pre-feasibility report for proposed api...

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Pre-Feasibility Report of Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and speciallity Agro chemicals (Newasa) PRE-FEASIBILITY REPORT FOR PROPOSED API INTERMEDIATE MANUFACTURING OF GALAXY LABORATORIES PRIVATE LIMITED At Plot No. B-10, MIDC Newasa Industrial Area, at Post Tukai – Shingve, Auranagabad – Pune Highway, Near Godegaon, Tal. Newasa, Ahmednagar – 414607 (Maharashtra)

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Page 1: PRE-FEASIBILITY REPORT FOR PROPOSED API …environmentclearance.nic.in/writereaddata/FormB/TOR/PFR/23_Oct... · Galaxy Laboratories is a venture capital company promoted with equity

Pre-Feasibility Report of

Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

PRE-FEASIBILITY REPORT

FOR

PROPOSED API INTERMEDIATE

MANUFACTURING

OF

GALAXY LABORATORIES

PRIVATE LIMITED

At

Plot No. B-10, MIDC Newasa Industrial Area, at Post Tukai – Shingve, Auranagabad –

Pune Highway, Near Godegaon, Tal. Newasa, Ahmednagar – 414607 (Maharashtra)

Page 2: PRE-FEASIBILITY REPORT FOR PROPOSED API …environmentclearance.nic.in/writereaddata/FormB/TOR/PFR/23_Oct... · Galaxy Laboratories is a venture capital company promoted with equity

Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

CHAPTER – 1

EXECUTIVE SUMMARY

Galaxy Laboratories is a venture capital company promoted with equity participation from

Industrial Development Bank of India (IDBI) in the year 1995.

The company is a manufacturer of Intermediates for API’s (Active Pharmaceutical

Ingredients) and specialty Agro Chemicals.

Galaxy is one of the leading manufacturers of the product Furfurylamine in the world.

Furfurylamine is used in an API known as Furosemide which is primarily used for the

treatment of hypertension, congestive heart failure and edema.

Besides the domestic API’s intermediates and Agro Chemicals market, it has a foreign

customer base in Belgium, Germany, Israel, Japan, Italy and Korea. It has created a name

for itself in the area of Catalytic Hydrogenation and Fractional Distillation.

One of existing manufacturing facility is located at Railway Station MIDC Aurangabad,

Maharashtra. The land area is 8158 sq. meters and the company has put up excellent

manufacturing facilities as per international standards and complies with the prevailing GMP

norms of MNC’s. The turnover of the financial year 2013-14 was 29 Crores. The

manufacturing Facilities are Multipurpose and versatile to handle advance technologies for

manufacturing API Intermediates and specialized Agro Chemicals.

NAME OF THE PROMOTERS AND THEIR TRACK RECORD :

Sr.

No

.

Name Age

(yrs)

Total

Experience

Educational

Qualifications

Experience in Brief

1. Shrikant

Deshmukh

60 36 years B Tech.

(Pharmaceuticals

& Fine

Chemicals),

UDCT, Mumbai.

Worked with multinational

companies’ viz. Hoechst

(Sanofi - Aventis), Roche

Products Ltd., and

Boehringer-Knoll at

various levels.

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

Prior to Galaxy

Laboratories, co-

promoter of Ariane

Orgachem Pvt. Ltd. (Now

AMRI India Ltd.) engaged

in manufacturing of APIs.

2. Nagesh

Walimbe

60 36 years Chemical

Engineer from

Indian Institute of

Technology ,

Mumbai (I.I.T.)

He has worked with

Multinational Companies

namely Hoechst India

Limited, Gharda

Chemicals Ltd, Lupin

Laboratories & Standard

Organics Ltd in varied

Capacities at Design &

Management levels in

India and abroad. He is

running his own

consultancy firm namely

Zen Chemiconsultech

Pvt. Ltd., Hyderabad.

Galalxy is proposing new unit at Newasa MIDC with latest technology as per the GMP for

producing the critical intermediates for API, Agro Products and Specialty Chemicals.

The products are Hydrogen Gas, Furfuraldehyde, Furfuryl Alcohol, Mono IsoPropyl Amine,

Di Methyl Amine Hydrochloride, Furfurylamine, 6-Chloro-5(2,3 Dichlorophenoxy) -2-

Methylthio 1H , Benzimidazole (Triclabendazole Crude), 5-Chloro-4-Amino-2,1,3-

Benzothiadiazole (TNZ), 2-Furoic Acid, Cyclohexenyl Ethyl Amine (CHEA).

The company is also putting up Agro Research Centre herewith well-equipped and designed

Research & Development Laboratory for API Intermediates.

The proposed project comes under 5(f) of the schedule in EIA notification 2006. Thus

environmental clearance is required for the said project. Particulars and details about the

proposed project are given in following table

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

Particulars Details

Name of the project

Proposed API Intermediate

manufacturing unit at Plot No. B10,

MIDC Newasa industrial area At Post.

Tukai - Shingve, Taluka. Newasa Dist.

Ahmednagar.

Site B-10, Tukai-Shingve,Tal. Newasa, Dist.

Ahmednagar

Area 48400 sqm

Water requirement 84 m3/day

Power requirement 320 KVA

Fuel requirement 750 TPA

DG Set 320 KVA

Man Power 350

Project cost 1430 Lacs

Page 5: PRE-FEASIBILITY REPORT FOR PROPOSED API …environmentclearance.nic.in/writereaddata/FormB/TOR/PFR/23_Oct... · Galaxy Laboratories is a venture capital company promoted with equity

Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

CHAPTER – 2

INTRODUCTION OF THE PROJECT

2.1 IDENTIFICATION OF PROJECT AND PROJECT PROPONENT

Galaxy Laboratories Private Limited an API Intermediate manufacturing unit is proposed at

Newasa MIDC on Pune- Aurangabad highway in Maharashtra. The company is a

manufacturer of Intermediates for API’s (Active Pharmaceutical Ingredients) and Specialty

Agro Chemicals.

PROPOSED PRODUCTS

The proposed Unit at Newasa is comprised of manufacturing 10 different products. The

details of products and the reasons for manufacturing are given in Table No 2.1.

Table No2.1

Sr.

No

Product Name CAS No. Capacity (per

annum)

Reason for identification/ End

use of Product

1 Hydrogen Gas 1333-74-0 18.72 Lacs

NM3

(250 NM3/Hr)

• Key raw material for

pharmaceutical, chemical,

agricultural, food, and allied

industries.

• Used increasingly for its property

of making the chemical

processes pollution free.

2 Furfuraldehyde 98-01-1 600 Tons • Key raw material in

manufacturing of Furfurylamine

and Furfuryl alcohol and 2-Furoic

Acid.

• The main outlet of furfural is that

it is a unique chemical feed stock

for other furan derivatives.

• Furfural is effective as a solvent

in phenolic resins and a wetting

agent. In the manufacture of

abrasive wheels, brake linings,

and refractory products for steel

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

industry.

• Refining of lubrication oils and

decolorizing agent (Oil Industry).

3 Furfuryl Alcohol 98-00-0 360 Tons • Chemical building block for drug

synthesis.

• Furfuryl alcohol plays a vital role

in the production of foundry sand

binders.

• It is extensively used to produce

cores and molds for metal

casting.

• Wood modification.

• Corrosion resistant for cement,

mortars and fiber-reinforced

plastics.

4 Mono Iso

Propyl Amine

75-31-0 120 Tons • Glyphosate herbicide

formulations.

• Regulating agent for plastic.

• Intermediate in organic synthesis

of coating materials, plastics,

pesticides, rubber chemicals,

pharmaceuticals and others.

• Used an additive in petroleum

industry.

5 Di Methyl

Amine

Hydrochloride

506-59-2 1200 Tons � Di Methyl Amine Hydrochloride

is used in an API drug named

Metformin. Metformin is an oral

andiabetic drug.

� Metformin works by suppressing

glucose production by the liver.

6 Furfurylamine 617-89-0 240 Tons • Used as a key raw material for

Furosemide (API Drug), this is

primarily used for the treatment

of hypertension, kidney stone,

congestive heart failure and

edema.

• It has a new application in agro

products.

7 6-Chloro-5(2,3 68786-66- 100 Tons � Triclabendazole (N-1) is used

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

Dichlorophenox

y)-2-Methylthio

1H

Benzimidazole

(Triclabendazol

e Crude)

3 in a drug named

Triclabendazole which is

developed as an oral route

drug, and displays high

efficacy against both

immature and adult liver

flukes, roundworms and

ectoparasites.

� It is also used as a veterinary

drug.

8 5-Chloro-4-

Amino-2,1,3-

Benzothiadiazol

e (TNZ)

30536-19-

7

24 Tons • 5-Chloro-4-Amino-2,1,3-Benzothiadiazole is used in an API drug called Tizanidine, which is a short-acting muscle relaxant. It works by blocking nerve impulses (pain sensations) that are sent to your brain. Tizanidine is used to treat spasticity by temporarily relaxing muscle tone.

9 2-Furoic Acid 29447-28-

9

60 Tons • 2-Furoic acid helps sterilize

and pasteurize many foods.

• 2-Furoic acid is used as an

intermediate in a drug named

Quinfamide. Quinfamide is a

drug that has anit-parasitic

properties. It is used to treat

chronic and sub-acute intestinal

amebiasis.

• 2-Furoic Acid is used as

speciality chemical in allied

industries.

10 Cyclohexenyl

Ethyl Amine

(CHEA)

3399-73-3 120 Tons • CHEA is used as an

intermediate for the drug named

dextromethorphan which is used

for treating cough.

PROJECT PROPONENT

Galaxy Laboratories is a venture capital company promoted with equity participation from

Industrial Development Bank of India (IDBI) in the year 1995. The company is a

manufacturer of Intermediates for API’s (Active Pharmaceutical Ingredients) and specialty

Agro Chemicals. It is one of the leading manufacturers of the product Furfurylamine in the

Page 8: PRE-FEASIBILITY REPORT FOR PROPOSED API …environmentclearance.nic.in/writereaddata/FormB/TOR/PFR/23_Oct... · Galaxy Laboratories is a venture capital company promoted with equity

Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

world. Furfurylamine is used in an API known as Furosemide which is primarily used for the

treatment of hypertension, congestive heart failure and edema.

