u.s. polymeric

I f

,t

U.S. POLYMERIC

HITCO MATERIALS DIVISION

([_ASA-CL_-179_I17) FXliC-EEi_'5.Xl_'J. 'XES_ CATA[_,_,(Jb'l.: }H 5E3q LC2 tiC,. 2 ([]5CC) 1_3 F

CSC L 1 IB

G3/27

_189- 13_. 0,_

FM 5834 LOT #2

D-09275

FINGERPRINT TEST DATA REPORT

NAS8-36298 COPY # 9

of 2

FILLER TESTING

NAS8-36298

U.S. POLYMERIC O.E. 71108

F iller _05 for NASA _ot#

I. Carbon Content, Z

QAI-5560_AMP_E

*2A-i *2*-2 .2A-399.31 99.18 99.40

NASA LOT# 2 AVERAGE 99.30

2. Ash Content, XPTM-71B

0.0 0.0 0.0

0.0 o.e 0.0AVG. 0. • 0. • 0. •


3. Atomic Absorption, ppm

CTM-53B

(Values are average of2 determinations)

#2A-I #2A-2 #2A-3 LOT#2

__ AVG.Na 7.0 7.5 9.0 7.8

K 1.5 1.0 2.5 1.7

Ca 2.5 1.5 2.0 2.0

MO 0.0 0.0 0.0 0.0Li 0.0 0.0 0.0 0.0

TOTAL 11. • 10. • 13.5 11.5

3a. Moisture Content, XCTM-53B

.041 .034 .039

AVG. .036 .027 .042

NASA LOT# 2 AVERAGE .035

3b. Ash Content, X

CTM-53B

0.005 0.000 0.015

0.000 0.025 0.000AVG. 0.003 0.013 0.008


4. pH, Units

ASTM D1512

4.60 4.40 4.50

AVG. 4.60 4.50 4.60


5. Particle Size, microns

S.E.M. procedure

(Average values areof 20 determinations)

AVG. .56 .57 .52

Maximum .90 1.25 1.17

Minimum .23 .20 .25

Std. Dev .22 .28 .24

NASA LOT# 2 AVERAGE SIZE .55

6a. TGA, *C at 50% Loss

CTM-51

842 850 857

NASA LOT# 2 AVERAGE 850


700 E. DYER ROAD, SANTA ANA, CALIFORNIA92707 * (714) 549-1101 * TWX (910) 505-1130 * FAX # (714) 549-2858-5-2437

of 2

Filler Lot _or NASA Lot# 2

6b. TGA

CTM-51

See Charts 6A-6C

7. Particle Size Distribution

CTM-72See Charts 7A-7C

7a. Partlcle Size, micronsCTM-72

2A£_ _ #2A-3.86 .97 .95

.e5 _ .92AVG. .86 1.02 .94


U.S. Polymeric

Hmmld M. Qurmlshl, Mmnager

Ouallty Assurance Department

J CHART 5A

ORIGINAL PAGE I$

OF POOR QUALITY

!

r!i

/

ORIGINAE P A"G-_.

OF POOR QUA.L,I'I-_,

CHART 6B

J

OP_C..NAL PAGE ._

Oi\ POOR (_UALI'I'Z,

CHART 6C

I

T

OB .POOR QuALi,r,r

"- _ _ _ _ _ ,..; _ ...;

• ,o _ _ _ , , , _ -.

_ _ _.'-'_.

L_

CHART 7A

V *

iJ

Z

_ _T,_!

_ _ _' _,., _ _., __._!

r.._ _,0_ _ _ "-

z

41,

ORIGINAL PAGE 1_

OE POOR QUALITY

ORIGINAL PAGE IS

OF POOl{ QUALITY.

o.--

z

t---

o.--L1"n

4IF

. • . .

...,..

cr _,

• . . • . • • . . :=1.

.-: , , , _ , _ _, , , , v

,._ ,_ - _

y.. _ ,'NI_ _'''

CHART 7C

..,-I

- rI ,q

E

!" I_ _r-,. I

i

JI

_._ --i._'i--i i 2 L , , •sr IZ, --

i-,-

-.,.a

=l.

v

i,l.I....a

o--

Z

i---

0'---I,,p'l

. o . . .

._o .

_r

v

gl_'_

l Qi i m m _

v

o

N

,II.

¢_ I,--

• • • . . • {=r,:,

J,;.,,{,,

p-!

[',i l

! :

. i

_2

_. -k iT

_' -±__ : .... _._e_ ,.-

TEST

6

2.

3.

4.

5.

6.

7.

8.

9.

10.

II.

12.

13.

14.

15.

TABLE OF CONTENTS

RESIN TESTING

NAS8-36298

U.S. Polymeric O.E. 71108

91LD Resin Lot for NASA Lot# 2

PAGE

Resin Solids ...................................... I

Specific Gravity .................................. 1

Brook_ield Viscosity .............................. I

Gel Time .......................................... 1

Atomic Absorption ................................. 1

Gas Chromatography ................................ I

TGA ............................................... 1

DSC ............................................... 1

HPLC .............................................. 1

GPC ............................................... I

pH ................................................ 2

Phenol Content .................................... 2

Chang's Index ..................................... 2

RDS ............................................... 2

NMR ............................................... 2

CHARTS

Gas Chromatography .................................. 6A - 6C

TGA ................................................. 7A - 7C

DSC ................................................. 8A - 8C

HPLC ................................................ 9A - 9C

GPC ................................................. 10A - 10C

RDS ................................................. 14A - 14C

NMR ................................................. 15A - 15C

RESIN TESTING

NAS8-36298

Page 1 of 2


I. Resin Solids, X

PTM-7C

91LD Resin Lot for NASA Lo_# 2

AVG.

#2-1 #2-___22 #2-370.8 70.4 71.7

70.8 70.2 71.2

7 1 ._..._9 72 ._.___00 7 • ._.__.5571.2 70.9 71.1

Lot# 2 AVERAGE 71.1

2. Specific Grsvlty @ 25-C

PTM-29C

1.141 1.140 1.139

Lot# 2 AVERAGE 1.140

3. Viscosity, Brookfleld, cps. @ 22.8°CPTM-14C

1250 1250 1500

Lot# 2 AVERAGE 1333

4. Gel Time, mln:sec

PTM-47B

3:30 3:38 3:34

Lot# 2 AVERAGE 3:34

5. Atomic Absorption, ppmCTM-53B

Ca

Mg

LIAVG.

Ns 4

K •

3

I

08

#2-2 #2-3 LOT1 AVG

4 8 5.3

• • 0.02 2 2.3

1 1 1.0

_ 0.__338 11 9.0

6. Volmtlles, Gas ChromatogrsphyCTM-55

See Charts 6A-6C

7. TGA, X Weight Loss st 500"CCTM-51 (AIR)

#2-1 #2-2 #2-3

39.5 40.1 39.4

Lot# 2 AVERAGE 39.7

See Chart 7A-7C

8. DSC, temperature "C

CTM-50A

183 191 183

Lot# 2 AVERAGE 186

See Chart 8A-8C

9. HPLC

CTM-49A

See Chart 9A-9C

10. GPC, Average molecular wt.CTM-49A

1718 1801 1598

Lot# 2 AVERAGE 1706

See Chart 10A-10C

(_ HITCO MATERIALS DIVISION700 E DYER ROAD, SANTA ANA. CALIFORNIA92707 • (714) 54_1101 = TW_ (910) 59_1130 . FAX # (714) 54_285_2437

o£ 2

91LD Resln Lot £or NASA _otl 2

11. pH, units

CTM-1B#2-1 #2-2 #2-38.5 8.3 8.4

Lot# 2 AVERAGE 8.4

12. Phenol Content,

CTM-55 Appendix I

AVG.

