final analytical report - records collections · the results apply only to the samples tested. this...

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

Region 6 Laboratory . Environmental Services Branch

10625 Fallstone Road, Houston, TX 77099 Phone: (281)983-2100 Fax: (281)983-2248

Final Analytical Report

13 J U L - ! PH U-3U

i .vi .•;•' •!*

Site Name Marion Pressure Treating

Sample Collection Date(s)~ 03/24/13 - 03/26/13

Contact- Bart Canellas (6SF-RL)

Report Date 06/11/13

Project # 13SF074

Work Order(s) 1303019 1303021 1303022

Analyses included in this report:

Chloride 300.0 (#) Nitrate - 353.2 Nitrite - 353.2 Sulfide 376.2

Report Narrative

Sample Management:

Metals ICP CLP Nitrate + Nitrite 353.2 Sulfate 300.0 Total Organic Carbon

686467

This report contains the chloride, nitrate, nitrite, nitrate-l-mtrite, sulfate, sulfide, and TOC are analyses done by the TCEQ Laboratory as well as the redigestion/reanalysis of sample 1303019-09 for metals by ICP. The semi-volatile and total metals data was previously reported.

Metals ICP:

Batch B3E0905:

Sample 1303019-09 was re-digested and analyzed due to prior QC problems. The prior analysis for the sample matrix spike and matrix spike duplicate had nearly all unacceptable recoveries except for the major analytes. Following the re-digestion and analysis the afifected analytes now fall within acceptable control limits. A corrective action (CA) was initiated and states a likely pipette malfimction as the reason for the initial QC failures.

MSl/MSDl: The sample concentration for iron exceeds the spike added concentration by a factor of foiu" or more and can not be reliably calculated.

005498

Report Narrative (cont'd)

TCEQ Data:

TOC-NPOCB:

Sample 1303019-06: The reproducibility of replicate sample injections was 17.94%, which is outside the acceptance limits of 10%. At low concentrations the variability of the measurement increases. The data is not likely afifected.

Sample 1303019-08: The reproducibility of replicate sample injections was 32.83%, which is outside acceptance limits of 10%. At low concentrations the variability of the measiu-ements increases. The data is not likely affected.

Sample 1303021-03: The reproducibility of replicates sample injections was 11.90%, which is outside the acceptance limits of 10%. At low concentrations the variability of measurements increase. The data is not likely afifected.

Sample 1303021-06: The reproducibility of replicate sample injections was 15.36%, which is outside the acceptance limits of 10%. At low concentrations the variability of the measurements increases. The data is not likely afifected.

Sample 1303021-07: The reproducibility of replicate sample injections was 16.39%, which is outside the acceptance limits of 10%. At low concentrations the variability of the measurements increase. The data is not likely affected.

N02:

Sample 1303019-08: The matrix spike recovery was 192%,which is outside of the acceptance limits. The precision of the matrix spike and the matrix spike duplicate was 73.7%, which is outside acceptance limits. The data is likely afifected.

Standard procedures for quality assurance and quality control were followed in the analysis and reporting of the sample results. The results apply only to the samples tested. This final report should only be reproduced in full.

Reporting limits are adjusted for sample size and matrix interference.

Lichard McMilliir ' ^ David Neleigh Region 6 Laboratory Manager Region 6 Laboratory Br^ch Chief

005499

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

Region 6 Environmental Services Branch Laboratory

10625 Fallstone Road Houston, Texas 77099

Sample Receipt and Disposal

Site Name: Marion Pressure Treating Project Number: 13SF074

Data Management Coordinator: Christy Warren

Data Management Coc^nator Signature Date

Date Transmitted: C^ / ( ( / 1 ^

Please have the U.S. EPA Project Manager/OfiBcer call the Data Management Coordinator at 3-2137 for any comments or questions.

Please sign and date this form below and return it with any comments to:

Christy Warren Data Management Coordinator Region 6 Laboratory 6MD-HS

/ / Received by and Date

Comments:

The laboratory routinely disposes of samples 90 days after all analyses have been completed. If you have a need to hold these samples in custody longer than 90 days, please sign below.

Signature Date

Please provide a reason for holding:

005500

Environmental Protection Agency

Region 6 Laboratory 10625 Fallstone Road, Houston, TX 77099

Phone:(281 )983-2100 Fax:(281)983-2248

ANALYTICAL REPORT FOR SAMPLES

Station ID Laboratory ID Sample lype Date Collected Date Received

MW-1

MW-15

MW-15-D

MW-18

MW-21

MW-4

MW-5

MW-16

MW-2

MW-20

MW-20-D

MW-3

1303019-03

1303019-04

1303019-05

1303019-06

1303019-07

1303019-08

1303019-09

1303021-03

1303021-05

1303021-06-

1303021-07

1303021-09

Liquid

Liquid

Liquid

Liquid

Liquid

Liquid

Liquid

Liquid

Liquid

Liquid

Liquid

Liquid

3/25/13

3/25/13

3/25/13

3/25/13

3/25/13

3/25/13

3/24/13

3/26/13

3/26/13

3/26/13

3/26/13

3/26/13

11:25

8:56

8:56

13:55

11:48

9:30

10:30

8:45

13:00

9:39

9:39

10:25

03/26/13 09:10

03/26/13 09:10

03/26/13 09:10

03/26/13 09:10

03/26/13 09:10

03/26/13 09:10

03/26/13 09:10

03/27/13 09:20

03/27/13 09:20

03/27/13 09:20

03/27/13 09:20

03/27/13 09:20

ReportName: 1303019,1303021,1303022 FINAL06 11 13 1452 Page 1 of 27 005501



Phone:(281)983-2100 Fax:(281)983-2248

Lab ID: 1303019-09RE1 Batch: B3E0905 SampleType: Liquid

Metals by CLP ILM05.3 - ICP

Date Collected: 03/24/13 Sample Vol: 50ml

Station ID: MW-5

Sample Qualifiers:

Targets

Analyte (CAS Number) Result lig/L

U 107 U

u 8,390

U

u u

18,000 3,160 258 U

2,400 U

19,000

u u

Analyte Qualifiers

Reporting Limit

100 10.0 5.0 5.0 150 10.0 20.0 20.0 25.0 150 5.0

20.0 1,000 10.0 500 20.0 20.0

Dilution Prepared Analyzed Aluminum (7429-90-5) Barium (7440-39-3) Beryllium (7440-41-7) Cadmium (744043-9) Calcium (7440-70-2) Chromium (7440-47-3) Cobalt (7440-48-4) Copper (7440-50-8) Iron (7439-89-6) Magnesium (7439-95-4) Manganese (7439-96-S) Nickel (7440-02-2) Potassium (7440-09-7) Silver (7440-22-4) Sodium (7440-23-5) Vanadium (7440-62-2) Zinc (7440-66-6)

1 05/09/13 05/14/13

ReportName: 1303019,1303021,1303022 FINAL 06 11 13 1452 Page 2 of27 005502



Phone:(281)983-2100 Fax:(281)983-2248

Metals by CLP ILM05.3 - ICP - QuaUty Control

Batch: B3E0905 Sample Type: Liquid

Blank (B3E0905-BLK1) Prepared: 5/9/2013 Analyzed: 5/14/2013

Targets

ANALYTE Result AnalyteReporting ^g/L Qualifiers Limit

Aluminum Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron

Magnesiimi Manganese

Nickel Potassixmi Silver

Sodium

Vanadium Zinc

u u u u u u u u u u u u u u u u u

100

10.0

5.0

5.0

150

10.0

20.0

20.0

25.0

150

5.0

20.0

1,000

10.0

500

20.0

20.0

LCS (B3E0905-BS1) Prepared: 5/9/2013 Analyzed: 5/14/2013

Targets

ANALYTE Result AnalyteReporting Spike fig/L Qualifiers Limit Level

%REC %REC Limits

Aluminum Barium Beryllium Cadmium

Calcium Chromium

953

1,810

46.4

46.4

92,200

368

100

10.0

5.0

5.0

150

10.0

1,000

2,000

50.0

50.0

100,000

400

95.3

90.5

92.8

92.8

92.2

92.0

75-125

75-125

75-125

75-125

75-125

75-125




Phone:(281)983-2100 Fax:(281)983-2248

Metals by CLP ILM05.3 - ICP - Quality Control

Batch: B3E0905 Sample lype: Liquid

LCS (B3E0905-BS1) Prepared: 5/9/2013 Analyzed: 5/14/2013

Targets (Continued)

ANALYTE Result AnalyteReporting Spike ^g/L Qualifiers Limit Level

%REC %REC Limits

Cobalt Copper Iron Magnesium Manganese Nickel Potassium Silver Sodium Vanadium Zinc

175

361

923

94,300

357

341

98,000

41.9

93,800

381

867

20.0

20.0

25.0

150

5.0

20.0

1,000

10.0

500

20.0

20.0

200

400

1,000

100,000

400

400

100,000

50.0

100,000

400

1,000

87.5

90.4

92.3

94.3

89.3

85.3

98.0

83.9

93.8

95.1

86.7

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

Source: 1303019-09RE1 Matrix Spike (B3E0905-MS1)

Prepared: 5/9/2013 Analyzed: 5/14/2013

Targets

ANALYTE Result AnalyteReporting Spike Som-ce ^g/L Qualifiers Limit Level Result %REC

%REC Limits

Aluminum Barium Beryllium

Cadmium Calcium

Chromium Cobalt

Copper Iron

Magnesium

Manganese

Nickel

964

1,940

46.2 .

46.6

99,700

364

171

364

16,800

97,500

591

333

100

10.0

5.0

5.0

150

10.0

20.0

20.0

25.0

150

5.0

20.0

1,000

2,000

50.0

50.0

100,000

400

200

400

1,000

100,000

400

400

14.0

107

0.04

1.1

8,390

18,000

3,160

258

0.4

95.0

91.5

92.4

90.8

91.3

90.9

85.6

91.0

NR '

94.3

83.3

83.2

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

»75-125

75-125

75-125

75-125




Phone:(281)983-2100 Fax:(281)983-2248

Metals by CLP ILM05.3 - ICP - Quality Control

Batch: B3E0905 Sample lype: Liquid

Source: 1303019-09RE1 Matrix Spike (B3E0905-MS1)

Prepared: 5/9/2013 Analyzed: 5/14/2013 .

^Targets (Continued)

ANALYTE Result AnalyteReporting Spike Source %REC Hg/L Qualifiers Limit Level Result %REC Limits

Potassium Silver Sodium Vanadium Zinc

100,000

42.7

111,000

384

872

1,000

10.0

500

20.0

20.0

100,000

50.0

100,000

400

1,000

2,400

0.8

19,000

0.4

3.9

97.9

83.7

92.2

96.0

86.8

75-125

75-125

75-125

75-125

75-125

Source: 1303019-09RE1 Matrix Spike Dup (B3E0905-MSD1)

Prepared: 5/9/2013 Analyzed: 5/14/2013

Targets

ANALYTE Result AnalyteReporting Spike Source %REC ^g/L Qualifiers Limit Level Result %REC Limits RPD

RPD Limit

Aluminimi Barium Beryllium Cadmiimi Calcium Chromiimi Cobalt Copper Iron

Magnesiimi

Manganese Nickel

Potassium Silver Sodium

Vanadium

Zinc

974

1,940

46.6

46.9

101,000

367

172

366

16,900

98,400

592

339

101,000

43.0

112,000

386

877

100

10.0

5.0

5.0

150

10.0

20.0

20.0

25.0

150

5.0

20.0

1,000

10.0

500

20.0

20.0

1,000

2,000

50.0

50.0

100,000

400

200

400

1,000

100,000

400

400

100,000

50.0

100,000

400

1,000

14.0

107

0.04

1.1

8,390

18,000

3,160

258

0.4

2,400

0.8

19,000

0.4

3.9

96.0

91.8

93.0

91.6

92.2

91.7

86.2

91.5

NR

95.2

83.6

84.7

98.8

84.4

93.1

96.4

87.3

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

»75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

1.04

0.30

0.73

0.83

0.91

0.82

0.70

0.64

0.40

0.94

0.22

1.76

0.91

0.85

0.82

0.44

0.57

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

ReportName: 1303019,1303021,1303022 FINAL 06 11 13 1452 Page 5 of 27 005505



Phone:(281)983-2100 Fax:(281)983-2248

Results

from

TCEQ Laboratory 5144 E. Sam Houston Prkwy N.