Galaxy promoted by Shrikant Deshmukh and Nagesh Walimbe both are having 36 years of

experience in chemical units worked with multinational companies. Hoechst India Ltd.,

Roche products Ltd. etc.

2.2 BRIEF DESCRIPTION OF NATURE OF THE PROJECT

The proposed Unit at Newasa aims at commercialization of ingeniously developed

technology from Agro based in the area of Furfural chemistry and value-added derivatives of

Furfural namely Furfuryl Alcohol and Furfurylamine. Galaxy has also proposed commercial

processes for API Intermediates. These technologies are mainly in the area of reductive

Amination by hydrogenation, catalytic hydrogenation with selectivity and isomerization.

The company is also setting up a Hydrogen Plant for the generation of in-house hydrogen

gas. Further, the company is adept at handling Hydrogen gas, Raney Nickel, Palladium-

Carbon, Platinum and other noble metal catalysts, as also in hazardous chemicals like

Carbon Di Sulphide, Fuming Nitric Acid, Thionyl Chloride, Phosphorous Oxychloride, Liquid

Ammonia etc.

2.3 NEED FOR THE PROJECT AND ITS IMPORTANCE TO THE COUNTRY

OR REGION

The products proposed to be manufactured by the company are a new generation product

range based on Reductive Amination by Hydrogenation, these are high value intermediates

involving Hydrogenation Technology and compounds require Ring Hydrogenation for the

manufacture lifesaving API’s.

The products developed by Galaxy are substantially of low prize compared to imported

material. This is due to much less consumption of Raw Materials, Less number of Chemical

steps involved in Manufacturing & being Green Technology.

Products viz 6-Chloro-5(2,3 Dichlorophenoxy)-2-Methylthio 1H Benzimidazole

(Triclabendazole Crude), 5-Chloro-4-Amino-2,1,3- Benzothiadiazole, 2-Furoic Acid proposed

to manufactured in the project have huge export potential and contribute highly in import

substitution for the country.

Hydrogen gas manufacturing will reduce import of hydrogen gas from China and Germany.

At present procurement of hydrogen gas is been done from outside of Maharashtra for our

Aurangabad plant. Due to establishment of Indian made hydrogen plant with M/s Muse

Consultants & Multifab Engineers (Mumbai) will be the first of its kind to be set up in

Newasa. Hydrogen gas will be available for captive consumption and also support/supply

other industries which have requirement for the same. Through this venture, India can

establish its name in the foreign market.

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

Manufacturing of Furfuraldehyde, furfural alcohol and furfuryl amine in India will considerably

reduce imports from International markets. The country will be self reliant and also reducing

dependability of Indian API and allied manufacturers on International market. Hence the

outflow of foreign exchange will be limited.

Galaxy is the only company who has successfully introduced Furfurylamine in India and has

become one of world’s largest manufacturer. Recent research has developed some high

value agro-products using 3-Hydroxy Pyridine and 2-Chloro-3-Hydroxy Pyridine as basic raw

materials. These two products are synthesized from Furfurylamine; therefore demand for

Furfurylamine is growing disproportionately.

Production of Mono Iso Propyl Amine (MIPA), Di Methyl Amine Hydrochloride (DMA.Hcl),

Cyclohexenyl Ethyl Amine (CHEA) will be profitable due to high tonnage production and no

dependability on petroleum products and in-house availability of hydrogen gas. These API

intermediates have very high potential because API’s made out of the intermediates have

come out of patent regulations in the international market since 2009. Therefore, Indian

MNC’s are launching these API’s, as a result, consumption of these intermediates have

increased rapidly.

Thus the setting up of proposed API unit at Newasa will contribute in economic growth of

India as well as region by increasing exports and limiting imports of material / chemicals. At

the same raising self reliance of the country on these products.

2.4 DEMAND-SUPPLY GAP

Demand-Supply Gap for Furfuraldehyde, Furfuryl Alcohol and Furfurylamine,

Hydrogen gas

The information given for the three products mentioned below is related to World Demand-

Supply gap.

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

Furfuraldehyde

Furfuryl Alcohol

53%

13%4%

4%

3%

5%

2%8%

6% 2%

World Demand for

Furfuryl Alcohol

(TPA)

China

USA

India

52%34%

9%5%

World Supply for

Furfuryl Alcohol

(TPA)

China

Thailand

USA

India

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

Furfurylamine

Hydrogen Gas

Hydrogen gas will not be exported. There is a huge demand for Hydrogen gas in the domestic

market and Galaxy will majorly consume it captively.

The below mentioned information is based on demand-supply gap for Hydrogen Gas in

domestic market (India).

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

Mono Iso Propyl Amine (MIPA)

For explaining the demand-supply gap, export demand has not been taken into consideration,

as the entire capacity is already being required by our current customers.

Supply:

Sources majorly imported

• Manufactured in India in unorganized sector

Di Methyl Amine Hydrochloride (DMA.HCl)

Supply

• Imported from China

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

• Small Manufacturers

• In-house production by API Companies

Cyclohexenyl Ethyl Amine (CHEA)

Supply

• Imported from China

• Small Manufacturers in India

6-Chloro-5(2,3 Dichlorophenoxy)-2-Methylthio 1H Benzimidazole (Triclabendazole Crude)

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

Supply

• Imported from China

• Small Manufacturers in India

• Currently the major supplier is Galaxy for domestic market.

5-Chloro-4-Amino-2,1,3- Benzothiadiazole (TNZ)

38%

14%

28%

10%

10%

Demand for TNZ (TPA)

Dr. Reddy's

Laboratories

(Hyderabad)

Med Concepta

Sun Pharma

(Baroda)

2-Furioc Acid

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

2.5 IMPORTS VS. INDIGENOUS PRODUCTION

SR.

NO.

PRODUCT IMPORT INDIGENOUS

1 Hydrogen Gas

(Hydrogen Plant)

Currently hydrogen plant is

imported from Germany or

China.

Galaxy along with Muse

Consultants is venturing into

setting up the first Indian made

Hydrogen plant.

This will give the country prestige

and importance to erect further

more hydrogen plants in the near

future at a low cost compared to

that of the foreign countries.

2 Furfuraldehyde The current unorganized

sectors of manufacturers in

India are not able to fulfill the

requirement of Furfural.

Lot of Furfural is required to

produce Furfural related

derivatives and therefore it is

imported from China &

Thailand.

Galaxy plans to make tie ups with

farmers producing corn, in and

around Newasa area and will

produce Furfural in huge quantity

for meeting the requirements of

manufacturers who focus on value

added derivatives of Furfural.

3 Furfuryl Alcohol Furfuryl Alcohol is currently

manufactured mostly in China.

As this is an important chemical

for many industries other than

Pharmaceuticals, manufacturing in

India will open a new export

market and will meet indigenous

requirement.

4 Mono Iso Propyl Amine Currently MIPA is being

imported in India by companies

like IPCA Laboratories Pvt. Ltd.

Indigenous production of MIPA will

promote exports and is helpful to

many industries as it has multiple

properties and used in varied

industries.

5 Di methyl amine

hydrochloride

Di methyl amine is being

imported in India from China.

This is used as an important raw

material for manufacturing an

important API drug known as

Metformin. Indigenous

manufacturing of this drug will help

Indian based API MNC’S in

sourcing this raw material from

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

Galaxy rather than importing it.

6 Furfurylamine Other than Galaxy there is only

one company called PENN

Specialty in the U.S.A. that

manufacture Furfurylamine.

Galaxy is the only manufacturer in

India that manufactures Furfuryl-

amine and supplies it to API

companies like IPCA Laboratories,

Amri India, Hemdeep and Sri

Krishna Laboratories.

This material is also exported to

Sanofi Aventis (Germany), Teva

Tech (Israel), Syngenta (USA),

and Sojitz (Japan).

7 6-Chloro-5(2,3

Dichlorophenoxy)-2-

Methylthio 1H

Benzimidazole

(Triclabendazole

Crude)

These raw materials were

imported from South East

Asian countries like China,

Thailand etc.

Galaxy Supplies these key raw

materials to company’s like:

• NGL Pharma Laboratories

• Sequent Scientific Ltd.

• Dr. Reddy’s Laboratories

• Sun Pharma

• Med Concepta

• Survival Technologies

• Wokhardt Limited

Galaxy has facilitated the supplies

of these MNC’s to provide key raw

materials for API drugs.

8 5-Chloro-4-Amino-

2,1,3- Benzothiadiazole

9 2-Furoic Acid

10 Cyclohexenyl Ethyl

Amine (CHEA)

2.6 EXPORT POSSIBILITY

All the products have potential of being exported as there has been a very niche

segment of manufacturers in India that manufacture these above mentioned molecules

and Galaxy’s share in the supply is a major one. These products are in high demand for

API MNC’S established in India and abroad.

Galaxy has established its name in the API Intermediate market and has been an

approved vendor for many MNC’S . When developing a new product, the company can

leverage the brand to market the products and can sell these products in the export

market.

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

2.7 DOMESTIC/EXPORT MARKETS

Already discussed in section 2.5 and 2.6

2.8 EMPLOYMENT GENERATION (DIRECT/INDIRECT) DUE TO THE PROJECT

The local areas will be benefited by way of generation of employment opportunities, increased

demand for local products and services. There will be an overall improvement in the income

level of the people.

The project creates employment to about 350 persons once the plant comes to the operational

stage and for 150 persons during construction stage. Top priority will be given to locals for

semi-skilled and unskilled jobs. With the development of this plant there will be a lot of scope

for more ancillary development, which in turn will benefit the nation.

There will be a certain enhancement of educational and medical standards of people in the

study area. There will be generally positive and beneficial impacts by way of economic

improvements, transportation, aesthetic environment and business generation. There will be an

overall upliftment of socio-economic status of the people in the area with the implementation of

the project.

Manufacturing of furfural requires corncobs in high tonnage which can be achieved by providing

the local farmers with seeds which will directly benefit the farmers in terms of agriculture and

the company for meeting its raw material needs. Biomass generated in this product is of good

fuel value and can be directly used as boiler fuel.

Agriculture – Cooperative Society will be formed, wherein the farmers will be benefited and

there will be growth in agriculture.

