phase ii esa report draft rwm - tranzon

Phase II ESA Report 12 Parcels

Bleachery Court, LLC

Concord, North Carolina

H&H Job No. BLC-001 September 10, 2013

i S:\AAA-Master Projects\Bleachery Court LLC - BLC\BLC-001 12 Parcels - Concord, NC\Phase II ESA\Report\Phase II ESA Report.docx

Table of Contents 1.0 Introduction and Background ....................................................................................................... 1

2.0 Soil Sampling ................................................................................................................................... 5

2.1 Sampling Methodology .............................................................................................................. 5

2.2 Sample Results ............................................................................................................................ 6

3.0 Groundwater Sampling .................................................................................................................. 7

3.1 Groundwater Sample Locations ................................................................................................. 7

3.2 Sampling Methodology .............................................................................................................. 9

3.3 Sample Results .......................................................................................................................... 10

4.0 Summary ........................................................................................................................................ 12

List of Tables

Table 1 Summary of Soil Analytical Results

Table 2 Summary of Groundwater Analytical Results

List of Figures

Figure 1 Site Location Map

Figure 2A Site Map – Southern Properties

Figure 2B Site Map – Northern Properties

List of Appendices

Appendix A Soil Boring and Monitoring Well Logs & Well Construction

Appendix B Laboratory Analytical Reports

Appendix C Groundwater Sampling Records and Field Calibration Log

1 S:\AAA-Master Projects\Bleachery Court LLC - BLC\BLC-001 12 Parcels - Concord, NC\Phase II ESA\Report\Phase II ESA Report.docx

Phase II ESA Report 12 Parcels

Bleachery Court, LLC Concord, North Carolina H&H Job No. BLC-001

1.0 Introduction and Background

Hart & Hickman, PC (H&H) has prepared this Phase II Environmental Site Assessment (ESA)

report to document soil and groundwater sampling conducted at the Bleachery Court, LLC

properties located at 300 Magnolia Street NW and 302 Moore Place NW (collectively the

“northern properties”) and 303/311 Bleachery Court and 254 Cedar Drive NW (collectively the

“southern properties”) in Concord, Cabarrus County, North Carolina. A Site Location Map is

included as Figure 1.

Northern Properties

The northern properties are comprised of seven parcels of land that total 13.91 acres that are

occupied by two vacant industrial buildings located at 300 Magnolia Street NW and 302 Moore

Place NW. A Phase I ESA conducted for the northern properties by H&H in June 2013

identified the following potential areas of concern:

A multi-level former textile mill previously operated in the central portion of the subject

site at the address 300 Magnolia Street NW from the early 1900s until the 2000s (Figure

2A). According to Sanborn Fire Insurance maps, the textile mill included textile carding

and spinning mills, a machine shop, an engine room, a boiler room, a water reservoir

(67,000-gallons), a cotton warehouse, a dye house, a 38,000-gallon water tower, and a

waste house. A rail spur previously extended off of the rail line located southwest of the

subject site and crossed the central portion of the 300 Magnolia Street NW property. A

majority of the former textile buildings were demolished in the 1990s and 2000s. A

warehouse building previously utilized for textile operations and for truck service

activities remains on the 300 Magnolia Street NW property has been vacant since the

2000s.


A former foundry and machine shop previously operated in two buildings located in the

northern portion of the subject site at the address 302 Moore Place NW (Figure 2A)

beginning in the 1930s until the structures were demolished in the 1950s/1960s. An

existing textile warehouse was reportedly constructed on the property located at 302

Moore Place NW in the 1970s and was previously occupied by Kerr Bleaching and

Finishing (1970s) for textile operations. The textile/storage warehouse is currently

vacant.

The environmental database report obtained as part of the Phase I ESA indicated that

Cabarrus Consolidating (300 Magnolia Street NW a.k.a. Magnolia Street and St. John

Street) previously operated on the subject site and reportedly maintained registration on

the following three underground storage tanks (USTs):

a 20,000-gallon diesel UST installed in May 1978 which was removed from the

property in January 1992;

a 10,000-gallon diesel UST installed in May 1976 which was removed from the

property in December 1987; and

a 550-gallon oil or waste oil UST installed in January 1964 which was removed

from the property in December 1999.

The status of the three USTs listed above is reported to be permanently closed and H&H

did not identify record of a release incident associated with the USTs. H&H did not

observe evidence of the former USTs during our site visit. H&H also requested

information and documents from site contact and property manager Mr. Robert Watson

regarding the former USTs. Mr. Watson did not have knowledge of the location of the

former USTs and he reported that the USTs were removed from the site prior to his

employment as property manager.


H&H identified a fill port and vent pipe associated with a heating oil UST (size not

reported) located in the eastern portion of the subject site on the 302 Moore Place NW

property (Figure 2A). Site contact Mr. Watson reported that the previous tenant, Concord

Warehousing Company, stored heating oil in the UST to heat the warehouse. Mr.

Watson was not aware of a release incident associated with the UST.

Cabarrus Consolidating (listed at 300 Magnolia Street NW) (Figure 2A) previously

generated spent halogenated solvent hazardous waste at the site. Resource Conservation

and Recovery Act (RCRA) violations were reported during compliance evaluations

conducted in 1994 and 1997. However, the enforcement actions were reportedly written

and informal and compliance was achieved for the violations. H&H did not locate record

of a release incident associated with the use, storage, and/or disposal of hazardous waste

at the site.

Southern Properties

The southern properties are comprised of five parcels of land that total 14.27 acres. The site is

occupied by a former boiler house located at 311 Bleachery Court, a vacant textile warehouse

located at 303 Bleachery Court, and a former embroidery shop located at 254 Cedar Drive NW.

A Phase I ESA conducted at the southern properties by H&H in June 2013 identified the

following potential areas of concern:

Two former textile mills previously operated at locations in the western (Kerr Bleaching

and Finishing Works) and southeastern (Cannon Mills Co.) portions of the property from

the early 1900s until the 1970s/1980s (Figure 2B). According to Sanborn Fire Insurance

maps, the former Kerr Bleaching and Finishing Works was comprised of multiple

industrial buildings and warehouses that included a finished product warehouse, a

150,000-gallon cistern, a chemical storage building, a box warehouse, a bleaching and

dye warehouse, a starch building, and a boiler building.

The former Cannon Manufacturing Co. Plant No. 3 was comprised of cotton warehouses,

weaving mills, a pump house, a water tower, a bleachery, a weaving warehouse, a boxing


and carding building, a machine shop, a boiler house, supply buildings, and carding and

spinning warehouse. A stream and a former rail spur extend in a southwesterly direction

through the central portion of the property.

During our site reconnaissance, H&H identified two groundwater monitoring wells

(labeled MW-9 and DMW-3) installed in the southeastern portion of the subject site

(Figure 2B). Site contact and property manager Mr. Robert Watson was not aware of the

purpose of the monitoring wells and he did not have copies of previous reports or

laboratory data that would provide record of groundwater quality from samples collected

from the monitoring wells.

The environmental database report obtained as part of the Phase I ESA indicated that

Cabarrus Consolidating and Management Co. previously operated at the site and is listed

in the UST and Facility Index System (FINDS) databases. According to information

provided in the Site report, the facility maintained registration on a 20,000-gallon diesel

UST installed in May 1974 and removed from the property in March 1988. H&H did not

observe evidence of the former UST during our site visit. H&H requested information

and documents from Mr. Watson regarding the former UST. Mr. Watson did not have

knowledge of the location of the former UST and he reported that the UST was removed

from the site prior to his employment as property manager.

To assess the potential areas of concern, H&H conducted Phase II ESA soil and groundwater

sampling in July 2013. Soil sampling was conducted in the area of the known heating oil UST

on the northern properties. The other potential areas of concern on both the northern and

southern properties were assessed by performing groundwater sampling in multiple locations in

and downgradient of potential areas of concern to determine if there were significant

groundwater impacts associated with historical site activities. The methods, results, and

conclusions of our Phase II ESA are presented in the following sections.


2.0 Soil Sampling

H&H conducted soil sampling activities to assess the potential for impact in the area of the

existing fuel oil UST basin area along the southeastern wall of the vacant warehouse and former

textile facility located at 302 Moore Place (northern properties). Prior to the sampling activities,

H&H notified the North Carolina One-Call Center to identify subsurface utilities. Details of soil

sampling activities and results are provided in the following sections.

2.1 Sampling Methodology

H&H personnel conducted the Phase II ESA soil sampling activities at the site on July 19, 2013.

A hand auger was initially used to locate the top and lateral extent of the UST. Then, two soil

borings, labeled SB-1 and SB-2, were advanced within five feet of the southwestern and

northeastern edges of the UST respectively. Soil boring locations are depicted in Figure 2A.

The borings were advanced using a track-mounted Geoprobe® 6620DT direct-push technology

(DPT) drill rig. The borings were advanced to approximately 15 ft below ground surface (bgs).

During boring advancement, continuous soil samples were collected from the borings using a

macro-core sampler lined with acetate sleeves. Soil samples collected from the borings were

described for lithologic purposes, inspected for the presence of staining and odors, and field-

screened for the presence of volatile organic compounds (VOCs) with a calibrated photo-

ionization detector (PID). Boring logs with lithologic descriptions and field screening results are

included in Appendix A. Soil samples collected for laboratory analysis were placed into

laboratory-supplied containers, which were then sealed, labeled, placed into laboratory-supplied

sample coolers, and covered with ice. The coolers were delivered under standard chain-of-

custody protocols to TestAmerica Laboratories of Nashville, Tennessee. The laboratory

analytical data report and chain-of-custody record are included in Appendix B.

The sample with the highest PID reading in SB-1 was detected at a depth of 9 - 11 ft bgs (5.3

ppm), and the highest PID reading in SB-2 (3.1 ppm) was detected at a depth of 9 – 11 ft bgs.


These soil samples were therefore submitted for analysis of gasoline range total petroleum

hydrocarbons (TPH-GRO) and diesel range TPH (TPH-DRO) by EPA Method 8015C.

2.2 Sample Results

A tabular summary of the analytical results of the soil samples collected from the fuel oil UST is

presented in Table 1. The laboratory analytical data report is included as Appendix B. The

analytical results were compared to the DENR Action Level of 10 mg/kg for TPH-GRO and

TPH-DRO.

The results of analysis of the samples indicated that TPH-GRO was detected in the SB-1 sample

at a concentration of 8.72 mg/kg, and TPH-GRO was detected at a concentration of 9.60 mg/kg

in the SB-2 sample. These concentrations are below the DENR UST Section Action Level of 10

mg/kg. TPH-DRO concentrations were below laboratory reporting limits for the samples

collected from both SB-1 and SB-2.


3.0 Groundwater Sampling

H&H conducted groundwater sampling activities at the site to assess the potential for significant

groundwater impact from historical site activities. Temporary monitoring wells were installed

and sampled in these areas in July 2013. In addition, H&H sampled the existing shallow

monitoring well (labeled MW-9) near the former boiler room located on the eastern portion of

the property. The methods and results of these groundwater assessment activities are presented

below.

3.1 Groundwater Sample Locations

Northern Properties

H&H installed three shallow temporary monitoring wells on the northern properties as part of

Phase II ESA activities completed at the site on July 19 and 22, 2013. The temporary wells were

installed using a track-mounted Geoprobe® 6620DT DPT rig. Temporary well locations are

shown in Figure 2A. The temporary wells were installed in the following locations:

300 Magnolia Street

N-TMW-1 was installed south-southeast and topographically downgradient of the former

truck service building.

N-TMW-2 was installed west-southwest and topographically downgradient of the former

Kerr Bleaching and Finishing Mill.


302 Moore Place

N-TMW-3 was installed west and topographically downgradient of the former foundry,

machine shop, and textile facility.

Southern Properties

H&H installed four shallow temporary monitoring wells and sampled one pre-existing

permanent monitoring well on the southern properties as part of Phase II ESA activities

completed at the site on July 18 and 19, 2013. The temporary wells were installed using a track-

mounted Geoprobe® 6620DT DPT rig. The temporary wells locations and existing monitor well

locations are shown in Figure 2B. The temporary wells and permanent well locations are as

follows:

Cedar Drive

S-TMW-1 was installed south and topographically downgradient of the former Cannon

Mill #3, a former spinning and weaving facility, and former warehouse.

S-TMW-2 was installed west and topographically downgradient the former machine shop

and weaving and towel bleaching mills.

Existing monitor well MW-9 is located west and topographically downgradient of the

former boiler room and former bleaching mill.

Bleachery Court

S-TMW-3 was installed southwest and topographically downgradient of the former

chemical building.

S-TMW-4 was installed southeast and topographically downgradient of the former Kerr

Bleaching and Finishing Mill, boiler room, and warehouse.

After the groundwater sampling was completed, the temporary wells located on the northern and

southern properties were abandoned and the borings were patched to match the surrounding

surface. Well boring logs and copies of the temporary well construction are included in

Appendix A.


Details of the groundwater sampling activities are provided in the following sections.