Houston, TX 77015




Phone:(281)983-2100 Fax:(281)983-2248

Batch: TCEQ

Batch: TCEQ

Miscellaneous Results (TCEQ)

Matrix: Liquid

Laboratory ID

1303019-03

1303019-04

1303019-05

1303019-06

1303019-07

1303019-08

1303021-03

1303021-05

1303021-06

1303021-07

1303021-09

Station ID

MW-1

MW-15

MW-15-D

MW-18

MW-21

MW-4

MW-16

MW-2

MW-20

MW-20-D

MW-3

Chloride

mg/L

41

50

51

30

8

9

26

8

14

14

11

Analyte Qualifier

Specific Method

300.0

300.0

300.0

300.0

300.0

300.0

300.0

300.0

300.0

300.0

300.0

Date Analyzed

04/03/13

04/03/13

04/03/13

04/03/13

04/03/13

04/03/13

04/03/13

04/03/13

04/03/13

04/03/13

04/03/13

Matrix: Liquid

Laboratory ID

1303019-03

1303019-04

1303019-05

1303019-06

1303019-07

1303019-08

1303021-03

1303021-05

1303021-06

1303021-07

1303021-09

Station ID

MW-1

MW-15

MW-15-D

MW-18

MW-21

MW-4

MW-16

MW-2

MW-20

MW-20-D

MW-3

Nitrate as N

mg/L

<0.02

<0.02

<0.02

<0.02

<0.02

0.18

<0.02

<0.02

<0.02

<0.02

<0.02

Analyte Qualifier

Specific Method

353.2

353.2

353.2

353.2

353.2

353.2

353.2

353.2

353.2

353.2

353.2

Date Analyzed

03/28/13

03/28/13

03/28/13

03/28/13

03/28/13

03/28/13

04/05/13

04/05/13

04/05/13

04/05/13

04/05/13




Phone:(281)983-2100 Fax:(281)983-2248

Batch: TCEQ

Batch: TCEQ


Matrix: Liquid

Laboratory ID

1303019-03

1303019-04

1303019-05

1303019-06

1303019-07

1303019-08

1303021-03

1303021-05

1303021-06

1303021-07

1303021-09

Station ID

MW-1

MW-15

MW-15-D

MW-18

MW-21

MW-4

MW-16

MW-2

MW-20

MW-20-D

MW-3

Nitrate+Nitrite as N

mg/L

<0.04

<0.04

<0.04

<0.04 .

