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ANAMA Package & Container Testing Services, Inc. 607 Fayette Avenue, Mamaroneck, NY 10543 Tel: (914) 899-3300 | Fax: (914) 899-3325 [email protected] | www.anamapackagetesting.com Project #2622-A Certification #+CM0471 Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021 Page 1 of 64 DEPARTMENT OF TRANSPORTATION PERFORMANCE ORIENTED PACKAGE TESTING CERTIFICATION Testing Performed by: ANAMA Package & Container Testing Services, Inc. (+CM) Approval CA2013040016 607 Fayette Avenue Mamaroneck, NY 10543 (914) 899-3300 Testing Performed for: Owen Oil Tools, Inc. 12001 County Road 1000 Godley, TX 76044 Ms. Debra Payne (817) 551-0540 [email protected] 4G Design Re-Qualification Testing 275# DW 1313-001 Fibrebord Box With: Iteration 1: 48-90.8 Grams; 3-22.5 Grams & 1-15.6 Kg Average Gross Weight Articles (B CUT 8250-032) Iteration 2: 10-1.27 Kg Average Gross Weight Barrier Bags (D JEC) Iteration 3: 9-2.38 Kg Average Gross Weight Barrier Bags (E KOD) Iteration 4: 5-4.38 Kg Average Gross Weight Inner Boxes (C ACE) Iteration 5: 50-400 Grams Average Gross Weight Anti-Stat Bags (G COR) 4G / Y 22.8 / S / ** USA / +CM0471 ** insert year the packaging is manufactured ________________________________________________________________________ Anton Cotaj, Certification Officer u n

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Page 1: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

ANAMA Package & Container Testing Services, Inc.

607 Fayette Avenue, Mamaroneck, NY 10543 Tel: (914) 899-3300 | Fax: (914) 899-3325

[email protected] | www.anamapackagetesting.com Project #2622-A

Certification #+CM0471 Date of Report: 10/17/2019

Periodic Retest Date: 10/17/2021 Page 1 of 64

DEPARTMENT OF TRANSPORTATION PERFORMANCE ORIENTED PACKAGE TESTING

CERTIFICATION

Testing Performed by: ANAMA Package & Container Testing Services, Inc. (+CM)

Approval CA2013040016 607 Fayette Avenue

Mamaroneck, NY 10543 (914) 899-3300

Testing Performed for: Owen Oil Tools, Inc.

12001 County Road 1000 Godley, TX 76044 Ms. Debra Payne (817) 551-0540

[email protected]

4G Design Re-Qualification Testing 275# DW 1313-001 Fibrebord Box With:

Iteration 1: 48-90.8 Grams; 3-22.5 Grams & 1-15.6 Kg Average Gross Weight Articles (B CUT 8250-032) Iteration 2: 10-1.27 Kg Average Gross Weight Barrier Bags (D JEC) Iteration 3: 9-2.38 Kg Average Gross Weight Barrier Bags (E KOD) Iteration 4: 5-4.38 Kg Average Gross Weight Inner Boxes (C ACE)

Iteration 5: 50-400 Grams Average Gross Weight Anti-Stat Bags (G COR) 4G / Y 22.8 / S / ** USA / +CM0471

** insert year the packaging is manufactured

________________________________________________________________________ Anton Cotaj, Certification Officer

u n

Page 2: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________

CA2013040016 Project #2622-A

ANAMA Package & Container Testing Services, Inc. 607 Fayette Avenue, Mamaroneck, NY 10543

Tel:(914) 899-3300 | Fax: (914) 899-3325 [email protected] | www.anamapackagetesting.com

Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 2 of 64

SECTION 1 - CERTIFICATION

4G Design Re-Qualification Testing of the Owen Oil Tools, Inc., Godley, TX Packages 275# DW 1313-001 Fibrebord Box With:

Iteration 1: 48-90.8 Grams; 3-22.5 Grams & 1-15.6 Kg Average Gross Weight Articles (B CUT 8250-032) Iteration 2: 10-1.27 Kg Average Gross Weight Barrier Bags (D JEC) Iteration 3: 9-2.38 Kg Average Gross Weight Barrier Bags (E KOD) Iteration 4: 5-4.38 Kg Average Gross Weight Inner Boxes (C ACE)

Iteration 5: 50-400 Grams Average Gross Weight Anti-Stat Bags (G COR) Requesting Party: Owen Oil Tools, Inc. Tel: (817) 551-0540 12001 County Road 1000, PO Box 765 Email: [email protected] Godley, TX 76044 Attn: Ms. Debra Payne ANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and certifies that the Owen Oil Tools, Inc., Godley, TX packaging prepared as for transport, referenced above and tested in October 2019 has passed the Standards of the US Department of Transportation, Title 49CFR, Performance Oriented Packaging Standards; Section 178. This package is also certified under IMDG and UN Recommendations of the Committee of Experts on the Transportation of Dangerous Goods. It is the responsibility of the shipper / end user to ensure appropriate use. The use of other packaging methods or components other than those documented in this report may render this report invalid.

SUMMARY OF PERFORMANCE TESTS Test Specification Test Level Time Results Drop 49 CFR 178.603 1.2 m N/A Pass

Stacking 49 CFR 178.606 256.5 kg 24 Hours Pass Cobb 49 CFR 178.516 116.3 gr/m² 30 Minutes Pass

Vibration 49 CFR 178.608 235 CPM 60 Minutes Pass Test Report #0471

UN Marking (49 CFR 178.503)

4G / Y 22.8 / S / **

USA / +CM0471

Package Identification Code 4G - Fibreboard Box (49 CFR 178.516) Performance Standard Y - Packaging meets Packing Group II and III Tests Authorized Gross Mass 22.8 kg (50.16 lbs) "S" Designation Denotes Inner Packaging Year of Manufacture ** Insert year the packaging is manufactured Country Authorizing The Mark USA

DOT UN Third-Party Certification Agency (+CM) ANAMA Package & Container Testing Services, Inc. Approval CA2013040016

Third Party Packaging Identification Number +CM0471

________________________________________________________________________ Anton Cotaj, Certification Officer

Page 3: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 3 of 64

____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________

CA2013040016 Project #2622-A

SECTION 2 – DESCRIPTION OF THE TESTED PACKAGE COMPONENTS

Iteration 1 (Box-1313-001 B CUT 8250-032): Forty-Eight (48) 90.8 grams average gross weight each small spiral wound fiberboard tube rings filled with Copper Innerts, placed in 2 layers, 24 tubes per layer; three (3) 22.5 grams average gross weight each solid product filled foil/plastic laminate bags each folded and placed into three (3) larger spiral wound fiberboard tube rings, one (1) ring on each corner of the cutter primary inner packagings and one (1) 15.7 kg gross weight casing cutter assembly secondary inner packaging, all installed within a center special slotted fibreboard container (International Box Code 0204) outer packaging with fibreboard top and bottom pads and fibreboard/honeycomb side fillers. The use of other packaging methods or components may render this report invalid. INNER PACKAGING DETAIL #1-1 - Reference Section 7 for drawings

SMALL FIBREBOARD TUBE RINGS Quantity 48

Style Spiral wound fiberboard Manufacturer/Supplier T & S Products, Arlington, TX T& S Part # OWEN2.125 X 1.25 Part # TUBE-2125-125 (2.125 x 1.25 x .555)

Material 26 Plies High Density Paperboard Laminated with PVOH Adhesive

Size (mm, OD) 71.2 x 51.7 Size (mm, ID) 42.8 x 51.7 Caliper 14.2 mm Average Tare Weight 87.8 grams Average Gross Weight 90.8 grams Average Net Weight 10.7 grams Location Arranged 4 X 6, 2-layers high within the box

