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ANALYTICAL SUMMARY REPORTANALYTICAL SUMMARY REPORTANALYTICAL SUMMARY REPORTANALYTICAL SUMMARY REPORT

This report was prepared by Energy Laboratories, Inc., 2393 Salt Creek Hwy., Casper, WY 82601. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative.

The results as reported relate only to the item(s) submitted for testing.

If you have any questions regarding these test results, please call.

Sample ID Client Sample ID Collect Date Receive Date Matrix Test

Report Approved By:

C10070053-001 Street Flow 1 07/01/10 14:15 07/01/10 Solid Metals by ICP/ICPMS, TotalCancelled SampleMercury, TotalE1109 DensityFlashpoint to 200°FUltrasonic ExtractionDiesel Range OrganicspH corrosivityDigestion, Total Metals CVAA Permanganate DigestCorrosivity pH prepSW8270C SVOCs, PAHs

Tetra Tech Inc

Project Name: Lobelles

Workorder No.: C10070053

605 N Warehouse Rd

Casper, WY 82601

July 19, 2010

Energy Laboratories, Inc. received the following 1 sample for Tetra Tech Inc on 7/1/2010 for analysis.

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Project: Lobelles

CLIENT: Tetra Tech Inc

Sample Delivery Group: C10070053 CASE NARRATIVE

07/19/10Report Date:

LABORATORY COMMENTSThe sample that was submitted (Street Flow 1) was heated to ELIs maximum Kinematic Viscosity temperature of 180 degrees F and was still to viscous to charge into the viscometer. The sample has been cancelled for Viscosity.

BRANCH LABORATORY SUBCONTRACT ANALYSISTests associated with analyst identified as ELI-B were subcontracted to Energy Laboratories, 1120 S. 27th St., Billings, MT, EPA Number MT00005.

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LABORATORY ANALYTICAL REPORT

Client: Tetra Tech Inc

Project: Lobelles

Lab ID: C10070053-001

Client Sample ID: Street Flow 1

Collection Date: 07/01/10 14:15

Matrix: Solid

Report Date: 07/19/10

DateReceived: 07/01/10

Analyses Result Units Analysis Date / ByRL Method

MCL/

QCLQualifiers

PHYSICAL PROPERTIES

07/06/10 12:56 / mkf0.010g/cc1.16Density E1109

07/12/10 10:35 / ph60°F > 200Flash Point (Ignitability) SW1010A140

07/02/10 09:20 / mkf0.01s.u.1.13Corrosivity - pH SW9045C

- Flashpoint has been corrected for barometric pressure.