1o. o4 11.09 _1.74Ao. so ll. e8

9.94 10.94 11.81

Lot# 2 AVERAGE 10.90

13. Chang's Index, ml.

CTM-5B

24.2 24.8 25.2

Lot# 2 AVERAGE 24.7

14. RDS, Minimum Viscosity, cps.CTM-57A

Mln, Visc. "C#2-1 278 107

#2-2 249 111

#2-3 239 113AVG. 255 110

See ChRrts 14A-14C

15. NMR

Vendor procedure

See Charts 15A-15C

U. S. Polymeric

Hmmid M. Quraishl, Manager

Quality Assurance Department

ORIGINAL PAGE 1_

OF POOP, QU,kLITY

TYPICAL GAS CHROMATOGRAPH SET-UP

ColumnLength 6"_,

Dia._Liquid _ase_It. S _._

|upport_

Carrier Gas -IJ-,tP_

htemeter

Inlet Prss___llPSi |Irate /Din

CflARTSPE_D....s_za[_Siz,_

hieDetector "FT_

Vo I taleSensi t. ,,

Flow Itateso.,pl/mi n_tlydro|en _ Ai r_$cavln|!

Split

Tmper_u rej, el;

Det. _ I_Column InitialFinal ,.2/Q I,.te_ I

Solvent ,'/__J_'... , _ J

conch..(z.,.J__.._._./_

GAS CHROMATOGRAPHY STANDARD SOLVENT

TEST METHOD CTM-55

STANDARD SOLVENT/MONOMER RETENTION TIME (MINS.)

MEOH .6

ETHANOL i,18

MECL2 1.28

ACETONE i.45

IPA 1,83

THF 3.O8

ACETONITRILE 3.2

CRESOL 4.O3

MEK 4,O8

FURFURAL 15,03

TOLUENE 17.98

CHLOROBENZENE 19,6

PHENOL 22,08

NOTE: THF WAS USED TO DILUTE THE RESIN SAMPLES.

ORI'G.rN'AL F'AGE KS

OF POOR QUALITM

•-%:_ REAL TIME CHROMRTOGRH_I :I.i.%

F--

f

f ---_

L

L ", \L

._..IN_L FULL SCALE MV =1008.08

SAMPLE' _I LD 2-1diS:C: C=011017E, 1Gt_._/ML

TIME II :49")RTE 12"I E_,E:6]F'ERATOR : .JGZ

RUN TIME:)ELAY TIME'":H At..I: 0

38.00 MINUTES13.00

_'I:: RET PEAK AREA E: _EAK'10. TIME AREA _. L HT.

2 ._5 17_95 1.70 204140 9

SIC5 2010908 B47 _ _= 1_37

39 22 05 162080 6

T OTFIL FIREB= 2:3E:26_ 1"tHRESHOLD= 1MI_q F't:: WIDTH= 15_I;'EA REJECT= 10E,0

075 2' 2355_ 2 11953397 3 84306,065 4 127093 2 96802 1 a700

UEFFTICRL SCALE

CHART 6A

F_CTOF'- 1Y

5_

6_

• I

19_

p

c-

SAMPLE: 91 LD 2-I

M Isc. : c=o. Ie_7_;1et$/l_.

TIME: 11:49DATE: 12/10/88OPERATOR: JGZ

_LIN TIME: 30.00DELAY TIME' 0.00CHAN: 0

MIHUTES

FK RET PERK RRER BNO. TIME AREA _ L

PEFII..HT.

5 1.70 204140 e.seE;6 3.05 2010908 04.594

39 22.05 162080 6.s18

TOTAL AREA= 2377120THRESHOLD= 1MIH PI::.WIDTH= 15RRER REJECT= 2300

2 I195S3 843061 $700

;)RIGiNAL FACE -c

OF. POOR QUM.ITY

Fr

PEFiL

I

r

I-

L__,

LL

L \L\

FINAL FULL

T I ME CH_TAMATO_.3RF.tM ,f::_;f:

SCALE M',.'.=IO0O O_

""_E,RMF'LE:

MISC:_1 LD 2 _-

"q JC=O. 101 _,-_IIg/ML

TIME I,::1.DATE 1.':--'.."10./8 t-OPERFIT "IR : .IG."

_.:I.tt4TIFIE: 30.00DELAY TIME: 0.00C.HRt4: 0

M I t,tLtT ES

PK PET PEAK AREA BNO T IME AF:ER % L

PEAKHT.

24 15 16 27 38 59 6

10 61E: 112.5 le_34 71.7,5 22

.6E: 1634

.43 185470 135890

.93 119280095 41333_,.., _E:..2_7 942558 939875 1060145 119498 10446015 197270

095108

7 93969 685

2 415342551549619070

6 1_7II 525

TOTAL R_:ER= 171171_TH_'ESHOLD= IHIN P_. NIDTM= 15_RE_ REJECT= I_00

3 14_o 2072 101813 72100

,_4 .E ....4 3544 2494 189I 5472 39_ 100153 9916

CHART 6B

VERTICAL SCALE

6_7 "--

10_

18_

25_

FFICTOR : I"g,

I

L

(

SAMPLE : -_J LD ."-',.MISC. • C:O. 101.',-_/HL

TIME: 16: I.-DATE" 1"=',."IA.."E;_._OF'EPRTOR : JGZ

RUH TIME: 30.00DELAY TIME: O.OOC:HAN: 0

M INUTE$

Pt( RET F'EAK AREA E:NO TIME AREA % L

PEAKHT.

=,., 1 . 7EI 135890 8 . 1,-?_5-', l'_"°c'c_ 71 350

7 3.95 41333 _ 47234 21.98 104460 _.,249

-_ 97 .35 2z.15 I 270 11 80_

IOTPL AREA= I¢71753THRESHOLD= IMIN.PK.WIDTH= 15AREA REJECT= 11000

'2 161E:13 721004 5852 10015

Q_I6

_.I_l: REAL TIME CHPOMATO_PAfq

ORIGINAL PAGE

OF POOR. QUALITy

VEFIT ICAL

CHART 6C

SCALE FHCTOR: 1X

wm •

L ,

FINAL FULL SCALE M)..) =1000.0(_

_,_h,-."._ " _1 LD 2'-_,r,11S F. C= 0. 1012 _, _;4_;/Ml.

TIME 16:5-_DATE 12.'10.-86,7PEg'ATO_: : .IGZ

_:UH TIME: 30.00DELAY TIME? O.O0f'.HAN : 0

M INUTES

F'}.i RET PEAK AREA E:N.A TI ME AREA :. L

PERKHT.

2'4 15 1

7 38 59 6

lC: 1 !_S "22

40 22

_ 420445 1258_ 81270 283 196320 528 2E;99700 8460 2293O_ 146483 614003 54263 115 165300 4

TOTALTHF'E$MI_R F_PEA

AREA= 3412211H i"lL D= 1t::. 1,_]DTH= lgRE JEC:T= 1000

12'3 3 435037 2 I"_.382 2 I14_5753 2 11447980 3 85372067 4 251043 4 69180 3 248590 2 9873844 3 9807

gAMFLE: 91 LD 2-3MISC. C=0.10126_M_/NL

TIME: 1_:58DATE: :2.."10.-.'8_OF'EF:RTOP: JGZ

RUN TIME: 30.00DELAY TIME: 0.O0CHAH- 0

MINUTES

PK RET PEAl:: AREA E:NO. TIME RPER % L

5 1._8 _1270 2.393 2g 1.83 196320 5.779 27 3.28 2899700 B5.364

39 22.03 54263 1.597 240 22.15 165300 4.86_ 3

TOTAL AREA= 3396853THPESHOLD= IMIN.PI_ WI[,TH= 15AREA REJECT= 6200

PEAt:.HT.

I14_5114478537298739807

_,._ CHART 7B

ORIGINAL I'I_GE IS

OF POOR QUALIT_ . . t::)

QC _l.LIj ',,e" ¢0ZCf) COLI.I,-',I"- '_LD r'l ,,_ COW QIN

ll_ O O IE

.p ,.-I Z a,o --, "_ //- . /©

O rl U= l}.