INNERT MATERIAL Count 20

Style/Description Trapezoidal Shaped Copper Frame Manufacturer Owen Oil Tools, Godley, TX Size (mm, OD) 31.6 x 27.5 x 44.6 Caliper 1.47 mm Average Tare Weight 41.0 grams Average Gross Weight (as tested) 63.7 grams Average Net Weight (as tested) 24.3 grams Test Material Putty Location Placed within the small fibre tubes

INNERT TEST MATERIAL

Count 18

Description White putty material

Average Net Weight (as tested) 24.3 grams

Location Placed within copper frame

Page 4: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 4 of 64

____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________

CA2013040016 Project #2622-A

INNER PACKAGING DETAIL #1-2 - Reference Section 7 for drawings

BARRIER BAG Quantity 2

Style/Description Laminated watervaporproof, greaseproof, flexible barrier bag with heat-sealed bottom and sides

Type MIL-PRF-131J, Type 1, Class 1, Style 1 Manufacturer Ludlow Coated Products, Inc., Columbus, GA Manufacturer/Supplier Uline, Inc. Waukegan, IL Uline Item # S-13006 Owen Part # BAG-0305-F100 3 X 5 Foil Bag Material of Construction Plastic/foil/plastic laminate, 5 Mil nominal gauge Minimum Thickness 0.120 mm (0.0045") Nominal Thickness 0.127 mm (0.005") Bursting Strength 65 lbs/inch² Dimension (mm, OD), flat 132.4 x 130 Dimension (mm, ID), flat 92.1 x 104.6 Bottom Seam Width 25.1 mm Side Seam Width 18.6 mm Average Tare Weight 4.3 grams Average Gross Weight (as tested) 27.6 grams Print INNERT

Method of Closure Each bag was filled with solid product (putty). Top of bags was left open to place the putty, bag was then folded and placed individually in the center of small fibreboard tube rings (Refer to Section 6.2)

Bag Width Bag Length INNERT TEST MATERIAL

Count 2

Description White putty material

Average Net Weight (as tested) 24.3 grams

Location Placed inside each barrier bag

Page 5: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 5 of 64

____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________

CA2013040016 Project #2622-A

INNER PACKAGING DETAIL #1-3 - Reference Section 7 for drawings

LARGE FIBREBOARD TUBE RINGS Quantity 4

Style Spiral wound fiberboard Manufacturer/Supplier T & S Products, Arlington, TX T& S Part # OWEN3.45 X 1.25 Part # TUBE-3450-125 (3.45 x1.25 x .555)

Material 26 Plies High Density Paperboard Laminated with PVOH Adhesive

Size (mm, OD) 115.1 x 31.5 Size (mm, ID) 87.6 x 31.5 Caliper 13.6 mm Average Tare Weight 94.0 grams

Location These empty rings were placed next to the cutter corners, 2 on each corner

Page 6: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 6 of 64

____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________

CA2013040016 Project #2622-A

INNER PACKAGING DETAIL #1-4 - Reference Section 7 for drawings

LARGE CASING CUTTER Quantity 1

Style/Description Machined steel cylindrical shape with steel lid Manufacturer Owen Oil Tools, Godley, TX Nominal Thickness 1.35 mm Dimension (mm, OD) 209.5 x 90.4 (closed with lid) Dimension (mm, OD) 209.5 x 75.1 (bottom piece without lid) Dimension (mm, ID) 175 x 46 (bottom piece) Print/Label CUT 8250-039-R3; 42074-1 Gross Weight (as tested) 15.66 kg with lid

LID Dimension (mm, OD) 209.5 x 35

Gross Weight (as tested) 5.96 kg Opening Cavity (mm, ID) 113.6 x 21.5

INNER PIECE Dimension (mm, OD) 113.6 x21.5

Gross Weight (as tested) 1.44 kg Lid Opening (mm, ID) 25.0 diameter

LID SCREWS Quantity 4

Style Allen screws Dimension (mm, OD) 7.8 x 16.8, 4.5 mm diameter body Average Tare Weight 2.7 grams

Location Placed on the bottom of shipper

Overall Inner Packaging Gross Weight (OIP1GW) Iteration 1: OIP1GW = 21.75 kg

Page 7: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 7 of 64

____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________

CA2013040016 Project #2622-A

Iteration 2 (Box-1313-001 D JEC): Ten (10) 1.27 kg average gross solid product filled metal-in film laminate bags, inner packagings installed upright within the double-flanged die-cut corrugated insert within the center special slotted fibreboard container (International Box Code 0204) outer packaging backfilled with top and bottom fibreboard pads. The use of other packaging methods or components may render this report invalid. INNER PACKAGING DETAIL #2-1 - Reference Section 7 for drawings

ESD SHIELDING BAG Quantity 10

Style/Description Lead free RoHs Compliant, Stat Shielding bag with heat-sealed side seams

Type RoHs Compliant 0217/617 Desco Part # 13366 Owen Part # BAG-0715-F100 7 X 15 Foil Bag Manufacturer Desco Industries, Chino, CA Material of Construction Metal-in film laminate, 3 Mil nominal gauge Minimum Thickness 0.065 mm Nominal Thickness 0.076 mm Dimension (mm, OD), flat 205 x 380 Dimension (mm, ID), flat 175 x 330 Side Seam Width 9.9 mm Top Seam Width 3.5 mm, 45 mm away from top edge Average Tare Weight 11.6 grams Average Gross Weight (as tested) 1263 grams Print EMI/STATIC SHIELD

Method of Closure Test material was inserted into bag. Air was expelled from bag, then bag was heat-sealed. Each bag contains 1 sand filled steel tube with plastic caps and 2 Desiccant bags.

Bag Width Bag Length

Page 8: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 8 of 64

____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________

CA2013040016 Project #2622-A

PRODUCT/ARTICLES - TEST MATERIAL DETAIL #2-1-1 - Reference Section 7 for drawings

METAL CYLINDER WITH STEEL PLUGS Quantity 10

Style/Description Machined metal halo cylinder Material of Construction Steel Manufacturer Owen Oil Tools, Godley, TX Nominal Thickness 1.65 mm Dimension (mm, OD), closed 59.3 x 210 Dimension (mm, OD) 57.5 x 208.0 Dimension (mm, ID) 52.7 x 208.0 Average Tare Weight 448.5 grams Average Gross Weight 1206.5 grams

PLUGS Quantity 2

Material of Construction Red plastic Manufacturer/Supplier Caplugs, Inc., Buffalo, NY

Plug ID 2 ¼ SC Nominal Thickness 0.99 mm

Dimension (mm, OD) 59.0 x 23.2 Dimension (mm, ID) 57.5 x 22.0

Average Tare Weight 6.1 grams Test Material Sand

Location Inserted individually within the ESD shielding bags INNER PACKAGING DETAIL #2-1-2 - Reference Section 7 for drawings

DESICCANT BAGS Quantity 20 (2 per bag)

Manufacturer Desiccare, Inc., Reno, NV

Material Silica Gel, Indicating Silica Gel, Clay, Molecular Sieve and Carbon

Owen Part # PAK-0250-100 Dimension (mm, OD) 57.9 x 10.6 x 87.6 Average Weight 22.0 grams

Location 2 desiccant bags were placed inside each ESD shielding bag

Page 9: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 9 of 64

____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________

CA2013040016 Project #2622-A

PRODUCT/ARTICLES – ADDITIONAL WEIGHT TEST MATERIAL DETAIL #2-2

METAL BLOCKS Quantity 8

Style/Description Solid steel block

Dimension (mm, OD), D X H 5 X 76 x 76 x 8.6, 430 grams each 2 X 76 x 76 x 3.4, 140 grams each

Overall Gross Weight 2.43 kg

Location Placed on both sides of the ESD shielding bags (to reach the desired weight)

PRODUCT/ARTICLES – ADDITIONAL WEIGHT TEST MATERIAL DETAIL #2-2

SAND-BAGS Quantity 6

Style/Description Solid steel block

Gross Weights 4 X 660 grams 2 X 2110 grams

Overall Gross Weight 6.86 kg

Location Placed on both sides of the ESD shielding bags (to reach the desired weight)