METALS - TOTAL

D 07/07/10 13:19 / cp0.9mg/kg18.8Arsenic SW6010B

07/07/10 13:19 / cp5.0mg/kg40.9Barium SW6010B

07/07/10 13:19 / cp0.5mg/kgNDCadmium SW6010B

07/07/10 13:19 / cp2.5mg/kg2.9Chromium SW6010B

07/07/10 13:19 / cp2.5mg/kg111Lead SW6010B

07/12/10 14:29 / rdw0.05mg/kg0.06Mercury SW7471A

07/07/10 13:19 / cp5.0mg/kgNDSelenium SW6010B

07/07/10 13:19 / cp0.5mg/kgNDSilver SW6010B

ORGANIC CHARACTERISTICS

07/08/10 11:31 / ph200mg/kg40600Diesel Range Organics (DRO) SW8015B

07/08/10 11:31 / ph50-150%REC116 Surr: o-Terphenyl SW8015B

POLYNUCLEAR AROMATIC HYDROCARBONS

07/07/10 08:39 / eli-b100mg/kgND2-Methylnaphthalene SW8270C

07/07/10 08:39 / eli-b100mg/kgNDAcenaphthene SW8270C

07/07/10 08:39 / eli-b100mg/kgNDAcenaphthylene SW8270C

07/07/10 08:39 / eli-b100mg/kgNDAnthracene SW8270C

07/07/10 08:39 / eli-b100mg/kgNDBenzo(a)anthracene SW8270C

07/07/10 08:39 / eli-b100mg/kgNDBenzo(a)pyrene SW8270C

07/07/10 08:39 / eli-b100mg/kgNDBenzo(b)fluoranthene SW8270C

07/07/10 08:39 / eli-b100mg/kgNDBenzo(g,h,i)perylene SW8270C

07/07/10 08:39 / eli-b100mg/kgNDBenzo(k)fluoranthene SW8270C

07/07/10 08:39 / eli-b100mg/kgNDChrysene SW8270C

07/07/10 08:39 / eli-b100mg/kgNDDibenzo(a,h)anthracene SW8270C

07/07/10 08:39 / eli-b100mg/kgNDFluoranthene SW8270C

07/07/10 08:39 / eli-b100mg/kgNDFluorene SW8270C

07/07/10 08:39 / eli-b100mg/kgNDIndeno(1,2,3-cd)pyrene SW8270C

07/07/10 08:39 / eli-b100mg/kgNDNaphthalene SW8270C

07/07/10 08:39 / eli-b100mg/kgNDPhenanthrene SW8270C

07/07/10 08:39 / eli-b100mg/kgNDPyrene SW8270C

07/07/10 08:39 / eli-b67-102%REC80.0 Surr: 2-Fluorobiphenyl SW8270C

S 07/07/10 08:39 / eli-b62-95%REC51.0 Surr: Nitrobenzene-d5 SW8270C

07/07/10 08:39 / eli-b65-121%REC80.0 Surr: Terphenyl-d14 SW8270C

- Due to the high level of organics present in the sample, 2 g of sample were extracted, as opposed to a normal 30 g. The sample extract would not concentrate to 1 mL and was brought to a 4 mL final volume. The sample extract was diluted an additional 10 times at analysis due to non-target compound sample matrix interference. The Reporting Limit reflects the initial sample mass, the sample extract final volume and the additional dilution.

PHYSICAL PROPERTIES

07/06/10 12:56 / mkf0.010g/cc1.16Density E1109




METALS - TOTAL





07/07/10 13:19 / cp2.5mg/kg111Lead SW6010B





























PHYSICAL PROPERTIES

07/06/10 12:56 / mkf0.010g/cc1.16Density E1109




METALS - TOTAL





07/07/10 13:19 / cp2.5mg/kg111Lead SW6010B





























Report

Definitions:

RL - Analyte reporting limit. MCL - Maximum contaminant level.

QCL - Quality control limit. ND - Not detected at the reporting limit.

D - RL increased due to sample matrix. S - Spike recovery outside of advisory limits.

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Batch ID: 26604

DIESEL RANGE ORGANICS CHROMATOGRAM

Sample Name: C10070053-001B ;0708FID1, $HC-8015-DRO-S, (1,10)

Raw File: G:\Org\FID1-C\DAT\070810_c\0708FID1.0016.RAW

Date & Time Acquired: 7/9/2010 02:54:14

Method File: G:\org\FID1-C\Methods\FID1_BASE_CAL_050510_R0.met

Calibration File: G:\org\FID1-C\Cals\FID1_050510_R0.CAL

Sample Weight: 1 Dilution: 10 S.A.: 1

Mean RF for Hydrocarbon Range Calculations: 18077.63

Rt range for Diesel Range Organics (C10 to C28): 7.18 to 16.85

Rt range for Oil Range Organics (C28 to C40+): 16.71 to End Time

SURROGATE COMPOUND RT ACTUAL MEASURED %REC

*o-Terphenyl_____________13.206 2000. 2326.738 116.34 -

DRO Area:7.334168E+07 DRO AMOUNT: 40570.39

TEH Area:2.116472E+08 TEH AMOUNT: 117076.8

Oil Area:1.410923E+08 OIL AMOUNT: 78047.98

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2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

Time - Minutes

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Project: Lobelles


Work Order: C10070053

QA/QC Summary Report


Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits QualCount

Method: SW1010A Batch: 100712A-FLSHPNT-S-H

Sample ID: LCS1_100712A 07/12/10 10:35Laboratory Control Sample Run: PM_FLASHPOINT A_100712

Flash Point (Ignitability) 101 96 1046091.2 °F


Sample ID: MBLK1_100712A 07/12/10 10:35Method Blank Run: PM_FLASHPOINT A_100712

Flash Point (Ignitability) 60> 200 °F


Qualifiers:

RL - Analyte reporting limit. ND - Not detected at the reporting limit.