<0.04

0.18

<0.04

<0.04

<0.04

<0.04

<0.04

Analyte Qualifier

Specific Method

353.2

353.2

353.2

353.2

353.2

353.2

353.2

353.2

353.2

353.2

353.2

Date Analyzed

03/28/13

03/28/13

03/28/13

03/28/13

03/28/13

03/28/13

04/05/13

04/05/13

04/05/13

04/05/13

04/05/13

Matrix: Liquid

Laboratory ID

1303019-03

1303019-04

1303019-05

1303019-06

1303019-07

1303019-08

1303021-03

1303021-05

1303021-06

1303021-07

1303021-09

Station ID

MW-1

MW-15

MW-15-D

MW-18

MW-21

MW-4

MW-16

MW-2

MW-20

MW-20-D

MW-3

Nitrite as N

mg/L

<0.02

<0.02

<0.02

<0.02

<0.02

<0.02

<0.02

0.04

<0.02

<0.02

<0.02

Analyte Qualifier

TQ06

Specific Method

353.2

353.2

353.2

353.2

353.2

353.2

353.2

353.2

353.2

353.2

353.2

Date Analyzed

03/26/13

03/26/13

03/26/13

03/26/13

03/26/13

03/26/13

03/27/13

03/27/13

03/27/13

03/27/13

03/27/13




Phone:(281)983-2100 Fax:(281)983-2248

Batch: TCEQ

Batch: TCEQ


Matrix: Liquid

Laboratory ID

1303019-03

1303019-04

1303019-05

1303019-06

1303019-07

1303019-08

1303021-03

1303021-05

1303021-06

1303021-07

1303021-09

Station ID

MW-1

MW-15

MW-15-D

MW-18

MW-21

MW-4

MW-16

MW-2

MW-20

MW-20-D

MW-3

Sulfate

mg/L

23

<5

<5

<5

<5

<5

<5

5

<5

<5

<5

Analyte Qualifier

Specific Method

300.0

300.0

300.0

300.0

300.0

300.0

300.0

300.0

300.0

300.0

300.0

Date Analyzed

04/03/13

04/03/13

04/03/13

04/03/13

04/03/13

04/03/13

04/03/13

04/03/13

04/03/13

04/03/13

04/03/13

Matrix: Liquid

Laboratory ID

1303019-03

1303019-04

1303019-05

1303019-06

1303019-07

1303019-08

1303021-03

1303021-05

1303021-06

1303021-07

1303021-09

Station ID

MW-1

MW-15

MW-15-D

MW-18

MW-21

MW-4

MW-16

MW-2

MW-20

MW-20-D

MW-3

Sulfide

mg/L

<0.01

<0.01

<0.01

0.02

<0.01

<0.01

<0.01

0.13

<0.01

<0.01

<0.01

Analyte Qualifier

Specific Method

376.2

376.2

376.2

376.2

376.2

376.2

376.2

376.2

376.2

376.2

376.2

Date Analyzed

03/27/13

03/27/13

03/27/13

03/27/13

03/27/13

03/27/13

03/27/13

03/27/13

03/27/13

03/27/13

03/27/13

ReportName: 1303019,1303021,1303022 FINAL06 11 13 1452 Page 9 of 27 005509



Phone:(281)983-2100 Fax:(281)983-2248

Batch: TCEQ


Matrix: Liquid

Laboratory ID

1303019-03

1303019-04

1303019-05

1303019-06

1303019-07

1303019-08

1303021-03

1303021-05

1303021-06

1303021-07

1303021-09

Station ID

MW-1

MW-15

MW-15-D

MW-18

MW-21

MW-4

MW-16

MW-2

MW-20

MW-20-D

MW-3

Total Organic Carbon, NPOC

mg/L

2

2

2

1

<1

<1

<1

15

<1

<1

<1

Analyte Qualifier

TQ07

TQ08

TQ09

TQIO

TQll

Specific Method

SM21 5310B

SM21 5310B

SM21 5310B

SM21 5310B

SM21 5310B

SM21 5310B

SM21 5310B

SM21 5310B

SM21 5310B

SM21 5310B

SM21 5310B

Date Analyzed

04/04/13

04/04/13

04/04/13

04/09/13

04/04/13

04/09/13

04/09/13

04/04/13

04/09/13

04/09/13

04/04/13


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CatiieTName.' FedEx

Ai[t>illMa'7993 43201020

CHAIN OF CUSTODY RECORD

Marion Pressure TreaUng (Company Superfund Site

Marion, LA

P r < ^ Coda; 1434262

No: 6432513-132943-0006

Lab: U ^ . EPARegbi 6 Laboslor^

Lab Contact: Ctutsty Wanen

Lai,PtKBier28i;.^2137-

Sampled

MW-15-0

ER-2

ER-3

MW.15

mv-i

' Matrix/Sampler

Water/Ryan

Gutti

Wa'ter/«.iaiti Kelly

, WateriRyan 1 Gi:tli

1 Water/Ryan

: Guth

, Water; Mat*

Ke«y

GolL Mothod

Grab

' Grab

Grab

Grab

Grab

Anatysls/Tumaround

THtHg(35)

TMtHsfM)

TMtHgt35)

TM«Hg(35)

TtJ+Hg(35).T»W<g(35)

Tag/Preservatlva/Botttes

6-490255 (Ice tti 4 C,pH< 2

HN03)(1L

' 6490334( lc8to4C.pH<2

HN63)(1)

&4903}7-(lcslo4C.pH<.2 '

tm03) t1 ) " i

1 W90270( lca lB4C.pM<2 | HN03y(1)

6-490226(!cB(o4C,pH<2 , HH03). 6-490227 (toe to 4 C, •

Station

Location

rjIW-15-0

ER-2

ER-3

(JlW-15

MW-5

\ Collected

0305001308:56

'. maizoia08:55

()3«a201308i00

03/75/201303:56

03/24E01310:30

For.LabUsa Only

pH<2HN03)(2)

MW.6

t/IW-7

1 Water/Mark

Kelly

Water/Mark

Kelly

Grab

ISrab

TM«Hg(35)

TMtHa(3S)

6^9f l230( lc8to4C.pH«2 HN03)(1)

6-!90236(lceto4C,pH<2 HN03)(1)

MW«

MW-7

03M2D1313:15.

03124/201,314;50

— 1 _

I Shipment for Case Coinpltts? N

SaiTiple(s) to be used lor Lab QC: MW.5

Ana ly^ Key: fM«Hg-Total Me^is + Hg

Samplea Tiansfened From Chain of Custody fl

Items/Rsason Rdnqutebad by i Dats

\Jk^ ttsms/Reason Relinquished By Data

i

RscEivadby Date

1

1

Time

a OS

> i . <^

22 e. 00 o <.»> a

!-: (a 2 o O to

fi-

X

^ I VO ^

Si o ts> VO . ^ VO o o

» i ON S

n

o g 3 ^

t&

005511

o

O

fro o H ^

t o n «> | v j

^

o ON i _ ^

»—» _ u>

^ 4^ l ^ I O

Page 1 of 1

USEPA CLP Generic COC (LAB COPY)

DataShfpped: 3/25/2013

CairierName: FedEx

AirbillNff. 7993 43191352


Marion Pressure Traattno Company Supetfimd Si!4.

Marlon, LA

Projecl Code: 1434252

Na:'6-032513-13504$-00p7 l ^ ^ ,U^ . , EPA;!:t$8i(»i S' l ibosloiy

lab Contatt OutstyWaiten

:UbPhonK2ai:9S3-2l37

Sample 9 ' Matrht^ampler' CoU. ! Method

" ^ - 2 ' ^

MW-6

MW-7

Water/Mark _ _ M y _

• Water/Mari'" Kely

WalBtf Marls' Kelly

Grab

Glab

Grab

Analysis/Turnaround

l;owA8N(35),lowABN(35)

LowABN(35).LoivA8N(35)

Lw/ABN(35),Lo«yABN(35)

' Teg/Prcserratne/Bottbis :

; 1 6^90332 {lcotO'4 0 , 6 - i

\ 450333 (IC8tO'4Ci'(2) 1

649(K28(IC81o4C),6.

49022:9 (I ts la 4 C) (2)

6-490234 (Ira to 4 q , 6- | , 490235(lcet<!,4iCl(2) j

1

SbUon Locatimi

ER^2

MW.€

WM7

Collected

0304/2013 08:55

03/24/201313:15

03B4)20W4:50

Fo rUbUse Only

,

i

—-I

"H

j _

TSilpmenl for Cass C a r r o t s ? N

I Special Instructions; i 'Samples Ttansfemtf From Chain q tCi tA i t ly <

:/Analysis Key: Low ABN=ljwr ABN

Tina I Jtems/Raasm J RelJrvqu^edBy ] Data ' ' (tecet/edby I ' D a a 1 T i i ta l

6 > o ( - ^ " p ^

§ • 5 O Ov

a t o

(O ^

£2 E. "vo a 00 o t>> a ' n

^ ^ 2 ° 0 w

P-SC

>fl 2 S I ^ P VO ^ 1 ^

t o o t o VO 4^ VO 00

lAJ m fD 2

dQ -

P i 5-

? a-. O g

? i

005512

o T3 O

z B l

• T O ei m n H - . UJ

o -»> t o - J

§ -* •—•

,_. U ) _ _ t

• u cy» K )

Page l o l l


DateSH^ped: 3/25/2013 GarrififNama; FedEx AiiblNo: 7933 431S 9713


Marion Pressure Tnsalng.Comiiani/.SupeifUnd SIta

lil3iipn.LA

Project Cijda: 1434262

No:6432513-141207-0008: LdrU.Si EPA.R^lonS Ubojatbry

U b Coitacj: Oifls^'MVarten

tab:P)isne;281-983.2137

Sample It • Matrii/Sampler Coll. ; Method

Analyslsfrumaraund Tag/Presaivativii/Botllss StaUon Location

Collactttl^

MW-15-D Water/Ryaii Gutli

Grab LowABN(35),U)wABN(35) 6-4902&1jlcel».'(C),6-'490262 (Its to4.(;f(2)

MW.1SD i 03/25/201308:56

For Lab Use

ER-3

~MW-f5

Water/Ryan Guth

Water/Ryan Gu!h

Grab

""Grab'

Lov/ABN(3S).Lp\vAfiN(35)

L(wABM3S),UwrABN(35)

&4g033S(lcstg44:).6-48gH6(lcetb4q(2)

ER-3 0305001308:00

6-490266 (lcsti>4C),'8. <902S7(teMC)(2)

MW-15 0305/201308:56

, Shipment for Case Complota? N

Special Instnjtiions:

Ana^'sis Key. Low A B N = L I W S N ^

Items/Reason '• ReBraulstieilby Date 1 Ri

; /§Z^ .&'_'.

