application areas: 7039test method astm d7039 and iso 20884 dimensions 37 cm (w) x 50 cm (d) x 34 cm...

better analysis counts

Application Areas: • Totalsulfuranalysisfromultralowsulfur

fuelstocrudes.

• Foruseinrefinerylabs,pipelineterminals,additiveplants,testingvansandinspectionlaboratories.

• ComplieswithASTMD7039andISO20884.

Features and Benefits:• LOD:0.4ppmat300s.

• DynamicRange: Standard: 0.4ppmto3000ppm XRpackage: 0.4ppmto10%

• Fitsonanybenchandcompatibleforuseinmobilelabsandvans:

37cm(w)x50cm(d)x34cm(h)

• Plug-it-inandmeasure:noadditionalutilitiesrequired.

• TouchScreenuserinterface.

• Userprogrammablemeasurementtime:30-900s.

• Onecalibrationcurvewillrunbothdieselandgasolineupto3000ppm

• Noconversiongasses,heatingelements,quartztubesorcolumns.

• 75Wair-cooledexcitationtube.

• Robustpolyamidewindowforeasycleaning.

Options: • ExtendedRangepackage:from0.4ppmup

to10%.

• LIMSdataoutputsoftwarecapability.

7039

Sulfur Analysis in Petroleum and Bio Fuels

Fromultralowsulfurdieselandgasolinetoheavyfueloilandcrudes,theSindie

7039analyzerdeliversunprecedentedprecisionandaccuracy.Theanalyzeristhe

ultimateeasy-to-useandrobustsulfuranalyzerforpetroleumandbiofuels.The

idealanalyticalsolutionfortheenergyindustrywheredetection,performanceand

reliabilityarecritical.SINDIE7039complieswithASTMD7039andISO20884

methods.Plugitinandmeasure.Resultswithonetouch.Unrivaledprecision.

PrecisionTypicalrepeatability(r)andreproducibility(R)values

indieselfuel,at95%confidence.300smeasurement

time.

Sulfur Concentration r R (ppm)

2 0.4 1.0

8 0.7 1.2

15 0.9 1.7

100 3 6

500 6 12

better analysis counts15 Tech Valley Drive • East Greenbush, New York 12061, USA • 518.880.1500 • Fax: 518.880.1510 e-mail: [email protected] • website: www.xos.com

© XOS (2012) MAR2012

Optic 1 Optic 2PolychromaticIncident X-rays

from tube

Sulfur

MWD XRF Monochromatic Wavelength Dispersive X-Ray Fluorescence (MWD XRF) utilizesstate-of-the-

artfocusingandmonochromatingopticstoincreaseexcitationintensityanddramaticallyimprove

signal-to-backgroundoverhighpowertraditionalWDXRFinstruments.Thisenablessignificantly

improveddetectionlimitsandprecisionandareducedsensitivitytomatrixeffects.Amonochromatic

andfocusedprimarybeamexcitesthesampleandsecondarycharacteristicfluorescencex-raysare

emittedfromthesample.Asecondmonochromatingopticselectsthesulfurcharacteristicx-rays

anddirectsthesex-raystothedetector.MWDXRFisadirectmeasurementtechniqueanddoesnot

requireconsumablegassesorsampleconversion.

SINDIE-XRCalibrationCurve

Low RangeCalibration

Test Method ASTM D7039 and ISO 20884

Dimensions 37 cm (w) x 50 cm (d) x 34 cm (h)

Power 100-120 VAC, 47-63 HZ at 6.0 Amps/200-240 VAC, 47-63 HZ at 6.0 Amps

Sample Cup Volume 10 ml

I/O Ports Ethernet 10/100 base T, RS232

Optional Computer Interface Pentium, 100MHz, 32MB RAM/Windows 98 or newer operating system

Ambient Temperature Requirements 5-40o C (40-104o C)

Dynamic Range Standard: 0.4 – 3000 ppm, XR Package: 0.4 ppm – 10%

Measurement User selectable: 30-900 s

Calibration 8 calibration curves. Automatic and Manual Calibration functionality.

Product Specifications


Application Areas: • Totalsulfuranalysisfromultralowsulfur

fuelstocrudes.

• Foruseinrefinerylabs,pipelineterminals,additiveplants,testingvansandinspectionlaboratories.

• ComplieswithASTMD7039andISO20884.

Features and Benefits:• LOD:0.15ppmat300s.

• DynamicRange: Standard: 0.15ppmto3000ppm XRpackage: 0.15ppmto10%

• Availablewith8cellauto-sampler.

• Fitsonanybenchandcompatibleforuseinmobilelabs/vans.

• Plug-it-inandmeasure:powerisonlyutility.

• Touchscreenuserinterface.

• UtilizesACCU-CELLpre-assembledandpre-ventedsamplecupsforenhancedpreci-sion,extremeease-of-useandenhancedproductivity.

• Userprogrammablemeasurementtime:30-900s.

• Onecalibrationcurvewillrunbothdieselandgasolineupto3000ppm.

• Noconversiongasses,heatingelements,quartztubesorcolumns.

• 75Wair-cooledexcitationtube.

• Robustpolyamidewindowforeasycleaning.

Options: • ExtendedRangepackage:from0.15ppm upto10%.