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Project: Lobelles






Method: SW6010B Batch: 26579

Sample ID: MB-26579 07/07/10 13:11Method Blank Run: ICP2-C_100706A7

Arsenic 0.5ND mg/kg

Barium 0.05ND mg/kg

Cadmium 0.03ND mg/kg

Chromium 0.070.2 mg/kg

Lead 0.3ND mg/kg

Selenium 1ND mg/kg

Silver 0.07ND mg/kg

Sample ID: LCS1-26579 07/07/10 13:15Laboratory Control Sample Run: ICP2-C_100706A7

Arsenic 104 80.9 1190.99180 mg/kg

Barium 108 82.5 1170.50390 mg/kg

Cadmium 107 82.1 1180.5059 mg/kg

Chromium 107 80.5 1190.50120 mg/kg

Lead 108 81.5 1190.56130 mg/kg

Selenium 95 77.5 1232.3110 mg/kg

Silver 107 66.2 1340.5071 mg/kg

Sample ID: C10070053-001CMS3 07/07/10 13:27Sample Matrix Spike Run: ICP2-C_100706A7

Arsenic 83 75 1250.9839 mg/kg

Barium 86 75 1250.5062 mg/kg

Cadmium 92 75 1250.5012 mg/kg

Chromium 98 75 1250.5027 mg/kg

Lead 75 1250.56120 mg/kg A

Selenium 80 75 1252.220 mg/kg

Silver 86 75 1250.5011 mg/kg

Sample ID: C10070053-001CMSD 07/07/10 13:31Sample Matrix Spike Duplicate Run: ICP2-C_100706A7

Arsenic 109 75 125 200.96 1445 mg/kg

Barium 97 75 125 200.50 3.464 mg/kg

Cadmium 101 75 125 200.50 7.313 mg/kg

Chromium 104 75 125 200.50 428 mg/kg

Lead 75 125 200.55 62220 mg/kg AR

Selenium 91 75 125 202.2 1122 mg/kg

Silver 96 75 125 200.50 9.112 mg/kg

Qualifiers:

RL - Analyte reporting limit. A - The analyte level was greater than four times the spike level. In accordance with the method % recovery is not calculated.

ND - Not detected at the reporting limit. R - RPD exceeds advisory limit.

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Project: Lobelles






Method: SW7471A Batch: 26642

Sample ID: MB-26642 07/12/10 14:25Method Blank Run: CVAA_C203_100712A

Mercury 0.005ND mg/kg

Sample ID: C10070053-001CMS 07/12/10 14:31Sample Matrix Spike Run: CVAA_C203_100712A

Mercury 96 80 1200.0500.99 mg/kg

Sample ID: C10070053-001CMSD 07/12/10 14:33Sample Matrix Spike Duplicate Run: CVAA_C203_100712A

Mercury 95 80 120 200.050 1.80.97 mg/kg

Sample ID: LCS1-26642 07/12/10 14:58Laboratory Control Sample Run: CVAA_C203_100712A

Mercury 91 80 1200.104.5 mg/kg

Qualifiers:


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Project: Lobelles






Method: SW8015B Batch: 26604

Sample ID: MB-26604 07/08/10 16:57Method Blank Run: FID1-C_100708A2

Diesel Range Organics (DRO) 10ND mg/kg

Surr: o-Terphenyl 86 50 1506.7

Sample ID: LCS-26604 07/08/10 17:42Laboratory Control Sample Run: FID1-C_100708A2

Diesel Range Organics (DRO) 91 60 14010616 mg/kg


Sample ID: LCSD-26604 07/08/10 18:28Laboratory Control Sample Duplicate Run: FID1-C_100708A2