4a _.._ +CO ,-J

- /"-J-/ " I

"i'%1

N_c) o, pI , two .o/ uJF-_ "_

_.-, i 0 < t:l:: II "_ ! -r m . _ i- li_l

_1 _'z. -/ _. cn F-- u') + bJI

._m,.,,."_<4 e .,,'¢ e _ I-_

E N C _ ,_, .... ,--, C:) C} Lr) 0 C:) 0 U') C:) C:) C:}0 "* _) _ lt_l (_ _-* i..l _ _..'_ . * •

.... C:) C:)

CHART 7C

.... OR/_I'NAL +PTTGE 1FSCHART 8B

+ Ii I

lull

C7:C

iiii

iNJ

L..ll,.d_ --

l-I.If_l

:::CC

iiiii!!!!!

IiI_II111

: : ." : :

: : : C C

', ; C : C

L : : : :

: : : : :

." : : :

:i::

=7::

: : : ?

iiii

1t0

CHART 8C

• I ,

iiii i i

::4

ii;

2". :

'it.-t-_,

:11

::?

iii

iii11|

CHART 9A

_" A FILE A:PHENO39. HDR TAKEN 09-05-1986 16:56:50

--******** AREA PERCENT REF'ORT

_, ****************************************************************************

Sample Name: 91LD,2-1,C=6.85 Operator Initials: OGZ *

hate: 09-05-1986 16:56:50 Method:F'HENOLIC DATA FILE: A:PHENO39. PTS *

nterface: 4 Cycle#: 39 Channel#: 0 Vial#: N.A. *

• _tarting Peak Width: 10 Threshold: .01 ********************************************************************************

Instrument Type: BECKMAN HF'LC Column Type: MICROBONDAF'AK C-IB *

Solvent Description: THF/WATER, 2:1 BY WEIGHT *

Operating Conditions: R.T., FLOWRATE=I.5 ML/MIN *• Detector O: 220NM/.5AU Detector 1: *

Misc. Information: LENGTH=25 *

*******************************************************************************

Starting Delay: 0.00 Ending Retention Time: 10.00

:'_ Ret Peak Area B Peak Normal iz ed Area/

Wo. Ti me Area % L Ht. % Hei ght

1.78 120482 75.1672 2 5050 100.000 2_c.9

4 2.05 39804 24.8328 2 4045 33.037 9.8

Tc al Area: 160286 Area Reject: 10C)0 One sample per 1.000 sec.

t_

Il,U.J

UIn

"I-

M

T

ID

u_

Iill_I

In

0..I

00

cl

ot-

I,,I

Z_

O_o_,0

0

JZ

XN

I,Lm

Z |t_UZ

IiJ 1_IN

"d_MI--

FILE A:F'HENO38.HDR TAKEN 09-05-1986 16:40:05

CHART 9B

******** AREA PERCENT REPORT ********

Starting Delay:

P; Ret

No. T i me

_ ****************************************************************************

_ample Name: 91LD,2-2,C=6.77 Operator Initials: JGZ *Date: 09-05-198616:40:05 Method:PHENOLIC DATA FILE: A:PHENO38.FTS *


tarting F'eak Width: 10 Threshold: .01 *

Instrument Type: BECKMAN HF'LC Column Type: MICROBONDAFAK C-18 *


Operating Conditions: R.T., FLOWRATE=I.5 ML/MIN *

Detector O: 220NM/.5AU Detector 1: *


*****************************************************************************

0.00 Ending Retention Time: 10.00

Peak Area B Peak Normalized Area/

Area % L Ht. % Height

1.7B 121012 74.99642 5109 10D.000 2,.73

4 2.05 40345 25.00362 4092 33.340 9.9

___.al Area: 161357 Area RejeEt: 1000 One sample per 1.0()0 sec.

X

d

IW_I

um

Z

Z

gz

0

IW.J

u

)B0.J

ff

0o

d

ON

01/3

,COC)

J1-

Z_01.1

IJ.

ii)

ZiWuZA. •

W 1.JND,4

Q_

ORIGIN'AL PAGE IS

OF POOR QUALITY

CHART 9C

-r r 67 opening raw data file A:LASTRUN.PTS53 creating file A:PHENO40.F'TS at line 4620

.,_ FILE A:PHENO37.HDR TAKEN 09-05-1986 16: 04:07

•_ ******* AREA F'ERCENT REF'DRT ********

_mple Name: 91LD,2-3,C=6.79 Operator Initials: 3GZ *I _te: 09-05-1986 16:04:07 Method:PHENOLIC DATA FILE: A:PHENO37.PTS *

Interface: 4 Cycle#: 37 Channel#: 0 Vial#: N.A. *

Ftarting Pea_:: Width: 10 Threshold: .01 *.. ****************************************************************************

_nstrument Type: BECKMAN HPLC Column Type: MICROBONDAFAK C-1B *


Operating Conditions: R.T., FLDWRATE=I.5 ML/MIN *

Detector 0: 220NM/.5AU Detector 1: *


. ****************************************************************************

;t _ting Delay: 0.00 Ending Retention Time: 10.00

:'k Ret Peak Area B Peak Normal ized Area/

_o Time Area % L Hr. % Height

1.78 121706 75.2396 2 5098 IC)0.0[)0 23.9

2.05 40052 24.7604 2 4076 32.909 9.8

F_tal Area: 161758 Area Reject: 1000 One sample per 1.C)00 sec.

t,.

)

!W

!

)

Z

r

d

I_J

I

2mC3,J

Z

00

d

ON

X_

OLO

0

.JX

X%O_

odZ ItlluZ

_Jt--

a_

L

oRIGD{_J_ P.AGg lg

OF EOOR Q_:AI,ITY

I

GPC CALIBRATION PLOT

*** Calibration Data ***

Calibration Name:

Mist Information:

Fit Type: 3

Lo9 Mo] Wt = A + B× + Cx^2 + D×'_3

Az 2.538977 B= 2.115815 C= -.5646824

Coefficient of Determination: 0.9902

Ret Time Molecular Weight

o

D= 3.606432E-02

Log Mol Wt

3.50 35000

4.33 15000

4.B3 3600

5.09 2350

6. O0 570

7. 17 92

7.50 72

Log Mol Wt GPCC_I,IBR_TIONPLOT

185

418

318

218

m

4.544

4.176

3.556

3.371

2.756

1.964

I.$57

m

m

I

D

m

I I I I I1

18 2.8 3.8 4.! 5.8 6.9Jleiention Time or Vol-,e

?.8

m

m

m

m

ORIGINAL PAGE IS

OF POOR QUALITY CHART 10A

" A FILE B:GF'C28 .HDR TAKEN ()8-C)5-1986 17:13:56

* Sample Name: 91LD 2-1 =2.68 Operator Initials: GBF *

* 9ate: 08-05-1986 14:C)5:42 Method: DATA FILE: B:GPC28 .F'_S *

* interface: 5 Cycle#: 28 Channel#: 0 Vial#: N.A. *

* _tarting Peak Width: 60 Threshold: 0 *********************************************************************************

* Instrument Type: HF'LCIBECKMAN Column Type: UL_RASTYF:AGEL 500A

* Solvent Description: THF *

* Operating Conditions: T=35C FLOWRATE=2.0ML/MIN *

* Detector O: 254NM/.1AU Detector 1: *

* Misc. Information: CALIBRATION/GPC *

*******************************************************************************

S+ artir,g Delay: O.C)OC tibration file: GPCPHEN

Mulecular Weight Distribution Averages

Baseline TIMES: 3.85 to 10.00 MW:

P _cess .TIMES: 3.85 to 10.00 MW:

T tal Area: 196902

Mw= 1718

M- = 370

M /Mn= 4. 6439

Mz= 4134

1501

Ending Retention Time: I0.()0

22295 to 2

22295 to 2

Mol Wt 5 418 IB

3 2IB 18

OR. _ _,.ml'A_ v, _._,-

OE FOOR QUA/.Zl_. CHART lOB

4 _ FILE B:GF'C22 .HDR TAKEN 08-05-19B6 17:18:27

oample Name: 91LD 2-2 C=2.b8 Operator Initials: GBF *

Date: 0S-05-1986 11:5B:33 Method: DATA FILE: B:GPC22 .PTS


tartir, g Peak Width: &O Threshold: 0 *

Instrument Type: HPLC/BECKMAN Column Type: ULTRASTYRASEL 500A *

Solvent Description: THF *

Operating Conditions: T=35C FLOWRATE=2.0ML/MIN *Detector O: 254NM/.1AU Detector 1: *

÷ Misc. Information: CALIBRATION/GPC *

_. ****************************************************************************

Starting Delay: 0.00 Ending Retention Time: 10.0£)

Se ibration file: GPCPHEN

Qc ecular Weight Distribution Averages

Baseline TIMES: 3.85 to

or_cess TIMES: 3. B5 to

Tc al Ar_: 240471

lw_ 1801

_n= 36B

M_ Mn= 4.8q45

M_ 4352

_ 1573

10. O0 MW: 22295 to 2

_oo_ t 0 210. C)O MW : _-_..-,

Mol Wt 518

418

Lo_ Mol Wt v:. l_eaz-6umx

3 2 118 18 18

CUB %

188

?5

56

Z5

69

18

CHART IOC

* 3ample Name: 91LD _ _ C=2.68 Operator Initials: GBF *

* Date: OB-O5-19B6 11:28:37 Method:GPC DATA FILE: A:GPC20.PTS *

* Interface: 5 Cycle#: 20 Channel#: 0 Vial#: N.A. *

* Btarting Peak Width: 60 Threshold: .01 **********************************************************************************

Starting De2 ay: 0.00Calibration file: GF'CPHEN

Instrumer,t Type: HF'LC/BECKMAN Column Type: ULTRASTYRAGEL 500A *

Solvent Description: THF *

Operating Conditions: T=35C FLOWRATE=2.0ML/MIN *

Detector O: 254NM/.1AU Detector 1: *

Misc. Information: CALIBRATION/GF'C *

*****************************************************************************

Ending Retention Time: I0.00

Averages

10.00 MW: 22295 to 2

10.00 MW: 22295 to 2

M tecular Weight Distribution

B_aeline TIMES: 3.85 to

Process TIMES: 3.85 to

T Lal Area: 271362°.

M = 1598

Mn= 260

M,-,/Mn= 6.1449

M = 3922

My= 1389

25

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5 I. 022e+002 9.49C_e+001 3. 799e+001 I :2B2e+OCll #. O00e+O00 "..._600e+O01

6 I_.971e+001 Bi175e+O01 "3.igBe+OOX--1.'125e+OO1---51.'OOOe-+-O00 ---'..8r_Oe_-_}K__-.P

7 "7.W26e÷OCil 7. OE_7e+(iO J 3. 550e+001 9. 945e+000 6. O00e+OOCi 4. O00e+OOi

E_ &. O97e+O01 ,6.O03e+O01 3. 397e+001 _ B. 65Cie÷OOCi _7_O00e+O00 4. I00e+001

_. _157e+001 --.5.200e+001_ --3.296e+00i _ _7o 728e÷OOO---E_JODOe+OOO-2 _o300e+DDJ___

1_:_ 5. 522e+(_01 " ;4.55qe÷OC)l - 31128e-_d;(_i- 6. 926e÷ObC_--_-_'-(_be+6(]O--- _4_-500e+-_EOi--7

I i 4.913e+001 3. 904e+001 2. _E}2e+OC)l 6.1&4e÷O00 a.DOOe+OOJ 4.70Oe+O01

12 4. 464e÷001 3* 4-_-_e÷£tOL-_?._. Ofi7e+OCil=-5._fiO2e+090____. IOOe+_O01--= _4+ 900e-,-DOl

13 4. 033e+OAI 2. 964e+OOi _2.735e+OD1 ....5. O57e+OO0 .i_.DCK_e+O01 5. I00e÷001

14 3. 706e+001 2. 634e÷001 2. 606e+001 4. &52e+O00 I. 30Cie*CiOl 5. 300e+O01

-- :I5 2. 322e+001 --2. 355e÷Or11 -L-2. _,4_--e÷001-2- 4. i65e_-000 -"I. 40_+001 - 5. 500e÷C.TOi-L:

6 2.9&SemCiOl 2. _52e+0C)I 2.060e+00_I _" 3.718e+000 -41. 500e+OOf 5. 700e+001

17 _ _'2-4e._'?.K*_--4-,-_Z&e+OO _ _.-,_;:l-7_.eli,T, lr._-_-_._27e+O_l13_-T---._A_OEbe_.-ZL1 .._.9.CIDe+C}_ _j --

18 2. 603e÷OCil :I . 94_e÷0(:11 I. 726e÷0CII -3. 268e+000 ....I ..70_-i-001 6. 100e+OOi

19 ,._, 466e+001 - 1,901e÷001 - -1 , 570e+0C)1-----3.094e+000_ -1 .BOOe÷OOl _ 300e+001 _.

20 _ 363e÷001 1 883e÷OOJ 1. 428e÷001 2. 965e+0CI0 I. 900e+001 6. 400e+0C)1

- 21 2. 217e+001 _I.S29e+001 -_ i. 254e+001 2.TBOe÷O00 2:00Cie*O01 6. _500e÷O0! -

22 2. 071e+001 1.77Be+001 I .061 e+O01 - 2. 598e÷_;0_3 _#10_le÷OCil- o. 800e-_Ki:1

":._'3 i. E_E_le÷('l(')-_ - _-_656e+C_,_ B. _i7;+OC)C) _o_5_e-+oclo _-._-CTOe÷OC)_--=7.OOOe+O01_. • . . .....

24 I. 760e_-,:',0! I. 597e_-001 ":7..-'x83e4.000-"-2.208e÷000 - _'_._e_-o01 --7. 200e+O0 I

25 !.574e+001 I. 449e+00] 6.153e-I-000 1.976e+DO0°'2. #OOe+O01 -7. 400e+001

2_ :I.46be÷001 . .1_3_7e+001 -5.297e-I-000 I ._40e+O00 2,_00e÷001 --'7.60(_e+O01

27 I. 299e_-001 I. 226e÷00:I 4. 304e+000 -_ ._31e+CiO0 2. _t'K._e+O01 7. BO{_e+O01

28 I. 160e÷O01 I. lOSe+O01 :_3._42e+000 I',456e+000 _2_._'00e+001 8.0C,(,6+00_I

29 I. 064e+001 I. Ol Ie_-OOi -:_ 3_305e+000 1. 335e+000- --2.800e+bC)l B. 2CiOe+OC)!

30 9.2_9e+000 _#.egoe+O0_ 2._95e+OOO---=;_i_5e',OON 2.gOOe+O0i- e._Or.,e+O0__3 _ 7. O52e+OOr._ =-2"7.710e_O00 --I. _;48e_-OCiO 9. _BCCe-O01- =3. O00e_-OO] - B.-6OOe+O0_1

--- "_o _"9°.3t_3e._OO0E_.9_7-e+O00 - -"_.._e._-OOO:-'_.-iT"_ge_-13t3_Z_-_._t_Oe+-O01 ÷ -E_. BOOem.r',O. 3

• . ;- ," • , " • . ::_ _--___',,",_ • -'-r -__ -- _ _-_..". _-_

_36 5. B27e+O00 --3._77e+000- 6. 155e-001 --4.BO6e-O01 -__oSOOe+OOi 9.500e+001

=:;_'_ ,6. O06e'_-{K)O -- 5. 839e+OOO-'_.i._D9e+OOD-- 7.-.535e--00i ,;3. 600e÷O01 :_.700e+O01

-- T_ --5.95_÷O00-"_:'_'98e_-OIYO--e'l. ---2_6e'_)CR:)-=-_'_".-_e=Z_-OOi-"_'_rjOe'+--O01 .:.._I.O.I Oe+O02

40 5. 391e+000-; _5.287e+000 I. 057e+000 6.'766e-00.| __3._-.90.0e+0_01 I ,O30e+rK_2

: I _. 839e÷000 3.6BBe__CK_--.__ ,ObBe+O00 -_BiTe--OOi L_OOOe+O01 --_,-050e+002

:.:43 _-3.582e+O_K_ ....G. _519e-_O0 __, 770e-_001 - :_ _.gae_-4_,_'__=!-'_i_--_P-_e+O02 7-

--_# - 2.4_7_+000 --2. 379e÷000 --_.,5._BOe-._D_i_3oi%Sb_,,O0.1 ...._300__-_-_L_;_I 1£_ -_

=........._-_. _a_+ooo___. _e_6oO-_-_ oe-ooz---_._=_--_5-i-7_7-_c_, _;-a _ _oe*oo_,6 2.529e+00(_ __2.4_e÷DDD ;__-_3.?,e-001---3. l-7_-e-_O1---4_-50(_e'_O0! ---I._5_Oe+__O[Q2_LL-c.