Overall Inner Packaging Gross Weight (OIP2GW) Iteration 2: OIP2GW = 21.94 kg

Page 10: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 10 of 64

____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________

CA2013040016 Project #2622-A

Iteration 3 (Box-1313-001 E KOD): Nine (9) 2.38 kg average gross solid product filled metal-in film laminate bags, inner packagings installed upright 3 X 3 within the center special slotted fibreboard container (International Box Code 0204) outer packaging with fibreboard partition system and fibreboard and honeycomb top and bottom pads. The use of other packaging methods or components may render this report invalid. INNER PACKAGING DETAIL #3-1 (ESD Shielding Bag) – Reference Section 8 for drawings

ESD SHIELDING BAG Quantity 9

Style/Description Lead free RoHs Compliant, Stat Shielding bag with heat-sealed sides

Type RoHs Compliant 0217/617 Desco Part # 13366 Owen Part # BAG-0715-F100 7 X 15 Foil Bag Manufacturer Desco Industries, Chino, CA Material of Construction Metal-in film laminate, 3 Mil nominal gauge Minimum Thickness 0.065 mm Nominal Thickness 0.076 mm Dimension (mm, OD), flat 205 x 380 Dimension (mm, ID), flat 170 x 305 Side Seam Width 8.5 mm & 11.9 mm Top Seam Width 5.0 mm, 6.5 mm away from top edge Average Tare Weight 11.4 grams Average Gross Weight (as tested) 2.36 kg Print EMI/STATIC SHIELD

Method of Closure Test material was inserted into bag. Air was expelled from bag, then bag was heat-sealed. Each bag contains 1 steel cylinder filled fibre tube with plastic caps

Bag Width Bag Length

Page 11: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 11 of 64

____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________

CA2013040016 Project #2622-A

PRODUCT/ARTICLES - TEST MATERIAL DETAIL #3-1-1– Reference Section 7 for drawings

FIBREBOARD TUBE Quantity 9

Manufacturer/Supplier T & S Products, Arlington, TX T& S Part # OWEN3.45 X 1.25 Owen Part # TUBE-1786-600 (3.4.25 x1.25 x .555)

Material 26 Plies High Density Paperboard Laminated with PVOH Adhesive

Size (mm, OD), closed 69.6 x 1555 Size (mm, OD) 67.1 x 152.2 Size (mm, ID) 55.4 x 152.2 Caliper 5.63 mm Average Tare Weight 124.4 grams Average Gross Weight 2355.2 grams Average Net Weight 2215.6 grams

PLUGS Quantity 2

Owen Part # CAP-A-1875A Material of Construction Blue plastic

Manufacturer/Supplier Alliance Plastics Company, Erie, PA Nominal Thickness 0.98 mm

Dimension (mm, OD) 68.4 x 26.4 Dimension (mm, ID) 66.0 x 25.3

Average Tare Weight 8.2 grams TUBE SEALING TAPE

Count 18 (2 per tube)

Description 3M Scotch brand Supper 33+ vinyl electrical tape Width X Length 19 mm x 880 mm Thickness 0.16 mm Average Tare Weight 2.9 grams Location Around each fibre tube cap

TEST MATERIAL Quantity 9 (1 per bag)

Style/Description Solid steel cylinder Dimension (mm, OD) 51 x 140.1 Gross Weight 2202 grams Location Placed inside the tube

Page 12: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 12 of 64

____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________

CA2013040016 Project #2622-A

PRODUCT/ARTICLES - TEST MATERIAL DETAIL #3-1-2- Reference Section 7 for drawings

FIBREBOARD TUBE PADS Quantity 27 (3 per tube)

Manufacturer DanHil Containers, LTD, Temple, TX Material 200# DW BC-flute corrugate Owen Part # DIV-1450-210 Dimension (mm, OD), D X H 46.7 x 46.7 Thickness 4.62 mm Average Tare Weight 1.85 grams Location 1 pad was placed over and 2 below the steel cylinder inside each tube

INNER PACKAGING DETAIL #3-1-3 - Reference Section 7 for drawings

DESICCANT BAGS Quantity 4

Manufacturer Desiccare, Inc., Reno, NV

Material Silica Gel, Indicating Silica Gel, Clay, Molecular Sieve and Carbon

Owen Part # PAK-0250-100 Dimension (mm, OD) 57.9 x 10.6 x 87.6 Average Weight 22.0 grams Location Placed outside next to the ESD shielding bags

Overall Inner Packaging Gross Weight (OIP3GW) Iteration 3: OIP3GW = 21.51 kg

Page 13: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 13 of 64

____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________

CA2013040016 Project #2622-A

Iteration 4 (Box-1313-001 C ACE): Five (5) 4.38 kg average gross solid product filled DW fibreboard boxes, inner packagings installed sideways 2 layers high within the center special slotted fibreboard container (International Box Code 0204) outer packaging backfilled with bubble sheets void space fillers. The use of other packaging methods or components may render this report invalid. INNER PACKAGING DETAIL #4-1 – Reference Section 7 for drawings

INNER FIBREBOARD BOX Quantity 5 Style Center Special Slotted Container (CSSC), FEDCO Style: 0204 Manufacturer/Supplier DanHil Containers, LTD, Temple, TX Part # 3838-009

File # 9551 DanHil # 1979-01XXx

Material of Construction Kraft/Kraft Vertical Corrugated, 40H Michelman outside with MRA

Dimension (mm, OD), L X W X H 115 x 112 x 253 Dimension (mm, ID), L X W X H 100 x 100 x 229 (Panel-To-Panel) Double-Wall BC-Flute Double-Wall BC-Flute BMC (Box Marked Certification) 275# (42-26-26-26-42) Tare Weight 152.2 grams Tested Basis Weight (lbs/1000ft²) 115.96 (44.0 – 24.9 – 28.6 – 25.9 – 43.2) Tested Caliper 6.51 mm

Method of Joining Panels Folded inside and stitched with eight (8) 12.5 mm wide staples

Mfr's Joint Flap Size 36 mm Mfr's Joint Location 5-2 corner as per the ASTM diagram Top Flap Gap/Meet Inner: Meet Outer: Meet Bottom Flap Gap/Meet Inner: Meet Outer: Meet Print None Average Gross Weight 4.38 kg Location Placed sideways, 3 on bottom layer and 2 on top layer

INNER BOX SEALING STAPLES – Refer to Section 6 for Closing Instructions Part # 3/4" C34 Stick Staples S-1396 Uline

Description Crown galvanized metal staples Manufacturer/Supplier Uline, Inc. Waukegan, IL Owen Part # STA-1125-0750S Dimension (mm) 18 x 31 (3/4" x 1-1/4") Quantity 4 (2 Top & 2 Bottom) Average Tare Weight 0.8 grams

Arrangement/Pattern Placed along the flap center seams, 38 mm (1-1/2") away from boxes outside edges, 38 mm (1-1/2") apart

Method of Closure See Section 6.2

Page 14: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 14 of 64

____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________

CA2013040016 Project #2622-A

PRODUCT/ARTICLES – ADDITIONAL WEIGHT TEST MATERIAL DETAIL #4-1-1

METAL BLOCKS Quantity 8

Style/Description Solid steel block Dimension (mm, OD) 76 x 76 x 9.4, 428 grams each Overall Gross Weight 3.72 kg

Location Placed on both sides of the barrier bags (to reach the desired weight)

INNER PACKAGING DETAIL #4-1-2 – Reference Section 7 for drawings

BUBBLE WRAP Quantity 3

Style/Description Anti-static bubble wrap Supplier Uline, Inc., Waukegan, IL Part # S-5270 Type 3/16" Bubble Antistatic LDPE Nominal Thickness 4.8 mm (3/16") Dimension (mm, OD) flat 1 X 305 x 1470 & 2 X 12 x 12 Tare Weight 28.2 grams all Location Placed over, below and around the inner articles