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

CHAPTER – 3

PROJECT DESCRIPTION

3.1 TYPE OF PROJECT INCLUDING INTERLINKED AND INTERDEPENDENT

PROJECTS

3.1.1 Type of Project

Galaxy Laboratories Private Limited is mainly engaged in manufacturing of API

Intermediates and Agro-Chemicals. The company in the proposed project aims at

commercialization of indigenously developed technology from Agro based in the area of

Furfural chemistry and value-added derivatives of Furfural namely Furfuryl Alcohol and

Furfurylamine. The company is setting up a Hydrogen Plant for the generation of in-

house hydrogen gas.

3.1.2 Interlinked and Interdependent Projects

One of the products Furfuraldehyde requires agro waste (corncob) as raw material.

Galaxy aims at making tie-ups with farmers in proximity with the Newasa for the

cultivation of corn. This will benefit the farmers as corn cultivation is pre-dominant in

Aurangabad district. Thus, the farmers and the company will be interdependent and will

benefited.

The Hydrogen plant being set-up at Newasa is the first Indian made Hydrogen plant.

Which is a raw material for Furfuryl alcohol, Furfuryl amine, CEA, CAB,MIA,

3.2 Location

The proposed chemical plant is located Plot No. B-10, MIDC Newasa Industrial Area, at

Post Tukai – Shingve, Auranagabad – Pune Highway, Near Godegaon, Tal.Newasa,

Ahmednagar – 414607 (Maharashtra). The latitude and longitude are 19018’20.12’’N ,

74051’18.38’’ to 19018’23.36’’ N, 74051’09.69’’E respectively.

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

Fig 3.1 Google image of Location

3.3 DETAILS OF ALTERNATE SITES CONSIDERED AND THE BASIS OF SELECTING

THE PROPOSED SITE:

3.3.1 Alternate Sites

API intermediate unit can be set-up in industrial areas and therefore four MIDC namely,

Waluj, Chikhalthana, Railway Station and Paithan could be considered. However,

comparatively the land that Newasa MIDC had an advantage in terms of location and well

developed infrastructure, close to State Highway.

The Newasa MIDC land is economical as compared to MIDC land available at the other sites

and as the project requires abundant land area, the Newasa MIDC land was preferred.

3.3.2 Selection of the Proposed Site

The project is being proposed to set-up at MIDC Newasa Industrial Area, as the location is

an industrial land under the authority of Maharashtra Industrial Development Corporation

(MIDC); it facilitates all statutory clearances required for running manufacturing companies

as compared to free hold land.

Newasa MIDC is not situated within the city limits, which was an advantage as no residential

area is in proximity and thus will not be affected by the ancillary effects of the manufacturing

unit. (For e.g. Noise, odor etc)

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The land is situated in the “D-Zone” of the development sector and the unit is entitled to

subsidiaries like power, interest cost, and sales tax.

Newasa Industrial area is in the vicinity of Taluka places namely, Kanad, Sillod, Soyagaon,

Vaijapur and Phulambri. Corns are extensively cultivated in all these areas, this will greatly

facilitate the procurement of corn cobs due to easy availability and cheaper transportation

costs.

The product Furfural can also be produced from bagasse as the main raw material. Bagasse

is abundantly available in Newasa region and is in vicinity to the company’s site in Newasa

owing to number of sugar factories located nearby.

3.4 SIZE OR MAGNITUDE OF OPERATION:

The proposed project will be set-up on 48400 sq.mtr (over 12 Acres) land at Newasa MIDC.

The facility will have a manufacturing plant with state of the art technology. The company is

also putting up agro research centre at the site with well-equipped and designed research

and development laboratory for API Intermediate.

The company has high consciousness for environmental protection and has established an

Effluent Treatment Plant for treating any type of chemical effluent.

Sr. No PRODUCT CAPACITY

1 Hydrogen Gas 18.72 Lacs NM3

2 Furfuraldehyde 600 Tons

3 Furfuryl Alcohol 360 Tons

4 Mono Iso Propyl Amine 120 Tons

5 Di Methyl Amine Hydrochloride 1200 Tons

6 Furfurylamine 240 Tons

7 6-Chloro-5(2,3 Dichlorophenoxy)-2-Methylthio 1H

Benzimidazole (Triclabendazole Crude)

100 Tons

8 5-Chloro-4-Amino-2,1,3- Benzothiadiazole 24 Tons

9 2-Furoic Acid 60 Tons

10 Cyclohexenyl Ethyl Amine (CHEA) 120 Tons

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3.5 PROJECT DESCRIPTION WITH PROCESS DETAILS

A) Hydrogen Gas from Methanol Cracking

• Galaxy Laboratories Private Limited (Newasa) is the first company, along with M/S.

Muse Consultants & Multifab Engineers (Mumbai) to set up the first Indian made

Hydrogen Plant.

• The Hydrogen Plant will work on the technology of producing hydrogen gas from

methanol cracking.

Technical Details

The basic reaction of methanol decomposition/ reforming comprises of two parts:

CH3OH + H2O = CO2 + 3H2

Heat of Reaction = - 49.5 kJ/mol

The basic process of methanol decomposition consists of the following steps:

• Mixing of methanol and Demineralized water (D.M. Water). • Preheating and evaporation of the methanol/water mixture. • Methanol decomposition and shift conversion. • Process gas cooling and condensate separation. • Purification in PSA unit. (The hydrogen is purified in a PSA unit operating with a

hydrogen recovery rate of approx. 75% - 80 %.)

Route of Synthesis for Hydrogen Gas

+

Methanol Water Hydrogen Gas Carbon di Oxide

(MW-32) (MW-18) (MW-2) (MW- 44)

H—H

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FLOW CHART FOR HYDROGEN GAS MANUFACTURING

Batch Tank Compressor

Pre-heater Separator Condenser

i) Methanol (1180 TPA)

ii) D.M.Water (675 TPA)

Evaporator

Reactor Filled

with Catalyst

(Stationary Bed

at 2800C)

Recovered Methanol + Water

(Recycled to Batch Time and to

Evaporator)

Cooling with

Cooling Water

Vent Gases (55-88% CO2 + 0-2% CO + 40% H2) v/v

14.22 Lacs NM3/Annum at 190 NM3/Hr

(Vent Gases are vented at 11 meter height with flame

arrester at the top)

PSA

Section

Seal Pot

H2

Purging

vessel

Hydrogen Purification Unit

Hydrogen Gas (Purity 99.99%)

Storage in MS cylinder having capacity 5.7 NM3 per cylinder at 150 Kg/cm2

(18.72 Lacs NM3/Annum at 250 NM

3/Hr)

Heating with Thermopac

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B) Furfuraldehyde (Furfural)

• Furfuraldehyde is an organic compound derived from a variety of agricultural

products such as corn cobs, oat, wheat bran and sawdust.

• The process of furfural includes hydrolysis of pentosan, which is present in

the above mentioned agricultural products.

• Galaxy is currently aiming at producing furfural from corn cobs using sulphur

trioxide and steam at high temperature.

• The R & D of Galaxy Laboratories Private Limited is in the process of

developing seeds for corn cobs with high pentosan content.

• The company has filed a patent for “A Process for Preparing Furfural”. (Copy

of Patent Novelty Search Report is enclosed)

Technical Details

Corn cobs are cut into 3 to 6 mm size and subjected to vapor phase hydrolysis using sulphur

trioxide gas and steam at elevated temperature and pressures in cylindrical vessel. The

process generates formation of Furfural along with other chemicals. The Furfural thus

generated is then taken out of the cylindrical vessel by using dry steam under pressure and

these vapors are cooled and fractionated to obtain Furfural along with other by-products

namely Acetic Acid, Acetone and Methanol. By employing specific conditions of temperature,

pressure and relative concentrations of sulphur trioxide, 9 to 12% furfural yield is extracted.

Route of Synthesis for Furfuraldehyde

Pentosan Furfuraldehyde

(MW-150) (MW- 96.09)

Dilute H2SO4

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FLOW CHART FOR FURFURAL MANUFACTURING

i) Corn Cobs

ii) Dilute H2SO4

Digester for

Corn Cobs Filter

Furfural

Crude &

Water

Distillation Unit

Spent Corn Cob To Boiler Feed

Caustic Lye

Top Layer

Bottom Layer

For Separation of Water

Layer for ETP

Reside sent to Hazardous

Waste Facility

Furfural Pure

(Output: 12 to 12.4 MT/ANNUM)

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C) Furfuryl Alcohol

Furfural (Furfuraldehyde) is reacted with Hydrogen Gas in liquid phase using Raney Nickel

Catalyst to form Furfuryl Alcohol. By employing specific conditions of temperature, pressure

and relative concentrations of these three components, a high selectivity is achieved at

relatively low pressures of Hydrogen leading to over 95% yield.

Technical Details:

Stage I:

In an 1100 Liters Autoclave, charge specific quantity of Furfural and Raney Nickel Catalyst.

Close the autoclave and flush it with nitrogen to remove trapped air in the empty space of the

autoclave. Then flush the autoclave with Hydrogen to remove Nitrogen from the empty place.

Keep 0.5 Kg/cm2 hydrogen gas pressure in the autoclave and slowly heat the reaction mass in

the autoclave at 139 to 140ºC. The pressure in the autoclave will start rising. Keep very slow

purging of Hydrogen gas and maintain Hydrogen gas at 15 to 15.5 Kg/cm2 and temperature at

139 to 140ºC. Apply intermittent heating or cooling to maintain these conditions. After 15 hours

of reaction start drawing sample for GC analysis and check for conversion. At the end of 20 to

22 hours Furfuryl Alcohol conversion will reach to 95 to 96% level with 4.5 to 3.5% level

Unreacted Furfural and impurity level of 0.4 to 0.6%. Stop the reaction at this stage by applying

cooling, release hydrogen, flush the Autoclave with nitrogen and filter the batch to get crude

Furfuryl Alcohol.

Stage II:

Crude Furfuryl Alcohol obtained in the Stage I is taken in a distillation still and distilled under

vacuum (5mm of Hg) to recover Furfuryl Alcohol (99.5%) & Furfural (98.5%).

