laboratory sstandard environmental & analytical

Laboratory StandardS Environmental & Analytical Laboratories, K. J. Tower, Pathalam, Udyogamandal P. O., Ernakulam District, Kerala

Accreditation Standard ISO/IEC 17025: 2005

Certificate Number TC-5402 of 27

Validity 14.10.2017 to 13.10.2019 Last Amended on 15.02.2019

Sl. Product / Material of Test

Specific Test Performed

Test Method Specification against which tests are performed

Range of Testing / Limits of Detection

Ruchi Guntuku Convenor

Sunita Rawat Program Manager

BIOLOGICAL TESTING

I. FOODS & AGRICULTURAL PRODUCTS

1. Milk and milk Products: (Raw/Pasteurized/Sterilized/UHT/Condensed/Evaporated -Milk, Cheese, Butter, Dahi, Yogurt, Paneer, Khoya, Shrikhand , Dairy Whitener, Skim Milk Powder, Sweets, Ghee )

Total Plate Count IS 5402: 2012/ ISO4833:1991 ≥ 10 cfu/g

≥ 1 cfu /ml

USFDA (BAM) –Chapter – 3 ≥ 10 cfu/g

≥ 1 cfu /ml

Coliform count: Enumeration Method

IS 5401 Part 1 - 2012 / ISO 4832:1991

≥ 10 cfu/g

≥ 1 cfu /ml


≥ 1 cfu /ml

USFDA (BAM) –Chapter – 4 ≥ 3 MPN/g or ml

E.coli: Enumeration Method

IS 5887 Part 1 -1976 (RA 2013)

≥ 10 cfu/g

≥ 1 cfu /ml

USFDA (BAM) –Chapter - 4 ≥ 10 cfu/g

≥ 1 cfu /ml

USFDA (BAM) –Chapter - 4 ≥ 3 MPN/g or ml

Enterobacteriaceae IS/ISO 7402: 1993(RA 2012) ≥ 10 cfu /g

≥ 1 cfu /ml

S.aureus: Enumeration Method

IS 5887 Part 2 -1976 (RA 2013)

≥ 10 cfu/g

≥ 1 cfu /ml


≥ 1 cfu /ml

Salmonella spp IS 5887 Part 3 -1999 (RA 2013) / ISO 6579: 2002

Present or Absent/25g or ml

USFDA (BAM) –Chapter – 5 Present or Absent/25g or ml

Shigella spp IS 5887 Part 7 -1999 (RA 2013)


USFDA (BAM) –Chapter - 6 Present or Absent/25g or ml











Bacillus cereus: Enumeration method

IS 5887 Part 6 -1999 (RA 2012)

≥ 10 cfu/g

≥ 1 cfu /ml


≥ 1 cfu /ml

Yeast and Mould IS 5403: 1999(RA 2013) ≥ 10 cfu/g

≥ 1 cfu /ml


≥ 1 cfu /ml

Listeria monocytogenes USFDA (BAM)-Chapter-10 Present or Absent/25g or ml

2. Processed foods and Canned products: (Cooked foods, Ready to eat foods, Snack items)

Total plate count IS 5402: 2012 / ISO 4833: 2003

≥ 10 cfu/g

≥ 1 cfu /ml


≥ 1 cfu /ml


IS 5401 Part 1 -2012 / ISO 4832: 1991

≥ 10 cfu/g

≥ 1 cfu /ml


≥ 1 cfu /ml

USFDA (BAM) –Chapter – 4 ≥ 3 MPN/g or ml


IS 5887 Part 1 -1976 (RA 2005)

≥ 10 cfu/g

≥ 1 cfu /ml


≥ 1 cfu /ml



IS 5887 Part 2 -1976 (RA 2013)

≥ 10 cfu/g

≥ 1 cfu /ml

USFDA (BAM) –Chapter –12 ≥ 10 cfu/g

≥ 1 cfu /ml


IS 5887 Part 6 -1999 (RA 2012)

≥ 10 cfu/g

≥ 1 cfu /ml


≥ 1 cfu /ml

Salmonella spp IS 5887 Part 3 -1999 (RA 2013) /ISO 6579: 2002












USFDA (BAM) –Chapter – 5 Present or Absent/25g or ml



USFDA (BAM) –Chapter - 6 Present or Absent/25g or ml

Vibrio cholerae USFDA (BAM) –Chapter -09 Present or Absent/25g or ml

IS 5887 Part 5 -1976 (RA 2013)


Vibrio parahaemolyticus IS 5887 Part 5 -1976 (RA 2013)


USFDA (BAM) –Chapter 09 Present or Absent/50 g or ml

Enterobacteriaceae IS 7402: 1993 (RA 2012) ≥ 10 cfu /g

≥ 1 cfu /ml

Yeast and Mould IS 5403: 1999 (RA 2013) ≥ 10 cfu/g

≥ 1 cfu /ml

USFDA (BAM) –Chapter -18

≥ 10 cfu/g

≥ 1 cfu /ml

Listeria monocytogenes

USFDA (BAM)-Chapter-10 Present or Absent/25g or ml

3. Nut and Nut products:

Total plate count. IS 5402: 2012 / ISO 4833: 2003

≥ 10 cfu/g



IS 5401 Part 1 -2012 / ISO 4832: 1991

≥ 10 cfu/g


USFDA (BAM) –Chapter - 4 ≥ 3 MPN/g

E.coli: Enumeration Method:

IS 5887 Part 1 -1976 (RA 2013)

≥ 10 cfu/g




IS 5887 Part 2 -1976 (RA 2013)

≥ 10 cfu/g











USFDA (BAM) –Chapter 12 ≥ 10 cfu/g


IS 5887 Part 6 -1999 (RA 2012)

≥ 10 cfu/g


Salmonella spp IS 5887 Part 3 -1999 (RA 2013)/ ISO 6579: 2002

Present or Absent/25g

USFDA (BAM) –Chapter –5 Present or Absent/25g



USFDA (BAM) –Chapter - 6 Present or Absent/25g

Vibrio cholerae USFDA (BAM) –Chapter 09 Present or Absent/25g

IS 5887 Part 5 -1976 (RA 2013)




USFDA (BAM) –Chapter 09 Present or Absent/50g

Enterobacteriaceae IS/ISO 7402: 1993 (RA 2012) ≥ 10 cfu /g




4. Fruits and Vegetables : (Raw, Thermally Processed or Frozen Fruits, Vegetable products, Juices and soups, Soup powders, purees

Total plate count IS 5402: 2012 / ISO 4833: 2003

≥ 10 cfu/g

≥ 1 cfu/ml


≥ 1 cfu/ml

Coliform count: Enumeration Method:

IS 5401 Part 1 -2012 / ISO 4832: 1991

≥ 10 cfu/g

≥ 1 cfu/ml


≥ 1 cfu/ml












and pastes, Ketchups and Sauces, Jams, Fruit Squashes , Syrups Dates, Dry fruits Fruit Beverages Pickles)


IS 5887 Part 1 -1976 (RA 2013)

≥ 10 cfu/g

≥ 1 cfu/ml


≥ 1 cfu/ml


≥ 1 cfu /ml


IS 5887 Part 2 -1976 (RA 2013)

≥ 10 cfu/g

≥ 1 cfu/ml


≥ 1 cfu/ml

Salmonella spp IS 5887 Part 3 -1999 (RA 2013)/ISO 6579: 2002


USFDA (BAM) –Chapter –5 Present or Absent/25g or ml



USFDA (BAM) –Chapter –6 Present or Absent/25g or ml

Vibrio cholerae USFDA (BAM) –Chapter 09 Present or Absent/25g or ml

IS 5887 Part 5 -1976 (RA 2013)




USFDA (BAM) –Chapter-09 Present or Absent/50g or ml


IS 5887 Part 6 -1999 (RA 2012)

≥ 10 cfu/g

≥ 1 cfu/ml

USFDA (BAM) –Chapter-14 ≥ 10 cfu/g

≥ 1 cfu/ml


≥ 1 cfu/ml

USFDA (BAM) –Chapter-18 ≥10 cfu/g

≥ 1 cfu/ml












5. Beverages: (Alcoholic / Non-Alcoholic, Carbonated and Non-carbonated)

Total plate count IS 5402: 2012/ISO 4833: 2003 ≥ 1 cfu /ml

USFDA (BAM) –Chapter - 3 ≥1cfu/ml


IS 5401 Part 1 -2012 / ISO 4832: 1991

≥1cfu/ml

USFDA (BAM) –Chapter –4 ≥1cfu/ml


IS 5887 Part 1 -1976 (RA 2013)

≥ 1 cfu /ml

USFDA (BAM) –Chapter –4 ≥ 1 cfu /ml

USFDA (BAM) –Chapter - 4 < 3 to >1100 MPN/g or ml


IS 5887 Part 2 -1976 (RA 2013)

≥ 1 cfu/ml

USFDA (BAM) –Chapter 12 ≥ 1 cfu/ml


IS 5887 Part 6 -1999 (RA 2012)

≥ 1 cfu/ml

USFDA (BAM) –Chapter-14 ≥ 1 cfu/ml

Yeast and Mould IS 5403: 1999(RA 2013) ≥1cfu/ml

USFDA (BAM) –Chapter-18 ≥1cfu/ml

Enterobacteriaceae

IS/ISO 7402: 1993(RA 2012) ≥ 1 cfu /ml

Listeria monocytogenes USFDA (BAM)-Chapter-10 Present or Absent/25ml

6.

Meat and Meat Products & Fish and Sea foods products : (Raw, Frozen, Canned, Cooked –Shrimp, Prawn, Lobster, Fish, Crab, Squid, Oyster, Chicken

Total plate count IS 5402: 2012/ ISO 4833: 2003 ≥10 cfu/g

USFDA (BAM) –Chapter –3 ≥10 cfu/g


IS 5401 Part 1 -2012/ ISO 4832: 1991

≥10 cfu/g

USFDA (BAM) –Chapter - 4 ≥10 cfu/g



IS 5887 Part 1 -1976 (RA 2013)

≥10 cfu/g













and Poultry Products, Mutton, Pork, Beef)


IS 5887 Part 2 -1976 (RA 2013)

≥10 cfu/g


Salmonella spp IS 5887 Part 3 -1999 (RA 2013) ISO 6579: 2002






Vibrio cholerae IS 5887 Part 5 -1976 (RA 2013)


USFDA (BAM) Chapter -09 Present or Absent/25g



USFDA (BAM) Chapter -09 Present or Absent/50g


IS 5887 Part 6 -1999 (RA 2012)

≥ 10 cfu/g


Enterobacteriaceae IS 7402: 1993 (RA 2012) ≥ 10 cfu /g

Yeast and Mould

IS 5403: 1999 (RA 2013) ≥10 cfu/g

USFDA(BAM)-Chapter-18 ≥10 cfu/g

Listeria monocytogenes USFDA (BAM)-Chapter-10 Present or Absent/25g

7.

