us epa region 4 yell ow bluff air study wilcox county ... · d , 08 h2s ppm cert date: r i 3 0 i...

US EPA Region 4 Yell ow Bluff Air Study

Wilcox County, Alabama SESD Project Identification Number: 11-0068

November 2010- December 2010

S02 CALIBRATION /VERIFICATION

AIR SAMPLING LOGBOOK

LOGBOOK_I_OF l_

DATES: I /7"\ /11 THRU: J/zij )/ I ,

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Wilcox County, Alabama

SESD Project Identification Number: 11-0068


THIS PAGE INTENTIONALLY BLANK

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S02 Calibration I Verification

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THIS PAGE INTENTIONALLY BLANK

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Station I.D. _'{_._BB_c-___ _

Site Description (Co~ CJL:rff,(t.. ~ ~ ~vNO ') Date: \ }-ztt}H Time: <t,.:3(:> Operator: ~ N~

I

CALIBRATION SYSTEM

Gas Calibrator ID: tf~ All 0 '15

S02 MONITOR

Monitor ID: Ef'A A--r7\z..0

SETIINGS: TEMPERATURES:

COEF: '_j b '-J INT.: 31 :-z_ c

MFC(s) Calibrated: lo I 'LI I ZPIO

Gas Cylinder Mfg.: SCdf AC)/. L.iQVIc€;&'Yi~CA

Cylinder ID: FF Ll J 8 S BKG: ~.Q PPB CHAMBER: y L( ,Ci C

RANGE: 5DD PPB CONVERTER: 3Z2- C

AVG. TIME: f.oo sec

50z. Concentration: I 0 ... 0~ ..HzS""PPM f

c.,t ,( t~ If

Cert Date: <t I 30 I ?.D 10

CALIBRATION SYSTEM S02 MONITOR I DATA LOGGER Total Flow Concentration Zero Air Cal. Gas Monitor Data Logger

Setting Setting Flow Flow cc/min. S02 (PPB) cc/min cc/min S02 (PPB) S02 (PPB)

\C\<l<i ZERO \qgq 0.00 {). z_ 0. \

\qqq- '-fov \90/ f9 3~~ ~03

\9~5 \ LJO \~ bO Zl./ ''Sl \31

\N \\\f!\ a:ruG tA\1atJ

SETTINGS CHANGED? OR NO (CIRLCE ONE)

COEF: \.\ ~:~ BKG: :).~~ PPB RANGE: Soo PPB AVG. TIME: (:, D sec

NEW SETIINGS: Note: If calibration settings changed, then you must re-verify.

of40

US EPA Region 4 Yell ow Bluff Air Study .



Continuation of field record for sample 1N vn~ Cf1\A ~ oN 1 ( Z\.f] n @¥:so

Other Notes/Sketch (Include North and Scale)

t4:f5vm5:) S~c:. ~ CS ~t5 Ta 5 uOfpb, ~S5 ~~\~ *\t) ~~lOGGr{l f:!s:S 'N'ELL~

~V}C'1Z.~ 'v~tlS S~!\.lf ~ ~N oJ~\61-f\ TO \r-1 fx6IJfV\. - \) (\?' .

Sample Team Leadcr/Samp!cr Signatmo/Dat~ ~ i I?<; I I I of 40

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Station l.D. 'fgS ------

SiteDescription \Co~ ~ ~ @({(K_ (~~J Date: \ \2'1 / U Time: q: SS Operator: C:f;J40 N~

CALIBRATION SYSTEM

Gas Calibrator 10: ~ ~ t]O "15 MFC(s) Calibrated: /0 I Z--1 I 10

Gas Cylinder Mfg.: SCalT Al6\. UQ.v·,~ kr'l'f{l{CA

Cylinder 10: ff '1 f ~5

S02 MONITOR

Monitor 10: ~A Al7lU

SETTINGS: TEMPERATURES:

COEF: L I blf INT.: 3\. \ BKG: 3.~9' PPB CHAMBER: l.( \.I .9

c

c Concentration: I D , 08 H2S PPM

Cert Date: R I 3 0 I Zol 0

RANGE: SOD PPB CONVERTER: 3Z2._ C

AVG. TIME: bO sec

CALIBRATION SYSTEM S02 MONITOR I DATA LOGGER Total Flow Concentration Zero Air Cal. Gas Monitor Data Logger Setting Setting Flow Flow

cc/min. S02 (PPB) cc/min cc/min S02 (PPB) S02 (PPB)

l q 90 ~I ZERO 1'1CJO .. \ 0.00 D. -:s~ 0, 'SZ~

\ 9~6.Y Ljoo l<io/.:~ 7cr JZfD YoS ~oz.

