-TP)


108 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-US

Client Matrix:

680-56861-6

Solid

Date Sampled: 04/15/2010 0845


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1714

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


82 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-LS

Client Matrix:

680-56861-8

Solid

Date Sampled: 04/15/2010 1005


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1733

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


0.050 U 0.0500.0502,4-D

0.050 U 0.0500.050Silvex (2,4,5-TP)


83 50 - 150pDCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-LS

Client Matrix:

680-56861-8

Solid

Date Sampled: 04/15/2010 1005


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1733

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


133 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-US

Client Matrix:

680-56861-9

Solid

Date Sampled: 04/15/2010 1100


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1751

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


0.050 U 0.0500.0502,4-D

0.050 U 0.0500.050Silvex (2,4,5-TP)


112 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-US

Client Matrix:

680-56861-9

Solid

Date Sampled: 04/15/2010 1100


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1751

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


93 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-LS

Client Matrix:

680-56861-11

Solid

Date Sampled: 04/15/2010 1110


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1810

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


0.050 U 0.0500.0502,4-D

0.050 U 0.0500.050Silvex (2,4,5-TP)


91 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-LS

Client Matrix:

680-56861-11

Solid

Date Sampled: 04/15/2010 1110


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1810

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


66 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-US

Client Matrix:

680-56861-12

Solid

Date Sampled: 04/15/2010 1145


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1829

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


0.050 U 0.0500.0502,4-D

0.050 U 0.0500.050Silvex (2,4,5-TP)


99 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-US

Client Matrix:

680-56861-12

Solid

Date Sampled: 04/15/2010 1145


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1829

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


81 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-US

Client Matrix:

680-56861-13

Solid

Date Sampled: 04/15/2010 1415


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1848

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


0.050 U 0.0500.0502,4-D

0.050 U 0.0500.050Silvex (2,4,5-TP)


112 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-US

Client Matrix:

680-56861-13

Solid

Date Sampled: 04/15/2010 1415


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1848

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


86 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-LS

Client Matrix:

680-56861-15

Solid

Date Sampled: 04/15/2010 1520


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1906

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


0.050 U 0.0500.0502,4-D

0.050 U 0.0500.050Silvex (2,4,5-TP)


80 50 - 150pDCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-LS

Client Matrix:

680-56861-15

Solid

Date Sampled: 04/15/2010 1520


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1906

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


126 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-US

Client Matrix:

680-56861-16

Solid

Date Sampled: 04/15/2010 1525


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1925

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


0.050 U 0.0500.0502,4-D

0.050 U 0.0500.050Silvex (2,4,5-TP)


98 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-US

Client Matrix:

680-56861-16

Solid

Date Sampled: 04/15/2010 1525


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1925

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


81 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-LS

Client Matrix:

680-56861-18

Solid

Date Sampled: 04/15/2010 1615


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1944

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


0.050 U 0.0500.0502,4-D

0.050 U 0.0500.050Silvex (2,4,5-TP)


108 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-LS

Client Matrix:

680-56861-18

Solid

Date Sampled: 04/15/2010 1615


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 1944

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


76 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-US

Client Matrix:

680-56861-19

Solid

Date Sampled: 04/15/2010 1620


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 2002

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


0.050 U 0.0500.0502,4-D

0.050 U 0.0500.050Silvex (2,4,5-TP)


105 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-US

Client Matrix:

680-56861-19

Solid

Date Sampled: 04/15/2010 1620


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 2002

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


88 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-US

Client Matrix:

680-56861-20

Solid

Date Sampled: 04/15/2010 1700


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 2021

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


0.050 U 0.0500.0502,4-D

0.050 U 0.0500.050Silvex (2,4,5-TP)


107 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-US

Client Matrix:

680-56861-20

Solid

Date Sampled: 04/15/2010 1700


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 2021

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


87 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-LS

Client Matrix:

680-56861-22

Solid

Date Sampled: 04/16/2010 0850


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 2040

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


0.050 U 0.0500.0502,4-D

0.050 U 0.0500.050Silvex (2,4,5-TP)


103 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-LS

Client Matrix:

680-56861-22

Solid

Date Sampled: 04/16/2010 0850


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 2040

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


77 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-US

Client Matrix:

680-56861-23

Solid

Date Sampled: 04/16/2010 0930


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 2059

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


0.050 U 0.0500.0502,4-D

0.050 U 0.0500.050Silvex (2,4,5-TP)


108 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-US

Client Matrix:

680-56861-23

Solid

Date Sampled: 04/16/2010 0930


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8151A

8151A

1.0

04/22/2010 2059

04/21/2010 0751




Instrument ID:



Injection Volume:


10 mL

10 mL

1 uL

SGS

Date Leached: 04/19/2010 1917


84 50 - 150DCAA


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-LS

Client Matrix:

680-56861-1

Solid

Date Sampled: 04/14/2010 0950


6010B Metals (ICP)-TCLP

Method: 6010B Analysis Batch: 680-168281 Instrument ID:

Preparation: Prep Batch: 680-166274 Lab File ID: 165047166275.chr

Dilution: 1.0 Leachate Batch: 680-166103 Initial Weight/Volume: 5 mL

Date Analyzed: 04/21/2010 2254 Final Weight/Volume: 50 mL

Date Prepared: 04/21/2010 1045

3010A

ICPD

Date Leached: 04/19/2010 1917


0.20 U 0.200.20Arsenic

1.0 U 1.01.0Barium

0.10 U 0.100.10Cadmium

0.20 U 0.200.20Chromium

0.20 U 0.200.20Lead

0.50 U 0.500.50Selenium

0.10 U 0.100.10Silver

7470A Mercury (CVAA)-TCLP

Method: 7470A Analysis Batch: 680-168285 Instrument ID:

Preparation: Prep Batch: 680-166296 Lab File ID: 1650474221091748.c

Dilution: 1.0 Leachate Batch: 680-166103 Initial Weight/Volume: 0.50 mL



7470A

LEEMAN1

Date Leached: 04/19/2010 1917


0.020 U 0.0200.020Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-LS

Client Matrix:

680-56861-3

Solid

Date Sampled: 04/14/2010 1255








3010A

ICPD

Date Leached: 04/19/2010 1917


0.20 U 0.200.20Arsenic

1.0 U 1.01.0Barium

0.10 U 0.100.10Cadmium

0.20 U 0.200.20Chromium

0.20 U 0.200.20Lead

0.50 U 0.500.50Selenium

0.10 U 0.100.10Silver







7470A

LEEMAN1

Date Leached: 04/19/2010 1917


0.020 U 0.0200.020Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-LS

Client Matrix:

680-56861-5

Solid

Date Sampled: 04/14/2010 1735








3010A

ICPD

Date Leached: 04/19/2010 1917


0.20 U 0.200.20Arsenic

1.0 U 1.01.0Barium

0.10 U 0.100.10Cadmium

0.20 U 0.200.20Chromium

0.20 U 0.200.20Lead

0.50 U 0.500.50Selenium

0.10 U 0.100.10Silver







7470A

LEEMAN1

Date Leached: 04/19/2010 1917


0.020 U 0.0200.020Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-3-US

Client Matrix:

680-56861-6

Solid

Date Sampled: 04/15/2010 0845








3010A

ICPD

Date Leached: 04/19/2010 1917


0.20 U 0.200.20Arsenic

1.0 U 1.01.0Barium

0.10 U 0.100.10Cadmium

0.20 U 0.200.20Chromium

0.20 U 0.200.20Lead

0.50 U 0.500.50Selenium

0.10 U 0.100.10Silver







7470A

LEEMAN1

Date Leached: 04/19/2010 1917


0.020 U 0.0200.020Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-LS

Client Matrix:

680-56861-8

Solid

Date Sampled: 04/15/2010 1005








3010A

ICPD

Date Leached: 04/19/2010 1917


0.20 U 0.200.20Arsenic

1.0 U 1.01.0Barium

0.10 U 0.100.10Cadmium

0.20 U 0.200.20Chromium

0.20 U 0.200.20Lead

0.50 U 0.500.50Selenium

0.10 U 0.100.10Silver







7470A

LEEMAN1

Date Leached: 04/19/2010 1917


0.020 U 0.0200.020Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-4-US

Client Matrix:

680-56861-9

Solid

Date Sampled: 04/15/2010 1100








3010A

ICPD

Date Leached: 04/19/2010 1917


0.20 U 0.200.20Arsenic

1.0 U 1.01.0Barium

0.10 U 0.100.10Cadmium

0.20 U 0.200.20Chromium

0.20 U 0.200.20Lead

0.50 U 0.500.50Selenium

0.10 U 0.100.10Silver







7470A

LEEMAN1

Date Leached: 04/19/2010 1917


0.020 U 0.0200.020Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-LS

Client Matrix:

680-56861-11

Solid

Date Sampled: 04/15/2010 1110








3010A

ICPD

Date Leached: 04/19/2010 1917


0.20 U 0.200.20Arsenic

1.0 U 1.01.0Barium

0.10 U 0.100.10Cadmium

0.20 U 0.200.20Chromium

0.20 U 0.200.20Lead

0.50 U 0.500.50Selenium

0.10 U 0.100.10Silver







7470A

LEEMAN1

Date Leached: 04/19/2010 1917


0.020 U 0.0200.020Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-5-US

Client Matrix:

680-56861-12

Solid

Date Sampled: 04/15/2010 1145








3010A

ICPD

Date Leached: 04/19/2010 1917


0.20 U 0.200.20Arsenic

1.0 U 1.01.0Barium

0.10 U 0.100.10Cadmium

0.20 U 0.200.20Chromium

0.20 U 0.200.20Lead

0.50 U 0.500.50Selenium

0.10 U 0.100.10Silver







7470A

LEEMAN1

Date Leached: 04/19/2010 1917


0.020 U 0.0200.020Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-6-US

Client Matrix:

680-56861-13

Solid

Date Sampled: 04/15/2010 1415








3010A

ICPD

Date Leached: 04/19/2010 1917


0.20 U 0.200.20Arsenic

1.0 U 1.01.0Barium

0.10 U 0.100.10Cadmium

0.20 U 0.200.20Chromium

0.20 U 0.200.20Lead

0.50 U 0.500.50Selenium

0.10 U 0.100.10Silver







7470A

LEEMAN1

Date Leached: 04/19/2010 1917


0.020 U 0.0200.020Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-LS

Client Matrix:

680-56861-15

Solid

Date Sampled: 04/15/2010 1520








3010A

ICPD

Date Leached: 04/19/2010 1917


0.20 U 0.200.20Arsenic

1.0 U 1.01.0Barium

0.10 U 0.100.10Cadmium

0.20 U 0.200.20Chromium

0.20 U 0.200.20Lead

0.50 U 0.500.50Selenium

0.10 U 0.100.10Silver







7470A

LEEMAN1

Date Leached: 04/19/2010 1917


0.020 U 0.0200.020Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-7-US

Client Matrix:

680-56861-16

Solid

Date Sampled: 04/15/2010 1525








3010A

ICPD

Date Leached: 04/19/2010 1917


0.20 U 0.200.20Arsenic

1.0 U 1.01.0Barium

0.10 U 0.100.10Cadmium

0.20 U 0.200.20Chromium

0.20 U 0.200.20Lead

0.50 U 0.500.50Selenium

0.10 U 0.100.10Silver







7470A

LEEMAN1

Date Leached: 04/19/2010 1917


0.020 U 0.0200.020Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-LS

Client Matrix:

680-56861-18

Solid

Date Sampled: 04/15/2010 1615








3010A

ICPD

Date Leached: 04/19/2010 1917


0.20 U 0.200.20Arsenic

1.0 U 1.01.0Barium

0.10 U 0.100.10Cadmium

0.20 U 0.200.20Chromium

0.20 U 0.200.20Lead

0.50 U 0.500.50Selenium

0.10 U 0.100.10Silver







7470A

LEEMAN1

Date Leached: 04/19/2010 1917


0.020 U 0.0200.020Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-8-US

Client Matrix:

680-56861-19

Solid

Date Sampled: 04/15/2010 1620








3010A

ICPD

Date Leached: 04/19/2010 1917


0.20 U 0.200.20Arsenic

1.0 U 1.01.0Barium

0.10 U 0.100.10Cadmium

0.20 U 0.200.20Chromium

0.20 U 0.200.20Lead

0.50 U 0.500.50Selenium

0.10 U 0.100.10Silver







7470A

LEEMAN1

Date Leached: 04/19/2010 1917


0.020 U 0.0200.020Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-1-US

Client Matrix:

680-56861-20

Solid

Date Sampled: 04/15/2010 1700








3010A

ICPD

Date Leached: 04/19/2010 1917


0.20 U 0.200.20Arsenic

1.0 U 1.01.0Barium

0.10 U 0.100.10Cadmium

0.20 U 0.200.20Chromium

0.20 U 0.200.20Lead

0.50 U 0.500.50Selenium

0.10 U 0.100.10Silver







7470A

LEEMAN1

Date Leached: 04/19/2010 1917


0.020 U 0.0200.020Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-LS

Client Matrix:

680-56861-22

Solid

Date Sampled: 04/16/2010 0850








3010A

ICPD

Date Leached: 04/19/2010 1917


0.20 U 0.200.20Arsenic

1.0 U 1.01.0Barium

0.10 U 0.100.10Cadmium

0.20 U 0.200.20Chromium

0.20 U 0.200.20Lead

0.50 U 0.500.50Selenium

0.10 U 0.100.10Silver







7470A

LEEMAN1

Date Leached: 04/19/2010 1917


0.020 U 0.0200.020Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

IBS-2-US

Client Matrix:

680-56861-23

Solid

Date Sampled: 04/16/2010 0930








3010A

ICPD

Date Leached: 04/19/2010 1917


0.20 U 0.200.20Arsenic

1.0 U 1.01.0Barium

0.10 U 0.100.10Cadmium

0.20 U 0.200.20Chromium

0.20 U 0.200.20Lead

0.50 U 0.500.50Selenium

0.10 U 0.100.10Silver







7470A

LEEMAN1

Date Leached: 04/19/2010 1917


0.020 U 0.0200.020Mercury


Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

IBS-1-LS

Client Matrix: % Moisture: 53.4

680-56861-1

Solid

Date Sampled: 04/14/2010 0950


Analyte Result Qual Units MDL RL Dil Method

Cyanide, Total 1.7 J mg/Kg 0.42 10 1.0 9012A

Analysis Batch: 680-166379 DryWt Corrected: YDate Analyzed: 04/22/2010 0919

Date Prepared: 04/21/2010 0600Prep Batch: 680-166233

Analyte Result Qual Units Dil Method

Ignitability NB mm/sec 1.0 1030

Analysis Batch: 680-166149 DryWt Corrected: NDate Analyzed: 04/20/2010 0830

pH 3.27 SU 1.0 9045C


Analyte Result Qual Units RL RL Dil Method

Sulfide 340 mg/Kg 130 130 1.0 9034




Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

IBS-3-LS


680-56861-3

Solid

Date Sampled: 04/14/2010 1255









pH 3.58 SU 1.0 9045C



Sulfide 480 mg/Kg 130 130 1.0 9034




Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

IBS-4-LS


680-56861-5

Solid

Date Sampled: 04/14/2010 1735









pH 5.00 SU 1.0 9045C



Sulfide 790 mg/Kg 150 150 1.0 9034




Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

IBS-3-US


680-56861-6

Solid

Date Sampled: 04/15/2010 0845



Cyanide, Total 20 U mg/Kg 0.85 20 1.0 9012A






pH 6.40 SU 1.0 9045C



Sulfide 610 mg/Kg 250 250 1.0 9034




Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

IBS-5-LS


680-56861-8

Solid

Date Sampled: 04/15/2010 1005









pH 3.88 SU 1.0 9045C



Sulfide 710 mg/Kg 190 190 1.0 9034




Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

IBS-4-US


680-56861-9

Solid

Date Sampled: 04/15/2010 1100









pH 6.36 SU 1.0 9045C



Sulfide 1900 mg/Kg 270 270 1.0 9034




Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

IBS-6-LS


680-56861-11

Solid

Date Sampled: 04/15/2010 1110









pH 3.67 SU 1.0 9045C



Sulfide 1500 mg/Kg 150 150 1.0 9034




Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

IBS-5-US


680-56861-12

Solid

Date Sampled: 04/15/2010 1145









pH 6.22 SU 1.0 9045C



Sulfide 4500 mg/Kg 340 340 1.0 9034




Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

IBS-6-US


680-56861-13

Solid

Date Sampled: 04/15/2010 1415









pH 6.57 SU 1.0 9045C



Sulfide 3600 mg/Kg 340 340 1.0 9034




Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

IBS-7-LS


680-56861-15

Solid

Date Sampled: 04/15/2010 1520









pH 6.15 SU 1.0 9045C



Sulfide 1300 mg/Kg 200 200 1.0 9034




Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

IBS-7-US


680-56861-16

Solid

Date Sampled: 04/15/2010 1525









pH 6.55 SU 1.0 9045C



Sulfide 1900 mg/Kg 230 230 1.0 9034




Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

IBS-8-LS


680-56861-18

Solid

Date Sampled: 04/15/2010 1615









pH 3.54 SU 1.0 9045C



Sulfide 1800 mg/Kg 240 240 1.0 9034




Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

IBS-8-US


680-56861-19

Solid

Date Sampled: 04/15/2010 1620









pH 6.49 SU 1.0 9045C



Sulfide 3700 mg/Kg 430 430 1.0 9034




Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

IBS-1-US


680-56861-20

Solid

Date Sampled: 04/15/2010 1700









pH 6.64 SU 1.0 9045C



Sulfide 3100 mg/Kg 160 160 1.0 9034




Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

IBS-2-LS


680-56861-22

Solid

Date Sampled: 04/16/2010 0850









pH 3.26 SU 1.0 9045C



Sulfide 350 mg/Kg 180 180 1.0 9034




Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

IBS-2-US


680-56861-23

Solid

Date Sampled: 04/16/2010 0930









pH 6.25 SU 1.0 9045C



Sulfide 3400 mg/Kg 280 280 1.0 9034




DATA REPORTING QUALIFIERS


Lab Section Qualifier Description

GC/MS VOA

Indicates the analyte was analyzed for but not detected.U

GC/MS Semi VOA


MS or MSD exceeds the control limitsF

Surrogate is outside control limitsX

GC Semi VOA



RPD of the MS and MSD exceeds the control limitsF

Surrogate is outside control limitsX

The %RPD between the primary and confirmation

column/detector is >40%. The lower value has been reported.

p

Metals


General Chemistry



Result is less than the RL but greater than or equal to the MDL

and the concentration is an approximate value.