: Samplestransferred From Cltaln of Custody "

2(l:3:1-i-?i

13

§•5 a a\ a to to » 22 e! 00 o <.>! P

* z 2 o o ei

fi-X

•fl 2

^ I 2 H VO ^ 0 0 . L J - J I ^

to o (O VO -(^ VO 00

« 2 dQ • ® B

^ I ^ 3

O o ora

005513

of 1


OateStiipped: 3/250013

CanierName: FedEx

AirbSINo: 7993 4318 3976

CHAIN OF CUSTOOY RECORD

Maran Pressure Treating Conpsny Superfund Site

Marion, LA

Project Coda: 1434262

No:6432513-1S243»l010 Lab: U.S, EPARegjon 6 laboratory

Lab Contact: duisty Waiisn

labPhani>:281-£!8MI37

73 •S o a z B> 3 o

u> o u> o

Sample t MatriifSampler CoO. MaUiod

' m i - \ '\ ' Watei/Ryan ' Grab

Guth^

M W 5 i " " ' ' Wtita/ Josa ' Grab ' Fbres

' " l . i w - 4 " " Water/Mark KsUy

Anatysls/Tumaround

Grab

L0'.vABN(35), LowABNiaS)

L(rjvABK(35)7LTOABS(35

L«/ABN(35).l.owABH(35)

Tsg/Prcsorvathre/Bpttles

WS0272( lcat04O.8. 490273 (lcet04C) (2)

F : W 9 0 2 » ( t e t o 4 C ) , 6 -; 490297 (Its t D 4 Q (2)

fr490290(l«il»4C).6-1 430281 (lea to 4 C) (2)

i ^.-- - -

Sbtlbn

Location

MW-1

HW-Z)

' MV\M

, Cdllocied

03/2500131125

"" 0305(21131^48

0305001309:30

—

ForUbtJso' :

billy.

1

1

.

-U

• • 1 ; :

' ; • i ' • • i

' ShlpniDotfbf.CaseXonipuite? N |

ll Instructions;

^ A i i a ^ Key: low ABN^Low ABN

Samplos Tianstemd Ernn ChiiniOl Ciistody.|)

• f l pr o s o

t o 00

VO oo u> .1) o o

s is 0 0

0 0

I O t o *. 0 0

1—.

o Ov t o \ J \

^ a o 13 n JO K p

J^ ffi o

§

d - J

o VO VO

« dQ ^^« O 0 ON

»9

o-o »9 p ^

o ^

B

|2' o B

5 B

£ s J o B >

OQ A B

«<

• f l IS

OQ

u> O LP O to

u> o o to to •fl

> r o Ov

Hems/Reason Retimiulshedb'f Date

% {Lk/^3.%

'/»d by ^ " Date 7 1"tw Items/Reason i Re|(nu^hedBy ! Paia^ | Recejiral'by

. . . ^ • ^ J r l ^ ^ ^ l Oo^ i ^ ^ O T

•&• UJ

o ^ to l/l ^ to

005514

Pago 1 of 1

USEPA CLP Conoric COC (LAB COPY)

OateShtpped: 305/2013

CairierKams: FedEx

AlrbilNo: 7993 43137630


fteton Pressuns Treating Cmipaiir Superfund SIta

Marion, LA

P n ^ Code: 1434262

No: 6432513-130552-0005 L ^ U.S. EPAf tagb i erlabOtatpiy

Lab Coitact ChrislyWanen

LabPlien9:281JB834l3»"

Sampio # Matrix/Samplor

• f l e i

f t

70 a o a. z 3

UJ O UJ o

UJ

o UJ o t o

o UJ o t o t o

> r o o\

Mlft^S Water/Mark Kelly

ColL fJethod^

Grab

Analysis/Turnaround

low ABN(35), Low ABN(35), Low A8N(3S). Low ABNtSS), l ow ABN(35).

low/\BN(35)

Tag/Pressrvative/Botlles Statlan Location

Collected

6^90220 (lea to 4,0).$-490221 (IC8 lo4C),-8. 490222 (Ice to 4 q , 6-490223 (ha to 4 0 ,6-490224 (lc« 194 C), 6-490225 (Ice ta 4 G) (6)

For Lab Usa <>tily

MW'S 03/24/201310:30

Ssmpie(s) 10 be used lor Lab QC: MW-5

Shipmenlfbr Case Completg? N

SaiTiptas Transferred From C M i ) o fCus tody*

Analysis Key: Low ABM'lov/ ABN

Items/Reason ; Relinquished by : Oato _Receivedby : Date Time Items/Reason ' ReSnquished By Date T Received by Date i Tons

I ,-_

4 - i -

G H ^ T ^ ' - o^<^' GioX fei-?^)

•fl §"5 P Ov a to

!S "fl oo p '

"vo a 0 0 o UJ a * n ^% 2 ° O (S

fi-X

•flg 2 H VO ^ 0 0 , UJ ^ I ^

t o o t o VO .U VO 0 0

dQ •

® i * I

o g 2 ^ O B

Lft UJ

to u< -J to

005515

Pagel o f l


DateShJpped:3O5O013 Cairiertfame: FedEx AWlWa 7393 43187537


Marlon Pressure Treaiirig^Company Superfund Site

Marion. LA

Project Code; 1434262

No:6W2513-1S1107-0009 lab>U.S. EPA Region eiaboait ty

Ubônlact Christ^ Warren

LabPhoiie:.28l433^2'i37

?0 •§ o a. Z

UJ o u>

o

UJ O UJ o t o

UJ

o UJ o t o t o

•fl g 00 ^ CT I—

Sample tt MatrixISamplor CoU. Method

AnalyBls/Tumaround Tag/Pmeivadve/Botlles Station Location

Collected

MW-1 Water/Ryan Gulh

Gtab I N02SD4CU35),TOCN03TN(35),S. (35)