(,A vl8Mll ~t\ \J<a ~f(="\~()~

,....... .......... SETTINGS CHANGED? YES OR ~(No .) (CIRLCE ONE)

NEw Sttlu"'v;:r. •L 1"P."Prih;. ~ •v<v. 11 \.,<lUU"

~lA. - o ' "' -COEF: T\TTr""'

"RAN liE: PPB AVG. TIME: ~~~~- .~ ~

'---' ' - of40

US EPA Region 4 Yellow Bluff Air Study



Continuation of field record for sample _'(_~..=..:=---------------Other Notes/Sketch (Include North and Scale)

S'mple T "''" Leade</Smnpl« Signatuce/D~ \\ '0-\ \ I\

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s

c




Station I.D. Y8 J\ -----=-----

Site Description '/CCkJ)W l:>UJf+7 Tcw~ ~LL

Date: l f 2-4{11 Time: 2.: t)o Operator:~ tJ~

CALIBRATION SYSTEM

Gas Calibrator IoErA A I/O\{ S

MFC(s) Calibrated: \ D 1 "2..'1 1 IV

Gas Cylinder Mfg.:~ A\(L 4 G.V\ lJC

S02 MONITOR

Monitor 10: E:PA 9 'l..bl-\5()

SETIINGS: TEMPERATURES:

COEF: () • S5 ~ INT.: '2.'5.4-AM-uticA

Cylinder 10: ~ f L\ l <g5 BKG: 3. )7_ PPB CHAMBER: lJ L' g c

c Concentration: b · og H2S PPM RANGE: 500 PPB CONVERTER: 371 C

Cert Date: <6 I S D I 'ZD \0 AVG. TIME: k,fD sec



\ 9<ll ZERO '9<61 0.00 - /..0 - o.t

ICf<6g L.Joo I eros lc:L 17 3<63 3~\

\9<l<6 JL.Jo ,q~ 2.7 .7m \~I \38~ 5

jf\ mlt-l- ~~' ~T\ct'J

SETTINGS CHANGED? @D OR NO (CIRLCE ONE)

NEW SETIINGS: Note: If calibration setting changed, then you must re-verify.

COEF: 6. Slg BKG: 3·'' PPB RANGE: :)o D PPB A VG. TIME: f.o0 sec '"-

of 40

~· ·




Continuation of field record for sample'ff:A ..J~...L-------------


IN fll & ~\{)~'flotJ ·-n-tz_ (~~ \E)"f'(P ttfY5 {)KN ~Cl"LA11t-)~ IN~ 0\,f"\Sfo~ cf=' THZ:..LPJ~u'L c~Y~'\Jc; ~~, ~~f'()oSS NG S~To ~E~~·· ~00~~ "Sf4£l1L£., \~~\JCZ£ \S lv~ 1 ~ bf§YJT \bcC, Hz:"A\ ~ BS~ -V"~~ <ON ~C) I.\ 15 SlD'Nl1 (1\S«NG. rrf1\f \S CJJV.iCSt<l\.. '-f 1 ~ .. ~ e C.... 6t~tf \i~~ N:)S\J SJ~ IU 5 OOwb,

l,..\8:~

0 (liz__ 0-l.

---- - .......