--"-#7"-5;-2 &_=DOO -:-G._+_O-Ci_T6____. 67e-._O_-:_,T_e-_:KI1 ="------_---'_A0e+002___ : .

- .s-..z.i_z:s,,+c,c<,=-_,es__-,-(<,o=,7i.__Be-C;_--____:];S.e:_CT-._._--_..OC_Z,__-;;_.-IBoW÷oo2-:.T9 5.591e+000 5. 426e+000 .I._49e+000 _-7. 010e-_001 --_.-_OOeeC_l 1.20(1_e'*'C_C)2 -

50 2.915e+000 --2.87Ge+O00 - _. 928e-001 ....._. _'Te"O-O I ---4.900e+O01 I .220e+002

._ ..-_-= _..----__-_=_::_. :._.... ..__.-_=_=-.-_.-....._.:.= ........... = -.....

............... !_;__. ....: ....._ . ---_- :- --:_. .=-,_.... " -

'_ .-:" ----.-.- .'_L --'-'-'-- -'_'" "-- ..... '- -;'"':"-- ---: ......

..................... ......

• --.__ . __ - ....... .

:A FINGERF'R!NT VISCOSITY PROFILE 91LI} RESIN-NASA-LOT'2--_ .................. -'_L....

.: -_-.-- -- ....... __

h _. ETA* ETA ...... ETA" TORQUE TIME

POISE POISE POISE GRAMS-CM - " MIN.-

=.I 4.18Ge+O00 4. C)73e+000 9. 518e-001 5. 246e-001 -5:_000e+001

2 "5. 029e+000 4.881 e+Cx'_O I. 2 _ I e+0C_0 6. 309e-001 5. lOOe+O01

3 _. 973e+00C_ 6. 753_-+000 1. 739e+CK-) 8. 739e--001 "5._-200e÷OO 1

5z_ I. 8&6e+O01 1. 754e+001 6. 376e+000 2. _4C_e+OC_O '5. _OOe+O01

Op._.,INAIC PAGE

Of POOR QUALrl_

...... -TE'_6.... DEG. -:!2 .

1.240e÷002. _

1. 260e+002

.2BOe+O02 -

.300e÷002

. --_.---._-_. =: - :- . _- -

. o

- _ --'-- .... _-_-2.'_- _.L"- i _ _T- --T_--._-'-_ .... -3.--_'- " "

.... 3_=_ £ ...................... [ ..................... __..L...........

• : :- :" :_.'_:._ Z_ ..... _ .-

...... __...... .:-.--__ _.;-_7-.. -- - -_--- _ ". --. 7: T " "- -'. "E"._-'-- ---G_,-.-: ";---'-,_._.-- -'-

_---.... ;-__: :--- -: . - =.._........ -.- _ -

". _. _. ________..___= ......... - ....... _......... :............. _ -.-- __. .=_....=-=-__ ...... =. _.-= ............... .-;.:__.__-.-=:____:_.__-- _ . .

---: -=- - -: " -- ----::-;-=--;-- ?--3-::-::_------':-_-_-- _:_ -----

SOLVENT ONLYSCAN

[.....

............... I. - -- ----i-

-o=o-- ,_..... .:Lz_..% -----:

_ .-_'e_.-_ .....

........... :: ................ 7:_:::_.:_:_-=_-_:-_._:-._______ ......

" --.: "=-..'f:.+';.'=._:4: ..........

.I

• "--L ..........

____-z_..--:-'-_.:-::.___ " :L': ......... "............ _2_-_&'_i2T]

................--- • :-=':--_---_.--.'i_ .....

............. I--

--:2 ..

[LT:_'_.I '-IT-T_.. _- T-_J

•. L i ..._ ................................ _-2--_-X_'__-_-:-:-'-_-,

:Z_ __ •

dI-- • .

lIJ Z UJ.J UJ ..J

< o _

I_.

0

!

i #i

_- "_i

o2 w _N-

F

÷

,

CHART 15B

I-

I-

[

I

I-

....... + ....

i .

TEST

la.

lb.

2a.

2b.

2c.

3.

4.

5.

6.

7a.

7b,

7c,

8a.

8b.

9a.

9b,

10a.

10b.

10c.

TABLE OF CONTENTS

FABRIC TESTING

NAS8-36298

Polymerlc O.E, 71108

Fabric for NASA Lot# 2

PAGE

CHARTS

Visual Inspection ................................... 3A - 3M

TGA ................................................. 6A - 6M

Breaking Strength, WARP ........................... I

Breaking Strength, FILL ........................... I

Carbon Assay ...................................... I

Hydrogen Assay .................................... 2

Nitrogen Assay .................................... 2

Visual Inspection ................................. 2


pH ................................................ 3

TGA ............................................... 3


MQisture Content .................................. 4

Ash Content ....................................... 4

Filament dlameterp WARP ........................... 4

Filament diameter, FILL ........................... 4

Thread Count, WARP ................................ 5

Thread Count, FILL ................................ 5

Areal weight ...................................... 5

Vclatlles ......................................... 6

Weight Change on Acetone Wash ..................... 6

FABRIC TESTING

NAS8-3629B

Page 1 of 6

U.S. POLYMERIC 0.£. 71108

SWB-8 Fabric for NASA Lot# 2

la. Breaking Strength, £bs/in, WARP #2-___I #2-2

ASTM D1682 PICK 61 42CENTER 55 44

PLAIN 75 60AVG. 63.7 48.7

#2-3

92

98

2772.3

#2-4 #2-...._5 #2-6 #2-7 #2-8 #2-9PICK 16 27 63 48 25 12

CENTER 69 84 65 87 14 41

PLA IN 7__6 7___7 66 8__8 4__8 7_3_3AVG. 53.7 62.7 64.7 74.3 29.0 42

#2-10 #2-1! #2-12 #2-13 LOT2PICK 24 59 71 38 44.5

CENTER 71 92 103 64 68.2

PLAIN 23 4__3 8_._.2.2 28 58.9AVG. 39.3 64.7 85.3 43.3 57.2

lb. Breaking Strength, Ibs/inoh, FILL #2-1 #2-2ASTM D1682 PICK 72 59

CENTER 83 66

PLAIN 67' 6"3AVG. 74.0 63.3

AVG

#2-377

63

7"371.0

2a. Carbon

MDQAI

#2-4 #2-5 #2-__6 #2-__._Z #2-8 #2-..__99PICK 92 28 71 102 25 53

CENTER 71 77 39 48 22 46

P L A I N 6__I 47" 7__00 27 19 5__55

AVG. 74.7 50.7 60.0 59.0 22.0 51.3

#2-10 #2-11 #_ #2-1.__3 _OT2

PICK 73 83 30 55 63.1

CENTER 20 83 58 51 55.9

PLAIN 58 8.._55 88 4..55AVG. 50.3 83.7 58.7 50.3 59.2

AVG

Assay, X #2-I #2-2 #2-____3

5560 PICK 99.2 99.6 99.8CENTER 99.6 99.8 99.6

PLAIN 99.0 98-9 99.___99

AVG. 99.27 99.43 99.77

#2-.._4 #2-.__._55 #2-...._6 #2-7 #2-8 #2-_._.._9PICK 99.1 99.2 99.9 99.7 99.7 99.7

CENTER 99.8 99.7 99.6 99.8 99.7 99.8

PLAIN 99.9 99.____!0 99.9 99.4 99.9 99..____99AVG. 99.60 99.30 99.80 99.63 99.77 99.80


700 E DYER ROAD, SANTA ANA, CALIFORNIA 92707 , (714) 549-1101 • TVV3((910) 595-1130 • FAX # (714) 549-2858-5-2437

o_ 6

_WB-8 Fabric _or NASA Lot# 2

2m. Carbon ksssy_

MDQAI 5560

PICK

CENTER

PLAIN

AVG.