MVJ-18 Water/ Ryan Gulh

MW-21 Water/Joss Flares

Grab

Grab

N02 S04 CL(35). TOC N03 TN(36). S-(35)

&490274(lceta4C).6-430275(lcaiO4C.pH<2 H2S04), 6490277 (pH> 3

w/NaQH,ZnOAe,lCB4C)(3)

&49028D(icela4C),6-43028i(ltst()4C,p}f<2 H2SO4).W902a3(pM»9

«IN30RZnQAc: la4Q(3)

MW-I 0305001311:25

l iWîa i 03^001313;55

For lab Use \ Only I

N02 S04 CL(35). TOC N03 TN(35), S-(35)

8-430^8<(lcs»4C),$-490299(lceia4C,pH<:2 H2SO4),6.4a)30ttpH>g '

usrNsOH.ZnOAc.lcs4C)(3)

MW-21 03/KOI513.11:48.

Special Instructions:

j Shiprnent forCase C ^ l e l B ? H

Samples TnnsIsmiS FnniCiialn oi Custoity^

i Analysis Kay; N02 S04 a=Nilt iM, Sullale. ChkirMe. TOC HS3 TN^TQC, NUrala, Nitratsîtite. 3^=$uaide

iby"

C o c i ^ p2AMfl «(/t i y ^ i ^ )

• f l I ' ' S o o B Ov <K t o

> v '•'<

K •fl 00 03

^ a 00 o UJ s

2 o O IS

fi-

il ^ ^ VO ' ^ o o . L.J ^

to o KJ VO 4k VO OO

« 2 dQ ^• ® B

^ I ? &•

o g

0 \ UJ o • -

t o L») ^ t o

005516

70 ft •a o a

UJ

o UJ

o UJ

o o to

UJ

o UJ o to to

> r •fl g o ^-• — ' t - ^

^ UJ o ^ t o Ln ^ t o

Page 1 of 1


Da-£Shipped:3O3S013

CarrterNams; FedEx

AirtiilMo: 799343195259

1 Samples , Matrix/Sampler

M W - i M ; Waiei/Ryan i Gulh

Co l l Method

Grab

! r/IW-15 i water/Ryan ' Gtab Gulh

fX'W-4 Water/Mark ' Grab KeBy i


MaiTO PresSBB Trealiig Company Supeifural Site

Maiton,lA

Project Code. 1434262

' Analysis/Turnaround ; Tao/Presorvative/Bottlas |

, N 6 2 5 0 4 0 ( 3 5 ) , TOC N 6 3 T N P 5 ) , S - | 6-49Q2S3(lcoto4C).6-(35) i 490254(lceto4C,pH<2 1

H2S04), 6-490256 (pH>9w/ NaOH, ZnOAc; lea 4 q ( 3 )

NO2S04CK35),T0CNO3TN(35).S- 9-49(1266 (Ice to 40 ) . 6- ; (35) j 490ffi9(lcel64C.jiH<,2 1

! H2S04). 6^90271 (pH> 9 tt/N30H.aOAclca4C)(3)

NO2SCMCl(35).T0CNO3TNt35).S- W90232( lca (»4O.e- , |35) 490293 (Ice to 4 C P H < 2 |

H2S04), 6-460295 (pH> 9 , i w/MaOH.ZnOAclca4C)t3)

; 1

Station

Location

MW15:( r

MW.,15

MW^

No:6r032513-120446-q004

late U.S.-EPA Ragbn 6 Labostoiy

l a b Coitlad: Qvisly Waiten

lab Phone; 281.9SJ.2137

Collected

' 03O6O01309;S6

, 0305/3)13 0 8 i 6 i

ForLabUss '••

1 O"" / '

1

i

03O5Q013J19.'30 < i 1 i

Special Instniaions

Analysis Key: N02 S04 Cl=Nitrite. Sulfate'Cliiorae; TOC_N03 TN^TOC] Hitr3te7NiJatet>iilrite.S-='SulfidB"

i^oelvedby ' Dale t m e i ltems/Reason~ Relini;uished By { Date

Shiprnent (or C a a ComplelB? N

Samptes transferred From ( ^ i n of Custody #

Items/Reason Relinquished by Daa Received by Date Tine

o o 0 Ov n to

- i i , Lr, to ^rt 00 g ~vo a 00 o UJ f3 • z 2 o

fi-ffi

•flg

VO ^ 00 , UJ ~J I ^

SJ o S> VO . U VO 00

dQ ^•

® B ^ I

o g

005517

http://281.9SJ.2137

TO n

T3 O

z Cl 3 f t

UJ

o UJ

o UJ

o UJ o to UJ

o UJ o to to

n o l i


DateShipped: 306/2013

CerriertJeme' FedEx

AirbJlINo: 7993 4329 0374

Sampled Matrix/Sampler Co l l . Method 1

ER-4 Water/Ryan Grab | Gulh '

MW.16 Water/Ryan Grab Guth i

MW-18 Water/Ryan Grab Guth


Marion Pressure Treating Company Superfund Site

Marten, L«

Project fiixtti; 1434262

Analysis/Tumaround

LowABN(35). L0WABN(35)

lowABN(35).LowABN(35)

LowASNp5),lowABN(35)

— •

6-490338 (Its 104 Q , 6-490339 (lea to 4 0 ( 2 )

W90260( Ice to4e) ,6 -490261 (Ice lb 4 C) (2)

6^60278 ( t o to 4 0) . 6 , 490279 (Ice to 4 0 ( 2 )

Station Location

ER-4

' _ MW-16

MW-18

No: 64325l^'i328564()11 U b : U.S? EP« R e s M e Labdralbry

LebCantactiChttstyWarien

•Lab,Rione'.28l4sj-2f3f

Collected

\ 0306/2013 07;55

1 0306/201308:45

i 1 0305001313:55

For t a b Use

1

1 >

i

Special Insbuctkxis:

• f l

§"5 P ov f t t o

>lv <-n t o •_. 00 ( ?

