SP-616 September 2006

The 10th International Symposium on

Materials in a Space Environment

&

The 8th International Conference on

Protection of Materials and Structures in a Space Environment

19–23 June 2006 Collioure, France

Sponsored by

Office National D’Études et de Recherches Aérospatiales (ONERA) Integrity Testing Laboratory (ITL)

European Space Agency (ESA) Centre National d'Etudes Spatiales (CNES)

Canadian Space Agency (CSA)

Programme Committee Chairpersons: Magdeleine DINGUIRARD, ONERA, France - Chairman of the 10th International Symposium on "Materials in a Space Environment " Jacob KLEIMAN, UTIAS / ITL Inc., Canada - Chairman of the 8th International Conference on "Protection of Materials and Structures in a Space Environment " Vice-chairpersons: Eric Werling, CNES, France Marc R.J. van Eesbeek, ESA / ESTEC, The Netherlands Darius Nikanpour, CSA/Canada Members: Johann Antonenko / ASTRIUM Germany Bruce Banks / NASA Glenn SFC Dave Edwards / NASA MSFC Alan Chambers / University of Southampton Christian Durin / CNES Barrie Dunn / ESA/ESTEC Eitan Grossman / SOREQ Cesare Lobascio / ALENIA SPAZIO Alberto Passerone / IENI-CNR Vladimir Skurat / Russian Academy of Science Masahito Tagawa / Kobe University Jean François Roussel / ONERA - DESP Organising Committee Chairperson: Alice Torgue, ONERA, France Members: Magdeleine Dinguirard, ONERA /DESP, France Anne-Marie Laborde, CNES, France Sophie Duzellier, ONERA, France Jacob Kleiman, UTIAS / ITL Inc., Canada Marc R.J. van Eesbeek, ESA / ESTEC, The Netherlands Eric Werling, CNES, France Publication Proceedings of the ‘10th ISMSE & 8th ICPMSE’

Collioure, France (ESA SP-616, September 2006) Edited by L. Conroy ESA Publications Division Published and distributed by ESA Publications Division ESTEC, Noordwijk, The Netherlands Price EUR 60 ISBN 92-9092-927-8 ISSN 1609-042X Copyright 2006 European Space Agency

CONTENTS

Foreword

Opening session Chairs: M. Dinguirard and J. Kleiman

"Capabilities of the Natural Environments Branch at NASA’s Marshall Space Flight Center" D. Edwards

"A European Materials Technology Board" J. Bosma

"Biological Contamination Control for Planetary Environment Protection" A. Debus

S1 New Materials

Chairs: B. Dunn and

"Recent Developments in Materials Research and their Possibilities for Use in Space Applications: Nano-Particle Based Polymer Composites and Ionic Liquids" A. Merstallinger, V. Liedtke, J. Wendrinsky, L. Baca, U. Fastner, N. Doerr & L. Gaillard

"In-Orbit Experiment of Inflatable and Rigidizable Structures" T. Bonnefond & S. I. Ivanov

"Incorporation of ITO Nanoparticles in Solar Reflector" S. Remaury, P. Nabarra, G. Hidden & J. Martinez Vega

E. Werling

“Self-Healing of Composite Structures in a Space Environment” R. Trask, I. Bond & C. Semprimoschnig

"Microstructural and Thermo-Optical Properties of Black Keronite Peo Coating on Aluminum Alloy Aa7075 for Spacecraft Materials Applications" S. Shrestha, P. Shashkov & B. Dunn

“Selecting Materials to Protect Inflatable Structures from the Space Environment” R. Destefanis, M. Faraud, V. Guarnieri, C. Lobascio, M. Nebiolo, R. Rampini, F. Angrilli, A. Bettella, A. Francesconi, C. Giacomuzzo & D. Pavarin

S2 New Materials 2

Chairs: A. Passerone and J. Antonenko

"Surface Modification of Conductive and Non-conductive Thermal Control Paints: Full Stabilization for Durability Enhancement in Space Environment" Y. Gudimenko, R. Ng, J. Kleiman, Z. Iskanderova, A. Grigorevski, L. Kiseleva, D. Edwards & M. Finckenor

"Development of La1-XsrxMnO3 Thermochromic Coating for Smart Spacecraft Thermal Radiator Application" X.X. Jiang, D. Mishikinis. G. Wang & D. Nikanpour

"Bimetallic Compatibility for Space Applications" A. de Rooij & L. Cavalli

"Synthesis of the Thermal Hardware Design for Vex Mission" C. Tonon & S. Penalva

S3 Charging

Chairs:

"Dark and Radiation Induced Conductivity on Space Used External Coatings" L. Lévy, B. Dirassen, R. Reulet, M. van Eesbeek & P. Molinié

"Proposed to Secondary Electron Emission and Photoelectron Emission Measurements Related to Engineering Design Optimization Guidelines and Spacecraft Charging" K. Nitta, H. Miyake, M. Takahashi & M. Cho

M. van Eesbeek and K. Toyoda

"Mitigation of GEO Satellite Solar Array Surface Charging: Laboratory Experiment" M. Cho, S. Hosoda, M. Iwata & K. Toyoda

S4 Synergetic Effects

Chairs: E. Grossman and M. Tagawa

"Beam Surface Scattering Studies of the Individual and Combined Interactions of VUV Radiations and Hyperthermal 0,02 or Ar with Fluorocarbon Surfaces" A. Brunsvold, H. Upadhyaya, J. Zhang & T. Minton

"Investigation into the Differences in Atomic Oxygen Erosion Yields of Materials in Ground Based Facilities Compared to Those in LEO" S. Miller, B. Banks & D. Waters

"Synergistic Effects of Vacuum UV on the AO Induced Erosion of Fluorinated Polymer" K. Yokota, K. Ikeda, A. Okamoto & M. Tagawa

Space Environment Effects on Fluorosilicone Rubber: In-Flight and ground Simulation Experiments A. Laikhtman. I. Gouzman, Y. Noter, E. Grossman, R. Verker & H. Pippin

"Combined Low Energy Environment Simulation of as Degradation Trend of GEO Satellite Thermal Control Coatings" W. Feng, Y. Ding, D. Yan, X. Liu, W. Wang & D. Li

S5 Contamination

Chairs: J.F. Roussel and C. Lobascio

"Optical Characteristics of Materials in a Space Environment" C. Soares, R. Mikatarian, W. Schmidl, P. Boeder & J. Alred

"External Contamination Observed on the Micro-Particles Capturer and Space Environment Exposure Device" N. Baba, M. Suzuki, I. Yamagata & J. Ishizawa

"Study of UV Enhancement of Contamination: Physics and Modeling" J.F. Roussel, A. Pereira, T. Tondu, D. Faye, M. van Eesbeek & O. Schmeitzky

"Kapton Surface and Optical Modifications Induced by Xe+ Bombardment Reproducing Interactions between Plasma Thrusters and Solar Panel" T. Tondu, Ch. Adanero-Donderis, V. Inguimbert & F. Darnon

"GAIA FEEP Caesium Ion Backflow Contamination: Preliminary Engineering Assessment" M. Briccarello, A. Passaro & F. Nania

Outgassing Process of Polymeric Composites under Influence of some Damaging Factors of Space Environment R. Khasanshine, A. Timofeev, A. Galygin, V. Kostiuk & M. Shuisky

"Overview of Contamination Modelling in EADS Astrium" C. Théroude, F. Fusero & J. Touaty

S6 Radiation

Chairs: D. Edwards and V. Skurat

“Accelerated Space Environmental Testing and Analysis of Ultra-Thin Polymer Films for Gossamer Space Structures” C. Semprimoschnig, P. Gray, M. Nehls & D. Edwards

"Computational Estimates of Effects of Sample Temperature and Radiation Intensity on the Destruction of Polytetrafluoroethylene (PTFE) and Teflon FEP Films by Vacuum Ultraviolet Radiation and Ionizing Radiation" V. Skurat

S7 Atomic Oxygen

Chairs: T. Minton and B. Banks

“Comparison of Atomic Oxygen Erosion Yields of Materials at Various Energies and Impact Angles" B. Banks, D. Waters, S. Thorson, K. de Groh, A. Snyder & S. Miller

"Atomic Oxygen Monitor Based on Carbon Actinometers" G. Galica, B. Green, P. Joshi, T. Nakamura, T. Abe, M. Kobayashi, H. Matsumoto, H. Koshiishi, T. Goka & Y. Kimoto

“Screen Printed Carbon Films for Atomic Oxygen Measurement" C. White, A. Chambers & G. Roberts

"Comparison of the Atomic Oxygen Erosion Depth and Cone Height of Various Materials at Hyperthermal Energy" D. Waters, B. Banks, S. Thorson, K. de Groh & S. Miller

"Undercutting Studies of Protected Kapton® H Exposed to In-Space and Ground-based Atomic Oxygen" A. Snyder & B.A. Banks