Overall Inner Packaging Gross Weight (OIP4GW) Iteration 4: OIP4GW = 21.47 kg

Page 15: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 15 of 64

____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________

CA2013040016 Project #2622-A

Iteration 5 (Box-1313-001 G COR): Fifty (50) 400 grams average gross solid product filled zip-locked anti-stat bags, inner packagings installed 5 x 5 2-layers high within the center special slotted fibreboard container (International Box Code 0204) outer packaging with fibreboard partition systems and fibreboard and honeycomb top and bottom pads and dividers. The use of other packaging methods or components may render this report invalid. INNER PACKAGING DETAIL #5-1 – Reference Section 7 for drawings

ANTI-STAT ZIP-LOC BAG Quantity 50

Style/Description Zip-lock bag with heat-sealed side seams Uline Part # S-3701 Owen Part # BAG-0304-100 Manufacturer Uline, Inc., Waukegan, IL Material of Construction Pink anti-stat LDPE, 3 Mil nominal gauge Minimum Thickness 0.065 mm Nominal Thickness 0.076 mm Dimension (mm, OD), flat 105 x 235 Dimension (mm, ID), flat 103 x 205 Side Seam Width, mm 1.5 mm Top Seam Width, mm 3.0 mm, 24.5 mm away from top edge Average Tare Weight 5.1 grams Average Gross Weight (as tested) 405.2 grams Print None

Method of Closure Test material was inserted into bag, then bag was press-and-seal closed. Each bag contains 1 steel cylinder and 1 Desiccant bag

Bag Width Bag Length PRODUCT/ARTICLES - TEST MATERIAL DETAIL #5-2

METAL CYLINDER Quantity 50

Style/Description Machined metal halo cylinder Material of Construction Steel Manufacturer Owen Oil Tools, Godley, TX Dimension (mm, OD) 51.1 x 25.6 Average Gross Weight 402.2 grams Location Inserted individually within the zip-locked bags

Page 16: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 16 of 64

____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________

CA2013040016 Project #2622-A

INNER PACKAGING DETAIL #5-3 - Reference Section 7 for drawings

DESICCANT BAGS Quantity 50 (1 per bag)

Manufacturer Desiccare, Inc., Reno, NV

Material Silica Gel, Indicating Silica Gel, Clay, Molecular Sieve and Carbon

Owen Part # PAK-0250-100 Dimension (mm, OD), D X H 16.5 x 3.3 x 25.6 Average Gross Weight 0.43 grams Location 1 desiccant bag was placed inside each zip-lock bag

Overall Inner Packaging Gross Weight (OIP5GW) Iteration 5: OIP5GW = 21.23 kg

Page 17: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 17 of 64

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CA2013040016 Project #2622-A

OUTER PACKAGING - Reference Section 7 for drawings

FIBREBOARD BOX – 4G Style Center Special Slotted Container (CSSC), FEDCO Style: 0204 Manufacturer/Supplier All Star Corrugated, Fort Worth TX Part # 1313-001 WHS-275BC

Spec. # 71290

Material of Construction Kraft/Kraft Vertical Corrugated, 40H Michelman outside with MRA

Dimension (mm, OD), L X W X H 354 x 354 x 267 Dimension (mm, ID), L X W X H 344 x 344 x 253 (Panel-To-Panel) Stacking Height (mm) 267 Number of Walls - Flute Type Double-Wall BC-Flute Average Tare Weight 759.4 grams BMC (Box Marked Certification) 275# (42-23-26-23-42) Tested Basis Weight (lbs/1000ft²) 42.78 – 24.85 – 26.78 – 24.19 – 42.13 Combined Weight (lbs/1000ft²) 111.70 Tested Burst Strength (lbs/inch²) 308.5 Tested Caliper 6.68 mm

Method of Joining Panels Stitched withy at least eight (8) 12.5 mm wide staples

Mfr's Joint Flap Size 35 mm Mfr's Joint Location 5-2 corner as per the ASTM diagram Top Flap Gap/Meet Inner: Meet Outer: Meet Bottom Flap Gap/Meet Inner: Meet Outer: Meet Print None

BOX SEALING STAPLES – Refer to Section 6 for Closing Instructions Part # 3/4" C34 Stick Staples S-1396 Uline

Description Crown galvanized metal staples Manufacturer/Supplier Uline, Inc. Waukegan, IL Owen Part # STA-1125-0750S Dimension (mm) 18 x 31 (3/4" x 1-1/4") Quantity 8 (4 Top & 4 Bottom) Average Tare Weight 0.8 grams

Arrangement/Pattern Placed along the flap seam, 38 mm (1-1/2") away from boxes outside edges, 38 mm (1-1/2") apart on both sides & 178 mm (7") apart on center

Method of Closure See Section 6.2

Page 18: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

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Page 18 of 64

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CA2013040016 Project #2622-A

OUTER PACKAGING DETAIL #1 - Reference Section 7 for drawings

PLAIN PAD

Quantity

Iteration 1: 7 Iteration 2: 2 Iteration 3: 4 Iteration 4: 0 Iteration 5: 3

Type Plain corrugated sheet

Material 275# (42/26/26/26/42) Kraft/Kraft BC-Flute Manufacturer/Supplier All Star Corrugated, Fort Worth TX ID 1313-104 WHS File # 113615 Size (mm, OD) 340 x 340 Caliper 6.68 mm Average Tare Weight 101.7 grams

Location

Iteration 1: 1 top, 2 under each tube layer and 2 on bottom Iteration 3: 2 pads were placed on top and 2 on the bottom Iteration 5: 2 pads sandwich the honeycomb pad on top, 1 pad was placed on the bottom

OUTER PACKAGING DETAIL #2 - Reference Section 7 for drawings

POWER CHARGER INSERT

Quantity Iteration 2: 1 Iterations 1, 3, 4, & 5: 0

Type D/C folded corrugated sheet

Material 275# (42/26/26/26/42) Kraft/Kraft BC-Flute Manufacturer/Supplier All Star Corrugated, Fort Worth TX ID PCI-001 POWER CHARGER INSERT Spec. # 202275 Size (mm, OD), flat 925 x 460 Size (mm. OD), set-up 345 x 340 x 244 D/C Opening (mm) 70 Caliper 5.91 mm Tare Weight 273.5 grams

Location Iteration 2: D/C insert with 10 circular openings and 62 mm flanged sides and front

Page 19: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

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Page 19 of 64

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CA2013040016 Project #2622-A

OUTER PACKAGING DETAIL #3 - Reference Section 7 for drawings

LARGE HONEYCOMB PAD

Quantity

Iteration 1: 0 Iteration 2: 4 Iteration 3: 2 Iteration 4: 0 Iteration 5: 4

Material Hexacomb Core Type 4 35# facing

Manufacturer/Supplier Pregis Hexacomb Corporation Manufacturer/Supplier All Star Corrugated, Fort Worth TX Spec # H0899413 Owen Part # PAD-HEX-100 Size (mm, OD) 345 x 3435 Caliper 25.4 mm Average Tare Weight 113.2 grams

Location

Iteration 2: 2 over and 2 bellow Metal-in Film Laminate Bags Iteration 3: 1 over and 1 bellow Metal-in Film Laminate Bags Iteration 3: 1 pad is sandwiched between 2 BC flute top pads, 1 pad was placed on the bottom of box Iteration 5: 2 pads are placed on top (sandwiching plain pad), 1 pad was placed between layers and 1 pad was placed on the bottom over the flat pad