J

RPD of the MS and MSD exceeds the control limitsF


of 173

QUALITY CONTROL RESULTS


of 173

Quality Control Results


Surrogate Recovery Report

8260B Volatile Organic Compounds (GC/MS)

Client Matrix: Solid TCLP

Lab Sample ID Client Sample ID

BFB DBFM TOL

%Rec %Rec %Rec

680-56861-1 IBS-1-LS 97 94 99

680-56861-3 IBS-3-LS 102 91 100

680-56861-5 IBS-4-LS 100 96 100

680-56861-6 IBS-3-US 99 96 101

680-56861-8 IBS-5-LS 100 95 100

680-56861-9 IBS-4-US 99 94 100

680-56861-11 IBS-6-LS 98 97 101

680-56861-12 IBS-5-US 98 97 99

680-56861-13 IBS-6-US 99 95 101

680-56861-15 IBS-7-LS 91 97 95

680-56861-16 IBS-7-US 103 91 99

680-56861-18 IBS-8-LS 101 89 97

680-56861-19 IBS-8-US 103 87 102

680-56861-20 IBS-1-US 103 87 101

680-56861-22 IBS-2-LS 99 89 101

680-56861-23 IBS-2-US 101 91 103

MB 680-166481/9 97 99 99

MB 680-166483/9 94 100 94

MB 680-166741/7 95 94 104

LB 680-166366/12-A 97 96 97

LB 680-166494/12-A 96 83 107

LCS 680-166481/6 97 96 92

LCS 680-166483/6 93 97 89

LCS 680-166741/4 103 95 104

LCSD 680-166481/7 95 98 92

LCSD 680-166483/7 93 96 90

LCSD 680-166741/5 106 96 104

680-56861-15 DU IBS-7-LS DU 90 97 95

Surrogate Acceptance Limits

BFB = 4-Bromofluorobenzene 75-120

DBFM = Dibromofluoromethane 75-121

TOL = Toluene-d8 (Surr) 75-120


of 173




8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)



TBP FBP 2FP NBZ PHL TPH

%Rec %Rec %Rec %Rec %Rec %Rec

680-56861-1 IBS-1-LS 108 85 27X 99 69 69

680-56861-3 IBS-3-LS 97 61 53 61 62 38

680-56861-5 IBS-4-LS 93 66 58 73 55 57

680-56861-6 IBS-3-US 91 56 49 57 58 56

680-56861-8 IBS-5-LS 107 55 49 56 57 45

680-56861-9 IBS-4-US 111 65 56 64 65 40

680-56861-11 IBS-6-LS 92 50 43 54 48 43

680-56861-12 IBS-5-US 105 63 59 69 62 42

680-56861-13 IBS-6-US 99 59 54 67 58 38

680-56861-15 IBS-7-LS 101 91 72 91 73 51

680-56861-16 IBS-7-US 94 81 60 81 65 43

680-56861-18 IBS-8-LS 117 69 61 71 71 38

680-56861-19 IBS-8-US 103 59 51 61 56 30

680-56861-20 IBS-1-US 112 63 61 68 73 41

680-56861-22 IBS-2-LS 119 64 38 75 68 50

680-56861-23 IBS-2-US 114 63 53 63 63 42

MB 680-166414/17-A 118 77 74 85 80 90

LB 680-166103/21-G 115 86 74 86 74 97

LB 680-166109/5-G 114 74 70 80 78 86

LCS 680-166414/18-A 98 79 48 83 78 76

680-56861-3 MS IBS-3-LS MS 91 71 63 69 70 41

680-56861-3 MSD IBS-3-LS MSD 81 64 52 62 56 35


TBP = 2,4,6-Tribromophenol 40-139

FBP = 2-Fluorobiphenyl 50-113

2FP = 2-Fluorophenol 36-110

NBZ = Nitrobenzene-d5 45-112

PHL = Phenol-d5 38-116

TPH = Terphenyl-d14 10-121


of 173




8081A_8082 Organochlorine Pesticides & PCBs (GC)



DCB1 DCB2 TCX1 TCX2

%Rec %Rec %Rec %Rec

680-56861-1 IBS-1-LS 81 105 69 78

680-56861-3 IBS-3-LS 62 93 86 103

680-56861-5 IBS-4-LS 65p 101 72 101

680-56861-6 IBS-3-US 81 99 80 89

680-56861-8 IBS-5-LS 67 93 75 91

680-56861-9 IBS-4-US 71 91 70 85

680-56861-11 IBS-6-LS 62 83 71 92

680-56861-12 IBS-5-US 65 81 72 83

680-56861-13 IBS-6-US 68 96 67 79

680-56861-15 IBS-7-LS 78 98 65 83

680-56861-16 IBS-7-US 68 97 65 77

680-56861-18 IBS-8-LS 47p 81 66p 102

680-56861-19 IBS-8-US 63 77 71 74

680-56861-20 IBS-1-US 79 106 86 90

680-56861-22 IBS-2-LS 54 75 47p 75

680-56861-23 IBS-2-US 80 95 75 84

MB 680-166252/21-A 74 87 74 85

LB 680-166103/21-D 88 109 66 78

LB 680-166109/5-D 88 103 78 78

LCS 680-166252/22-A 60 67 77 84

680-56861-1 MS IBS-1-LS MS 85 118X 73 94

680-56861-1 MSD IBS-1-LS MSD 85p 127X 66 89


DCB = DCB Decachlorobiphenyl 14-115

TCX = Tetrachloro-m-xylene 35-120


of 173




8151A Herbicides (GC)



DCPA1 DCPA2

%Rec %Rec

680-56861-1 IBS-1-LS 161X 90p

680-56861-3 IBS-3-LS 114 84

680-56861-5 IBS-4-LS 135 86p

680-56861-6 IBS-3-US 108 82

680-56861-8 IBS-5-LS 133 83p

680-56861-9 IBS-4-US 112 93

680-56861-11 IBS-6-LS 91 66

680-56861-12 IBS-5-US 99 81

680-56861-13 IBS-6-US 112 86

680-56861-15 IBS-7-LS 126 80p

680-56861-16 IBS-7-US 98 81

680-56861-18 IBS-8-LS 108 76

680-56861-19 IBS-8-US 105 88

680-56861-20 IBS-1-US 107 87

680-56861-22 IBS-2-LS 103 77

680-56861-23 IBS-2-US 108 84

MB 680-166235/18-A 160X 73p

LB 680-166109/5-B 97 96

LCS 680-166235/19-A 101 92

680-56861-23 MS IBS-2-US MS 100 88

680-56861-23 MSD IBS-2-US MSD 97 87


DCPA = DCAA 50-150


of 173



WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/22/2010 1652

Method Blank - Batch: 680-166481

Date Prepared:

Instrument ID:

Lab File ID:




Prep Batch: N/A

04/22/2010 1652

aq181.d

5 mL

5 mL

Units: mg/L

Method: 8260B

Preparation: 5030B

MSAMB 680-166481/9

Analyte Result Qual MDL RL

0.0010 U 0.00100.0010Benzene



0.0010 U 0.00100.0010Chloroform



0.010 U 0.0100.0102-Butanone (MEK)




Surrogate % Rec Acceptance Limits

4-Bromofluorobenzene 97 75 - 120

Dibromofluoromethane 99 75 - 121

Toluene-d8 (Surr) 99 75 - 120




SolidClient Matrix:

20Dilution:

Date Analyzed:

Lab Sample ID:

04/22/2010 1927

TCLP SPLPE Leachate Blank - Batch: 680-166481

Date Prepared:

Instrument ID:

Lab File ID:



Date Leached:


Prep Batch: N/A

04/22/2010 1927

04/21/2010 1605

a371.d

5 mL

5 mL

Units: mg/L

Method: 8260B

Preparation: 5030B

TCLP

MSALB 680-166366/12-A



0.020 U 0.0200.020Benzene



0.020 U 0.0200.020Chloroform



0.20 U 0.200.202-Butanone (MEK)











Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/22/2010 1455

04/22/2010 1525

Lab Control Sample/

Lab Control Sample Duplicate Recovery Report - Batch: 680-166481

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:



Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:



mg/L

04/22/2010 1455

Prep Batch: N/A


aq173.d

5 mL

5 mL

aq175.d

5 mL

5 mL

mg/L

04/22/2010 1525


Prep Batch: N/A

Method: 8260B

Preparation: 5030B

MSA

MSA

LCS 680-166481/6

LCSD 680-166481/7

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

9596 77 - 119 1 30Benzene

8383 71 - 135 0 30Carbon tetrachloride

9899 85 - 116 1 30Chlorobenzene

9997 82 - 120 1 30Chloroform

8990 66 - 132 1 301,2-Dichloroethane

104104 62 - 141 0 301,1-Dichloroethene

9998 33 - 157 1 302-Butanone (MEK)

103102 76 - 126 1 30Tetrachloroethene

9593 84 - 115 2 30Trichloroethene

8567 59 - 144 25 50Vinyl chloride

Surrogate LCS % Rec LCSD % Rec Acceptance Limits

4-Bromofluorobenzene 97 95 75 - 120

Dibromofluoromethane 96 98 75 - 121

Toluene-d8 (Surr) 92 92 75 - 120




WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/22/2010 1707


Date Prepared:

Instrument ID:

Lab File ID:




Prep Batch: N/A

04/22/2010 1707

aq182.d

5 mL

5 mL

Units: mg/L

Method: 8260B

Preparation: 5030B

MSA2MB 680-166483/9


0.0010 U 0.00100.0010Benzene



0.0010 U 0.00100.0010Chloroform



0.010 U 0.0100.0102-Butanone (MEK)











Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/22/2010 1510

04/22/2010 1539

Lab Control Sample/


1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:




Date Prepared:

Units:

Instrument ID:

Lab File ID:



mg/L

04/22/2010 1510

Prep Batch: N/A


aq174.d

5 mL

5 mL

aq176.d

5 mL

5 mL

mg/L

04/22/2010 1539


Prep Batch: N/A

Method: 8260B

Preparation: 5030B

MSA2

MSA2

LCS 680-166483/6

LCSD 680-166483/7


% Rec.

9998 77 - 119 0 30Benzene


9797 85 - 116 1 30Chlorobenzene

9598 82 - 120 3 30Chloroform

9090 66 - 132 1 301,2-Dichloroethane

8991 62 - 141 2 301,1-Dichloroethene

9898 33 - 157 1 302-Butanone (MEK)



7983 59 - 144 5 50Vinyl chloride




Toluene-d8 (Surr) 89 90 75 - 120




mg/LUnits:

Solid

Dilution: 20

Date Analyzed:

Duplicate - Batch: 680-166483

Lab Sample ID:

Client Matrix:

Date Prepared:

Date Leached:

04/22/2010 2335

04/22/2010 2335

04/21/2010 1605

Instrument ID:

Lab File ID:




Prep Batch: N/A a388.d

5 mL

5 mL

Method: 8260B

Preparation: 5030B

TCLP

MSA2680-56861-15


Analyte QualLimitRPDResultSample Result/Qual

1.531.3 14.0Benzene

0.0200.020 U NC UCarbon tetrachloride

0.0200.020 U NC UChlorobenzene

0.0200.020 U NC UChloroform

0.0200.020 U NC U1,2-Dichloroethane

0.0200.020 U NC U1,1-Dichloroethene

0.200.20 U NC U2-Butanone (MEK)

0.0200.020 U NC UTetrachloroethene

0.0200.020 U NC UTrichloroethene

0.0200.020 U NC UVinyl chloride








WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/26/2010 1226


Date Prepared:

Instrument ID:

Lab File ID:




Prep Batch: N/A

04/26/2010 1226

pq162.d

5 mL

5 mL

Units: mg/L

Method: 8260B

Preparation: 5030B

MSP2MB 680-166741/7


0.0010 U 0.00100.0010Benzene



0.0010 U 0.00100.0010Chloroform



0.010 U 0.0100.0102-Butanone (MEK)











SolidClient Matrix:

20Dilution:

Date Analyzed:

Lab Sample ID:

04/26/2010 1356


Date Prepared:

Instrument ID:

Lab File ID:



Date Leached:


Prep Batch: N/A

04/26/2010 1356

04/22/2010 1610

p0232.d

5 mL

5 mL

Units: mg/L

Method: 8260B

Preparation: 5030B

TCLP

MSP2LB 680-166494/12-A



0.020 U 0.0200.020Benzene



0.020 U 0.0200.020Chloroform



0.20 U 0.200.202-Butanone (MEK)











Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/26/2010 1024

04/26/2010 1055

Lab Control Sample/


1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:




Date Prepared:

Units:

Instrument ID:

Lab File ID:



mg/L

04/26/2010 1024

Prep Batch: N/A


pq154.d

5 mL

5 mL

pq156.d

5 mL

5 mL

mg/L

04/26/2010 1055


Prep Batch: N/A

Method: 8260B

Preparation: 5030B

MSP2

MSP2

LCS 680-166741/4

LCSD 680-166741/5


% Rec.

9597 77 - 119 2 30Benzene


104102 85 - 116 2 30Chlorobenzene

9891 82 - 120 7 30Chloroform

107114 66 - 132 7 301,2-Dichloroethane

8074 62 - 141 7 301,1-Dichloroethene

9493 33 - 157 1 302-Butanone (MEK)



7771 59 - 144 7 50Vinyl chloride




Toluene-d8 (Surr) 104 104 75 - 120




WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/28/2010 1535


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:



04/22/2010 1439

g0887.d

1000 mL

1 mL

1 uL

Units: mg/L

Method: 8270C

Preparation: 3520C

MSGMB 680-166414/17-A







0.020 U 0.0200.020Methyl Phenols,Total



0.050 U 0.0500.050Pyridine




2,4,6-Tribromophenol 118 40 - 139

2-Fluorobiphenyl 77 50 - 113

2-Fluorophenol 74 36 - 110

Nitrobenzene-d5 85 45 - 112

Phenol-d5 80 38 - 116

Terphenyl-d14 90 10 - 121




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/28/2010 1559


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

Date Leached:



04/22/2010 1439

04/19/2010 1917

g0888.d

200 mL

1 mL

1 uL

Units: mg/L

Method: 8270C

Preparation: 3520C

TCLP

MSGLB 680-166103/21-G











0.25 U 0.250.25Pyridine








Phenol-d5 74 38 - 116





SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/28/2010 1623


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

Date Leached:



04/22/2010 1439

04/19/2010 1917

g0889.d

200 mL

1 mL

1 uL

Units: mg/L

Method: 8270C

Preparation: 3520C

TCLP

MSGLB 680-166109/5-G











0.25 U 0.250.25Pyridine








Phenol-d5 78 38 - 116





Water

1.0

04/28/2010 1647Date Analyzed:

Lab Control Sample - Batch: 680-166414

Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

g0890.d

04/22/2010 1439



1000 mL

1 mL

1 uL

Units: mg/L

Method: 8270C

Preparation: 3520C

MSGLCS 680-166414/18-A

Analyte QualLimit% Rec.ResultSpike Amount

0.100 0.0742 74 38 - 1101,4-Dichlorobenzene

0.100 0.0929 93 49 - 1282,4-Dinitrotoluene

0.100 0.0715 71 33 - 110Hexachloroethane

0.100 0.0757 76 48 - 119Hexachlorobenzene

0.100 0.0730 73 40 - 110Hexachlorobutadiene

0.100 0.0810 81 46 - 110Nitrobenzene

0.100 0.0861 86 37 - 132Pentachlorophenol

0.100 0.0602 60 10 - 110Pyridine

0.100 0.0850 85 47 - 1222,4,5-Trichlorophenol

0.100 0.0821 82 46 - 1202,4,6-Trichlorophenol






Phenol-d5 78 38 - 116





Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/28/2010 1846

04/28/2010 1910

Solid

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 680-166414

1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Leached:

Date Prepared:

Date Leached:

Instrument ID:

Lab File ID:



Injection Volume:

Instrument ID:

Lab File ID:



Injection Volume:

Client Matrix: Solid



04/22/2010 1439

04/22/2010 1439

04/19/2010 1917

04/19/2010 1917



g0895.d

200 mL

1 mL

1 uL

g0896.d

200 mL

1 mL

1 uL

Method: 8270C

Preparation: 3520C

TCLP

MSG

MSG

680-56861-3

680-56861-3



Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS

% Rec.

63 60 38 - 110 5 401,4-Dichlorobenzene

95 84 49 - 128 12 402,4-Dinitrotoluene

64 56 33 - 110 14 40Hexachloroethane

68 58 48 - 119 15 40Hexachlorobenzene

55 51 40 - 110 7 40Hexachlorobutadiene

67 59 46 - 110 13 40Nitrobenzene

89 83 37 - 132 6 40Pentachlorophenol

59 0 10 - 110 NC 40 U FPyridine

83 71 47 - 122 15 402,4,5-Trichlorophenol

77 67 46 - 120 13 402,4,6-Trichlorophenol

Surrogate MS % Rec MSD % Rec Acceptance Limits

2,4,6-Tribromophenol 91 81 40 - 139

2-Fluorobiphenyl 71 64 50 - 113

2-Fluorophenol 63 52 36 - 110

Nitrobenzene-d5 69 62 45 - 112

Phenol-d5 70 56 38 - 116

Terphenyl-d14 41 35 10 - 121




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/22/2010 1536


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

Date Leached:



04/21/2010 1423

04/19/2010 1917

md22009.d

20 mL

10 mL

2 uL

Units: mg/L

Column ID: PRIMARY

Method: 8081A_8082

Preparation: 3520C

TCLP

SGMLB 680-166103/21-D




0.0050 U 0.00500.0050Endrin


0.0025 U 0.00250.0025Heptachlor


0.0025 U 0.00250.0025Methoxychlor



DCB Decachlorobiphenyl 109 14 - 115

Tetrachloro-m-xylene 78 35 - 120




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/22/2010 1555


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

Date Leached:



04/21/2010 1423

04/19/2010 1917

md22010.d

20 mL

10 mL

2 uL

Units: mg/L

Column ID: PRIMARY

Method: 8081A_8082

Preparation: 3520C

TCLP

SGMLB 680-166109/5-D




0.0050 U 0.00500.0050Endrin


0.0025 U 0.00250.0025Heptachlor


0.0025 U 0.00250.0025Methoxychlor











WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/22/2010 1615


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:



04/21/2010 1423

md22011.d

1000 mL

10 mL

2 uL

Units: mg/L

Column ID: PRIMARY

Method: 8081A_8082

Preparation: 3520C

SGMMB 680-166252/21-A



0.00010 U 0.000100.00010Endrin


0.000050 U 0.0000500.000050Heptachlor


0.000050 U 0.0000500.000050Methoxychlor

0.0050 U 0.00500.0050Toxaphene










Water

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

md22012.d

04/21/2010 1423



1000 mL

10 mL

2 uL

Units: mg/L

Column ID: PRIMARY

Method: 8081A_8082

Preparation: 3520C

SGMLCS 680-166252/22-A


0.000200 0.000182 91 38 - 144Endrin

0.000100 0.0000893 89 31 - 118gamma-BHC (Lindane)

0.000100 0.0000973 97 30 - 133Heptachlor

0.000100 0.0000980 98 34 - 126Heptachlor epoxide

0.000200 0.000132 66 p10 - 243Methoxychlor










Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/22/2010 2321

04/22/2010 2340

Solid

Matrix Spike/


1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Leached:

Date Prepared:

Date Leached:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:




04/21/2010 1423

04/21/2010 1423

04/19/2010 1917

04/19/2010 1917



md22033.d

20 mL

10 mL

2 uL

PRIMARY

md22034.d

20 mL

10 mL

2 uL

PRIMARY

Method: 8081A_8082

Preparation: 3520C

TCLP

SGM

SGM

680-56861-1

680-56861-1




% Rec.