% (CONTINUED)

#2-10 #2-11 #2-12 #2-13 LOT2 AVG99.9 99.9 99.4 99.9 99.6299.6 99.5 99.8 99.9 99.71

99.2 99.4 99.6 99.9 99.5399.57 99.60 99.60 99.90 99.62

% #2-1 #2-22b, Hydrogen Assay,MDQAI 5560

#2-3

PICK .03 .02 .01

CENTER .03 .01 .01

PLAIN .02 .02 ,01AVG. .027 .017 .010

#2-___!4 #2-5 #2-s #2-7PICK ,02 .01 .02 <.01

CENTER .01 <.01 .02 <.01

PLAIN .01 <.0___._1 .01 <.0..__/1AVG. .013 EST .004 .017 EST .001

#2-8

<. 01

<.01

<.01

EST. 001

#2-9

<.01

<.01

<.01

EST .001

#2-1____9_ePICK <.01 .01

CENTER <.01 <.01

PLAIN .01AVG. EST .004 EST .004

#_-12 #2-13 LOT2 AVG<.01 <.01 .010

.01 <.01 .007

.01 <.01 .007

EST .007 EST .001 .008

2_. Nitrogen Assay,MDQAI 5560

% #2-1 #2-2 #2-3PICK .22 .19 .11

CENTER .21 .23 .09

PLAIN .09 .09 .16AVG. .17 .17 .12

#2-4 #2-5 #2-6 #2-7 #2-8 #2-9PICK .1 .1 .1 .1 .2 .3

CENTER .1 .02 .1 .1 .2 .2

PLAIN ,1 .1 .1 .04 .1 .1AVG. .1 .073 .1 .08 .167 .2

#2-10 #2-11 #2-1_ #2-13 60T2PICK .1 .1 .1 .; .14

CENTER .2 .1 .2 .1 .14

PLAIN .2 .1 .1 .02 .10AVG. ,167 ,1 .133 .073 .127

A.VG

3. Visual Inmpectlon

OCi-102

See Charts 3A-3M

4. Specific Gravity,PTM-84

Units #2-1 #2-2 #2-3PICK 1.7376 2.0163 2.0137

CENTER 1.7742 2.0569 2.0601

PLAIN 1.9094 _ 0466 2.0501AVG. 1.807 2.040 2.041

4.

.

.

7S.

_WB-8

Gravity, Units

Fabric for NASA Lot# 2

(CONTINUED)

Page 3 of 6

#2-4 #2-5 #2-__6 #2-7 #2-8 #2-9PICK 2.1453 2.1458 2.2223 2.0307 2.1896 1.7857

CENTER 2.1874 2.7238 2.1354 2.0625 2.1918 1.8273

PLAIN _.1789 _.2718 2.1337 _.1014 2._909 1.7342

AVG. 2.171 2.380 2.164 2.065 2.191 1.782

#2-10 #2-11 #2-12 #2-13 LOT2 AVG

PICK 1.6823 1.7784 1.5362 1.6062 1.9146

CENTER 1.8032 1.7732 1.6435 1.7198 1.9969

PLAIN _.7129 _.7895 _.7164 _.7572 1.9689AVG. 1.733 1.780 1.632 1.694 1.960

pH, Units

CTM-24B

AVG.

#2-I #2-___22 #2-___336.6 4.2 6.1

6.3 4.___2 6._._22AVG. 6.45 4.2 6.15

#2-4 #2-5 #2-__6 #2-7 #2-8 #2-96.0 6.2 6.4 6.0 6.4 6.9

6..___z 6._..3_2 6.4 6. e 6...__4 7._.._6.15 6.2 6.4 6.0 6.4 6.95

#2-10

6.2

6.2

AVG. 6.2

TGA, "C at 50X Weight LossCTM-51 (AIR)

Atomic Absorption, ppm

CTM-53B

#2-11 #2-12 # 2-I_________3 LOT2 AVG6.6 6.0 6.6 6.18

6.5 6.___0 6..__e9 6.206.55 6. • 6.85 6.19

SET UP# 1

#2-2 939#2-4 926

#2-5 934

#2-7 913#2-9 879

#2-11 876

#2-13 905AVG. 910

See Chart 6A-6M

.21Na 3

K 1Ca 31

Mg •

Li ...0_0AVG. 35

#2-5 #2-6 #2-7

5 6 4

2 1 1

16 13 15

I 1 0

_@0 __0 __o24 21 20

#2-4

Na 3

K 2

Ca 25

Mg •

AVG. 30

SET UP# 2

#2-1 867

#2-3 881#2-6 834

#2-8 825

#2-10 833#2-12 782

AVG. 837

42-2 #2-34 6

1 1

32 16

• 1

__0 o37 24

#2-8 #2-99 11

1 1

77 101

I 1

88 114

o£ 6


7a. Atomic Absorption, ppm (CONTINUED)

CTM-53B

#2-10 #2-11 #2-12 #2-13

Na 7 6 4 4

K I I 1 1

Ca 62 54 29 30

Mg • • • 1

AVG. 70 61 34 36

LOT2 AVG

5.5

1.2

38.5

0.5

0.0

45.7

7b. Moisture Content, X

CTM-53B

#2-1 .020

#2-2 .025#2-3 .020

#2-4 .015

#2-5 .005

#2-6 .015

#2-7 .o05

Lot#

#2-8 .000

#2-9 .010

#2-10 .015

#2-11 .010

#2-12 .005

#2-13 .005

2 AVERAGE .011

7(3. Ash Content,

CTM-53B

#2-1 .020

#2-2 .035#2-3 .020

#2-4 .020

#2-5 .010

#2-6 .035

_2-7 .030Lot#

#2-8 .080

#2-9 .059

#2-10 .070

#2-11 .055

#2-12 .005

#2-13 .029

2 AVERAGE .036

88. Filament diameter,

S.E.M. procedure

(diameters are an

10 measurements)

microns, WARP

average o£

AVERAGE 9.12

Minimum 8.25

Maximum 9.75

Std. Dev 0.52

#2-2 #2-39.60 9.64

8.00 8.9510.90 10.30

0.94 0.43

#2-___44AVERAGE 9.58

Minimum 7.95

Maximum 11.25

Std. Dev 1.15

#2-5 #2-_ #2-7 #2-8 #2-910.03 9.36 9.65 9.28 9.74

8.75 8.00 8.05 8.00 8.3512.45 10.60 11.50 11.00 10.45

1.21 0.89 0.97 0.90 0.56

AVERAGE 9.85

Minimum 7.75

Maximum 12.00

Std. Dev 1.28

#2-12 #2-13 _OT2 AVG

e. 55 9.18 10.11 9.59

8.55 8.10 8.25 7.75

10.55 10.05 12.05 12.45

0.66 0.64 1.25 0.92

8b. Filament diameter,

S.E.M. procedure(diameters are an

10 measurements)

microns, FILL

average of

#2-1

AVERAGE 10.00

Minimum 9.00

Maximum 13.50

Std. Dev 1.34

98.

9b.

10a.

Thread Count,

PTM-5A

AVG.