Herbs, Spices and condiments: ( Seasoning powder, Curry and Mixed Masala, Coriander Powder, Chilly Powder, Turmeric powder,

Total plate count IS 5402: 2012 / ISO 4833:2003 ≥10 cfu/g

USFDA (BAM) –Chapter – 3 ≥10 cfu/g


IS 5401 Part 1 -2012 / ISO 4832: 1991

≥10 cfu/g

USFDA (BAM )-Chapter - 4 ≥10 cfu/g



IS 5887 Part 1 -1976 (RA 2013)

≥10 cfu/g











Pepper, Dried ginger, Dried Cardamom, Cloves, Cumin)


USFDA (BAM) –Chapter –4 ≥ 3 MPN/g


IS 5887 Part 2 -1976 (RA 2013)

≥10 cfu/g


Salmonella spp IS 5887 Part 3 -1999 (RA 2013) / ISO 6579: 2002













IS 5887 Part 6 -1999 (RA 2012)

≥ 10 cfu/g



≥ 1 cfu /ml

Yeast and Mould IS 5403: 1999 (RA 2013) ≥10 cfu/g


Listeria monocytogenes USFDA (BAM)-Chapter-10 Present or Absent/ 25g

II. AYUSH PRODUCTS:

1.

Ayush Products: (Arishtam, Lehyam,

Aerobic plate count

API (Part 2): 2008(1st edition)

Appendix 2, Section2.4 ≥ 10 cfu /g

≥ 1 cfu /ml











Bhasmam, Choornam, Lepam, Syrup,Capsule, Ghritam,Thailam and Raw Materials)

Yeast and Mould API (Part 2): 2008(1st edition)

Appendix 2, Section2.4 ≥ 10 cfu /g

≥ 1 cfu /ml

E.coli API (Part 2): 2008(1st edition)

Appendix 2, Section2.4 Present or Absent/1g/ml

Staphylococcus aureus API (Part 2): 2008(1st edition)


Salmonella API (Part 2): 2008(1st edition)


Pseudomonas aeruginosa

API (Part 2): 2008(1st edition)


III. ENVIRONMENT AND POLLUTION:

1. Air : Aerobic Plate Count APHA 5th Edition-Chapter 3 ≥ 1 cfu /Plate

Yeast and Mould APHA 5th Edition- Chapter 3 ≥ 1 cfu /Plate

2. Swab: Total Plate Count ISO 18593:2004 ≥ 1 cfu /cm2

Yeast and Mould ≥ 1 cfu / cm2

S.aureus Absent/Swab

Coliforms Absent/Swab

E.coli Absent/Swab

Salmonella Absent/Swab

3. Sewage treated water:

Faecal coliform IS 1622: 1981 (RA 2014) <2 to >1600 MPN/100ml

IV. WATER:

1.

Raw water, Bore well Water, Surface water, Potable, Drinking Water

Standard Plate Count IS 1622: 1981 (RA 2014) ≥1 cfu/ml

Coliform:

IS 1622: 1981 (RA 2014) 2 MPN/100 ml to 1600 MPN/100ml

Coliforms: Membrane filtration Method

IS 1622: 1981 (RA 2014) Present or Absent/100 ml

Faecal Coliform:


E.coli:












Coliform: Membrane filtration Method

IS 15185: 2016 Present or Absent/250 ml

E.coli: Membrane filtration Method


Salmonella spp: Membrane filtration Method


Yeast and Mould IS 5403: 1999 (RA 2013) Present or Absent/250 ml


Present or Absent/250 ml






IS 13428 Annex D 2005 Present or Absent/ 250 ml

2. Swimming Pool Water:

Standard Plate Count IS 3328: 1993 (RA 2013) Annexure A

≥1cfu/ml

Coliforms IS 1622: 1981 (RA 2014)

2 MPN/100 ml to 1600 MPN/100ml

Coliforms Membrane filtration Method

IS 1622: 1981 (RA 2014)

Present or Absent/ml

3. Processed water: Standard Plate Count IS 1622: 1981 (RA 2014) ≥1 cfu/ml

Coliforms IS 1622: 1981 (RA 2014) 2 MPN/100 ml to 1600 MPN/100ml


IS 13428 Annex D 2005 Present or Absent/250 ml











CHEMICAL TESTING

I. ATMOSPHERIC POLLUTION

1. Ambient Air Quality/Work Environment and Indoor Air Quality

Suspended Particulate Matter

IS 5182 (Part 4):1999 (RA:2014)

2.0 µg/m3 to1500

µg/m3

Particulate Matter (size Less than 10µm) or PM10

IS 5182(Part 23):2006 (RA:2012)

5.0 µg/m3 to 1000

µg/m3

Particulate Matter (size Less than 2.5µm) or PM2.5

EPA 40 CFR Part 50 Appendix-L

2.0 µg/m3 to 500

µg/m3

Sulphur Dioxide as SO2 IS 5182 (Part 2):2001 (RA:2012)

2.0 µg/m3 to100

µg/m3

Nitrogen dioxide as NO2 IS 5182(Part 6):2006 (RA:2012)

2.0 µg/m3 to 200

µg/m3

Ozone as (O3) IS 5182(Part 9):1974 (RA:2014)

5.0 µg/m3 to 1000

µg/m3

Ammonia as (NH3) InHouse Method: SEAAL/SOP/18 Issue Date : 01/15.12.2017

20 µg/m3 to 700

µg/m3

Hydrogen Sulphide IS 5182(Part 7):1973 (RA:2014)

2.0 µg/m3 to 100

µg/m3

Carbon Monoxide as CO

IS 5182(Part 10):1999 (RA:2014).(b) Indicator Tube Method.