117 130 38 - 144 11 30Endrin

118 130 31 - 118 10 30 Fgamma-BHC (Lindane)

115 81 30 - 133 34 30 p FHeptachlor

118 118 34 - 126 0 30Heptachlor epoxide

79 79 10 - 243 0 30 p pMethoxychlor


DCB Decachlorobiphenyl 118 85 14 - 115X p

Tetrachloro-m-xylene 94 89 35 - 120


DCB Decachlorobiphenyl 85 127 14 - 115X

Tetrachloro-m-xylene 73 66 35 - 120




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/22/2010 1522


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

Date Leached:



04/21/2010 0751

04/19/2010 1917

sd22005.d

10 mL

10 mL

1 uL

Units: mg/L

Column ID: PRIMARY

Method: 8151A

Preparation: 8151A

TCLP

SGSLB 680-166109/5-B



0.050 U 0.0500.0502,4-D

0.050 U 0.0500.050Silvex (2,4,5-TP)


DCAA 97 50 - 150


DCAA 96 50 - 150

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/22/2010 1540


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:



04/21/2010 0751

sd22006.d

1000 mL

10 mL

1 uL

Units: mg/L

Column ID: PRIMARY

Method: 8151A

Preparation: 8151A

SGSMB 680-166235/18-A


0.00050 U 0.000500.000502,4-D

0.00050 U 0.000500.00050Silvex (2,4,5-TP)


DCAA 73 50 - 150p


DCAA 160 50 - 150X




Water

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

sd22007.d

04/21/2010 0751



1000 mL

10 mL

1 uL

Units: mg/L

Column ID: PRIMARY

Method: 8151A

Preparation: 8151A

SGSLCS 680-166235/19-A


0.00200 0.00207 103 50 - 1502,4-D

0.00200 0.00198 99 50 - 150Silvex (2,4,5-TP)


DCAA 101 50 - 150


DCAA 92 50 - 150

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/22/2010 2117

04/22/2010 2136

Solid

Matrix Spike/


1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Leached:

Date Prepared:

Date Leached:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:




04/21/2010 0751

04/21/2010 0751

04/19/2010 1917

04/19/2010 1917



sd22024.d

10 mL

10 mL

1 uL

PRIMARY

sd22025.d

10 mL

10 mL

1 uL

PRIMARY

Method: 8151A

Preparation: 8151A

TCLP

SGS

SGS

680-56861-23

680-56861-23




% Rec.

93 95 50 - 150 2 302,4-D

93 95 50 - 150 2 30Silvex (2,4,5-TP)


DCAA 100 97 50 - 150


DCAA 88 87 50 - 150




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/21/2010 2136


Date Prepared:

Instrument ID:

Lab File ID:



Date Leached:



04/21/2010 1045

04/19/2010 1917

165047166275.chr

5 mL

50 mL

Units: mg/L

Method: 6010B

Preparation: 3010A

TCLP

ICPDLB 680-166103/21-E



0.20 U 0.200.20Arsenic

1.0 U 1.01.0Barium

0.10 U 0.100.10Cadmium

0.20 U 0.200.20Chromium

0.20 U 0.200.20Lead

0.50 U 0.500.50Selenium

0.10 U 0.100.10Silver

Water

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



165047166275.chr

04/21/2010 1045



5 mL

50 mL

Units: mg/L

Method: 6010B

Preparation: 3010A

ICPDLCS 680-166274/22-A


20.0 19.2 96 75 - 125Arsenic

20.0 20.3 101 75 - 125Barium

0.500 0.499 100 75 - 125Cadmium

2.00 1.99 99 75 - 125Chromium

5.00 4.94 99 75 - 125Lead

20.0 19.7 99 75 - 125Selenium

0.500 0.496 99 75 - 125Silver




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/21/2010 1757


Date Prepared:

Instrument ID:

Lab File ID:



Date Leached:



04/21/2010 1049

04/19/2010 1917

165047166275.chr

5 mL

50 mL

Units: mg/L

Method: 6010B

Preparation: 3010A

TCLP

ICPDLB 680-166109/5-E



0.20 U 0.200.20Arsenic

1.0 U 1.01.0Barium

0.10 U 0.100.10Cadmium

0.20 U 0.200.20Chromium

0.20 U 0.200.20Lead

0.50 U 0.500.50Selenium

0.10 U 0.100.10Silver

Water

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



165047166275.chr

04/21/2010 1049



5 mL

50 mL

Units: mg/L

Method: 6010B

Preparation: 3010A

ICPDLCS 680-166275/8-A


20.0 19.1 96 75 - 125Arsenic

20.0 20.1 100 75 - 125Barium

0.500 0.502 100 75 - 125Cadmium

2.00 1.97 98 75 - 125Chromium

5.00 4.91 98 75 - 125Lead

20.0 20.1 101 75 - 125Selenium

0.500 0.487 97 75 - 125Silver




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/22/2010 0920


Date Prepared:

Instrument ID:

Lab File ID:



Date Leached:



04/21/2010 1203

04/19/2010 1917

1650474221091748.chr

0.50 mL

50 mL

Units: mg/L

Method: 7470A

Preparation: 7470A

TCLP

LEEMAN1LB 680-166109/5-F



0.020 U 0.0200.020Mercury

Water

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



1650474221091748.chr

04/21/2010 1203



0.50 mL

50 mL

Units: mg/L

Method: 7470A

Preparation: 7470A

LEEMAN1LCS 680-166294/10-A


0.250 0.235 94 80 - 120Mercury

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/22/2010 0940

04/22/2010 0949

Solid

Matrix Spike/


1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Leached:

Date Prepared:

Date Leached:

Instrument ID:

Lab File ID:



Instrument ID:

Lab File ID:






04/21/2010 1203

04/21/2010 1203

04/19/2010 1917

04/19/2010 1917



1650474221091748.chr

0.50 mL

50 mL

1650474221091748.chr

0.50 mL

50 mL

Method: 7470A

Preparation: 7470A

TCLP

LEEMAN1

LEEMAN1

680-56861-23

680-56861-23




% Rec.

89 89 80 - 120 0 20Mercury




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/22/2010 0952


Date Prepared:

Instrument ID:

Lab File ID:



Date Leached:



04/21/2010 1205

04/19/2010 1917

1650474221091748.chr

0.50 mL

50 mL

Units: mg/L

Method: 7470A

Preparation: 7470A

TCLP

LEEMAN1LB 680-166103/21-F



0.020 U 0.0200.020Mercury

Water

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



1650474221091748.chr

04/21/2010 1207



0.50 mL

50 mL

Units: mg/L

Method: 7470A

Preparation: 7470A

LEEMAN1LCS 680-166296/24-A


0.250 0.203 81 80 - 120Mercury

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/22/2010 1110

04/22/2010 1112

Solid

Matrix Spike/


1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Leached:

Date Prepared:

Date Leached:

Instrument ID:

Lab File ID:



Instrument ID:

Lab File ID:






04/21/2010 1205

04/21/2010 1205

04/19/2010 1917

04/19/2010 1917



1650474221091748.chr

0.50 mL

50 mL

1650474221091748.chr

0.50 mL

50 mL

Method: 7470A

Preparation: 7470A

TCLP

LEEMAN1

LEEMAN1

680-56861-19

680-56861-19




% Rec.

