m. pittman icuil 2010 - watkins glen, ny, october 2010 1 icuil 2010 xuv beamlines for applications...

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M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou, J. C. Lagron, M. Pittman , D. Ros, S. Daboussi, D. Zimmer, J. Demailly, B. Cros

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Page 1: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 20101

ICUIL 2010

XUV beamlines for applications at LASERIX facility

O. Guilbaud, S. Kazamias, K. Cassou, J. C. Lagron, M. Pittman, D. Ros, S. Daboussi, D. Zimmer, J. Demailly, B. Cros

Page 2: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 20102

OUTLINE

1 – The LASERIX facility : an overview

2 – Research on XUV sources and applications from 2007 to 2009

4 – Prospects and conclusion

3 – Present status of LASERIX (2010)

Page 3: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 20103

1- The LASERIX facility:

an overview

Page 4: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 20104

OUTLINE

Paris-Sud XI University (Orsay) - Laser Center of PSU (CLUPS)Integrated in Federation for Light-Matter Interaction (LUMAT) in 2010

Status : Soft X ray Laser platform for applications

Director : David ROS

Location : ENSTA Palaiseau (coll. LOA & ILE)

Operation : 2003 - 2008 : development room at LOA (turquoise room) May 2009 : Moving to new building next to LUIRE-ILE (Bât. P)

Staff (10 pers.) : 5 researchers & professors, 2 engineers, 2 technicians, 2 PhD

Collaborations :Laser → ILE, LOA (Palaiseau, F), CEA (Saclay & CESTA, F)XUV sources → LPGP (Orsay, F), LOA, LULI, LCFIO (Palaiseau, F), GSI (Darmstadt, DE),

PALS (RT)

Page 5: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 20105

GOAL

LASERIX

Facility for XUV experiments

HRR

Laser driver

PW class

Ti:Sa

2 J - 10 Hz

XUV Laser

High rep. rate > 10nm - 1 µJ - 10 Hz

40 J – 0.1 HzXUV Laser

High energy> 4-8 nm - 20 µJ – 0.1 Hz

Compressor

100 mJ - 10 Hz –40 fs à 10 ps

HHG : > 20 nm - 10 Hz

Compressor100 mJ - 10 Hz –40 fs à 10 ps

HHG : > 20 nm - 10 HzHE

→ XUV wavelengths : 8 nm à 32 nm→ XUV energy : > µJ→ XUV rep. rate : 0.1 Hz & 10 Hz→ Multibeam - optically synchronized (IR fs-ps & HHG)

Page 6: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 20106

Laser amplification for PW Performances

Demonstration of36 J @ 0.1 Hz

with 72J pump energy

F. Plé et al., Opt. Lett., Vol. 32 (2007)M. Pittman et al., ICUIL 2006 (Cassis)

Diameter: 100 mm

Thickness : 20 mm

Absorption (@ 532nm) : 97%

Ti:Sa Crystal (Crystal Systems)

4 Pass-Amplifier

Transverse lasing suppression with

Index matching liquid + absorbing dye

Liquid IN

Liquid OUT

IR beam

8 beams – 100 J – 0.1 Hz pumping

Homogenized pump laser Profiles

Page 7: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 20107

Research on XUV sources and applications : 6 years in 1 slide

2004 - 2006 : Laser installation in a development room (90m2)& demonstration of laser amplification @ 40 J / 0.1 Hz

2007 - 2009 : → X-ray and HHG sources @ 10 Hz→ increase reliability→ first applications @ 10 Hz

IR

XUV

David ROS in X-Ray lasers conference, Belfast 2008 : « Waiting for moving in the new building at end of this year » 

Started may 2009

Page 8: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 20108

2 – Research on XUV sources and applications

from 2007 to 2009

Page 9: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 20109

Arrangement of the experimental area

2007 : XUV laser & experiments

40 J – 0.1Hz Amplifier

IR Beam

XUV Beam

2 J - 10Hz Front-end

Pulse Compressor

XUV Generation

Experiment Chamber

Page 10: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 201010

XUV Generation by transient collisionnal excitation : GRIP scheme

Solid Target

Stretched laser pulse(500 ps, 0.5 J)

DelayedCompressed laser pulse

(4 ps, 0.7 J)

XUV beam

Plasma column

Page 11: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 201011

XUV Development : DGRIP principle (single beam pumping technique)

Solid Target

XUV beam

Plasma column

Stretched laser pulse(500 ps, 0.5 J)

+Delayed

Compressed laser pulse (4 ps, 0.7 J)

ONE BEAM

Page 12: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 201012

Öffner stretcher

Regenerative amplifier

Amplifiers

Compression

Regen cavity selects the propagation direction the two pulses propagate along the same beam path

XUV Development : DGRIP scheme

Page 13: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 201013

XUV Development : demonstrated beamlines

Demonstrated applicationDouble-stand breaks in DNA samples

induced with X-ray laser

F. Lindau et al., Opt. Exp.15, 9486 (2006)K. Cassou et al. Opt. Lett.32, 2 (2007)

X-ray laser source

Wavelengths:

18,9 nm (Mo ni-like,4d-4p) and 22.6 nm (4f-4d)

13,9 nm (Ag ni-like, 4d-4p)

Repetition rate : 10 HzSource size 20 µm x 60 µmDivergence 5 mrad x10 mradEnergy : >1 J

Wavelength

Gas cell

HHG source

H43 = 18.9 nm

Page 14: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 201014

XUV Development : diagnostics & automation

XUV diagnostics

Spatial

Energy

Near field imaging

~300 shots on the same place of the target

(DGRIP configuration)