1.15 mg/m3 to 100

mg/m3

Lead as Pb IS 5182(Part 22):2004 (RA:2014)

0.01 µg/m3 to 10

µg/m3

Nickel as Ni USEPA Compendium method IO-3.4 Jun-1999 &IO-3.2 Jun-1999

5.0 ng/m3 to 100

ng/m3

Arsenic as As USEPA Compendium method IO-3.4 Jun-1999

0.1 ng/m3 to 10

ng/m3











Benzene as (C6H6) IS 5182(Part 11):2006 (RA 2012)

4.0 µg/m3 to 100

µg/m3

Benzo(α)Pyrene Particulate Phase only

IS 5182(Part 12):2004 (RA:2014)

0.80 ng/m3 to 500

ng/m3

2. Stack Emission/ Process/Vent Emissions

Temperature IS 11255(Part 3):2008 30 °C to 650 °C

Velocity IS 11255(Part 3):2008 1.5 m/s to 60 m/s

Volume of Gas Discharged

IS 11255(Part 3):2008 100 Nm3/hr to 40,00000 Nm3/hr

Particulate Matter IS 11255(Part 1):1985 (RA:2014)

5.0 mg/Nm3 to

1000 mg/Nm3

Sulphur Dioxide as SO2 IS 11255(Part 2):1985 (RA:2014)

3.0 mg/Nm3 to

1500 mg/Nm3

Oxides of Nitrogen as NOX

IS 11255(Part 7):2005 (RA:2012)

2.0 mg/Nm3 to

750 mg/Nm3

Hydrogen Sulphide IS 11255(Part 4):2006 (RA:2012)

2.0 mg/m3 to 100

mg/m3

Ammonia IS 11255(Part 6):1999 (RA:2014)

5.0 mg/m3 to 200

mg/m3

Carbon Monoxide as CO

IS 13270:1992:(RA:2014)- Orsat analysis

0.2 % to 5 %

Carbon Dioxide as CO2 IS 13270:1992:(RA:2014)- Orsat analysis

0.2 % to 10 %

Oxygen as O2 IS 13270:1992:(RA:2014)- Orsat analysis

0.2 % to 21 %

3. Noise Level Monitoring

Leq, Lmax, Lmin IS 9989:1981(RA:2008) 30 dB(A) to 130 dB(A)

4. Illumination Monitoring

Illumination In House Method: SEAAL/SOP/16 Issue Date : 01/03.04.2017

0 to 2,00,000 LUX

II. WATER

1.

Drinking water/ Surface Water/ Ground Water/ Water from

Colour IS 3025(Part 4):1983 (RA:2012)

1 Hazen to 500 Hazen

Odour IS 3025(Part 5):1983 (RA:2012)

Qualitative (Objectionable/











Purifiers Unobjectionable)

Turbidity IS 3025(Part 10):1984 (RA:2012)

0.1 NTU to 1000 NTU

pH IS 3025(Part 11):1983 (RA:2012)

1 Unit to 14 Unit

Conductivity IS 3025(Part 14):1984 (RA:2013)

10 µs/cm to 100000 µs/cm

Taste (Drinking Water only)

IS 3025(Part 8):1984 (RA:2012)

Qualitative (Agreeable/Disagreeable)

Total Dissolved Solids IS 3025(Part 16):1984 (RA:2012)

10 mg/L to 100000 mg/L

Total Solids IS 3025(Part 15):1984 (RA:2014)

1 mg/L to 100000 mg/L

Total Hardness as CaCO3

IS 3025(Part 21): 2009(RA:2014)

1 mg/L to 2500 mg/L

Calcium as Ca IS 3025(Part 40):1991 (RA:2014)

1 mg/L to 1500 mg/L

Magnesium as Mg IS 3025(Part 46):1994 (RA:2014)

1 mg/L to 1500 mg/L

Total Alkalinity as CaCO3

IS 3025(Part 23):1986 (RA:2014)

1 mg/L to 2500 mg/L

Acidity as CaCO3 IS 3025(Part 22):1986 (RA:2014) APHA (23rdEdition) 2310-B: 2017

1 mg/L to 5000 mg/L

Phenolphthalein Alkalinity as CaCO3

IS 3025 (Part 23): 1986 (RA 2014) APHA (23

rd Edition)

2320-B: 2017

1 mg/L to 500 mg/L

Carbonate Hardness as CaCO3

IS 3025(Part 21): 2009 (RA: 2014) APHA (23

rdEdition)

2340-A, C & 2320 B: 2017

1 mg/L to 5000 mg/L











Non- Carbonate Hardness as CaCO3

IS 3025 (Part 21): 2009 (RA: 2014) APHA (23

rd Edition)