3.2 Sampling Methodology

The wells were installed using the DPT rig to advance a 2-inch diameter macro-core boring until

refusal or groundwater was encountered (approximately 25 ft bgs), then installing PVC well

screen to bracket the water table and riser in the boring. A filter sand pack was installed from the

bottom of each temporary well boring to approximately 2 ft above the PVC well screen, and a 2

ft thick bentonite seal was then installed above the filter sand pack. Temporary monitoring well

boring logs are provided in Appendix A.

Following installation of each temporary monitoring well, H&H measured depth-to-groundwater

in each well relative to the approximate elevation of the ground surface. N-TMW-1 reached

refusal on partially weathered rock prior to encountering the water table. H&H attempted

borings in multiple locations in this area but each encountered refusal before encountering

groundwater in each boring. Therefore, H&H was unable to collect a groundwater sample at the

N-TMW-1 location. On the northern properties, the depth-to-water (DTW) measurements in

wells N-TMW-2 and N-TMW-3 ranged from approximately 9.5 to 18 ft bgs. On the southern

properties, DTW measurement in the wells ranged from approximately 6 to 12 ft bgs.

Following DTW measurements, H&H personnel purged groundwater from each well using low-

flow techniques and dedicated polyethylene tubing until field measurements of temperature, pH,

and conductivity stabilized. When field parameters stabilized, groundwater samples were

collected in laboratory-supplied containers which were then sealed, labeled, placed into

laboratory-supplied sample coolers, and covered with ice. The coolers were delivered under

standard chain-of-custody protocols to TestAmerica Laboratories. The laboratory analytical data

report and chain-of-custody record are included in Appendix B. Low-flow sampling records that

include DTW measurements and field groundwater quality parameter measurements are

provided in Appendix C. The samples collected from the temporary monitoring wells were


submitted for analysis of VOCs by EPA Method 8260 and semi-VOCs (SVOCs) by EPA

Method 8270.

3.3 Sample Results

A tabular summary of the analytical results of the groundwater samples collected from the six

temporary monitoring wells and one existing shallow groundwater monitoring well are presented

in Table 2. Groundwater data were compared to NC DENR 15A NCAC 02L.0202 Ground

Water Quality Standards (NC groundwater standards). A discussion of the analytical results for

groundwater samples collected from the northern and southern properties are presented below.

Northern Property

Results of analysis of the groundwater samples collected from N-TMW-2 and N-TMW-3 did not

indicate the presence of compounds above laboratory detection limits.

Southern Property

Analytical results of sample S-TMW-1 collected near the former Cannon Mill #3, former

spinning and weaving building, and former warehouse did not indicate the presence of detectable

levels of analyzed VOCs and SVOCs.

Analytical results of sample S-TMW-2 sample collected near the former weaving and towel

bleaching mill indicated the presence of the SVOC bis(2-ethylhexyl)phthalate at a concentration

of 31.9 µg/L, which is slightly higher than its NC groundwater standard of 3 µg/L. No other

compounds were detected in groundwater above NC groundwater standards.

Analytical results of the S-TMW-3 sample collected near the former chemical building indicated

that the VOCs benzene (6.35 µg/L) and p-isopropyltoluene (59.6 µg/L) were detected slightly

above their NC groundwater standards of 1 µg/L and 25 µg/L, respectively. No other

compounds were detected above laboratory reporting limits.


Analytical results of sample S-TMW-4 collected near the former Kerr bleaching and finishing

facility, boiler room, and warehouse indicated the presence of several VOCs and SVOCs but at

concentrations below their NC groundwater standards.

Analytical results of the existing permanent monitoring well identified as MW-9 located near the

boiler room and towel bleaching mill indicated the presence of the VOC 1,2-dichloroethane at a

concentration of 1.22 µg/L which is slightly higher than the NC groundwater standard of 0.4

µg/L. No other compounds were detected above NC groundwater standards.

Please note that none of the detected compound concentrations exceeded the DENR Inactive

Hazardous Sites Branch (IHSB) residential or industrial vapor intrusion screening levels

indicating that the groundwater impacts do not pose a significant risk to indoor air in potential

future on-site buildings.


4.0 Summary

H&H has completed Phase II ESA activities at the Bleachery Court, LLC northern and southern

properties in Concord, NC. The results of the ESA assessment activities indicate the following:

Northern Properties

TPH-DRO and TPH-GRO were not detected above DENR action levels in the area of

the existing fuel oil UST on the eastern portion of the building located at 302 Moore

Place NW.

No compounds were detected above NC groundwater standards in the groundwater

samples collected from the northern properties. There is no evidence of groundwater

impact at the northern properties.

Southern Properties

Low levels of four compounds were detected in three temporary wells and one existing

monitor well in concentrations slightly above NC groundwater standards collected from

the southern properties. No high concentration groundwater impacts were identified in

the southern properties. The detected concentrations did not exceed the DENR IHSB

residential or industrial vapor intrusion screening levels indicating that the groundwater

impacts do not pose a significant risk to indoor air in potential future on-site buildings.

Based upon our experience, it would be highly unlikely that DENR would require active

remediation of the groundwater impacts or that DENR would actively request further

assessment or remediation of the impacts. The presence of the groundwater impacts

slightly above groundwater standards could be easily managed through a Brownfields

agreement with DENR.

Table 1 (Page 1 of 1)Summary of Soil Analytical Results

Bleachery Court, LLCConcord, North Carolina

H&H Job No. BLC-001

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Table 1(Page 1 of 1)Hart & Hickman, PC

8015C 8015C

SB-1 (9-11) 7/19/13 Fuel Oil UST 9-11 8.72 <6.25

SB-2 (9-11) 7/19/13 Fuel Oil UST 9-11 9.60 <6.62

10 10

Notes:Concentrations reported in milligrams per kilogram (mg/kg)TPH = Total Petroleum Hydrocarbons; DRO = Diesel Range Organics; GRO = Gasoline Range UST = Underground Storage Tank

Action Level (mg/kg)

Sample IDDate

Collected

Potential Area of

ConcernSample Depth

(ft) TPH

-GR

O

Analytical Method

TPH

-DR

O

Table 2 (Page 1 of 1)Summary of Groundwater Analytical Results

Bleachery Court, LLC12 parcels

Concord, North CarolinaH&H Job No. BLC-001

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Table 2 (Page 1 of 1)Hart & Hickman, PC

Ben

zene

1,2-

Dic

hlor

oeht

ane

Diis

opro

pyl E

ther

Eth

ylbe

nzen

e

p-Is

opro

pylto

luen

e

N-TMW-2 7/22/13 Former Kerr Bleaching & Finishing Mill <5.00 <1.00 <1.00 <2.00 <1.00 <1.00 <3.00 <8.93 <1.79 <1.79

N-TMW-3 7/22/13Former Machine Shop, Textile Mill, &

Foundary <5.00 <1.00 <1.00 <2.00 <1.00 <1.00 <3.00 <8.62 <1.72 <1.72

S-TMW-1 7/18/13 Former Cannon Mill & Warehouses <5.00 <1.00 <1.00 <2.00 <1.00 <1.00 <3.00 <8.33 <1.67 <1.67

S-TMW-2 7/18/13 Former Weaving and Towel Bleaching Mills 19.9 <1.00 <1.00 <2.00 <1.00 <1.00 <3.00 31.9 <1.67 <1.67

S-TMW-3 7/18/13 Former Chemical Building <5.00 6.35 <1.00 <2.00 <1.00 59.6 <3.00 <8.33 <1.67 <1.67

S-TMW-4 7/19/13 Former Kerr Bleaching & Finishing Mill <5.00 <1.00 <1.00 <2.00 2.20 <1.00 8.32 <8.93 2.66 2.34

MW-9 7/18/13 Former Boiler Room <5.00 <1.00 1.22 7.38 <1.00 <1.00 <3.00 <8.33 <1.67 <1.67

6,000 1 0.4 70 600 25 500 3 300 200

4,600,000 13 20 NS 30 NS 95 NS NS NS

20,000,000 70 98 NS 150 NS 420 NS NS NS

Notes:Method follows parameter in parenthesesConcentrations reported in micrograms per liter (ug/L)Only those compounds detected are shownBold indicates concentration exceeds North Carolina 2L Groundwater Qualty StandardsVOCs = Volatile Organic Compounds; SVOCs = Semi-Volatile Organic CompoundsNS = No Screening Level

Analytical Method VOCs (EPA Method 8260) SVOCs (EPA Method 8270)

Xyl

enes

, Tot

al

NC 2L Groundwater Standards (ug/L)

Date Collected Potential Area of Concern Fl

uora

nthe

ne

Sample ID Bis

(2-e

thyl

hexy

l) ph

thal

ate

Ace

tone

DENR IHSB Residential Vapor Intrusion Screening Level (ug/L)

DENR IHSB Industrial Vapor Intrusion Screening Level (ug/L)

Pyr

ene

Appendix A

Soil Boring and Monitoring Well Logs & Well Construction Records

2.8

3.2

3.6

6.4

9.6

9

7.8

7.5

7.3

9.6

9.8

Gravel parking/loading areaMoist, slightly firm, tan brown silty SAND with gravel

Moist, firm, dark grey sandy SILT

Moist, stiff, brown orange clayey SILT

Moist, very stiff, brown orange silty CLAY

Refusal of PWR at 22' BGS

Bottom of borehole at 22.0 feet.

0.2

0.2

0.2

0.2

0.2

0.2

0.2

0.2

0.2

0.2

0.2

OpenBorehole

Bentonite

1" PVCRiser

Sand FilterPack

1" PVCSlottedScreen

DRAWN BY: RWM

BORING COMPLETED: 7/19/13DRILLING CONTRACTOR: Probe Technology Remarks:DRILL RIG/ METHOD: 6620DT / DPTSAMPLING METHOD: Macrocore Sampler

hand auger to 5' BGS

BORING STARTED: 7/19/13

LOGGED BY: RWMTOTAL DEPTH: 22 ft.TOP OF CASING ELEV:DEPTH TO WATER:

DE

PT

H(f

t)

DE

PT

H(f

t)

LIT

HO

LOG

Y

RE

CO

VE

RY

(%

)

SA

MP

.

MATERIAL DESCRIPTIONOV

A (

ppm

)B

KG

.

SA

MP

LE T

YP

EN

UM

BE

R BORING DIAGRAM

Sheet 1 of 1

BORING NUMBER N-TMW-1

PROJECT: Bleachery Court - Northern Property

JOB NUMBER: BLC-001

LOCATION: Concord, North Carolina

BO

RIN

G L

OG

- H

AR

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MA

N.G

DT

- 8

/13

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\BLC

-001

BLE

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.GP

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2923 South Tryon Street-Suite 100

Charlotte, North Carolina 28203

704-586-0007(p) 704-586-0373(f)

3334 Hillsborough Street

Raleigh, North Carolina 27607

919-847-4241(p) 919-847-4261(f)

0

5

10

15

20

0

5

10

15

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2.7

2.6

3.1

3.4

3.3

3.8

4.1

4.8

4.8

Organic TopsoilSlightly moist, slightly firm, tan brown silty SAND with concrete andbrick fragments

Moist, very stiff, orange brown silty CLAY

Saturated, very stiff, orange brown silty CLAY

Refusal on PWR at 17' BGS


0.4

0.4

0.4

0.4

0.4

0.4

0.4

0.4

0.4

OpenBorehole

Bentonite

1" PVCRiser

Sand FilterPack

1" PVCSlottedScreen

DRAWN BY: RWM





DE

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t)

DE

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Sheet 1 of 1



JOB NUMBER: BLC-001


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704-586-0007(p) 704-586-0373(f)



919-847-4241(p) 919-847-4261(f)

0

5

10

15

0

5

10

15

3.1

3.2

5.7

4.7

4.7

4

4.4

5.6

6.1

6.6

8.1

7.5

7.3

Gravel Covered AreaSlightly moist, stiff, red brown silty CLAY

Moist, medium stiff, orange brown silty CLAY with fine to mediumsand and mica

Moist, loose, yellow brown, silty SAND with rock fragments

Moist, loose, grey brown silty SAND with rock fragments

Very moist, loose, rose quartz and mica fragmentsSaturated, slightly firm, tan brown, sandy SILT with rock fragments


0.1

0

0.1

0

0

0

0

0

0

0

0

0

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OpenBorehole

1" PVCRiser

Bentonite

Sand FilterPack

1" PVCSlottedScreen

DRAWN BY: RWM





DE

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t)

DE

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t)

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ppm

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Sheet 1 of 1



JOB NUMBER: BLC-001


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704-586-0007(p) 704-586-0373(f)



919-847-4241(p) 919-847-4261(f)

0

5

10

15

20

25

0

5

10

15

20

25

Blind Boring

Refusal at 17.5' BGS


OpenBorehole

Bentonite

1" PVCRiser

Sand FilterPack

1" PVCSlottedScreen

DRAWN BY: RWM




LOGGED BY: RWMTOTAL DEPTH: 17.5 ft.TOP OF CASING ELEV:DEPTH TO WATER:

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704-586-0007(p) 704-586-0373(f)



919-847-4241(p) 919-847-4261(f)

0

5

10

15

0

5

10

15

5.7

5.7

4.7

4.1

5.3

4.9

6.6

Grassy areaMoist, slightly firm, dark brown sandy SILT with gravel

Very moist, slightly firm, tan brown, sandy SILT

Very moist, stiff, orange brown silty CLAY

Saturated, slightly firm, tan brown, sandy SILT


0.6

0.5

0.4

0.6

0.6

0.6

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BORING NUMBER SB-1


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15

5.7

3.1

3.7

2.8

3.1

3.4

3.3

Grassy areaMoist, slightly firm, dark brown sandy SILT with gravel

Very moist, slightly firm, tan brown, sandy SILT

Very moist, stiff, orange brown silty CLAY

Saturated, slightly firm, tan brown, sandy SILT


0.6

0.6

0.6

0.6

0.6

0.6

0.6

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BORING NUMBER SB-2


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919-847-4241(p) 919-847-4261(f)

0

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0

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10

15

1.3

1.1

3.5

3.8

4

6.1

5.9

Organic TopsoilMoist, slightly firm, tan brown silty SAND with charcoal, bricks, andcement fragments

Moist, firm, brown orange sandy SILT

Saturated, slightly firm, tan brown sandy SILT with rock fragments


0.4

0.4

0.4

0.3

0.6

0.4

0.3

OpenBorehole

1" PVCRiser

Bentonite

Sand FilterPack

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BORING NUMBER S-TMW-1

PROJECT: Bleachery Court - Southern Property

JOB NUMBER: BLC-001


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0

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20

0

5

10

15

20

2.3

2.6

3.1

3.3

7.1

Organic TopsoilSlightly moist, loose, tan brown silty SAND with charcoal, brick, andcement fragments

Saturated, slightly firm, brown orange sandy SILT

Refusal on PWR at 11.65' BGS


0.4

0.5

0.4

0.4

0.4

OpenBorehole

Bentonite

1" PVCRiser

Sand FilterPack

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LOGGED BY: RWMTOTAL DEPTH: 11.65 ft.TOP OF CASING ELEV:DEPTH TO WATER:

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919-847-4241(p) 919-847-4261(f)

0.0

2.5

5.0

7.5

10.0

12.5

0.0

2.5

5.0

7.5

10.0

12.5

7.8

4.8

4.6

5.1

5.8

5.2

13.3

14.7

71.3

78.1

Organic TopsoilSlightly moist, firm, brown red silty SAND with gravel, brick, andconcrete fragments

Moist, firm, dark grey sandy SILT

Saturated, firm, dark grey sandy SILT with gravel

Slight odor


1

1

0.7

0.8

1

1

1

1

1

1

OpenBorehole

1" PVCRiser

Bentonite

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919-847-4241(p) 919-847-4261(f)

0

5

10

15

20

0

5

10

15

20

5.6

4.7

4.3

5.1

6.4

7.8

Concrete

Moist, slightly firm, dark grey silty SAND

Saturated, slightly firm, dark grey silty SAND


0.3

0.4

0.4

0.4

0.4

0.4

Bentonite

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Sand FilterPack

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704-586-0007(p) 704-586-0373(f)



919-847-4241(p) 919-847-4261(f)

0.0

2.5

5.0

7.5

10.0

12.5

15.0

0.0

2.5

5.0

7.5

10.0

12.5

15.0

Appendix B

Laboratory Analytical Reports

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Nashville2960 Foster Creighton DriveNashville, TN 37204Tel: (615)726-0177

TestAmerica Job ID: 490-31469-1TestAmerica Sample Delivery Group: BLC-001Client Project/Site: Bleachery Properties

For:Hart & Hickman, PC2923 S Tryon StreetSuite 100Charlotte, North Carolina 28203

Attn: John Lopez

Authorized for release by:8/2/2013 9:36:26 AM

Ken Hayes, Project Manager [email protected]

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

Preliminary Data

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https://secure.testamericainc.com/TotalAccess/login.aspx

http://www.testamericainc.com/AskTheExpert/Expert_index.htm

http://www.testamericainc.com

mailto:[email protected]

Table of Contents

Client: Hart & Hickman, PCProject/Site: Bleachery Properties

TestAmerica Job ID: 490-31469-1SDG: BLC-001

Preliminary Data

Page 2 of 59TestAmerica Nashville

8/2/2013

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49

Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59

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Sample SummaryTestAmerica Job ID: 490-31469-1Client: Hart & Hickman, PC

SDG: BLC-001Project/Site: Bleachery Properties

Lab Sample ID Client Sample ID ReceivedCollectedMatrix

490-31469-1 S-TMW-1 Water 07/18/13 11:05 07/23/13 08:15

490-31469-2 S-TMW-2 Water 07/18/13 17:00 07/23/13 08:15

490-31469-3 S-TMW-3 Water 07/18/13 15:45 07/23/13 08:15

490-31469-4 S-TMW-4 Water 07/19/13 09:50 07/23/13 08:15

490-31469-5 N-TMW-2 Water 07/22/13 10:10 07/23/13 08:15

490-31469-6 N-TMW-3 Water 07/22/13 08:45 07/23/13 08:15

490-31469-8 SB-1 (9-11) Soil 07/19/13 14:45 07/23/13 08:15

490-31469-9 SB-2 (9-11) Soil 07/19/13 15:30 07/23/13 08:15

490-31469-10 MW-9 Water 07/18/13 12:35 07/23/13 08:15

TestAmerica Nashville

Preliminary Data

Page 3 of 59 8/2/2013

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Case NarrativeClient: Hart & Hickman, PC TestAmerica Job ID: 490-31469-1

Project/Site: Bleachery Properties SDG: BLC-001

Job ID: 490-31469-1

Laboratory: TestAmerica Nashville

Narrative

Job Narrative

490-31469-1

Comments

No additional comments.

Receipt

The samples were received on 7/23/2013 8:15 AM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperatures of the 2 coolers at receipt time were 1.6º C and 5.6º C.

GC/MS VOA

No analytical or quality issues were noted.

GC/MS Semi VOA

Method(s) 8270D: Surrogate recovery for the following sample(s) was outside control limits: S-TMW-3 (490-31469-3). Evidence of matrix

interference is present; therefore, re-extraction and/or re-analysis was not performed.

Method(s) 8270D: The laboratory control sample (LCS) and / or the laboratory control sample duplicate (LCSD) for the original batch

95266 and the re-extract batch 96460 recovered outside control limits (out-of-hold) for the following analyte: Isophorone. Samples are

QNS for further analysis; though results confirmed. In-hold run reported.

Method(s) 8270D: The laboratory control sample (LCS) and / or the laboratory control sample duplicate (LCSD) for the original batch

95266 and the re-extract batch 96460 recovered outside control limits for the following analyte: Isophorone. Samples are QNS for further

analysis; though results confirmed.

No other analytical or quality issues were noted.

GC VOA

Method(s) 8015C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with

batch 95713.


GC Semi VOA


Organic Prep

Method(s) 3510C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with

batches 95266 and 96460.


VOA Prep



Preliminary Data

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Definitions/GlossaryTestAmerica Job ID: 490-31469-1Client: Hart & Hickman, PC


Qualifiers

GC/MS Semi VOA

Qualifier Description

* LCS or LCSD exceeds the control limits

Qualifier

X Surrogate is outside control limits

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)


Preliminary Data

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Client Sample ResultsTestAmerica Job ID: 490-31469-1Client: Hart & Hickman, PC


Lab Sample ID: 490-31469-1Client Sample ID: S-TMW-1Matrix: WaterDate Collected: 07/18/13 11:05

Date Received: 07/23/13 08:15

Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL

Acetone ND 5.00 ug/L 07/25/13 02:11 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

1.00 ug/L 07/25/13 02:11 1Benzene ND

1.00 ug/L 07/25/13 02:11 1Bromobenzene ND

1.00 ug/L 07/25/13 02:11 1Bromochloromethane ND

1.00 ug/L 07/25/13 02:11 1Bromodichloromethane ND

1.00 ug/L 07/25/13 02:11 1Bromoform ND

1.00 ug/L 07/25/13 02:11 1Bromomethane ND

50.0 ug/L 07/25/13 02:11 12-Butanone (MEK) ND

1.00 ug/L 07/25/13 02:11 1Carbon disulfide ND

1.00 ug/L 07/25/13 02:11 1Carbon tetrachloride ND

1.00 ug/L 07/25/13 02:11 1Chlorobenzene ND

1.00 ug/L 07/25/13 02:11 1Chlorodibromomethane ND

1.00 ug/L 07/25/13 02:11 1Chloroethane ND

1.00 ug/L 07/25/13 02:11 1Chloroform ND

1.00 ug/L 07/25/13 02:11 1Chloromethane ND

1.00 ug/L 07/25/13 02:11 12-Chlorotoluene ND


1.00 ug/L 07/25/13 02:11 1cis-1,2-Dichloroethene ND

1.00 ug/L 07/25/13 02:11 1cis-1,3-Dichloropropene ND

10.0 ug/L 07/25/13 02:11 11,2-Dibromo-3-Chloropropane ND

1.00 ug/L 07/25/13 02:11 11,2-Dibromoethane (EDB) ND

1.00 ug/L 07/25/13 02:11 1Dibromomethane ND

1.00 ug/L 07/25/13 02:11 11,2-Dichlorobenzene ND



1.00 ug/L 07/25/13 02:11 1Dichlorodifluoromethane ND

1.00 ug/L 07/25/13 02:11 11,1-Dichloroethane ND


1.00 ug/L 07/25/13 02:11 11,1-Dichloroethene ND

1.00 ug/L 07/25/13 02:11 11,2-Dichloroethene, Total ND

1.00 ug/L 07/25/13 02:11 11,2-Dichloropropane ND



1.00 ug/L 07/25/13 02:11 11,1-Dichloropropene ND

2.00 ug/L 07/25/13 02:11 1Diisopropyl ether ND

1.00 ug/L 07/25/13 02:11 1Ethylbenzene ND

2.00 ug/L 07/25/13 02:11 1Hexachlorobutadiene ND

5.00 ug/L 07/25/13 02:11 12-Hexanone ND

1.00 ug/L 07/25/13 02:11 1Isopropylbenzene ND

5.00 ug/L 07/25/13 02:11 1Methylene Chloride ND

5.00 ug/L 07/25/13 02:11 14-Methyl-2-pentanone (MIBK) ND

1.00 ug/L 07/25/13 02:11 1Methyl tert-butyl ether ND

5.00 ug/L 07/25/13 02:11 1Naphthalene ND

1.00 ug/L 07/25/13 02:11 1n-Butylbenzene ND

1.00 ug/L 07/25/13 02:11 1N-Propylbenzene ND

1.00 ug/L 07/25/13 02:11 1p-Isopropyltoluene ND

1.00 ug/L 07/25/13 02:11 1sec-Butylbenzene ND

1.00 ug/L 07/25/13 02:11 1Styrene ND

1.00 ug/L 07/25/13 02:11 1tert-Butylbenzene ND


Preliminary Data

Page 6 of 59 8/2/2013

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Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)RL MDL

1,1,1,2-Tetrachloroethane ND 1.00 ug/L 07/25/13 02:11 1


1.00 ug/L 07/25/13 02:11 11,1,2,2-Tetrachloroethane ND

1.00 ug/L 07/25/13 02:11 1Tetrachloroethene ND

1.00 ug/L 07/25/13 02:11 1Toluene ND

1.00 ug/L 07/25/13 02:11 1trans-1,2-Dichloroethene ND

1.00 ug/L 07/25/13 02:11 1trans-1,3-Dichloropropene ND

1.00 ug/L 07/25/13 02:11 11,2,3-Trichlorobenzene ND


1.00 ug/L 07/25/13 02:11 11,1,1-Trichloroethane ND


1.00 ug/L 07/25/13 02:11 1Trichloroethene ND

1.00 ug/L 07/25/13 02:11 1Trichlorofluoromethane ND

1.00 ug/L 07/25/13 02:11 11,2,3-Trichloropropane ND

1.00 ug/L 07/25/13 02:11 11,2,4-Trimethylbenzene ND


1.00 ug/L 07/25/13 02:11 1Vinyl chloride ND

3.00 ug/L 07/25/13 02:11 1Xylenes, Total ND

4-Bromofluorobenzene (Surr) 112 70 - 130 07/25/13 02:11 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

