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PERFORMANCE EVALUATION
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Scheduled StudyLPTP16-S3 4967010820-Jul-2016 Through 02-Sep-2016 RTC Labcode
MT00945EPA Labcode
Participating Laboratory:Energy Laboratories-HelenaJon HagerE 3161 Lyndale AvenueHelena MT 59601 US
Thank you for participating in study LPTP16-S3. Additional information about this study may be found onlineat www.sigmaaldrich.com/pt.
Sigma-Aldrich RTC Inc.2931 Soldier Springs RoadLaramie, WY 82070 USA1-307-742-5452www.sigmaaldrich.com
This report shall not be reproduced except in full, without written approval of the laboratory. The data andresults reported in this document are the property of the participating laboratory and are confidential. If youwish to appeal an evaluation listed in this report, please call our QA Supervisor at (307) 742-5452 or [email protected]
Sincerely,
Jennifer DuhonProficiency Testing Supervisor
LPTP16-S3
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AccreditorsEvaluations of this dataset will be sent to the accreditor(s) listed below using your laboratory's labcode listed above eachaccrediting agency. If any of the information listed below is incorrect, please contact RTC immediately.
RTC is accrediated to perform PT programs for the scope of accredation to ISO/IEC 17043under ANAB certificate AP-1469
LPTP16-S3
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Medium Level Volatile Aromatics
Method:EPA 8260B (1996) [10184802]
Analyte ResultUnitsAssigned
ValueAccept.Window Z Evaluation
Benzene 1,2 5620 ug/Kg 5630 4040 to7210 -0.02 Acceptable
4375 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:1.0144, b:-23.1327,c:0.0910, d:20.8707
Chlorobenzene 1,2 3420 ug/Kg 3290 2330 to4250 0.4 Acceptable
4475 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:0.9950, b:123.9983,c:0.0752, d:81.8833
1,2-Dichlorobenzene 1,2 7840 ug/Kg 7960 5810 to10100 -0.17 Acceptable
4610 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:1.0058, b:33.2037,c:0.0835, d:56.7766
1,3-Dichlorobenzene 1,2 5230 ug/Kg 5410 3790 to7020 -0.33 Acceptable
4615 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:0.9994, b:68.8728,c:0.0807, d:108.8153
1,4-Dichlorobenzene 1,2 7240 ug/Kg 7290 5410 to9180 -0.08 Acceptable
4620 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:0.9796, b:84.9657,c:0.0741, d:82.1266
Ethylbenzene 1,2 9640 ug/Kg 8230 5570 to10900 1.59 Acceptable
4765 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:1.0062, b:72.8042,c:0.1069, d:20.5270
Naphthalene 1,2 3760 ug/Kg 3840 2170 to5510 -0.14 Acceptable
5005 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:1.0092, b:-147.4204,c:0.0896, d:204.0207
Styrene 1,2 6720 ug/Kg 6930 4160 to9700 -0.23 Acceptable
5100 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary Evaluation Parameter - a:1, b:0, c:0.1333, d:0
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Toluene 1,2 2500 ug/Kg 2220 1520 to2920 1.21 Acceptable
5140 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:1.0099, b:-3.1595,c:0.0985, d:15.5403
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Method:EPA 8260B (1996) (Continued)
Analyte ResultUnitsAssigned
ValueAccept.Window Z Evaluation
1,2,4-Trichlorobenzene 1,2
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Medium Level Volatile Halocarbons
Method:EPA 8260B (1996) [10184802]
Analyte ResultUnitsAssigned
ValueAccept.Window Z Evaluation
Bromodichloromethane 1,2 6620 ug/Kg 6890 4580 to9200 -0.35 Acceptable
4395 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:1.0554, b:-51.4544,c:0.1066, d:68.3365
Bromoform 1,2
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1,1-Dichloroethane 1,2
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Method:EPA 8260B (1996) (Continued)
Analyte ResultUnitsAssigned
ValueAccept.Window Z Evaluation
1,2-Dichloroethane 1,2 8480 ug/Kg 8870 6560 to11200 -0.51 Acceptable
4635 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:0.9833, b:197.4423,c:0.0590, d:248.0448
1,1-Dichloroethylene 1,2 11300ug/Kg 86604330 to13000 1.83 Acceptable
4640 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:1, b:0, c:0.16667,d:0
cis-1,2-Dichloroethylene 1,2 3090 ug/Kg 2920 1750 to4090 0.44 Acceptable
4645 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary Evaluation Parameter - a:1, b:0, c:0.1333, d:0
1,2-Dichloropropane 1,2 4110 ug/Kg 3320 2320 to4320 2.38 Acceptable
4655 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary Evaluation Parameter - a:1, b:0, c:0.10, d:0
trans-1,2-Dichloroethylene 1,2
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5115 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:1.0083, b:36.6090,c:0.1108, d:56.3068
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Method:EPA 8260B (1996) (Continued)
Analyte ResultUnitsAssigned
ValueAccept.Window Z Evaluation
1,1,1-Trichloroethane 1,2 5540ug/Kg 57504140 to
7360 -0.39 Acceptable
5160 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:1.0197, b:-56.4801,c:0.0837, d:60.6064
1,1,2-Trichloroethane 1,2 7020ug/Kg 65904580 to
8600 0.64 Acceptable
5165 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:0.9983, b:47.7354,c:0.1018, d:2.8755
Trichloroethene (Trichloroethylene) 1,2 6720ug/Kg 61504220 to
8090 0.88 Acceptable
5170 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:0.9890, b:161.3820,c:0.0939, d:76.8331
1,2,3-Trichloropropane 1,2 6830ug/Kg 45002150 to
6850 2.98 Acceptable
5180 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:0.9225, b:230.3408,c:0.1215, d:220.1008
Group Analysis SummaryAcceptable : 21 / 22Score : 95.45% - (Acceptable)
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Medium Level Volatile Ketone/Ethers
Method:EPA 8260B (1996) [10184802]
Analyte ResultUnitsAssigned
ValueAccept.Window Z Evaluation
Acetone 1,2 33600ug/Kg 18300 0 to 37700 2.36 Acceptable
4315 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:0.9105, b:72.792,c:0.3202, d:70.9627
2-Butanone (Methyl ethyl ketone, MEK) 1,2 13400ug/Kg 86002440 to14700 2.34 Acceptable
4410 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:0.8688, b:472.7627,c:0.1877, d:295.7230
2-Hexanone 1,2 17800ug/Kg 147007350 to22100 1.27 Acceptable
4860 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:1, b:0, c:0.16667,d:0
4-Methyl-2-pentanone (MIBK) 1,2 11700ug/Kg 91405300 to13000 2 Acceptable
4995 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary
Evaluation Parameter - a:0.9537, b:-38.8138,c:0.1005, d:313.1912
Methyl tert-butyl ether (MTBE) 1,2 8320 ug/Kg 8660 6060 to11300 -0.39 Acceptable
5000 / SPE002H-25G - Lot LRAB1274/Analyst:KW/ Analysis Date: 2016-09-01
Evaluation Criteria - 1Voluntary Evaluation Parameter - a:1, b:0, c:0.10, d:0
LPTP16-S3
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Minerals
Method:EPA 300.0 2.1 (1993) [10053200]
Analyte ResultUnitsAssigned
ValueAccept.Window Z Evaluation
Bromide 1,2 61.3 mg/Kg 74.2 54.2 to94.3 -1.93 Acceptable
1540 / SPE013-30G - Lot LRAA8537/Analyst:SW/ Analysis Date: 2016-08-11
Evaluation C