Sample ID: C10070019-002AMS 07/09/10 01:22Sample Matrix Spike Run: FID1-C_100708A2



Sample ID: C10070019-002AMSD 07/09/10 02:08Sample Matrix Spike Duplicate Run: FID1-C_100708A2

Diesel Range Organics (DRO) 82 60 140 2010 11543 mg/kg


Qualifiers:


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Project: Lobelles






Method: SW8270C Batch: B_47451

Sample ID: MB-47451 07/07/10 05:47Method Blank Run: SUB-B15026923

2-Methylnaphthalene 0.33ND mg/kg

Acenaphthene 0.33ND mg/kg

Acenaphthylene 0.33ND mg/kg

Anthracene 0.33ND mg/kg

Benzo(a)anthracene 0.33ND mg/kg

Benzo(a)pyrene 0.33ND mg/kg

Benzo(b)fluoranthene 0.33ND mg/kg

Benzo(g,h,i)perylene 0.33ND mg/kg

Benzo(k)fluoranthene 0.33ND mg/kg

Chrysene 0.33ND mg/kg

Dibenzo(a,h)anthracene 0.33ND mg/kg

Fluoranthene 0.33ND mg/kg

Fluorene 0.33ND mg/kg

Indeno(1,2,3-cd)pyrene 0.33ND mg/kg

Naphthalene 0.33ND mg/kg

Phenanthrene 0.33ND mg/kg

Pyrene 0.33ND mg/kg

Surr: 2,4,6-Tribromophenol 74 65 1240.33

Surr: 2-Fluorobiphenyl 66 67 1020.33 S

Surr: 2-Fluorophenol 66 50 1080.33

Surr: Nitrobenzene-d5 77 62 950.33

Surr: Phenol-d5 72 56 1020.33

Surr: Terphenyl-d14 88 65 1210.33

Sample ID: LCS-47451 07/07/10 06:21Laboratory Control Sample Run: SUB-B15026923

2-Methylnaphthalene 87 49 1010.332.9 mg/kg

Acenaphthene 80 68 950.332.7 mg/kg

Acenaphthylene 78 36 920.332.6 mg/kg

Anthracene 74 67 1090.332.5 mg/kg

Benzo(a)anthracene 95 66 1150.333.2 mg/kg

Benzo(a)pyrene 86 60 1150.332.8 mg/kg

Benzo(b)fluoranthene 77 57 1230.332.6 mg/kg

Benzo(g,h,i)perylene 89 70 1080.333.0 mg/kg

Benzo(k)fluoranthene 75 57 1100.332.5 mg/kg

Chrysene 92 63 1070.333.1 mg/kg

Dibenzo(a,h)anthracene 90 65 1100.333.0 mg/kg

Fluoranthene 90 79 1100.333.0 mg/kg

Fluorene 81 69 980.332.7 mg/kg

Indeno(1,2,3-cd)pyrene 71 57 1260.332.4 mg/kg

Naphthalene 84 56 1000.332.8 mg/kg

Phenanthrene 95 67 1050.333.2 mg/kg

Pyrene 82 70 1060.332.7 mg/kg

Surr: 2,4,6-Tribromophenol 95 65 1240.33

Surr: 2-Fluorobiphenyl 85 67 1020.33

Qualifiers:


S - Spike recovery outside of advisory limits.

