on-line process control using modular fluidic delivery and...
TRANSCRIPT
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October 24, 2013
On-Line Process Control Using Modular Fluidic Delivery
and Fast Micro Process Gas Chromatography: From
Sample Point to the DCS Connection
Sampling Platforms for the Field and Laboratory
Mike Cost – Senior Engineer Analytical Products
Parker Instrumentation Products Division
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Analytical Products: The Big Picture (Process/Lab)
Sample Conditioning – Parker IntraFlow™
Sample Disposal Vent Master™
Sample Extraction
Parker IPD/IPDE
DBB Probe
Sample Transport Heat Traced Tube Bundles
Process analysis requires
efficient control of
temperature, pressure and
flow at all levels of
analytical architecture
Change Over System
Key Products: Gen II R-MaxTM - Analysis
Vent MasterTM - Pressure
IntraflowTM – Heat/Pressure/Flow
IntraflowTM – Gas Blending/Calibration
The package = IPD, Veriflo, Porter, IPDE
IntraflowTM Gas Blending
+
DATA !!
Gas Generators
Process/On-Line Laboratory
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Parker Analytical Products: Conditioning for Analysis
• Most important physical parameters for process/lab
analytical measurement: Pressure, Flow and Temperature
3
How? Pressure Control – Parker Vent MasterTM
or IntraflowTM
Flow Control – Porter Mass Flow,
Volumetric or SC423XL Flow Controllers -
IntralfowTM
Temperature Control – Intertec Smart
Blocktherm or Varitherm Heaters, steam
or fluid flow through pegboard, Veriflo
Vaporizing Regulators - IntraflowTM
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Sampling Flow Architecture: Process and the
Laboratory
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Sampling
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IntraflowTM Parker Modular (NeSSITM) System
Slip-fit intra-
fitting connectors
Same screw size
throughout
ISA/ANSI SP76.00.02
Compliant
Mounting
“Pegboard”
Field connectors
(top or end)
Same plane
flowpaths
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Design Driver
• Simplicity Overcomes Limitations
Intraflow™ Fitting Intraflow™ System
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Design Driver
• Simplicity Overcomes Limitations
IntraFlow™ Fitting IntraFlow™ System
Parker Tube Fitting Conventional Sampling™ System
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Pressure & Temperature
Ratings
Heated Pegboard:
1/2” (12.7mm)
Aluminum
500psig
2500psig
1/8” (12.7mm)
316SS
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Pegboard Heating Option: Low Pressure Steam
9
-40 C air purge supply @ 60psig / 4
bar & 20 SLPM, outlet temp 46 C
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Temperature Control: Conductive Heating
10
• Temperature setpoint 500C
• Heat transferred efficiently to components
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IntraFlow™ Fitting
IntraflowTM Substrates/Flowpath Options: The Library is Has Become Much Larger to Accommodate
Laboratory and Process Applications (over 100 flow options)
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Standard of
Flexibility
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IntraFlow™ Fitting
Eductor
Stream
Selection
Versatility of IntraflowTM
fitting allows multiple
options for flow and
sample conditioning
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Sample System Variability Accommodated
13
Stack Gas Monitoring:
• O2 Analyzer
• Eductor
• Flow Monitoring
• Pressure Control/Monitoring
• Sample Stream Selection
• Remote Calibration/Validation
Manual Liquid Sample Control:
• Manual Valve Isolation
• Space Reduction
• Sample Header Implementation
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Why Modular Sampling Systems?
• Modularity provides greater flexibility - multiple
flow path options and expansion available; customization
• Integration of traditional hardware with
modular components feasible – high particulate
laden samples
• Superior temperature control – heating and
cooling
• Lower cost to operate – maintenance simplified and
system changes are completed with a single device
• Lower sample stream volumes – micro-reactors
and R&D
• Faster turnover rates – close-coupled analysis
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IntraflowTM: Applications Versatility
15 0 500 1000 1500 2000 2500 3000 35000
0.2
0.4
0.6
0.8
1
1.2
Raman Shift (cm-1
)
No
rm
alized
In
ten
sit
y (
Arb
. U
nit
s)
Normalized Standard Spectra
• PEEK substrate and fluidic control hardware
• RAMAN and NMR technology
implemented from a single sampling
platform
• Standardized platform provides ability to
machine specialized sampling systems
• Sampling system allows integration of
conventional hardware (i.e. pumps,
analytical systems, etc.)
• Intraflow microreactor
sample conditioning system
• Analytical platform
• Provided sample
introduction and purge
• Portability
• Pump for liquid recirculation
• Fluidic control hardware
• Sensor Interface
• Temperature Control
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IntraflowTM: Sampling Applications Review
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Applications Detail
• Falcon Calidus GC
• Parker IntraflowTM
sampling system
• Carrier gas
• Transportable
• Biotech
• Refinery
IntraflowTM and MicroFast GC Analyzer Applications
Courtesy of Falcon Analytical
MicroGC coupled with Parker IntraflowTM Sample
Conditioning System provides realization modularity concepts
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Specifications
• Falcon Analytical
Process GC
• Parker IntraflowTM
sampling system
• Carrier gas generation
or cylinder supply
• Cart mounted for
Mobility
IntraflowTM and Transportable Analyzer Applications
Courtesy of Falcon Analytical
Mobile Unit with Support Equipment
Mounted - Bring the Lab to the Field
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Biotech: Fermenter Headspace Analysis
19
• Multiple stream continuous
analysis
• Space constrained area
• Atmospheric pressure sample
• Moisture laden sample
Application Overview:
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IntraflowTM and Falcon Calidus GC: Flow
Architecture
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Integrated IntraflowTM Sampling System
Sampling Pump
Permeation Tube
Heated Backplane 600C
Solenoid Valves
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The Results Are… THE SAME
regardless of installation site
84
seconds
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Modular Intraflow NeSSI, Modular Calidus GC, Modular
Calidus Process Analyzer
Results in Minutes
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Falcon Analyzer Reporting via MODBUS to DCS
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• Polygas C 9
• Automatic report
• 4.1%
• Notes
• All 3 analyzers functioning beautifully
• Realtime chromatograms on the Calidus PC screen
• End of run reports show for every GC at run end
Courtesy of Falcon Analytical
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Analytical Products: The Big Picture (Process/Lab)
Sample Conditioning – Parker IntraFlow™
Sample Disposal Vent Master™
Sample Extraction
Parker IPD/IPDE
DBB Probe
Sample Transport Heat Traced Tube Bundles
Process analysis requires
efficient control of
temperature, pressure and
flow at all levels of
analytical architecture
Change Over System
Key Products: Gen II R-MaxTM - Analysis
Vent MasterTM - Pressure
IntraflowTM – Heat/Pressure/Flow
IntraflowTM – Gas Blending/Calibration
DATA !!
Gas Generators
Process/On-Line Laboratory
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Parker Systems and Analytics: The Complete Solution
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Parker – IPD: Analytical Products Installed Base
Parker IntraflowTM first modular platform installed for major grass roots project ExxonMobil SPT - Singapore
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Acknowledgments
• Brian Marquadt, Charlie Branham,
Michael Roberto, and Thomas Dearing– Applied Physics Laboratory University of Washington
• Kin – Tek Laboratories
• CPAC –University of Washington
• Falcon Analytical
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