OUTER PACKAGING DETAIL #4 - Reference Section 7 for drawings

SMALL HONEYCOMB FILLER

Quantity Iteration 1: 4 Iterations 2, 3, 4 & 5: None

Material Hexacomb Core Type 4 35# facing

Manufacturer/Supplier Pregis Hexacomb Corporation Manufacturer/Supplier All Star Corrugated, Fort Worth TX Spec # H0687483 Owen Part # PAD-HEX-1X2 Size (mm, OD) 51 x 275 Caliper 25.4 mm Average Tare Weight 14.8 grams Location Iteration 1: These honeycomb fillers were placed around the cutter casing

Page 20: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

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Page 20 of 64

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CA2013040016 Project #2622-A

OUTER PACKAGING DETAIL #5 - Reference Section 7 for drawings

9-CELL PARTITION SYSTEM

Quantity Iteration 3: 1 Iterations 1, 2, 4 & 5: None

Type Interlocked die-cut corrugated sheets Material 275# (42/26/26/26/42) Kraft/Kraft BC-Flute Manufacturer/Supplier DanHil Containers, LTD, Temple, TX Part # 1313-016 PTN File # 7045 Size (mm, OD) 330 x 330 x 150 Cell Size (mm, OD) 85 x 85 x 150 Caliper 6.58 mm Average Tare Weight 323.4 grams

Location Iteration 3: 8 die-cut sheets interlocked with each other forming a 3 X 3 closed cell partition system

OUTER PACKAGING DETAIL #6 - Reference Section 7 for drawings

CORRUGATED TRAY

Quantity Iteration 5: 2 Iterations 1, 2, 3 & 4: None

Type Tray with locking ends Material 200# (42/26/42) Kraft/Kraft B-Flute Manufacturer/Supplier DanHil Containers, LTD, Temple, TX Part # 1313-TRAY File # 43736 Size (mm, OD) 340 x 340 x 51 Size (mm, ID) 325 x 325 x 47 Caliper 3.15 mm Average Tare Weight 148.1 grams

Location Iteration 5: These trays were placed 2 layers high. Each contains 50 bags within the partition system cells

OUTER PACKAGING DETAIL #7 - Reference Section 7 for drawings

25-CELL PARTITION SYSTEM

Quantity Iteration 5: 1 Iterations 1, 2, 3 & 4: None

Type Interlocked die-cut corrugated sheets Material 275# (42/26/26/26/42) Kraft/Kraft BC-Flute Manufacturer/Supplier DanHil Containers, LTD, Temple, TX Part # 1313-016 DIV File # 5797 Size (mm, OD) 320 x 320 x 45 Caliper 5.62 mm Average Tare Weight 100 grams

Location Iteration 5: 8 die-cut sheets interlocked with each other forming a 3 X 3 closed cell partition system

Page 21: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

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Page 21 of 64

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CA2013040016 Project #2622-A

INNER PACKAGING DETAIL #8 – Reference Section 7 for drawings

BUBBLE WRAP

Quantity

Iteration 1: 0 Iteration 2: 2 Iteration 3: 0 Iteration 4: 7 Iteration 5: 0

Style/Description Anti-static bubble wrap Supplier Uline, Inc., Waukegan, IL Part # S-5270 Type 3/16" Bubble Antistatic LDPE Nominal Thickness 4.8 mm (3/16")

Dimension (mm, OD) flat Iteration 2: 300 x 1520 Iteration 4: 3 X 610 x 610 & 4 X 305 x 610

Average Tare Weight Iteration 2: 19 grams Iteration 4: 21.7 grams & 10.9 grams respectively

Location

Iteration 2: These bubble sheets were placed over and around the Metal-in Film Laminate Bags Iteration 4: Larger bubble sheet fills void space on top layer; smaller sheet fills the void space on bottom layer

Overall Outer Package Tare Weight (OPTW)

Iteration 1: OPTW1 = [759.4 + (8 x 0.8)] + (7 x 101.7) + (4 x 14.8) OPTW1 = 765.8 + 711.9 + 59.2 = 1536.9 grams Iteration 2: OPTW2 = [759.4 + (4 x 0.8)] + (2 x 101.7) + 273.5 OPTW2 = 765.8 + 203.4 + 273.5 = 1242.7 grams Iteration 3: OPTW3 = [759.4 + (8 x 0.8)] + (4 x 101.7) + (2 x 113.2) + 323.4 OPTW3 = 765.8 + 406.8 + 226.4 + 323.4 = 1722.4 grams Iteration 4: OPTW4 = [759.4 + (8 x 0.8)] + {{5 x [152.2 x (4 x 0.8) + 28.2} + (3 x 21.7) + (4 x 10.9)} = 765.8 + (5 x 183.6) + 65.1 + 43.6 = 874.6 + 918 OPTW4 = 1792.6 grams Iteration 5: OPTW5 = [759.4 + (8 x 0.8)] + (3 x 101.7) + (4 x 113.2) + (2 x 148.1) + (2 x 100) = 765.8 + 305.1 + 452.8 + 296.2 + 200 OPTW5 = 2019.9 grams

Page 22: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

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CA2013040016 Project #2622-A

SECTION 3 – TEST DESCRIPTIONS & TEST RESULTS

Drop Test – 49 CFR 178.603

Test Specimen/Contents Characteristics -

Number of Packages Tested 25 (5 for each iteration) Packing Group Number PG II Product State Solid Dummy Load (Liquid) Steel disks or blocks & sand Drop Height Multiplier 0.67 for PG III; 1 for PG II & 1.5 for PG I Drop Height Used 1.2 m Conditioning Temperature & Duration, 49 CFR178.603(c) 24 Hours @ 73 °F & 50 % R.H. Content (Dummy Load) Test Temperature 73 °F & 50 % R.H.

Test Method -

• The inner packagings were filled to 95% overflow capacity with solid dummy load. • The packages were assembled as per closing instruction (Reference Section 6). • Assembled packages were dropped onto a solid steel plated concrete floor. • Drops were conducted within 60 seconds of removal of the assembled packages from the

conditioning chamber.

Drop Test Results - Iteration 1

Drop / Sample #

Test Weight (kg) Box Orientation Results

1-1 23.08 Top (mfr's) corner (Corner 1-2-5)

Box outside impact corner was slightly crushed around, approximately 3" in diameter, however box was still in-tact

and capable and safe for further handling. There was no leakage of the filling substance

1-2 22.99 Top surface (Face 1) There was no visible damage to the outer packaging, there was no leakage of the filling substance

1-3 23.09 Short side (Face 5) There was no visible damage to the outer packaging, there was no leakage of the filling substance

1-4 23.01 Long side (Face 2) There was no visible damage to the outer packaging, there was no leakage of the filling substance

1-5 23.11 Bottom surface (Face 3) There was no visible damage to the outer packaging, there was no leakage of the filling substance

Drop 1 – Top Corner

Drop 2 – Top Surface

Drop 3 – Short Side

Drop 4 – Long Side

Drop 5 – Bottom Surface

Page 23: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

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CA2013040016 Project #2622-A

Drop Test Results - Iteration 2

Drop / Sample #

Test Weight (kg) Box Orientation Results

2-1 22.98 Top (mfr's) corner (Corner 1-2-5)

Box outside impact corner was slightly crushed around, approximately 3" in diameter, however box was still in-tact

and capable and safe for further handling. There was no leakage of the filling substance

2-2 23.01 Top surface (Face 1) There was no visible damage to the outer packaging, there was no leakage of the filling substance

2-3 23.03 Short side (Face 5) There was no visible damage to the outer packaging, there was no leakage of the filling substance

2-4 23.01 Long side (Face 2) There was no visible damage to the outer packaging, there was no leakage of the filling substance

2-5 23.06 Bottom surface (Face 3) There was no visible damage to the outer packaging, there was no leakage of the filling substance

Drop 1 – Top Corner

Drop 2 – Top Surface

Drop 3 – Short Side

Drop 4 – Long Side

Drop 5 – Bottom Surface

Drop Test Results - Iteration 3

Drop / Sample #

Test Weight (kg) Box Orientation Results

3-1 23.02 Top (mfr's) corner (Corner 1-2-5)