,----- - ~

I

I

I L:::~--------'- - - J

0

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1




Station I.D. ~ -----'--'-----

Site Description '/£A-w\~ BuJr-=?=' lO'v~N \-\ALL

Date: ( jz_vt / /( Time: Ito:(£) 2_ Operator:~ ~

CALIBRATION SYSTEM S02 MONITOR

Gas Calibrator ID:~t>.. (:\1loLf:)

MFC(s) Calibrated: l 0 I -z._ I 1 I D

Gas Cylinder Mfg.:5C01T Ati- L\~v \Q<i..... l J /><'1'1\ 'L( ...... \. <:.A

Cylinder ID:W I l~S

Monitor 10: \::Pf'. lj'ZJO li:fi>


COEF: 0, 0·-;g INT.: 2G''" ~) BKG: 3- \l PPB CHAMBER: 4 L .C'\

c

c

Concentration: I 0. ot H2S PPM RANGE: pO PPB CONVERTER: ·31'l C

Cert Date: 1:> I ~o I ·2e 10 A VG. TIME: ((:,0 sec

CALIBRATION SYSTEM S02 MONITOR/ DATA LOGGER Total Flow Concentration Zero Air Cal. Gas Monitor Data Logger Setting Setting Flow Flow


\ 9c4QJ ZERO 1990 0.00 t), s-7 0,·z~

\<q(~ Lft:>o \qot~ '79 ·. \ 40\ Lt 0\

(.__A ~IES(lA-1 CN \lt ~f\CAllcN

/ .........

SETTINGS CHANGED? YES OR ® (CIRLCE ONE)

NEW· .r...--c. '-''-'•. Note: If calibration setting changed, then you must re-verify. .... COEF: ----BKG: ~tJA RANGE: PPtl -.. ·" . ..IJMF: sec -- ---

of 40




Continuation of field record for sample _'@t....-:::.-=A_,!__I_!./_z;_~~~~I}L---------Other Notes/Sketch (Include North and Scale)

Sample Team LeadedSrunploc Signatuw~~=~;;~".~ \\ "P'\ \ \)

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'

Station I.D.




-------

Site Description ---1~\N Bl.JJ'f""r\0\NN ~ Date: 1 }!5] f i Time: )7t Li.S Operator: ~ Nc:Atj


Gas C "brator 10: Monitor 10:

MFC(s) Calibra I I SETTINGS: TEMPERATURES:

Gas Cylinder Mf ... · COEF: INT.:

Cylinder ID: ~ BKG: PPB CHAMBER:

Concentration:

H21'1r// RANGE: PPB CONVERTER:

AVG. TIME: Cert Date: I I ~ Lf sec

~M CALffiRATION SYSTEM ""~ A S02 MONITOR I DATA LOGGER

Total Flow Concentration Zero Air Cal. Gas'\ \\Monitor Data Logger Setting Setting Flow Flow cc/min. S02 (PPB) cc/min cc/min SO_{(JPB) S02 (PPB)

ZERO 0.00 ~ ~ c:)/

~ '\

""' ~ ~

c

c

c

SETTINGS CHANGED? YES OR NO (CIRLCE ONE)

~ NEW SETTINGS: Note: If calibration setting changed, then you must re-verify.

COEF: BKG: PPB RANGE: PPB AVG. TIME: sec - of 40




Continuation of field record for sample _;'I:.....:Bl\:::::--.2..--------------


[:;o.NNlo~ f\'\tN~ I \-PJfL, ~ ~<;(l ~W(4: b/)([A ~ Hz..S/~<._ ~'{Ci{(_,

Sample Team Leader/Sampler Signature/Date------------

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l


Wilcox County, .Alabama SESD Project Identification Number: 11-0068


Station I.D. "f8B ------ ,. (' . . ;

Site Description ~0 ~~:; A"JE (Aar_ (~vt.J\)) U?tsrf\1 ~~ Date: \ { 1.1P{ f I Time: C\ ~53 Operator: c~ rJOAi-\-

CAUBRATION SYSTEM_·

Gas Calibrator 10:-t:eA trJ 1 oY.:E:;

MFC(s) Calibrated: lo I L.l I 10 S::o~ A lt\. U QV\ DE_

Gas Cylinder Mfg.: JN.t\"lJU LA

Cylinder 10: V\= \-{\ <35

·, } . : 502 MONITOR .. .. . . -- , A"Tl 1-zit, Monitor 10: ff~ ~fs=~ ·

....

. . -~"!-~ . \ .. . ·f ~ '· .,

' . ';


COEF: I. l /o 'j_ INT. : 34!> .. 6 BKG: 3.3<=t PPB CHAMBER:44, 9

..

c

c I <1 50-t & l\~\11 Concentration: D · Do .,.;gs PPM RANGE: SoO PPB CONVERTER:3<:_2._ C

Cert Date: <3 AVG. TIME: <00 sec


cc/min . S02 (PPB) cc/min cc/min S02 (PPB) S02 (PPB) ..