of 14

Project: Lobelles







Sample ID: LCS-47451 07/07/10 06:21Laboratory Control Sample Run: SUB-B15026923

Surr: 2-Fluorophenol 74 50 1080.33

Surr: Nitrobenzene-d5 85 62 950.33

Surr: Phenol-d5 83 56 1020.33

Surr: Terphenyl-d14 85 65 1210.33

Sample ID: B10070154-002AMS 07/07/10 07:30Sample Matrix Spike Run: SUB-B15026920

Acenaphthene 55 68 95 4025 027 mg/kg S

Acenaphthylene 51 69 92 4025 025 mg/kg S

Anthracene 43 67 109 4025 021 mg/kg S

Benzo(a)anthracene 71 66 115 4025 036 mg/kg

Benzo(a)pyrene 40 60 115 4025 020 mg/kg S

Benzo(b)fluoranthene 80 57 123 4025 040 mg/kg

Benzo(g,h,i)perylene 57 70 108 4025 028 mg/kg S

Benzo(k)fluoranthene 46 57 110 4025 023 mg/kg S

Chrysene 26 63 107 4025 013 mg/kg S

Dibenzo(a,h)anthracene 49 65 110 4025 025 mg/kg S

Fluoranthene 53 79 110 4025 026 mg/kg S

Fluorene 33 69 98 4025 039 mg/kg S

Indeno(1,2,3-cd)pyrene 74 57 126 4025 037 mg/kg

Pyrene 56 70 106 4025 028 mg/kg S

Surr: 2,4,6-Tribromophenol 47 65 124 4025 0 S

Surr: 2-Fluorobiphenyl 46 67 102 4025 0 S

Surr: 2-Fluorophenol 41 50 108 4025 0 S

Surr: Nitrobenzene-d5 65 62 95 4025 0

Surr: Phenol-d5 40 56 102 4025 0 S

Surr: Terphenyl-d14 51 65 121 4025 0 S


Sample ID: B10070154-002AMSD 07/07/10 08:05Sample Matrix Spike Run: SUB-B15026920

Acenaphthene 56 68 95 4025 2.228 mg/kg S

Acenaphthylene 55 69 92 4025 8.528 mg/kg S

Anthracene 47 67 109 402523 mg/kg S

Benzo(a)anthracene 75 66 115 4025 4.237 mg/kg

Benzo(a)pyrene 49 60 115 402525 mg/kg S

Benzo(b)fluoranthene 86 57 123 4025 7.543 mg/kg

Benzo(g,h,i)perylene 51 70 108 4025 1126 mg/kg S

Benzo(k)fluoranthene 48 57 110 402524 mg/kg S

Chrysene 47 63 107 402524 mg/kg S

Dibenzo(a,h)anthracene 50 65 110 402525 mg/kg S

Fluoranthene 55 79 110 4025 3.527 mg/kg S

Fluorene 36 69 98 4025 341 mg/kg S

Indeno(1,2,3-cd)pyrene 81 57 126 4025 8.240 mg/kg

Pyrene 57 70 106 4025 329 mg/kg S

Surr: 2,4,6-Tribromophenol 48 65 12425 S

Qualifiers:



of 14

Project: Lobelles







Sample ID: B10070154-002AMSD 07/07/10 08:05Sample Matrix Spike Run: SUB-B15026920

Surr: 2-Fluorobiphenyl 47 67 10225 S

Surr: 2-Fluorophenol 39 50 10825 S

Surr: Nitrobenzene-d5 48 62 9525 S

Surr: Phenol-d5 40 56 10225 S

Surr: Terphenyl-d14 52 65 12125 S


Sample ID: B10070154-002AMS 07/07/10 07:30Sample Duplicate Run: SUB-B1502693

2-Methylnaphthalene 4025 12190 mg/kg

Naphthalene 4025 2363 mg/kg

Phenanthrene 4025 1778 mg/kg

Sample ID: B10070154-002AMSD 07/07/10 08:05Sample Duplicate Run: SUB-B1502693

2-Methylnaphthalene 4025 6.8210 mg/kg

Naphthalene 4025 3269 mg/kg

Phenanthrene 4025 1778 mg/kg

Qualifiers:



of 14

Project: Lobelles






Method: SW9045C Batch: 26584

Sample ID: LCS-R134486 07/02/10 09:20Laboratory Control Sample Run: ORION 3 STAR PH_100702A

Corrosivity - pH 99 90 1100.0106.99 s.u.

Sample ID: C10070053-001ADUP 07/02/10 09:20Sample Duplicate Run: ORION 3 STAR PH_100702A

Corrosivity - pH 100.010 2.71.10 s.u.

Qualifiers:


of 14

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