Box outside impact corner was slightly crushed around, approximately 3" in diameter, however box was still in-tact

and capable and safe for further handling. There was no leakage of the filling substance

3-2 23.03 Top surface (Face 1) There was no visible damage to the outer packaging, there was no leakage of the filling substance

3-3 23.04 Short side (Face 5) There was no visible damage to the outer packaging, there was no leakage of the filling substance

3-4 23.05 Long side (Face 2) There was no visible damage to the outer packaging, there was no leakage of the filling substance

3-5 2305 Bottom surface (Face 3) There was no visible damage to the outer packaging, there was no leakage of the filling substance

Drop 1 – Top Corner

Drop 2 – Top Surface

Drop 3 – Short Side

Drop 4 – Long Side

Drop 5 – Bottom Surface

Page 24: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 24 of 64

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CA2013040016 Project #2622-A

Drop Test Results - Iteration 4

Drop / Sample #

Test Weight (kg) Box Orientation Results

4-1 23.05 Top (mfr's) corner (Corner 1-2-5)

Box outside impact corner was slightly crushed around, approximately 3" in diameter, however box was still in-tact

and capable and safe for further handling. There was no leakage of the filling substance

4-2 23.03 Top surface (Face 1) There was no visible damage to the outer packaging, there was no leakage of the filling substance

4-3 23.02 Short side (Face 5) There was no visible damage to the outer packaging, there was no leakage of the filling substance

4-4 23.04 Long side (Face 2) There was no visible damage to the outer packaging, there was no leakage of the filling substance

4-5 22.95 Bottom surface (Face 3) There was no visible damage to the outer packaging, there was no leakage of the filling substance

Drop 1 – Top Corner

Drop 2 – Top Surface

Drop 3 – Short Side

Drop 4 – Long Side

Drop 5 – Bottom Surface

Drop Test Results - Iteration 5

Drop / Sample #

Test Weight (kg) Box Orientation Results

5-1 23.10 Top (mfr's) corner (Corner 1-2-5)

Box outside impact corner was slightly crushed around, approximately 3" in diameter, however box was still in-tact

and capable and safe for further handling. There was no leakage of the filling substance

5-2 23.01 Top surface (Face 1) There was no visible damage to the outer packaging, there was no leakage of the filling substance

5-3 23.11 Short side (Face 5) There was no visible damage to the outer packaging, there was no leakage of the filling substance

5-4 23.05 Long side (Face 2) There was no visible damage to the outer packaging, there was no leakage of the filling substance

5-5 22.92 Bottom surface (Face 3) There was no visible damage to the outer packaging, there was no leakage of the filling substance

Drop 1 – Top Corner

Drop 2 – Top Surface

Drop 3 – Short Side

Drop 4 – Long Side

Drop 5 – Bottom Surface

Page 25: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

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CA2013040016 Project #2622-A

Drop Test Pass/Fail Criteria -

A package is considered to successfully pass the drop tests if for each sample tested: • For packaging containing liquid, there is no leakage of the filling substance from the inner packaging. • There is no damage to the outer packaging likely to adversely affect safety during transport. • Inner receptacles, inner packagings or articles must remain completely within the outer packaging. • Any discharge from a closure is slight and ceases immediately after impact or pressure equalization with no further

leakage. • No rupture is permitted in packagings for materials in Class 1 which would permit spillage of loose explosive

substances or articles from the outer packaging.

Stacking Test - 49 CFR 178.606 (See Section 5.2 for Calculation)

Test Specimen/Contents Characteristics Number of Packages Tested 15 (3 for each iteration) Product State Solid Dummy Load (Solid) Steel disks or blocks & sand Conditioning of Outer Packaging - 49 CFR 178.602(d) 24 Hours @ 73 °F & 50 % R.H. Test Temperature 73 °F & 50 % R.H. Test Method Free standing, static (dead weight) test Test Duration 24 hours Minimum calculated stacking test weight 250.8 kg (551.76 lbs) per package Actual stacking test weight 256.5 kg (565 lbs) per package Test Method -

The inner packagings were filled to 95% overflow capacity with dummy load. The packages were assembled as per closing instruction (Reference Section 6). Stacking test load (dead weight) of 256.5 kg was applied individually to the top of the three (3) assembled packages per iteration using wood load spreaders and the weight was maintained for 24 hours.

Test Results – Iteration 1

Test Sample # Test Sample Weight (kg)

Test Load (Kg) Duration Stacking Test Results

1-6 23.01 256.5 24 Hours

Boxes did not show any signs of

deterioration or distortion, there was

no leakage of the filling substance

1-7 23.01 256.5 24 Hours

1-8 23.28 256.5 24 Hours

Page 26: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

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CA2013040016 Project #2622-A

Stacking Test Results – Iteration 2

Test Sample # Test Sample Weight (kg)

Test Load (Kg) Duration Stacking Test Results

2-6 23.11 256.5 24 Hours

Boxes did not show any signs of

deterioration or distortion, there was

no leakage of the filling substance

2-7 23.05 256.5 24 Hours

2-8 23.17 256.5 24 Hours

Stacking Test Results – Iteration 3

Test Sample # Test Sample Weight (kg)

Test Load (Kg) Duration Stacking Test Results

3-6 22.99 256.5 24 Hours

Boxes did not show any signs of

deterioration or distortion, there was

no leakage of the filling substance

3-7 22.94 256.5 24 Hours

3-8 23.22 256.5 24 Hours

Stacking Test Results – Iteration 4

Test Sample # Test Sample Weight (kg)

Test Load (Kg) Duration Stacking Test Results

4-6 23.00 256.5 24 Hours

Boxes did not show any signs of

deterioration or distortion, there was

no leakage of the filling substance

4-7 23.25 256.5 24 Hours

4-8 23.25 256.5 24 Hours

Page 27: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

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CA2013040016 Project #2622-A

Stacking Test Results – Iteration 5

Test Sample # Test Sample Weight (kg)

Test Load (Kg) Duration Stacking Test Results

5-6 23.03 256.5 24 Hours

Boxes did not show any signs of

deterioration or distortion, there was

no leakage of the filling substance

5-7 23.08 256.5 24 Hours

5-8 23.21 256.5 24 Hours

Pass/Fail Criteria -

A package is considered to successfully pass the stack tests if for each sample tested: • No test sample shows any deterioration or distortion that could adversely affect safety during transport causing

instability in stacks of packages, or cause damage to inner packagings that is likely to reduce safety in transport. • There no leakage of the filling substance from the inner receptacle, or inner packaging.

Page 28: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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CA2013040016 Project #2622-A

Vibration Test - 49 CFR 178.608

Test Specimen/Contents Characteristics -

Number of Packages Tested 15 (3 simultaneously, 3 samples from each iteration, same samples used for stacking test)

Product State Solid Dummy Load (Solid) Steel disks or blocks & sand Conditioning of Outer Packaging - 49 CFR 178.602(d) 24 Hours @ 73 °F & 50 % R.H. Test Temperature Ambient Test Method ASTM D999-08 Rotary Motion Vibration Test Duration 60 minutes Test Frequency 235 CPM

Test Method -

The inner packagings were filled to 95% overflow capacity with dummy load. The packages were re-assembled as per closing instruction (Reference Section 6). Three (3) assembled packages from each iteration were simultaneously placed on a rotary vibration table platform having 25.4 mm peak-to-peak displacement and vibrated in normal shipping orientation for one (1) hour at 235 CPM such that a 1.6 mm thickness could be passed between the bottom of the samples and the platform. Immediately thereafter, the packages were removed from the platform and turned on its side for examination.