"vo a 00 o UJ 13 < ft

2 o fi-ffi o ..* o a

B

O B

5 B

Shipment for .C^Coinpteto? Y

SampteeTiaitsfeitred Froth Chain of CCslody4

Analysis Key: low ABN=low ABN

- J • o to o

t o VO .U VO 00

dQ

o

ON

^ 3

^ a o B >

VQ

n

a

O

o

•fl g IB Ov

OQ ^ ft t—»

00 UJ

o — t o Ln ^ t o

005518

Pa^lofl


OsteShipped: 3060013

CanierNaiia: FedEx

AirbiKNo: 7993 4328 4379


Marion Pressure Treating Company Superfund SHe

Marion, LA

ProjeaCode: 1434262

Nb :e432613-140647JOa i4

lab: U.'s:£PA Region 6 laboratory

. lab Contectv Christ/Warren

lab Phone; 281 •8a-2t37

?<3 ft •a o

z a 3 ft

U J

o

Sample tl Matrix/Sampler CoU. I Method

ER.4 Water/ Ryan Gulh

Grab

MW-1

M W i l

M W T "

Water/ Ryan i Grab

Gulh - _

Water/ R ^ n Grab

Gulh •

Water/Jose

Flores

WaterfMark" KsUy

Analysis/Turnaround

TMtHg{35)

Tag/Pieservative/BotUes Station Location

CoUected

Grab

Grab

TM+Hg{q5)

™*H3(35) '

~TM+Hg(35r

6-490340 (Ice to 4 C,pH< 2 I HN03)(1)

ER-4 0306001307:55

TMTHg(35)

6-490276 (Ice l b4C .pH< 2

I Hl«)3)ffl i "6430282( l<at i )4C,pH<2"

j HN03H1)

MW-1

"MW-IT

0305001311-.25

0305001313:55

6-190300 (Ice to 4 C,pH< 2 HN03)(1)

i 6490234 (Ice to 4 a p H < 2 •• HN03)(1)

MVV-21

' MW-4

0305001311:48

0305001309:30

For Lab Use Only

Special InstniclKns.

, /^nahj'Sis Key: THHHg=To|al Mejals t Hg

Shipment for Case Complete? Y

- I

Samples Transferred Fism Chain ot Custody t

• f l

§"5 a ov ft to

> N <-*> t o • r t 0 0 isV

"vo a 00 o UJ 3 > ft • z 2 °

P-ffi

• f lg

VO ^ 0 0 , UJ - J I ^ to o S> VO .U VO 0 0

dQ q*

p i B

^ 3

o g s SI

U J

o UJ o to

U J

o U J o to to

> r o Ov

• f l O Q > - ' f t • -

Items/Reason Relinquished by Date !

V ^ ^ 3- ) ' -1 ^ : t f f i i f L j i i v l

led by Date Tin» | i Items/Reason Relinquished By

MiJM, -)/!^L)ii : - .

Date Reoahed by [ Date Tune

VO UJ O ^ • < , ^

to Ol -J to

005519

of 1


DateShlpped: 3/260013

CatrjerName: FedEx

AirbllNo: 7993 43281630


Marioi Pressure TteaCng Company Superfund SSe

Marion, LA

Project Code: 1434262

No: 6r032613-1<l32164015 Lab; t L l E P A Reglotiie Idloiatory

iabConlaqu Christy Warren

LabPhbrie:'281-8S3>2137

TO f t

T3 O

a

UJ o UJ o so

UJ

o UJ o to U J

o UJ o to to •Tl

•fl g [o Ov

OQ ^ f t • -to — O UJ o ^ to Ln •^ to

Sampto 1}

MW-16

MW-2

MW-20

Matrix/Sampler

Water/Ryan ' Guth

Water/Ryan Guth

Water/Jose ,

CoU Method

Grab.

Grab

Grab

Anatysls/Tumaround

Flores

TM*H8t35)

" " t H i S g ^ ' "

"TMitigissT

MW-2frO Water/Joss Flores

Grab Tf.1+Hgi35)

MW-3 Water/Ryan ! Grab _ ^ ^ Gulh I

TM*Hg(35)

Tas/Pieservattve/Botflss

6490264 (Ice M C ; p H < 2 JfN03){1) _ _

8-490K4 (Ice ttVc. pH'< 2 HN03)(1)^

Station Locatlan

' I W 1 8 "~

CoDectsd : ForLabUss Oiily

MWr2

0306001308:45

0306001313.-00

e490306(lceti>4C.pH<2 HN03)(1)

MW.20 03 /a /»13 09:39

6490312(lcBlo4C,pH<2 HN03)(;t)

MW-20-D 0306001309:39

6-490318 (Ice b 4 C , p H < 2 MW-3 HN03)(1)

03O6O01J102S

^ Shipment to.r Case Complete? Y

. Special Instructions: : Samples Traosferred FromChabi of Custody #

• Analysis Key. TM->Ha=Tolal Metals • Hg

Items/Reason ReEnquished by (}ate

• f l

o o B Ov ft to >v <-n

^ a 00 o UJ p

^ ^ 2 » O ta

fi-ffi

•fl g ^ I 0 0 -VO r ^ OO , U J - J I ^ to O f O VO * > VO 0 0

/ ^ rt

dQ N^»

o p o\ ^ ^

o-o ^ » rt' o ^

w i. 1 o B 5 ffi B

£

1 {^ o B

n

«<

005520

•fl p

OQ f t t o

Page l o l l


OateShipped; 306/2013

Carriert^ame: FedEx

Airi)iIINo; 7993 4329 4818


Marion Pressure Treating Company Superfund S

Merloni L/\

Ptoiect Code: 1434232

No: 6-032$13-13S320-0013 lab: U.S. EPA RegibnB l^oratory

U b Cotttecl: CI\rIsty:Wanei)

Lab Phone; 281-883^13;!