• 8cellAutosampler.

• LIMSdataoutputsoftwarecapability.

7039G3

Sulfur Analysis with Unprecedented Precision

Nocompromisesindetection,performanceandreliability-theSINDIE7039G3

analyzeristheidealsulfuranalyticalsolutionfortheenergyindustry.Fromultra

lowsulfurdieselandgasolinetoheavyfueloilandcrudes,theanalyzerdelivers

unprecedentedprecisionandaccuracy.TheSindie7039G3bench-topanalyzeris

easy-to-use,robustandcomplieswithbothASTMD7039andISO20884methods.

Plugitinandmeasure.Resultswithonetouch.Unrivaledprecision.

PrecisionTypicalrepeatability(r)andreproducibility(R)valuesin

dieselfuel,at95%confidence.300smeasurementtime.


2 0.3 0.7

5 0.5 0.8

8 0.6 1.0

15 0.8 1.4

100 2 4

500 5 10


© XOS (2012) MAR2012


from tube

Sulfur

MWD XRF Monochromatic Wavelength Dispersive X-Ray Fluorescence (MWD XRF) utilizesstate-of-the-artfocusingandmonochromatingopticstoincreaseexcitationintensityanddramaticallyimprovesignal-to-backgroundoverhighpowertraditionalWDXRFinstruments.Thisenablessignificantlyimproveddetectionlimitsandprecisionandareducedsensitivitytomatrixeffects.Amonochromaticandfocusedprimarybeamexcitesthesampleandsecondarycharacteristicfluorescencex-raysareemittedfromthesample.Asecondmonochromatingopticselectsthesulfurcharacteristicx-raysanddirectsthesex-raystothedetector.MWDXRFisadirectmeasurementtechniqueanddoesnotrequireconsumablegassesor

sampleconversion.

SINDIE Autosampler•8samplecellcapacity

•Increasesproductivity

•UtilitizesXOSAccu-Cellcups

ACCU-CELL Sample Cups•Noassemblyofseparatefilm&cupcomponents

•Pre-ventedsamplecups

•Eliminatessample&cupcontamination

•Onedischargeof1mlpipettewillfillthecup



Test Method ASTM D7039 and ISO 20884





Optional Computer Interface Pentium, 100 MHz, 32 MB RAM/Windows 98 or newer operating system

Ambient Temperature Requirements 5-40o C (40-104o C)

Dynamic Range Standard: 0.15 – 3000 ppm, XR Package: 0.15 ppm – 10%


Calibration 8 calibration curves. Automatic and Manual Calibration functionality



Application Areas: • Total sulfur analysis from ultra low sulfur fuels to crudes.

• For use in refinery labs, pipeline terminals, additive plants and inspection laboratories.

• Complies with ASTM D2622, D7039 and ISO 20884.

Features and Benefits:• LOD: 0.4 ppm at 300 s.

• Dynamic Range: 0.4 ppm to 10%

• Fits on any bench: 37 cm (w) x 50 cm (d) x 34 cm (h).

• Plug-it-in and measure: power is only utility.

• Touch Screen user interface.

• User programmable measurement time: 30-900 s.

• Two calibrations covers both gasoline and diesel matrices over full dynamic range:

- 0.4 – 3000 ppm wt - 0.3 – 10% wt

• No conversion gasses, heating elements, quartz tubes or columns.

• 75 W air-cooled excitation tube.

• Robust polyamide window for easy cleaning.

Options:• LIMS data output software capability.

Sulfur Analysis with Compliance Flexibility

The Sindie 2622 bench-top analyzer complies with ASTM D2622, D7039 and ISO

20884 methods, enabling complete flexibility in sulfur analysis. No compromises in

detection, performance and reliability - the SINDIE 2622 analyzer is the ideal sulfur

analytical solution from ultra low sulfur diesel and gasoline to heavy fuel oil and

crudes. One analyzer – three compliance solutions.

PrecisionTypical repeatability (r) and reproducibility (R) values

in diesel fuel, at 95% confidence. 300s measurement

time.


4 0.4 1.0

8 0.7 1.2

15 0.9 1.7

100 3 6

500 6 12


© XOS (2012) MAR2012


from tube

Sulfur

MWD XRF Monochromatic Wavelength Dispersive X-Ray Fluorescence (MWD XRF) utilizes state-of-the-

art focusing and monochromating optics to increase excitation intensity and dramatically improve

signal-to-background over high power traditional WD XRF instruments. This enables significantly

improved detection limits and precision and a reduced sensitivity to matrix effects. A monochromatic

and focused primary beam excites the sample and secondary characteristic fluorescence x-rays are

emitted from the sample. A second monochromating optic selects the sulfur characteristic x-rays

and directs these x-rays to the detector. MWD XRF is a direct measurement technique and does not

require consumable gasses or sample conversion.



Test Method ASTM D7039, D2622 and ISO 20884





Ambient Temperature Requirements 5-40o C (40-104o F)

Dynamic Range 0.4 ppm – 10%


Calibration 8 calibration curves. Automatic and Manual Calibration functionality.


application areas: 7039test method astm d7039 and iso 20884 dimensions 37 cm (w) x 50 cm (d) x 34 cm...

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