Test Results - Iterations 1 & 2

Test Sample # Test Sample Weight (kg)

Frequency (CPM)

Duration (Minutes) Vibration Test Results

1-6 23.01 235 60

There was no rupture or

deterioration of boxes, there was no

leakage of the filling substance

1-7 23.01 235 60

1-8 23.28 235 60

2-6 23.11 235 60

There was no rupture or

deterioration of boxes, there was no

leakage of the filling substance

2-7 23.05 235 60

2-8 23.17 235 60

Page 29: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

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CA2013040016 Project #2622-A

Vibration Test Results - Iterations 3, 4 & 5

Test Sample # Test Sample Weight (kg)

Frequency (CPM)

Duration (Minutes) Vibration Test Results

3-6 22.99 235 60

There was no rupture or

deterioration of boxes, there was no

leakage of the filling substance

3-7 22.94 235 60

3-8 23.22 235 60

4-6 23.00 235 60

There was no rupture or

deterioration of boxes, there was no

leakage of the filling substance

4-7 23.06 235 60

4-8 23.25 235 60

5-6 23.03 235 60

There was no rupture or

deterioration of boxes, there was no

leakage of the filling substance

5-7 23.08 235 60

5-8 23.21 235 60

Vibration Test Pass/Fail Criteria -

A package is considered to successfully pass the vibration test, if for each sample tested after it was immediately removed from table platform and turned on its side: • There is no leakage or rupture from any of the packaging. • No test sample shows any deterioration which could adversely affect safety or container strength, during transport

liable to reduce packaging strength.

Page 30: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

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CA2013040016 Project #2622-A

Cobb (Water Absorption) Test - 49 CFR 178.516

Test Specimen/Contents Characteristics - Number of Samples Tested 5 Test Duration 30 Minutes Test Intensity 100 mL Distilled Water Conditioning of Test Samples 24 Hours @ 73 °F & 50 % R.H. Test Method - ISO International Standard 535-1976 (E), Cobb Method

Test Results -

Sample # #1 #2 #3 #4 #5 Average Results

grams/m² 117.4 120.8 116.3 113.8 113.2 116.3 Pass

Pass/Fail Criteria -

• An increase in mass of greater than 155 grams/m² over the 30-minute duration of the tests represents an unacceptable level of water absorption

SECTION 4 – SHIPPERS RESPONSIBILITY

• It is the responsibility of the end shipper to determine authorization for use under these regulations. • It is the shippers responsibility to determine if the packaging is compatible for products to be shipped. • Use of the marking of this certification for any variations without further testing as allowed under US DOT 49

CFR Section 178.601 will be at complete responsibility of the shipper. By continuing to place the UN Markings on Packagings, the packaging manufacturer or shipper is certifying that each packaging is constructed in the same manner as the originally tested and certified packaging, and that each packaging is capable of withstanding the prescribed performance tests.

• According to 49 CFR Section 178.601 (1) Variation 1 - variations are permitted in inner packaging of a tested combination packaging without further testing of the package, provided an equivalent level of performance is maintained as described in 178.601 (1) Variation 4 (i),(A),(B),(C),(D),(E) and (F) and (ii).

• According to US DOT 49 CFR Section 178.601 (e), the packaging manufacturer shall achieve successful test results for the periodic retesting at intervals established by the manufacturer of sufficient frequency to ensure that each packaging produced by manufacturer is capable of passing the design qualification test. Changes in retest frequency are subject to the approval of the Associate Administrator for Hazardous Materials Safety. For combination packaging, the periodic retest must be conducted at least once every 24 months.

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CA2013040016 Project #2622-A

SECTION 5 - CALCULATIONS

5.1 Certified Package Gross Mass Calculations Based on Test Level

Overall Inner Package Gross Weight (OIPGW)

Iteration 1: 21.75 kg Iteration 2: 21.94 kg Iteration 3: 21.51 kg Iteration 4: 21.47 kg Iteration 5: 21.23 kg

Overall Outer Package Tare Weight (OPTW)

Iteration 1: 1536.9 grams Iteration 2: 1242.7 grams Iteration 3: 1722.4 grams Iteration 4: 1792.6 grams Iteration 5: 2019.9 grams

Test Material Specific Gravity (TMSG) - Packing Group Number II

Minimum Package Weight as Tested (PGW)

Iteration 1: 22.99 kg Iteration 2: 22.98 kg Iteration 3: 22.94 kg Iteration 4: 22.95 kg Iteration 5: 22.92 kg

Packing Group Multiplication Factor (PMF) 1.0

Formula for Calculating Certified Gross Mass

(CGW)

CGW = Minimum PGW

CGW = Minimum PGW = 22.92 kg CGW = 22.8 kg (50.16 lbs)

Certified Package Marking Y = 22.8 (50.16 lbs)

5.2 Stacking Strength Test Calculations

Test Load (TL) TL = [(SH - PH) - 1] x CGW (static)

TL = [(SH - PH) - 1] x CGW x 1.5 (dynamic)

Overall Stacking Height of Packages (SH) 3000 mm (10 feet)

Overall Stacking Height of Package (PH) 267 mm

TL (Static)

TL = [(3000/267) - 1] x 22.8 = 14 (rounded up) x 22.8

TL = 250.8 kg (551.76 lbs)

Rounded up to at 256.5 kg (565 lbs) per package for test purposes

Page 32: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Appendix A – Regulatory & Industry Standard References

Regulatory Standard References:

Test 1. 2. 3. 4. 5.

49 CFR UN Regulation IMDG ICAO IATA

Drop Test 178.603 6.1.5.3 6.1.5.3 6.4.3 6.3.3

Stacking Test 178.606 6.1.5.6 6.1.5.6 6.4.6 6.3.6

Hydrostatic Pressure 173.27(c) 4.1.1.4 4.1.1.4 4.1.1.6 5.0.2.9

Cobb Test 178.516 6.1.4.12.1 6.3.11.1 6.2.12.2

Vibration Test 178.608 - - 4.1.1.1 5.0.2.7

1. United States Code of Federal Regulations (CFR), Title 49, Transportation, Parts 100-199 2. The United Nations Recommendations on The Transport of Dangerous Goods – Model Regulations (Orange Book) 3. International Maritime Dangerous Goods Code (IMDG) 4. Technical Instructions for the Safe Transport of Dangerous Goods by Air (ICAO) 5. International Air Transport Association (IATA), Dangerous Goods Regulations

Industry Standard References:

Drop Test ASTM D5276 Standard Test Method for Drop Test of Loaded Containers by Free Fall

Stacking Test ASTM D4577 Standard Test Method for Compression Resistance of a Container Under Constant Load

Hydrostatic Pressure ASTM D7660 Standard Guide for Conducting Internal Pressure Tests on United Nations

(UN) Packagings

Cobb Test ISO 535 Paper and Board – Determination of Water Absorption – Cobb Method

Vibration Test ASTM D999 Standard Test Method for Vibration Testing of Shipping Containers

• American Society for Testing and Materials (ASTM) • International Organization for Standardization (ISO)

Page 33: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Appendix B – Test Equipment & Instrumentation

No. Test Machine, Model # and Serial # Capacity Calibration

Date Re-Calibration

Date

1. Drop Table, Lansmont Corporation: Model #PDT-56-ED; Serial #M-1245 11" ÷ 72" 2/22/2019 2/22/2020

2. Drop Table, Gaynes Eng. Inc., Serial #G-13673-2 12" ÷ 120" 2/22/2019 2/22/2020 3. Vibration Table, Gaynes Eng. Inc.: Model #6000V 3000 lbs 2/22/2019 2/22/2020

4. Compression Machine, TechLab Systems: Model #Validator; S/N #1005971T078 5000 lbs 2/22/2019 2/22/2020

5. VWR Traceable Digital Thermometer: Serial #51234531 (for Conditioning, Freezer), -58° ÷ 302° F 2/13/2019 2/13/2020

6. AMETEK Digital Thermometer: Model #DT-8350 -50° ÷ 450° F 2/22/2019 2/22/2020

7. Paperless Temperature & Humidity Recorder, Dickson: Model #TH660 (for Cold Chamber) -148° ÷ 350° F 2/22/2019 2/22/2020