2340-A, C & 2320 B: 2017

1 mg/L to 5000 mg/L

Chloride as Cl-

IS 3025(Part 32):1988 (RA:2014)

1 mg/L to 2500 mg/L

ResidualChlorine IS 3025(Part 26):1986 (RA:2014) APHA (23

rd Edition)

4500-Cl B: 2017

1 mg/L to 10 mg/L

Nitrate as NO3 APHA (23rd

Edition) 4500-NO3 B: 2017

1 mg/L to 100 mg/L

Nitrite as NO2 IS 3025(Part 34):1988 (RA:2014) APHA (23

rd Edition)

4500-NO2 B: 2017

0.02 mg/L to 10 mg/L

Sulphate as SO4 IS 3025(Part 24):1986 (RA:2014)

1 mg/L to 500 mg/L

Iron as Fe IS 3025(Part 53):2003 (RA:2014)

0.1 mg/L to 50 mg/L

Fluoride as F IS 3025(Part 60):2008 (RA: 2013) APHA (23

rd Edition)

4500-F-B, D: 2017

0.1 mg/L to 20 mg/L

Silica as SiO2 IS 3025(Part 35):1988 (RA:2014) APHA (23

rd Edition)

4500-SiO2 C, D: 2017


Dissolved Phosphate as P

IS 3025(Part 31):1988 (RA:2014) APHA (23

rd Edition)

4500-P B,D: 2017


Total Phosphate as P IS 3025(Part 31):1988 (RA:2014) APHA (23

rd Edition)












4500-P B,D: 2017

Hexavalent Chromium as Cr

6+

APHA (23rd

Edition) 3500 Cr B: 2017 IS 3025(Part 52):2003 (RA:2014)


Phenolic Compounds as C6H5OH

IS 3025(Part 43):1992 (RA:2014) APHA (23

rd Edition) 5530-

B,C,D: 2017

0.01mg/L to100 mg/L

Lead as Pb IS 3025(Part 47):1994 (RA:2014) APHA (23

rd Edition)

3111-B: 2017


Arsenic as As IS 3025(Part 37):1988 (RA:2014) APHA (23

rd Edition) 3114-C:

2017 APHA (23rd

Edition) 3120-B: 2017

0.002 mg/L to 10 mg/L

Nickel as Ni IS 3025(Part 54):2003 (RA:2014) APHA (23

rd Edition)

3111-B: 2017


Mercury as Hg IS 3025(Part 48):1994 (RA:2014) APHA (23

rdEdition)

3112-B: 2017

0.002 mg/L to 10 mg/L

Aluminum as Al IS 3025(Part 55):2003 (RA:2014) APHA (23

rd Edition)

3111-D: 2017


Manganese as Mn IS 3025(Part 59):2006 (RA:2012) APHA (23

rd Edition)

3111-B: 2017

0.05 mg/L to 100 mg/L











Copper as Cu IS 3025(Part 42):1992 (RA:2014) APHA (23

rd Edition)

3111-B: 2017

0.05 mg/L to 100mg/L

Cadmium as Cd IS 3025(Part 41):1992 (RA:2014) APHA (23

rd Edition)

3111-B: 2017

0.03 mg/L to 100 mg/L

Total Chromium as Cr IS 3025(Part 52):2003 (RA:2014) APHA (23

rd Edition)

3111-B: 2017

0.40 mg/L to 100 mg/L

2.

Water for Construction Purpose

pH IS 3025(Part 11):1983 (RA:2012) APHA (23

rd Edition)

4500-H+

B: 2017

1 to 14

Organic Solids IS 3025(Part 18):1984 (RA:2012)

1 mg/L to 10000 mg/L

Inorganic Solids IS 3025(Part 18):1984 (RA:2012)


Sulphate as SO4 IS 3025(Part 24):1986 (RA;2014) APHA (23

nrd Edition) 4500-

SO4-E: 2017

1 mg/L to 5000 mg/L

Chloride as Cl IS 3025(Part 32):1988 (RA:2014) APHA (23

nrdEdition)

4500 Cl-B: 2017


Suspended Matter IS 3025(Part 17):1984 (RA:2012) APHA (23

rd Edition)

2540-D: 2017












Water Neutralization To Neutralize 100ml Sample of Water, Using Phenolphthalein as An indicator, Using 0.02N NaOH

IS 3025(Part 22):1986 (RA:2014)

0.1 ml to 50 ml

Water Neutralization To Neutralize 100ml Sample of Water, Using Mixed indicator Using 0.02N H2SO4

IS 3025(Part 23):1986 (RA:2014)

0.1 ml to 50 ml

3.