Dibromofluoromethane (Surr) 100 07/25/13 02:11 170 - 130

1,2-Dichloroethane-d4 (Surr) 107 07/25/13 02:11 170 - 130

Toluene-d8 (Surr) 99 07/25/13 02:11 170 - 130

Method: 8270D - Semivolatile Organic Compounds (GC/MS)RL MDL

Acenaphthene ND 1.67 ug/L 07/25/13 10:37 07/26/13 19:09 1


1.67 ug/L 07/25/13 10:37 07/26/13 19:09 1Acenaphthylene ND

1.67 ug/L 07/25/13 10:37 07/26/13 19:09 1Anthracene ND

1.67 ug/L 07/25/13 10:37 07/26/13 19:09 1Benzo[a]anthracene ND

1.67 ug/L 07/25/13 10:37 07/26/13 19:09 1Benzo[a]pyrene ND

1.67 ug/L 07/25/13 10:37 07/26/13 19:09 1Benzo[b]fluoranthene ND

1.67 ug/L 07/25/13 10:37 07/26/13 19:09 1Benzo[g,h,i]perylene ND

1.67 ug/L 07/25/13 10:37 07/26/13 19:09 1Benzo[k]fluoranthene ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1Bis(2-chloroethoxy)methane ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1Bis(2-chloroethyl)ether ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1bis (2-chloroisopropyl) ether ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1Bis(2-ethylhexyl) phthalate ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 14-Bromophenyl phenyl ether ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1Butyl benzyl phthalate ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1Carbazole ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 14-Chloroaniline ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 14-Chloro-3-methylphenol ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 12-Chloronaphthalene ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 12-Chlorophenol ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 14-Chlorophenyl phenyl ether ND

1.67 ug/L 07/25/13 10:37 07/26/13 19:09 1Chrysene ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1Cresols ND

1.67 ug/L 07/25/13 10:37 07/26/13 19:09 1Dibenz(a,h)anthracene ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1Dibenzofuran ND


Preliminary Data

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Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL

1,2-Dichlorobenzene ND 8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1


8.33 ug/L 07/25/13 10:37 07/26/13 19:09 11,3-Dichlorobenzene ND


8.33 ug/L 07/25/13 10:37 07/26/13 19:09 13,3'-Dichlorobenzidine ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 12,4-Dichlorophenol ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1Diethyl phthalate ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 12,4-Dimethylphenol ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1Dimethyl phthalate ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1Di-n-butyl phthalate ND

20.8 ug/L 07/25/13 10:37 07/26/13 19:09 14,6-Dinitro-2-methylphenol ND

20.8 ug/L 07/25/13 10:37 07/26/13 19:09 12,4-Dinitrophenol ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 12,4-Dinitrotoluene ND


8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1Di-n-octyl phthalate ND

1.67 ug/L 07/25/13 10:37 07/26/13 19:09 1Fluoranthene ND

1.67 ug/L 07/25/13 10:37 07/26/13 19:09 1Fluorene ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1Hexachlorobenzene ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1Hexachlorobutadiene ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1Hexachlorocyclopentadiene ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1Hexachloroethane ND

1.67 ug/L 07/25/13 10:37 07/26/13 19:09 1Indeno[1,2,3-cd]pyrene ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1Isophorone ND *

1.67 ug/L 07/25/13 10:37 07/26/13 19:09 11-Methylnaphthalene ND


8.33 ug/L 07/25/13 10:37 07/26/13 19:09 12-Methylphenol ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 13 & 4 Methylphenol ND

1.67 ug/L 07/25/13 10:37 07/26/13 19:09 1Naphthalene ND

20.8 ug/L 07/25/13 10:37 07/26/13 19:09 12-Nitroaniline ND



8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1Nitrobenzene ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 12-Nitrophenol ND


8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1N-Nitrosodi-n-propylamine ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1n-Nitrosodiphenylamine(as

diphenylamine)

ND

20.8 ug/L 07/25/13 10:37 07/26/13 19:09 1Pentachlorophenol ND

1.67 ug/L 07/25/13 10:37 07/26/13 19:09 1Phenanthrene ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 1Phenol ND

1.67 ug/L 07/25/13 10:37 07/26/13 19:09 1Pyrene ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:09 11,2,4-Trichlorobenzene ND

20.8 ug/L 07/25/13 10:37 07/26/13 19:09 12,4,5-Trichlorophenol ND


2-Fluorobiphenyl (Surr) 58 29 - 120 07/25/13 10:37 07/26/13 19:09 1


2-Fluorophenol (Surr) 22 07/25/13 10:37 07/26/13 19:09 110 - 120

Nitrobenzene-d5 (Surr) 59 07/25/13 10:37 07/26/13 19:09 127 - 120

Phenol-d5 (Surr) 16 07/25/13 10:37 07/26/13 19:09 110 - 120

Terphenyl-d14 (Surr) 48 07/25/13 10:37 07/26/13 19:09 113 - 120


Preliminary Data

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Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)

2,4,6-Tribromophenol (Surr) 63 10 - 120 07/25/13 10:37 07/26/13 19:09 1



Preliminary Data

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Acetone 16.9 5.00 ug/L 07/25/13 02:42 1


1.00 ug/L 07/25/13 02:42 1Benzene ND




1.00 ug/L 07/25/13 02:42 1Bromoform ND
































5.00 ug/L 07/25/13 02:42 12-Hexanone ND










1.00 ug/L 07/25/13 02:42 1Styrene ND



Preliminary Data

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1.00 ug/L 07/25/13 02:42 1Toluene ND


















Toluene-d8 (Surr) 101 07/25/13 02:42 170 - 130














8.33 ug/L 07/25/13 10:37 07/26/13 19:32 1Bis(2-ethylhexyl) phthalate 31.9



8.33 ug/L 07/25/13 10:37 07/26/13 19:32 1Carbazole ND






1.67 ug/L 07/25/13 10:37 07/26/13 19:32 1Chrysene ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:32 1Cresols ND




Preliminary Data

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1.67 ug/L 07/25/13 10:37 07/26/13 19:32 1Fluorene ND




















diphenylamine)

ND



8.33 ug/L 07/25/13 10:37 07/26/13 19:32 1Phenol ND

1.67 ug/L 07/25/13 10:37 07/26/13 19:32 1Pyrene ND








Phenol-d5 (Surr) 20 07/25/13 10:37 07/26/13 19:32 110 - 120

Terphenyl-d14 (Surr) 48 07/25/13 10:37 07/26/13 19:32 113 - 120


Preliminary Data

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Preliminary Data

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Acetone ND 5.00 ug/L 07/25/13 03:12 1


1.00 ug/L 07/25/13 03:12 1Benzene 6.35




1.00 ug/L 07/25/13 03:12 1Bromoform ND
































5.00 ug/L 07/25/13 03:12 12-Hexanone ND








1.00 ug/L 07/25/13 03:12 1p-Isopropyltoluene 59.6


1.00 ug/L 07/25/13 03:12 1Styrene ND



Preliminary Data

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1.00 ug/L 07/25/13 03:12 1Toluene ND


















Toluene-d8 (Surr) 101 07/25/13 03:12 170 - 130

















8.33 ug/L 07/25/13 10:37 07/26/13 19:56 1Carbazole ND






1.67 ug/L 07/25/13 10:37 07/26/13 19:56 1Chrysene ND

8.33 ug/L 07/25/13 10:37 07/26/13 19:56 1Cresols ND




Preliminary Data

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1.67 ug/L 07/25/13 10:37 07/26/13 19:56 1Fluorene ND




















diphenylamine)

ND



8.33 ug/L 07/25/13 10:37 07/26/13 19:56 1Phenol ND

1.67 ug/L 07/25/13 10:37 07/26/13 19:56 1Pyrene ND








Phenol-d5 (Surr) 25 07/25/13 10:37 07/26/13 19:56 110 - 120

Terphenyl-d14 (Surr) 10 X 07/25/13 10:37 07/26/13 19:56 113 - 120


Preliminary Data

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Preliminary Data

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Acetone ND 5.00 ug/L 07/25/13 03:43 1


1.00 ug/L 07/25/13 03:43 1Benzene ND




1.00 ug/L 07/25/13 03:43 1Bromoform ND






























1.00 ug/L 07/25/13 03:43 1Ethylbenzene 2.20


5.00 ug/L 07/25/13 03:43 12-Hexanone ND










1.00 ug/L 07/25/13 03:43 1Styrene ND



Preliminary Data

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1.00 ug/L 07/25/13 03:43 1Toluene ND













3.00 ug/L 07/25/13 03:43 1Xylenes, Total 8.32





Toluene-d8 (Surr) 101 07/25/13 03:43 170 - 130

















8.93 ug/L 07/25/13 10:37 07/26/13 20:20 1Carbazole ND






1.79 ug/L 07/25/13 10:37 07/26/13 20:20 1Chrysene ND

8.93 ug/L 07/25/13 10:37 07/26/13 20:20 1Cresols ND




Preliminary Data

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1.79 ug/L 07/25/13 10:37 07/26/13 20:20 1Fluoranthene 2.66

1.79 ug/L 07/25/13 10:37 07/26/13 20:20 1Fluorene ND




















diphenylamine)

ND



8.93 ug/L 07/25/13 10:37 07/26/13 20:20 1Phenol ND

1.79 ug/L 07/25/13 10:37 07/26/13 20:20 1Pyrene 2.34








Phenol-d5 (Surr) 19 07/25/13 10:37 07/26/13 20:20 110 - 120

Terphenyl-d14 (Surr) 22 07/25/13 10:37 07/26/13 20:20 113 - 120


Preliminary Data

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Preliminary Data

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Lab Sample ID: 490-31469-5Client Sample ID: N-TMW-2Matrix: WaterDate Collected: 07/22/13 10:10



Acetone ND 5.00 ug/L 07/25/13 04:13 1


1.00 ug/L 07/25/13 04:13 1Benzene ND




1.00 ug/L 07/25/13 04:13 1Bromoform ND
































5.00 ug/L 07/25/13 04:13 12-Hexanone ND










1.00 ug/L 07/25/13 04:13 1Styrene ND



Preliminary Data

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1.00 ug/L 07/25/13 04:13 1Toluene ND


















Toluene-d8 (Surr) 101 07/25/13 04:13 170 - 130

















8.93 ug/L 07/25/13 10:37 07/26/13 20:43 1Carbazole ND






1.79 ug/L 07/25/13 10:37 07/26/13 20:43 1Chrysene ND

8.93 ug/L 07/25/13 10:37 07/26/13 20:43 1Cresols ND




Preliminary Data

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1.79 ug/L 07/25/13 10:37 07/26/13 20:43 1Fluorene ND




















diphenylamine)

ND



8.93 ug/L 07/25/13 10:37 07/26/13 20:43 1Phenol ND

1.79 ug/L 07/25/13 10:37 07/26/13 20:43 1Pyrene ND








Phenol-d5 (Surr) 23 07/25/13 10:37 07/26/13 20:43 110 - 120

Terphenyl-d14 (Surr) 64 07/25/13 10:37 07/26/13 20:43 113 - 120


Preliminary Data

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Preliminary Data

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Acetone ND 5.00 ug/L 07/25/13 04:43 1


1.00 ug/L 07/25/13 04:43 1Benzene ND




1.00 ug/L 07/25/13 04:43 1Bromoform ND
































5.00 ug/L 07/25/13 04:43 12-Hexanone ND










1.00 ug/L 07/25/13 04:43 1Styrene ND



Preliminary Data

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1.00 ug/L 07/25/13 04:43 1Toluene ND


















Toluene-d8 (Surr) 101 07/25/13 04:43 170 - 130

















8.62 ug/L 07/25/13 10:37 07/26/13 21:07 1Carbazole ND






1.72 ug/L 07/25/13 10:37 07/26/13 21:07 1Chrysene ND

8.62 ug/L 07/25/13 10:37 07/26/13 21:07 1Cresols ND




Preliminary Data

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1.72 ug/L 07/25/13 10:37 07/26/13 21:07 1Fluorene ND




















diphenylamine)

ND



8.62 ug/L 07/25/13 10:37 07/26/13 21:07 1Phenol ND

1.72 ug/L 07/25/13 10:37 07/26/13 21:07 1Pyrene ND








Phenol-d5 (Surr) 20 07/25/13 10:37 07/26/13 21:07 110 - 120

Terphenyl-d14 (Surr) 57 07/25/13 10:37 07/26/13 21:07 113 - 120


Preliminary Data

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Preliminary Data

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Lab Sample ID: 490-31469-8Client Sample ID: SB-1 (9-11)Matrix: SoilDate Collected: 07/19/13 14:45

Percent Solids: 79.5Date Received: 07/23/13 08:15

Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)RL MDL

GRO (C6-C10) 8.72 6.59 mg/Kg ☼ 07/25/13 12:20 07/27/13 09:53 1


a,a,a-Trifluorotoluene 94 50 - 150 07/25/13 12:20 07/27/13 09:53 1


Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)RL MDL

Diesel Range Organics [C10-C28] ND 6.25 mg/Kg ☼ 07/24/13 09:52 07/25/13 18:27 1


o-Terphenyl (Surr) 75 50 - 150 07/24/13 09:52 07/25/13 18:27 1


General ChemistryRL RL

Percent Solids 80 0.10 % 07/23/13 16:10 1



Preliminary Data

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Lab Sample ID: 490-31469-9Client Sample ID: SB-2 (9-11)Matrix: SoilDate Collected: 07/19/13 15:30


Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)RL MDL

GRO (C6-C10) 9.60 7.49 mg/Kg ☼ 07/25/13 12:20 07/27/13 10:34 1


a,a,a-Trifluorotoluene 99 50 - 150 07/25/13 12:20 07/27/13 10:34 1


Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)RL MDL

Diesel Range Organics [C10-C28] ND 6.62 mg/Kg ☼ 07/24/13 09:52 07/25/13 18:43 1


o-Terphenyl (Surr) 71 50 - 150 07/24/13 09:52 07/25/13 18:43 1


General ChemistryRL RL

Percent Solids 75 0.10 % 07/23/13 16:10 1



Preliminary Data

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Lab Sample ID: 490-31469-10Client Sample ID: MW-9Matrix: WaterDate Collected: 07/18/13 12:35



Acetone ND 5.00 ug/L 07/25/13 05:14 1


1.00 ug/L 07/25/13 05:14 1Benzene ND




1.00 ug/L 07/25/13 05:14 1Bromoform ND






















1.00 ug/L 07/25/13 05:14 11,2-Dichloroethane 1.22







2.00 ug/L 07/25/13 05:14 1Diisopropyl ether 7.38



5.00 ug/L 07/25/13 05:14 12-Hexanone ND










1.00 ug/L 07/25/13 05:14 1Styrene ND



Preliminary Data

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1.00 ug/L 07/25/13 05:14 1Toluene ND


















Toluene-d8 (Surr) 99 07/25/13 05:14 170 - 130

















8.33 ug/L 07/25/13 10:37 07/26/13 21:30 1Carbazole ND






1.67 ug/L 07/25/13 10:37 07/26/13 21:30 1Chrysene ND

8.33 ug/L 07/25/13 10:37 07/26/13 21:30 1Cresols ND




Preliminary Data

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1.67 ug/L 07/25/13 10:37 07/26/13 21:30 1Fluorene ND




















diphenylamine)

ND



8.33 ug/L 07/25/13 10:37 07/26/13 21:30 1Phenol ND

1.67 ug/L 07/25/13 10:37 07/26/13 21:30 1Pyrene ND








Phenol-d5 (Surr) 21 07/25/13 10:37 07/26/13 21:30 110 - 120

Terphenyl-d14 (Surr) 66 07/25/13 10:37 07/26/13 21:30 113 - 120


Preliminary Data

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Preliminary Data

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QC Sample ResultsTestAmerica Job ID: 490-31469-1Client: Hart & Hickman, PC


Method: 8260B - Volatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 490-94960/6

Matrix: Water Prep Type: Total/NA

Analysis Batch: 94960

RL MDL

Acetone ND 5.00 ug/L 07/24/13 22:07 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

ND 1.00 ug/L 07/24/13 22:07 1Benzene

ND 1.00 ug/L 07/24/13 22:07 1Bromobenzene

ND 1.00 ug/L 07/24/13 22:07 1Bromochloromethane

ND 1.00 ug/L 07/24/13 22:07 1Bromodichloromethane

ND 1.00 ug/L 07/24/13 22:07 1Bromoform

ND 1.00 ug/L 07/24/13 22:07 1Bromomethane

ND 50.0 ug/L 07/24/13 22:07 12-Butanone (MEK)

ND 1.00 ug/L 07/24/13 22:07 1Carbon disulfide

ND 1.00 ug/L 07/24/13 22:07 1Carbon tetrachloride

ND 1.00 ug/L 07/24/13 22:07 1Chlorobenzene

ND 1.00 ug/L 07/24/13 22:07 1Chlorodibromomethane

ND 1.00 ug/L 07/24/13 22:07 1Chloroethane

ND 1.00 ug/L 07/24/13 22:07 1Chloroform

ND 1.00 ug/L 07/24/13 22:07 1Chloromethane

ND 1.00 ug/L 07/24/13 22:07 12-Chlorotoluene

ND 1.00 ug/L 07/24/13 22:07 14-Chlorotoluene

ND 1.00 ug/L 07/24/13 22:07 1cis-1,2-Dichloroethene

ND 1.00 ug/L 07/24/13 22:07 1cis-1,3-Dichloropropene

ND 10.0 ug/L 07/24/13 22:07 11,2-Dibromo-3-Chloropropane

ND 1.00 ug/L 07/24/13 22:07 11,2-Dibromoethane (EDB)

ND 1.00 ug/L 07/24/13 22:07 1Dibromomethane

ND 1.00 ug/L 07/24/13 22:07 11,2-Dichlorobenzene



ND 1.00 ug/L 07/24/13 22:07 1Dichlorodifluoromethane

ND 1.00 ug/L 07/24/13 22:07 11,1-Dichloroethane

ND 1.00 ug/L 07/24/13 22:07 11,2-Dichloroethane

ND 1.00 ug/L 07/24/13 22:07 11,1-Dichloroethene

ND 1.00 ug/L 07/24/13 22:07 11,2-Dichloroethene, Total

ND 1.00 ug/L 07/24/13 22:07 11,2-Dichloropropane



ND 1.00 ug/L 07/24/13 22:07 11,1-Dichloropropene

ND 2.00 ug/L 07/24/13 22:07 1Diisopropyl ether

ND 1.00 ug/L 07/24/13 22:07 1Ethylbenzene

ND 2.00 ug/L 07/24/13 22:07 1Hexachlorobutadiene

ND 5.00 ug/L 07/24/13 22:07 12-Hexanone

ND 1.00 ug/L 07/24/13 22:07 1Isopropylbenzene

ND 5.00 ug/L 07/24/13 22:07 1Methylene Chloride

ND 5.00 ug/L 07/24/13 22:07 14-Methyl-2-pentanone (MIBK)

ND 1.00 ug/L 07/24/13 22:07 1Methyl tert-butyl ether

ND 5.00 ug/L 07/24/13 22:07 1Naphthalene

ND 1.00 ug/L 07/24/13 22:07 1n-Butylbenzene

ND 1.00 ug/L 07/24/13 22:07 1N-Propylbenzene

ND 1.00 ug/L 07/24/13 22:07 1p-Isopropyltoluene

ND 1.00 ug/L 07/24/13 22:07 1sec-Butylbenzene

ND 1.00 ug/L 07/24/13 22:07 1Styrene


Preliminary Data

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Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)




RL MDL

tert-Butylbenzene ND 1.00 ug/L 07/24/13 22:07 1

MB MB


ND 1.00 ug/L 07/24/13 22:07 11,1,1,2-Tetrachloroethane

ND 1.00 ug/L 07/24/13 22:07 11,1,2,2-Tetrachloroethane

ND 1.00 ug/L 07/24/13 22:07 1Tetrachloroethene

ND 1.00 ug/L 07/24/13 22:07 1Toluene

ND 1.00 ug/L 07/24/13 22:07 1trans-1,2-Dichloroethene

ND 1.00 ug/L 07/24/13 22:07 1trans-1,3-Dichloropropene

ND 1.00 ug/L 07/24/13 22:07 11,2,3-Trichlorobenzene

ND 1.00 ug/L 07/24/13 22:07 11,2,4-Trichlorobenzene

ND 1.00 ug/L 07/24/13 22:07 11,1,1-Trichloroethane

ND 1.00 ug/L 07/24/13 22:07 11,1,2-Trichloroethane

ND 1.00 ug/L 07/24/13 22:07 1Trichloroethene

ND 1.00 ug/L 07/24/13 22:07 1Trichlorofluoromethane

ND 1.00 ug/L 07/24/13 22:07 11,2,3-Trichloropropane

ND 1.00 ug/L 07/24/13 22:07 11,2,4-Trimethylbenzene

ND 1.00 ug/L 07/24/13 22:07 11,3,5-Trimethylbenzene

ND 1.00 ug/L 07/24/13 22:07 1Vinyl chloride

ND 3.00 ug/L 07/24/13 22:07 1Xylenes, Total


MB MB

Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery

98 07/24/13 22:07 1Dibromofluoromethane (Surr) 70 - 130

102 07/24/13 22:07 11,2-Dichloroethane-d4 (Surr) 70 - 130

101 07/24/13 22:07 1Toluene-d8 (Surr) 70 - 130

Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-94960/3



Acetone 250 247.8 ug/L 99 54 - 145

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Benzene 50.0 49.39 ug/L 99 80 - 121

Bromobenzene 50.0 49.50 ug/L 99 68 - 130

Bromochloromethane 50.0 49.46 ug/L 99 78 - 129

Bromodichloromethane 50.0 50.66 ug/L 101 75 - 129

Bromoform 50.0 53.60 ug/L 107 46 - 145

Bromomethane 50.0 48.61 ug/L 97 41 - 150

2-Butanone (MEK) 250 265.1 ug/L 106 62 - 133

Carbon disulfide 50.0 48.60 ug/L 97 77 - 126

Carbon tetrachloride 50.0 49.02 ug/L 98 64 - 147

Chlorobenzene 50.0 49.65 ug/L 99 80 - 120

Chlorodibromomethane 50.0 51.84 ug/L 104 69 - 133

Chloroethane 50.0 46.38 ug/L 93 72 - 120

Chloroform 50.0 49.59 ug/L 99 73 - 129

Chloromethane 50.0 42.55 ug/L 85 12 - 150

2-Chlorotoluene 50.0 49.32 ug/L 99 75 - 126

4-Chlorotoluene 50.0 48.87 ug/L 98 75 - 130

cis-1,2-Dichloroethene 50.0 49.67 ug/L 99 76 - 125


Preliminary Data

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cis-1,3-Dichloropropene 50.0 51.56 ug/L 103 74 - 140

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

1,2-Dibromo-3-Chloropropane 50.0 49.80 ug/L 100 54 - 125

1,2-Dibromoethane (EDB) 50.0 52.19 ug/L 104 80 - 129

Dibromomethane 50.0 53.03 ug/L 106 71 - 125

1,2-Dichlorobenzene 50.0 51.18 ug/L 102 80 - 121



Dichlorodifluoromethane 50.0 52.65 ug/L 105 37 - 127

1,1-Dichloroethane 50.0 51.50 ug/L 103 78 - 125

1,2-Dichloroethane 50.0 52.40 ug/L 105 77 - 121

1,1-Dichloroethene 50.0 47.67 ug/L 95 79 - 124

1,2-Dichloroethene, Total 100 100.4 ug/L 100 78 - 126

1,2-Dichloropropane 50.0 51.59 ug/L 103 75 - 120



1,1-Dichloropropene 50.0 50.10 ug/L 100 80 - 122

Diisopropyl ether 50.0 48.93 ug/L 98 61 - 142

Ethylbenzene 50.0 49.02 ug/L 98 80 - 130

Hexachlorobutadiene 50.0 47.81 ug/L 96 49 - 146

2-Hexanone 250 273.3 ug/L 109 60 - 142

Isopropylbenzene 50.0 49.41 ug/L 99 80 - 141

Methylene Chloride 50.0 49.86 ug/L 100 79 - 123

4-Methyl-2-pentanone (MIBK) 250 267.1 ug/L 107 60 - 137

Methyl tert-butyl ether 50.0 48.60 ug/L 97 72 - 133

Naphthalene 50.0 53.68 ug/L 107 62 - 138

n-Butylbenzene 50.0 50.11 ug/L 100 68 - 132

N-Propylbenzene 50.0 48.53 ug/L 97 75 - 129

p-Isopropyltoluene 50.0 49.76 ug/L 100 75 - 128

sec-Butylbenzene 50.0 48.92 ug/L 98 76 - 128

Styrene 50.0 49.42 ug/L 99 80 - 127

tert-Butylbenzene 50.0 48.02 ug/L 96 76 - 126

1,1,1,2-Tetrachloroethane 50.0 49.65 ug/L 99 74 - 135

1,1,2,2-Tetrachloroethane 50.0 51.97 ug/L 104 69 - 131

Tetrachloroethene 50.0 48.47 ug/L 97 80 - 126

Toluene 50.0 49.52 ug/L 99 80 - 126

trans-1,2-Dichloroethene 50.0 50.72 ug/L 101 79 - 126

trans-1,3-Dichloropropene 50.0 53.43 ug/L 107 63 - 134

1,2,3-Trichlorobenzene 50.0 51.55 ug/L 103 62 - 133


1,1,1-Trichloroethane 50.0 49.82 ug/L 100 78 - 135

1,1,2-Trichloroethane 50.0 52.25 ug/L 105 80 - 124

Trichloroethene 50.0 48.04 ug/L 96 80 - 123

Trichlorofluoromethane 50.0 47.51 ug/L 95 65 - 124

1,2,3-Trichloropropane 50.0 54.47 ug/L 109 70 - 131

1,2,4-Trimethylbenzene 50.0 49.26 ug/L 99 77 - 126

1,3,5-Trimethylbenzene 50.0 48.36 ug/L 97 77 - 127

Vinyl chloride 50.0 52.56 ug/L 105 68 - 120

Xylenes, Total 100 98.88 ug/L 99 80 - 132


Preliminary Data

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4-Bromofluorobenzene (Surr) 70 - 130