The company has filed a patent for “A Process for Preparing Furfuryl Alcohol”. (Copy of Patent

novelty search report is enclosed)

Route of Synthesis for Furfuryl Alcohol

+ +

Furfural Hydrogen Gas Furfuryl Alcohol

H—H

Nickel Catalyst

Tetrahydro Furfural

Alcohol

(MW-96.09) (MW-2) (MW-98.10) (MW-102.13)

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FLOW CHART FOR FURFURAL ALCOHOL MANUFACTURING

i) Furfural Crude Liquid

ii) Nickel Catalyst

iii) Hydrogen Gas

Autoclave

20 to 25 Kg/cm2

90 to 95 ºC

High Vacuum

Fractional

Distillation System

Pressure Filter

Furfural Alcohol

Crude Transferred

to Distillation

Pure Furfuryl Alcohol

Residue sent to Hazardous Waste

Facility

(Output 7.2 to 7.6 MT/Annum)

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D) Mono Iso Propyl Amine (MIPA)

Stage I

In a high pressure Autoclave charge acetone, Liquor Ammonia and Nickel Catalyst.

Close the autoclave. Take 5 kg pressure of Hydrogen Gas in the autoclave and start stirring

and heating. Heat the reaction contents to 55°C, hydrogenation starts. Maintain reaction

temperature in the range 55 to 65°C by circulating cooling water in the jacket. Carry out

reaction of Hydrogenation at 55 to 65°C maintaining Hydrogen pressure at 5 to 6 kg/cm2 for

three hours. When the absorption of hydrogen gas in the reaction mass is ceased, draw a

sample and analyzed on gas chromatogram to confirm complete conversion of Acetone.

Cool the reaction mass in the autoclave to 40 to 50°C by providing cooling in the jacket.

Settle the reaction mass for 1 hour. Release Hydrogen gas pressure from the autoclave.

Flush the autoclave with Nitrogen gas and filter the batch using sparkler filter to obtain crude

MIPA. This filtrate is taken for fractional distillation. Catalyst is deactivated with dilute

Hydrochloric acid and sent to the manufacturer for regeneration.

Stage II

The crude MIPA obtained from the above step is fractionated in a fractional distillation unit to

separate pure MIPA along with various impure fraction containing impurities. During the

course of fractional distillation, samples are drawn at regular intervals and distillation column

is continuously monitored by controlling vacuum & temperature to separate various

impurities as impure fractions. By maintaining proper reflux ratios and other conditions, pure

MIPA is collected as main fraction a special receiver assigned for it. It is then checked for

final quality testing and if found ok then packed and transferred to finished goods storage.

Route of Synthesis for Mono Iso Propyl Amine

+ +

Acetone Ammonia Hydrogen Gas Mono Propyl Amine

(MW-58.08) (MW-17) (MW-2) (MW-59.11)

H—H

Nickel Catalyst

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FLOW CHART FOR MONO ISO PROPYL AMINE MANUFACTURING

i) Acetone

ii) Ammonia (Liquor)

iii) Nickel Catalyst

iv) Hydrogen Gas Autoclave

5 to 6 Kg/cm2 55

to 65 ºC

Pressure Filter

Mono Iso Propyl

Amine Crude

Transferred to

Distillation

High Vacuum

Fractional

Distillation System

Pure Mono Iso Propyl Amine

Residue sent to Hazardous Waste

Facility

(Output 2.4 to 2.6 MT/Annum)

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E) Di Methyl Amine Hydrochloride (DMA.HCl)

Stage I

In a reactor fitted with column condenser & receiver, charge Dimethylamine (40%) dissolved

in Water. Start stirring and add required quantity of Hydrochloric (30%) to adjust pH of the

reaction mixture at 6 to 6.5. Stir the contents for 1 hour and apply slow heating and vacuum

to distill out specific quantity of water while maintaining reaction temperature at 45 to 50°C.

Cool the contents to 25°C and centrifuge the crystallized DMA.HCl. Collect the Mother

Liquor and use for next batch.

Stage II

The Crystalline DMA.HCl obtained above is the dried in Rotary Cone Vacuum Dryer (RCVD)

for 8 hours at 40°C. It is then unloaded and packed in Fiber board Drums.

Route of Synthesis for Di Methyl Amine Hydrochloride

+

Dimethylamine Hydrochloric Acid Dimethylamine Hydrochloride

(MW-45.10) (MW-36.50) (MW-81.60)

H—CL

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FLOW CHART FOR DI METHYL AMINE HYDROCHLORIDE MANUFACTURING

i) Di Methyl Amine

ii) HCl

Reactor

Centrifuge

Dryer

Mother Liquor

Recycle

Pure Di Methyl

Amine HCl

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F) Furfurylamine

It is produced by Reductive Amination of Furfural with Ammonia and Hydrogen Gas in liquid

phase using Raney Nickel catalyst to form Furfurylamine with very high level of selective

leading to primary amines.

Technical Details:

Stage I:

In an 1100 Liters Autoclave, charge specific quantity of Furfural, ammonia and Raney Nickel

Catalyst. Close the autoclave and flush it with nitrogen to remove trapped air in the empty

space of the autoclave. Then flush the autoclave with Hydrogen to remove Nitrogen from the

empty place. Keep 0.5 Kg/cm2 hydrogen gas pressure in the autoclave and slowly heat the

reaction mass in the autoclave at 139 to 140ºC. The pressure in the autoclave will start rising.

Keep very slow purging of Hydrogen gas and maintain Hydrogen gas at 12 to 13.5 Kg/cm2 and

temperature at 65 to 95ºC.

Apply intermittent heating or cooling to maintain these conditions. After 22 hours of reaction

start drawing sample for GC analysis and check for conversion. At the end of 20 to 22 hours

Furfurylamine conversion will reach to 94.5 to 95% level with total impurities in the range 5 to

5.5% level with no trace of Unreacted Furfural. Stop the reaction at this stage by applying

cooling, release hydrogen, flush the Autoclave with nitrogen and filter the batch to get crude

Furfurylamine.

Stage II:

Crude Furfurylamine obtained in the Step 1 is taken in a distillation still and distilled under

vacuum (2mm of Hg) to recover Furfurylamine (99.5%).

The company has filed a patent for “Improved Process for Furfurylamine”. (Copy of patent is

enclosed)

Route of Synthesis for Furfurylamine

+ +

Furfuraldehyde Ammonia Hydrogen Gas Furfurylamine

(MW-96.09) (MW-17) (MW-2) (MW-97)

H—H

Nickel Catalyst

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FLOW CHART FOR FURFURYLAMINE MANUFACTURING

i) Furfural Crude

ii) Ammonia (Liquor)

iii) Nickel Catalyst

iv) Hydrogen Gas Autoclave

18 to 20 Kg/cm2

95 to 105 ºC

Pressure Filter

Furfurylamine

Crude Transferred

to Distillation

High Vacuum

Fractional

Distillation System

Pure Furfurylamine

Residue sent to Hazardous Waste

Facility

(Output 4.8 to 5.2 MT/Annum)

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G) 6-Chloro-5(2,3 Dichlorophenoxy)-2-Methylthio 1H Benzimidazole (Triclabendazole

Crude)

Stage I: (Condensation & Hydrolysis)

Charge Dimethyl Formamide and 2, 3 Dichloro Phenol. Start stirring and heat at temperature

50 to 60˚C. Charge potassium carbonate, stop heating, start cooling and add nitro

compound at temperature 30 to 40˚C. Start heating, start distillation and complete. Charge

methanol, start stirring and add caustic solution, maintain temperature at 50 to 55 ˚C. Then

charge water at 40˚C. After addition is complete, stir for 30 min and then start centrifuge.

Stage II: (Hydrogenation)

Charge Methanol, PNA, & Catalyst, and flush with Nitrogen and Hydrogen. Start stirring and

hydrogen feeding. Give heat by applying steam in jacket and heat upto 45-46°C and stop

heating. Continue reaction at 55-60°C till hydrogen pressure inside is upto 5kg/cm2. Use

cooling water circulation in jacket, once there is no further rise in temperature and drop in

pressure is noticed at 5kg/cm2 for at least 30 minutes. When the end point of reaction is

indicated, stop hydrogen purging and stirring and allow settling for 1 Hr. Release hydrogen

pressure slowly up to 0.5 kg/cm2, flush with nitrogen pressure and filter through pressure

filter.

Stage III: (Cyclization)

Charge Methanolic solution in room temperature, add caustic lye under continuous stirring

and cool to 40°C. Start CS2 addition at 40°C and complete addition in 6 Hrs. After CS2

addition stir for ½ Hr. Start heating and reflux for 10 Hrs. Charge water, heat to 80°C and

maintain for one Hr. Cool to 60°C and start addition of acetic acid between 3-4 Hrs. After

addition of acetic acid stir for ½ Hr. Check the pH of reaction mass is 6 – 7. Centrifuge and

unload the material.

Stage IV: (Methylation)

Charge Methanol with above stage – III material at room temperature and stir for 1 Hr and

slowly add DMS at 35 - 40°C. Start heating slowly to 65°C to maintain reflux for 8 Hrs. After

completing the reaction, cool the reaction & filter through centrifuge.

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Stage V: (Charcoal Treatment & Neutralization with Ammonia)

Charge Methanol and above stage – IV material and heat upto 60-65°C. Charge charcoal

and maintain for 1 Hr. Filter the reaction mass and collect the filtrate in SS reactor. Cool the

reaction mass at room temperature and add Liquor ammonia. Centrifuge the material and

dry to get the product in powder form.