S8 Ground Testing

Chairs: M. van Eesbeek and J. Dever

"Critical Review of the Design of Space Environment Simulators: Lessons Learnt" J. Kleiman, S. Horodetsky, V. Sergeev, V. Issoupov & R. Ng

"Review of Methods for Determination of Thermal Emissivity" T. Rohr, C. Borrero Del Pino & M. van Eesbeek

"Investigation into Ground Simulations Tests Used to Evaluate Synergistic Effects on Materials" E. Miyazaki & H. Shimamura

"Recovery of Degradation on Thermal Control Film after Irradiation" M. Iwata

"Effect of Extreme Space Environment on Materials: MEDIASE and MESOX Solar Facilities" M. Balat-Pichelin, J. Badie & J. Sans

“Environmental Testing of Thermal Control Materials at High Temperature under High Intensity UV Exposure" S. Heltzel, C. Semprimoschnig & M. van Eesbeek

“Spacecraft Materials Test Techniques Utilising High Power Lasers" A. Tighe, M. van Eesbeek & D. Wernham

S9 Micrometeoroids and Debris

Chairs: C. Durin and A. Chambers

"Damages and Matter Ejection during High Velocity Impacts on Brittle Structures: Implications for Space Environment" Y. Michel, N. Leroux, C. Durin, C. Espinosa, A. Moussi, J. Chevalier & J. Barrau

"Synergistic Effect of Simulated Hypervelocity Space Debris and Atomic Oxygen (AO) on Durability of POSS-Polyimide Hybrid Nanocomposite" R. Verker, E. Grossman, I. Gouzman, A. Laikhtman, S. Katz, M. Freankel, S. Mamman, G. Lempert & N. Eliaz

Fracture Menhanisms of Composite Materials under Hypervelocity Impact S. Katz, E. Grossman, I. Gouzman, M. Murat, R. Verker, S. Mamman, M. Fraenkel, E. Wiesel, & D. Wagner

S10 Flight Experiments

Chairs: C. Soares and E. Werling

"Effects of the Space Environment on Polymer Film Materials Exposed on the Materials International Space Station Experiment (Misse 1 and 2)" J. Dever, S. Miller & E. Sechkar

"Analyses of the Misse Peace Polymers International Space Station Environmental Exposure Experiment" K. de Groh, B. Banks, C. McCarthy, L. Berger, R. Rucker, L. Roberts & L. Berger

"Overview of the Micro-Particles Capturer and Space Environment Exposure Device (Mpac&Seed) Experiment" I. Yamagata, Y. Kimoto, E. Miyazaki, J. Ishizawa, H. Shimamura, N. Baba, K. Imagawa & M. Suzuki

“Induced Contamination onto JAXA Micro-particles Capturer and Space Environment Exposure Device – Comparison of Predictions and Measurements" C. Pankop, K. Smith, C. Soares, R. Mikatarian, & N. Baba

"The Investigation of Thermo-Optical Characteristics of Thermo-Regulating Covers on Geostationary Orbit" A. Gorodetsky, S. Naumov, V. Borisov, S. Sokolova & V. Kovtun

Poster Papers "Materials for Inflatable Aerobrake De-Orbiting System" C. Dupuy T. Bonnefond, B. Defoort, O. Le Couls & J. Siguier

"Cold Welding and Fretting Tests on Quasicrystals Coatings under Vacuum" M. Sales, A. Merstallinger, M. Cekada & J. Dolinsek, A. Ustinov, S. Polishchuk, P. Brunet & J.M. Dubois

"Development of Thermal Control Coatings at CNES: New Black Silicone Paints" S. Remaury & P. Nabarra

"The Perfomance of Novel Polyetherimides in a Low Earth Orbit Environment" M. Stienstra, T. Dingemans & T. Rohr

"Engineering-Scale Fabrication and Space-Environment Testing for Re-Entry C-Sic Ceramic Matrix Composites and Oxidation Protection Systems Made by the Fast Sol-Gel" V. Liedtke, I. Olivares & Y. Haruvy

"Development of a High-Stable Antistatic White Thermal Control Coating and its Performance under Simulated Space Radiation in GEO" Y. Zeng, Y. Li, H. Yu, J. Shi, W. Liu & W. Feng

"The ESA Venus Express Mission – from a Materials Engineering Perspective" C. Semprimoschnig, S. Heltzel, M. v. Eesbeek, J. Williamson, A. Tighe & A. Polsak