Surrogate

101

LCS LCS

Qualifier Limits%Recovery

99Dibromofluoromethane (Surr) 70 - 130

1031,2-Dichloroethane-d4 (Surr) 70 - 130

102Toluene-d8 (Surr) 70 - 130

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-94960/4



Acetone 250 229.3 ug/L 92 54 - 145 8 21

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Benzene 50.0 48.09 ug/L 96 80 - 121 3 17

Bromobenzene 50.0 47.48 ug/L 95 68 - 130 4 20

Bromochloromethane 50.0 47.80 ug/L 96 78 - 129 3 17

Bromodichloromethane 50.0 48.69 ug/L 97 75 - 129 4 18

Bromoform 50.0 52.86 ug/L 106 46 - 145 1 16

Bromomethane 50.0 47.72 ug/L 95 41 - 150 2 50

2-Butanone (MEK) 250 260.4 ug/L 104 62 - 133 2 19

Carbon disulfide 50.0 47.60 ug/L 95 77 - 126 2 21

Carbon tetrachloride 50.0 48.58 ug/L 97 64 - 147 1 19

Chlorobenzene 50.0 48.80 ug/L 98 80 - 120 2 14

Chlorodibromomethane 50.0 50.30 ug/L 101 69 - 133 3 15

Chloroethane 50.0 45.89 ug/L 92 72 - 120 1 20

Chloroform 50.0 47.61 ug/L 95 73 - 129 4 18

Chloromethane 50.0 41.37 ug/L 83 12 - 150 3 31

2-Chlorotoluene 50.0 48.43 ug/L 97 75 - 126 2 17

4-Chlorotoluene 50.0 47.63 ug/L 95 75 - 130 3 18

cis-1,2-Dichloroethene 50.0 49.03 ug/L 98 76 - 125 1 17

cis-1,3-Dichloropropene 50.0 49.99 ug/L 100 74 - 140 3 15

1,2-Dibromo-3-Chloropropane 50.0 46.37 ug/L 93 54 - 125 7 24

1,2-Dibromoethane (EDB) 50.0 50.33 ug/L 101 80 - 129 4 15

Dibromomethane 50.0 50.82 ug/L 102 71 - 125 4 16

1,2-Dichlorobenzene 50.0 49.89 ug/L 100 80 - 121 3 15



Dichlorodifluoromethane 50.0 51.24 ug/L 102 37 - 127 3 18

1,1-Dichloroethane 50.0 50.20 ug/L 100 78 - 125 3 17

1,2-Dichloroethane 50.0 49.24 ug/L 98 77 - 121 6 17

1,1-Dichloroethene 50.0 46.55 ug/L 93 79 - 124 2 17

1,2-Dichloroethene, Total 100 98.30 ug/L 98 78 - 126 2 33

1,2-Dichloropropane 50.0 50.14 ug/L 100 75 - 120 3 17



1,1-Dichloropropene 50.0 48.93 ug/L 98 80 - 122 2 17

Diisopropyl ether 50.0 47.22 ug/L 94 61 - 142 4 50

Ethylbenzene 50.0 47.85 ug/L 96 80 - 130 2 15

Hexachlorobutadiene 50.0 47.05 ug/L 94 49 - 146 2 23

2-Hexanone 250 258.4 ug/L 103 60 - 142 6 15


Preliminary Data

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Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-94960/4



Isopropylbenzene 50.0 49.16 ug/L 98 80 - 141 1 16

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Methylene Chloride 50.0 47.88 ug/L 96 79 - 123 4 17

4-Methyl-2-pentanone (MIBK) 250 251.6 ug/L 101 60 - 137 6 17

Methyl tert-butyl ether 50.0 46.42 ug/L 93 72 - 133 5 16

Naphthalene 50.0 50.93 ug/L 102 62 - 138 5 26

n-Butylbenzene 50.0 49.16 ug/L 98 68 - 132 2 18

N-Propylbenzene 50.0 48.08 ug/L 96 75 - 129 1 17

p-Isopropyltoluene 50.0 48.75 ug/L 98 75 - 128 2 16

sec-Butylbenzene 50.0 47.79 ug/L 96 76 - 128 2 16

Styrene 50.0 49.02 ug/L 98 80 - 127 1 24

tert-Butylbenzene 50.0 47.84 ug/L 96 76 - 126 0 16

1,1,1,2-Tetrachloroethane 50.0 48.41 ug/L 97 74 - 135 3 16

1,1,2,2-Tetrachloroethane 50.0 49.70 ug/L 99 69 - 131 4 20

Tetrachloroethene 50.0 41.94 ug/L 84 80 - 126 14 16

Toluene 50.0 48.50 ug/L 97 80 - 126 2 15

trans-1,2-Dichloroethene 50.0 49.27 ug/L 99 79 - 126 3 16

trans-1,3-Dichloropropene 50.0 50.60 ug/L 101 63 - 134 5 14

1,2,3-Trichlorobenzene 50.0 50.21 ug/L 100 62 - 133 3 25

1,2,4-Trichlorobenzene 50.0 47.95 ug/L 96 63 - 133 4 19

1,1,1-Trichloroethane 50.0 47.29 ug/L 95 78 - 135 5 17

1,1,2-Trichloroethane 50.0 49.33 ug/L 99 80 - 124 6 15

Trichloroethene 50.0 46.62 ug/L 93 80 - 123 3 17

Trichlorofluoromethane 50.0 48.95 ug/L 98 65 - 124 3 18

1,2,3-Trichloropropane 50.0 52.77 ug/L 106 70 - 131 3 19

1,2,4-Trimethylbenzene 50.0 48.30 ug/L 97 77 - 126 2 16

1,3,5-Trimethylbenzene 50.0 48.46 ug/L 97 77 - 127 0 17

Vinyl chloride 50.0 51.52 ug/L 103 68 - 120 2 17

Xylenes, Total 100 96.04 ug/L 96 80 - 132 3 15


Surrogate

100

LCSD LCSD





Client Sample ID: S-TMW-1Lab Sample ID: 490-31469-1 MS



Acetone ND 250 223.3 ug/L 89 45 - 141

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Benzene ND 50.0 47.21 ug/L 94 75 - 133

Bromobenzene ND 50.0 51.33 ug/L 103 60 - 138

Bromochloromethane ND 50.0 44.02 ug/L 88 67 - 139

Bromodichloromethane ND 50.0 49.93 ug/L 100 70 - 140

Bromoform ND 50.0 49.61 ug/L 99 42 - 147

Bromomethane ND 50.0 23.89 ug/L 48 16 - 163

2-Butanone (MEK) ND 250 245.3 ug/L 98 50 - 138


Preliminary Data

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Carbon disulfide ND 50.0 36.74 ug/L 73 48 - 152

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Carbon tetrachloride ND 50.0 50.16 ug/L 100 62 - 164

Chlorobenzene ND 50.0 49.30 ug/L 99 80 - 129

Chlorodibromomethane ND 50.0 50.20 ug/L 100 66 - 140

Chloroethane ND 50.0 43.00 ug/L 86 58 - 137

Chloroform ND 50.0 47.72 ug/L 95 66 - 138

Chloromethane ND 50.0 30.98 ug/L 62 10 - 169

2-Chlorotoluene ND 50.0 52.49 ug/L 105 67 - 138

4-Chlorotoluene ND 50.0 52.18 ug/L 104 69 - 138

cis-1,2-Dichloroethene ND 50.0 50.79 ug/L 102 68 - 138

cis-1,3-Dichloropropene ND 50.0 51.77 ug/L 104 71 - 141

1,2-Dibromo-3-Chloropropane ND 50.0 45.40 ug/L 91 52 - 126

1,2-Dibromoethane (EDB) ND 50.0 48.98 ug/L 98 75 - 137

Dibromomethane ND 50.0 48.35 ug/L 97 58 - 140

1,2-Dichlorobenzene ND 50.0 50.93 ug/L 102 79 - 128



Dichlorodifluoromethane ND 50.0 40.12 ug/L 80 40 - 127

1,1-Dichloroethane ND 50.0 47.94 ug/L 96 71 - 139

1,2-Dichloroethane ND 50.0 49.97 ug/L 100 64 - 136

1,1-Dichloroethene ND 50.0 43.01 ug/L 86 70 - 142

1,2-Dichloroethene, Total ND 100 97.38 ug/L 97 60 - 152

1,2-Dichloropropane ND 50.0 51.11 ug/L 102 67 - 131



1,1-Dichloropropene ND 50.0 48.05 ug/L 96 76 - 139

Diisopropyl ether ND 50.0 48.75 ug/L 97 10 - 200

Ethylbenzene ND 50.0 48.81 ug/L 98 79 - 139

Hexachlorobutadiene ND 50.0 55.21 ug/L 110 45 - 155

2-Hexanone ND 250 252.7 ug/L 101 50 - 150

Isopropylbenzene ND 50.0 51.91 ug/L 104 80 - 153

Methylene Chloride ND 50.0 43.58 ug/L 87 64 - 139

4-Methyl-2-pentanone (MIBK) ND 250 253.4 ug/L 101 50 - 147

Methyl tert-butyl ether ND 50.0 45.14 ug/L 90 66 - 141

Naphthalene ND 50.0 53.17 ug/L 106 55 - 140

n-Butylbenzene ND 50.0 54.61 ug/L 109 66 - 141

N-Propylbenzene ND 50.0 52.24 ug/L 104 69 - 142

p-Isopropyltoluene ND 50.0 52.15 ug/L 104 71 - 137

sec-Butylbenzene ND 50.0 52.72 ug/L 105 73 - 138

Styrene ND 50.0 48.57 ug/L 97 61 - 148

tert-Butylbenzene ND 50.0 52.27 ug/L 105 70 - 138

1,1,1,2-Tetrachloroethane ND 50.0 49.24 ug/L 98 73 - 141

1,1,2,2-Tetrachloroethane ND 50.0 51.83 ug/L 104 56 - 143

Tetrachloroethene ND 50.0 40.99 ug/L 82 72 - 145

Toluene ND 50.0 47.73 ug/L 95 75 - 136

trans-1,2-Dichloroethene ND 50.0 46.59 ug/L 93 66 - 143

trans-1,3-Dichloropropene ND 50.0 52.72 ug/L 105 59 - 135

1,2,3-Trichlorobenzene ND 50.0 52.14 ug/L 104 55 - 138


Preliminary Data

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1,2,4-Trichlorobenzene ND 50.0 51.38 ug/L 103 60 - 136

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

1,1,1-Trichloroethane ND 50.0 50.29 ug/L 101 76 - 149

1,1,2-Trichloroethane ND 50.0 50.11 ug/L 100 74 - 134

Trichloroethene ND 50.0 46.52 ug/L 93 73 - 144

Trichlorofluoromethane ND 50.0 47.50 ug/L 95 58 - 139

1,2,3-Trichloropropane ND 50.0 54.40 ug/L 109 53 - 144

1,2,4-Trimethylbenzene ND 50.0 50.97 ug/L 102 69 - 136

1,3,5-Trimethylbenzene ND 50.0 52.07 ug/L 104 69 - 139

Vinyl chloride ND 50.0 45.58 ug/L 91 56 - 129

Xylenes, Total ND 100 98.60 ug/L 99 74 - 141


Surrogate

106

MS MS





Client Sample ID: S-TMW-1Lab Sample ID: 490-31469-1 MSD



Acetone ND 250 230.6 ug/L 92 45 - 141 3 21

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Benzene ND 50.0 47.75 ug/L 95 75 - 133 1 17

Bromobenzene ND 50.0 51.26 ug/L 103 60 - 138 0 20

Bromochloromethane ND 50.0 44.53 ug/L 89 67 - 139 1 17

Bromodichloromethane ND 50.0 50.05 ug/L 100 70 - 140 0 18

Bromoform ND 50.0 49.68 ug/L 99 42 - 147 0 16

Bromomethane ND 50.0 31.31 ug/L 63 16 - 163 27 50

2-Butanone (MEK) ND 250 247.2 ug/L 99 50 - 138 1 19

Carbon disulfide ND 50.0 36.95 ug/L 74 48 - 152 1 21

Carbon tetrachloride ND 50.0 50.46 ug/L 101 62 - 164 1 19

Chlorobenzene ND 50.0 49.20 ug/L 98 80 - 129 0 14

Chlorodibromomethane ND 50.0 49.66 ug/L 99 66 - 140 1 15

Chloroethane ND 50.0 41.94 ug/L 84 58 - 137 2 20

Chloroform ND 50.0 48.49 ug/L 97 66 - 138 2 18

Chloromethane ND 50.0 32.20 ug/L 64 10 - 169 4 31

2-Chlorotoluene ND 50.0 51.54 ug/L 103 67 - 138 2 17

4-Chlorotoluene ND 50.0 51.19 ug/L 102 69 - 138 2 18

cis-1,2-Dichloroethene ND 50.0 51.55 ug/L 103 68 - 138 1 17

cis-1,3-Dichloropropene ND 50.0 51.89 ug/L 104 71 - 141 0 15

1,2-Dibromo-3-Chloropropane ND 50.0 47.90 ug/L 96 52 - 126 5 24

1,2-Dibromoethane (EDB) ND 50.0 48.75 ug/L 97 75 - 137 0 15

Dibromomethane ND 50.0 49.91 ug/L 100 58 - 140 3 16

1,2-Dichlorobenzene ND 50.0 50.28 ug/L 101 79 - 128 1 15



Dichlorodifluoromethane ND 50.0 40.64 ug/L 81 40 - 127 1 18


Preliminary Data

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Client Sample ID: S-TMW-1Lab Sample ID: 490-31469-1 MSD