Route of Synthesis for 6-Chloro-5(2,3 Dichlorophenoxy)-2-Methylthio 1H

Benzimidazole (Triclabendazole Crude)

Stage I: (Condensation & Hydrolysis)

+

2,3 Dichlorophenol 3,4-Dichloro-6-Nitro Acetanilide

4-chloro-5(2,3-dichloro

phenoxy)-2-nitrophenyl

acetamide

(MW-163.00) (MW-249.05) (MW-375.59)

K2CO3

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+ H2O

Stage II: (Hydrogenation)

4-chloro-5(2,3-dichloro

phenoxy)-2-nitrophenyl

acetamide

MeOH/Caustic Lye

5-chloro-4-(2,3-

dichlorophenoxy)-2-

nitroaniline

Water

(MW-375.59) (MW-18.00) (MW-333.55)

H2/R.N.Catalyst/MeOH

5-chloro-4-(2,3-

dichlorophenoxy)-2-

nitroaniline

4-chloro-5-(2,3-

dichlorophenoxy)-1,2-

Phenylenediamine

Hydrogen Gas

(MW-333.55) (MW-6.00) (MW-303.55)

3H2

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Stage III: (Cyclization)

Stage IV: (Methylation)

Stage V: (Charcoal Treatment & Neutralization with Ammonia)

CS2/Caustic Lye/CH3COOH

4-chloro-5-(2,3-

dichlorophenoxy)-1,2-

Phenylenediamine

5-chloro-6-(2,3-dichlorophenoxy)-

1,3- dihydro Benzimidazole-2-

Thione

Carbon Di Sulfide

CH3OH

(MW-303.55) (MW-76.04) (MW-345.55)

DMS

5-chloro-6-(2,3-dichlorophenoxy)-

1,3- dihydro Benzimidazole-2-

Thione

5-chloro-6-(2,3-dichlorophenoxy)-2-

Methylthio-1H-Benzimidazole

Methosulphate

Di Methyl Sulphate

(MW-345.55) (MW-126) (MW-471.55)

MeOH/Charcoal

Ammonia

5-chloro-6-(2,3-dichlorophenoxy)-2-

Methylthio-1H-Benzimidazole

Methosulphate

6-chloro-5-(2,3-dichlorophenoxy)-2-

Methylsulfonyl-1H-Benzimidazole

(MW-471.55) (MW-359.65)

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FLOW CHART FOR 6-CHLORO-5(2,3 DICHLOROPHENOXY)-2-METHYLTHIO 1H BENZIMIDAZOLE (TRICLABENDAZOLE CRUDE)

MANUFACTURING

Stage I: (Condensation & Hydrolysis)

Stage II: (Hydrogenation)

mm

SSR

(Condensation)

i) Dimethyl Formamide

ii) 2,3 Dichloro Phenol

iii) Potassium Carbonate

SSR

(Hydrolysis)

Centrifuge 4-Chloro-5-(2, 3- Dichloro

phenoxy)-2-nitroaniline

(Stage-I)

Dimethyl

Formamide

Recovery

vi) Methanol

vii) Stage-I

viii) Raney Nickel

Catalyst

ix) Nitrogen Gas

x) Hydrogen Gas

SSR

Filtration

4-Chloro-5-(2, 3-

Dichlorophenoxy)-1, 2-

Phenylenediamine (Stage-II)

SSR

(Hydrolysis)

Centrifuge 4-Chloro-5-(2, 3- Dichloro

phenoxy)-2-nitroaniline (Stage-

I)

i) Methanol

ii) Caustic Lye

iii) Water

ML

Transferred

to Recovery

i) Methanol

ii) Stage-I

iii) Raney Nickel Catalyst

iv) Nitrogen Gas

v) Hydrogen Gas

SSR

Filtration

4-Chloro-5-(2, 3-

Dichlorophenoxy)-1, 2-

Phenylenediamine (Stage-II)

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Stage III: (Cyclization)

Stage IV: (Methylation)

i) Stage-II with Methanol

ii) Caustic Lye

iii) Carbon Disulphate

iv) Acetic Acid

SSR

Centrifuge

5-Chloro-4-(2,3-

dichlorophenoxy)-1,3-

dihydrobenzimidazole-2-

thione (Stage-III)

ML

Transferred

to Recovery

i) Methanol

ii) Stage-III

iii) Dimethyl Sulphate

GLR

Centrifuge

5-Chloro-6-(2,3-Dichlorophenoxy)-

2-(Methylsulphate)-1H-

Benzimidazole (Stage-IV)

Methanol ML

Transferred to

Recovery

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Stage V: (Charcoal Treatment & Neutralization with Ammonia)

i) Methanol

ii) Stage-IV

iii) Charcoal

GLR

Filtration

SSR

Centrifuge

Drying

Milling

6-Chloro-5(2,3-Dichloro

phenoxy)-2-Methylsulfonyl-

1-H Benzimidazole

(Triclabendazole Crude N-

1) (Stage-V)

Liquor

Ammonia

Methanol ML

Transferred to

Recovery

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H) 5-Chloro-4-Amino-2,1,3- Benzothiadiazole

Stage I (Hydrogenation)

• Charge Ethyl Acetate • Charge PCONA (Para Chloro Nitro Aniline)

• Charge Raney Nickel Catalyst • Apply Hydrogen Gas & Hydrogen Pressure 4 Kg/cm2 • Continue Hydrogenation by Maintaining Temperature at 60 – 65°C • After Completion of reaction, filter reaction mass through Nutsche filter and wash the

bed with 50.0 L Ethyl Acetate • Take Ethyl Acetate filtrate in clean and dry vessel and distill Ethyl Acetate under

vacuum below 35-40°C • Drain the material in the drum

Stage II (Cyclization)

• Charge Dimethyl Formamide • Charge Stage I Material, stir the material for 30 Minutes at Room Temperature • Add Thionyl Chloride in 3-4 Hrs at 30 – 35°C • After Completion of reaction, quench the reaction mass in chilled water • Adjust the pH by the caustic solution pH upto 7 • Centrifuge the material

Stage III (Nitration)

• Charge Sulphuric Acid & cool to 10°C • Charge Stage II, stir the material for 30 Minutes at Room Temperature • After that slowly add Nitric acid, Temperature should be below 20°C • After completion of reaction mass, quench in chilled water • Centrifuge the material

Stage IV (Reduction)

• Charge Water / Toluene • Slowly add Iron powder

• Charge Stage III, heat slowly to 60°C and maintain for 2-3 hours • After completion of reaction, filter the reaction mass and collect the filtrate in SSR • Start toluene recovery under vacuum temperature 50-55°C • Filter the material in centrifuge and wash with methanol and suck dried to unload the

material • Dry the material at temperature 60-65°C, unload and pack the material as finished

product.

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Route of Synthesis for 5-Chloro-4-Amino-2,1,3-Benzothiadiazole

Stage I (Hydrogenation)

Stage II (Cyclization)

Catalyst/H2/Ethyl Acetate

(MW-172.57) (MW-142.60)

Para Chloro Ortho Nitro

Aniline

4-Chlorobenzene-1,2-

Diamine

DMF/SOCl2

4-Chlorobenzene-1,2-

Diamine

5-Chloro-2,1,3-

Benzothiadiazole

(MW-142.60) (MW-170.62)

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Stage III (Nitration)

Stage IV (Reduction)

H2SO4/HNO3

5-Chloro-2,1,3-

Benzothiadiazole 5-Chloro-4-Nitro-2,1,3-

Benzothiadiazole

(MW-170.62) (MW-216.00)

Iron/Toluene

Methanol

5-Chloro-4-Nitro-2,1,3-

Benzothiadiazole

5-Chloro-4-Amino-

2,1,3-Benzothiadiazole

(MW-216.00) (MW-185.63)

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FLOW CHART FOR 5-CHLORO-4-AMINO-2,1,3- BENZOTHIADIAZOLE MANUFACTURING

Stage I (Hydrogenation)

Stage II (Cyclization)

i) Ethyl Acetate

ii) PCONA

iii) Raney Nickel

iv) Hydrogen Gas

v) Nitrogen Gas

SSR

Filter

Spent Catalyst

sent for

Reaction

SSR

4-Chlorobenzene-

1, 2-Diamine

(Stage-I)

Ethyl Acetate

Recovery

i) Di Methyl Formamide

ii) Stage-I

iii) Thionyl Chloride

GLR

GLR

Centrifuge

5-Chloro-2, 1, 3-

Benzothiadiazole (Stage-II)

Caustic Lye Quenching with

Water & Ice

ML Transferred to

ETP

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Stage III (Nitration)

Stage IV (Reduction)

i) Sulphuric Acid

ii) Stage-II

iii) Nitric Acid

SSR

Sintex

Centrifuge

Quenching with

Water & Ice

ML Transferred to

ETP

5-Chloro-4-Nitro-2, 1, 3-

Benzothiadiazole (Stage-III)

v) Water

vi) Toluene

vii) Iron

viii) Stage

SSR

Iron slug

transferred to

hazard waste

Centrifuge

Toluene

Recovery

Methanol

Washing

Filter

SSR

Drying

Milling

5-Chloro-4-Amino-2,

1, 3-Benzothiadiazole

(Stage-IV)

ML Transferred

to recovery

Sulphuric Acid

Stage-II

Sintex

Centrifuge

5-Chloro-4-Nitro-2, 1, 3-

Benzothiadiazole (Stage-III)

i) Water

ii) Toluene

iii) Iron

iv) Stage-III

SSR

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I) 2-Furoic Acid

Stage I (Oxidation)

• Charge filter water and add Caustic Flakes under cooling.

• Start chilling upto 10 to 15°C.

• Start purging of chlorine at temperature below 15°C.

• Check pH & assay of hypochlorite solution.

• Addition of Furfural Aldehyde at temperature below 20°C.

• Digestion of reaction mass for 5 to 6 hours.

• Check pH & assay of hypochlorite solution. (Limit NMT 1%)

• Charge sodium chloride and stir for 60 minutes.

• Adjust the pH 7 (Neutral) by Hydrochloric Acid.

• Reaction mass to be transferred to GLR-03.

• Addition of Hydrochloric Acid upto pH Range 2 to 2.5.

• Check the pH & stir for 50 minutes.

• Centrifuge the material.

• Wash with 20% NaCl solution and unload the material.

Stage II (Purification)

• Charge filter water and charge 2-Furoic Acid crude material.

• Heat upto 50°C, then charge charcoal and start heating upto 95 to 100°C.

• Maintain temperature at 90 to 95°C for 1 hour.

• Start filtration & filtrate to be collected in GLR-02.

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• Stir & start cooling at room temperature.

• Start brine circulation, chill upto 15 to 20°C and maintain 1 hour.

• Centrifuge the material & wash with chilled water.

• Unload the material.

• Dry the material temperature at 65 to 70°C.

• Dry the material till LOD (Limit NMT 0.5%)

• Unload the material & Pack.