\~en ZERO (9~( 0.00 (l). (?)(!) Q, .<D3 . (, \ <\'\(t> Lt(j)([) .,qo,.9 19.fLI 4o2 399 f'\"t<l? f 40J )GSl.l Z7. b<6 \'SCf \st.s

SETTINGS CHANGED? YES OR ~ (CIRLCE ONE)

NEW SETTINGS: Note: If calibration setting changed, then you must re~verify. '; ,

COEF: ---- BKG: ____ .PPB RANGE: ___ P.PB AVG. TIME: _ _ .sec - -· of 40



November 2010 - December 2010

Continuation of field record for sample _'j'-'13:::_B-=------------Other Notes/Sketch (Include North and Scale)

~ qlb/11 ~\.J"\ ~'iefiL J~ ~At~f ~A-T~ )0~ ~ ~~11~-~G+za-D£\-:S$~-s ¥~ fo% Gf(;\~<l-'" P..~ s-~eo ,_Nest~,. c®Mt.l-'5 ~vbf1\ 8~ ~ L-ttJZ. A-1 \Z:oo ~f§L \-\- 2S -~·

. '

-(\~·~ ~~ Sample Team Leader/Sampler Signature~--=---- ) \'·. ~ \v X \\ ~ t l(

""" of 40

;\

US EPA Region 4 Yellow Bluff Air Study



Station I.D. '{BA ---=------

Site Description Ycr).)..IJW 8UJ~ frO\"JN ~

Date: \ ( U {I f Time: \ S ~'OS Operator: __,~=--· --~--'-"=----· ~-----

CALIBRATION SYSTEM

Gas CalibratoYft: f\lloYS MFC(s) Calibrated: lo 1 G I 1 I D

<.:::U:>'"f A $1._\.lt:l)$,~ ~

Gas Cylinder Mfg.: ff'"= 1 J Jg~ It:!! ,\'lkl.\

Cylinder ID: FF '1 \% S Concentration: J D_ O%> H2S PPM

Cert Date: '3 1 '?:f:> 1 --zo \0

CALIBRATION SYSTEM Total Flow Concentration Zero Air Cal. Gas

Setting Setting Flow Flow cc/min. S02 (PPB) · cc/min cc/min

\ ~ ~l. \ ZERO \'1~1.\ 0.00

) 9<64, 3 4oo \905.1_ ~ JZ.'C

lctgs_-, ll40 lqssq Zl. (JSC:,

MID c:;nJL}( -z/P/5 .SETTINGS CHANGED? YES OR

S02 MONITOR 9Z{p\..\S'O ,( -zbl''

MonitoriD:~ ~~:J.IU er


COEF: 0' 5/f INT.: L_~ , fo c

BKG: 3.\1 PPB CHAMBER: 4 3 ~ I c RANGE: $oO PPB CONVERTER: 378 c

A VG. TIME: b(/) sec

S02 MONITOR I DATA LOGGER

Monitor Data Logger S02 (PPB) S02 (PPB)

a>. J I -®,b)

~~6 4e>~

\l-f 1.1 140

GtKK r--.

~ (CIRLCE ONE)

NEW SETTINGS: Note: If calibration setting changed, then you must re-verify.

COEF: BKG: PPB RANGE: PPB AVG. TIME: sec ..__ of 40




Continuation of field record for sample -teA ~~-----------------------


<f7w ~fj\_;j ocit \~TCJ MA-/Nrfj{~c( MOO( ArT ~~M--r'tLT/ rs~os .. ~~M-'-f2.£(( ~ssw·~ .. ~ c}P/::s c\-\~ U<-x~ ~ S-n+Td) \N ClA\{J ~/--l<Jlo_) Dlr--rA [ON'J t()£()'1() ~ Sb2/ \-tzS ~8\.:1 ~ r~Uflv tl\k:O

\:1t)\J~Y r M as·JR. fJ\'10 <}'al-J'tAl ~l wrtt Olif~,

Srunple T "'"' Leadec/Samplcr SignaUrre!Oate ~ f ( ~~ (/ of40




Station I.D. -------

Site Description '/~'N tSu.Jrr~wtJ -t-1etZ.