1,1-Dichloroethane ND 50.0 48.65 ug/L 97 71 - 139 1 17

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

1,2-Dichloroethane ND 50.0 50.60 ug/L 101 64 - 136 1 17

1,1-Dichloroethene ND 50.0 44.10 ug/L 88 70 - 142 3 17

1,2-Dichloroethene, Total ND 100 99.18 ug/L 99 60 - 152 2 33

1,2-Dichloropropane ND 50.0 52.12 ug/L 104 67 - 131 2 17



1,1-Dichloropropene ND 50.0 49.39 ug/L 99 76 - 139 3 17

Diisopropyl ether ND 50.0 49.26 ug/L 99 10 - 200 1 50

Ethylbenzene ND 50.0 48.94 ug/L 98 79 - 139 0 15

Hexachlorobutadiene ND 50.0 54.91 ug/L 110 45 - 155 1 23

2-Hexanone ND 250 260.0 ug/L 104 50 - 150 3 15

Isopropylbenzene ND 50.0 50.29 ug/L 101 80 - 153 3 16

Methylene Chloride ND 50.0 45.87 ug/L 92 64 - 139 5 17

4-Methyl-2-pentanone (MIBK) ND 250 251.7 ug/L 101 50 - 147 1 17

Methyl tert-butyl ether ND 50.0 46.37 ug/L 93 66 - 141 3 16

Naphthalene ND 50.0 52.54 ug/L 105 55 - 140 1 26

n-Butylbenzene ND 50.0 54.10 ug/L 108 66 - 141 1 18

N-Propylbenzene ND 50.0 50.90 ug/L 102 69 - 142 3 17

p-Isopropyltoluene ND 50.0 51.61 ug/L 103 71 - 137 1 16

sec-Butylbenzene ND 50.0 52.41 ug/L 105 73 - 138 1 16

Styrene ND 50.0 48.63 ug/L 97 61 - 148 0 24

tert-Butylbenzene ND 50.0 51.31 ug/L 103 70 - 138 2 16

1,1,1,2-Tetrachloroethane ND 50.0 49.69 ug/L 99 73 - 141 1 16

1,1,2,2-Tetrachloroethane ND 50.0 50.36 ug/L 101 56 - 143 3 20

Tetrachloroethene ND 50.0 41.14 ug/L 82 72 - 145 0 16

Toluene ND 50.0 47.95 ug/L 96 75 - 136 0 15

trans-1,2-Dichloroethene ND 50.0 47.63 ug/L 95 66 - 143 2 16

trans-1,3-Dichloropropene ND 50.0 53.15 ug/L 106 59 - 135 1 14

1,2,3-Trichlorobenzene ND 50.0 52.22 ug/L 104 55 - 138 0 25

1,2,4-Trichlorobenzene ND 50.0 51.08 ug/L 102 60 - 136 1 19

1,1,1-Trichloroethane ND 50.0 51.05 ug/L 102 76 - 149 1 17

1,1,2-Trichloroethane ND 50.0 49.59 ug/L 99 74 - 134 1 15

Trichloroethene ND 50.0 46.42 ug/L 93 73 - 144 0 17

Trichlorofluoromethane ND 50.0 47.77 ug/L 96 58 - 139 1 18

1,2,3-Trichloropropane ND 50.0 53.88 ug/L 108 53 - 144 1 19

1,2,4-Trimethylbenzene ND 50.0 50.75 ug/L 101 69 - 136 0 16

1,3,5-Trimethylbenzene ND 50.0 51.54 ug/L 103 69 - 139 1 17

Vinyl chloride ND 50.0 47.13 ug/L 94 56 - 129 3 17

Xylenes, Total ND 100 99.40 ug/L 99 74 - 141 1 15


Surrogate

104

MSD MSD






Preliminary Data

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Method: 8270D - Semivolatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 490-95266/1-A


Analysis Batch: 95546 Prep Batch: 95266

RL MDL


MB MB


ND 2.00 ug/L 07/25/13 10:37 07/26/13 17:58 1Acenaphthylene

ND 2.00 ug/L 07/25/13 10:37 07/26/13 17:58 1Anthracene

ND 2.00 ug/L 07/25/13 10:37 07/26/13 17:58 1Benzo[a]anthracene

ND 2.00 ug/L 07/25/13 10:37 07/26/13 17:58 1Benzo[a]pyrene

ND 2.00 ug/L 07/25/13 10:37 07/26/13 17:58 1Benzo[b]fluoranthene

ND 2.00 ug/L 07/25/13 10:37 07/26/13 17:58 1Benzo[g,h,i]perylene

ND 2.00 ug/L 07/25/13 10:37 07/26/13 17:58 1Benzo[k]fluoranthene

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Bis(2-chloroethoxy)methane

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Bis(2-chloroethyl)ether

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1bis (2-chloroisopropyl) ether

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Bis(2-ethylhexyl) phthalate

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 14-Bromophenyl phenyl ether

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Butyl benzyl phthalate

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Carbazole

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 14-Chloroaniline

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 14-Chloro-3-methylphenol

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 12-Chloronaphthalene

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 12-Chlorophenol

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 14-Chlorophenyl phenyl ether

ND 2.00 ug/L 07/25/13 10:37 07/26/13 17:58 1Chrysene

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Cresols

ND 2.00 ug/L 07/25/13 10:37 07/26/13 17:58 1Dibenz(a,h)anthracene

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Dibenzofuran

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 11,2-Dichlorobenzene



ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 13,3'-Dichlorobenzidine

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 12,4-Dichlorophenol

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Diethyl phthalate

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 12,4-Dimethylphenol

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Dimethyl phthalate

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Di-n-butyl phthalate

ND 25.0 ug/L 07/25/13 10:37 07/26/13 17:58 14,6-Dinitro-2-methylphenol

ND 25.0 ug/L 07/25/13 10:37 07/26/13 17:58 12,4-Dinitrophenol

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 12,4-Dinitrotoluene

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 12,6-Dinitrotoluene

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Di-n-octyl phthalate

ND 2.00 ug/L 07/25/13 10:37 07/26/13 17:58 1Fluoranthene

ND 2.00 ug/L 07/25/13 10:37 07/26/13 17:58 1Fluorene

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Hexachlorobenzene

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Hexachlorobutadiene

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Hexachlorocyclopentadiene

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Hexachloroethane

ND 2.00 ug/L 07/25/13 10:37 07/26/13 17:58 1Indeno[1,2,3-cd]pyrene

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Isophorone

ND 2.00 ug/L 07/25/13 10:37 07/26/13 17:58 11-Methylnaphthalene

ND 2.00 ug/L 07/25/13 10:37 07/26/13 17:58 12-Methylnaphthalene


Preliminary Data

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RL MDL

2-Methylphenol ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1

MB MB


ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 13 & 4 Methylphenol

ND 2.00 ug/L 07/25/13 10:37 07/26/13 17:58 1Naphthalene

ND 25.0 ug/L 07/25/13 10:37 07/26/13 17:58 12-Nitroaniline



ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Nitrobenzene

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 12-Nitrophenol

ND 25.0 ug/L 07/25/13 10:37 07/26/13 17:58 14-Nitrophenol

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1N-Nitrosodi-n-propylamine

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1n-Nitrosodiphenylamine(as

diphenylamine)

ND 25.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Pentachlorophenol

ND 2.00 ug/L 07/25/13 10:37 07/26/13 17:58 1Phenanthrene

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 1Phenol

ND 2.00 ug/L 07/25/13 10:37 07/26/13 17:58 1Pyrene

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 11,2,4-Trichlorobenzene

ND 25.0 ug/L 07/25/13 10:37 07/26/13 17:58 12,4,5-Trichlorophenol

ND 10.0 ug/L 07/25/13 10:37 07/26/13 17:58 12,4,6-Trichlorophenol

2-Fluorobiphenyl (Surr) 64 29 - 120 07/26/13 17:58 1

MB MB

Surrogate

07/25/13 10:37

Dil FacPrepared AnalyzedQualifier Limits%Recovery

44 07/25/13 10:37 07/26/13 17:58 12-Fluorophenol (Surr) 10 - 120

66 07/25/13 10:37 07/26/13 17:58 1Nitrobenzene-d5 (Surr) 27 - 120

35 07/25/13 10:37 07/26/13 17:58 1Phenol-d5 (Surr) 10 - 120

85 07/25/13 10:37 07/26/13 17:58 1Terphenyl-d14 (Surr) 13 - 120

74 07/25/13 10:37 07/26/13 17:58 12,4,6-Tribromophenol (Surr) 10 - 120

Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-95266/2-A



Acenaphthene 40.0 34.19 ug/L 85 46 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Acenaphthylene 40.0 35.68 ug/L 89 48 - 120

Anthracene 40.0 35.96 ug/L 90 58 - 130

Benzo[a]anthracene 40.0 32.60 ug/L 81 57 - 120

Benzo[a]pyrene 40.0 31.01 ug/L 78 57 - 124

Benzo[b]fluoranthene 40.0 27.56 ug/L 69 51 - 125

Benzo[g,h,i]perylene 40.0 35.61 ug/L 89 51 - 123

Benzo[k]fluoranthene 40.0 28.32 ug/L 71 51 - 120

Bis(2-chloroethoxy)methane 40.0 31.29 ug/L 78 44 - 120

Bis(2-chloroethyl)ether 40.0 30.67 ug/L 77 47 - 120

bis (2-chloroisopropyl) ether 40.0 30.56 ug/L 76 44 - 120

Bis(2-ethylhexyl) phthalate 40.0 41.16 ug/L 103 47 - 138

4-Bromophenyl phenyl ether 40.0 38.56 ug/L 96 47 - 127

Butyl benzyl phthalate 40.0 35.53 ug/L 89 51 - 146

Carbazole 40.0 35.63 ug/L 89 54 - 123


Preliminary Data

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4-Chloroaniline 40.0 19.76 ug/L 49 44 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

4-Chloro-3-methylphenol 40.0 27.17 ug/L 68 44 - 120

2-Chloronaphthalene 40.0 33.82 ug/L 85 39 - 120

2-Chlorophenol 40.0 27.52 ug/L 69 40 - 120

4-Chlorophenyl phenyl ether 40.0 34.52 ug/L 86 50 - 120

Chrysene 40.0 34.08 ug/L 85 55 - 120

Cresols 80.0 50.28 ug/L 63 33 - 120

Dibenz(a,h)anthracene 40.0 37.82 ug/L 95 50 - 125

Dibenzofuran 40.0 34.37 ug/L 86 50 - 120




3,3'-Dichlorobenzidine 40.0 39.12 ug/L 98 46 - 129

2,4-Dichlorophenol 40.0 28.01 ug/L 70 38 - 120

Diethyl phthalate 40.0 34.12 ug/L 85 54 - 128

2,4-Dimethylphenol 40.0 28.69 ug/L 72 21 - 126

Dimethyl phthalate 40.0 33.44 ug/L 84 53 - 127

Di-n-butyl phthalate 40.0 32.09 ug/L 80 54 - 140

4,6-Dinitro-2-methylphenol 40.0 36.46 ug/L 91 19 - 150

2,4-Dinitrophenol 40.0 29.11 ug/L 73 20 - 150

2,4-Dinitrotoluene 40.0 34.01 ug/L 85 46 - 132

2,6-Dinitrotoluene 40.0 37.07 ug/L 93 54 - 128

Di-n-octyl phthalate 40.0 28.33 ug/L 71 50 - 142

Fluoranthene 40.0 31.91 ug/L 80 56 - 120

Fluorene 40.0 34.91 ug/L 87 52 - 120

Hexachlorobenzene 40.0 37.24 ug/L 93 48 - 131

Hexachlorobutadiene 40.0 29.20 ug/L 73 28 - 120

Hexachlorocyclopentadiene 40.0 21.46 ug/L 54 17 - 120

Hexachloroethane 40.0 28.19 ug/L 70 30 - 120

Indeno[1,2,3-cd]pyrene 40.0 37.09 ug/L 93 54 - 125

Isophorone 40.0 18.25 * ug/L 46 47 - 120

1-Methylnaphthalene 40.0 29.48 ug/L 74 36 - 120

2-Methylnaphthalene 40.0 28.67 ug/L 72 31 - 120

2-Methylphenol 40.0 26.13 ug/L 65 38 - 120

3 & 4 Methylphenol 40.0 24.15 ug/L 60 33 - 120

Naphthalene 40.0 32.61 ug/L 82 37 - 120

2-Nitroaniline 40.0 33.40 ug/L 84 46 - 131

3-Nitroaniline 40.0 ND ug/L 61 54 - 121

4-Nitroaniline 40.0 33.78 ug/L 84 55 - 123

Nitrobenzene 40.0 29.75 ug/L 74 36 - 120

2-Nitrophenol 40.0 28.27 ug/L 71 32 - 120

4-Nitrophenol 40.0 ND ug/L 36 10 - 120

N-Nitrosodi-n-propylamine 40.0 35.42 ug/L 89 51 - 120

n-Nitrosodiphenylamine(as

diphenylamine)