Route of Synthesis for 2-Furoic Acid

+ +

HCl

Furfural Sodium Hypochlorite 2-Furoic Acid

(MW-96) (MW-73.50) (MW-112)

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FLOW CHART FOR 2-FURIOC ACID MANUFACTURING

Stage I (Oxidation)

Stage II (Purification)

v) Water

vi) Caustic Flakes

vii) Chlorine

viii) Furfural

SSR

GLR

Centrifuge

Hydrochloric Acid Aqueous mother

liquor containing

Sodium Chloride

2-Furoic Acid Crude

iv) Water

v) Stage-I

vi) Charcoal

GLR

Filter

Centrifuge

Aqueous mother

liquor (Recycle)

2-Furoic Acid Pure

GLR

Drying Milling 2-Furoic Acid (Pure)

Packing

i) Water

ii) Caustic Flakes

iii) Chlorine

iv) Furfural

SSR

GLR

Centrifuge

Hydrochloric

Acid

2-Furoic Acid Crude

i) Water

ii) Stage-I

iii) Charcoal

GLR

Filter

ix) Water

x) Caustic Flakes

xi) Chlorine

xii) Furfural

SSR

GLR

Centrifuge

2-Furoic Acid Crude

GLR

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J) Cyclohexenyl Ethyl Amine (CHEA)

Stage I

In a high pressure Autoclave, charge Cyclohexenyl Acetonitrile (CHAN), Catalyst and

Toluene. Close the autoclave. Take 10 kg pressure of Hydrogen Gas in the autoclave

and start stirring and heating. Heat the reaction contents to 70°C. Hydrogenation

starts. Maintain reaction temperature in the range 70 to 80°C by circulating cooling

water in the jacket. Carry out reaction of Hydrogenation at 70 to 80°C and maintain

10 to 15 kg/cm2 pressure for six hours. When the absorption of hydrogen gas in the

reaction mass is ceased, draw a sample and analyze on gas chromatogram to

confirm complete conversion of CHAN. Cool the reaction mass in the autoclave to 40

to 50°C by providing cooling in the jacket. Settle the reaction mass for 1 hour.

Release Hydrogen gas pressure from the autoclave. Flush the autoclave with

Nitrogen gas and filter the batch using sparkler filter to obtain crude Cyclohexenyl

Ethylamine (CHEA) and toluene mixture. This filtrate is taken for fractional distillation.

Catalyst is deactivated with dilute Hydrochloric acid and sent to the manufacturer for

regeneration.

Stage II

The crude Cyclohexenyl Ethylamine obtained from stage I is fractionated in a

fractional distillation unit to separate pure Cyclohexenyl Ethylamine along with

Toluene and various impure fraction containing impurities. During the course of

fractional distillation, samples are drawn at regular interval and fractional column is

continuously monitored by controlling vacuum & temperature to separate various

impurities as impure fractions. By maintaining proper reflux ratios and other

conditions pure Cyclohexenyl ethyl amine is collected as main fraction in a special

receiver assigned for it. It is then checked for final quality testing and if found ok,

pack and transfer to finished goods storage.

Route of Synthesis Cyclohexenyl Ethyl Amine (CHEA)

+

H—H

Nickel Catalyst

Toluene

Cyclohexene-1-

Acetonitrile

Hydrogen Gas Cyclohexenyl Ethylamine

(MW-121.18) (MW-2) (MW-125.21)

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FLOW CHART FOR CYCLOHEXENYL ETHYL AMINE (CHEA) MANUFACTURING

i) Cyclohexenyl Acetonitrile

ii) Toluene

iii) Nickel Catalyst

iv) Hydrogen Gas Autoclave

10 to 15 Kg/cm2

70 to 80ºC

Pressure Filter

Cyclohexenyl Ethyl

Amine Crude

Transferred to

Distillation

High Vacuum

Fractional

Distillation System

Toluene Recycled for

Process

Residue sent to Hazardous Waste

Facility

(Output 2.4 to 2.6 MT/Annum)

Pure Cyclohexenyl Ethyl

Amine

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3.6 RAW MATERIAL REQUIRED ALONG WITH ESTIMATED QUANTITY, LIKELY

SOURCE, MARKETING AREA OF FINAL PRODUCTS, MODE OF TRANSPORT OF RAW

MATERIALS AND FINISHED PRODUCTS:

3.6.1 Raw Material Required Along with Estimated Quantity

List of Raw Material and their annual consumption Sr. No.

Name of Raw Material Raw Material Consumption Per Annum

Unit

Hydrogen Gas (Capacity: 18.72 Lacs NM3 TPA)

1 Methanol 1180.00 TPA

2 D.M Water 675.00 TPA

Furfuraldehyde (Capacity: 600 TPA)

1 Corn Cobs 7038.00 TPA 2 Sulphuric Trioxide 210.00 TPA

Furfuryl Alcohol (Capacity: 360 TPA)

1 Furfuraldehyde 396.00 TPA

2 Raney Nickel Catalyst 18.00 TPA

3 Hydrogen Gas (NM3) 129.60 TPA 4 Nitrogen Gas (NM3 14.40 TPA

Mono Isopropyl Amine (Capacity: 120 TPA)

1 Acetone 146.00 TPA

2 Ammonia (Liquor) 34.50 TPA

3 Raney Nickel Catalyst 6.00 TPA

4 Hydrogen Gas (NM3) 43.20 TPA

5 Nitrogen Gas (NM3) 4.80 TPA Di Methyl Amine Hydrochloride (Capacity: 1200 TPA)

1 Di Methyl Amine (40%) 2088.00 TPA

2 HCl (30%) 1030.00 TPA

Furfurylamine (Capacity: 240 TPA)

1 Furfuraldehyde 280.00 TPA

2 Ammonia Gas 52.80 TPA

3 Raney Nickel Catalyst 12.00 TPA

4 Hydrogen Gas (NM3) 86.40 TPA 5 Nitrogen Gas (NM3) 9.60 TPA

6-Chloro-5(2,3- Dichlorophenoxy)-2-Methylthio 1H Benzimidazole Triclabendazole (Crude) (N-1) (Capacity: 100 TPA)

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1 2,3 Dichloro Phenol 72.50 TPA

2 4,5 Dichloro-2-Nitroacetanilide 109.00 TPA

3 Dimethyl formamide 110.00 TPA 4 Potassium Carbonate 66.70 TPA

5 Methanol 1800.00 TPA

6 Caustic Lye 115.00 TPA

7 Hydrogen Gas (NM3) 32.00 TPA

8 Raney Nickel Catalyst 1.80 TPA

9 Carbon disulphide 47.00 TPA

10 Acetic Acid 40.00 TPA

11 Di methyl Sulphate 67.00 TPA

5-Chloro-4-Amino-2,1,3-Benzothiadiazole (TNZ) (Capacity: 24 TPA)

1 Para Chloro ortho nitro aniline 36.00 TPA

2 Ethyl acetate 30.00 TPA

3 Raney Nickel Catalyst 0.432 TPA

4 Hydrogen Gas (NM3) 12.48 TPA

5 Dimethylformamide 84.00 TPA

6 Thionyl chloride 39.00 TPA

7 Caustic Lye 36.00 TPA

8 Sulphuric Acid 180.00 TPA

9 Nitric Acid 12.33 TPA

10 Iron Powder 26.40 TPA

11 Toluene 56.00 TPA

12 Methanol 28.80 TPA

2-Furoic Acid (Capacity: 60 TPA)

1 Furfural Aldehyde 90.00 TPA

2 Caustic Flakes 128.40 TPA

3 Chlorine 75.60 TPA

4 Sodium Chloride 57.60 TPA

5

Charcoal

750.00

TPA

Cyclohexenyl Ethyl Amine (Capacity: 120 TPA)

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1 Cyclohexenyl Acetonitrile 162.00 TPA

2 Toluene 24.12 TPA

3 Raney Nickel Catalyst 6.00 TPA

4 Hydrogen Gas (NM3) 69.12

TPA

5 Nitrogen Gas (NM3) 4.90

TPA

3.6.2 Raw Material Source

Sr.No Product Source of Raw Materials for Products

Key Raw Materials Raw Material Source

1 Hydrogen Gas Methanol • It is indigenously and abundantly

available in India.

• Non-Petroleum based and therefore

their availability is without much

variation in input prices.

2 Furfuraldehyde Corncobs/Bagasse • Corncobs are available in Aurangabad

distreict predominantly in Kannad,

Sillod, Soyagaon, Vaijapur, Phulambri

and Jalgaon district.

• Bagasse is abundantly available in

Ahmednagar district as many sugar

factories are located nearby.

3 Furfuryl Alcohol

Furfuraldehyde

• Galaxy is going to manufacture

Furfuraldehyde, it can be consumed

captively whenever required.

4 Furfurylamine Furfuraldehyde • Galaxy is going to manufacture

Furfuraldehyde, it can be consumed

captively whenever required.

5 2-Furioc Acid Furfuraldehyde Same as above

6 Mono Iso Propyl Amine Acetone • It is indigenously and abundantly

available in India.

7 Di Methyl Amine

Hydrochloride

Di Methyl Amine

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• Non-Petroleum based and therefore

their availability is without much

variation in input prices.

8 Cyclohexenyl Ethyl

Amine (CHEA)

Cyano Acetic Acid • Cyano Acetic Acid is available only in

China and can be imported in huge

quantity when required.

9 6-Chloro-5(2,3

Dichlorophenoxy)-2-

Methylthio 1H

Benzimidazole

(Triclabendazole

Crude)

4,5-Dichloro 2-Nitro

Acetanilide (TC-III)

• Triclabendazole Crude is a product

which involves multiple stages and the

previous output becomes the raw

material input for the next stage of

operation.

• Galaxy will procures material from

outside for the first three stages and

processes it ahead.

10 5-Chloro-4-Amino-

2,1,3- Benzothiadiazole

(TNZ)

Para Chloro Ortho

Nitro Aniline

• It is indigenously and abundantly

available in India.

3.6.3 Marketing Area of Final Products

Galaxy proposes to continue its existing strategy of direct marketing both for the

domestic market as well as for its new products for exports.

Furfural, Furfuryl Alcohol and Furfurylamine are in great demand in India and the

consumption of these chemicals is increasing rapidly.

Company’s API Intermediates namely, 2-Furioc Acid, 5-Chloro-4-Amino-2,1,3-

Benzothiadiazole (TNZ), 6-Chloro-5(2,3 Dichlorophenoxy)-2-Methylthio 1H

Benzimidazole (Triclabendazole Crude), Cyclohexenyl Ethyl Amine (CHEA), Di Methyl

Amine Hydrochloride are currently being sold to multi-national companies (MNC’s) like

Dr. Reddy’s Laboratories, Sequent Scientific, Wochardt Ltd, Survival Technologies, NGL

Pharma, etc. The company has identified higher demand for these products from existing

and new customers.