91 89 80 - 120 2 20Mercury




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/20/2010 0830


Date Prepared:

Instrument ID:

Lab File ID:




Prep Batch: N/A

1.0 mL

N/A

Units: mm/sec

Method: 1030

Preparation: N/A

N/A

No Equipment AssignedMB 680-166149/1

Analyte Result Qual NONE NONE

NBIgnitability

mm/secUnits:

Solid

Dilution: 1.0

Date Analyzed:


Lab Sample ID:

Client Matrix:

Date Prepared:

04/20/2010 0830

Instrument ID:

Lab File ID:




Prep Batch: N/A

1.0 mL

N/A

Method: 1030

Preparation: N/A

N/A

No Equipment Assigned680-56861-1


NBNB NCIgnitability

mm/secUnits:

Solid

Dilution: 1.0

Date Analyzed:


Lab Sample ID:

Client Matrix:

Date Prepared:

04/20/2010 0830

Instrument ID:

Lab File ID:




Prep Batch: N/A

1.0 mL

N/A

Method: 1030

Preparation: N/A

N/A



NBNB NCIgnitability




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/22/2010 0919


Date Prepared:

Instrument ID:

Lab File ID:





04/21/2010 0600

1.00 g

50 mL

Units: mg/Kg

Method: 9012A

Preparation: 9012A

N/A

LATCHATMB 680-166233/1-A


5.0 U 5.00.21Cyanide, Total

Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



04/21/2010 0600



1.00 g

50 mL

Units: mg/Kg

Method: 9012A

Preparation: 9012A

N/A

LATCHATLCS 680-166233/2-A


7.51 7.39 98 75 - 125Cyanide, Total

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/22/2010 0919

04/22/2010 0919

Solid

Matrix Spike/


1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:



Instrument ID:

Lab File ID:






04/21/2010 0600

04/21/2010 0600



1.01 g

50 mL

1.03 g

50 mL

Method: 9012A

Preparation: 9012A

N/A

N/A

LATCHAT

LATCHAT

680-56861-3

680-56861-3


% Rec.

68 36 75 - 125 35 30 F FCyanide, Total




mg/KgUnits:

Solid

Dilution: 1.0

Date Analyzed:


Lab Sample ID:

Client Matrix:

Date Prepared:

04/22/2010 0919

04/21/2010 0737

Instrument ID:

Lab File ID:





1.04 g

50 mL

Method: 9012A

Preparation: 9012A

N/A

LATCHAT680-56861-22


6.116.4 J 5 30 JCyanide, Total




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/20/2010 1134


Date Prepared:

Instrument ID:

Lab File ID:





04/20/2010 0829

1.01 g

6 mL

Units: mg/Kg

Method: 9034

Preparation: 9030B

N/A

No Equipment AssignedMB 680-166084/1-A

Analyte Result Qual RL RL

59 U 5959Sulfide

Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



04/20/2010 0829



1.00 g

6 mL

Units: mg/Kg

Method: 9034

Preparation: 9030B

N/A

No Equipment AssignedLCS 680-166084/2-A


2500 1550 62 50 - 150Sulfide




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

04/20/2010 1530


Date Prepared:

Instrument ID:

Lab File ID:





04/20/2010 0911

1.01 g

6 mL

Units: mg/Kg

Method: 9034

Preparation: 9030B

N/A

No Equipment AssignedMB 680-166099/1-A

Analyte Result Qual RL RL

59 U 5959Sulfide

Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



04/20/2010 0911



1.00 g

6 mL

Units: mg/Kg

Method: 9034

Preparation: 9030B

N/A

No Equipment AssignedLCS 680-166099/2-A


2500 1640 65 50 - 150Sulfide

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

04/20/2010 1530

04/20/2010 1530

Solid

Matrix Spike/


1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:



Instrument ID:

Lab File ID:






04/20/2010 0913

04/20/2010 0913



1.00 g

6 mL

1.01 g

6 mL

Method: 9034

Preparation: 9030B

N/A

N/A

No Equipment Assigned

No Equipment Assigned

680-56861-22

680-56861-22


% Rec.

44 44 50 - 150 1 50 F FSulfide




Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



N/A


Prep Batch: N/A

20 mL

20 mL

Units: SU

Method: 9045C

Preparation: N/A

N/A

No Equipment AssignedLCS 680-166329/1


7.00 7.020 100 63 - 158pH

SUUnits:

Solid

Dilution: 1.0

Date Analyzed:


Lab Sample ID:

Client Matrix:

Date Prepared:

04/20/2010 1000

Instrument ID:

Lab File ID:




Prep Batch: N/A

20 mL

20 mL

N/A

Method: 9045C

Preparation: N/A

N/A



6.5906.57 0 40pH

SUUnits:

Solid

Dilution: 1.0

Date Analyzed:


Lab Sample ID:

Client Matrix:

Date Prepared:

04/20/2010 1000

Instrument ID:

Lab File ID:




Prep Batch: N/A

20 mL

20 mL

N/A

Method: 9045C

Preparation: N/A

N/A



6.2906.25 1 40pH


of 173

Login Sample Receipt Check List


Login Number: 56861

Question T / F/ NA Comment

Creator: Daughtry, Beth

List Source: TestAmerica Savannah

List Number: 1

Radioactivity either was not measured or, if measured, is at or below

background

N/A

The cooler's custody seal, if present, is intact. True

The cooler or samples do not appear to have been compromised or

tampered with.

True

Samples were received on ice. True 6 coolers rec'd 4/17/10; 7th cooler rec'd on 4/19

Cooler Temperature is acceptable. True

Cooler Temperature is recorded. True 4/17 Rcpt - 0.8, 1.4, 0.9, 0.6, 1.9, 2.0 C; 4/19

recpt @ 0.2 C

COC is present. True

COC is filled out in ink and legible. True

COC is filled out with all pertinent information. True

There are no discrepancies between the sample IDs on the containers and

the COC.

True

Samples are received within Holding Time. True

Sample containers have legible labels. False Client labeled outside baggie on soil containers

had to place on containers

Containers are not broken or leaking. True

Sample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

There is sufficient vol. for all requested analyses, incl. any requested

MS/MSDs

True

VOA sample vials do not have headspace or bubble is <6mm (1/4") in

diameter.

True

If necessary, staff have been informed of any short hold time or quick TAT

needs

True

Multiphasic samples are not present. N/A

Samples do not require splitting or compositing. N/A

Is the Field Sampler's name present on COC? True

Sample Preservation Verified True


of 173

j56861-2 std tal l2 final report - mdeq · 2017-06-09 · job narrative 680-56861-2 receipt all...

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