Footprint (Far field ~2m from source)

Multilayer mirror photocurrent (pico-amperemeter)

& Calibrated near field imaging

0.00E+00

5.00E+06

1.00E+07

1.50E+07

2.00E+07

2.50E+07

3.00E+07

0 50 100 150 200 250 300 350

shot number

ne

ar

fie

ld e

ne

rgy

(a

.u)

0.00E+00

5.00E+06

1.00E+07

1.50E+07

2.00E+07

2.50E+07

3.00E+07

0 50 100 150 200 250 300 350

Page 15: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 201015

XUV Development : diagnostics & automation

Automation of experiments (B. Zielbauer, coll. GSI)

50 mm

Fresh target surface every 200 shots

System stops when the desired number of shots / integrated signal is reached

Up to 25000 shots of 300 nJ in 2 h 4,3.1014 photons (65 eV) / cm2

Page 16: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 201016

Users : • LCAM (Univ. Paris XI) : E. Porcel, C. Le Sech, S. Lacombe • GPS (Univ. Paris VI) : A.-M. Penhoat, A. TouatiBackground • Effect of pulsed ionising radiation on DNA• Investigation of direct effects• Single strand or double strand break of DNA moleculesExperimental method• Irradiation of plasmids (DNA loops)• Accumulation of a XUV dose perfectly known and uniform• Strand rate estimation by an ex-situ electrophoresis

Example of application using the optimized XUV source

DNA samples irradiation

Courtesy of B. Zielbauer (GSI, DE)

Page 17: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 201017

3 – Present status of LASERIX from 2010

Page 18: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 201018

Present status of LASERIX 2010 : Implementation in the new building

ADONISlaser driver

Comp. 2J - 10Hz

SXRL 10 Hz

HHG 10 Hz

SXRL 0.1 Hz

Comp.40J -0.1Hz

SXRL 0.1 Hz

HHG 0.1 Hz

Page 19: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 201019

ADONIS : The Laser driver Scheme

FRONT-END10Hz - 4 Pass Preamplifier

Oscillator

Verdi 5V

Öffner Stretcher

Dazzler

10Hz - Regenerativeamplifier

QL - CFR

0.1Hz - 8 x 12.5J – 527nm pump lasers (100J)

Femtolaser fs-20

0.1

Hz

Nd

:Gla

ss

0.1

Hz

Nd

:Gla

ss

AMPLI - HE

MZ

10Hz – fs Booster Pre-amplifier

QL - ULTRA

FR

PK CA

SPK C

PK C

PK C

QL - ULTRA

2.5J – 0.1Hz

10Hz - 4 Pass Direct water cooled Power Amplifier

PROPULSE

PROPULSE

10Hz - 4 Pass Cryogenic Power Amplifier

PROPULSE

PROPULSE

PROPULSE

PROPULSE

PROPULSE

PROPULSE

AMPLI - HC

0.1

Hz

Nd

:Gla

ss

0.1

Hz

Nd

:Gla

ss

XU

V

HC

/2 moving plate (0.1 Hz)

>10 mJ – 50 fs – 10 Hz (IR probes, HHG…)

1J - 0.1Hz / 10Hz 40 fs

> 50 mJ – 40 fs – 10 Hz (IR probes, HHG…)2.5J – 10Hz (99% shots )

/2

10 J - 0.1 Hz 40 fs - 100 ps

XU

V

HE

20 J - 0.1 Hz 500 ps

0.1Hz - 4 x 20J – 527nm pump lasers (80J) – LBO SHG

Page 20: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 201020

Ground floor

Overview of the laser driver ADONIS and SXRL sources area

Page 21: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 201021

Overview of the experimental area

Page 22: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 201022

4- Prospects and Conclusion

Page 23: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 201023

LASERIX Beamlines

SXRL 10Hz

HHG10Hz

Exp. 1

Exp. 2

ADONIS

2.5J 10Hz

100mJ 10Hz

SXRL - HC

40J 0.1Hz

100mJ 0.1Hz

SXRL 0.1HzExp. 3

HHG0.1Hz

SXRL - HE

Ongoing → ready for 2011

Coming soon → expected for 2012

Page 24: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 201024

Status and ongoing work

Present situation• ADONIS (Laser driver) operating at 2.5 J – 10 Hz

• Two 10 Hz compressed IR beamlines available : 1.4 J / 1 ps to 100 ps (SXRL) 100 mJ / 40 fs (IR probe or HHG pumping)

• 100 J / 0.1 Hz pump lasers ready with DKDP, LBO installed soon (160 J expected)→ 4 beams (2 tables) will be shared with ILE (LUIRE & APPOLON)

• 10 Hz SXRL and HHG under development→ expected with optimized performances before end 2010 (GRIP &

DGRIP)

• Full Command-control of the entire installation under development→ expected before summer 2011 (coll. Amplitude Technologies)

Coming soon• 10 Hz SXRL beamline opening for experiments (coll.) → beginning 2011

• 40 J – 0.1 Hz amplifier (8 pump beams) & compressor → planned for beginning 2011

• 0.1 Hz high energy SXRL development → planned for mid-2011

• 0.1 Hz SXRL HE beamline opening for experiments (coll.) → end 2011

Page 25: M. Pittman ICUIL 2010 - Watkins Glen, NY, October 2010 1 ICUIL 2010 XUV beamlines for applications at LASERIX facility O. Guilbaud, S. Kazamias, K. Cassou,

M. PittmanICUIL 2010 - Watkins Glen, NY, October 201025

THANK YOU