Swimming Pool Water

pH IS 3025(Part 11):1983 (RA:2012) APHA (23

rd Edition)

4500-H+

B: 2017

1 to 14

Colour IS 3025(Part 4):1983 (RA:2012)


Odour IS 3025(Part 5):1983 (RA:2012)

Qualitative (Objectionable/ Unobjectionable)

Turbidity IS 3025(Part 10):1984 (RA;2012)

0.1 NTU to 1000 NTU

Taste IS 3025(Part 8):1984 (RA:2012)

Qualitative (Agreeable/ Disagreeable)


1.0 mg/L to 100000 mg/L


IS 3025(Part 23):1986 (RA:2014)

1 mg/L to 2500 mg/L

Chloride as Cl IS 3025(Part 32):1988 (RA:2014) APHA (23

rdEdition)

4500 Cl-B: 2017












ResidualChlorine IS 3025(Part 26):1986 (RA:2014) APHA (23

rd Edition)

4500-Cl B: 2017

1 mg/L to 10 mg/L

Oxygen Observed in 4hrs@ 27°C

IS 3025(Part 63):2007 (RA: 2013)

0.05 mg/L to 100 mg/L


0.1 mg/L to 50 mg/L

Lead as Pb IS 3025(Part 47):1994 (RA:2014) APHA (23rd Edition) 3111-B: 2017


Aluminum as Al IS 3025(Part 55):2003 (RA:2014) APHA (23

rd Edition)

3111-D: 2017


4. Reagent Grade Water

Specific Conductivity

IS 3025(Part 14):1984 (RA: 2013) APHA (23

rd Edition)

2510-B: 2017

5 µmohs/cm to 10000 µmohs/cm

pH IS 3025(Part 11):1983 (RA:2012) APHA (23

rdEdition)

4500-H+ B: 2017

1 to 14

Total Solids Or Non Volatile Residue at 105° C

IS 3025(Part 15):1984 (RA 2014) APHA (23

rd Edition)

2540-B: 2017

1 mg/L to 100 mg/L

Silica as Sio2 IS 3025(Part 35):1988 (RA:2014) APHA (23

rd Edition)

4500-SiO2 C, D: 2017

0.01 mg/L to 5 mg/L

Colour Retention of KMno4 at 27° C

IS 1070:1992 (RA:2013) Annexure A

10 min to 60 min











III. POLLUTION AND ENVIRONMENT

1.

Waste Water (Effluents/ Sewage)

Colour IS 3025(Part 4):1983 (RA:2012)


pH IS 3025(Part 11):1983 (RA:2012)

1 to 14

Conductivity IS 3025(Part 14):1984 (RA: 2013)

10 µs/cm to 100000 µs/cm

Temperature IS 3025(Part 9):1984 (RA:2006) APHA (23

rd Edition)

2550-B:2017

20 °C to 45 °C

Total Solids IS 3025(Part 15):1984 (RA:2014)

10 mg/L to 50000 mg/L


10 mg/L to 50000 mg/L

Total Suspended Solids IS 3025(Part 17):1984 (RA:2012)


Oil & Grease IS 3025(Part 39):1991 (RA:2014)

5 mg/L to 500 mg/L

Fixed Soilds

IS 3025(Part 18):1984 (RA:2012) APHA (23

rd Edition)

2540-E: 2017


Volatile Solids

IS 3025(Part 18):1984 (RA:2012) APHA (23

rd Edition)

2540-E: 2017


Acidity as CaCO3 IS 3025(Part 22):1986 (RA:2014) APHA (23

rd Edition)

2310-B: 2017

1 mg/L to 5000 mg/L











Phenolphthalein Alkalinity as CaCO3

IS 3025(Part 23):1986 (RA:2014) APHA (23

rd Edition)

2320-B: 2017

1 mg/L to 500 mg/L


IS 3025(Part 23):1986 (RA:2014) APHA (23

rd Edition)

2320-B: 2017

1 mg/L to 5000 mg/L

Total Hardness as CaCO3

IS 3025 (Part 21): 2009 (RA: 2014) APHA (23

rd Edition)

2340-C: 2017


Carbonate Hardness as CaCO3

IS 3025(Part 21):2009 (RA:2014) APHA (23

rd Edition)

2340-A, C & 2320 B: 2017

1 mg/L to 5000 mg/L

Non- Carbonate Hardness as CaCO3

IS 3025 (Part 21): 2009 (RA:2014) APHA (23

rd Edition)

2340-A, C & 2320 B: 2017

1 mg/L to 5000 mg/L

Calcium as Ca IS 3025(Part 40):1991 (RA:2014)

1 mg/L to 1500 mg/L

Magnesium as Mg IS 3025(Part 46):1994 (RA:2014)

1 mg/L to 1500 mg/L

Residual Chlorine IS 3025(Part 26):1986 (RA:2014) APHA (23

rd Edition)

4500-Cl B: 2017

1 mg/L to 10 mg/L

Chloride as Cl IS 3025(Part 32):1988 (RA:2014)

1 mg/L to 100000 mg/L

Chemical Oxygen Demand (COD)

IS 3025(Part 58):2006 (RA:2012)

10 mg/L to 200000 mg/L

Biochemical Oxygen Demand for 3 days @ 27°C

IS 3025(Part 44):1993 (RA:2014)

2 mg/L to100000 mg/L











Dissolved Oxygen IS 3025(Part 38):1989 (RA:2014) APHA (23

rd Edition)

4500-O-B, C: 2017

0.2 mg/L to 8 mg/L

Ammonical Nitrogen as NH3-N

IS 3025(Part 34):1988 (RA:2014) APHA (23

rd Edition)

4500-NH3 B,C: 2017

1 mg/L to 500 mg/L

Free Ammonia as NH3 IS 3025(Part 34):1988 (RA:2014) APHA (23

rd Edition)

NH3 B,C: 2017


Nitrate as NO3 APHA (23rd Edition) 4500-NO3 B: 2017

1 mg/L to 100 mg/L

Total Kjeldhal Nitrogen IS 3025(Part 34):1988 (RA:2014) APHA (23

rd Edition)