"Space Charge Detection on Kapton® and Teflon® Polymers Films by the Open Pulsed Electro-Acoustic Method" C. Perrin, V. Griseri, D. Payan, K. Fukunaga, T. Maeno, D. Schwander, L. Lévy & C. Laurent

"Investigation of the Contribution of Charged Particles under the Radiation Belts to the Surface Dose of Spacecraft" O. Grigoryan, L. Novikov, V. Sinolits, A. Petrov, V. Petrov & V. Sheveleva

"Secondary Electron Emission and Photoemission Yields of External Dielectric Coatings used in Space" I. Montero, L. Galán, A. Pardo, P. Rios, J. Sacedón, M. Van Eesbeek & L. Lévy

"Laboratory and Numerical Modeling of Internal Charging of Spacecraft Dielectric Materials" A. Akishin, V. Mileev & L. Novikov

"Simulation of Surface Potential caused by Electron Charging in Polyethylene" H. Rehouma, P. Segur, G. Teyssedre, C. Laurent, J. Roussel & D. Payan

"Matching Space Materials to the Space Environment" M. Nehls, D. Edwards & M. Chipara

"Post-Flight Investigations on Thermal Control Material from HST" M. Moser, C. Semprimoschnig, M. van Eesbeek & R. Pippan

"Space Environment Impact on the Apparent Thermal Conductivity and Diffusivity of Spacecraft Materials" E. Litovsky, V. Issoupov, J. Kleiman & N. Menn

"ESA/TEC-QM Outgassing Database" J. Williamson, K. Jokela, & G. Van Papendrecht

"Matrex-Material Recording Experience: Materials Data Base for Space Application" P. Guigue, V. Inguimbert, l. Levy, D. Faye & M. van Eesbeek

"Space Environment Impact on the Apparent Thermal Conductivity and Diffusivity of Spacecraft Materials" E. Litovsky & J. Kleiman

"Catalicity and Ageing of Thermal Protection of Space Vehicules during Atmospheric Reentry" L. Benabdelmoumene, C. Guyon, S. Cavadias & J. Amouroux,

"Development of Hybrid Processing Routes for Ceramic Matrix Composites: Pip/Cvi Combinations" D. Jehl, M.A. Dourges, G. Couegnat, R. Pailler & A. Guette

"Study on Varietion of Offgas Test Results for a Component" S. Eguchi, Y. Matsuo, S. Tachihara & N. Takeuchi

"Analysis of the Durability of Polymeric Materials in Space - Application of Scanning Thermal Microscopy" H. Fischer & C. Semprimoschnig

"3d Modelling of Thermochemical Ablation in Carbon-Based Materials: Effect of Anisotropy on Surface Roughness Onset" J. Lachaud, Y. Aspa, G. Vignoles & J. -M. Goyhénèche

"Vault Structured Materials for S/C Lightweight Application" S. Mirtsch, F. Mirtsch, M. Stahl, O. Romberg, H. Segelke & M. van Eesbeek

"Innovative Disassembling Adhesives Research: Dismantling Structural-Bonded Joints" M. Olive, P. Dalet & E. Papon

"Coefficient of Moisture Expansion (Cme) and Thermal Expansion (Cte) of Printed Circuit Boards" A. Poenninger & M. Kiniger

"Cold Spray Coatings for Polymer Composite Substrates" A. Sturgeon, B. Dunn, S. Celotto & B. O’Neill

"Outgassing Effects of a Kapton Acrylic Adhesive Tape" A. Laikhtman, R. Verker, I. Gouzman, Y. Noter & E. Grossman

"Development of a System for Real Time Measurement of Particle Fallout" C. Clark, D. Gibson, H. Lyall, E. Waddell, M. van Eesbeek & D. Wernham

"Contamination Induced Optical Damage in High Power Laser Diodes" O. Gilard, D. Faye, A. Aguila, F. Neumayer, P. Renucci, S. Minec-Dube, & G. Quadri

On contamination of Spacecraft surfaces by Outgassed Products R. Khasanshin, A. Timofeev, A. Galygin & A. Shachorin

"ONERA/DESP Experimental and Simulation Tools for ION-Matter Interaction Characterization at Oblique Incidence" T. Tondu, V. Inguimbert & F. Darnon

"Co2-Laser Assisted Atomic Oxygen Beam Sources: Research, Development and Optimization of Operational Parameters" J. Kleiman, S. Horodetsky, V. Sergeyev & V. Issoupov