AVG.

Thread Count,PTM-5A

AVG.

AVG.

Areal Weight

PTM-3A


per inch, WARP #2-I

AVG.

4141

4041

4_!140.8

Pmge

#2-2

4443

4544

4444

5o_ 6

#2-3

40

4040

41

4__o40.2

#2-4 #2-5 #2-6 #2-7 #2-8 #2-944 43 40 39 36 4044 43 40 38 36 40

43 42 40 39 36 41

43 43 40 39 36 41

4_.4 4_22 4__0 3_.8 35 4_!I43.6 42.6 40 38.6 35.8 40.6

LOT2 AVG

39.9

39.6

39.8

39.8

39.5

39.7

#2-10 _ #2-12 #2-13

35 40 42 35

35 39 42 34

36 39 41 35

35 39 41 34

3_.55 40 40 3.435.2 39.4 41.2 34.4

per inch, FILL #2-I38

38

38

38

38AVG. 38. •

#2 -2

38

38

38

38

3838. •

#2-3

35

36

35

36

3635.6

#2-4 #2-_____55 #2-6 #2-7 #2-8 #2-_.___99

38 39 38 39 37 37

38 38 38 39 39 37

39 38 37 39 39 38

39 38 37 39 38 37

39 38 37 3-0 40 3-038.6 38.2 37.4 38. s 38.6 37.4

_OT2 AVG38.2

38.3

38.3

38.3

38.438.3

#2-2

3. 516

3. 510

3. 722

3. 583

#2-10 _ _ #2-15

39 41 39 39

38 41 39 39

39 41 39 38

38 42 39 39

3-0 41 39 3938.4 41.2 39.0 38.8

gm/4x4LEFT

CENTER

RIGHT

AVG.

as received, #2-1

3. 416

3. 234

3. 327

3. 326

#2-_____33. 214

3. 196

3. 375

3. 262

of 6

SWB-8 Fabric _or NASA Lot# 2

10a. Areal WeightPTH-3A

LEFT

CENTERRIGHT

AVG.

as received, gm/4x4

#2-8

3. 2462. 970

3.079

3.098

#2-9

3.1452.933

3.121

LEFTCENTER

RIGHT

AVG.

#2-4 #2-___55 #2-6 #2-___Z3.607 3.640 3.464 3.8063.533 3.569 3.366 3.566

3.636 3.762 3.377 3.71_3,592 3,657 3.402 3.694

#2-10 #2-11 #2-12 #2-133,275 3,562 3.587 3.056

3,159 3,263 2,759 3.149

3.015 3.477 3.379 2.8483.150 3.434 3.242 3.018

LOT2 AVG

3.4263.247

3.3843.352

10b. Volatlles

PTM-3Aas received, X

AVG.

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TABLE OF CONTENTS

PREPREG TESTING

NAS8-36298


FM 5834 NASA LOT# 2 U.S.P. LOT# D09275

PAGE

Resln Content, Soxhlet ............................ 1

Filler Content, Soxhlet ........................... I

Cloth Content, Scxhlet ............................ I

Volatile Content .................................. 1

Flow .............................................. 1

Resin Content, Dry Basis .......................... 2

Tack .............................................. 2

Gel Tlme .......................................... 2


Mclsture Content .................................. 2

Ash Content ....................................... 3

TGA ............................................... 3

DSC ............................................... 3

Infrared (IRZB} Baseline .......................... 3

Environmental History ............................. 3


Tensile Strength .................................. 4

Tensile Modulus ................................... 4

Tensile Elongation ................................ 4

Flexural Strength ................................. 4

Flexural Modulus .................................. 5

Compressive Strength .............................. 5

Compressive Modulus ............................... 5

Double Shear Strength ............................. 5

Barccl Hardness ................................... 5

Residual Volatlles ................................ 6

Resin Content, Pyrolysis .......................... 6

Acetone Extraction ................................ 6

CTE, with ply ..................................... 6

CTE, crossply ..................................... 6

CHARTS

8A - 8G

9A - 9G

10A - 10G

21A - 21G

Uo So

PREPREG TESTING

NAS8-36298

POLYMERIC O.E. 71108

11.

FM 5834 NASA LOT#

Resin Content, Soxhlet, X

CTM-6D

U.S.P. LOT# D09275

AVG.

ROLL#1 ROLL#2 ROLL#3 ROLL#4 ROLL#5

START START _TART START START37.5 36.0 35.1 36.3 37.9

39.6 36.3 35.4 35.8 37.3

37.1 35.2 35.2 35.6 39.338.1 35.8 35.2 35.9 38.2

NASA LOT# 2

lb. Filler Content, Soxhlet, X

CTM-6D

AVG.

15.6 15.0 14.6 15.1 15.8

16.5 15.1 14.7 14.9 15.5

15.8 14.9 14.7 14.9 15.9

NASA LOT# 2

Ic. Cloth Content, Soxhlet, X

CTM-6D

AVG.

46.9 49.0 50.3 48.6 46.3

43.9 48.6 49.9 49.3 47.2

47.5 50.3 50.1 49.6 44.346.1 49.3 50.1 49.2 45.9

NASA LOT# 2

2. Volatile Content, X

PTM-17B

AVG.

4.5 5.4 5.4 5.5 5.1

4.3 5.7 5.5 5. a 5.44.___33 5.___4 5.2 _ 5.__._s4.4 5.5 5.4 5.4 5.4

NASA LOT# 2

3. Flow, X

PTM-19G

AVG.

Page 1 of 6

ROLL#6 ROLL#7

_TART START38.0 37.237.4 37.7

38.2 37.837.9 37.6

AVERAGE 36.9

15.8 15.5

15.6 15.7

15.8 15.6

AVERAGE 15.4

46.2 47.3

47.0 46.6

45.9 46.5

46.4 46.8

AVERAGE 47.7

5.6 6.1

5.5 5.5

5. s5.5 5.8

AVERAGE 5.3

11.0 18.8 13.5 18.4 19.1 17.2 19.0

11.7 20.3 17.6 19.5 20.0 17.9 20.2

11.9 19.6 16.0 19.4 19.0 18.0 19.7



700 E DYER ROAD, SANTA ANA. CALIFORNIA 92707 • (714) 549-1101 • "rwx (910) 595-1130 • FAX # {714) 549-2858-5-2437

of 6

FM 5834 NASA LOT# 2 U.S.P. LOT# D09275

4. Resin Content, Dry Basis,

PTM-16F, Type II

ROLL#1 ROLL#2 ROLL#3

START START START

38.3 38.7 41.5

38.8 41.0 41.6

38.9 36.6 39.4AVG. 38.7 38.8 40.8

ROLL#4 ROLL#5 ROLL#6 ROLL#7

START START START START

37.7 42.4 38.0 43.3

40.1 41.6 38.4 42.7

34.5 41.3 39.4 dl.837.4 41.8 38.6 42.6


5. Tack, Ibs

PTM-80

60 44 36 40 48 35 42

NASA LOT#2 AVERAGE 44

6. Gel Time, Seconds

PTM-20E

87 68 70

7a. Atomic Absorption,CTM-53B

ppm

62 73 65 63

NASA LOT# 2 AVERAGE 70



Na 8 7 13 6

K 2 2 I 1

Ca 18 17 16 15

Mg 2 2 I I

TOTAL 30 28 31 23


START START STARTNa 6 10 5

K 2 1 1Ca 16 35 58

Mg 1 1 2

TOTAL 25 47 66

LOT#2

AVG.