4500-Norg B: 2017

1 mg/L to 100mg/L

Nitrite as NO2 IS 3025(Part 34):1988 (RA:2014) APHA (23

rd Edition)

4500-NO2 B: 2017

0.02 mg/L to10 mg/L

Sulphate as SO4 IS 3025(Part 24):1986 (RA:2014)

1 mg/L to 5000 mg/L



Fluoride as F IS 3025(Part 60):2008 (RA: 2013) APHA (22nd Edition) 4500-F-B, D: 2012

0.1 mg/L to 20 mg/L

Silica as SiO2 IS 3025(Part 35):1988 (RA:2014) APHA (23

rd Edition)

4500-SiO2 C, D: 2017












Dissolved Phosphate as P

IS 3025(Part 31):1988 (RA:2014) APHA (23

rd Edition)

4500-P B,D: 2017


Total Phosphate as P IS 3025(Part 31):1988 (RA:2014) APHA (23

rd Edition)

4500-P B,D: 2017


Sulphide as S IS 3025(Part 29):1986 (RA:2014) APHA (23

rd Edition)

4500-S F: 2017

1 mg/L to 100 mg/L

Hexavalent Chromium as Cr

6+

IS 3025(Part 52):2003 (RA:2014) APHA (23

rd Edition)

3500 Cr B: 2017


Phenolic Compounds as C6H5OH

IS 3025(Part 43):1992 (RA:2014) APHA (23

nrd Edition)

5530-B,C,D: 2017

0.01 mg/L to100 mg/L

Lead as Pb IS 3025(Part 47):1994 (RA:2014) APHA (23rd Edition) 3111-B: 2017


Arsenic as As IS 3025(Part 37):1988 (RA:2014) APHA (23

rd Edition)

3114-C: 2017 APHA (23

rd Edition)

3120-B:2017

0.002 mg/L to 10 mg/L

Nickel as Ni IS 3025(Part 54):2003 (RA:2014) APHA (23

rd Edition)

3111-B: 2017












Mercury as Hg IS 3025(Part 48):1994 (RA:2014) APHA (23

rd Edition)

3112-B: 2017

0.002 mg/L to10 mg/L

Aluminium as Al IS 3025(Part 55):2003 (RA:2014)


Manganese as Mn APHA (23rd

Edition) 3111-B: 2017

0.05 mg/L to 100 mg/L

Copper as Cu IS 3025(Part 42):1992 (RA;2014) APHA (23

rd Edition)

3111-B: 2017

0.05 mg/L to 100 mg/L

Cadmium as Cd IS 3025(Part 41):1992 (RA:2014) APHA (23

rd Edition)

3120-B: 2017

0.03 mg/L to 100 mg/L

Total Chromium as Cr IS 3025(Part 52):2003 (RA:2014) APHA (23

rd Edition)

3111-B: 2017

0.40 mg/L to 100 mg/L

2. Soil/Sediment/Sludge/Solid/ Semi-Solid

pH IS 10158:1982(RA:2009) 1 to 14

Conductivity IS 14767:2000(RA:2016) 1 mS/cm to 200 mS/cm

Moisture IS 2720(Part 2):1973 (RA:2015)

0.1 to 50 %

Organic Matter IS 2720(Part 22):1972 (RA:2015)

0.1% to 50 %

Total Kjeldahl Nitrogen as N

IS 14684:1999(RA:2014) 0.05 % to 10 %

Total Phosphorus as P IS 10158:1982(RA:2009) 10 mg/kg to 1000 mg/kg

Lead as Pb EPA 3050 B Dec-1996, EPA 7000B Feb-2007

5 mg/kg to 1000 mg/kg

Nickel as Ni EPA 3050 B Dec-1996, EPA 7000B Feb-2007

2.5 mg/kg to 1000 mg/kg











Manganese as Mn EPA 3050 B Dec-1996, EPA 7000B Feb-2007


Copper as Cu EPA 3050 B Dec-1996, EPA 7000B Feb-2007


Cadmium as Cd EPA 3050 B Dec-1996, EPA 7000B Feb-2007


IV. FOOD AND AGRICULTURAL PRODUCTS

1. Dairy & Dairy Products (Raw &Processed Milk, Curd, Paneer, Cheese, Dairy Based confectioneries Evaporated /Condensed Butter, Ice cream and other dairy products, Infant milk food)

Moisture FSSAI Manual-Milk and Milk Product-2016, 10.2, pp 86-87

0.5 95 g/100g to 95 g/100g

Total ash IS: 1165: 2002 (RA:2013)/ FSSAI Manual-Milk and Milk Product-2016, 10.7 pp 90-91

0.2 g/100g to 10 g/100g

Ash insoluble in Dil.HCl FSSAI Manual-Milk and Milk Product-2016, 10.8 pp 91-92

0.1 g/100g to 5 g/100g

Protein IS 1479(Part 2): 1961 (RA:2013) FSSAI Manual-Milk and Milk Product-2016, 19.1 pp 166-172

0.5 g/100g to 80 g/100g

Fat IS: 11721:2013 FSSAI Manual-Milk and Milk Product-2016,10.3 p88

0.5 g/100g to 100 g/100g

Total Solids FSSAI Manual-Milk and Milk Product-2016, 1.3.3 pp36-37

5.0 g/100g to100 g/100g

Solid Not Fat FSSAI Manual-Milk and Milk Product-2016, 15.2 p 138

5.0 g/100g to100 g/100g

Titrable acidity IS: 1165: 2002 FSSAI Manual-Milk and Milk Product-2016, 10.4 pp 88-89