"Development of Small Reliable Atomic Oxygen Sensors of Polymeric Carbon Filled Resistor Compositions" Z. Iskanderova, J. Kleiman, V. Issupov, A. Chambers, G. Roberts & C. White

"Atomic Oxygen Concentration for Material Exposure Acceleration Tests in Low Earth Orbit" M. Tagawa, H. Doi & K. Yokota

"Hyperthermal Atomic Oxygen Collisions on the Mechanical Properties of High-Modulus Aramid Fibers" L. Ghosh & N. Ohmae,

"Surface Pre-Treatment of Silicone-Based Thermal Control Paints to Reduce Outgassing and Contamination in Space" Z. Iskanderova, J. Kleiman, Y. Gudimenko R. Ng, V. Issoupov & D.A. Kaute

Compact Energetic Light Particle Detector and Spectrometer G. Galica, B. Green, T. Nakamura, H. Matsumoto, H. Koshiishi, T. Goka, Y. Kimoto, T. Abe, S. Badono & S. Murata

Material Degradation of Spacecrafts due to Synegistic Environmental Effects using MC-50 Cyclotron D. W. Wim, H. Lee, D. I. Kim, Y. Huh, T. Yang, Y. S. Kim & Y. H. Kim

Probing the Effects of Molecular Structure on the Erosion of Hydrocarbon-Based Polymers by Atomic Oxygen D. Minton, D. Stockdale, D.-C. Lee, L. Yu & T. Minton

"Characterisation of Electrical Properties of Printed Circuit Board Base Laminates" A. Bulletti, L. Capineri, M. Materassi & B. Dunn

"Measurement of Thermo-Optical Properties as a Function of Temperature" A. Polsak, T. Rohr, C. Semprimoschnig & M. van Eesbeek

"About Adequacy of Ground-Based Tests of Polymers at Higher Atomic Oxygen Energy (20-30 Ev)" V. Chernik L. Novikov & A. Akishin

"Space Environment Effects on Flexible Materials in LEO Orbits" G. Bitetti, S. Mileti, M. Marchetti & P. Miccichè

"Simulation Conditions Impact on Space Degradation Evaluation of Thermo-Optical Materials Properties" J. Marco & S. Remaury

"Investigation of the Degradation of Thermal Control Materials by Thermal Analysis" S. Heltzel, C. Semprimoschnig & M. van Eesbeek

"Resistance of Black Coatings under Simulated Environments" T. Rohr, C. Borrero Del Pino, S. Heltzel, M. van Eesbeek, M. Stienstra & S. Wagner

"DIRAC: An New Exo-Atmospheric Simulator and IR Imaging Facility" J. Pavie, F. Gault, F. Oelhoffen & L. Puigsegur

"Study of the Material Microstructure Stability for the Micrometeorites Protection of MIR Space Complex" E. Kablov, V.Minakov, I. Deev & E. Nikishin

"Ground-Based Tests of Thin-Film Structures and Protective Shields" L. Novikov, S. Bednyakov, I. Ermolaev, N. Pilyugin, N. Semkin & K. Voronov

"Space Debris: Analysis of Hardware after Exposure to Space" J. Mandeville, A. Moussi & J. Siguier

"The Southampton Transient Oxygen and Radiation Monitor (Storm)" D. Goulty, C. White, S. Gabriel, G. Roberts, A. Chambers & N. Ross

“Results of the Space Environment Exposure Experiment “SM/MPAC&SEED” on the International Space Station: Flexible Optical Solar Reflector” E. Miyazaki & I. Yamagata

"Results of the Space-Environment Exposure Experiment “SM/MPAC&SEED” on the International Space Station (2): Siloxane Coated Polyimide Films, and Silicone Based Paints and Adhesives" J. Ishizawa, K. Mori, F. Imai, I. Yamagata & M. Suzuki

"Characterisation of Teflon Fep (Hst, Ldef) Following Long Term Exposure to LEO" M. Fink, E. Semerad, G. Mozdzen, J. Wendrinsky, G. Hulla, R. Kolm, I. Gebeshuber, H. Störi, B. Dunn, M. van Eesbeek, T. Rohr & M. Moser

"Passive Measurement of Atomic Oxygen, UV Fluence and Radiation Effect on the ISS using Seed Experiment" Y. Kimoto, K. Yano, J. Ishizawa, E. Miyazaki & I. Yamagata

Degradation of Tension-Loaded Polyimide Films in a Space Environment: Results of the SM/MPAC&Seed Mission H. Shimamura & I. Yamagata

List of Participants

Workshop Photo Gallery