Galaxy has already developed its own marketing network for local as well as for exports. As a policy, company has restricted intermediaries’ since inception. Since Galaxy’s brand is well established for Furfurylamine, Furfuryl Alcohol and other existing products the company would not face constraints in marketing the proposed products. Galaxy stands fully committed to its quality since beginning and this has given the company brand name in local and export market. Company is well known for its products.

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The processes developed for MIPA, DMA.HCl ensures high profitability due to high

yields and in-house availability of Hydrogen Gas with no dependability on petroleum

products & their ever increasing prices. Therefore, Galaxy can market these products at

a competitive price compared to the others.

The demand for Hydrogen gas is increasing for its property of making the chemical

processes pollution free. The captive consumption of hydrogen gas will benefit the other

products of the company by making them cost effective.

Galaxy will have tie-ups with agents to transport the surplus hydrogen gas to customers

with requirement of the same.

3.6.4 Mode of Transportation of Raw Materials and Finished Products

The aforesaid raw materials are transported by road/sea/air to the manufacturer’s site at

Newasa (Pune-Aurangabad Highway).

3.7 RESOURCE OPTIMIZATION/RECYCLING AND REUSE ENVISAGED IN THE

PROJECT

Corn cob which is a waste will be used as a raw material for manufacturing of

furfuraldehyde. Biomass generated in this product is of good fuel value and can be directly

used as boiler fuel. After treatment of waste water these water will be used for gardening.

3.7 AVAILABILTY OF WATER ITS SOURCE, ENERGY/POWER REQUIREMENT AND

SOURCE SHOULD BE GIVEN

Sr.No PARTICULARS REQUIREMENT SOURCE

1 Water 84 M3/Day Water will be supplied by

Newasa MIDC.

2 Power 320 KVA

(Capacity of

Transformer)

The power is given by the

MSEB (Maharashtra State

Electricity Board). Subsidies

are provided by MSEB on

completion of the project.

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3.8 QUANTITY OF WASTE TO BE GENERATED (LIQUID AND SOLID) AND SCHEME

FOR THEIR MANAGEMENT/DISPOSAL

Sr.

No

Product Waste Quantity Management /

treatment

1 Hydrogen Gas Vent Gases

Carbon di oxide

CO2 - 55-88% +

Carbon Oxide

CO - 0-2% +

Hydrogen

H2 - 40% v/v

14.22 Lacs

NM3/Annum at

190 NM3/Hr

The vent gases will

be collected in the

seal pot, of which

Hydrogen is

discharged through

11 Mtr height

chimney with flame

arrester and CO2 will

be collected from the

seal pot and sold.

2 Furfuraldehyde Distillation Residue 12 to 12.4

MT/ANNUM

The waste will be

collected and treated

in Common

hazardous waste

management &

treatment facility at

Ranjangaon.

3 Furfuryl Alcohol Distillation Residue Output 7.2 to 7.6

MT/Annum

4 Furfurylamine Distillation Residue 4.8 to 5.2

MT/Annum

5 Mono Iso Propyl

Amine

Distillation Residue 2.4 to 2.6

MT/Annum

6 Cyclohexenyl Ethyl

Amine (CHEA)

Distillation Residue 2.4 to 2.6

MT/Annum

7 Di Methyl Amine

Hydrochloride

Nil Zero Discharge -

8 2-Furioc Acid Acidic Water 360 M3/Annum Acidic Water treated

at Effluent Treatment

Plant (ETP) and

used for green belt

development and for

dust suppression /

sprinkling purpose.

9 6-Chloro-5(2,3

Dichlorophenoxy)-2-

Slight Alkaline Water 600 M3/Annum Slight Alkaline Water

treated at Effluent

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Methylthio 1H

Benzimidazole

(Triclabendazole

Crude)

(7.5 to 8 pH) Treatment Plant

(ETP) and used for

green belt

development and for

dust suppression /

sprinkling purpose.

10 5-Chloro-4-Amino-

2,1,3-

Benzothiadiazole

(TNZ)

Neutral Water

(6.5 to 7 pH)

504 M3/Annum Neutral Water

treated at Effluent

Treatment Plant

(ETP)and used for

green belt

development and for

dust suppression /

sprinkling purpose.

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3.10 SCHEMATIC REPRESENTATIONS OF THE FEASIBILITY DRAWING WHICH GIVE

INFORMATION OF EIA PURPOSE

The applicability of the EIA Notification 2006, for the proposed project was explored by considering different possibilities & provision made in the said notification considering the products & project location.

Screening Category B

(As project is in notified industrial area)

Project falls under B1 category as per EIA notification 2006 it falls

in category 5(f) of schedule I, EIA study is required

Form I, PFR+ Proposed TOR

Scoping by SEAC

TOR approved by SEAC

EIA study & Preparation of Report

Submission of EIA report to Dept. of Environment Maharashtra

Appraisal by SEAC

Recommended Not Recommended

Approval from SEIAA

Grant of EC Rejected

Project concept

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CHAPTER – 4

SITE ANALYSIS

4.1 CONNECTIVITY

Connectivity The Site is located on Aurangabad-Pune Highway.

Distance from Pune : 177 Km

Distance from Aurangabad: 73 Km

Distance from Ahmednagar : 22 Km

Distance from Mumbai : 290 Km

Distance from Nearest Village (Godegaon): 1 Km

Distance from Nearest Hospital

(Shaneshwar Gramin Rugnalay – Shanishingnapur) : 10 Km

Distance from Nearest Fire Station (Ahmednagar MIDC): 22 Km

Distance from Nearest Police Station (Sonai): 1 Km

Distance from Nearest Airport (Aurangabad): 75 Km

Distance from Nearest Bus Stand (Godegaon): 1 Km

Distance from Nearest Railway Station (Ahmednagar): 24 Km

Distance from Nearest Sea Port (Mumabai) : 340 Km

4.2 LAND FORM, LAND USE AND LAND OWNERSHIP

Sr. No Particulars Description

1 Land Form MIDC Industrial Land (Newasa)

2 Land Use Barren land

3 Land Ownership Maharashtra Industrial Development Corporation -

Nashik (Leased to Galaxy Laboratories Pvt Ltd for

99 years)

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

4.2 TOPOGRAPHY

Topography of land is more or less plain terrain without much undulation.

Google Map

4.4 EXISTING LAND USE PATTERN

Total Land Area = 48400 Sq.Mtr

Built Up area = 10275.26 Sq.Mtr

Below mentioned table gives brief information regarding environmental setting of the project

site:

Sr.No Particulars Distance from the Site

1 Forest 5.85 km

2 Water Bodies

Stream

Panas odha

Bhar bhordi odha

4.8 km

4.6 km

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

(Dam)

40 Km

3 National Park Nil

4 Wildlife Sanctuary Nil

5 Eco Sensitive Areas

Ahmednagar reserved forest

Bahirwadi Reserved Forest

6.5 km

9.3 km

6 River- Ghodegaon river 4.6 Km

7 Coastal Regulation Zone (CRZ) Nil

4.5 EXISTING INFRASTRUCTURE

The proposed site is well connected by road. State highway SH-60 is 200 m away from the

site. As the site is in notified industrial area all infrastructure are well developed and in

place

4.6 SOIL CLASSIFICATION

The soil in the area is black cotton soil (Plain Terrain).

4.7 CLIMATIC DATA FROM SECONDARY SOURCES

The climatic condition of this area is semi-arid. The maximum temperatures goes upto 45°C

during summer in the month of May and the minimum temperature goes down to 10°C

during winter in the month January – February. The wind in this area is light to moderate

during summer and winter. The rainfall of this district is 750mm. Generally light and

moderate, particularly during the morning hours. While during the afternoon hours the winds

were stronger.

4.8 SOCIAL INFRASTRUCTURE

Social Infrastructure will be developed as per need based in the villages of the vicinity of the

project.

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

CHAPTER – 5

PLANNING BRIEF

5.1 PLANNING CONCEPT

The proposed project is based on eco friendly technology of Hydrogenation and value added

derivates, which will be manufactured from Furfuraldehyde. The following are points of focus

in the Proposed Project:

Manufacturing of Hydrogen Gas from the first of its kind - Indian Made Hydrogen Plant.

Corns and sugarcane are extensively cultivated in near by areas, this will greatly facilitate

the procurement of corn cobs and baggasse and manufacturing Furfural from agricultural

waste (Corn Cob).Thus promoting corn and sugarcane cultivation near by villages.

Manufacturing value added derivatives of Furfural i.e. Furfuryl Alcohol, Furfurylamine & 2-

Furoic acid

For increasing production capacity of Triclabendazole (N-1), 5-Chloro-4-Amino-2,1,3-

Benzothiadiazole (TNZ) & CHEA which is being manufactured at our Aurangabad unit

presently. We are proposing these chemicals in API Unit (Newasa) also, for meeting present

customer increase in demands.

Vision of this project is to manufacture pollution free API intermediates, which are in huge

demand in API, Agro and other allied industries.

The project is situated in the “D-Zone” of the development sector and the unit is entitled to

subsidiaries like power, interest cost, and sales tax.

Project site is not situated within the city limits, no thick residential area is in proximity and

thus will not be affected by the ancillary effects of the manufacturing unit. (For e.g. Noise,

odor etc)

The proposed project is about 50 km from the existing plant of Galaxy at Aurangabad and is

located adjacent to Aurangabad- Pune Highway. The location is strong in infrastructure and

greatly facilitates for transportation of raw material and finished products.

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

5.2 POPULATION PROJECTION

There are no major human settlements in the vicinity of the project site. The manpower

requirement will be sourced from the local areas to the extent possible; hence not much of

settlement of outside people in the area. However, population concentration may increase

around the project site due to increase in ancillary activities

5.3 LAND USE PLANNING

Given below is the land use planning with break-up details of the defined areas:

SR.NO ITEM AREA IN SQ.MTRS

1 Built-Up Area

(Manufacturing Area, Administrative Building,

Security Cabins, R & D Laboratory, Wash room

facilities, Water Tanks, etc.)

2350

2 Storage

(Methanol Storage, Raw Material Storage,

Finished Goods Storage etc.)