Date: 1('2.7/// Time: l7~$r0 Operator:~ Noot1-

CALIBRATION SYSTEM

Gas librator ID: ______ _

MFC(s) Calib ed: __ __;/ __ __;/ __ _

Gas Cylinder . -------

Cylinder 10: ____ ~----

Concentration: ___ H~1 P PMM ~ Cert Date: ___ / ___ / ~ -i

"

CALIBRATION SYSTEM

S02 MONITOR

l ,j,

Monitor ID: ----------


COEF: ___ _ INT. : _ ___ _ c

BKG: ____ PPB CHAMBER: _ __ C

RANGE: ___ PPB CONVERTER: _ _ C

AVG. TIME: __ sec

S02 MONITOR I DATA LOGGER Total Flow

Setting cc/min.

Concentration Setting

S02 (PPB)

Zero Air Flow

cc/min

Cal. G~' r\ ~onitor Flow ""-! '

cc/min 1'\. 2 (PPB) Data Logger S02 (PPB)

ZERO 0.00

~ fr-----~----4----+---~-------~'~-----~ ~ - '

SETTINGS CHANGED? YES OR NO (CIRLCE ONE) ~ NEw SETTINGS: Note: If calibration setting changed, then you must re-verify.

COEF: BKG: PPB RANGE: PPB A VG. TIME: sec · ~~·-----------------------------------------------------------~ of40




Continuation of field record for sample _"f~M~~----~------Other Notes/Sketch (Include North and Scale)

,,

Lb'N('llDffJW ~~l MIN~ 1 PstJ) ~D~ ~L-Py:;> ~ ~fl\ ~ H-z:S(~oc_ ~rz~-f.\ ~~ \7:30~

Srunple Terun Le•dcr/Srunplcr Signature!Dat~ ·. ~ ~ \ \ "Z/ "\

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'

'

: ..




Station I.D. 'f8g ---'-------

SiteDescription ~~ ~~ ~1€ ~(~)~lN~0

Date: ( { Z -J{r I Time:. \!:so Operator: ~ Nt:¥z:tt -==-~--~-~-~-~----

. ..


GasC ibrator 10: Monitor 10:

MFC(s) Calibr ed : I I SEITINGS: TEMPERATURES:

Gas Cylinder M .; COEF: INT. : c

Cylinder ID: ~ BKG: PPB CHAMBER: c

Concentration: H~ RANGE: PPB CONVERTER: c

Cert Date: I AVG. TIME: sec I '~ .. ~~

CALIBRATION SYSTEM ~ M S02 MONITOR I DATA LOGGER Total Flow Concentration Zero Air cru~

~~ Monitor Data Logger Setting Setting Flow Flow

cc/min. S02 (PPB) cc/rnin cc/min A02 (PPB) S02 (PPB)

ZERO 0.00 ~ I

~~ ~

{

""' ·c._ ~

~ -. " SETTINGS CHANGED? YES OR NO (CIRLCE ONE)

~ NEw SEITINGs: Note: If calibration setting changed, then you must re-verify.

COEF: BKG: PPB RANGE: PPB AVG. TIME: ..__.,..

of 40




Continuation of field record for sample _'f_bfJ ________ , ·_, _____ _

Other Notes/Sketch (In~lud'e North and Scale)

S-le Team Leade</Samp!cr Signatuno/Da~ L \ z:r (II

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Station I.D. _'f@-'--..::.· · ___ _

Site Description tfD~u ~24Z.-~ ~(~cQNJ ')~#b Date: \ lzcz/ II Time: C1 ~ 0() Operator: cd'tfb N~

CALIBRATION SYSTEM

Gas Calibrator IO:gA ~ J I 0 '1 S MFC(s) Calibrated: I 0 I 2-/ I 'ZD} 0

S:...d\ fA\<t u QIJ\\)£ Gas Cylinder Mfg.: Af./10(2.J..Gt4

Cylinder 10: ~ L1l<ZS5

4 S02 MONITOR

Monitor 10: . · Effi A l"li <: (p

SEITINGS: TEMPERATURES:

COEF: l J C, Lf INT.: 3\~3 c BKG: 3.'10 PPB CHAMBER: L( L-f • C) c

I · <Sat- ~ , )zl>)J) Concentration: 0 ..c:?6 1;:12S'PPM RANGE: 5 C) 0 PPB CONVERTER: 32Zc Cert Date: $ I 3o I 2f:? I 0 A V G. TIME: (cfl) sec



\q<lz.. ZERO )cyz 2_. 0.00 <!),. (7)1 ({),0

l q2{0 ~ LJc;R> \C(C6 7 '1_ lq .\3 \...{o3 L~oLLY

19~~.4 ll\@ jq<)7. <g L/Jo~ lsb,"3 157.0

A ~5T UD'i '{~ ~~\ Vf\)1 ON SETTINGS CHANGED? YES OR (CIRLCE ONE)

NEW SEITINGS: Note: If calibration setting changed, then you must re-verify.

COEF: ---- BKG: _ ___ PPB RANGE: ___ .PPB AVG. TIME: __ sec

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Continuation of field record for sample -~_:__(5_8-=-------------Other Notes/Sketch (Include North and Scale)

~ S-r\JG-f 'Vw~\a:r\\~ ~·£D o!c ~ ()ZtOTffi \0 Q~r: ~~7U{l -J~ o~-<Atl € ift Mfflv~f'11f1r!Vt 11 too, \:AlAr ~~<i0 ~M ~ W(-,0CCQ.:

Srunplo Torun Leadcr/Samplcr Signature/D~~ \ l zg I \ I

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b




Station I.D. _Y-l--8-==---...!...-f:\-=----

Site Description '/~~ BLUfF T~~ ~

Date: 1{2-<3{[( Time: J(:L{5 Operator: ~ NO~H I

CALIBRATION SYSTEM

Gas Calibrator 10: t:f>A 77ct''i2 S02 MONITOR

MFC(s) Calibrated : \ D I "ZI 1 ZP ( 0 x.o-rr A\CC u~ u1o~

Gas Cylinder Mfg.: &Mffl.c.A Cylinder 10: (f L11 <6 5

Monitor 10: -E'fA '\'ZCo4~

SETTINGS : TEMPERATURES:

COEF: ([), S l~ INT. : 7.9'. 4 BKG: S.(8 PPB CHAMBER: 4). \

c

c t (]) o "":)Oz (., \\u.{u

Concentration: \({) • 1 D rt2S..fPM RANGE: _5oO PPB CONVERTER: 376 C

Cert Date: f:> 1 --z_:,o 1 '2:D t 0 AVG. TIME: CQQ) sec

CALIBRATION SYSTEM S02 MONITOR I DATA LOGGER Total Flow Concentration Zero Air Cal. Gas

Data Logger Setting Setting Flow Flow Monitor S02 (PPB) cc/min. S02 (PPB) cc/min cc/min S02 (PPB)

\q<bs.eo ZERO ~'l~S.Co 0.00 - &. s -([). 6

\ q~"3.S 4(1)({) \<i CG, .5 71./" '-<~5.0 '-t0<!)

\~<65:1- (Lf(Z) '957.~ 2.7.~~ \37.~ \~7

EN QoF"'3" JtfOj d 'P/5 ~ '-

SETTINGS CHANGED? YES OR (CIRLCE ONE)

NEW SETTINGS: Note: If calibration setting changed, then you must re-verify.

COEF: - --- BKG: PPB

--~-RANGE: ___ PPB AVG. TIME: __ .sec

of40




Continuation of field record for sample _\f8A..,__,_~'-------___.:.. _____ _ Other Notes/Sketch (Include North'and Scale)

hJfN-fzr.A f~sw z/f/5 uZxTW~% 60TUtJ£G \tl ---riK bAff>. AN~£a ~~ 6Cf?- t- \ N'E. l¥t1f" ~~~ ( MA=t"t::L 'f ( l1 :"So . ~A

. . .

jN'OJJD\-N6 ~~' \'1\lt-~V\t., ~ ~<;(. ~~

~ t):J\J'IN\D~, I •

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us epa region 4 yell ow bluff air study wilcox county ... · d , 08 h2s ppm cert date: r i 3 0 i...

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