8I

25

1

36

7b. Moisture Content,

CTM-53B


START START START START START

3.11 2.85 3.44 2.97 3.13

NASA LOT#

ROLL#6 ROLL#7

START START

3.77 2.83

2 AVERAGE 3.16

of 6

FM 5834 NASA LOT# _ U.S.P. LOT# D09275

7c. Ash Content, %

CTM-53B


START START START.04 .04 .03

ROLL#4 ROLL#5 ROLL#6 ROLL#7START FTART START FTART

.04 .04 .o2 .04NASA LOT# 2 AVERAGE .03

8. TGA, % Weight Loss at 500"C

CTM-5i (Nitrogen)

7.1 4.9 7.6 6.4 6.9 7.9 6.5


See Chart 8A-SG

9. DSC, "CCTM-50A ROLL#I-S

ROLL#2-S

ROLL#3-SROLL#4-S

ROLL#5-SROLL#6-S

_OLL#7-S

NASA LOT# 2

FIRST TEMPERATURE

182

182

182182

181

183

180AVERAGE 182

SECOND TEMPERATURE

240

243

241243

241

239243

241

See Chart 9A-gG

10. Infrared (IRZB) Basellne

CTM-21C


START START _TART START1.08 1.09 1.09 1.07 1.07

NASA LOT# 2

ROLL#6 ROLL#7

FTART START1.05 1.08AVERAGE 1.08

See Chart 10A-lOG

11. Envlronmentml History Date manufactured: 28 Nay 1986

Packaged in: Polyethylene bagsupported in

cardboard carton

Date shipped: a July _986 in40"F truck

12. Specific Grmvltyt Cured, Units

ASTM D 792

i 1,516 1,513 1.500

1.513 1.527 1.501

1.511 _ 1,499AVG. 1.513 1.522 1.500

I._I_ 1.50s 1.496 l,Sil1,523 1.509 1.485 1,5_2

1.50__.___4_ i.si_____31.520 1.507 1.491 1.512


13a,

13b.

13C.

14a.

FM 5834 NAS_ LOT#

Tensile Strength, ksl, WARP

FTMS 406-1011

AVG.

U.S.P. LOT# D09275


START START START START START22.87 24.71 29.95 27.64 22,81

25.17 21.18 30.48 26.27 22.37

24.65 25.99 25.90 25.48 20.25

24.40 22.83 27.55 22.55 22.68

23.67 _3.47 27.46 26.0__4 21.0_.__._8824.15 23.64 28.27 25.60 21.84

NASA LOT#

Tensile Modulus, msi, WARP

FTMS 406-1011

4.59 4.88 4.57 5.34

5.66 5.38 5.18 6.17

4.74 4.84 4.99 5.454.93 5,06 4.92 5.36

5.02 4.80 5.34 4.914.99 4.99 5.00 5.45AVG.

Tensile Elongation, %, WARPFTMS 406-1011

.50 .62 .68 .60

-- .53 .65 .53

.60 .65 .58 .54

.54 .55 .64 .51

.54 .58 _ .ss

.55 .se .63 .55AVG.

Flexursl Strength, ksl, WARP

FTMS 406-1031

33.89 37.80 47.66 37.41

36.63 38.59 43.56 37.08

41.72 36.87 45.82 40.61

38.59 32.49 45.90 39.15

40.45 31.68. 44.35 34.6038.26 35.49 45.46 37.77AVG.

2

Page 4 o_ 6

ROLL#6 ROLL#7

START START

29.86 28.65

29.89 27.54

28.63 24.87

31.79 27.13

29.72 25.1329.98 26.70

AVERAGE 25.74

38.21 43.37 39.23

33.17 42.09 41.7337.20 44.55 41.86

32.90 44.63 42.03

43.66 41.5935.88 43.66 41.29

NASA LOT@ 2 AVERAGE 39.69

.68 .55 .64

.64 .60 .63

.53 -- .57

.64 .53 .60

.62 .57 .55

.62 .56 .60


3.95 5.79 5.61

4.20 5.48 5.26

4.43 -- 5.40

4.36 6.15 5.80

4.16 6.02 5.38

4.22 5.86 5.49


14b.

15B.

15b.

16.

17.

F M 5834 NASA LOT#

Flexural Modulus, msi, WARPFTMS 406-1031

AVG.

2 U.S.P. LOT# D09275


START START START START START

4.32 4,28 6.06 4.46 4.32

4.16 4,80 5.58 4.44 3.70

4.08 4.72 5.68 4.50 4.06

4.38 3.82 6.04 4.40 3.96

4.38 4.32 4.88 4.42 4.24

4.26 4.39 5.65 4.44 4.06

NASA LOT# 2

Compressive Strength, ksi, WARPFTMS 406-1021

Page 5 o£ 6

AVG.

ROLL#6 ROLL#7

STAR.___./_T START4.94 4.76

4.82 4.66

5.22 4.32

5.28 4.88

5.02 4.68

5.06 4.66

AVERAGE 4.65

26.50 24.88 27.59 25.71 26.56 29.07 28.84

22.75 24.65 26.86 26.83 23. S5 27.76 26.08

24.73 24.14 27.22 25.94 26.89 27.90 27.80

25.37 23.31 26.15 26.68 24.98 28.33 30.12

_5.15 _3.19 27.42 25.47 27.17 28.7_ 28.5124.90 24.03 27.05 26.12 25.91 28.36 28.27


Compressive Modulus, msl, WARP

FTMS 406-1021

5. 12 4.96 5.07 5.25 4.86

4.44 4.59 4.56 5.26 4.54

5.04 4.22 5.02 4.97 5.02

5.09 4.50 4.67 5.32 4.794.4._.._.66 _ 4. e9 4.6.__.._9

4, 97 4.55 4.82 5.14 4.78NASA LOT# 2

AVG.

Double Shear Strength, ksl

FTMS 406-1041A

AVG.

3.55 2.98 3.21 3.66 3.33

3.42 3.33 3.60 3.62 3.39

3.26 3.09 3.85 3.48 3.35

3.42 3.21 3.35 3.49 3.373.36 3.62 3.54 3.93

3.4e 3.25 3.51 3.64 3.3sNASA LOT# 2

Barcol Hardness,

ASTM D-2583

(Average of 10

Units

determinations)

69.5 68.8 70.5 70.4 69.7

NASA LOT# 2

5.23 4.83

4.50 4.52

4.62 4.69

4.75 4.92

4.884.80 4.77

AVERAGE 4.83

3.08 3.62

3.48 3.21

3.31 3.43

3.57 3.94

3.32 3.54AVERAGE 3.44

70.8 72.4

AVERAGE 70.3

18.

19.

20.

21S.

21b

FM 5834 NASA LOT# 2

Residual Volstlles,

PTM-98


_TART START _TART2.32 2.34 2.62

2.35 2.28 2.63

2.36 2.37 2.60

AVG. 2.34 2.33 2.62

Resin Content,CTM-14B

Pyrolysis, %

39.44 35.74 35.92

37.60 35.74 34.23

_9.39 36.82 36.5__4AVG. 38.61 36.10 35.56

Acetone Extraction, %CTM-18A

AVG.

-.15 .81 °59

1.19 -.46 .16

.72 .54 .40

.58 .30 .38

CTE, In/in "F,

PTM-61B

-.27

1.07

AVG. .40

wlth PLY

• 75

.46

• 62

-. 26

-.51

-. 39

CTE, in/inPTM-61B

13.44

9.80

AVG. 11.62

°F, Crosl

11.31

11.19

PLY

11.20

11.20

Page 6 o£ 6

U.S.P. LOT# D09275



2.35 2.49 2.39 2.49

2.28 2.77 2.41 2.37

2.34 2.73 2.46 2.45

2.33 2.66 2.42 2.44


36.23 38.50 40.14 36.08

37.24 37.34 38.56 34.60

37.69 34.35 39.48 34.36

37.05 36.73 39.40 35.01


.69 1.98 .00 -.55

1.38 -.16 -.62 .38

.86 .16 3.66 -.22

.98 .66 1.01 -.13


.58 1.09 .10 -6.92

.61 .86 .77 .78

.60 .98 .44 -3.07

NASA LOT# 2 AVERAGE -.06

13.79

12.96

13.38

13.12 15.62 14.38

_5.75 14.09

12.94 15.69 14.24


See Chart 21A-21G

U.S. Polymeric

Hamld M. Quralshl, Manager

Quality Assurance Department

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