40.0 44.47 ug/L 111 58 - 149

Pentachlorophenol 40.0 39.14 ug/L 98 21 - 150

Phenanthrene 40.0 36.94 ug/L 92 56 - 120

Phenol 40.0 14.16 ug/L 35 14 - 120


Preliminary Data

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Pyrene 40.0 36.37 ug/L 91 53 - 129

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


2,4,5-Trichlorophenol 40.0 34.54 ug/L 86 40 - 129

2,4,6-Trichlorophenol 40.0 36.05 ug/L 90 39 - 135

2-Fluorobiphenyl (Surr) 29 - 120

Surrogate

66

LCS LCS


372-Fluorophenol (Surr) 10 - 120

59Nitrobenzene-d5 (Surr) 27 - 120

28Phenol-d5 (Surr) 10 - 120

65Terphenyl-d14 (Surr) 13 - 120

762,4,6-Tribromophenol (Surr) 10 - 120

Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics)


Matrix: Solid Prep Type: Total/NA


RL MDL

GRO (C6-C10) ND 5.00 mg/Kg 07/27/13 07:07 1

MB MB


a,a,a-Trifluorotoluene 98 50 - 150 07/27/13 07:07 1

MB MB

Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery




GRO (C6-C10) 10.0 11.07 mg/Kg 111 70 - 130

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

a,a,a-Trifluorotoluene 50 - 150

Surrogate

118

LCS LCS


Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)




RL MDL

Diesel Range Organics [C10-C28] ND 5.00 mg/Kg 07/24/13 09:52 07/25/13 12:36 1

MB MB


o-Terphenyl (Surr) 91 50 - 150 07/25/13 12:36 1

MB MB

Surrogate

07/24/13 09:52

Dil FacPrepared AnalyzedQualifier Limits%Recovery


Preliminary Data

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Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)

(Continued)




Diesel Range Organics

[C10-C28]

40.0 48.43 mg/Kg 121 54 - 130

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

o-Terphenyl (Surr) 50 - 150

Surrogate

111

LCS LCS


Client Sample ID: Matrix SpikeLab Sample ID: 490-31440-C-1-D MS




[C10-C28]

5.63 44.2 36.55 mg/Kg 70 10 - 142☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Surrogate

64

MS MS


Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-31440-C-1-E MSD




[C10-C28]

5.63 43.9 36.16 mg/Kg 70 10 - 142 1 47☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


Surrogate

61

MSD MSD


Method: Moisture - Percent Moisture

Client Sample ID: DuplicateLab Sample ID: 490-31468-E-1 DU



Percent Solids 93 94 % 1 20

Analyte

DU DU

DUnitResult Qualifier

Sample

Result

Sample

Qualifier LimitRPD

RPD


Preliminary Data

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QC Association SummaryTestAmerica Job ID: 490-31469-1Client: Hart & Hickman, PC


GC/MS VOA


Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 8260B490-31469-1 S-TMW-1 Total/NA

Water 8260B490-31469-1 MS S-TMW-1 Total/NA

Water 8260B490-31469-1 MSD S-TMW-1 Total/NA




Water 8260B490-31469-5 N-TMW-2 Total/NA

Water 8260B490-31469-6 N-TMW-3 Total/NA

Water 8260B490-31469-10 MW-9 Total/NA

Water 8260BLCS 490-94960/3 Lab Control Sample Total/NA

Water 8260BLCSD 490-94960/4 Lab Control Sample Dup Total/NA

Water 8260BMB 490-94960/6 Method Blank Total/NA

GC/MS Semi VOA

Prep Batch: 95266


Water 3510C490-31469-1 S-TMW-1 Total/NA




Water 3510C490-31469-5 N-TMW-2 Total/NA

Water 3510C490-31469-6 N-TMW-3 Total/NA

Water 3510C490-31469-10 MW-9 Total/NA

Water 3510CLCS 490-95266/2-A Lab Control Sample Total/NA

Water 3510CMB 490-95266/1-A Method Blank Total/NA



Water 8270D 95266490-31469-1 S-TMW-1 Total/NA




Water 8270D 95266490-31469-5 N-TMW-2 Total/NA

Water 8270D 95266490-31469-6 N-TMW-3 Total/NA

Water 8270D 95266490-31469-10 MW-9 Total/NA

Water 8270D 95266LCS 490-95266/2-A Lab Control Sample Total/NA

Water 8270D 95266MB 490-95266/1-A Method Blank Total/NA

GC VOA

Prep Batch: 95316


Soil 5035490-31469-8 SB-1 (9-11) Total/NA

Soil 5035490-31469-9 SB-2 (9-11) Total/NA



Soil 8015C 95316490-31469-8 SB-1 (9-11) Total/NA

Soil 8015C 95316490-31469-9 SB-2 (9-11) Total/NA


Preliminary Data

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QC Association SummaryTestAmerica Job ID: 490-31469-1Client: Hart & Hickman, PC


GC VOA (Continued)

Analysis Batch: 95713 (Continued)


Solid 8015CLCS 490-95713/38 Lab Control Sample Total/NA

Solid 8015CMB 490-95713/48 Method Blank Total/NA

GC Semi VOA

Prep Batch: 94933


Solid 3550C490-31440-C-1-D MS Matrix Spike Total/NA

Solid 3550C490-31440-C-1-E MSD Matrix Spike Duplicate Total/NA

Soil 3550C490-31469-8 SB-1 (9-11) Total/NA

Soil 3550C490-31469-9 SB-2 (9-11) Total/NA

Solid 3550CLCS 490-94933/2-A Lab Control Sample Total/NA

Solid 3550CMB 490-94933/1-A Method Blank Total/NA



Solid 8015C 94933490-31440-C-1-D MS Matrix Spike Total/NA

Solid 8015C 94933490-31440-C-1-E MSD Matrix Spike Duplicate Total/NA

Solid 8015C 94933LCS 490-94933/2-A Lab Control Sample Total/NA

Solid 8015C 94933MB 490-94933/1-A Method Blank Total/NA



Soil 8015C 94933490-31469-8 SB-1 (9-11) Total/NA

Soil 8015C 94933490-31469-9 SB-2 (9-11) Total/NA

General Chemistry



Solid Moisture490-31468-E-1 DU Duplicate Total/NA

Soil Moisture490-31469-8 SB-1 (9-11) Total/NA

Soil Moisture490-31469-9 SB-2 (9-11) Total/NA


Preliminary Data

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Lab ChronicleClient: Hart & Hickman, PC TestAmerica Job ID: 490-31469-1


Client Sample ID: S-TMW-1 Lab Sample ID: 490-31469-1Matrix: WaterDate Collected: 07/18/13 11:05


Analysis 8260B 07/25/13 02:11 AJF1 94960 TAL NSH

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Prep 3510C 95266 07/25/13 10:37 RCH TAL NSHTotal/NA

Analysis 8270D 1 95546 07/26/13 19:09 JLS TAL NSHTotal/NA




Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA






Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA






Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA



Client Sample ID: N-TMW-2 Lab Sample ID: 490-31469-5Matrix: WaterDate Collected: 07/22/13 10:10



Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




Preliminary Data

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Lab ChronicleClient: Hart & Hickman, PC TestAmerica Job ID: 490-31469-1


Client Sample ID: N-TMW-3 Lab Sample ID: 490-31469-6Matrix: WaterDate Collected: 07/22/13 08:45



Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA



Client Sample ID: SB-1 (9-11) Lab Sample ID: 490-31469-8Matrix: SoilDate Collected: 07/19/13 14:45


Prep 5035 07/25/13 12:20 JLP95316 TAL NSH

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8015C 1 95713 07/27/13 09:53 AMC TAL NSHTotal/NA

Prep 3550C 94933 07/24/13 09:52 JLP TAL NSHTotal/NA

Analysis 8015C 1 95402 07/25/13 18:27 JML TAL NSHTotal/NA

Analysis Moisture 1 94830 07/23/13 16:10 CEC TAL NSHTotal/NA

Client Sample ID: SB-2 (9-11) Lab Sample ID: 490-31469-9Matrix: SoilDate Collected: 07/19/13 15:30


Prep 5035 07/25/13 12:20 JLP95316 TAL NSH

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8015C 1 95713 07/27/13 10:34 AMC TAL NSHTotal/NA

Prep 3550C 94933 07/24/13 09:52 JLP TAL NSHTotal/NA

Analysis 8015C 1 95402 07/25/13 18:43 JML TAL NSHTotal/NA

Analysis Moisture 1 94830 07/23/13 16:10 CEC TAL NSHTotal/NA

Client Sample ID: MW-9 Lab Sample ID: 490-31469-10Matrix: WaterDate Collected: 07/18/13 12:35



Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA



Laboratory References:

TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177


Preliminary Data

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Method SummaryTestAmerica Job ID: 490-31469-1Client: Hart & Hickman, PC


Method Method Description LaboratoryProtocol

SW8468260B Volatile Organic Compounds (GC/MS) TAL NSH

SW8468270D Semivolatile Organic Compounds (GC/MS) TAL NSH

SW8468015C Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) TAL NSH

SW8468015C Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) TAL NSH

EPAMoisture Percent Moisture TAL NSH

Protocol References:

EPA = US Environmental Protection Agency

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177


Preliminary Data

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Certification SummaryClient: Hart & Hickman, PC TestAmerica Job ID: 490-31469-1


Laboratory: TestAmerica NashvilleAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date

393ACIL 10-30-13

A2LA ISO/IEC 17025 0453.07 12-31-13

Alaska (UST) State Program 10 UST-087 07-24-14

Arizona State Program 9 AZ0473 05-05-14

Arkansas DEQ State Program 6 88-0737 04-25-14

California NELAP 9 1168CA 10-31-13

Connecticut State Program 1 PH-0220 12-31-13

Florida NELAP 4 E87358 06-30-14

Illinois NELAP 5 200010 12-09-13

Iowa State Program 7 131 05-01-14

Kansas NELAP 7 E-10229 10-31-13

Kentucky (UST) State Program 4 19 06-30-14

Louisiana NELAP 6 30613 06-30-14

Maryland State Program 3 316 03-31-14

Massachusetts State Program 1 M-TN032 06-30-14

Minnesota NELAP 5 047-999-345 12-31-13

Mississippi State Program 4 N/A 06-30-14

Montana (UST) State Program 8 NA 01-01-15

Nevada State Program 9 TN00032 07-31-13 *

New Hampshire NELAP 1 2963 10-10-13

New Jersey NELAP 2 TN965 06-30-14

New York NELAP 2 11342 04-01-14

North Carolina DENR State Program 4 387 12-31-13

North Dakota State Program 8 R-146 06-30-14

Ohio VAP State Program 5 CL0033 01-19-14

Oklahoma State Program 6 9412 08-31-13

Oregon NELAP 10 TN200001 04-29-14

Pennsylvania NELAP 3 68-00585 06-30-14

Rhode Island State Program 1 LAO00268 12-30-13

South Carolina State Program 4 84009 (001) 02-28-14

South Carolina State Program 4 84009 (002) 02-23-14

Tennessee State Program 4 2008 02-23-14

Texas NELAP 6 T104704077-09-TX 08-31-13

USDA Federal S-48469 11-02-13

Virginia NELAP 3 460152 06-14-14

Washington State Program 10 C789 07-19-14

West Virginia DEP State Program 3 219 02-28-14

Wisconsin State Program 5 998020430 08-31-13

Wyoming (UST) A2LA 8 453.07 12-31-13


* Expired certification is currently pending renewal and is considered valid.

Preliminary Data

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Preliminary Data

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Preliminary Data

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Preliminary Data

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Preliminary Data

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Login Sample Receipt Checklist

Client: Hart & Hickman, PC Job Number: 490-31469-1

SDG Number: BLC-001

Login Number: 31469

Question Answer Comment

Creator: McBride, Mike

List Source: TestAmerica Nashville

List Number: 1

TrueRadioactivity wasn't checked or is </= background as measured by a

survey meter.

TrueThe cooler's custody seal, if present, is intact.

N/ASample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or

tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time.

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

N/ASample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested

MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


Preliminary Data

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Appendix C

Low-Flow Sampling Records and Calibration Record

phase ii esa report draft rwm - tranzon

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