Sampte S '. MatrixISampler

f t t 3 O

a. Z p> 3 f t

UJ

o UJ

o UJ

o o to

UJ

o UJ o to to

MW-16 Wats/Ryan Gulh

MW.20

MW-20-O

Water/Jose Flotes

Water/ Jose Ftores

ColL Jlethod

GtST"

Grab

Grab

Atutysfs/Turnaround

N02 S04 CL(35). TOC N03 TN(35). S-(35)

taglPressrvatlve/Botlles

6490282 (Ics to 4 C j " . ? " " 490263 (Ice to4C,'PH< 2 H2S04), 6490265 ( p h > 9

WNaOH.ZnOAeilce4C){3)

Stalioii Locatian

Coltected

MW-16

N02 S04 a(35), TOC N03 TN|35). S-(35)

N02 S04 CL(35), TOC N03 TN(35), S-(35)

6490304 (Ice to 4 0 . 6 -4303b5( loeta4C,pH<2 H2S04), 6430307 (pH> 9 |

v</NaOH.ZnOAc, l ta40(3y | ~ 6480310 ( lce lo4 0 . 6 - " ^

490311( lceto4C.pH<2 ] H2SO4).6M90313(pH>3 !

w/NaOH,ZnOAc,lcs4C)(3)

MW-20

0306001308:45:

For Lab Use Only

0306001309:33

MW-20.D 0 3 0 6 0 0 1 3 0 9 3


Special Instructions;

Arialysirkey. N02 SCMClSi i r i te. Sr^teJCWoMe, TOC" N03"tN»f0Ci"Nitate, Kiirate^Nil'rile. S-°SulWe "

. Samples Transferred From Chahi of Custody It

Items/Reason Re&nqutshed by Date Received by Date i Time Relinquished By ; Dale ; Recei»edby Date T i ihe j

• f l

o o B Ov ft «o ^ <-« t o Hrt

22 E ! ~v5 a 00 o UJ B 1 f t

2 ° fi-ffi Q • f l

?d

-5>^ I --3 to O t o VO . ^ VO OO

rt 2 dQ ^•

P 1 B

OS »

t ^ =?

p (^

o ^

1-4 4^ t o IJ\ - 1 to

005521

•fl g pj Ov

OQ ft t o t o UJ

o ^ t o vyi •-J t o

Page 1 of 1


OaieShipped; 3050013

CanierName; FedEx

Ai-bWo; 7993 4327 9050


Marian Pressure Treating Company Siqierfiind Site

Marian,'LA

Prajea Code: 14342S2

No:6-032613-144342-0016

Leh U:S. EPA Regteii.e^labpratey

Lab'Conlaci; Chris;y:Vyarren

labPlio>is:'2S1.r983.2137

TO ft •o o

UJ o UJ o

<.>J o UJ o to

UJ

o UJ o to to

Sampte # Matrii/Sampter Coll. Analyslsn'umaround Mothod

FM/.2 Water/Ryan Grab LowABN(35).LowASN(35) Gulh 1

fJW.3 Water/Ryan Grab L O ' A A B N ( 3 5 ) . I O W A B N ( 3 5 ) Gulh j

'

Tes/Preser\'ativ^i>ttIos

6490320 jlce 10 4 .0 .6 -490321 (Icslo 4 : 0 (2)

fl.e(J314(lcaio><fe).6-490315 ( I c s j oAO (2)

' Station ^ i l lacted Location

MW-2 03OS201313.«

MW-3 : 03i2M'Ol3102S

i 1 i

i ' ,

i i

^ , 1

! 1 ^

:

' ; f

i

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CarrierName: FedEx

AirbiTNo: 7993 4327 6051


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Project Code: 1434262

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Analysis Key: N02S04"CL=Niirite~Sullate;Chloride, tOCNOiTMSrOCTNiiate,Ntoie^Nit i te,S-'^lWe""


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MarionPressutetreaiihg Company Superfund Site

Marion, LA

Projed Code; 1434262

No: S:032613-1342S9:«012

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DateSh%;!SJ; 3/23/2013

CarrisiNsni: FedEx

Aiblfi^o: 7933 8502 4219

CHAIN OF CUSTODYRECORD

Marioo Piessute Treaftig Cffinpany Superfund Sle

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Phone:(281 )983-2100 Fax:(281 )983-2248

Notes and Definitions

TQl 1 The reproducibility (%CV) of replicate sample injections of AA53041 was 16.39%, which is outside the acceptance limits of 10%. At low concentrations the variability of the measurements increases. The data is not likely affected.

TQIO The reproducibility (%CV) of replicate sample injections of AA53040 was 15.36%, which is outside the acceptance limits of 10%. At low concentrations the variability of the measurements increases. The data is not likely afifected.

TQ09 The reproducibility (%CV) of replicate sample injections of AA53038 was 11.90%, which is outside the acceptance limits of 10%. At low concentrations the variability of the measurements increases. The data is not likely affected.

TQ08 The reproducibility (%CV) of replicate sample injections of AA53011 was 32.83%, which is outside the acceptance limits of 10%. At low concentrations the variability of the measurements increases. The data is not likely affected.

TQ07 The reproducibility (%CV) of replicate sample injections of AA53009 was 17.94%, which is outside the acceptance limits of 10%. At low concentrations the variability of the measurements increases. The data is not likely afifected.

TQ06 The matrix spike recovery was 192 %, which is outside of the (80-120%) acceptance limits. The precision (%RPD) of matrix spike and matrix spike duplicate was 73.7%, which is outside of the (20%) acceptance limits. The data is likely afifected.

A This sample was extracted at a single acid pH.

HTS Sample was prepared and/or analyzed past recommended holding time. Concentrations should be considered minimum values.

ABN Acid Base Neutrals (Semivolatile Compounds)

AES Atomic Emission Spectrometer

BS Blank Spike

CVAA Cold Vapor Atomic Absorption

DCB Decachlorobiphenyl

ECD Electron Capture Detector

GC Gas Chromatograph

ICP Inductively Coupled Plasma

ISTD Intemal Standard

LCS Laboratory Control Sample




Phone:(281)983-2100 Fax:(281)983-2248

MS Mass Spectrometer

MS/MSD Matrix Spike/Matrix Spike Duplicate

NA Not Applicable

NPD Nitrogen Phosphorous Detector

NR Not Reported

PCB Polychlorinatedbiphenyl

RL Reporting Limit

RT Retention Time

TCLP Toxicity Characteristic Leaching Procedure

TCMX Tetrachloro-meta-xylene

U Undetected

VOA Volatile Organic Analysis

# Out of QC limits

Initial pressure in air analyses is the pressure at which the canister was received in psia (pounds per square inch absolute pressure).

The pH reported for Volatile liquid samples was tested using a 0-14 pH indicator strip for the purpose of verifying chemical preservation.

The statistical software used for the reporting of toxicity data is ToxCalc 5.0.32, Environmental Toxicity Data Analysis System 1994-2007 Tidepool Scientific Software.


final analytical report - records collections · the results apply only to the samples tested. this...

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