8. Paperless Temperature & Humidity Recorder, Dickson: Model #TH635 (for Conditioning Room)

-140° ÷ 185° F, 0% ÷ 95% RH 2/22/2019 2/22/2020

9. Thermometer & Hygrometer, Omega Engineering: Model #RH520 (for Hot Chamber)

-20° ÷ 140° F, 10% ÷ 95% RH 2/22/2019 2/22/2020

10. Bench Scale, SeiKo Scale Division: Model #WA200001XP; S/N #160808009 10mg ÷ 20 kg 5/16/2019 5/16/2020

10. Mettler Toledo D-72458 Albstadt: Model #BBK-462-35ST; S/N #2986871-7CK 0 ÷ 35 kg 4/19/2019 4/19/2020

11. Mettler Toledo D-72458 Albstadt: Model #XS16001L; S/N #B112123112 0 ÷ 16.1 kg 4/19/2019 4/19/2020

12. Analytical Balance, PCA, Germany: Model #AB200; S/N #2626 10mg ÷ 200 g 5/16/2019 5/16/2020

13. Bench Scale, Ohaus: Serial #5040335-5XZ 0 ÷ 200 lbm 5/16/2019 5/16/2020

14. Caliper, Fowler: Model #54-100-112-1 ; S/N: 1205A58182 0 ÷ 12" 5/16/2019 5/16/2020

15. Mitutoyo Cor. Micrometer: Model #Absolute Digimatic CD-8C; S/N: 4934 0 ÷ 6" 5/16/2019 5/16/2020

16. Electronic Torque-Meter, Kaps-All: Model #EB-650; S/N #11051 3 ÷ 100 inch-lbs 4/19/2019 4/19/2020

17. Toque Wrench, CDI, Model No. 301LDIN 0 ÷ 30 inch-lbs 5/16/2019 5/16/2020

18. Omega Digital Pressure Gauge: Model #DPG7010-200; S/N #1305276 0 ÷ 200 psi 5/15/2019 5/15/2020

19. Omega Digital Pressure Gauge: Model #DPG8001-30V30; S/N #16121406000 -30" ÷ 30 psi 2/13/2019 2/13/2020

20. Winters Pressure Gauge, WG2-6 0 - 60 psi 5/16/2019 5/16/2020

21. Ashcroft Pressure Gauge, V/300 Psi Model #DG 25: S/N #16080906005 -30 - 300 psi 10/21/2018 10/21/2019

22. The Mullen Tester, B.F Perkins and Son: Serial #14047 0 ÷ 800 psi 0 ÷ 300 psi 5/16/2019 5/16/2020

23 The Mullen Tester, B.F Perkins and Son: Serial #2180 0 ÷ 800 psi 0 ÷ 1500 psi 5/16/2019 5/16/2020

24. ECT Tester, Testing Machines, Inc.: S/N #13748 0 ÷ 120 lbs 5/16/2019 5/16/2020 25. Measuring Tape, Ultra-Touch: ANAMA TM1 & TM2 0 ÷ 25 Feet 5/16/2019 5/16/2020

26. Measuring Tape, Stanley Power Lock, 33-425; ANAMA TM3 0 ÷ 25 Feet 5/16/2019 5/16/2020

27. Measuring Tape, Made In China; ANAMA TM4 0 ÷ 25 Feet 5/16/2019 5/16/2020

28. Presto Dart Impact Tester, Model No. PDI-350; S/N: 2010167076 21" ÷ 1.7 feet 2/22/2019 2/22/2020

Page 34: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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SECTION 6 – PACKAGING ASSEMBLY (CLOSING) INSTRUCTIONS

Note: Packages were re-assembled same way as received.

Iteration 1 - Step-By-Step Packaging Assembly Demonstration

Inner Packaging Components

Casing Cutter Erected Box 2 Plain Bottom Pads Casing Cutter Installation

8 Large Tubes & 4 Hexacomb Pads 4 Plain Layer Dividers 1 Bottom Layer Tubes

Installation 1 Plain Layer Divider 2

Top Layer Tubes Installation 1 Plain Top Pad Box Top Closure Pattern Box Bottom Closure

Pattern

Page 35: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Iteration 2 - Step-By-Step Packaging Assembly Demonstration

Inner Packaging Components 1 Plain Bottom Pad Installation

Die-Cut Flanged Insert Installation

Inner Packaging Installation 1 Plain Top Pad Installation Box Top Closure Pattern Box Bottom Closure

Pattern

Page 36: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Iteration 3 - Step-By-Step Packaging Assembly Demonstration

Inner Packaging Components

Closed ESD Shielding Bags Erected Box 1 Plain Bottom Pad 1 Hexacomb Bottom Pad

Partition System Installation

ESD Shielding Bags Installation 1 Plain Top Pad 1 Hexacomb Top Pad

Box Top Closure Pattern Box Bottom Closure Pattern

Page 37: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Iteration 4 - Step-By-Step Packaging Assembly Demonstration

Inner Packaging Components

5 Closed Inner Boxes Erected Outer Box 1 Plain Bottom Pad Bottom Layer Inner Boxes

Bottom Layer Bubble Wrap Installation Top Layer Inner Boxes Top Layer Bubble Wrap

Installation 1 Plain Top Pad

Box Top Closure Pattern Box Bottom Closure Pattern

Page 38: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Iteration 5 - Step-By-Step Packaging Assembly Demonstration

Inner Packaging Components

Closed Zip-Locked Bags 2 Product Filled Trays Erected Box 1 Plain Bottom Pad

1 Hexacomb Bottom Pad Bottom Layer Filled Tray Installation 1 Hexacomb Divider Pad Top Layer Filled Tray

Installation

1 Hexacomb Top Pad 1 1 Plain Top Pad 1 Hexacomb Top Pad 2

Box Top Closure Pattern Box Bottom Closure Pattern

Page 39: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Manufacturer’s Closing Instructions:

Iteration 1:

Page 40: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Iteration 2:

Page 41: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Iteration 2 (Continued):

Page 42: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Iteration 2 (Continued):

Page 43: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Iteration 3:

Page 44: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Iteration 4:

Page 45: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Iteration 5:

Page 46: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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SECTION 7 – PACKAGE SPECIFICATIONS & DRAWINGS

Fibre Tube Specification – Iteration 1, CUT-8250

Page 47: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 47 of 64

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Fibre Tube Specification – Iteration 1, CUT-8250

Page 48: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 48 of 64

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Barrier Bag Specification – Iteration 1

Page 49: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 49 of 64

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Barrier Bag Specification – Iteration 1

Page 50: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Barrier Bag Specification – Iteration 3

Page 51: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 51 of 64

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Fibre Tube Specification – Iteration 3

Page 52: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Desiccant Bag Specification

Page 53: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Inner Box Drawing & Specification – Iteration 4

Page 54: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 54 of 64

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Anti-Stat Bag Specification – Iteration 5

Page 55: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Outer Box Drawing & Specification

Page 56: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Plain Pad Drawing & Specification

Page 57: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 57 of 64

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Honeycomb Pad Drawing & Specification

Page 58: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 58 of 64

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Honeycomb Pad Drawing & Specification

Page 59: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 59 of 64

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Power Charger Insert Drawing & Specification

Page 60: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 60 of 64

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9-Cell Partition Drawing & Specification

Page 61: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 61 of 64

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25-Slot Partition Drawing & Specification

Page 62: DEPARTMENT OF TRANSPORTATION PERFORMANCE … 2019.10.17.pdfANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under §107.403 and

Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 62 of 64

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Corrugated Tray Drawing & Specification

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Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

Page 63 of 64

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Anti-Static Sheet Specification

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Owen Oil Tools, Inc. Certification #+CM0471

Date of Report: 10/17/2019 Periodic Retest Date: 10/17/2021

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Carton Sealing Staples Specification