2448

3 Green Belt 4715

4 Effluent Treatment Plant (ETP) 1377

5 Corn Cultivation Area (For R & D) 5040

6 Internal Roads 5136

7 Open Space 27334

Total Area 48400

5.4 ASSESSMENT OF INFRASTRUCTURE DEMAND (PHYSICAL & SOCIAL)

The project site is located in notified industrial area wherein all required physical

infrastructure are available as well as underdevelopment (i.e Road, water supply, Electricity,

etc)

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

The project site is situated near Aurangabad and Ahmednagar district which gives easy

access to workers for facilities such as hospitals, Markets and education for workers

children.

Corporate social responsibility will be taken up in the form of setting-up school, hospital,

recreational activities (playground) for villages.

5.5 AMENITIES/FACILITIES

Facilities like drinking water, canteen, and sanitation facility will be provided in the proposed

plant as basic requirements for workers. Transportation facilities will be provided for

employees not in proximity from the unit.

On commencement of the manufacturing site, further amenities will be identified and

incorporated.

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

CHAPTER – 6

PROPOSED INFRASTRUCTURE

6.1 INDUSTRIAL AREA (PROCESSING AREA)

The processing area consists of the following:

A) Manufacturing Unit:

This unit will comprise of all the equipments and machineries required for

manufacturing of API intermediates. The manufacturing unit will be split into

Hydrogenation Plant along with distillation columns and Multi-purpose plant.

B) Hydrogen Plant:

The Hydrogen Plant is a stand-alone unit erected at a considerable distance from the

manufacturing unit and will comprise of a control room which will operate and monitor

the functioning of the Hydrogen plant for the production of Hydrogen gas. The set-up

for the Hydrogen Plant is independent to that of the manufacturing unit.

C) Utilities:

All the utilities required to start operation of the manufacturing and hydrogen plant

comprising of transformer, boiler, thermo-packs, DG set etc are set-up in proximity.

D) Warehouse:

The unit proposes to have the following warehouses:

• Raw Material

• Intermediate

• Finished

• Cold Storage

• Hazardous Material

A) Quality Control Laboratory:

The quality control laboratory will be set-up for the purpose of testing and analysis.

B) Effluent Treatment Plant (ETP):

The ETP is set-up for processing industrial waste/effluent and using the treated water

for gardening.

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

6.2 RESIDENTIAL AREA (NON-PROCESSING AREA)

The non-processing area consists of the following:

A) Administrative Block:

The administrative block comprises of:

• Main Office

• Conference Room

• Reception

• Pantry

• Rest Rooms

• Guest House

A) Security Cabins:

There are two security cabins one at the entrance and the other at the second

service road entrance.

B) Sanitation Area:

Restrooms and bathrooms are placed at relevant distances within the site.

C) Canteen:

The company will allocate a canteen for employees to have their meals. The canteen

will accommodate 100 employees at once.

D) Parking Area:

The company will allocate sufficient parking area for 2-wheeler, 4-wheeler and for

heavy vehicles.

6.3 GREEN BELT

About one-third of total land availability is reserved for plantation. The company has already

done plantation in the perimeter of the land area. The company has also dedicated an area

for corn research, wherein corn cultivation is done. Lawns will be spread for aesthetically

balancing the land area.

SR.NO ITEM AREA IN SQ.MTRS

1 Green Belt 4715

2 Corn Cultivation Area 5040

3 Lawns 520

Total Area 10275

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

6.4 SOCIAL INFRASTRUCTURE

Depending on the growth of the company the required social infrastructure will be provided.

6.5 CONNECTIVITY

The present site is located on Aurangabad-Pune Highway and is well connected. The traffic

on this highway is not dense and is a free-flow route.

SR.N

O

COMPONENT DESCRIPTION

1 Road Maharashtra SH-60:- 200 m

2 Railway Ahmednagar: 24 Km

3 Airport Aurangabad: 75 Km

4 Sea Port Nhava Sheva Mumbai: 340 Km

6.6 DRINKING WATER MANAGEMENT (SOURCE & SUPPLY OF WATER)

Drinking water will be purified with RO (Reverse Osmosis) system. The source of the water

will be from MIDC which will be purified for drinking purpose.

6.7 SEWERAGE SYSTEM

Sewage pipes would be laid in the entire company for the removal and disposal of mainly

non-harmful liquid wastes from the offices, canteen, and domestic waste coming from

different sections. This domestic effluent collected through sanitation areas will be collected

through well-designed sewer network and disposed to septic tanks and soak pit.

6.8 INDUSTRIAL WASTE MANAGEMENT

The following is the brief description of the Effluent Treatment Plant (ETP) for treating industrial waste.

Stage 1:

All waste discharged from the plant which is in the form of liquid, solid, and sludge is collected in the Effluent Collection Tank. The waste collected is both acidic and alkaline.

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

Stage 2:

The waste is then filtered from Effluent Collection Tank (where the maximum amount of sludge settles and is sent to the Sludge Drying Bed 1), and the effluent flows through oil & grease traps where oil and grease is collected in the trap and the effluent is collected in a Pre-Neutralization Tank.

Stage 3:

The effluent in Pre-Neutralization Tank is sent to Neutralization Tank. If the effluent is acidic (Above pH 7), Caustic Lye is used for neutralization. If the waste water is alkaline (Below pH 7), HCl is used for neutralization.

Stage 4:

After the effluent is neutralized, it is sent to the Primary Settling Tank through a pre-filter. From pre-filter effluent is collected in Primary tank, where it allows the settling of solids and the solids are drained out to the Sludge Drying Bed 1 and the effluent flows to the Aeration Tank.

Stage 5:

The bacteria in the Aeration Tank are developed to remove the COD (Chemical Oxygen Demand) & BOD (Biochemical Oxygen Demand) from the effluent by developing a suitable culture which is called as Mixed Liquor Suspended Solids (MLSS). The culture is formed to reduce the organic and inorganic load by treating it with urea, cow dung or jaggery.

Stage 6:

After aeration, the effluent is collected in Secondary Settling Tank to remove excess bacteria/sludge. The sludge is then drained to the Sludge Drying Bed 2, whereas the treated effluent is collected in a Pre-Filter Tank.

The remaining water in the Sludge Drying Bed 1 is drained and is moved back to Effluent Collection Tank for reprocess. The remaining water in the Sludge Drying Bed 2 is drained and moved to Pre-Neutralization Tank for reprocess.

Stage 7:

The treated effluent in the Pre-Filter Tank is passed to the multimedia filter. The multimedia filter contains sand and carbon used to filter the treated effluent for removing the odor and suspended solids. The water after filtration is then used for gardening.

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

The sludge collected in the Drying Beds will be disposed to CHWTH facility authorized by (MPCB-Maharashtra Pollution Control Board).

Effluent Treatment Laboratory Details:

Company has provided a full fledge laboratory to undertake all chemical analysis related to ETP work.

The laboratory is provided with all necessary equipment to run the ETP properly to achieve required specification of the treated water.

6.9 SOLID WASTE MANAGEMENT

The solid waste will be collected by CHWTH facility authorized by (MPCB-Maharashtra

Pollution Control Board).

6.10 POWER REQUIREMENT & SUPPLY/SOURCE

The capacity of the transformer is 320 KVA. The power is given by the MSEB (Maharashtra

State Electricity Board). Subsidies are provided by MSEB on completion of the project

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

Flow Diagram of Effluent Treatment Plant

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

CHAPTER – 7

REHABILITATION AND RESETTLEMENT

(R & R) PLAN

This chapter is not applicable for the proposed project as there is no rehabilitation and

resettlement required in the project site as there are no habitations. No personnel are

affected due to this project.

This property is under the authority of Maharashtra Industrial Development Corporation

(Regional Office - Nashik) and is exclusively allocated for Industries.

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

CHAPTER – 8

RPROJECT SHEDULE AND COST ESTIMATION

Sr. No.

Heads of expenditure Expenditure Incurred till the

date of application

Expenditure to be Incurred

Total

1 Land 201 - 201

2 Site Development 46 46

3 Building/Civil Works -

1) Factory - 250 0

2) Administration -

TOTAL - 250

4 Plant & Machinery -

1) Imported - 0

2) Indigenous 40.56 681.44 722

5 Laboratory Equipments - 25 25

6 Deposits, Statutory fees etc 6 20 26

7 Miscellaneous Fixed Assets 10 10

8 Pre-Operative Expenses -

a) Manpower cost during Construction Period

- -

b) Interest during

c) Construction Period

- -

9 Effluent Treat Plant 50 50

10 Contingency - 25 25

11 Margin money for working capital

- 75 75

TOTAL 293.56 1136.44 1430

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Pre-Feasibility Report of

M/S Galaxy Laboratories Pvt. Ltd, an intermediate manufacturing unit for API and

speciallity Agro chemicals (Newasa)

CHAPTER – 9

ANALYSIS OF PROPOSAL

(FINIAL RECOMMENDATIONS)

Due to implementation of proposed chemical unit the people of nearby areas / villages will be

benefited by way of generation of direct as well as indirect employment opportunities.

Skilled and Unskilled workers will be procured from nearby villages and for other other

employment /staff preference will be given to local villagers based on the skill, merit cum need

basis.

During construction stage approx. 150 persons will be hired. The project creates employment to

approx. 350 persons once the plant comes to the operational stage.

With the development of this plant there will be a lot of scope for more ancillary development,

which in turn will benefit the local people.

This will uplift financial and social condition of local people leading to overall improvement in

the income level of the people.

Manufacturing of furfural requires corncobs or bagasse in high tonnage which can be achieved

by providing the local farmers with seeds which will directly benefit the farmers in terms of fixed

income and cultivation of corn round the year.

Agriculture – Cooperative Society will be formed, wherein the farmers will be benefited and

there will be growth in agriculture.

Corporate social responsibility will be taken up in the form of setting-up school, hospital,

recreational activities (playground) for villages by Galaxy.

Hence, there will be an overall upliftment of socio-economic status of the people in the area

with the implementation of the project.

Manufacturing of furfural, furfurylamine, furfuryl alcohal in India will avoid imports from

international markets. The country will be self reliant thus reducing dependability of Indian API,

allied manufacturers on International market and forex (foreign exchange) risk. And the

products have potential being exported as these products are in high demand which has

positive financial effects at national and to the regional level.

Need based survey will be carried out in near by villages during baseline data generation and

details CSR will be outlined accordingly.