0.5 g/100g to 40 g/100g

pH IS 3507: 1966 (RA:2013) 1 to 14

2. Fruit and vegetable products (Fresh and

Moisture FSSAI Manual-Fruit and Vegetable Product-2016, 4.1 pp 34-35

0.5 g/100g to 95 g/100g











thermally processed fruit and vegetable products, canned fruit, fruit concentrate, pulps, Beverages, sauces, beverages,jam,jelly,Pickels

Total Ash FSSAI Manual-Fruit and Vegetable Product-2016, 11.3 pp 41-42

0.5 g/100g to 15 g/100g

Ash insoluble in Dil.HCl FSSAI Manual-Fruit and Vegetable Product-2016, 5.3 pp 35-36

0.1 g/100g to 5 g/100g

Acidity as acetic acid IS: 2860:1964 (RA: 2008) FSSAI Manual-Fruit and Vegetable Product-2016 2.4, pp 12-14

0.1 g/100g to 5 g/100g

Protein FSSAI Manual-Fruit and Vegetable Product-2016.

0.5 g/100g to 20 g/100g

3. Meat and meat products & Fish & Fish products

Moisture FSSAI Manual-Meat & Meat and Fish & Fish Product-2016, 2.2 p 59

0.5 g/100g to 70 g/100g

Protein IS 5960(Part1):1996 (RA:2009) FSSAI Manual-Meat & Meat and Fish & Fish Product-2016, 2.2 pp 38-39

0.5 g/100g to 85 g/100g

Total Fat FSSAI Manual-Meat & Meat and Fish & Fish Product-2016, 2.1 p 38

0.5 g/100g to 65 g/100g

4. Nut and Nut products (Ground nut kernel, Pistacho, Almond , cashew kernel. Walnut, dry fruits and dates)

Moisture IS 4684:1975 (RA:2010) 1 g/100g to 25 g/100g

Total Ash IS 4684:1975 (RA:2010) 0.1 g/100g to 15 g/100g

Total Fat IS 4684:1975 (RA:2010) 1 g/100g to 65 g/100g

Acid insoluble ash IS 4684:1975 (RA:2010) 0.01 g/100g to 2.5 g/100g

Protein

IS 4684:1975 (RA:2010) 0.2 g/100g to 75 g/100g











5. Cereal & Pulses(Atta, maida, Suji, Rawa, Barley, Whaat, maize, Jawar, Lentils, Urd, Moong, Channa, Rice, Oats, Beans, Corn Products, Custard, Macaroni)

Moisture IS:7874(Part 1):1975 (RA:2014)

1 g/100g to 20 g/100g

Acid insoluble ash IS:7874(Part 1):1975 (RA:2014)

0.05 g/100g to 10 g/100g

Total ash IS:7874(Part 1):1975 (RA:2014)

0.5 g/100g to 10 g/100g

Protein IS:7874(Part 1):1975 (RA:2014)

0.2 g/100g to 90 g/100g

Fat IS:7874(Part 1):1975 (RA:2014)

0.5 g/100g to 20 g/100g

6. Spices and Condiments (Caraway,Cardamom, Whole Chilli, Capsicum, Cinnamon, Mace, Cassia, Coriander, Pepper Nutmeg, Mustard, (black & white) , Poppy, Turmeric, curry powder, Mixed masala, aniseed and ajowan)

Moisture IS: 1797:1985 (RA: 2013) FSSAI Manual-Spices and Condiments-2016, 3.0 pp 2-5

1.0 g/100g to 50 g/100g

Total ash IS: 1797:1985 (RA: 2013) FSSAI Manual-Spices and Condiments-2016, 4.0 pp 12-13

0.5 g/100g to 20 g/100g

Ash Insoluble in Dil.HCl IS: 1797:1985 (RA: 2013) FSSAI Manual-Spices and Condiments-2016, 5.0 p 14

0.1 g/100g to 5 g/100g

7. Oils And Fats (Including Ground nut/ Sesame/ Linseed oil/Mahua Rape-seed/ Coconut/ Corn/ Rice bran/ Sunflower / Mustard oil/Soya bean Oil/

Moisture IS: 548(Part 1):1964 (RA:2015) FSSAI Manual-Oils and Fats-2016, 3.1, pp 5-6

0.01 g/100g to 5 g/100g

Peroxide Value IS: 548(Part 1):1964 (RA:2015)

1 meq/Kg to 100 meq/Kg

Specific gravity IS: 548(Part 1):1964 (RA:2015)

0.5 to 1.5

Iodine Value IS: 548(Part 1):1964 (RA:2015)

5 to 250











Ghee/Fish oil/Palmolein/ Palm kernel//Poppy seed)

FSSAI Manual-Oils and Fats-2016, 12.0 pp 26-30

Saponification Value IS: 548(Part 1):1964 (RA:2015) FSSAI Manual-Oils and Fats-2016, 9.0, pp 18-20

50 to 400

Acid Value IS: 548(Part 1):1964 (RA:2015) FSSAI Manual-Oils and Fats-2016, 1.0, pp 23-25

0.50 to 100

laboratory sstandard environmental & analytical

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